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\\\\\\\\\\\\\\\\\\\\\\\\\\\\\\\\\\\\\\\\\\\\\\\\\\\\\\\\\\\\\\\\\\\\\\\\3.4.5.2 Penentuan Angka Peroksida
(Sudarmadji, 1997)
Ditimbang sebanyak 5 gram minyak goreng hasil penjernihan dan
dimasukkan ke dalam Erlenmeyer kemudian ditambahkan 30 ml larutan asam
asetat 95% - klroroform 97% (3:2), dikocok sampai bahan terlarut semua,
selanjutnya ditambahkan 0,5 larutan KI. Didiamkan selama 1 menit sambil
digoyang, setelah itu ditambahkan 30 ml akuades. Campuran dititrasi dengan 0,1
ml N Na2S2O3 sampai warna kuning hampir hilang, ditambahkan 0,5 ml larutan
pati 1 % dan dititrasi kembali sampai warna biru mulai hilang. Dihitung angka
peroksida yang dinyatakan dalam miliequivalen dari peroksida dalam setiap 1000
g sampel.
3.4.5.3 Analisa Kekeruhan Minyak Goreng dengan Spektronik 20
3.4.5.3.1 Pembuatan Larutan Stok Ba 1000 ppm
Dilarutkan padatan BaCl2 sebanyak 152 mg dengan akuades 50 mL di
dalam beaker glass dan ditambah H2SO4 2M sebanyak 20 mL, kemudian ditetesi
H2SO4 sampai tidak ada endapan. Larutan diencerkan dalam labu ukur 100 mL
sampai tanda batas. Didapat larutan stok Ba 1000 ppm.
Angka Peroksida =
ml.Na2S2O3 x N.thio x 1000
Sampel (g)