Vous êtes sur la page 1sur 138

LAMPIRAN -1

PROSEDUR ANALISA

Universitas Sumatera Utara

LAMPIRAN -1A
PROSEDUR ANALISA WARNA LOVIBOND

1. Tujuan
Metode ini menentukan warna dengan membandingkan cahaya yang dipancarkan
melalui kedalaman tertentu dari lemak, minyak atau asam lemak terhadap warna
cahaya asal dari sumber yang sama, dipancarkan melalui standart.

2. Batasan
Dapat digunakan untuk minyak-minyak hewan, tumbuh-tumbuhan dan asam
lemak

3. Peralatan
3.1. Lovibond Tintometer Model E AF 900
3.2. Lighting cabinet, two 60 watt pearls lamps
3.3. Color racks, consisting of red, yellow, blue, and neutral
Racks with color reading as follow Red : 0.1-0.9; 1.0-9.0; 10.0-70.0
Yellow

: 0.1-0.9; 1.0-9.0; 10.0-70.0

Blue

: 0.1-0.9; 1.0-9.0; 10.0-04.0

Neutral

: 0.1-0.9; 1.0-3.0

3.4. Glass cell, made of optical glass, 1" and 5.25"

4. Bahan-bahan:
None Applicable

Universitas Sumatera Utara

5. Langkah kerja
5.1. Cairkan contoh 100 C diatas titik leleh jika masih padat dan saring jika perlu
untuk menghilangkan pengotor padat
5.2. Tuangkan contoh yang tersedia secukupnya ke dalam sel bersih dan kering
5.3. Tempatkan sel yang mengandung contoh kedalam pemegang sel secara
benar.
5.4. Setelah penutupan ruang sel, segera tentukan warna contoh. Mula-mula
digunakan rak warna kuning 10 terhadap merah 1.
5.5. Atur sampai perbandingan warna yang akurat dicapai, tanpa perlu
mempertahankan ratio 10 kuning terhadap 1 merah dan gunakan angka biru
atau netral yang rendah untuk memperoleh perbandingan, tapi tidak lebih
dari 9.0 biru atau 3.0 netral
5.6. Mencatat ukuran cell dan pembacaan warna merah, kuning, biru atau netral
pada pembentukan perbandingan warna.
5.7. Hasil dinyatakan dalam bentuk seperti dibawah ini :
5.7.1. Pembacaan angka merah, kuning, dan biru atau netral diperlukan
untuk memperoleh perbandingan
5.7.2. Panjang sell yang digunakan
5.8. Pengukuran warna diambil pada satu panjang sel tidak boleh dipakai untuk
menghitung nilai warna untuk panjang sell yang lain.
5.9. Sebaiknya ketajaman (kejelasan) warna tidak pernah lebih besar dari 20 total
lovibond color
6. Rujukan
AOCS Ce 13e-92

Universitas Sumatera Utara

LAMPIRAN -1B
PROSEDUR PEMBUATAN METYL ESTER ASAM LEMAK.

1. Tujuan
Metil ester dari asam lemak dan minyak dipisahkan dan ditentukan secara
kuantitatif dengan GLC menggunakan packed column tertentu atau asam lemak
langsung dipisah dan ditentukan secara kuantitatif dengan GLC menggunakan
capillary column tertentu.

2. Batasan
Metode ini berlaku untuk asam lemak dan minyak nabati yang mempunyai atom
karbon 6 sampai 20 setelah dirubah menjadi ester untuk packed atau langsung
asam lemak untuk capillary column.

3. Peralatan
3.1. Analytical balance
3.2. Block heater
3.3. Thermometer
3.4. Screw vial, 5 ml

4. Bahan-bahan
4.1. BF 3 = methanol solution, reagent grade
4.2. Sodium chlorida saturated solution
4.3. Solvent, n-hexane, reagent grade
4.4. Methanol, reagent grade
Universitas Sumatera Utara

4.5. NaOH 0.5 N in methanol


Larutkan 20 +0.05 g, reagent grade NaOH dalam 1 L metanol

5. Langkah kerja
5.1. Determination carbon chain for fats and oils
5.1.1

Timbang sampel sekitar 0.02 gram kedalam vial 5 ml yang tertutup

5.1.2

Tambahkan 2 ml 0.05N NaOH metanol, dan panaskan didalam blok


pemanas pada suhu yang diatur 68+ 10C selama 10 menit.

5.1.3

Tambahkan 2 ml larutan reagen BF 3 metanol, dan panaskan didalam


blok pemanas pada suhu yang diatur 68+ 10C selama 15 menit

5.1.4

Keluarkan dari blok pemanas dan didinginkan pada suhu ruangan

5.1.5

Tambahkan 2 ml heksan dan 1 ml larutan NaCl jenuh, kocok dan


biarkan selama 1 menit, sekarang larutan heksan siap di injeksikan.

5.2. Determination carbon chain ini pack column


5.2.1. Timbang sampel sekitar 0.02 ml gram kedalam vial 5 ml yang
tertutup.
5.2.2. Tambahkan 2 ml larutkan reagen BF 3 metanol, dan panaskan didalam
blok pemanas pada suhu yang diatur 68 + 10C selama 15 menit
5.2.3. Keluarkan dari blok pemanas dan dinginkan pada suhu ruangan.
5.2.4. Tambahkan 2 ml heksan dan 1 ml larutan NaCl jenuh, kocok dan
biarkan selama 2 menit, sekarang larutan heksan siap untuk di
injeksikan.
5.3. Determination carbon chain ini capillary column
5.3.1. Timbang sampel sekitar 0.02 gram kedalam vial 5 ml yang tertutup
5.3.2. Tambahkan 2 ml heksan dan kocok, jika sampel tidak larut panaskan
beberapa menit untuk melarutkannya.
5.3.3. Sekarang larutan heksan siap untuk di injeksikan.

6. Rujukan
AOCS CE2-66

Universitas Sumatera Utara

LAMPIRAN -1C.
PROSEDUR ANALISA KOMPOSISI ASAM LEMAK

1. Tujuan
Metil ester dari asam lemak dipisahkan dan ditentukan secara kuantitatif dengan
GLC menggunakan packed colomn tertentu asam lemak langsung dipisah dan
ditentukan secara kuantitatif dengan GLC menggunakan capillary coloumn
tertentu.

2. Batasan
Metode ini berlaku untuk asam lemak dan minyak nabati yang mempunyai atom
karbon 6 sampai 20 setelah dirubah menjadi metil ester untuk packed column
atau langsung asam lemak untuk capillary column.

3. Peralatan
3.1. Syringe, 10 1
3.2. Shimadzu Gas chromatograph, GC-14B
3.2.1. Injector Insert glass type, splitless mode
3.2.2. Detector Flame Ionization detector, range 102
3.2.3. Columns
For methyl esters of fatty acid- GP 10% SP 216 PS on 100/120
Supelcoport.
Supelco Cat. No. 1-1879, square Loop
Universitas Sumatera Utara

For fatty acids :


-

HP-FFAP, Cross linked polyethylene glycol-TPA phase


15 m x 0.53 mm x 1.0 m, Hawlett Packard Part No. 19095F 123

Coloum Glass, 20% DEGS Chromosorb WHP on 60/80


Temp. Max 2000C, P/N 221-14368-31/7G (3.2-3.1), Lenght 3 M

Coloum Stainless, GP 10% SP-216-PS on 100/120 Supelcoport


Temp. Max 2000C, Lenght 2 M

Flow rate of Gas :


Gases
Packed Kpa
Nitrogen
90
Hydrogen
60
Air
50
Temperature
Programs Injector, 0C
Detector0C
Samples
Column, 0C
Initial temp, 0C
Initial time, min.
Program rate, 0C/min
Final temp. 0C
Final time, min

Capilllary KPa
40
55
30

Packed
220
230
CPO
C 12 PKO
RBD PS
C 18
120
140
100
0
0
0
10
10
10
190
190
190
15
15
15

Capillary
230
250
C 8 -C 10
C 8, C 18

C 16 -C 18
170
0
10
190
8

100
0
10
230
5

3.3. Recording system, Chromatopac C-R6A


Attenuation, mV/full scale

Width

Slope, V/min

70 max

Drift

Minimum Area, Count

1000 max

TDBL

Chart speed, mm/min

3.4. Screw cap vial, 5 ml


3.5. Analytical balance, 0.0001 g accuracy

4. Bahan-bahan
4.1. Solvent,n-hexane, reagent grade
Universitas Sumatera Utara

4.2. Carries gas, nitrogen with ultra high purity (UHP)


4.3. Hydrogen, Ultra high purity
4.4. Air, industrial grade, free from oil and moisture

5. Langkah Kerja
5.1. Preparation sample
5.1.1. Methyl ester
5.1.1.1.Penyediaan metil ester merujuk pada lampiran 6
5.1.2. Fatty Acid
5.1.2.1.Timbang sampel sekitar 0.02 gram kedalam vial 5 ml yang
bertutup.
5.1.2.2.Tambahkan 2 ml heksan dan kocok, jika sampel tidak larut
panaskan beberapa menit untuk melarutkannya.
5.2. Prosedur
5.2.1. Pilih keadaan yang optimal dari sistem GC dan file Chromatopact
untuk sampel yang tepat
5.2.2. Dengan menggunakan, injeksikan 1 kedalam kolom, dan start GC.
5.2.3. Identifikasikan puncak-puncak dari kromatogram, menggunakan
kromatogram standar sebagai petunjuk.
5.3. Perhitungan
ACi x FCi x 100
Calculation : % Ci = Sum (FCi x ACi

Dimana

% Ci

= Kandungan rantai karbon i dalam % berat

ACi

= Area rantai karbon i

FCi

= Faktor respons rantai karbon i

Sum (ACixFCi) = jumlah dari FCi x Aci

6. Rujukan
6.1. User Manual, Shimadzu Chromatopac C R6A & C-R8A
6.2. User Manual, Shimadzu Chromatograph GC 14B
Universitas Sumatera Utara

7. Informasi-informasi lain yang dibutuhkan


1.1. Packed column hanya sesuai untuk metil ester
1.2. HP-FFAP untuk C8C10 Fatty Acid

LAMPIRAN -1D
PEMBUATAN LARUTAN STANDAR NATRIUM TIOSULFAT (NA 2 S 2 O 3 )
1. Tujuan
Cara ini menunjukkan pembuatan dan membakukan larutan natrium tiosulfat
secara kuantitatif.

2. Batasan
Hanya dapat digunalan untuk larutan Natrium Thiosulfat

3. Peralatan
3.1. Analytical balance, 0.0001 g accuracy
3.2. Burrete, accurately calibrate 50 ml
3.3. Cylinder glass, 25 ml, 100 ml
3.4. Reagent bottle, 5000 ml
3.5. Volumetric pipette, 5 ml
3.6. Erlenmeyer flask, 300 ml
3.7. Volumetric dispenser 20 ml

4. Bahan-bahan
4.1. CO 2 free distilled water

Universitas Sumatera Utara

Didihkan air suling selama 20 menit dan dinginkan dengan penutup untuk
mencegah penyerapan CO 2 .
4.2. Potasium Iodium solution, 15%
Larutkan 150 gram Kalium Iodium ke dalam 1000 ml air suling
4.3. Starch Indicator, 1%
Larutkan 1 gram serbuk starch ke dalam 100 ml air suling yang panas dan
dinginkan.
4.4. Standart primer kalium dikromat 0.1 N
4.5. Larutkan 2.4518 gram yang telah dikeringkan dan dinginkan dalam labu ukur
500 ml dengan air destilat dan terakan sampai tanda batas dan simpan dalam
botol gelap.
5. Langkah Kerja
5.1. Preparation of Sodium solution, 0.1N & 0.01N
Larutkan dalam 124,5 + 0.1 gr Natrium thisulfat ke dalam air suling dan
larutkan hingga 5 L.
5.2. Sodium Thiosulfate Standardization 0.1N
Pipet 25 ml larutan kalium dichromat ke dalam erlenmeyer 300 ml,
tambahkan 5 ml asam klorida pekat, 20 ml larutan kalium iodida dan aduk.
Diamkan selama 5 menit, dan kemudian tambahkan 100 ml air suling. Titrasi
dengan larutan natrium thiosulfat, aduk sampai warna kuning pucat.
Tambahkan 1-2 ml indikator starch dan lanjutkan titrasi secara perlahan
hingga warna biru benar benar tak kelihatan.
5.3. Sodium Thiosulfat Standardization
5.4. Encerkan 100 ml larutan N 2 S 2 O 3 0,1N ke dalam 1000 ml labu ukur dengan
air destillat dan terakan sampai tanda batas.
Untuk standarisasi, pipet 2 ml larutan kalium dichromat ke dalam erlenmeyer
300 ml . Tambahkan 5 ml asam klorida pekat, 20 ml larutan kalium iodium
dan aduk. Diamkan selama 5 menit, dan kemudian tambahkan 100 ml air
suling. Titrasi dengan larutan natrium thiosulfat, aduk sampai warna kuning
pucat. Tambahkan 1-2 ml indikator starch dan lanjutkan titrasi secara
perlahan hingga warna biru benar-benar tak kelihatan.
5.5. Perhitungan
Universitas Sumatera Utara

20.394 x wt of K 2 Cr 2 O 7 x fp
ml of Na 2 S 2 O 3
Normality of Na 2 SO 2 O 3 =

6. Rujukan
AOCS Official Method Tg 1-64.

LAMPIRAN -1E
PEMBUATAN LARUTAN STANDAR WIJS

1. Tujuan
Prosedur ini menggambarkan pembuatan larutan wijs dari iodine monochlorida

2. Batasan
Cara ini hanya digunakan untuk membuat larutan wijs dari iodine monochlorida
komersil.

3. Peralatan
3.1. Cylinder glass, 100, 1000 ml
3.2. Erlenmeyer flask, 500 ml
3.3. Filter paper
3.4. Magnetic stirrer
3.5. Reagent bottle, 5000 ml, amber
3.6. Volumentric pippete, 10 ml

4. Bahan-bahan
4.1. Acetic acid glacial
Universitas Sumatera Utara

4.2. Distilled water


4.3. Iodine monochloride
4.4. Potasium Iodida Solution, 15%
4.5. Cyclo hexane
4.6. Starch indikator
4.7. Sodium thiodulfate solution, 0.1N
4.8. Sulfuric acid, 2%

5. Langkah kerja
5.1. Stock solution :
Tambahkan 317 +0.1 g iodine monochloride ke 1 L asam asetat glasial, aduk
hingga larut selanjutnya saring dengan kertas saring whatman 41H atau
sejenisnya ke botol yang bersih dan kering. Saring dengan segera untuk
mencegah terjadinya kontaminasi terhadap air dan simpan di tempat yang
sejuk. Buang larutan bila terbentuk endapan.
5.2. Wijs Solution :
Dengan menggunakan glas ukur tuangkan 117.0 + 0.1 ml larutan stock ke
botol 5 L yang telah terisi asam asetat, kemudian aduk hingga merata.
5.3. Wijs standardization
Menentukan perbandingan I/Cl yang mana harus dalam batas 1.10 + 0.1
seperti prosedur berikut :
5.3.1. Iodine content :
Tuangkan 150 ml larutan chroline jenuh ke dalam erlenmeyer 500 ml,
dan tambahkan beberapa butir butiran kaca.
5.3.2. Pipet 5 ml larutan wijs ke dalam larutan erlenmeyer yang telah berisi
chlorine jenuh, aduk dan panaskan hingga mendidih.
5.3.3. Didihkan dengan cepat selama 10 menit, dinginkan dan tambahkan 30
ml asam sulfat 2% dan 15 ml larutan iodida.
5.3.4. Aduk dengan baik dan segera titrasi dengan larutan natrium thiosulfat
0.1N dengan starch sebagai indikator.
5.4. Total Halogen Content
5.4.1. Tuangkan 150 ml air destillat yang baru mendidih ke erlenmeyer 500
ml yang bersih dan kering.
Universitas Sumatera Utara

5.4.2. Tambahkan 15 ml larutan kalium iodida 15%


5.4.3. Pipet 20 ml larutan Wijs ke dalam erlenmeyer tersebut, aduk hingga
homogen
5.4.4. Titrasi dengan natrium tiosulfat 0.2N dengan starch sebagai indikator.
5.5. Perhitungan :
Halogen ratio :
Dimana :

2A
3B 2A

A = Volumen natrium thiosulfat untuk menitrasi kandungan


iodine
B = Volume natrium thiosulfat untuk menitrasi kandungan
halogen total.

6. Rujukan
AOCS Official Method Tg 1-64

Universitas Sumatera Utara

LAMPIRAN -1F
PROSEDUR ANALISA BILANGAN IODIUM

1. Tujuan
Bilangan iodine adalah suatu ukuran ketidakjenuhan dari minyak industri dan
turunnya dan dinyatakan dalamistilah gram iodin terserap setiap 100 gram contoh
(% iodine terserap).

2. Batasan
Dapat digunakan untuk minyak-minyak industri dan turunnya, seperti minyak
kering alami atau buatan dan asam lemaknya.

3. Peralatan
3.1. Analytical balance, accurate up to 0.0001 gr
3.2. Burrete or Automatic piston burrete with stirrer, 50 ml
3.3. Erlenmeyer flask with stopper, 250 to 300 ml
3.4. Volumetric dispenser, 30 ml, 1 ml adjustabilty
3.5. Volumetric pippete, 15,25 ml
3.6. Graduate cylinder, 100 ml

4. Bahan-bahan
4.1. Sodium Thiosulfate Solution. 0,1N
Merujuk ke pada lampiran 8
4.2. Wijs Solution
Merujuk pada lampiran 9
4.3. Pottasium Iodida Solution, 15%
Larutkan 150 g kalium Iodida dalam 1000 ml air demin
4.4. Starch indicator solution
Buat pasta 1 gram starch dengan sedikit air dingin. Tambahkan sambil
diaduk dengan 100 ml air mendidih.
4.5. Sikloheksana sebagai pengganti karbon tetraklorida seperti rekomendasi

Universitas Sumatera Utara

5. Langkah Kerja
5.1. Cairkan sampel jika masih padat dan timbang seperti berikut ini : (catatan 7).
Sample
Caprylic, Capric Aicd,
Lauric Acid, Myristic
Acid, TPSA,
Hydrogenated, TPSA,
DPSA, RGSA, Stearic
65%

Weight,g

5 + 0.5

Sample

Weight,g

CPKO, SPKOFA

0.70-1.00

RBDPS, SRBDPSFA

0.40-0.60

CPS, SCPSA and Oleic Acid

0.30-0.50

CPO, SPOFA

0.10-0.20

5.2. Tambahkan 10 ml Sikloheksana, pipet 15 ml larutan Wijs dalam labu yang


mengandung contoh dan aduk dengan baik
5.3. Buat dan lakukan penentuan blanko sekaligus sama dengan contoh.
5.4. Simpan labu-labu di dalam tempat gelap selama 30 menit pada suhu 25 + 50C
5.5. Pindahkan labu ke penyimpanan, tambahkan 10 ml larutan Kl, 100 ml air
suling.
5.6. Titrasi dengan larutan 0.1N Na 2 S 2 O 3 , penambahannya secara bertahap dan
dengan pengadukan yang kuat dan tetap sampai warna kuning hampir
lenyap. Tambahkan 1-2 larutan indikator kanji dan lanjutkan titrasi sampai
warna biru lenyap seketika.
5.7. Perhitungan :
Iodine value, gI 2 /100g
Where :

( Vb Vs) x N x 12.69
=
W

Vb

= ml Na 2 S 2 O 3 0.1 dipakai pada titrasi blanko

Vs

= ml Na 2 S 2 O 3 0.1 dipakai pada titrasi contoh

= Normalitas Na 2 S 2 O 3

= Gram contoh

6. Rujukan
AOCS Official Method Tg 1-64

7. Informasi-informasi lain yang dibutuhkan


7.1. Larutan Wijs harus lebih 100-150% terhadap jumlah terserap
Universitas Sumatera Utara

7.2. Untuk Oleic acid, menggunakan 25 ml larutan Wijs, 20 ml Cyclohexane dan


20 ml larutan Kl 15%
LAMPIRAN -1G
PROSEDUR ANALISA HEAT STABILITY

1. Tujuan
Metode ini mengukur stabilitas warna dari asam lemak (fatty acid) setelah
pemanasan dalam kondisi analisa khusus.

2. Batasan
Berlaku untuk semua fatty acid normal

3. Peralatan
Oil batch
Mixer
Thermometer
Tubes Thermal Resistance
Filter paper
Colorimeter

4. Bahan-bahan
4.1. Sulfuric Acid (corrosive material)

5. Langkah Kerja
5.1. Pembuatan larutan khusus Asam sulfat 1 : 1
Masukkan 1 bagian asam sulfat ke dalam 1 bagian air dengan hati hati,
jangan
sampai terbalik.
5.2. Perlakuan Sampel
Jika sampel yang diuji tidak cair pada suhu ruangan, cairkan dengan
pemanasan
di water batch sampai suhu tidak lebih dari 10 oC di atas titer sampel.
Universitas Sumatera Utara

5.3. Perlakuan Peralatan


5.3.1. Pastikan sebelum oil batch digunakan, sudah diverifikasi dahulu suhunya
dengan menggunakan thermometer standar.
5.3.2.

Tabung harus dicuci bersih dengan asam sulfat (1:1), kemudian dibilas
dengan air distillat dan dikeringkan.

5.4. Cara Kerja


5.4.1. Set wadah minyak ke suhu 205 + 2 oC dan jaga suhu dalam kisaran khusus
ini.
5.4.2. Isi tabung yang bersih dan kering hingga kedalaman 12.7 cm dengan
sampel dan masukkan dalam wadah minyak.
5.4.3. Atur volume di dalam wadah minyak hingga ketinggian 14 cm dari bagian
bawah gelas tabung. Bila meletakkan beberapa tabung gelas di dalam oil
batch, suhunya tidak turun lebih dari 5 oC di bawah suhu minimum oil
batch dan waktu untuk menaikkan suhu menjadi 205 oC tidak lebih dari 5
menit.
5.4.4. Atur waktu 60 menit untuk samplel yang memiliki bilangan iodium di atas
15 atau atur 120 menit jika sampel memiliki bilangan iodium lebih kecil
atau sama dengan 15.
5.4.5. Pindahkan tabung dari oil batch dan lihat warna menggunakan AOCS
official Method Td 1a - 65 atau Lovibond Color.

6. Rujukan
AOCS Official Method Td 3a-64

7. Informasi-informasi lain yang dibutuhkan


Kebersihan glassware sangat penting. Metode yang disarankan dibersihkan
dengan detergent dan dibilas dengan asam sulfat. Larutan dikromat jangan
dilakukan.

Universitas Sumatera Utara

LAMPIRAN -2A
Tabel L1. Mutu Umpan Hidrogenated Splitted Crude Stearic Acid
(HSRBDPSFA).

No

Item Analisa

Color 51/4, R/Y

Komposisi (% berat):

Bilangan Iodium (IV) Umpan, g /


100 g
0,7
0,6

5,8/44,4

4,9/42,1

Asam laurat, C 12

0,1

0,1

Asam miristat, C 14

1,3

1,3

Asam palmitat, C 16

59,5

56,8

Asam stearat, C 18

38.6

41,3

Asam oleat, C 18-1

Asam linoleat, C 18-2

Asam arachidat, C 20

0,4

0,4

Unknown, Unk

0,1

0,1

Sumber : PT. Flora Sawita Chemindo, 2008

Universitas Sumatera Utara

LAMPIRAN -2B
Tabel L2. Hasil Perhitungan Nilai Rata-rata Warna Distillat Asam Stearat Berbasis
RBDPS.

No

Kecepatan

Bilangan

Alir

Iodium (IV)

Umpan,

Umpan,

ton/jam

g/ 100 g
0,7

5,5

0,6

0,7

5,75

0,6

0,7

6,00

0,6

Warna R DAS
Suhu Bottom
MD,
C0

Warna Y DAS

R
R-1

R-2

Rata -

Y
Y-1

Y-2

rata

Rata
- rata

218

0,1

0,1

0,1

0,7

0,7

0,7

220

0,1

0,1

0,1

0,7

0,7

0,7

222

0,1

0,1

0,1

0,7

0,7

0,7

218

0,1

0,1

0,1

0,7

0,7

0,7

220

0,1

0,1

0,1

0,7

0,7

0,7

222

0,1

0,1

0,1

0,7

0,7

0,7

218

0,1

0,1

0,1

0,7

0,7

0,7

220

0,1

0,1

0,1

0,7

0,7

0,7

222

0,1

0,1

0,1

0,7

0,7

0,7

218

0,1

0,1

0,1

0,7

0,7

0,7

220

0,1

0,1

0,1

0,7

0,7

0,7

222

0,1

0,1

0,1

0,7

0,7

0,7

218

0,1

0,1

0,1

0,7

0,7

0,7

220

0,1

0,1

0,1

0,7

0,7

0,7

222

0,1

0,1

0,1

0,7

0,7

0,7

218

0,1

0,1

0,1

0,7

0,7

0,7

220

0,1

0,1

0,1

0,7

0,7

0,7

222

0,1

0,1

0,1

0,7

0,7

0,7

Keterangan : R = Red ; Y = Yellow ; R = harga rata rata R-1 dan R-2; Y Rata rata
= harga rata rata Y-1 dan Y-2 sesuai simbol Warna Lovibond

Universitas Sumatera Utara

234

LAMPIRAN -2C
Tabel L3. Rata-rata Heat Stability dan Produksi Fraksi Ringan dan Distillat Asam
Stearat (DAS) dari RBDPS.
Kecepatan
No

Alir
Umpan,
(ton/jam)

Bilangan
Iodium
(IV)
Umpan,
g/100 g

0,7
1

0,7

H/S - 2

H/S

LE

DAS

kg/jam

kg/jam

MD,
C0

218

0,4

3,8

0,4

4,1

0,40

3,95

82,73

4923,75

220

0,4

4,8

0,5

5,2

0,45

5.00

93,25

4937,25

222

0,5

5,4

0,5

5,8

0,50

5,60

98,55

4967,51

218

0,3

3,7

0.3

3,8

0,30

3,75

95,125

4925,05

220

0,3

4,8

0,4

5,0

0,35

4,90

95,58

4936,85

222

0,4

5,2

0,4

5,3

0,40

5,25

91,40

4949,8

218

0,4

3,9

0,5

4,0

0,45

3,95

86,25

5146,00

220

0,5

4,9

0,5

5,3

0,50

5,10

98,33

5161,50

222

0,6

5,4

0,5

5,8

0,55

5,60

102,93

5194,00

218

0,4

4,0

0,4

3,8

0,40

3,95

99,30

5150,00

220

0,4

4,9

0,5

5,1

0,45

5,00

100,06

5161,25

222

0,5

5,3

0,5

5,4

0,50

5,35

100,65

5196,00

218

0,5

4,0

0,5

4,2

0,50

4,10

90,30

5370,60

220

0,6

5,0

0,6

5,3

0,55

5,15

99,60

5385,90

222

0,6

5,8

0,6

6.0

0,60

5,90

83,70

5435.65

218

0,5

4,0

0,4

4,1

0,45

4,05

103,20

5377,20

220

0,5

4,9

0,5

5,2

0,50

5,05

103,80

5386,30

222

0,6

5,4

0,5

5,5

0,55

5,45

105,30

5444,70

5,75
0,6

0,7
3

H/S 1

Bottom

5,50
0,6

Suhu

6,00
0,6

Keterangan : H/S = heat stability ; R = red ; Y = yellow ; H/S = heat stability rata rata.

Universitas Sumatera Utara

LAMPIRAN -2D
Tabel L4. Hasil Perhitungan Rata - rata Respon Yield Destillat LE, AS dan Residue serta Distillat -2.

Kec. Alir
No

Umpan,
ton/jam

Yield Fraksi Ringan (LE)


IV Umpan,
g/ 100 g

0,7

5,50

0,6

0,7

5,75

0,6

0,7

6,00

0,6

Yield Distillat Asam Stearat

Yield Residue

Yield Dist -2

Suhu B MD
0

LE-1

LE-2

LE

DAS-1

DAS-2

DAS

Res-1

Res-2

Res

(Dest-2)-1

(Dist-2)-2

Dist-2

kg/jam

kg/jam

kg/jam

kg/jam

kg/jam

kg/jam

kg/jam

kg/jam

kg/jam

kg/jam

kg/jam

kg/jam

218

96,750

94,00

95,375

4922,50

4925,,00

4923.75

283,00

285,00

284,00

198,52

196,00

197,26

220

95,150

96,10

95,625

4936,50

4938,00

4937,25

280,00

281,00

280,50

188,85

184,90

186.75

222

99,00

98,00

98,500

4965,015

4970,00

4967,51

277,00

278,00

277,50

158,99

154,00

156,49

218

82,50

83,00

82,750

4924,00

4926,10

4925,05

280,60

277,00

278,80

212,90

214,90

213,90

220

93,50

93,00

93,250

4937,50

4936,20

4936,85

275,50

276,00

275,75

194,00

194,80

194.40

222

95,40

97,10

96,250

4970,50

4969,10

4969,80

274,00

275,00

274,50

160,10

158,80

159,45

218

100,80

97,80

99,300

5143,40

5148,60

5146,00

297,30

299,40

298,35

208,50

204,20

206,35

220

99,48

100,63

100,055

5161,20

5161,80

5161,50

292,67

293,00

292,835

196,65

194,57

195,70

222

102,35

103,50

102,925

5192,30

5195,70

5194,00

287,50

289,80

288,50

167,85

161,00

164,425

218

85,70

86,80

86,250

5148,00

5152,00

5150,00

293,30

291,50

292,40

223,00

219,70

221,35

220

94,88

97,17

96,025

5161,78

5160,63

5161,25

288,50

288,80

288,65

204,84

203,40

204,12

222

100,10

101,20

110,150

5196,30

5195,70

5196,00

284,05

286,35

285,20

169,55

166,75

168,15

218

105,00

101,40

103,200

5368,20

5373,00

5370,60

308,00

309,00

308,50

218,80

216,60

217,70

220

103,20

104,44

103,800

5385,60

5386,20

5385,90

304,20

305,40

304,80

207,80

204,00

205,90

222

107,40

109,20

108,300

5435,10

5436,20

5435.65

301,20

302,40

301,80

156,30

152,20

154,25

218

90,15

90,60

90,375

5372,40

5382,00

5377,20

303,00

302,5

302,75

234,60

225,40

230,00

220

98,40

100,80

99,600

5385,00

5388,00

5386,30

300,60

301,80

301,20

216,00

209,40

212,70

222

104,40

106,20

105,300

5444,20

5445,20

5444,70

297,00

298,20

297,60

152,60

152,20

152,40

Universitas Sumatera Utara

LAMPIRAN -2E
Tabel L5. Hasil Perhitungan Rata-rata Bilangan Iodium (IV) Distillat Asam
Stearat Berbasis RBDPS.
Kecepatan
No

Alir Umpan,
ton/jam

Bilangan
Iodium (IV)
Umpan,
g/ 100 g
0,7

5,5
0,6

0,7
2

5,75
0,6

0,7
3

6,00
0,6

Bilangan Iodium (IV) DAS

Suhu

IV Rata -

Bottom MD,

IV 1

IV 2

C0

gr/100 gr

gr/100 gr

218

0.15

0,15

0.150

220

0.15

0,17

0.160

222

0,17

0,17

0,170

218

0.14

0,15

0.145

220

0,16

0.15

0.155

222

0,16

0.16

0.160

218

0.16

0,16

0.160

220

0,17

0,17

0,170

222

0,17

0,17

0,170

218

0,16

0,15

0.155

220

0.16

0,17

0.165

222

0,17

0.16

0.165

218

0,16

0.17

0.165

220

0.18

0,17

0.175

222

0,18

0,18

0,180

218

0,16

0.16

0,160

220

0,17

0.17

0,170

222

0,18

0.17

0.175

rata
gr/100 gr

Universitas Sumatera Utara

LAMPIRAN -2F
Tabel L6. Hasil Perhitungan Rata - Rata Bilangan Asam Residue Berbasis
RBDPS.
Kecepatan Alir
No

Umpan,
ton/jam

Bilangan
Iodium (IV)
Umpan,
100 g

0,7
1

5,5
0,6

0,7
2

5,75
0,6

0,7
3

6,00
0,6

g/

Bilangan Asam (AV) Residue

Suhu
Bottom MD,

AV 1,

AV 2,

AV Rata - rata,

218

33,5

36,5

35,00

220

25,8

28,0

26,90

222

25,5

27,5

26,50

218

28,3

27,8

28,05

220

23,9

24,5

24,20

222

23,6

25,1

24,30

218

33,6

36,4

35,00

220

26,0

27,6

26,80

222

25,0

27,5

26,25

218

28,5

27,8

28,15

220

24,5

24,8

24,65

222

24,0

24,8

24,40

218

34,0

37,0

35,50

220

26,5

27,5

27,00

222

25,8

27,8

26,80

218

28,2

28,0

28,10

220

25,0

24.5

24.75

222

23,80

24,6

24,20

C0

Keterangan : AV = Acid Value (Bilangan Asam) dalam mg KOH/gram

Universitas Sumatera Utara

LAMPIRAN -2G
Tabel L7. Perbandingan Mutu Distillat Asam Stearat (berbasis RBDPS) Hasil
Optimasi
Mutu DAS
Sebelum
Optimasi (*)
0,10,2R/0,70,9Y

Mutu DAS
Sesudah
Optimasi

0,5-0,8R/67,5Y

0,55R/5,45
Y

0,15 - 0,24

0,175

total
keduanya
1,0 %
maks

< 1,0

total
keduanya
0,30 %
maks

C 16 , asam palmitat

56 - 63

In specs

59,00

C 18 , asam stearat

37 42

Sering <
37.0

40,25

< 1,0

total
keduanya
0,45 %

No

Parameter Mutu

Warna (Colour) 5 ,
Lovibond

Heat Stability (H/S)5 ,


Lovibond

Bilangan Iodium (IV), gr/100


gr

Komposisi, % berat :
C 12 , asam laurat
C 14 , asam miristat

C 20 , asam arachidat
Unk

Standar
Mutu
DAS
0,1R/
0,8Y maks
0,6
R/6,0Y
maks
0,20 maks

total
keduanya
1,0 %
maks

0.1/0.7

Universitas Sumatera Utara

LAMPIRAN 3A
General Linear Model: Yield AS versus F Umpan, IV Umpan, Suhu B MD
Factor
F Umpan
IV Umpan
Suhu B MD

Type
fixed
fixed
fixed

Levels
3
2
3

Values
5.50, 5.75, 6.00
0.6, 0.7
218, 220, 222

Analysis of Variance for Yield AS, using Adjusted SS for Tests


Source
P
F Umpan
0.000
IV Umpan
0.004
Suhu B MD
0.000
F Umpan*IV Umpan
0.105
F Umpan*Suhu B MD
0.000
IV Umpan*Suhu B MD
0.081
F Umpan*IV Umpan*Suhu B MD
0.681
Error
Total

S = 2.49864

R-Sq = 99.99%

DF

Seq SS

Adj SS

Adj MS

1251684

1251684

625842

100243.94

70

70

70

11.25

17999

17999

9000

1441.52

32

32

16

2.56

793

793

198

31.74

36

36

18

2.90

14

14

0.58

18
35

112
1270741

112

R-Sq(adj) = 99.98%

Unusual Observations for Yield AS


Obs
31
32

Yield AS
5372.40
5382.00

Fit
5377.20
5377.20

SE Fit
1.77
1.77

Residual
-4.80
4.80

St Resid
-2.72 R
2.72 R

R denotes an observation with a large standardized residual.

Universitas Sumatera Utara

LAMPIRAN -3B
One-way ANOVA: Yield AS_0.6 versus F Umpan_0.6
Source
F Umpan_0.6
Error
Total
S = 25.65

Level
5.50
5.75
6.00

N
6
6
6

DF
2
15
17

SS
631841
9870
641711

MS
315920
658

R-Sq = 98.46%

Mean
4943.9
5169.1
5402.8

StDev
20.8
21.5
32.9

F
480.10

P
0.000

R-Sq(adj) = 98.26%

Individual 95% CIs For Mean Based on


Pooled StDev
--+---------+---------+---------+------(-*)
(-*)
(*-)
--+---------+---------+---------+------4950
5100
5250
5400

Pooled StDev = 25.7

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of F Umpan_0.6
Simultaneous confidence level = 88.31%

F Umpan_0.6 = 5.50 subtracted from:


F Umpan_0.6
5.75
6.00

Lower
193.60
427.33

Center
225.17
458.90

Upper
256.74
490.47

---+---------+---------+---------+-----(*-)
(-*-)
---+---------+---------+---------+------200
0
200
400

F Umpan_0.6 = 5.75 subtracted from:


F Umpan_0.6
6.00

Lower
202.16

Center
233.73

Upper
265.30

---+---------+---------+---------+-----(-*)
---+---------+---------+---------+------200
0
200
400

Universitas Sumatera Utara

LAMPIRAN -3C
MTB > Oneway 'Yield AS_0.7' 'F Umpan_0.7';
SUBC>
Fisher 5.

One-way ANOVA: Yield AS_0.7 versus F Umpan_0.7


Source
F Umpan_0.7
Error
Total
S = 24.61

Level
5.50
5.75
6.00

N
6
6
6

DF
2
15
17

SS
619875
9085
628960

MS
309937
606

R-Sq = 98.56%

Mean
4942.8
5167.2
5397.4

StDev
20.1
22.0
30.5

F
511.75

P
0.000

R-Sq(adj) = 98.36%

Individual 95% CIs For Mean Based on


Pooled StDev
--+---------+---------+---------+------(-*)
(*-)
(-*)
--+---------+---------+---------+------4950
5100
5250
5400

Pooled StDev = 24.6

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of F Umpan_0.7
Simultaneous confidence level = 88.31%

F Umpan_0.7 = 5.50 subtracted from:


F Umpan_0.7
---5.75
6.00
*)

Lower

Center

Upper

194.05
424.26

224.33
454.55

254.62
484.83

---+---------+---------+---------+-(*-)
(---+---------+---------+---------+--

----200

200

400

F Umpan_0.7 = 5.75 subtracted from:


F Umpan_0.7
---6.00

Lower

Center

Upper

199.93

230.21

260.50

---+---------+---------+---------+-(-*)

Universitas Sumatera Utara

---+---------+---------+---------+-----200

200

400

LAMPIRAN -3D
One-way ANOVA: Yield AS_5.50 versus IV Umpan_5.50
Source
IV Umpan_5.50
Error
Total
S = 20.45

Level
0.6
0.7

N
6
6

DF
1
10
11

SS
3
4181
4184

MS
3
418

R-Sq = 0.08%

Mean
4943.9
4942.8

StDev
20.8
20.1

F
0.01

P
0.930

R-Sq(adj) = 0.00%

Individual 95% CIs For Mean Based on


Pooled StDev
------+---------+---------+---------+--(------------------*-----------------)
(------------------*-----------------)
------+---------+---------+---------+--4930
4940
4950
4960

Pooled StDev = 20.4

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of IV Umpan_5.50
Simultaneous confidence level = 95.00%

IV Umpan_5.50 = 0.6 subtracted from:


IV Umpan_5.50
---+0.7
)

Lower

Center

Upper

--------+---------+---------+------

-27.37

-1.06

25.24

(----------------*------------------------+---------+---------+------

---+-15

15

30

Universitas Sumatera Utara

LAMPIRAN -3E
One-way ANOVA: Yield AS_5.75 versus IV Umpan_5.75
Source
IV Umpan_5.75
Error
Total
S = 21.75

Level
0.6
0.7

N
6
6

DF
1
10
11

SS
11
4731
4741

R-Sq = 0.23%

Mean
5169.1
5167.2

StDev
21.5
22.0

MS
11
473

F
0.02

P
0.883

R-Sq(adj) = 0.00%

Individual 95% CIs For Mean Based on


Pooled StDev
-+---------+---------+---------+-------(----------------*---------------)
(----------------*---------------)
-+---------+---------+---------+-------5148
5160
5172
5184

Pooled StDev = 21.8

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of IV Umpan_5.75
Simultaneous confidence level = 95.00%

IV Umpan_5.75 = 0.6 subtracted from:


IV Umpan_5.75
0.7

Lower
-29.88

Center
-1.90

Upper
26.08

IV Umpan_5.75
0.7

+---------+---------+---------+--------(------------------*-----------------)
+---------+---------+---------+---------30
-15
0
15

MTB > Oneway 'Yield AS_6.00' 'IV Umpan_6.00';


SUBC>
Fisher 5.

Universitas Sumatera Utara

LAMPIRAN -3F
One-way ANOVA: Yield AS_6.00 versus IV Umpan_6.00
Source
IV Umpan_6.00
Error
Total
S = 31.69

Level
0.6
0.7

N
6
6

DF
1
10
11

SS
88
10044
10132

R-Sq = 0.87%

Mean
5402.8
5397.4

StDev
32.9
30.5

MS
88
1004

F
0.09

P
0.773

R-Sq(adj) = 0.00%

Individual 95% CIs For Mean Based on


Pooled StDev
-----+---------+---------+---------+---(-----------------*-----------------)
(-----------------*-----------------)
-----+---------+---------+---------+---5376
5392
5408
5424

Pooled StDev = 31.7

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of IV Umpan_6.00
Simultaneous confidence level = 95.00%

IV Umpan_6.00 = 0.6 subtracted from:


IV Umpan_6.00
---+0.7

Lower

Center

Upper

--------+---------+---------+------

-46.19

-5.42

35.35

(---------------*---------------)
--------+---------+---------+------

---+-25

25

50

Universitas Sumatera Utara

LAMPIRAN -3G
MTB > Oneway 'Yield AS_218' 'F Umpan_218';
SUBC>
Fisher 5.

One-way ANOVA: Yield AS_218 versus F Umpan_218


Source
F Umpan_218
Error
Total
S = 4.024

Level
5.50
5.75
6.00

N
4
4
4

DF
2
9
11

SS
404104.0
145.7
404249.7

MS
202052.0
16.2

R-Sq = 99.96%

Mean
4924.40
5148.00
5373.90

StDev
1.53
3.54
5.81

F
12480.91

P
0.000

R-Sq(adj) = 99.96%

Individual 95% CIs For Mean Based on Pooled


StDev
+---------+---------+---------+--------*)
*
(*
+---------+---------+---------+--------4920
5040
5160
5280

Pooled StDev = 4.02

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of F Umpan_218
Simultaneous confidence level = 88.66%

F Umpan_218 = 5.50 subtracted from:


F Umpan_218
----5.75
6.00
*)

Lower

Center

Upper

217.16
443.06

223.60
449.50

230.04
455.94

--+---------+---------+---------+-*)

--+---------+---------+---------+------200

200

400

F Umpan_218 = 5.75 subtracted from:


F Umpan_218
----6.00

Lower

Center

Upper

--+---------+---------+---------+--

219.46

225.90

232.34

*)
--+---------+---------+---------+--

-----200

200

400

Universitas Sumatera Utara

LAMPIRAN -3H
MTB > Oneway 'Yield AS_220' 'F Umpan_220';
SUBC>
Fisher 5.

One-way ANOVA: Yield AS_220 versus F Umpan_220


Source
F Umpan_220
Error
Total

DF
2
9
11

S = 0.9486

R-Sq = 100.00%

Level
5.50
5.75
6.00

N
4
4
4

SS
403471.6
8.1
403479.7

Mean
4937.05
5161.35
5386.20

StDev
0.84
0.56
1.30

MS
201735.8
0.9

F
224198.66

P
0.000

R-Sq(adj) = 100.00%

Individual 95% CIs For Mean Based on


Pooled StDev
---------+---------+---------+---------+
*)
*
*
---------+---------+---------+---------+
5040
5160
5280
5400

Pooled StDev = 0.95

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of F Umpan_220
Simultaneous confidence level = 88.66%

F Umpan_220 = 5.50 subtracted from:


F Umpan_220
5.75
6.00

Lower
222.785
447.633

Center
224.303
449.150

Upper
225.820
450.667

F Umpan_220
5.75
6.00

-+---------+---------+---------+-------*
*)
-+---------+---------+---------+--------200
0
200
400

F Umpan_220 = 5.75 subtracted from:


F Umpan_220
6.00

Lower
223.330

Center
224.847

Upper
226.365

F Umpan_220
6.00

-+---------+---------+---------+-------*
-+---------+---------+---------+--------200
0
200
400

Universitas Sumatera Utara

LAMPIRAN -3I
MTB > Oneway 'Yield AS_222' 'F Umpan_222';
SUBC>
Fisher 5.

One-way ANOVA: Yield AS_222 versus F Umpan_222


Source
F Umpan_222
Error
Total
S = 3.521

Level
5.50
5.75
6.00

N
4
4
4

DF
2
9
11

SS
444900.8
111.6
445012.4

MS
222450.4
12.4

R-Sq = 99.97%

Mean
4968.65
5195.00
5440.18

StDev
2.49
1.82
5.26

F
17943.69

P
0.000

R-Sq(adj) = 99.97%

Individual 95% CIs For Mean Based on


Pooled StDev
------+---------+---------+---------+--*
*
*)
------+---------+---------+---------+--5040
5160
5280
5400

Pooled StDev = 3.52

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of F Umpan_222
Simultaneous confidence level = 88.66%

F Umpan_222 = 5.50 subtracted from:


F Umpan_222
---5.75
6.00
(*

Lower

Center

Upper

220.72
465.89

226.35
471.52

231.98
477.15

---+---------+---------+---------+-*)

---+---------+---------+---------+-----200

200

400

F Umpan_222 = 5.75 subtracted from:


F Umpan_222
---6.00

Lower

Center

Upper

---+---------+---------+---------+--

239.54

245.17

250.80

*)
---+---------+---------+---------+--

----200

200

400

Universitas Sumatera Utara

LAMPIRAN -3J
Results for: Worksheet 3
MTB > Oneway 'Yield AS_5.50' 'Suhu B MD_5.50';
SUBC>
Fisher 5.

One-way ANOVA: Yield AS_5.50 versus Suhu B MD_5.50


Source
Suhu B MD_5.50
Error
Total
S = 1.758

Level
218
220
222

N
4
4
4

DF
2
9
11

SS
4156.29
27.81
4184.10

R-Sq = 99.34%

Mean
4924.40
4937.05
4968.65

StDev
1.53
0.84
2.49

MS
2078.14
3.09

F
672.52

P
0.000

R-Sq(adj) = 99.19%

Individual 95% CIs For Mean Based on


Pooled StDev
--------+---------+---------+---------+(*)
(*-)
(*-)
--------+---------+---------+---------+4935
4950
4965
4980

Pooled StDev = 1.76

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of Suhu B MD_5.50
Simultaneous confidence level = 88.66%

Suhu B MD_5.50 = 218 subtracted from:


Suhu B
MD_5.50
220
222

Lower
9.838
41.442

Center
12.650
44.254

Upper
15.462
47.066

----+---------+---------+---------+----(*)
(*)
----+---------+---------+---------+-----25
0
25
50

Suhu B MD_5.50 = 220 subtracted from:


Suhu B
MD_5.50
222

Lower
28.792

Center
31.604

Upper
34.416

----+---------+---------+---------+----(*)
----+---------+---------+---------+-----25
0
25
50

Universitas Sumatera Utara

LAMPIRAN -3K
MTB > Oneway 'Yield AS_5.75' 'Suhu B MD_5.75';
SUBC>
Fisher 5.

One-way ANOVA: Yield AS_5.75 versus Suhu B MD_5.75


Source
Suhu B MD_5.75
Error
Total
S = 2.318

Level
218
220
222

N
4
4
4

DF
2
9
11

SS
4693.13
48.35
4741.48

R-Sq = 98.98%

Mean
5148.00
5161.35
5195.00

StDev
3.54
0.56
1.82

MS
2346.56
5.37

F
436.76

P
0.000

R-Sq(adj) = 98.75%

Individual 95% CIs For Mean Based on Pooled


StDev
+---------+---------+---------+--------(-*-)
(-*-)
(*-)
+---------+---------+---------+--------5145
5160
5175
5190

Pooled StDev = 2.32

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of Suhu B MD_5.75
Simultaneous confidence level = 88.66%

Suhu B MD_5.75 = 218 subtracted from:


Suhu B
MD_5.75
220
222

Lower
9.645
43.295

Center
13.352
47.003

Upper
17.060
50.710

-----+---------+---------+---------+---(*-)
(-*)
-----+---------+---------+---------+----25
0
25
50

Suhu B MD_5.75 = 220 subtracted from:


Suhu B
MD_5.75
222

Lower
29.942

Center
33.650

Upper
37.358

-----+---------+---------+---------+---(*-)
-----+---------+---------+---------+----25
0
25
50

Universitas Sumatera Utara

LAMPIRAN -3L
MTB > Oneway 'Yield AS_6.00' 'Suhu B MD_6.00';
SUBC>
Fisher 5.

One-way ANOVA: Yield AS_6.00 versus Suhu B MD_6.00


Source
Suhu B MD_6.00
Error
Total
S = 4.585

Level
218
220
222

N
4
4
4

DF
2
9
11

SS
9942.6
189.2
10131.8

R-Sq = 98.13%

Mean
5373.90
5386.20
5440.18

StDev
5.81
1.30
5.26

MS
4971.3
21.0

F
236.47

P
0.000

R-Sq(adj) = 97.72%

Individual 95% CIs For Mean Based on


Pooled StDev
------+---------+---------+---------+--(--*--)
(-*--)
(--*--)
------+---------+---------+---------+--5380
5400
5420
5440

Pooled StDev = 4.59

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of Suhu B MD_6.00
Simultaneous confidence level = 88.66%

Suhu B MD_6.00 = 218 subtracted from:


Suhu B
MD_6.00
220
222

Lower
4.966
58.941

Center
12.300
66.275

Upper
19.634
73.609

--------+---------+---------+---------+(--*-)
(-*-)
--------+---------+---------+---------+-35
0
35
70

Suhu B MD_6.00 = 220 subtracted from:


Suhu B
MD_6.00
222

Lower
46.641

Center
53.975

Upper
61.309

--------+---------+---------+---------+(-*--)
--------+---------+---------+---------+-35
0
35
70

Universitas Sumatera Utara

LAMPIRAN -3M
Results for: Worksheet 2
MTB > Oneway 'Yield AS_0.6' 'Suhu B MD_0.6';
SUBC>
Fisher 5.

One-way ANOVA: Yield AS_0.6 versus Suhu B MD_0.6


Source
Suhu B MD_0.6
Error
Total
S = 205.3

Level
218
220
222

N
6
6
6

DF
2
15
17

SS
9322
632389
641711

R-Sq = 1.45%

Mean
5150.8
5161.5
5203.5

StDev
202.2
201.1
212.5

MS
4661
42159

F
0.11

P
0.896

R-Sq(adj) = 0.00%

Individual 95% CIs For Mean Based on


Pooled StDev
------+---------+---------+---------+--(--------------*--------------)
(--------------*--------------)
(--------------*--------------)
------+---------+---------+---------+--5040
5160
5280
5400

Pooled StDev = 205.3

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of Suhu B MD_0.6
Simultaneous confidence level = 88.31%

Suhu B MD_0.6 = 218 subtracted from:


Suhu B
MD_0.6
220
222

Lower
-241.9
-199.9

Center
10.8
52.8

Upper
263.4
305.4

--------+---------+---------+---------+(---------------*--------------)
(--------------*---------------)
--------+---------+---------+---------+-160
0
160
320

Suhu B MD_0.6 = 220 subtracted from:


Suhu B
MD_0.6
222

Lower
-210.7

Center
42.0

Upper
294.7

--------+---------+---------+---------+(---------------*--------------)

Universitas Sumatera Utara

--------+---------+---------+---------+-160
0
160
320

LAMPIRAN -3N
MTB > Oneway 'Yield AS_0.7' 'Suhu B MD_0.7';
SUBC>
Fisher 5.

One-way ANOVA: Yield AS_0.7 versus Suhu B MD_0.7


Source
Suhu B MD_0.7
Error
Total
S = 203.3

Level
218
220
222

N
6
6
6

DF
2
15
17

SS
8714
620246
628960

R-Sq = 1.39%

Mean
5146.8
5161.6
5199.1

StDev
199.9
200.6
209.4

MS
4357
41350

F
0.11

P
0.901

R-Sq(adj) = 0.00%

Individual 95% CIs For Mean Based on


Pooled StDev
------+---------+---------+---------+--(--------------*--------------)
(--------------*--------------)
(-------------*--------------)
------+---------+---------+---------+--5040
5160
5280
5400

Pooled StDev = 203.3

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of Suhu B MD_0.7
Simultaneous confidence level = 88.31%

Suhu B MD_0.7 = 218 subtracted from:


Suhu B
MD_0.7
220
222

Lower
-235.5
-198.0

Center
14.8
52.3

Upper
265.0
302.5

---------+---------+---------+---------+
(----------------*----------------)
(---------------*----------------)
---------+---------+---------+---------+
-150
0
150
300

Suhu B MD_0.7 = 220 subtracted from:


Suhu B
MD_0.7
222

Lower
-212.7

Center
37.5

Upper
287.7

---------+---------+---------+---------+
(----------------*---------------)

Universitas Sumatera Utara

---------+---------+---------+---------+
-150
0
150
300

LAMPIRAN -3O
Results for: Worksheet 5
MTB > Oneway 'Yield AS_218' 'IV Umpan_218';
SUBC>
Fisher 5.

One-way ANOVA: Yield AS_218 versus IV Umpan_218


Source
IV Umpan_218
Error
Total
S = 201.0

Level
0.6
0.7

N
6
6

DF
1
10
11

SS
47
404203
404250

R-Sq = 0.01%

Mean
5150.8
5146.8

StDev
202.2
199.9

MS
47
40420

F
0.00

P
0.973

R-Sq(adj) = 0.00%

Individual 95% CIs For Mean Based on


Pooled StDev
----+---------+---------+---------+----(-----------------*-----------------)
(------------------*-----------------)
----+---------+---------+---------+----5000
5100
5200
5300

Pooled StDev = 201.0

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of IV Umpan_218
Simultaneous confidence level = 95.00%

IV Umpan_218 = 0.6 subtracted from:


IV Umpan_218
--+0.7

Lower

Center

Upper

--------+---------+---------+-------

-262.6

-4.0

254.7

(-----------------*----------------)
--------+---------+---------+-------

--+-150

150

300

Universitas Sumatera Utara

LAMPIRAN -3P
MTB > Oneway 'Yield AS_220' 'IV Umpan_220';
SUBC>
Fisher 5.

One-way ANOVA: Yield AS_220 versus IV Umpan_220


Source
IV Umpan_220
Error
Total
S = 200.9

Level
0.6
0.7

N
6
6

DF
1
10
11

SS
0
403480
403480

R-Sq = 0.00%

Mean
5161.5
5161.6

StDev
201.1
200.6

MS
0
40348

F
0.00

P
1.000

R-Sq(adj) = 0.00%

Individual 95% CIs For Mean Based on


Pooled StDev
--+---------+---------+---------+------(-----------------*-----------------)
(-----------------*-----------------)
--+---------+---------+---------+------5000
5100
5200
5300

Pooled StDev = 200.9

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of IV Umpan_220
Simultaneous confidence level = 95.00%

IV Umpan_220 = 0.6 subtracted from:


IV Umpan_220
-+-0.7

Lower

Center

Upper

-------+---------+---------+--------

-258.4

0.0

258.4

(----------------*----------------)
-------+---------+---------+--------

-+--150

150

300

Universitas Sumatera Utara

LAMPIRAN -3Q
MTB > Oneway 'Yield AS_222' 'IV Umpan_222';
SUBC>
Fisher 5.

One-way ANOVA: Yield AS_222 versus IV Umpan_222


Source
IV Umpan_222
Error
Total
S = 210.9

Level
0.6
0.7

N
6
6

DF
1
10
11

SS
59
444953
445012

R-Sq = 0.01%

Mean
5203.5
5199.1

StDev
212.5
209.4

MS
59
44495

F
0.00

P
0.972

R-Sq(adj) = 0.00%

Individual 95% CIs For Mean Based on


Pooled StDev
---------+---------+---------+---------+
(------------------*-------------------)
(------------------*------------------)
---------+---------+---------+---------+
5100
5200
5300
5400

Pooled StDev = 210.9

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of IV Umpan_222
Simultaneous confidence level = 95.00%

IV Umpan_222 = 0.6 subtracted from:


IV Umpan_222
--+0.7
)

Lower

Center

Upper

--------+---------+---------+-------

-275.8

-4.4

266.9

(-----------------*-----------------

Universitas Sumatera Utara

--------+---------+---------+--------+-150

150

300
MTB > Save "C:\Program Files\MINITAB 14\Data\MINITAB.MPJ.26";
SUBC>
Project;
SUBC>
Replace.

5/10/2009 5:57:13 PM

LAMPIRAN -4A
7/13/2009 9:33:10 PM
Welcome to Minitab, press F1 for help.

General Linear Model: IV DAS versus F Umpan, IV Umpan, Suhu B MD


Factor
F Umpan
IV Umpan
Suhu B MD

Type
fixed
fixed
fixed

Levels
3
2
3

Values
5.50, 5.75, 6.00
0.6, 0.7
218, 220, 222

Analysis of Variance for IV DAS, using Adjusted SS for Tests


Source
P
F Umpan
0.000
IV Umpan
0.010
Suhu B MD
0.000
F Umpan*IV Umpan
0.920
F Umpan*Suhu B MD
0.679
IV Umpan*Suhu B MD
0.920
F Umpan*IV Umpan*Suhu B MD
0.986
Error
Total

DF

Seq SS

Adj SS

Adj MS

0.0012056

0.0012056

0.0006028

18.08

0.0002778

0.0002778

0.0002778

8.33

0.0012722

0.0012722

0.0006361

19.08

0.0000056

0.0000056

0.0000028

0.08

0.0000778

0.0000778

0.0000194

0.58

0.0000056

0.0000056

0.0000028

0.08

0.0000111

0.0000111

0.0000028

0.08

18
35

0.0006000
0.0034556

0.0006000

0.0000333

Universitas Sumatera Utara

S = 0.00577350

R-Sq = 82.64%

R-Sq(adj) = 66.24%

LAMPIRAN -4B
Results for: Worksheet 2
One-way ANOVA: IV DAS_0.6 versus F Umpan_0.6
Source
F Umpan_0.6
Error
Total
S = 0.007746

Level
5.50
5.75
6.00

N
6
6
6

DF
2
15
17

SS
0.0006778
0.0009000
0.0015778

MS
0.0003389
0.0000600

R-Sq = 42.96%

Mean
0.15333
0.16167
0.16833

StDev
0.00816
0.00753
0.00753

F
5.65

P
0.015

R-Sq(adj) = 35.35%

Individual 95% CIs For Mean Based on


Pooled StDev
-------+---------+---------+---------+-(--------*-------)
(-------*--------)
(-------*--------)
-------+---------+---------+---------+-0.1520
0.1600
0.1680
0.1760

Pooled StDev = 0.00775

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of F Umpan_0.6
Simultaneous confidence level = 88.31%

Universitas Sumatera Utara

F Umpan_0.6 = 5.50 subtracted from:


F Umpan_0.6
5.75
6.00

Lower
-0.001199
0.005468

Center
0.008333
0.015000

Upper
0.017865
0.024532

F Umpan_0.6
5.75
6.00

---+---------+---------+---------+-----(-------*-------)
(------*-------)
---+---------+---------+---------+------0.012
0.000
0.012
0.024

F Umpan_0.6 = 5.75 subtracted from:


F Umpan_0.6
6.00

Lower
-0.002865

F Umpan_0.6
6.00

---+---------+---------+---------+-----(-------*------)
---+---------+---------+---------+------0.012
0.000
0.012
0.024

Center
0.006667

Upper
0.016199

LAMPIRAN -4C
One-way ANOVA: IV DAS_0.7 versus F Umpan_0.7
Source
F Umpan_0.7
Error
Total
S = 0.008433

Level
5.50
5.75
6.00

N
6
6
6

DF
2
15
17

SS
0.0005333
0.0010667
0.0016000

MS
0.0002667
0.0000711

R-Sq = 33.33%

Mean
0.16000
0.16667
0.17333

StDev
0.01095
0.00516
0.00816

F
3.75

P
0.048

R-Sq(adj) = 24.44%

Individual 95% CIs For Mean Based on Pooled


StDev
---------+---------+---------+---------+
(--------*--------)
(--------*---------)
(---------*--------)
---------+---------+---------+---------+
0.1600
0.1680
0.1760
0.1840

Pooled StDev = 0.00843

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of F Umpan_0.7
Simultaneous confidence level = 88.31%

Universitas Sumatera Utara

F Umpan_0.7 = 5.50 subtracted from:


F Umpan_0.7
5.75
6.00

Lower
-0.003711
0.002956

Center
0.006667
0.013333

Upper
0.017044
0.023711

F Umpan_0.7
5.75
6.00

----+---------+---------+---------+----(--------*-------)
(--------*--------)
----+---------+---------+---------+-----0.012
0.000
0.012
0.024

F Umpan_0.7 = 5.75 subtracted from:


F Umpan_0.7
6.00

Lower
-0.003711

Center
0.006667

Upper
0.017044

F Umpan_0.7
6.00

----+---------+---------+---------+----(--------*-------)
----+---------+---------+---------+-----0.012
0.000
0.012
0.024

LAMPIRAN -4D
Results for: Worksheet 4
One-way ANOVA: IV DAS_5.50 versus IV Umpan_5.50
Source
IV Umpan_5.50
Error
Total

DF
1
10
11

S = 0.009661

R-Sq = 12.50%

Level
0.6
0.7

N
6
6

Mean
0.15333
0.16000

SS
0.0001333
0.0009333
0.0010667

StDev
0.00816
0.01095

MS
0.0001333
0.0000933

F
1.43

P
0.260

R-Sq(adj) = 3.75%

Individual 95% CIs For Mean Based on


Pooled StDev
----+---------+---------+---------+----(------------*------------)
(------------*-----------)
----+---------+---------+---------+----0.1470
0.1540
0.1610
0.1680

Pooled StDev = 0.00966

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of IV Umpan_5.50

Universitas Sumatera Utara

Simultaneous confidence level = 95.00%

IV Umpan_5.50 = 0.6 subtracted from:


IV Umpan_5.50
0.7

Lower
-0.005761

Center
0.006667

Upper
0.019095

IV Umpan_5.50
0.7

------+---------+---------+---------+--(--------------*---------------)
------+---------+---------+---------+---0.0080
0.0000
0.0080
0.0160

LAMPIRAN -4E
One-way ANOVA: IV DAS_5.75 versus IV Umpan_5.75
Source
IV Umpan_5.75
Error
Total

DF
1
10
11

S = 0.006455

R-Sq = 15.25%

Level
0.6
0.7

N
6
6

Mean
0.16167
0.16667

SS
0.0000750
0.0004167
0.0004917

StDev
0.00753
0.00516

MS
0.0000750
0.0000417

F
1.80

P
0.209

R-Sq(adj) = 6.78%

Individual 95% CIs For Mean Based on


Pooled StDev
--------+---------+---------+---------+(----------*-----------)
(----------*-----------)
--------+---------+---------+---------+0.1600
0.1650
0.1700
0.1750

Pooled StDev = 0.00645

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of IV Umpan_5.75

Universitas Sumatera Utara

Simultaneous confidence level = 95.00%

IV Umpan_5.75 = 0.6 subtracted from:


IV Umpan_5.75
0.7

Lower
-0.003304

Center
0.005000

Upper
0.013304

IV Umpan_5.75
0.7

----+---------+---------+---------+----(-------------*-------------)
----+---------+---------+---------+-----0.0060
0.0000
0.0060
0.0120

LAMPIRAN -4F
One-way ANOVA: IV DAS_6.00 versus IV Umpan_6.00
Source
IV Umpan_6.00
Error
Total

DF
1
10
11

S = 0.007853

R-Sq = 10.84%

Level
0.6
0.7

N
6
6

Mean
0.16833
0.17333

SS
0.0000750
0.0006167
0.0006917

StDev
0.00753
0.00816

MS
0.0000750
0.0000617

F
1.22

P
0.296

R-Sq(adj) = 1.93%

Individual 95% CIs For Mean Based on


Pooled StDev
--------+---------+---------+---------+(--------------*-------------)
(--------------*-------------)
--------+---------+---------+---------+0.1650
0.1700
0.1750
0.1800

Pooled StDev = 0.00785

Fisher 95% Individual Confidence Intervals

Universitas Sumatera Utara

All Pairwise Comparisons among Levels of IV Umpan_6.00


Simultaneous confidence level = 95.00%

IV Umpan_6.00 = 0.6 subtracted from:


IV Umpan_6.00
0.7

Lower
-0.005102

Center
0.005000

Upper
0.015102

IV Umpan_6.00
0.7

----+---------+---------+---------+----(-------------*--------------)
----+---------+---------+---------+-----0.0070
0.0000
0.0070
0.0140

LAMPIRAN -4G
Results for: Worksheet 3
One-way ANOVA: IV DAS_218 versus F Umpan_218
Source
F Umpan_218
Error
Total
S = 0.005

Level
5.50
5.75
6.00

N
4
4
4

DF
2
9
11

SS
0.0004667
0.0002250
0.0006917

R-Sq = 67.47%

Mean
0.14750
0.15750
0.16250

StDev
0.00500
0.00500
0.00500

MS
0.0002333
0.0000250

F
9.33

P
0.006

R-Sq(adj) = 60.24%

Individual 95% CIs For Mean Based on


Pooled StDev
-------+---------+---------+---------+-(-------*-------)
(-------*-------)
(-------*-------)
-------+---------+---------+---------+-0.1470
0.1540
0.1610
0.1680

Universitas Sumatera Utara

Pooled StDev = 0.00500

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of F Umpan_218
Simultaneous confidence level = 88.66%

F Umpan_218 = 5.50 subtracted from:


F Umpan_218
5.75
6.00

Lower
0.002002
0.007002

Center
0.010000
0.015000

Upper
0.017998
0.022998

F Umpan_218
5.75
6.00

---+---------+---------+---------+-----(-------*-------)
(-------*-------)
---+---------+---------+---------+------0.010
0.000
0.010
0.020

F Umpan_218 = 5.75 subtracted from:


F Umpan_218
6.00

Lower
-0.002998

F Umpan_218
6.00

---+---------+---------+---------+-----(-------*-------)
---+---------+---------+---------+------0.010
0.000
0.010
0.020

Center
0.005000

Upper
0.012998

LAMPIRAN -4H
One-way ANOVA: IV DAS_220 versus F Umpan_220
Source
F Umpan_220
Error
Total
S = 0.006872

Level
5.50
5.75
6.00

N
4
4
4

DF
2
9
11

SS
0.0004667
0.0004250
0.0008917

MS
0.0002333
0.0000472

R-Sq = 52.34%

Mean
0.15750
0.16750
0.17250

StDev
0.00957
0.00500
0.00500

F
4.94

P
0.036

R-Sq(adj) = 41.74%

Individual 95% CIs For Mean Based on


Pooled StDev
---+---------+---------+---------+-----(---------*---------)
(--------*---------)
(---------*--------)
---+---------+---------+---------+-----0.1520
0.1600
0.1680
0.1760

Universitas Sumatera Utara

Pooled StDev = 0.00687

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of F Umpan_220
Simultaneous confidence level = 88.66%

F Umpan_220 = 5.50 subtracted from:


F Umpan_220
5.75
6.00

Lower
-0.000992
0.004008

Center
0.010000
0.015000

Upper
0.020992
0.025992

F Umpan_220
5.75
6.00

---+---------+---------+---------+-----(--------*--------)
(---------*--------)
---+---------+---------+---------+------0.012
0.000
0.012
0.024

F Umpan_220 = 5.75 subtracted from:


F Umpan_220
6.00

Lower
-0.005992

Center
0.005000

F Umpan_220
6.00

---+---------+---------+---------+-----(--------*--------)
---+---------+---------+---------+------0.012
0.000
0.012
0.024

Upper
0.015992

LAMPIRAN -4I
One-way ANOVA: IV DAS_222 versus F Umpan_222
Source
F Umpan_222
Error
Total
S = 0.005270

Level
5.50
5.75
6.00

N
4
4
4

DF
2
9
11

SS
0.0003500
0.0002500
0.0006000

MS
0.0001750
0.0000278

R-Sq = 58.33%

Mean
0.16500
0.16750
0.17750

StDev
0.00577
0.00500
0.00500

F
6.30

P
0.019

R-Sq(adj) = 49.07%

Individual 95% CIs For Mean Based on


Pooled StDev
---+---------+---------+---------+-----(--------*-------)
(-------*--------)
(--------*-------)
---+---------+---------+---------+------

Universitas Sumatera Utara

0.1610

0.1680

0.1750

0.1820

Pooled StDev = 0.00527

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of F Umpan_222
Simultaneous confidence level = 88.66%

F Umpan_222 = 5.50 subtracted from:


F Umpan_222
5.75
6.00

Lower
-0.005931
0.004069

Center
0.002500
0.012500

Upper
0.010931
0.020931

F Umpan_222
5.75
6.00

--------+---------+---------+---------+(--------*-------)
(-------*--------)
--------+---------+---------+---------+-0.010
0.000
0.010
0.020

F Umpan_222 = 5.75 subtracted from:


F Umpan_222
6.00

Lower
0.001569

Center
0.010000

Upper
0.018431

F Umpan_222
6.00

--------+---------+---------+---------+(-------*-------)
--------+---------+---------+---------+-0.010
0.000
0.010
0.020

LAMPIRAN -4J
Results for: Worksheet 4
One-way ANOVA: IV DAS_5.50 versus Suhu B MD_5.50
Source
Suhu B MD_5.50
Error
Total
S = 0.007071

DF
2
9
11

SS
0.0006167
0.0004500
0.0010667

R-Sq = 57.81%

MS
0.0003083
0.0000500

F
6.17

P
0.021

R-Sq(adj) = 48.44%

Individual 95% CIs For Mean Based on


Pooled StDev

Universitas Sumatera Utara

Level
218
220
222

N
4
4
4

Mean
0.14750
0.15750
0.16500

StDev
0.00500
0.00957
0.00577

+---------+---------+---------+--------(------*-------)
(------*-------)
(-------*-------)
+---------+---------+---------+--------0.140
0.150
0.160
0.170

Pooled StDev = 0.00707

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of Suhu B MD_5.50
Simultaneous confidence level = 88.66%

Suhu B MD_5.50 = 218 subtracted from:


Suhu B
MD_5.50
220
222
Suhu B
MD_5.50
220
222

Lower
-0.001311
0.006189

Center
0.010000
0.017500

Upper
0.021311
0.028811

------+---------+---------+---------+--(--------*---------)
(---------*--------)
------+---------+---------+---------+---0.012
0.000
0.012
0.024

Suhu B MD_5.50 = 220 subtracted from:


Suhu B
MD_5.50
222
Suhu B
MD_5.50
222

Lower
-0.003811

Center
0.007500

Upper
0.018811

------+---------+---------+---------+--(--------*---------)
------+---------+---------+---------+---0.012
0.000
0.012
0.024

LAMPIRAN -4K
One-way ANOVA: IV DAS_5.75 versus Suhu B MD_5.75
Source
Suhu B MD_5.75
Error
Total
S = 0.005

DF
2
9
11

SS
0.0002667
0.0002250
0.0004917

R-Sq = 54.24%

MS
0.0001333
0.0000250

F
5.33

P
0.030

R-Sq(adj) = 44.07%

Individual 95% CIs For Mean Based on


Pooled StDev

Universitas Sumatera Utara

Level
218
220
222

N
4
4
4

Mean
0.15750
0.16750
0.16750

StDev
0.00500
0.00500
0.00500

-------+---------+---------+---------+-(---------*--------)
(--------*---------)
(--------*---------)
-------+---------+---------+---------+-0.1560
0.1620
0.1680
0.1740

Pooled StDev = 0.00500

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of Suhu B MD_5.75
Simultaneous confidence level = 88.66%

Suhu B MD_5.75 = 218 subtracted from:


Suhu B
MD_5.75
220
222
Suhu B
MD_5.75
220
222

Lower
0.002002
0.002002

Center
0.010000
0.010000

Upper
0.017998
0.017998

-+---------+---------+---------+-------(----------*-----------)
(----------*-----------)
-+---------+---------+---------+--------0.0070
0.0000
0.0070
0.0140

Suhu B MD_5.75 = 220 subtracted from:


Suhu B
MD_5.75
222
Suhu B
MD_5.75
222

Lower
-0.007998

Center
0.000000

Upper
0.007998

-+---------+---------+---------+-------(----------*----------)
-+---------+---------+---------+--------0.0070
0.0000
0.0070
0.0140

LAMPIRAN -4L
One-way ANOVA: IV DAS_6.00 versus Suhu B MD_6.00
Source
Suhu B MD_6.00
Error
Total
S = 0.005

DF
2
9
11

SS
0.0004667
0.0002250
0.0006917

R-Sq = 67.47%

MS
0.0002333
0.0000250

F
9.33

P
0.006

R-Sq(adj) = 60.24%

Universitas Sumatera Utara

Level
218
220
222

N
4
4
4

Mean
0.16250
0.17250
0.17750

StDev
0.00500
0.00500
0.00500

Individual 95% CIs For Mean Based on


Pooled StDev
------+---------+---------+---------+--(-------*-------)
(-------*--------)
(--------*-------)
------+---------+---------+---------+--0.1610
0.1680
0.1750
0.1820

Pooled StDev = 0.00500

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of Suhu B MD_6.00
Simultaneous confidence level = 88.66%

Suhu B MD_6.00 = 218 subtracted from:


Suhu B
MD_6.00
+-----220
222
--)

Lower

Center

Upper

0.002002
0.007002

0.010000
0.015000

0.017998
0.022998

---+---------+---------+--------(-------*-------)
(-------*-------+---------+---------+---------

+------0.010

0.000

0.010

0.020

Suhu B MD_6.00 = 220 subtracted from:


Suhu B
MD_6.00
222
Suhu B
MD_6.00
222

Lower
-0.002998

Center
0.005000

Upper
0.012998

---+---------+---------+---------+-----(-------*-------)
---+---------+---------+---------+------0.010
0.000
0.010
0.020

LAMPIRAN -4M
Results for: Worksheet 2
One-way ANOVA: IV DAS_0.6 versus Suhu B MD_0.6
Source

DF

SS

MS

Universitas Sumatera Utara

Suhu B MD_0.6
Error
Total

2
15
17

S = 0.008165

R-Sq = 36.62%

Level
218
220
222

N
6
6
6

Mean
0.15333
0.16333
0.16667

0.0005778
0.0010000
0.0015778

StDev
0.00816
0.00816
0.00816

0.0002889
0.0000667

4.33

0.033

R-Sq(adj) = 28.17%

Individual 95% CIs For Mean Based on


Pooled StDev
-+---------+---------+---------+-------(---------*---------)
(---------*---------)
(---------*---------)
-+---------+---------+---------+-------0.1470
0.1540
0.1610
0.1680

Pooled StDev = 0.00816

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of Suhu B MD_0.6
Simultaneous confidence level = 88.31%

Suhu B MD_0.6 = 218 subtracted from:


Suhu B
MD_0.6
Lower
+-----220
-0.000048
222
0.003286
--)

Center

Upper

0.010000
0.013333

0.020048
0.023381

---+---------+---------+--------(---------*---------)
(---------*---------+---------+---------+---------

+------0.010

0.000

0.010

0.020

Suhu B MD_0.6 = 220 subtracted from:


Suhu B
MD_0.6
Lower
+-----222
-0.006714

Center

Upper

---+---------+---------+---------

0.003333

0.013381

(---------*---------)
---+---------+---------+---------

+------0.010

0.000

0.010

0.020

LAMPIRAN -4N
One-way ANOVA: IV DAS_0.7 versus Suhu B MD_0.7

Universitas Sumatera Utara

Source
Suhu B MD_0.7
Error
Total

DF
2
15
17

S = 0.007746

R-Sq = 43.75%

Level
218
220
222

N
6
6
6

Mean
0.15833
0.16833
0.17333

SS
0.0007000
0.0009000
0.0016000

StDev
0.00753
0.00983
0.00516

MS
0.0003500
0.0000600

F
5.83

P
0.013

R-Sq(adj) = 36.25%

Individual 95% CIs For Mean Based on


Pooled StDev
-+---------+---------+---------+-------(--------*-------)
(-------*--------)
(--------*-------)
-+---------+---------+---------+-------0.1520
0.1600
0.1680
0.1760

Pooled StDev = 0.00775

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of Suhu B MD_0.7
Simultaneous confidence level = 88.31%

Suhu B MD_0.7 = 218 subtracted from:


Suhu B
MD_0.7
+---220
)
222
-----)

Lower

Center

Upper

-----+---------+---------+---------

0.000468

0.010000

0.019532

(---------*---------

0.005468

0.015000

0.024532

(---------*--------+---------+---------+---------

+----0.010

0.000

0.010

0.020

Suhu B MD_0.7 = 220 subtracted from:


Suhu B
MD_0.7
-+---222

Lower

Center

Upper

-----+---------+---------+--------

-0.004532

0.005000

0.014532

(---------*---------)
-----+---------+---------+--------

-+----0.010

0.000

0.010

0.020

Universitas Sumatera Utara

LAMPIRAN -4O
Results for: Worksheet 3
One-way ANOVA: IV DAS_218 versus IV Umpan_218
Source
IV Umpan_218
Error
Total
S = 0.007853

Level
0.6
0.7

N
6
6

DF
1
10
11

SS
0.0000750
0.0006167
0.0006917

MS
0.0000750
0.0000617

R-Sq = 10.84%

Mean
0.15333
0.15833

StDev
0.00816
0.00753

F
1.22

P
0.296

R-Sq(adj) = 1.93%

Individual 95% CIs For Mean Based on


Pooled StDev
--------+---------+---------+---------+(--------------*-------------)
(--------------*-------------)
--------+---------+---------+---------+0.1500
0.1550
0.1600
0.1650

Pooled StDev = 0.00785

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of IV Umpan_218
Simultaneous confidence level = 95.00%

IV Umpan_218 = 0.6 subtracted from:


IV Umpan_218
0.7

Lower
-0.005102

Center
0.005000

Upper
0.015102

IV Umpan_218
0.7

----+---------+---------+---------+----(-------------*--------------)
----+---------+---------+---------+-----0.0070
0.0000
0.0070
0.0140

Universitas Sumatera Utara

LAMPIRAN -4P
One-way ANOVA: IV DAS_220 versus IV Umpan_220
Source
IV Umpan_220
Error
Total
S = 0.009037

Level
0.6
0.7

N
6
6

DF
1
10
11

SS
0.0000750
0.0008167
0.0008917

R-Sq = 8.41%

Mean
0.16333
0.16833

StDev
0.00816
0.00983

MS
0.0000750
0.0000817

F
0.92

P
0.360

R-Sq(adj) = 0.00%

Individual 95% CIs For Mean Based on


Pooled StDev
-+---------+---------+---------+-------(------------*-------------)
(-------------*------------)
-+---------+---------+---------+-------0.1560
0.1620
0.1680
0.1740

Pooled StDev = 0.00904

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of IV Umpan_220
Simultaneous confidence level = 95.00%

IV Umpan_220 = 0.6 subtracted from:


IV Umpan_220
0.7

Lower
-0.006625

Center
0.005000

IV Umpan_220
0.7

-----+---------+---------+---------+---(-------------*--------------)
-----+---------+---------+---------+----0.0080
0.0000
0.0080
0.0160

Upper
0.016625

Universitas Sumatera Utara

LAMPIRAN -4Q
One-way ANOVA: IV DAS_222 versus IV Umpan_222
Source
IV Umpan_222
Error
Total
S = 0.006831

Level
0.6
0.7

N
6
6

DF
1
10
11

SS
0.0001333
0.0004667
0.0006000

MS
0.0001333
0.0000467

R-Sq = 22.22%

Mean
0.16667
0.17333

StDev
0.00816
0.00516

F
2.86

P
0.122

R-Sq(adj) = 14.44%

Individual 95% CIs For Mean Based on Pooled


StDev
---------+---------+---------+---------+
(-----------*------------)
(------------*-----------)
---------+---------+---------+---------+
0.1650
0.1700
0.1750
0.1800

Pooled StDev = 0.00683

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of IV Umpan_222
Simultaneous confidence level = 95.00%

IV Umpan_222 = 0.6 subtracted from:


IV Umpan_222
0.7

Lower
-0.002121

Center
0.006667

Upper
0.015455

IV Umpan_222
0.7

---+---------+---------+---------+-----(------------*-----------)
---+---------+---------+---------+------0.0070
0.0000
0.0070
0.0140

7/14/2009 5:49:26 AM

Universitas Sumatera Utara

LAMPIRAN 5A
7/29/2009 8:24:37 AM
Welcome to Minitab, press F1 for help.

General Linear Model: HS DAS, Red versus F Umpan, IV Umpan, Suhu B


MD
Factor
F Umpan
IV Umpan
Suhu B MD

Type
fixed
fixed
fixed

Levels
3
2
3

Values
5.50, 5.75, 6.00
0.6, 0.7
218, 220, 222

Analysis of Variance for HS DAS, Red, using Adjusted SS for Tests


Source
P
F Umpan
0.000
IV Umpan
0.000
Suhu B MD
0.000
F Umpan*IV Umpan
0.387
F Umpan*Suhu B MD
0.964
IV Umpan*Suhu B MD
0.868
F Umpan*IV Umpan*Suhu B MD
0.964
Error
Total

S = 0.0440959

DF

Seq SS

Adj SS

Adj MS

0.107222

0.107222

0.053611

27.57

0.046944

0.046944

0.046944

24.14

0.060556

0.060556

0.030278

15.57

0.003889

0.003889

0.001944

1.00

0.001111

0.001111

0.000278

0.14

0.000556

0.000556

0.000278

0.14

0.001111

0.001111

0.000278

0.14

18
35

0.035000
0.256389

0.035000

0.001944

R-Sq = 86.35%

R-Sq(adj) = 73.46%

Universitas Sumatera Utara

LAMPIRAN 5B
Results for: Worksheet 16
One-way ANOVA: HS DAS, Red_0.6 versus F Umpan_0.6
Source
F Umpan_0.6
Error
Total
S = 0.05774

Level
5.50
5.75
6.00

N
6
6
6

DF
2
15
17

SS
0.07000
0.05000
0.12000

MS
0.03500
0.00333

R-Sq = 58.33%

Mean
0.35000
0.45000
0.50000

StDev
0.05477
0.05477
0.06325

F
10.50

P
0.001

R-Sq(adj) = 52.78%

Individual 95% CIs For Mean Based on


Pooled StDev
-------+---------+---------+---------+-(------*------)
(------*------)
(------*-------)
-------+---------+---------+---------+-0.350
0.420
0.490
0.560

Pooled StDev = 0.05774

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of F Umpan_0.6
Simultaneous confidence level = 88.31%

F Umpan_0.6 = 5.50 subtracted from:


F Umpan_0.6
5.75
6.00

Lower
0.02895
0.07895

F Umpan_0.6
5.75
6.00

--+---------+---------+---------+------(------*------)
(------*------)
--+---------+---------+---------+-------0.10
0.00
0.10
0.20

Center
0.10000
0.15000

Upper
0.17105
0.22105

F Umpan_0.6 = 5.75 subtracted from:


F Umpan_0.6
6.00

Lower
-0.02105

Center
0.05000

Upper
0.12105

Universitas Sumatera Utara

F Umpan_0.6
6.00

--+---------+---------+---------+------(------*------)
--+---------+---------+---------+-------0.10
0.00
0.10
0.20

LAMPIRAN 5C
One-way ANOVA: HS DAS, Red_0.7 versus F Umpan_0.7
Source
F Umpan_0.7
Error
Total
S = 0.05676

Level
5.50
5.75
6.00

N
6
6
6

DF
2
15
17

SS
0.04111
0.04833
0.08944

MS
0.02056
0.00322

R-Sq = 45.96%

Mean
0.45000
0.50000
0.56667

StDev
0.05477
0.06325
0.05164

F
6.38

P
0.010

R-Sq(adj) = 38.76%

Individual 95% CIs For Mean Based on


Pooled StDev
---+---------+---------+---------+-----(-------*-------)
(-------*--------)
(-------*--------)
---+---------+---------+---------+-----0.420
0.480
0.540
0.600

Pooled StDev = 0.05676

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of F Umpan_0.7
Simultaneous confidence level = 88.31%

F Umpan_0.7 = 5.50 subtracted from:


F Umpan_0.7
5.75
6.00

Lower
-0.01985
0.04681

Center
0.05000
0.11667

Upper
0.11985
0.18652

F Umpan_0.7
5.75
6.00

----+---------+---------+---------+----(------*------)
(------*------)
----+---------+---------+---------+-----0.10
0.00
0.10
0.20

F Umpan_0.7 = 5.75 subtracted from:


F Umpan_0.7

Lower

Center

Upper

Universitas Sumatera Utara

6.00

-0.00319

0.06667

0.13652

F Umpan_0.7
6.00

----+---------+---------+---------+----(------*------)
----+---------+---------+---------+-----0.10
0.00
0.10
0.20

LAMPIRAN 5D
Results for: Worksheet 17
One-way ANOVA: HS DAS, Red_5.50 versus IV Umpan_5.50
Source
IV Umpan_5.50
Error
Total
S = 0.05477

Level
0.6
0.7

N
6
6

DF
1
10
11

SS
0.03000
0.03000
0.06000

R-Sq = 50.00%

Mean
0.35000
0.45000

StDev
0.05477
0.05477

MS
0.03000
0.00300

F
10.00

P
0.010

R-Sq(adj) = 45.00%

Individual 95% CIs For Mean Based on Pooled


StDev
+---------+---------+---------+--------(---------*---------)
(---------*---------)
+---------+---------+---------+--------0.300
0.350
0.400
0.450

Pooled StDev = 0.05477

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of IV Umpan_5.50
Simultaneous confidence level = 95.00%

IV Umpan_5.50 = 0.6 subtracted from:


IV Umpan_5.50
0.7

Lower
0.02954

Center
0.10000

Upper
0.17046

IV Umpan_5.50
0.7

+---------+---------+---------+--------(---------*---------)
+---------+---------+---------+---------0.070
0.000
0.070
0.140

Universitas Sumatera Utara

LAMPIRAN 5D
One-way ANOVA: HS DAS, Red_5.75 versus IV Umpan_5.75
Source
IV Umpan_5.75
Error
Total
S = 0.05916

Level
0.6
0.7

N
6
6

DF
1
10
11

SS
0.00750
0.03500
0.04250

R-Sq = 17.65%

Mean
0.45000
0.50000

StDev
0.05477
0.06325

MS
0.00750
0.00350

F
2.14

P
0.174

R-Sq(adj) = 9.41%

Individual 95% CIs For Mean Based on


Pooled StDev
-+---------+---------+---------+-------(-------------*------------)
(------------*------------)
-+---------+---------+---------+-------0.400
0.440
0.480
0.520

Pooled StDev = 0.05916

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of IV Umpan_5.75
Simultaneous confidence level = 95.00%

IV Umpan_5.75 = 0.6 subtracted from:


IV Umpan_5.75
0.7

Lower
-0.02611

Center
0.05000

Upper
0.12611

IV Umpan_5.75
0.7

---+---------+---------+---------+-----(-----------*------------)
---+---------+---------+---------+------0.060
0.000
0.060
0.120

Universitas Sumatera Utara

LAMPIRAN 5E
One-way ANOVA: HS DAS, Red_6.00 versus IV Umpan_6.00
Source
IV Umpan_6.00
Error
Total
S = 0.05774

Level
0.6
0.7

N
6
6

DF
1
10
11

SS
0.01333
0.03333
0.04667

R-Sq = 28.57%

Mean
0.50000
0.56667

StDev
0.06325
0.05164

MS
0.01333
0.00333

F
4.00

P
0.073

R-Sq(adj) = 21.43%

Individual 95% CIs For Mean Based on


Pooled StDev
-+---------+---------+---------+-------(----------*----------)
(---------*----------)
-+---------+---------+---------+-------0.450
0.500
0.550
0.600

Pooled StDev = 0.05774

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of IV Umpan_6.00
Simultaneous confidence level = 95.00%

IV Umpan_6.00 = 0.6 subtracted from:


IV Umpan_6.00
0.7

Lower
-0.00760

Center
0.06667

Upper
0.14094

IV Umpan_6.00
0.7

--+---------+---------+---------+------(-----------*-----------)
--+---------+---------+---------+-------0.060
0.000
0.060
0.120

Universitas Sumatera Utara

LAMPIRAN 5F
Results for: Worksheet 18
One-way ANOVA: HS DAS, Red_218 versus F Umpan_218
Source
F Umpan_218
Error
Total
S = 0.05270

Level
5.50
5.75
6.00

N
4
4
4

DF
2
9
11

SS
0.03167
0.02500
0.05667

MS
0.01583
0.00278

R-Sq = 55.88%

Mean
0.35000
0.42500
0.47500

StDev
0.05774
0.05000
0.05000

F
5.70

P
0.025

R-Sq(adj) = 46.08%

Individual 95% CIs For Mean Based on


Pooled StDev
---------+---------+---------+---------+
(--------*--------)
(--------*-------)
(--------*-------)
---------+---------+---------+---------+
0.350
0.420
0.490
0.560

Pooled StDev = 0.05270

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of F Umpan_218
Simultaneous confidence level = 88.66%

F Umpan_218 = 5.50 subtracted from:


F Umpan_218
5.75
6.00

Lower
-0.00931
0.04069

Center
0.07500
0.12500

Upper
0.15931
0.20931

F Umpan_218
5.75

---+---------+---------+---------+-----(--------*-------)

Universitas Sumatera Utara

6.00

(-------*--------)
---+---------+---------+---------+------0.10
0.00
0.10
0.20

F Umpan_218 = 5.75 subtracted from:


F Umpan_218
6.00

Lower
-0.03431

F Umpan_218
6.00

---+---------+---------+---------+-----(-------*-------)
---+---------+---------+---------+------0.10
0.00
0.10
0.20

Center
0.05000

Upper
0.13431

LAMPIRAN 5G
One-way ANOVA: HS DAS, Red_220 versus F Umpan_220
Source
F Umpan_220
Error
Total
S = 0.06455

Level
5.50
5.75
6.00

N
4
4
4

DF
2
9
11

SS
0.04500
0.03750
0.08250

MS
0.02250
0.00417

R-Sq = 54.55%

Mean
0.40000
0.47500
0.55000

StDev
0.08165
0.05000
0.05774

F
5.40

P
0.029

R-Sq(adj) = 44.44%

Individual 95% CIs For Mean Based on


Pooled StDev
---------+---------+---------+---------+
(--------*--------)
(--------*---------)
(--------*--------)
---------+---------+---------+---------+
0.400
0.480
0.560
0.640

Pooled StDev = 0.06455

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of F Umpan_220
Simultaneous confidence level = 88.66%

F Umpan_220 = 5.50 subtracted from:


F Umpan_220
5.75
6.00

Lower
-0.02825
0.04675

Center
0.07500
0.15000

Upper
0.17825
0.25325

F Umpan_220
5.75
6.00

-----+---------+---------+---------+---(-------*--------)
(--------*-------)

Universitas Sumatera Utara

-----+---------+---------+---------+----0.12
0.00
0.12
0.24

F Umpan_220 = 5.75 subtracted from:


F Umpan_220
6.00

Lower
-0.02825

Center
0.07500

Upper
0.17825

F Umpan_220
6.00

-----+---------+---------+---------+---(-------*--------)
-----+---------+---------+---------+----0.12
0.00
0.12
0.24

LAMPIRAN 5H
One-way ANOVA: HS DAS, Red_222 versus F Umpan_222
Source
F Umpan_222
Error
Total
S = 0.05270

Level
5.50
5.75
6.00

N
4
4
4

DF
2
9
11

SS
0.03167
0.02500
0.05667

MS
0.01583
0.00278

R-Sq = 55.88%

Mean
0.45000
0.52500
0.57500

StDev
0.05774
0.05000
0.05000

F
5.70

P
0.025

R-Sq(adj) = 46.08%

Individual 95% CIs For Mean Based on


Pooled StDev
----+---------+---------+---------+----(-------*--------)
(--------*--------)
(-------*--------)
----+---------+---------+---------+----0.420
0.490
0.560
0.630

Pooled StDev = 0.05270

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of F Umpan_222
Simultaneous confidence level = 88.66%

F Umpan_222 = 5.50 subtracted from:


F Umpan_222
5.75
6.00

Lower
-0.00931
0.04069

Center
0.07500
0.12500

Upper
0.15931
0.20931

F Umpan_222

---+---------+---------+---------+------

Universitas Sumatera Utara

5.75
6.00

(--------*-------)
(-------*--------)
---+---------+---------+---------+------0.10
0.00
0.10
0.20

F Umpan_222 = 5.75 subtracted from:


F Umpan_222
6.00

Lower
-0.03431

Center
0.05000

Upper
0.13431

F Umpan_222
6.00

---+---------+---------+---------+-----(-------*-------)
---+---------+---------+---------+------0.10
0.00
0.10
0.20

LAMPIRAN 5I
Results for: Worksheet 19
One-way ANOVA: HS DAS, Red_5.50 versus Suhu B MD_5.50
Source
Suhu B MD_5.50
Error
Total
S = 0.06667

Level
218
220
222

N
4
4
4

DF
2
9
11

SS
0.02000
0.04000
0.06000

R-Sq = 33.33%

Mean
0.35000
0.40000
0.45000

StDev
0.05774
0.08165
0.05774

MS
0.01000
0.00444

F
2.25

P
0.161

R-Sq(adj) = 18.52%

Individual 95% CIs For Mean Based on


Pooled StDev
-+---------+---------+---------+-------(----------*----------)
(----------*----------)
(---------*----------)
-+---------+---------+---------+-------0.280
0.350
0.420
0.490

Pooled StDev = 0.06667

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of Suhu B MD_5.50
Simultaneous confidence level = 88.66%

Suhu B MD_5.50 = 218 subtracted from:


Suhu B

Universitas Sumatera Utara

MD_5.50
+--220
222
-)

Lower

Center

Upper

------+---------+---------+---------

-0.05664
-0.00664

0.05000
0.10000

0.15664
0.20664

(----------*----------)
(----------*--------------+---------+---------+---------

+---0.10

0.00

0.10

0.20

Suhu B MD_5.50 = 220 subtracted from:


Suhu B
MD_5.50
+--222

Lower

Center

Upper

------+---------+---------+---------

-0.05664

0.05000

0.15664

(----------*----------)
------+---------+---------+---------

+---0.10

0.00

0.10

0.20

LAMPIRAN 5J
One-way ANOVA: HS DAS, Red_5.75 versus Suhu B MD_5.75
Source
Suhu B MD_5.75
Error
Total
S = 0.05

Level
218
220
222

N
4
4
4

DF
2
9
11

SS
0.02000
0.02250
0.04250

R-Sq = 47.06%

Mean
0.42500
0.47500
0.52500

StDev
0.05000
0.05000
0.05000

MS
0.01000
0.00250

F
4.00

P
0.057

R-Sq(adj) = 35.29%

Individual 95% CIs For Mean Based on


Pooled StDev
---------+---------+---------+---------+
(---------*--------)
(--------*---------)
(---------*--------)
---------+---------+---------+---------+
0.420
0.480
0.540
0.600

Pooled StDev = 0.05000

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of Suhu B MD_5.75
Simultaneous confidence level = 88.66%

Universitas Sumatera Utara

Suhu B MD_5.75 = 218 subtracted from:


Suhu B
MD_5.75
+--220
222
--)

Lower

Center

Upper

------+---------+---------+---------

-0.02998
0.02002

0.05000
0.10000

0.12998
0.17998

(---------*---------)
(--------*------------+---------+---------+---------

+---0.080

0.000

0.080

0.160

Suhu B MD_5.75 = 220 subtracted from:


Suhu B
MD_5.75
+--222

Lower

Center

Upper

------+---------+---------+---------

-0.02998

0.05000

0.12998

(---------*---------)
------+---------+---------+---------

+---0.080

0.000

0.080

0.160

LAMPIRAN 5K
One-way ANOVA: HS DAS, Red_6.00 versus Suhu B MD_6.00
Source
Suhu B MD_6.00
Error
Total
S = 0.05270

Level
218
220
222

N
4
4
4

DF
2
9
11

SS
0.02167
0.02500
0.04667

R-Sq = 46.43%

Mean
0.47500
0.55000
0.57500

StDev
0.05000
0.05774
0.05000

MS
0.01083
0.00278

F
3.90

P
0.060

R-Sq(adj) = 34.52%

Individual 95% CIs For Mean Based on


Pooled StDev
-+---------+---------+---------+-------(---------*---------)
(---------*---------)
(---------*---------)
-+---------+---------+---------+-------0.420
0.480
0.540
0.600

Pooled StDev = 0.05270

Fisher 95% Individual Confidence Intervals

Universitas Sumatera Utara

All Pairwise Comparisons among Levels of Suhu B MD_6.00


Simultaneous confidence level = 88.66%

Suhu B MD_6.00 = 218 subtracted from:


Suhu B
MD_6.00
---220
222
-)

Lower

Center

Upper

----+---------+---------+---------+-

-0.00931
0.01569

0.07500
0.10000

0.15931
0.18431

(---------*----------)
(---------*------------+---------+---------+---------+-

----0.080

0.000

0.080

0.160

Suhu B MD_6.00 = 220 subtracted from:


Suhu B
MD_6.00
---222

Lower

Center

Upper

----+---------+---------+---------+-

-0.05931

0.02500

0.10931

(---------*----------)
----+---------+---------+---------+-

----0.080

0.000

0.080

0.160

LAMPIRAN 5L
Results for: Worksheet 20
One-way ANOVA: HS DAS, Red_0.6 versus Suhu B MD_0.6
Source
Suhu B MD_0.6
Error
Total
S = 0.07746

Level
218
220
222

N
6
6
6

DF
2
15
17

SS
0.03000
0.09000
0.12000

R-Sq = 25.00%

Mean
0.38333
0.43333
0.48333

StDev
0.07528
0.08165
0.07528

MS
0.01500
0.00600

F
2.50

P
0.116

R-Sq(adj) = 15.00%

Individual 95% CIs For Mean Based on


Pooled StDev
-------+---------+---------+---------+-(----------*----------)
(----------*----------)
(-----------*----------)

Universitas Sumatera Utara

-------+---------+---------+---------+-0.360
0.420
0.480
0.540
Pooled StDev = 0.07746

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of Suhu B MD_0.6
Simultaneous confidence level = 88.31%

Suhu B MD_0.6 = 218 subtracted from:


Suhu B
MD_0.6
--220
222

Lower

Center

Upper

-----+---------+---------+---------+-

-0.04532
0.00468

0.05000
0.10000

0.14532
0.19532

(---------*---------)
(---------*---------)
-----+---------+---------+---------+-

---0.10

0.00

0.10

0.20

Suhu B MD_0.6 = 220 subtracted from:


Suhu B
MD_0.6
--222

Lower

Center

Upper

-----+---------+---------+---------+-

-0.04532

0.05000

0.14532

(---------*---------)
-----+---------+---------+---------+-

---0.10

0.00

0.10

0.20

LAMPIRAN 5M
One-way ANOVA: HS DAS, Red_0.7 versus Suhu B MD_0.7
Source
Suhu B MD_0.7
Error
Total
S = 0.06236

DF
2
15
17

SS
0.03111
0.05833
0.08944

R-Sq = 34.78%

MS
0.01556
0.00389

F
4.00

P
0.041

R-Sq(adj) = 26.09%

Individual 95% CIs For Mean Based on

Universitas Sumatera Utara

Level
218
220
222

N
6
6
6

Mean
0.45000
0.51667
0.55000

StDev
0.05477
0.07528
0.05477

Pooled StDev
----+---------+---------+---------+----(--------*--------)
(--------*--------)
(--------*--------)
----+---------+---------+---------+----0.600
0.420
0.480
0.540

Pooled StDev = 0.06236

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of Suhu B MD_0.7
Simultaneous confidence level = 88.31%

Suhu B MD_0.7 = 218 subtracted from:


Suhu B
MD_0.7
--220
222

Lower

Center

Upper

----+---------+---------+---------+--

-0.01007
0.02326

0.06667
0.10000

0.14341
0.17674

(--------*---------)
(--------*---------)
----+---------+---------+---------+--

---0.080

0.000

0.080

0.160

Suhu B MD_0.7 = 220 subtracted from:


Suhu B
MD_0.7
--222

Lower

Center

Upper

----+---------+---------+---------+--

-0.04341

0.03333

0.11007

(--------*---------)
----+---------+---------+---------+--

---0.080

0.000

0.080

0.160

LAMPIRAN 5O
Results for: Worksheet 21
One-way ANOVA: HS DAS, Red_218 versus IV Umpan_218
Source
IV Umpan_218

DF
1

SS
0.01333

MS
0.01333

F
3.08

P
0.110

Universitas Sumatera Utara

Error
Total

10
11

S = 0.06583

R-Sq = 23.53%

Level
0.6
0.7

N
6
6

Mean
0.38333
0.45000

0.04333
0.05667

StDev
0.07528
0.05477

0.00433

R-Sq(adj) = 15.88%

Individual 95% CIs For Mean Based on


Pooled StDev
-----+---------+---------+---------+---(-----------*-----------)
(-----------*-----------)
-----+---------+---------+---------+---0.500
0.350
0.400
0.450

Pooled StDev = 0.06583

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of IV Umpan_218
Simultaneous confidence level = 95.00%

IV Umpan_218 = 0.6 subtracted from:


IV Umpan_218
0.7

Lower
-0.01802

Center
0.06667

Upper
0.15135

IV Umpan_218
0.7

----+---------+---------+---------+----(-------------*-------------)
----+---------+---------+---------+-----0.060
0.000
0.060
0.120

LAMPIRAN 5P
One-way ANOVA: HS DAS, Red_220 versus IV Umpan_220
Source
IV Umpan_220

DF
1

SS
0.02083

MS
0.02083

F
3.38

P
0.096

Universitas Sumatera Utara

Error
Total

10
11

S = 0.07853

R-Sq = 25.25%

Level
0.6
0.7

N
6
6

Mean
0.43333
0.51667

0.06167
0.08250

StDev
0.08165
0.07528

0.00617

R-Sq(adj) = 17.78%

Individual 95% CIs For Mean Based on


Pooled StDev
+---------+---------+---------+--------(-----------*-----------)
(-----------*-----------)
+---------+---------+---------+--------0.360
0.420
0.480
0.540

Pooled StDev = 0.07853

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of IV Umpan_220
Simultaneous confidence level = 95.00%

IV Umpan_220 = 0.6 subtracted from:


IV Umpan_220
0.7

Lower
-0.01769

Center
0.08333

Upper
0.18435

IV Umpan_220
0.7

---+---------+---------+---------+-----(-----------*------------)
---+---------+---------+---------+------0.080
0.000
0.080
0.160

LAMPIRAN 5Q
One-way ANOVA: HS DAS, Red_222 versus IV Umpan_222

Universitas Sumatera Utara

Source
IV Umpan_222
Error
Total

DF
1
10
11

S = 0.06583

R-Sq = 23.53%

Level
0.6
0.7

N
6
6

Mean
0.48333
0.55000

SS
0.01333
0.04333
0.05667

StDev
0.07528
0.05477

MS
0.01333
0.00433

F
3.08

P
0.110

R-Sq(adj) = 15.88%

Individual 95% CIs For Mean Based on


Pooled StDev
-----+---------+---------+---------+---(-----------*-----------)
(-----------*-----------)
-----+---------+---------+---------+---0.450
0.500
0.550
0.600

Pooled StDev = 0.06583

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of IV Umpan_222
Simultaneous confidence level = 95.00%

IV Umpan_222 = 0.6 subtracted from:


IV Umpan_222
0.7

Lower
-0.01802

Center
0.06667

Upper
0.15135

IV Umpan_222
0.7

----+---------+---------+---------+----(-------------*-------------)
----+---------+---------+---------+-----0.060
0.000
0.060
0.120

8/2/2009 8:41:36 AM

LAMPIRAN -6A

Universitas Sumatera Utara

5/8/2009 6:04:08 AM
General Linear Model: HS AS Yellow versus F Umpan, IV Umpan, Suhu B
MD
Factor
F Umpan
IV Umpan
Suhu B MD

Type
fixed
fixed
fixed

Levels
3
2
3

Values
5.50, 5.75, 6.00
0.6, 0.7
218, 220, 222

Analysis of Variance for HS AS Yellow, using Adjusted SS for Tests


Source
P
F Umpan
0.034
IV Umpan
0.007
Suhu B MD
0.000
F Umpan*IV Umpan
0.837
F Umpan*Suhu B MD
0.942
IV Umpan*Suhu B MD
0.175
F Umpan*IV Umpan*Suhu B MD
0.946
Error
Total

S = 0.180278

DF

Seq SS

Adj SS

Adj MS

0.26722

0.26722

0.13361

4.11

0.30250

0.30250

0.30250

9.31

15.58389

15.58389

7.79194

239.75

0.01167

0.01167

0.00583

0.18

0.02444

0.02444

0.00611

0.19

0.12500

0.12500

0.06250

1.92

0.02333

0.02333

0.00583

0.18

18
35

0.58500
16.92306

0.58500

0.03250

R-Sq = 96.54%

R-Sq(adj) = 93.28%

Universitas Sumatera Utara

LAMPIRAN -6B
5/8/2009 10:38:31 AM
One-way ANOVA: HS AS Yellow_0.6 versus F Umpan_0.6
Source
F Umpan_0.6
Error
Total

DF
2
15
17

S = 0.6813

R-Sq = 1.99%

Level
5.50
5.75
6.00

N
6
6
6

SS
0.141
6.963
7.104

Mean
4.6333
4.7500
4.8500

MS
0.071
0.464

StDev
0.7062
0.6834
0.6535

F
0.15

P
0.860

R-Sq(adj) = 0.00%

Individual 95% CIs For Mean Based on


Pooled StDev
---------+---------+---------+---------+
(--------------*--------------)
(--------------*--------------)
(--------------*--------------)
---------+---------+---------+---------+
4.40
4.80
5.20
5.60

Pooled StDev = 0.6813

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of F Umpan_0.6
Simultaneous confidence level = 88.31%

F Umpan_0.6 = 5.50 subtracted from:


F Umpan_0.6
--+
5.75
-)
6.00
---)

Lower

Center

Upper

---------+---------+---------+-------

-0.7218

0.1167

0.9551

(---------------*---------------

-0.6218

0.2167

1.0551

(---------------*---------------------+---------+---------+-------

--+
-0.50

0.00

0.50

1.00

F Umpan_0.6 = 5.75 subtracted from:


F Umpan_0.6
--+
6.00
-)

Lower

Center

Upper

---------+---------+---------+-------

-0.7385

0.1000

0.9385

(----------------*-----------------------+---------+---------+-------

--+
-0.50

0.00

0.50

1.00

Universitas Sumatera Utara

LAMPIRAN -6C
5/8/2009 10:38:31 AM
One-way ANOVA: HS DAS Yellow_0.7 versus F Umpan_0.7
Source
F Umpan_0.7
Error
Total

DF
2
15
17

S = 0.7907

R-Sq = 1.45%

Level
5.50
5.75
6.00

N
6
6
6

Mean
4.8500
4.8833
5.0500

SS
0.138
9.378
9.516

MS
0.069
0.625

StDev
0.7740
0.7782
0.8191

F
0.11

P
0.896

R-Sq(adj) = 0.00%

Individual 95% CIs For Mean Based on


Pooled StDev
------+---------+---------+---------+--(----------------*----------------)
(----------------*----------------)
(----------------*----------------)
------+---------+---------+---------+--4.40
4.80
5.20
5.60

Pooled StDev = 0.7907

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of F Umpan_0.7
Simultaneous confidence level = 88.31%

F Umpan_0.7 = 5.50 subtracted from:


F Umpan_0.7
--+
5.75
6.00
--)

Lower

Center

Upper

---------+---------+---------+-------

-0.9397
-0.7730

0.0333
0.2000

1.0064
1.1730

(----------------*---------------)
(---------------*----------------------+---------+---------+-------

--+
-0.60

0.00

0.60

1.20

F Umpan_0.7 = 5.75 subtracted from:

Universitas Sumatera Utara

F Umpan_0.7
--+
6.00
-)

Lower

Center

Upper

---------+---------+---------+-------

-0.8064

0.1667

1.1397

(---------------*----------------------+---------+---------+-------

--+
-0.60

0.00

0.60

1.20

LAMPIRAN -6D
5/27/2009 10:40:11 AM
One-way ANOVA: HS AS Yellow_5.50 versus IV Umpan_5.50
Source
IV Umpan_5.50
Error
Total
S = 0.7408

Level
0.6
0.7

N
6
6

DF
1
10
11

SS
0.141
5.488
5.629

R-Sq = 2.50%

Mean
4.6333
4.8500

StDev
0.7062
0.7740

MS
0.141
0.549

F
0.26

P
0.623

R-Sq(adj) = 0.00%

Individual 95% CIs For Mean Based on


Pooled StDev
-+---------+---------+---------+-------(----------------*----------------)
(----------------*----------------)
-+---------+---------+---------+-------4.00
4.40
4.80
5.20

Pooled StDev = 0.7408

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of IV Umpan_5.50
Simultaneous confidence level = 95.00%

IV Umpan_5.50 = 0.6 subtracted from:


IV Umpan_5.50
0.7

Lower
-0.7364

IV Umpan_5.50
0.7

------+---------+---------+---------+--(---------------*--------------)

Center
0.2167

Upper
1.1697

Universitas Sumatera Utara

------+---------+---------+---------+---0.60
0.00
0.60
1.20
MTB > Oneway 'HS AS Yellow_5.75' 'IV Umpan_5.75';
SUBC>
Fisher 5.

LAMPIRAN -6E
5/27/2009 10:40:11 AM
One-way ANOVA: HS AS Yellow_5.75 versus IV Umpan_5.75
Source
IV Umpan_5.75
Error
Total
S = 0.7323

Level
0.6
0.7

N
6
6

DF
1
10
11

SS
0.053
5.363
5.417

R-Sq = 0.98%

Mean
4.7500
4.8833

StDev
0.6834
0.7782

MS
0.053
0.536

F
0.10

P
0.759

R-Sq(adj) = 0.00%

Individual 95% CIs For Mean Based on


Pooled StDev
--------+---------+---------+---------+(----------------*---------------)
(----------------*----------------)
--------+---------+---------+---------+4.40
4.80
5.20
5.60

Pooled StDev = 0.7323

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of IV Umpan_5.75
Simultaneous confidence level = 95.00%

IV Umpan_5.75 = 0.6 subtracted from:


IV Umpan_5.75
0.7

Lower
-0.8088

Center
0.1333

Upper
1.0754

IV Umpan_5.75

------+---------+---------+---------+---

Universitas Sumatera Utara

0.7

(--------------*---------------)
------+---------+---------+---------+---0.60
0.00
0.60
1.20

LAMPIRAN -6F
5/27/2009 10:40:11 AM
One-way ANOVA: HS AS Yellow_6.00 versus IV Umpan_6.00
Source
IV Umpan_6.00
Error
Total
S = 0.7409

Level
0.6
0.7

N
6
6

DF
1
10
11

SS
0.120
5.490
5.610

R-Sq = 2.14%

Mean
4.8500
5.0500

StDev
0.6535
0.8191

MS
0.120
0.549

F
0.22

P
0.650

R-Sq(adj) = 0.00%

Individual 95% CIs For Mean Based on


Pooled StDev
------+---------+---------+---------+--(----------------*----------------)
(----------------*----------------)
------+---------+---------+---------+--4.40
4.80
5.20
5.60

Pooled StDev = 0.7409

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of IV Umpan_6.00
Simultaneous confidence level = 95.00%

IV Umpan_6.00 = 0.6 subtracted from:


IV Umpan_6.00
0.7

Lower
-0.7532

Center
0.2000

Upper
1.1532

Universitas Sumatera Utara

IV Umpan_6.00
0.7

------+---------+---------+---------+--(---------------*---------------)
------+---------+---------+---------+---0.60
0.00
0.60
1.20

LAMPIRAN -6G
5/27/2009 10:40:11 AM
One-way ANOVA: HS AS Yellow_218 versus F Umpan_218
Source
F Umpan_218
Error
Total

DF
2
9
11

S = 0.1269

R-Sq = 42.00%

Level
5.50
5.75
6.00

N
4
4
4

Mean
3.8500
3.9250
4.0750

SS
0.1050
0.1450
0.2500

StDev
0.1732
0.0957
0.0957

MS
0.0525
0.0161

F
3.26

P
0.086

R-Sq(adj) = 29.11%

Individual 95% CIs For Mean Based on


Pooled StDev
---+---------+---------+---------+-----(---------*--------)
(---------*--------)
(---------*--------)
---+---------+---------+---------+-----3.75
3.90
4.05
4.20

Pooled StDev = 0.1269

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of F Umpan_218
Simultaneous confidence level = 88.66%

F Umpan_218 = 5.50 subtracted from:

Universitas Sumatera Utara

F Umpan_218
---+5.75
6.00
----)

Lower

Center

Upper

--------+---------+---------+------

-0.1280
0.0220

0.0750
0.2250

0.2780
0.4280

(---------*---------)
(---------*------------+---------+---------+------

---+-0.20

0.00

0.20

0.40

F Umpan_218 = 5.75 subtracted from:


F Umpan_218
---+6.00
-)

Lower

Center

Upper

--------+---------+---------+------

-0.0530

0.1500

0.3530

(---------*----------------+---------+---------+------

---+-0.20

0.00

0.20

0.40

LAMPIRAN -6H
5/27/2009 10:40:11 AM
MTB > Oneway 'HS AS Yellow_220' 'F Umpan_220';
SUBC>
Fisher 5.

One-way ANOVA: HS AS Yellow_220 versus F Umpan_220


Source
F Umpan_220
Error
Total

DF
2
9
11

S = 0.1886

R-Sq = 12.73%

Level
5.50
5.75
6.00

N
4
4
4

Mean
4.9500
5.0500
5.1000

SS
0.0467
0.3200
0.3667

StDev
0.1915
0.1915
0.1826

MS
0.0233
0.0356

F
0.66

P
0.542

R-Sq(adj) = 0.00%

Individual 95% CIs For Mean Based on


Pooled StDev
----+---------+---------+---------+----(-------------*-------------)
(--------------*-------------)
(-------------*-------------)
----+---------+---------+---------+----4.80
4.95
5.10
5.25

Pooled StDev = 0.1886

Fisher 95% Individual Confidence Intervals

Universitas Sumatera Utara

All Pairwise Comparisons among Levels of F Umpan_220


Simultaneous confidence level = 88.66%

F Umpan_220 = 5.50 subtracted from:


F Umpan_220
+----5.75
6.00

Lower

Center

Upper

----+---------+---------+---------

-0.2016
-0.1516

0.1000
0.1500

0.4016
0.4516

(-----------*-----------)
(-----------*-----------)
----+---------+---------+---------

+-----0.25

0.00

0.25

0.50

F Umpan_220 = 5.75 subtracted from:


F Umpan_220
+----6.00

Lower

Center

Upper

----+---------+---------+---------

-0.2516

0.0500

0.3516

(-----------*-----------)
----+---------+---------+---------

+-----0.25

0.00

0.25

0.50

LAMPIRAN -6I
5/27/2009 10:40:11 AM
MTB > Oneway 'HS AS Yellow_222' 'F Umpan_222';
SUBC>
Fisher 5.

One-way ANOVA: HS AS Yellow_222 versus F Umpan_222


Source
F Umpan_222
Error
Total

DF
2
9
11

S = 0.2544

R-Sq = 19.38%

Level
5.50
5.75
6.00

N
4
4
4

Mean
5.4250
5.4750
5.6750

SS
0.1400
0.5825
0.7225

StDev
0.2630
0.2217
0.2754

MS
0.0700
0.0647

F
1.08

P
0.379

R-Sq(adj) = 1.46%

Individual 95% CIs For Mean Based on


Pooled StDev
-----+---------+---------+---------+---(-----------*-----------)
(-----------*-----------)
(-----------*-----------)
-----+---------+---------+---------+---5.25
5.50
5.75
6.00

Universitas Sumatera Utara

Pooled StDev = 0.2544

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of F Umpan_222
Simultaneous confidence level = 88.66%

F Umpan_222 = 5.50 subtracted from:


F Umpan_222
--+-5.75
6.00
-)

Lower

Center

Upper

-------+---------+---------+-------

-0.3569
-0.1569

0.0500
0.2500

0.4569
0.6569

(----------*-----------)
(----------*----------------+---------+---------+-------

--+--0.35

0.00

0.35

0.70

F Umpan_222 = 5.75 subtracted from:


F Umpan_222
--+-6.00

Lower

Center

Upper

-------+---------+---------+-------

-0.2069

0.2000

0.6069

(-----------*----------)
-------+---------+---------+-------

--+--0.35

0.00

0.35

0.70

LAMPIRAN -6J
MTB > Oneway 'HS AS Yellow_5.50' 'Suhu B MD_5.50';
SUBC>
Fisher 5.

One-way ANOVA: HS AS Yellow_5.50 versus Suhu B MD_5.50


Source
Suhu B MD_5.50
Error
Total
S = 0.2128

Level
218
220
222

N
4
4
4

DF
2
9
11

SS
5.2217
0.4075
5.6292

R-Sq = 92.76%

Mean
3.8500
4.9500
5.4250

StDev
0.1732
0.1915
0.2630

MS
2.6108
0.0453

F
57.66

P
0.000

R-Sq(adj) = 91.15%

Individual 95% CIs For Mean Based on


Pooled StDev
+---------+---------+---------+--------(---*---)
(----*---)
(---*---)
+---------+---------+---------+--------3.60
4.20
4.80
5.40

Universitas Sumatera Utara

Pooled StDev = 0.2128

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of Suhu B MD_5.50
Simultaneous confidence level = 88.66%

Suhu B MD_5.50 = 218 subtracted from:


Suhu B
MD_5.50
220
222
)

Lower

Center

Upper

--+---------+---------+---------+------

0.7596
1.2346

1.1000
1.5750

1.4404
1.9154

(----*----)
(---*-----+---------+---------+---------+------

-0.70

0.00

0.70

1.40

Suhu B MD_5.50 = 220 subtracted from:


Suhu B
MD_5.50
222

Lower

Center

Upper

--+---------+---------+---------+------

0.1346

0.4750

0.8154

(----*----)
--+---------+---------+---------+------

-0.70

0.00

0.70

1.40

LAMPIRAN -6K
MTB > Oneway 'HS AS Yellow_5.75' 'Suhu B MD_5.75';
SUBC>
Fisher 5.

One-way ANOVA: HS AS Yellow_5.75 versus Suhu B MD_5.75


Source
Suhu B MD_5.75
Error
Total
S = 0.1780

Level

DF
2
9
11

SS
5.1317
0.2850
5.4167

R-Sq = 94.74%

Mean

StDev

MS
2.5658
0.0317

F
81.03

P
0.000

R-Sq(adj) = 93.57%

Individual 95% CIs For Mean Based on


Pooled StDev
------+---------+---------+---------+---

Universitas Sumatera Utara

218
220
222

4
4
4

3.9250
5.0500
5.4750

0.0957
0.1915
0.2217

(----*---)
(---*---)
(---*----)
------+---------+---------+---------+--5.50
4.00
4.50
5.00

Pooled StDev = 0.1780

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of Suhu B MD_5.75
Simultaneous confidence level = 88.66%

Suhu B MD_5.75 = 218 subtracted from:


Suhu B
MD_5.75
--220
222

Lower

Center

Upper

+---------+---------+---------+------

0.8404
1.2654

1.1250
1.5500

1.4096
1.8346

(---*---)
(---*---)
+---------+---------+---------+------

---0.70

0.00

0.70

1.40

Suhu B MD_5.75 = 220 subtracted from:


Suhu B
MD_5.75
--222

Lower

Center

Upper

+---------+---------+---------+------

0.1404

0.4250

0.7096

(---*---)
+---------+---------+---------+------

---0.70

0.00

0.70

1.40

LAMPIRAN -6L
MTB > Oneway 'HS AS Yellow_6.00' 'Suhu B MD_6.00';
SUBC>
Fisher 5.

One-way ANOVA: HS AS Yellow_6.00 versus Suhu B MD_6.00


Source
Suhu B MD_6.00
Error
Total
S = 0.1986

DF
2
9
11

SS
5.2550
0.3550
5.6100

R-Sq = 93.67%

MS
2.6275
0.0394

F
66.61

P
0.000

R-Sq(adj) = 92.27%

Universitas Sumatera Utara

Level
218
220
222

N
4
4
4

Mean
4.0750
5.1000
5.6750

StDev
0.0957
0.1826
0.2754

Individual 95% CIs For Mean Based on


Pooled StDev
------+---------+---------+---------+--(---*---)
(---*---)
(---*--)
------+---------+---------+---------+--5.40
6.00
4.20
4.80

Pooled StDev = 0.1986

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of Suhu B MD_6.00
Simultaneous confidence level = 88.66%

Suhu B MD_6.00 = 218 subtracted from:


Suhu B
MD_6.00
-220
222

Lower

Center

Upper

-+---------+---------+---------+------

0.7073
1.2823

1.0250
1.6000

1.3427
1.9177

(---*---)
(---*---)
-+---------+---------+---------+------

--0.80

0.00

0.80

1.60

Suhu B MD_6.00 = 220 subtracted from:


Suhu B
MD_6.00
-222

Lower

Center

Upper

-+---------+---------+---------+------

0.2573

0.5750

0.8927

(---*---)
-+---------+---------+---------+------

--0.80

0.00

0.80

1.60

LAMPIRAN -6M
5/8/2009 6:04:08 AM
MTB > Oneway 'HS AS Yellow_0.6' 'Suhu B MD_0.6';
SUBC>
Fisher 5.

Universitas Sumatera Utara

One-way ANOVA: HS AS Yellow_0.6 versus Suhu B MD_0.6


Source
Suhu B MD_0.6
Error
Total
S = 0.1374

Level
218
220
222

N
6
6
6

DF
2
15
17

SS
6.8211
0.2833
7.1044

MS
3.4106
0.0189

R-Sq = 96.01%

Mean
3.9000
4.9833
5.3500

StDev
0.1549
0.1472
0.1049

F
180.56

P
0.000

R-Sq(adj) = 95.48%

Individual 95% CIs For Mean Based on


Pooled StDev
----+---------+---------+---------+----(-*-)
(--*-)
(-*-)
----+---------+---------+---------+----4.00
4.50
5.00
5.50

Pooled StDev = 0.1374

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of Suhu B MD_0.6
Simultaneous confidence level = 88.31%

Suhu B MD_0.6 = 218 subtracted from:


Suhu B
MD_0.6
220
222

Lower
0.9142
1.2809

Center
1.0833
1.4500

Upper
1.2525
1.6191

---------+---------+---------+---------+
(--*--)
(--*--)
---------+---------+---------+---------+
0.00
0.60
1.20
1.80

Suhu B MD_0.6 = 220 subtracted from:


Suhu B
MD_0.6
222

Lower
0.1975

Center
0.3667

Upper
0.5358

---------+---------+---------+---------+
(--*--)
---------+---------+---------+---------+
0.00
0.60
1.20
1.80

LAMPIRAN -6N
5/8/2009 6:04:08 AM
MTB > Oneway 'HS AS Yellow_0.7' 'Suhu B MD_0.7';

Universitas Sumatera Utara

SUBC>

Fisher 5.

One-way ANOVA: HS AS Yellow_0.7 versus Suhu B MD_0.7


Source
Suhu B MD_0.7
Error
Total
S = 0.2047

Level
218
220
222

N
6
6
6

DF
2
15
17

SS
8.8878
0.6283
9.5161

MS
4.4439
0.0419

R-Sq = 93.40%

Mean
4.0000
5.0833
5.7000

StDev
0.1414
0.2137
0.2449

F
106.09

P
0.000

R-Sq(adj) = 92.52%

Individual 95% CIs For Mean Based on


Pooled StDev
------+---------+---------+---------+--(--*--)
(--*--)
(--*--)
------+---------+---------+---------+--4.20
4.80
5.40
6.00

Pooled StDev = 0.2047

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of Suhu B MD_0.7
Simultaneous confidence level = 88.31%

Suhu B MD_0.7 = 218 subtracted from:


Suhu B
MD_0.7
220
222

Lower

Center

Upper

-+---------+---------+---------+-------

0.8315
1.4481

1.0833
1.7000

1.3352
1.9519

(---*--)
(--*--)
-+---------+---------+---------+-------

-0.80

0.00

0.80

1.60

Suhu B MD_0.7 = 220 subtracted from:


Suhu B
MD_0.7
222

Lower

Center

Upper

-+---------+---------+---------+-------

0.3648

0.6167

0.8685

(--*--)
-+---------+---------+---------+-------

-0.80

0.00

0.80

1.60

Universitas Sumatera Utara

LAMPIRAN -6O
7/10/2009 7:46:39 AM

Welcome to Minitab, press F1 for help.


Retrieving project from file: 'C:\Program Files\MINITAB
14\Data\MINITAB.MPJ.23'
MTB > Unstack ( 'IV Umpan' 'HS AS Yellow');
SUBC>
Subscripts 'Suhu B MD';
SUBC>
NewWS;
SUBC>
VarNames.

Results for: Worksheet 8


MTB > Oneway 'HS AS Yellow_218' 'IV Umpan_218';
SUBC>
Fisher 5.

One-way ANOVA: HS AS Yellow_218 versus IV Umpan_218


Source
IV Umpan_218
Error
Total
S = 0.1483

Level
0.6
0.7

N
6
6

DF
1
10
11

SS
0.0300
0.2200
0.2500

MS
0.0300
0.0220

R-Sq = 12.00%

Mean
3.9000
4.0000

StDev
0.1549
0.1414

F
1.36

P
0.270

R-Sq(adj) = 3.20%

Individual 95% CIs For Mean Based on


Pooled StDev
---+---------+---------+---------+-----(------------*------------)
(------------*------------)
---+---------+---------+---------+-----3.80
3.90
4.00
4.10

Pooled StDev = 0.1483

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of IV Umpan_218
Simultaneous confidence level = 95.00%

IV Umpan_218 = 0.6 subtracted from:


IV Umpan_218
+-----0.7

Lower

Center

Upper

---+---------+---------+---------

-0.0908

0.1000

0.2908

(------------*-----------)
---+---------+---------+---------

+------0.15

0.00

0.15

0.30

Universitas Sumatera Utara

LAMPIRAN -6P
MTB > Oneway 'HS AS Yellow_220' 'IV Umpan_220';
SUBC>
Fisher 5.

One-way ANOVA: HS AS Yellow_220 versus IV Umpan_220


Source
IV Umpan_220
Error
Total
S = 0.1835

Level
0.6
0.7

N
6
6

DF
1
10
11

SS
0.0300
0.3367
0.3667

R-Sq = 8.18%

Mean
4.9833
5.0833

StDev
0.1472
0.2137

MS
0.0300
0.0337

F
0.89

P
0.367

R-Sq(adj) = 0.00%

Individual 95% CIs For Mean Based on


Pooled StDev
---------+---------+---------+---------+
(-------------*-------------)
(-------------*-------------)
---------+---------+---------+---------+
4.92
5.04
5.16
5.28

Pooled StDev = 0.1835

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of IV Umpan_220
Simultaneous confidence level = 95.00%

IV Umpan_220 = 0.6 subtracted from:


IV Umpan_220
--+--0.7
----)

Lower

Center

Upper

------+---------+---------+-------

-0.1360

0.1000

0.3360

(---------------*---------------+---------+---------+-------

--+---0.15

0.00

0.15

0.30

Universitas Sumatera Utara

LAMPIRAN -6Q
MTB > Oneway 'HS AS Yellow_222' 'IV Umpan_222';
SUBC>
Fisher 5.

One-way ANOVA: HS AS Yellow_222 versus IV Umpan_222


Source
IV Umpan_222
Error
Total
S = 0.1884

Level
0.6
0.7

N
6
6

DF
1
10
11

SS
0.3675
0.3550
0.7225

MS
0.3675
0.0355

R-Sq = 50.87%

Mean
5.3500
5.7000

StDev
0.1049
0.2449

F
10.35

P
0.009

R-Sq(adj) = 45.95%

Individual 95% CIs For Mean Based on


Pooled StDev
-+---------+---------+---------+-------(--------*-------)
(--------*--------)
-+---------+---------+---------+-------5.20
5.40
5.60
5.80

Pooled StDev = 0.1884

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of IV Umpan_222
Simultaneous confidence level = 95.00%

IV Umpan_222 = 0.6 subtracted from:


IV Umpan_222
0.7

Lower
0.1076

Center
0.3500

Upper
0.5924

IV Umpan_222
0.7

+---------+---------+---------+--------(---------*---------)
+---------+---------+---------+---------0.25
0.00
0.25
0.50

MTB > Save "C:\Program Files\MINITAB 14\Data\MINITAB.MPJ.23";


SUBC>
Project;
SUBC>
Replace.
Saving file as: 'C:\Program Files\MINITAB 14\Data\MINITAB.MPJ.23'
Existing file replaced.
MTB > Save "C:\Program Files\MINITAB 14\Data\MINITAB.MPJ.23";
SUBC>
Project;
SUBC>
Replace.

7/10/2009 8:31:46 PM

Universitas Sumatera Utara

LAMPIRAN 7A
8/17/2009 6:22:32 PM
Welcome to Minitab, press F1 for help.

General Linear Model: AV Residue versus F Umpan, IV Umpan, Suhu BMD


Factor
F Umpan
IV Umpan
Suhu BMD

Type
fixed
fixed
fixed

Levels
3
2
3

Values
5.50, 5.75, 6.00
0.6, 0.7
218, 220, 222

Analysis of Variance for AV Residue, using Adjusted SS for Tests


Source
F Umpan
IV Umpan
Suhu BMD
F Umpan*IV Umpan
F Umpan*Suhu BMD
IV Umpan*Suhu BMD
F Umpan*IV Umpan*Suhu BMD
Error
Total

S = 1.21906

DF
2
1
2
2
4
2
4
18
35

R-Sq = 94.69%

Seq SS
0.344
135.334
294.976
0.341
0.101
45.802
0.288
26.750
503.936

Adj SS
0.344
135.334
294.976
0.341
0.101
45.802
0.288
26.750

Adj MS
0.172
135.334
147.488
0.170
0.025
22.901
0.072
1.486

F
0.12
91.07
99.24
0.11
0.02
15.41
0.05

P
0.891
0.000
0.000
0.892
0.999
0.000
0.995

R-Sq(adj) = 89.68%

Universitas Sumatera Utara

LAMPIRAN 7B
Results for: Worksheet 3
One-way ANOVA: AV Residue_0.6 versus F Umpan_0.6
Source
F Umpan_0.6
Error
Total
S = 1.948

Level
5.50
5.75
6.00

N
6
6
6

DF
2
15
17

SS
0.13
56.94
57.07

MS
0.06
3.80

R-Sq = 0.23%

Mean
25.533
25.733
25.683

StDev
2.023
1.908
1.913

F
0.02

P
0.983

R-Sq(adj) = 0.00%

Individual 95% CIs For Mean Based on


Pooled StDev
--+---------+---------+---------+------(----------------*----------------)
(----------------*----------------)
(----------------*----------------)
--+---------+---------+---------+------24.0
25.0
26.0
27.0

Pooled StDev = 1.948

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of F Umpan_0.6
Simultaneous confidence level = 88.31%

F Umpan_0.6 = 5.50 subtracted from:


F Umpan_0.6
+--5.75
6.00

Lower

Center

Upper

------+---------+---------+---------

-2.197
-2.247

0.200
0.150

2.597
2.547

(---------------*---------------)
(---------------*---------------)
------+---------+---------+---------

+---1.5

0.0

1.5

3.0

F Umpan_0.6 = 5.75 subtracted from:


F Umpan_0.6
+--6.00

Lower

Center

Upper

------+---------+---------+---------

-2.447

-0.050

2.347

(---------------*---------------)
------+---------+---------+---------

+---1.5

0.0

1.5

3.0

Universitas Sumatera Utara

LAMPIRAN 7C
One-way ANOVA: AV Residue_0.7 versus F Umpan_0.7
Source
F Umpan_0.7
Error
Total
S = 4.553

Level
5.50
5.75
6.00

N
6
6
6

DF
2
15
17

SS
0.6
311.0
311.5

R-Sq = 0.18%

Mean
29.467
29.350
29.767

StDev
4.493
4.569
4.597

MS
0.3
20.7

F
0.01

P
0.987

R-Sq(adj) = 0.00%

Individual 95% CIs For Mean Based on


Pooled StDev
--------+---------+---------+---------+(---------------*---------------)
(--------------*---------------)
(---------------*---------------)
--------+---------+---------+---------+27.5
30.0
32.5
35.0

Pooled StDev = 4.553

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of F Umpan_0.7
Simultaneous confidence level = 88.31%

F Umpan_0.7 = 5.50 subtracted from:


F Umpan_0.7
+-5.75
6.00

Lower

Center

Upper

-------+---------+---------+---------

-5.720
-5.303

-0.117
0.300

5.487
5.903

(---------------*---------------)
(---------------*---------------)
-------+---------+---------+---------

+--3.5

0.0

3.5

7.0

F Umpan_0.7 = 5.75 subtracted from:


F Umpan_0.7
+--

Lower

Center

Upper

-------+---------+---------+---------

Universitas Sumatera Utara

6.00

-5.187

0.417

6.020

(---------------*---------------)
-------+---------+---------+---------

+--3.5

0.0

3.5

7.0

LAMPIRAN 7D
Results for: Worksheet 4
One-way ANOVA: AV Residue_5.50 versus IV Umpan_5.50
Source
IV Umpan_5.50
Error
Total
S = 3.484

Level
0.6
0.7

N
6
6

DF
1
10
11

SS
46.4
121.4
167.8

MS
46.4
12.1

R-Sq = 27.66%

Mean
25.533
29.467

StDev
2.023
4.493

F
3.82

P
0.079

R-Sq(adj) = 20.43%

Individual 95% CIs For Mean Based on


Pooled StDev
-----+---------+---------+---------+---(---------*----------)
(---------*----------)
-----+---------+---------+---------+---24.0
27.0
30.0
33.0

Pooled StDev = 3.484

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of IV Umpan_5.50
Simultaneous confidence level = 95.00%

IV Umpan_5.50 = 0.6 subtracted from:


IV Umpan_5.50
----0.7
--)

Lower

Center

Upper

---+---------+---------+---------+-

-0.549

3.933

8.415

(------------*----------

Universitas Sumatera Utara

---+---------+---------+---------+-----3.5

0.0

3.5

7.0

LAMPIRAN 7E
One-way ANOVA: AV Residue_5.75 versus IV Umpan_5.75
Source
IV Umpan_5.75
Error
Total
S = 3.501

DF
1
10
11

SS
39.2
122.6
161.8

MS
39.2
12.3

R-Sq = 24.25%

F
3.20

P
0.104

R-Sq(adj) = 16.67%

Individual 95% CIs For Mean Based on Pooled


StDev
Level
0.6
0.7

N
6
6

Mean
25.733
29.350

StDev
1.908
4.569

+---------+---------+---------+--------(------------*------------)
(-----------*------------)
+---------+---------+---------+--------22.5
25.0
27.5
30.0

Pooled StDev = 3.501

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of IV Umpan_5.75
Simultaneous confidence level = 95.00%

IV Umpan_5.75 = 0.6 subtracted from:


IV Umpan_5.75
----0.7
-)

Lower

Center

Upper

---+---------+---------+---------+-

-0.887

3.617

8.121

(------------*-----------

Universitas Sumatera Utara

---+---------+---------+---------+-----3.5

0.0

3.5

7.0

LAMPIRAN 7F
One-way ANOVA: AV Residue_6.00 versus IV Umpan_6.00
Source
IV Umpan_6.00
Error
Total
S = 3.521

Level
0.6
0.7

N
6
6

DF
1
10
11

SS
50.0
123.9
174.0

MS
50.0
12.4

R-Sq = 28.75%

Mean
25.683
29.767

StDev
1.913
4.597

F
4.04

P
0.072

R-Sq(adj) = 21.63%

Individual 95% CIs For Mean Based on


Pooled StDev
-----+---------+---------+---------+---(----------*---------)
(---------*----------)
-----+---------+---------+---------+---24.0
27.0
30.0
33.0

Pooled StDev = 3.521

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of IV Umpan_6.00
Simultaneous confidence level = 95.00%

IV Umpan_6.00 = 0.6 subtracted from:

Universitas Sumatera Utara

IV Umpan_6.00
----0.7
---)

Lower

Center

Upper

---+---------+---------+---------+-

-0.446

4.083

8.612

(------------*-----------+---------+---------+---------+-

-----3.5

0.0

3.5

7.0

LAMPIRAN 7G
Results for: Worksheet 5
One-way ANOVA: AV Residue_218 versus F Umpan_218
Source
F Umpan_218
Error
Total
S = 4.260

Level
5.50
5.75
6.00

N
4
4
4

DF
2
9
11

SS
0.2
163.3
163.5

R-Sq = 0.11%

MS
0.1
18.1

Mean
31.525
31.575
31.800

StDev
4.200
4.127
4.445

F
0.00

P
0.995

R-Sq(adj) = 0.00%

Individual 95% CIs For Mean Based on


Pooled StDev
---+---------+---------+---------+-----(------------------*------------------)
(------------------*-------------------)
(------------------*------------------)
---+---------+---------+---------+-----27.5
30.0
32.5
35.0

Pooled StDev = 4.260

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of F Umpan_218

Universitas Sumatera Utara

Simultaneous confidence level = 88.66%

F Umpan_218 = 5.50 subtracted from:


F Umpan_218
-+5.75
6.00

Lower

Center

Upper

--------+---------+---------+--------

-6.764
-6.539

0.050
0.275

6.864
7.089

(----------------*----------------)
(----------------*----------------)
--------+---------+---------+--------

-+-4.0

0.0

4.0

8.0

F Umpan_218 = 5.75 subtracted from:


F Umpan_218
-+6.00

Lower

Center

Upper

--------+---------+---------+--------

-6.589

0.225

7.039

(----------------*----------------)
--------+---------+---------+--------

-+-4.0

0.0

4.0

8.0

LAMPIRAN 7H
One-way ANOVA: AV Residue_220 versus F Umpan_220
Source
F Umpan_220
Error
Total
S = 1.547

Level
5.50
5.75
6.00

N
4
4
4

DF
2
9
11

SS
0.21
21.53
21.74

MS
0.11
2.39

R-Sq = 0.97%

Mean
25.550
25.725
25.875

StDev
1.816
1.408
1.377

F
0.04

P
0.957

R-Sq(adj) = 0.00%

Individual 95% CIs For Mean Based on


Pooled StDev
--+---------+---------+---------+------(----------------*-----------------)
(----------------*-----------------)
(-----------------*----------------)
--+---------+---------+---------+------24.0
25.0
26.0
27.0

Universitas Sumatera Utara

Pooled StDev = 1.547

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of F Umpan_220
Simultaneous confidence level = 88.66%

F Umpan_220 = 5.50 subtracted from:


F Umpan_220
+-5.75
6.00

Lower

Center

Upper

-------+---------+---------+---------

-2.299
-2.149

0.175
0.325

2.649
2.799

(---------------*----------------)
(---------------*----------------)
-------+---------+---------+---------

+--1.5

0.0

1.5

3.0

F Umpan_220 = 5.75 subtracted from:


F Umpan_220
+-6.00

Lower

Center

Upper

-------+---------+---------+---------

-2.324

0.150

2.624

(---------------*---------------)
-------+---------+---------+---------

+--1.5

0.0

1.5

3.0

LAMPIRAN 7I
One-way ANOVA: AV Residue_222 versus F Umpan_222
Source
F Umpan_222
Error
Total
S = 1.623

DF
2
9
11

SS
0.06
23.69
23.76

MS
0.03
2.63

R-Sq = 0.26%

F
0.01

P
0.988

R-Sq(adj) = 0.00%

Individual 95% CIs For Mean Based on

Universitas Sumatera Utara

Level
5.50
5.75
6.00

N
4
4
4

Mean
25.425
25.325
25.500

StDev
1.607
1.513
1.740

Pooled StDev
-----+---------+---------+---------+---(-----------------*------------------)
(-----------------*------------------)
(-----------------*-----------------)
-----+---------+---------+---------+---24.0
25.0
26.0
27.0

Pooled StDev = 1.623

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of F Umpan_222
Simultaneous confidence level = 88.66%

F Umpan_222 = 5.50 subtracted from:


F Umpan_222
-+5.75
6.00

Lower

Center

Upper

--------+---------+---------+--------

-2.695
-2.520

-0.100
0.075

2.495
2.670

(----------------*-----------------)
(----------------*-----------------)
--------+---------+---------+--------

-+-1.5

0.0

1.5

3.0

F Umpan_222 = 5.75 subtracted from:


F Umpan_222
-+6.00

Lower

Center

Upper

--------+---------+---------+--------

-2.420

0.175

2.770

(----------------*----------------)
--------+---------+---------+--------

-+-1.5

0.0

1.5

3.0

LAMPIRAN 7J
Results for: Worksheet 4
One-way ANOVA: AV Residue_5.50 versus Suhu BMD_5.50

Universitas Sumatera Utara

Source
Suhu BMD_5.50
Error
Total
S = 2.800

Level
218
220
222

N
4
4
4

DF
2
9
11

SS
97.24
70.56
167.80

R-Sq = 57.95%

Mean
31.525
25.550
25.425

StDev
4.200
1.816
1.607

MS
48.62
7.84

F
6.20

P
0.020

R-Sq(adj) = 48.60%

Individual 95% CIs For Mean Based on


Pooled StDev
------+---------+---------+---------+--(--------*--------)
(--------*--------)
(--------*--------)
------+---------+---------+---------+--24.5
28.0
31.5
35.0

Pooled StDev = 2.800

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of Suhu BMD_5.50
Simultaneous confidence level = 88.66%

Suhu BMD_5.50 = 218 subtracted from:


Suhu
BMD_5.50
-220
222

Lower

Center

Upper

------+---------+---------+---------+-

-10.454
-10.579

-5.975
-6.100

-1.496
-1.621

(----------*----------)
(----------*----------)
------+---------+---------+---------+-

--8.0

-4.0

0.0

4.0

Suhu BMD_5.50 = 220 subtracted from:


Suhu
BMD_5.50
222

Lower
-4.604

Center
-0.125

Upper
4.354

------+---------+---------+---------+--(-----------*----------)
------+---------+---------+---------+---8.0
-4.0
0.0
4.0

LAMPIRAN 7K

Universitas Sumatera Utara

One-way ANOVA: AV Residue_5.75 versus Suhu BMD_5.75


Source
Suhu BMD_5.75
Error
Total
S = 2.665

Level
218
220
222

N
4
4
4

DF
2
9
11

SS
97.93
63.90
161.83

R-Sq = 60.51%

Mean
31.575
25.725
25.325

StDev
4.127
1.408
1.513

MS
48.96
7.10

F
6.90

P
0.015

R-Sq(adj) = 51.74%

Individual 95% CIs For Mean Based on


Pooled StDev
------+---------+---------+---------+--(-------*--------)
(--------*-------)
(-------*--------)
------+---------+---------+---------+--24.5
28.0
31.5
35.0

Pooled StDev = 2.665

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of Suhu BMD_5.75
Simultaneous confidence level = 88.66%

Suhu BMD_5.75 = 218 subtracted from:


Suhu
BMD_5.75
-220
222

Lower

Center

Upper

------+---------+---------+---------+-

-10.112
-10.512

-5.850
-6.250

-1.588
-1.988

(---------*----------)
(---------*----------)
------+---------+---------+---------+-

--8.0

-4.0

0.0

4.0

Suhu BMD_5.75 = 220 subtracted from:


Suhu
BMD_5.75
222

Lower
-4.662

Center
-0.400

Upper
3.862

------+---------+---------+---------+--(----------*----------)
------+---------+---------+---------+---8.0
-4.0
0.0
4.0

Universitas Sumatera Utara

LAMPIRAN 7L
One-way ANOVA: AV Residue_6.00 versus Suhu BMD_6.00
Source
Suhu BMD_6.00
Error
Total
S = 2.868

Level
218
220
222

N
4
4
4

DF
2
9
11

SS
99.91
74.05
173.96

R-Sq = 57.43%

Mean
31.800
25.875
25.500

StDev
4.445
1.377
1.740

MS
49.96
8.23

F
6.07

P
0.021

R-Sq(adj) = 47.98%

Individual 95% CIs For Mean Based on


Pooled StDev
------+---------+---------+---------+--(--------*--------)
(--------*--------)
(--------*--------)
------+---------+---------+---------+--24.5
28.0
31.5
35.0

Pooled StDev = 2.868

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of Suhu BMD_6.00
Simultaneous confidence level = 88.66%

Suhu BMD_6.00 = 218 subtracted from:


Suhu
BMD_6.00
+-220
222

Lower

Center

Upper

-------+---------+---------+---------

-10.513
-10.888

-5.925
-6.300

-1.337
-1.712

(----------*-----------)
(----------*-----------)
-------+---------+---------+---------

+--8.0

-4.0

0.0

4.0

Suhu BMD_6.00 = 220 subtracted from:


Suhu
BMD_6.00
222

Lower
-4.963

Center
-0.375

Upper
4.213

-------+---------+---------+---------+-(----------*-----------)
-------+---------+---------+---------+--8.0
-4.0
0.0
4.0

Universitas Sumatera Utara

LAMPIRAN 7M
Results for: Worksheet 3
One-way ANOVA: AV Residue_0.6 versus Suhu BMD_0.6
Source
Suhu BMD_0.6
Error
Total
S = 0.4398

Level
218
220
222

N
6
6
6

DF
2
15
17

SS
54.163
2.902
57.065

MS
27.082
0.193

R-Sq = 94.92%

Mean
28.100
24.533
24.317

StDev
0.283
0.372
0.601

F
140.00

P
0.000

R-Sq(adj) = 94.24%

Individual 95% CIs For Mean Based on


Pooled StDev
-+---------+---------+---------+-------(--*--)
(--*---)
(---*--)
-+---------+---------+---------+-------24.0
25.2
26.4
27.6

Pooled StDev = 0.440

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of Suhu BMD_0.6
Simultaneous confidence level = 88.31%

Suhu BMD_0.6 = 218 subtracted from:


Suhu
BMD_0.6
--+
220
222

Lower

Center

Upper

---------+---------+---------+-------

-4.1079
-4.3246

-3.5667
-3.7833

-3.0254
-3.2421

(--*---)
(---*--)
---------+---------+---------+-------

--+
-3.0

-1.5

0.0

1.5

Suhu BMD_0.6 = 220 subtracted from:


Suhu
BMD_0.6
-+
222

Lower

Center

Upper

---------+---------+---------+--------

-0.7579

-0.2167

0.3246

(---*--)
---------+---------+---------+--------

-+
-3.0

-1.5

0.0

1.5

Universitas Sumatera Utara

LAMPIRAN 7N
One-way ANOVA: AV Residue_0.7 versus Suhu BMD_0.7
Source
Suhu BMD_0.7
Error
Total
S = 1.289

Level
218
220
222

N
6
6
6

DF
2
15
17

SS
286.61
24.92
311.54

MS
143.31
1.66

R-Sq = 92.00%

Mean
35.167
26.900
26.517

StDev
1.628
0.921
1.219

F
86.25

P
0.000

R-Sq(adj) = 90.93%

Individual 95% CIs For Mean Based on


Pooled StDev
-----+---------+---------+---------+---(---*---)
(---*--)
(--*---)
-----+---------+---------+---------+---27.0
30.0
33.0
36.0

Pooled StDev = 1.289

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of Suhu BMD_0.7
Simultaneous confidence level = 88.31%

Suhu BMD_0.7 = 218 subtracted from:


Suhu
BMD_0.7
+
220
222

Lower

Center

Upper

---------+---------+---------+---------

-9.853
-10.236

-8.267
-8.650

-6.680
-7.064

(---*----)
(---*----)
---------+---------+---------+---------

+
-7.0

-3.5

0.0

3.5

Suhu BMD_0.7 = 220 subtracted from:


Suhu
BMD_0.7
222

Lower
-1.970

Center
-0.383

Upper
1.203

---------+---------+---------+---------+
(----*---)
---------+---------+---------+---------+
-7.0
-3.5
0.0
3.5

Universitas Sumatera Utara

LAMPIRAN 7O
Results for: Worksheet 5
One-way ANOVA: AV Residue_218 versus IV Umpan_218
Source
IV Umpan_218
Error
Total
S = 1.168

Level
0.6
0.7

N
6
6

DF
1
10
11

SS
149.81
13.65
163.47

MS
149.81
1.37

R-Sq = 91.65%

Mean
28.100
35.167

StDev
0.283
1.628

F
109.73

P
0.000

R-Sq(adj) = 90.81%

Individual 95% CIs For Mean Based on


Pooled StDev
--+---------+---------+---------+------(---*----)
(----*---)
--+---------+---------+---------+------27.5
30.0
32.5
35.0

Pooled StDev = 1.168

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of IV Umpan_218
Simultaneous confidence level = 95.00%

IV Umpan_218 = 0.6 subtracted from:


IV Umpan_218
--0.7

Lower

Center

Upper

-----+---------+---------+---------+-

5.564

7.067

8.570

(----*----)
-----+---------+---------+---------+-

--0.0

3.0

6.0

9.0

Universitas Sumatera Utara

LAMPIRAN 7P
One-way ANOVA: AV Residue_220 versus IV Umpan_220
Source
IV Umpan_220
Error
Total
S = 0.7024

Level
0.6
0.7

N
6
6

DF
1
10
11

SS
16.803
4.933
21.737

MS
16.803
0.493

R-Sq = 77.30%

Mean
24.533
26.900

StDev
0.372
0.921

F
34.06

P
0.000

R-Sq(adj) = 75.03%

Individual 95% CIs For Mean Based on


Pooled StDev
-+---------+---------+---------+-------(-----*------)
(-----*-----)
-+---------+---------+---------+-------24.0
25.0
26.0
27.0

Pooled StDev = 0.702

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of IV Umpan_220
Simultaneous confidence level = 95.00%

IV Umpan_220 = 0.6 subtracted from:


IV Umpan_220
---+0.7
)

Lower

Center

Upper

--------+---------+---------+------

1.4631

2.3667

3.2702

(-------*-------------+---------+---------+------

---+0.0

1.2

2.4

3.6

Universitas Sumatera Utara

LAMPIRAN 7Q
One-way ANOVA: AV Residue_222 versus IV Umpan_222
Source
IV Umpan_222
Error
Total
S = 0.9611

Level
0.6
0.7

N
6
6

DF
1
10
11

SS
14.520
9.237
23.757

MS
14.520
0.924

R-Sq = 61.12%

Mean
24.317
26.517

StDev
0.601
1.219

F
15.72

P
0.003

R-Sq(adj) = 57.23%

Individual 95% CIs For Mean Based on


Pooled StDev
------+---------+---------+---------+--(--------*--------)
(--------*--------)
------+---------+---------+---------+--24.0
25.0
26.0
27.0

Pooled StDev = 0.961

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of IV Umpan_222
Simultaneous confidence level = 95.00%

IV Umpan_222 = 0.6 subtracted from:


IV Umpan_222
0.7

Lower
0.9637

Center
2.2000

Upper
3.4363

IV Umpan_222
0.7

+---------+---------+---------+--------(---------*----------)
+---------+---------+---------+---------1.2
0.0
1.2
2.4

Universitas Sumatera Utara

LAMPIRAN 8A
12/18/2009 11:03:21 PM
Welcome to Minitab, press F1 for help.

General Linear Model: Res Yield versus F Umpan, IV Umpan, Suhu MD


Factor
F Umpan
IV Umpan
Suhu MD

Type
fixed
fixed
fixed

Levels
3
2
3

Values
5.50, 5.75, 6.00
0.6, 0.7
218, 220, 222

Analysis of Variance for Res Yield, using Adjusted SS for Tests


Source
F Umpan
IV Umpan
Suhu MD
F Umpan*IV Umpan
F Umpan*Suhu MD
IV Umpan*Suhu MD
F Umpan*IV Umpan*Suhu MD
Error
Total

S = 1.12607

DF
2
1
2
2
4
2
4
18
35

R-Sq = 99.43%

Seq SS
3534.34
178.53
261.07
0.08
11.89
6.85
1.61
22.82
4017.21

Adj SS
3534.34
178.53
261.07
0.08
11.89
6.85
1.61
22.82

Adj MS
1767.17
178.53
130.54
0.04
2.97
3.43
0.40
1.27

F
1393.64
140.80
102.94
0.03
2.35
2.70
0.32

P
0.000
0.000
0.000
0.967
0.094
0.094
0.862

R-Sq(adj) = 98.90%

Unusual Observations for Res Yield


Obs
7
8

Res Yield
280.600
277.000

Fit
278.800
278.800

SE Fit
0.796
0.796

Residual
1.800
-1.800

St Resid
2.26 R
-2.26 R

Universitas Sumatera Utara

R denotes an observation with a large standardized residual.

LAMPIRAN 8B
Results for: Worksheet 2
One-way ANOVA: Res Yield_0.6 versus F Umpan_0.6
Source
F Umpan_0.6
Error
Total
S = 2.737

Level
5.50
5.75
6.00

N
6
6
6

DF
2
15
17

SS
1752.48
112.34
1864.83

MS
876.24
7.49

R-Sq = 93.98%

Mean
276.35
288.75
300.52

StDev
2.31
3.35
2.43

F
117.00

P
0.000

R-Sq(adj) = 93.17%

Individual 95% CIs For Mean Based on


Pooled StDev
--------+---------+---------+---------+(--*--)
(--*--)
(--*--)
--------+---------+---------+---------+280.0
288.0
296.0
304.0

Pooled StDev = 2.74

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of F Umpan_0.6
Simultaneous confidence level = 88.31%

F Umpan_0.6 = 5.50 subtracted from:


F Umpan_0.6
----

Lower

Center

Upper

---+---------+---------+---------+--

Universitas Sumatera Utara

5.75
6.00
)

9.032
20.799

12.400
24.167

15.768
27.534

(-*--)
(--*----+---------+---------+---------+--

----12

12

24

F Umpan_0.6 = 5.75 subtracted from:


F Umpan_0.6
--6.00

Lower

Center

Upper

---+---------+---------+---------+---

8.399

11.767

15.134

(--*--)
---+---------+---------+---------+---

---12

12

24

LAMPIRAN 8C
One-way ANOVA: Res Yield_0.7 versus F Umpan_0.7
Source
F Umpan_0.7
Error
Total
S = 3.577

Level
5.50
5.75
6.00

N
6
6
6

DF
2
15
17

SS
1781.9
191.9
1973.8

MS
891.0
12.8

R-Sq = 90.28%

Mean
280.67
293.28
305.03

StDev
3.01
4.46
3.07

F
69.64

P
0.000

R-Sq(adj) = 88.98%

Individual 95% CIs For Mean Based on


Pooled StDev
---+---------+---------+---------+-----(---*---)
(---*--)
(---*---)
---+---------+---------+---------+-----280.0
288.0
296.0
304.0

Pooled StDev = 3.58

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of F Umpan_0.7
Simultaneous confidence level = 88.31%

F Umpan_0.7 = 5.50 subtracted from:

Universitas Sumatera Utara

F Umpan_0.7
---5.75
6.00
-)

Lower

Center

Upper

8.210
19.965

12.612
24.367

17.013
28.768

---+---------+---------+---------+-(---*--)
(--*----+---------+---------+---------+--

----12

12

24

F Umpan_0.7 = 5.75 subtracted from:


F Umpan_0.7
--6.00

Lower

Center

Upper

---+---------+---------+---------+---

7.353

11.755

16.157

(---*--)
---+---------+---------+---------+---

---12

12

24

LAMPIRAN 8D
Results for: Worksheet 3
One-way ANOVA: Res Yield_5.50 versus IV Umpan_5.50
Source
IV Umpan_5.50
Error
Total
S = 2.683

Level
0.6
0.7

N
6
6

DF
1
10
11

SS
55.90
72.01
127.91

R-Sq = 43.70%

Mean
276.35
280.67

StDev
2.31
3.01

MS
55.90
7.20

F
7.76

P
0.019

R-Sq(adj) = 38.07%

Individual 95% CIs For Mean Based on


Pooled StDev
----+---------+---------+---------+----(--------*---------)
(---------*--------)
----+---------+---------+---------+----275.0
277.5
280.0
282.5

Pooled StDev = 2.68

Fisher 95% Individual Confidence Intervals

Universitas Sumatera Utara

All Pairwise Comparisons among Levels of IV Umpan_5.50


Simultaneous confidence level = 95.00%

IV Umpan_5.50 = 0.6 subtracted from:


IV Umpan_5.50
----0.7
---)

Lower

Center

Upper

--+---------+---------+---------+--

0.865

4.317

7.769

(----------*---------+---------+---------+---------+--

-----3.0

0.0

3.0

6.0

LAMPIRAN 8E
One-way ANOVA: Res Yield_5.75 versus IV Umpan_5.75
Source
IV Umpan_5.75
Error
Total
S = 3.947

Level
0.6
0.7

N
6
6

DF
1
10
11

SS
61.5
155.8
217.3

MS
61.5
15.6

R-Sq = 28.31%

Mean
288.75
293.28

StDev
3.35
4.46

F
3.95

P
0.075

R-Sq(adj) = 21.14%

Individual 95% CIs For Mean Based on


Pooled StDev
---------+---------+---------+---------+
(-----------*----------)
(-----------*-----------)
---------+---------+---------+---------+
288.0
291.0
294.0
297.0

Pooled StDev = 3.95

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of IV Umpan_5.75

Universitas Sumatera Utara

Simultaneous confidence level = 95.00%

IV Umpan_5.75 = 0.6 subtracted from:


IV Umpan_5.75
----0.7
--)

Lower

Center

Upper

---+---------+---------+---------+-

-0.549

4.528

9.605

(-----------*------------+---------+---------+---------+-

-----4.0

0.0

4.0

8.0

LAMPIRAN 8F
One-way ANOVA: Res Yield_6.00 versus IV Umpan_6.00
Source
IV Umpan_6.00
Error
Total
S = 2.766

Level
0.6
0.7

N
6
6

DF
1
10
11

SS
61.20
76.48
137.68

R-Sq = 44.45%

Mean
300.52
305.03

StDev
2.43
3.07

MS
61.20
7.65

F
8.00

P
0.018

R-Sq(adj) = 38.90%

Individual 95% CIs For Mean Based on


Pooled StDev
--------+---------+---------+---------+(---------*---------)
(---------*---------)
--------+---------+---------+---------+300.0
302.5
305.0
307.5

Pooled StDev = 2.77

Universitas Sumatera Utara

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of IV Umpan_6.00
Simultaneous confidence level = 95.00%

IV Umpan_6.00 = 0.6 subtracted from:


IV Umpan_6.00
----0.7
----)

Lower

Center

Upper

--+---------+---------+---------+--

0.959

4.517

8.074

(-----------*--------+---------+---------+---------+--

-----3.0

0.0

3.0

6.0

LAMPIRAN 8G
Results for: Worksheet 4
One-way ANOVA: Res Yield_218 versus F Umpan_218
Source
F Umpan_218
Error
Total
S = 3.471

Level
5.50
5.75

N
4
4

DF
2
9
11

SS
1183.0
108.4
1291.4

MS
591.5
12.0

R-Sq = 91.60%

Mean
281.40
295.38

StDev
3.44
3.62

F
49.09

P
0.000

R-Sq(adj) = 89.74%

Individual 95% CIs For Mean Based on


Pooled StDev
---+---------+---------+---------+-----(---*---)
(---*---)

Universitas Sumatera Utara

6.00

305.63

3.35

(---*---)
---+---------+---------+---------+-----300
310
280
290

Pooled StDev = 3.47

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of F Umpan_218
Simultaneous confidence level = 88.66%

F Umpan_218 = 5.50 subtracted from:


F Umpan_218
---5.75
6.00
--)

Lower

Center

Upper

---+---------+---------+---------+--

8.423
18.673

13.975
24.225

19.527
29.777

(----*---)
(---*----+---------+---------+---------+--

----12

12

24

F Umpan_218 = 5.75 subtracted from:


F Umpan_218
--6.00

Lower

Center

Upper

---+---------+---------+---------+---

4.698

10.250

15.802

(----*---)
---+---------+---------+---------+---

---12

12

24

LAMPIRAN 8H
One-way ANOVA: Res Yield_220 versus F Umpan_220
Source
F Umpan_220
Error
Total
S = 2.477

Level

DF
2
9
11

SS
1237.62
55.20
1292.82

MS
618.81
6.13

R-Sq = 95.73%

Mean

StDev

F
100.89

P
0.000

R-Sq(adj) = 94.78%

Individual 95% CIs For Mean Based on


Pooled StDev
------+---------+---------+---------+---

Universitas Sumatera Utara

5.50
5.75
6.00

4
4
4

278.13
290.74
303.00

2.78
2.42
2.19

(---*--)
(--*---)
(---*--)
------+---------+---------+---------+--280.0
288.0
296.0
304.0

Pooled StDev = 2.48

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of F Umpan_220
Simultaneous confidence level = 88.66%

F Umpan_220 = 5.50 subtracted from:


F Umpan_220
---5.75
6.00
*--)

Lower

Center

Upper

8.656
20.913

12.618
24.875

16.579
28.837

----+---------+---------+---------+(---*--)
(------+---------+---------+---------+-

----12

12

24

F Umpan_220 = 5.75 subtracted from:


F Umpan_220
--6.00

Lower

Center

Upper

----+---------+---------+---------+--

8.296

12.257

16.219

(--*---)
----+---------+---------+---------+--

---12

12

24

LAMPIRAN 8I
One-way ANOVA: Res Yield_222 versus F Umpan_222
Source
F Umpan_222
Error
Total

DF
2
9
11

SS
1125.66
46.27
1171.93

MS
562.83
5.14

F
109.47

P
0.000

Universitas Sumatera Utara

S = 2.267

Level
5.50
5.75
6.00

N
4
4
4

R-Sq = 96.05%

Mean
276.00
286.93
299.70

StDev
1.83
2.39
2.52

R-Sq(adj) = 95.17%

Individual 95% CIs For Mean Based on


Pooled StDev
--------+---------+---------+---------+(--*--)
(---*--)
(---*--)
--------+---------+---------+---------+304.0
280.0
288.0
296.0

Pooled StDev = 2.27

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of F Umpan_222
Simultaneous confidence level = 88.66%

F Umpan_222 = 5.50 subtracted from:


F Umpan_222
---5.75
6.00
-)

Lower

Center

Upper

7.298
20.073

10.925
23.700

14.552
27.327

----+---------+---------+---------+(--*--)
(--*----+---------+---------+---------+-

----12

12

24

F Umpan_222 = 5.75 subtracted from:


F Umpan_222
--6.00

Lower

Center

Upper

----+---------+---------+---------+--

9.148

12.775

16.402

(--*--)
----+---------+---------+---------+--

---12

12

24

LAMPIRAN 8J
Results for: Worksheet 5
One-way ANOVA: Res Yield_5.50 versus Suhu MD_5.50

Universitas Sumatera Utara

Source
Suhu MD_5.50
Error
Total
S = 2.763

DF
2
9
11

SS
59.20
68.71
127.91

MS
29.60
7.63

R-Sq = 46.28%

F
3.88

P
0.061

R-Sq(adj) = 34.35%

Individual 95% CIs For Mean Based on Pooled


StDev
Level
218
220
222

N
4
4
4

Mean
281.40
278.13
276.00

StDev
3.44
2.78
1.83

+---------+---------+---------+--------(---------*---------)
(---------*----------)
(---------*---------)
+---------+---------+---------+--------273.0
276.0
279.0
282.0

Pooled StDev = 2.76

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of Suhu MD_5.50
Simultaneous confidence level = 88.66%

Suhu MD_5.50 = 218 subtracted from:


Suhu
MD_5.50
---220
222

Lower

Center

Upper

+---------+---------+---------+-----

-7.695
-9.820

-3.275
-5.400

1.145
-0.980

(-------*--------)
(--------*--------)
+---------+---------+---------+-----

----10.0

-5.0

0.0

5.0

Suhu MD_5.50 = 220 subtracted from:


Suhu
MD_5.50
--222

Lower

Center

Upper

+---------+---------+---------+------

-6.545

-2.125

2.295

(--------*--------)
+---------+---------+---------+------

---10.0

-5.0

0.0

5.0

LAMPIRAN 8K

Universitas Sumatera Utara

One-way ANOVA: Res Yield_5.75 versus Suhu MD_5.75


Source
Suhu MD_5.75
Error
Total
S = 2.868

Level
218
220
222

N
4
4
4

DF
2
9
11

SS
143.25
74.03
217.28

MS
71.62
8.23

R-Sq = 65.93%

Mean
295.38
290.74
286.93

StDev
3.62
2.42
2.39

F
8.71

P
0.008

R-Sq(adj) = 58.36%

Individual 95% CIs For Mean Based on Pooled


StDev
-+---------+---------+---------+-------(-------*--------)
(-------*-------)
(-------*-------)
-+---------+---------+---------+-------284.0
288.0
292.0
296.0

Pooled StDev = 2.87

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of Suhu MD_5.75
Simultaneous confidence level = 88.66%

Suhu MD_5.75 = 218 subtracted from:


Suhu
MD_5.75
--220
222

Lower

Center

Upper

--+---------+---------+---------+----

-9.220
-13.038

-4.632
-8.450

-0.045
-3.862

(------*-------)
(-------*-------)
--+---------+---------+---------+----

---12.0

-6.0

0.0

6.0

Suhu MD_5.75 = 220 subtracted from:


Suhu
MD_5.75
222

Lower

Center

Upper

--+---------+---------+---------+------

-8.405

-3.818

0.770

(-------*------)
--+---------+---------+---------+------

-12.0

-6.0

0.0

6.0

Universitas Sumatera Utara

LAMPIRAN 8L
One-way ANOVA: Res Yield_6.00 versus Suhu MD_6.00
Source
Suhu MD_6.00
Error
Total
S = 2.732

Level
218
220
222

N
4
4
4

DF
2
9
11

SS
70.52
67.17
137.68

MS
35.26
7.46

R-Sq = 51.22%

Mean
305.63
303.00
299.70

StDev
3.35
2.19
2.52

F
4.72

P
0.040

R-Sq(adj) = 40.37%

Individual 95% CIs For Mean Based on


Pooled StDev
---+---------+---------+---------+-----(--------*--------)
(--------*--------)
(--------*--------)
---+---------+---------+---------+-----297.5
301.0
304.5
308.0

Pooled StDev = 2.73

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of Suhu MD_6.00
Simultaneous confidence level = 88.66%

Suhu MD_6.00 = 218 subtracted from:


Suhu
MD_6.00
---220
222

Lower

Center

Upper

-+---------+---------+---------+----

-6.995
-10.295

-2.625
-5.925

1.745
-1.555

(--------*-------)
(--------*--------)
-+---------+---------+---------+----

----10.0

-5.0

0.0

5.0

Suhu MD_6.00 = 220 subtracted from:


Suhu
MD_6.00
-222

Lower

Center

Upper

-+---------+---------+---------+------

-7.670

-3.300

1.070

(-------*--------)
-+---------+---------+---------+------

--10.0

-5.0

0.0

5.0

Universitas Sumatera Utara

LAMPIRAN 8M
Results for: Worksheet 6
One-way ANOVA: Res Yield_0.6 versus Suhu MD_0.6
Source
Suhu MD_0.6
Error
Total
S = 10.87

Level
218
220
222

N
6
6
6

DF
2
15
17

SS
92
1772
1865

MS
46
118

R-Sq = 4.96%

Mean
291.32
288.53
285.77

StDev
10.82
11.39
10.38

F
0.39

P
0.683

R-Sq(adj) = 0.00%

Individual 95% CIs For Mean Based on


Pooled StDev
-----+---------+---------+---------+---(------------*-------------)
(------------*-------------)
(------------*-------------)
-----+---------+---------+---------+---280.0
287.0
294.0
301.0

Pooled StDev = 10.87

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of Suhu MD_0.6
Simultaneous confidence level = 88.31%

Suhu MD_0.6 = 218 subtracted from:


Suhu
MD_0.6
220
222

Lower
-16.16
-18.93

Center
-2.78
-5.55

Upper
10.59
7.83

---------+---------+---------+---------+
(------------*-------------)
(------------*-------------)
---------+---------+---------+---------+
-10
0
10
20

Suhu MD_0.6 = 220 subtracted from:


Suhu
MD_0.6
222

Lower
-16.14

Center
-2.77

Upper
10.61

---------+---------+---------+---------+
(------------*-------------)
---------+---------+---------+---------+
-10
0
10
20

Universitas Sumatera Utara

LAMPIRAN 8N
One-way ANOVA: Res Yield_0.7 versus Suhu MD_0.7
Source
Suhu MD_0.7
Error
Total
S = 10.95

DF
2
15
17

SS
176
1798
1974

MS
88
120

R-Sq = 8.89%

F
0.73

P
0.497

R-Sq(adj) = 0.00%

Individual 95% CIs For Mean Based on Pooled


StDev
Level
218
220
222

N
6
6
6

Mean
296.95
292.71
289.32

StDev
11.05
10.88
10.92

+---------+---------+---------+--------(------------*-------------)
(------------*-------------)
(------------*-------------)
+---------+---------+---------+--------280.0
287.0
294.0
301.0

Pooled StDev = 10.95

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of Suhu MD_0.7
Simultaneous confidence level = 88.31%

Suhu MD_0.7 = 218 subtracted from:


Suhu
MD_0.7
220
222

Lower
-17.71
-21.11

Center
-4.24
-7.63

Upper
9.24
5.84

-+---------+---------+---------+-------(-------------*------------)
(------------*-------------)
-+---------+---------+---------+--------20
-10
0
10

Suhu MD_0.7 = 220 subtracted from:


Suhu
MD_0.7
222

Lower
-16.87

Center
-3.40

Upper
10.08

-+---------+---------+---------+-------(-------------*------------)
-+---------+---------+---------+--------20
-10
0
10

Universitas Sumatera Utara

LAMPIRAN 8O
Results for: Worksheet 7
One-way ANOVA: Res Yield_218 versus IV Umpan_218
Source
IV Umpan_218
Error
Total
S = 10.94

Level
0.6
0.7

N
6
6

DF
1
10
11

SS
95
1196
1291

MS
95
120

R-Sq = 7.37%

Mean
291.32
296.95

StDev
10.82
11.05

F
0.80

P
0.393

R-Sq(adj) = 0.00%

Individual 95% CIs For Mean Based on


Pooled StDev
--------+---------+---------+---------+(-------------*-------------)
(-------------*-------------)
--------+---------+---------+---------+287.0
294.0
301.0
308.0

Pooled StDev = 10.94

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of IV Umpan_218
Simultaneous confidence level = 95.00%

IV Umpan_218 = 0.6 subtracted from:


IV Umpan_218
--0.7

Lower

Center

Upper

----+---------+---------+---------+--

-8.44

5.63

19.70

(-------------*-------------)
----+---------+---------+---------+--

---10

10

20

Universitas Sumatera Utara

LAMPIRAN 8P
One-way ANOVA: Res Yield_220 versus IV Umpan_220
Source
IV Umpan_220
Error
Total
S = 11.14

Level
0.6
0.7

N
6
6

DF
1
10
11

SS
52
1240
1293

MS
52
124

R-Sq = 4.05%

Mean
288.53
292.71

StDev
11.39
10.88

F
0.42

P
0.530

R-Sq(adj) = 0.00%

Individual 95% CIs For Mean Based on


Pooled StDev
--+---------+---------+---------+------(-------------*--------------)
(-------------*--------------)
--+---------+---------+---------+------280.0
287.0
294.0
301.0

Pooled StDev = 11.14

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of IV Umpan_220
Simultaneous confidence level = 95.00%

IV Umpan_220 = 0.6 subtracted from:


IV Umpan_220
---0.7

Lower

Center

Upper

----+---------+---------+---------+-

-10.15

4.18

18.51

(-------------*--------------)
----+---------+---------+---------+-

----10

10

20

Universitas Sumatera Utara

LAMPIRAN 8Q
One-way ANOVA: Res Yield_222 versus IV Umpan_222
Source
IV Umpan_222
Error
Total
S = 10.65

DF
1
10
11

SS
38
1134
1172

MS
38
113

R-Sq = 3.23%

F
0.33

P
0.576

R-Sq(adj) = 0.00%

Individual 95% CIs For Mean Based on Pooled


StDev
Level
0.6
0.7

N
6
6

Mean
285.77
289.32

StDev
10.38
10.92

+---------+---------+---------+--------(---------------*---------------)
(---------------*---------------)
+---------+---------+---------+--------276.0
282.0
288.0
294.0

Pooled StDev = 10.65

Fisher 95% Individual Confidence Intervals


All Pairwise Comparisons among Levels of IV Umpan_222
Simultaneous confidence level = 95.00%

IV Umpan_222 = 0.6 subtracted from:


IV Umpan_222
-+-0.7
---)

Lower

Center

Upper

-------+---------+---------+--------

-10.15

3.55

17.25

(----------------*--------------------+---------+---------+--------

-+--8.0

0.0

8.0

16.0

12/19/2009 11:02:00 PM

Universitas Sumatera Utara

LAMPIRAN -9A

PENGOLAHAN DATA SPC


Tabel L8. Tabel SPC Yield DAS.
Pengukuran

Sub

Range

STD
BKA

BKB

0.02

90.806

90.781

0.14

90.806

90.781

0.05

0.01

90.806

90.781

0.02

90.836

90.751

0.05

0.04

90.806

90.781

0.02

90.836

90.751

0.03

0.05

0.01

90.806

90.781

0.02

90.836

90.751

0.04

0.05

0.02

90.806

90.781

0.02

90.836

90.751

0.02

0.05

0.01

90.806

90.781

0.02

90.836

90.751

90.794

0.06

0.05

0.03

90.806

90.781

0.02

90.836

90.751

90.794

0.09

0.05

0.05

90.806

90.781

0.02

90.836

90.751

X1

X2

DEV

Grup

X1

X2

X3

X4

90.78

90.77

90.81

90.78

90.785

90.794

0.03

0.05

91.00

90.74

90.73

90.72

90.798

90.794

0.28

0.05

90.80

90.80

90.78

90.80

90.795

90.794

0.02

90.79

90.73

90.83

90.80

90.788

90.794

0.03

90.78

90.79

90.80

90.81

90.795

90.794

90.77

90.78

90.81

90.80

90.790

90.794

90.78

90.80

90.79

90.80

90.793

90.794

90.83

90.80

90.77

90.79

90.798

90.87

90.78

90.77

90.78

90.800

BKA

BKB

0.02

90.836

90.751

0.02

90.836

90.751

10

90.78

90.79

90.78

90.83

90.795

90.794

0.05

0.05

0.02

90.806

90.781

0.02

90.836

90.751

11

90.81

90.79

90.78

90.80

90.795

90.794

0.03

0.05

0.01

90.806

90.781

0.02

90.836

90.751

12

90.77

90.80

90.81

90.80

90.795

90.794

0.04

0.05

0.02

90.806

90.781

0.02

90.836

90.751

13

90.80

90.80

90.79

90.80

90.798

90.794

0.01

0.05

0.00

90.806

90.781

0.02

90.836

90.751

14

90.79

90.78

90.79

90.80

90.790

90.794

0.01

0.05

0.01

90.806

90.781

0.02

90.836

90.751

15

90.76

90.80

90.80

90.82

90.795

90.794

0.06

0.05

0.03

90.806

90.781

0.02

90.836

90.751

16

90.80

90.81

90.76

90.84

90.803

90.794

0.08

0.05

0.03

90.806

90.781

0.02

90.836

90.751

17

90.81

90.76

90.78

90.80

90.788

90.794

0.05

0.05

0.02

90.806

90.781

0.02

90.836

90.751

18

90.80

90.78

90.79

90.80

90.793

90.794

0.02

0.05

0.01

90.806

90.781

0.02

90.836

90.751

19

90.80

90.79

90.78

90.80

90.793

90.794

0.02

0.05

0.01

90.806

90.781

0.02

90.836

90.751

20

90.80

90.80

90.80

90.78

90.795

90.794

0.02

0.05

0.01

90.806

90.781

0.02

90.836

90.751

21

90.80

90.77

90.78

90.79

90.785

90.794

0.03

0.05

0.01

90.806

90.781

0.02

90.836

90.751

22

90.80

90.79

90.77

90.80

90.790

90.794

0.03

0.05

0.01

90.806

90.781

0.02

90.836

90.751

23

90.78

90.78

90.81

90.81

90.795

90.794

0.03

0.05

0.02

90.806

90.781

0.02

90.836

90.751

Universitas Sumatera Utara

24

90.83

90.79

90.80

90.77

90.798

90.794

0.06

0.05

0.03

90.806

90.781

0.02

90.836

90.751

25

90.79

90.79

90.79

90.80

90.793

90.794

0.01

0.05

0.00

90.806

90.781

0.02

90.836

90.751

Untuk X SPC :

Untuk S SPC :

X1= 2269.8 R = 1.15

S = 0.57

X2 = 90.7935 R = 0.05

S = 0.02

n=4

A1 = 1.88

A2 = 0,279

BKA = X2 + A2R = 90.806

BKA = X2 + A1S = 90.836

BKB = X2 A2R = 90.781

BKA = X2 A1S = 90.751

LAMPIRAN -9B

PENGOLAHAN DATA SPC


Tabel L9. Data SPC Bilangan Iodium DAS
Pengukuran

Sub
Grup

X1

X2

X3

Range
X4

X1

X2

STD
R

BKA

BKB

DEV

BKA

BKB

0.18

0.18

0.17

0.17

0.175

0.1741

0.01

0.01

0.01

0.178

0.170

0.01

0.188

0.161

0.17

0.17

0.18

0.18

0.175

0.1741

0.01

0.01

0.01

0.178

0.170

0.01

0.188

0.161

0.18

0.17

0.17

0.18

0.175

0.1741

0.01

0.01

0.01

0.178

0.170

0.01

0.188

0.161

0.17

0.16

0.18

0.18

0.173

0.1741

0.02

0.01

0.01

0.178

0.170

0.01

0.188

0.161

0.18

0.16

0.18

0.18

0.175

0.1741

0.02

0.01

0.01

0.178

0.170

0.01

0.188

0.161

0.18

0.18

0.17

0.17

0.175

0.1741

0.01

0.01

0.01

0.178

0.170

0.01

0.188

0.161

0.18

0.17

0.18

0.17

0.175

0.1741

0.01

0.01

0.01

0.178

0.170

0.01

0.188

0.161

0.18

0.17

0.17

0.17

0.173

0.1741

0.01

0.01

0.00

0.178

0.170

0.01

0.188

0.161

0.17

0.17

0.17

0.18

0.173

0.1741

0.01

0.01

0.00

0.178

0.170

0.01

0.188

0.161

10

0.17

0.17

0.18

0.18

0.175

0.1741

0.01

0.01

0.01

0.178

0.170

0.01

0.188

0.161

11

0.17

0.18

0.17

0.18

0.175

0.1741

0.01

0.01

0.01

0.178

0.170

0.01

0.188

0.161

12

0.18

0.17

0.17

0.17

0.173

0.1741

0.01

0.01

0.00

0.178

0.170

0.01

0.188

0.161

13

0.17

0.17

0.18

0.18

0.175

0.1741

0.01

0.01

0.01

0.178

0.170

0.01

0.188

0.161

14

0.17

0.17

0.18

0.17

0.173

0.1741

0.01

0.01

0.00

0.178

0.170

0.01

0.188

0.161

15

0.18

0.18

0.16

0.18

0.175

0.1741

0.02

0.01

0.01

0.178

0.170

0.01

0.188

0.161

16

0.18

0.18

0.17

0.16

0.173

0.1741

0.02

0.01

0.01

0.178

0.170

0.01

0.188

0.161

17

0.18

0.17

0.16

0.18

0.173

0.1741

0.01

0.01

0.01

0.178

0.170

0.01

0.188

0.161

18

0.17

0.18

0.17

0.17

0.173

0.1741

0.01

0.01

0.00

0.178

0.170

0.01

0.188

0.161

19

0.18

0.18

0.18

0.16

0.175

0.1741

0.02

0.01

0.01

0.178

0.170

0.01

0.188

0.161

20

0.16

0.18

0.18

0.18

0.175

0.1741

0.02

0.01

0.01

0.178

0.170

0.01

0.188

0.161

21

0.17

0.18

0.18

0.16

0.173

0.1741

0.02

0.01

0.01

0.178

0.170

0.01

0.188

0.161

22

0.18

0.18

0.17

0.18

0.178

0.1741

0.01

0.01

0.00

0.178

0.170

0.01

0.188

0.161

Universitas Sumatera Utara

23

0.18

0.17

0.18

0.17

0.175

0.1741

0.01

0.01

0.01

0.178

0.170

0.01

0.188

0.161

24

0.16

0.18

0.18

0.18

0.175

0.1741

0.02

0.01

0.01

0.178

0.170

0.01

0.188

0.161

25

0.18

0.16

0.17

0.18

0.173

0.1741

0.02

0.01

0.01

0.178

0.170

0.01

0.188

0.161

Untuk X SPC :

Untuk S SPC :

X1= 4.4

R = 0.3

S = 0.18

X2 = 0.174

R = 0.01

S = 0.01

n=4

A2 = 0,279

A1 = 1.88

BKA = X2 + A2R = 0.178

BKA = X2 + A1S = 0.188

BKB = X2 A2R = 0.170

BKA = X2 A1S = 0.161

LAMPIRAN - 9C

PENGOLAHAN DATA SPC


Tabel L10. Data SPC Heat StabilityRed DAS
Pengukuran

Sub
Grup

X1

Range

X2

X3

X4

X1

X2

STD
R

BKA

BKB

DEV

BKA

BKB

0.5

0.5

0.6

0.6

0.550

0.558

0.100

0.096

0.06

0.585

0.531

0.055

0.662

0.454

0.6

0.5

0.6

0.5

0.550

0.558

0.100

0.096

0.06

0.585

0.531

0.055

0.662

0.454

0.6

0.5

0.6

0.5

0.550

0.558

0.100

0.096

0.06

0.585

0.531

0.055

0.662

0.454

0.5

0.6

0.5

0.6

0.550

0.558

0.100

0.096

0.06

0.585

0.531

0.055

0.662

0.454

0.6

0.5

0.6

0.5

0.550

0.558

0.100

0.096

0.06

0.585

0.531

0.055

0.662

0.454

0.6

0.5

0.6

0.5

0.550

0.558

0.100

0.096

0.06

0.585

0.531

0.055

0.662

0.454

0.6

0.5

0.6

0.6

0.575

0.558

0.100

0.096

0.05

0.585

0.531

0.055

0.662

0.454

0.6

0.5

0.6

0.6

0.575

0.558

0.100

0.096

0.05

0.585

0.531

0.055

0.662

0.454

0.6

0.5

0.5

0.6

0.550

0.558

0.100

0.096

0.06

0.585

0.531

0.055

0.662

0.454

10

0.5

0.6

0.5

0.6

0.550

0.558

0.100

0.096

0.06

0.585

0.531

0.055

0.662

0.454

11

0.5

0.5

0.6

0.6

0.550

0.558

0.100

0.096

0.06

0.585

0.531

0.055

0.662

0.454

12

0.6

0.5

0.5

0.6

0.550

0.558

0.100

0.096

0.06

0.585

0.531

0.055

0.662

0.454

13

0.6

0.5

0.6

0.5

0.550

0.558

0.100

0.096

0.06

0.585

0.531

0.055

0.662

0.454

14

0.6

0.5

0.6

0.6

0.575

0.558

0.100

0.096

0.05

0.585

0.531

0.055

0.662

0.454

15

0.6

0.5

0.6

0.6

0.575

0.558

0.100

0.096

0.05

0.585

0.531

0.055

0.662

0.454

16

0.6

0.5

0.6

0.5

0.550

0.558

0.100

0.096

0.06

0.585

0.531

0.055

0.662

0.454

17

0.5

0.6

0.6

0.6

0.575

0.558

0.100

0.096

0.05

0.585

0.531

0.055

0.662

0.454

18

0.5

0.6

0.5

0.6

0.550

0.558

0.100

0.096

0.06

0.585

0.531

0.055

0.662

0.454

19

0.5

0.6

0.5

0.6

0.550

0.558

0.100

0.096

0.06

0.585

0.531

0.055

0.662

0.454

20

0.5

0.6

0.6

0.6

0.575

0.558

0.000

0.096

0.05

0.585

0.531

0.055

0.662

0.454

21

0.6

0.6

0.6

0.5

0.575

0.558

0.100

0.096

0.05

0.585

0.531

0.055

0.662

0.454

Universitas Sumatera Utara

22

0.6

0.6

0.5

0.6

0.575

0.558

0.100

0.096

0.05

0.585

0.531

0.055

0.662

0.454

23

0.6

0.5

0.5

0.6

0.550

0.558

0.100

0.096

0.06

0.585

0.531

0.055

0.662

0.454

24

0.6

0.5

0.6

0.5

0.550

0.558

0.100

0.096

0.06

0.585

0.531

0.055

0.662

0.454

25

0.6

0.6

0.5

0.5

0.550

0.558

0.100

0.096

0.06

0.585

0.531

0.055

0.662

0.454

Untuk X SPC :

Untuk S SPC :

X1= 14.0

R = 2.4

S = 1.38

X2 = 0.558

R = 0.096

S = 0.06

n=4

A2 = 0,279

A1 = 1.88

BKA = X2 + A2R = 0.585

BKA = X2 + A1S = 0.662

BKB = X2 A2R = 0.531

BKA = X2 A1S = 0.454

LAMPIRAN -9D

PENGOLAHAN DATA SPC


Tabel L11. Data SPC Heat Stability Yellow DAS
Pengukuran

Sub

Range

STD
BKA

BKB

BKA

BKB

0.10

5.47

5.37

0.10

5.47

5.37

0.09

5.585

5.257

0.09

5.585

0.18

0.10

5.47

5.257

5.37

0.09

5.585

0.20

0.18

0.08

5.257

5.47

5.37

0.09

5.585

5.421

0.20

0.18

5.257

0.10

5.47

5.37

0.09

5.585

5.425

5.421

0.20

5.257

0.18

0.10

5.47

5.37

0.09

5.585

5.4

5.400

5.421

5.257

0.20

0.18

0.08

5.47

5.37

0.09

5.585

5.257

5.4

5.4

5.450

5.3

5.4

5.425

5.421

0.10

0.18

0.06

5.47

5.37

0.09

5.585

5.257

5.421

0.20

0.18

0.10

5.47

5.37

0.09

5.585

5.4

5.4

5.5

5.257

5.450

5.421

0.10

0.18

0.06

5.47

5.37

0.09

5.585

5.257

5.3

5.5

5.5

5.5

5.5

5.4

5.5

5.450

5.421

0.20

0.18

0.10

5.47

5.37

0.09

5.585

5.257

5.3

5.425

5.421

0.20

0.18

0.10

5.47

5.37

0.09

5.585

13

5.5

5.3

5.257

5.5

5.5

5.450

5.421

0.20

0.18

0.10

5.47

5.37

0.09

5.585

14

5.4

5.257

5.4

5.4

5.5

5.425

5.421

0.10

0.18

0.05

5.47

5.37

0.09

5.585

15

5.257

5.5

5.3

5.5

5.4

5.425

5.421

0.20

0.18

0.10

5.47

5.37

0.09

5.585

5.257

16

5.5

5.3

5.4

5.4

5.400

5.421

0.20

0.18

0.08

5.47

5.37

0.09

5.585

5.257

17

5.5

5.5

5.3

5.3

5.400

5.421

0.20

0.18

0.12

5.47

5.37

0.09

5.585

5.257

18

5.4

5.4

5.5

5.3

5.400

5.421

0.20

0.18

0.08

5.47

5.37

0.09

5.585

5.257

19

5.3

5.5

5.4

5.4

5.400

5.421

0.20

0.18

0.08

5.47

5.37

0.09

5.585

5.257

20

5.3

5.4

5.5

5.4

5.400

5.421

0.20

0.18

0.08

5.47

5.37

0.09

5.585

5.257

Grup

X1

X2

DEV

X1

X2

X3

X4

5.3

5.4

5.5

5.5

5.425

5.421

0.20

0.18

5.5

5.5

5.4

5.3

5.425

5.421

0.10

0.18

5.4

5.5

5.5

5.3

5.425

5.421

0.20

5.3

5.4

5.4

5.5

5.400

5.421

5.5

5.5

5.3

5.4

5.425

5.3

5.4

5.5

5.5

5.4

5.3

5.5

5.5

5.5

5.5

5.5

10

5.5

11
12

Universitas Sumatera Utara

21

5.3

5.4

5.6

5.4

5.425

5.421

0.20

0.18

0.13

5.47

5.37

0.09

5.585

5.257

22

5.3

5.4

5.5

5.4

5.400

5.421

0.20

0.18

0.08

5.47

5.37

0.09

5.585

5.257

23

5.4

5.4

5.4

5.5

5.425

5.421

0.10

0.18

0.05

5.47

5.37

0.09

5.585

5.257

24

5.5

5.5

5.5

5.3

5.450

5.421

0.20

0.18

0.10

5.47

5.37

0.09

5.585

5.257

25

5.4

5.5

5.3

5.4

5.400

5.421

0.20

0.18

0.08

5.47

5.37

0.09

5.585

5.257

Untuk X SPC :

Untuk S SPC :

X1= 135.5

R = 4.5

S = 2.18

X2 = 5.421

R = 0.18

S = 0.09

n=4

A2 = 0,279

A1 = 1.88

BKA = X2 + A2R = 5.471

BKA = X2 + A1S = 5.585

BKB = X2 A2R = 5.371

BKA = X2 A1S = 5.257

LAMPIRAN -9E

PENGOLAHAN DATA SPC


Tabel L12. Data SPC Bilangan Asam Residue.
Pengukuran

Sub
Grup
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17

X1

X2

X3

24.6
0
24.6
0
24.7
0
24.5
0
24.6
0
24.6
0
24.5
0
24.6
0
24.6
0
24.6
0
24.6
0
24.6
0
24.7
0
24.6
0
24.7
0
24.7
0
24.6
0

24.5
0
24.7
0
24.7
0
24.6
0
24.7
0
24.6
0
24.7
0
24.6
0
24.6
0
24.7
0
24.7
0
24.7
0
24.6
0
24.7
0
24.7
0
24.7
0
24.7
0

24.7
0
24.7
0
24.6
0
24.7
0
24.5
0
24.7
0
24.8
0
24.6
0
24.7
0
24.5
0
24.8
0
24.6
0
24.7
0
24.5
0
24.6
0
24.5
0
24.6
0

X4

X1

X2

Rang
e
R

STD
R

BKA

BKB

DEV

BKA

BKB

24.70

24.625

24.650

0.10

0.13

0.10

24.687

24.613

0.07

24.785

24.515

24.70

24.675

24.650

0.10

0.13

0.05

24.687

24.613

0.07

24.785

24.515

24.70

24.675

24.650

0.10

0.13

0.05

24.687

24.613

0.07

24.785

24.515

24.70

24.625

24.650

0.10

0.13

0.10

24.687

24.613

0.07

24.785

24.515

24.70

24.625

24.650

0.20

0.13

0.10

24.687

24.613

0.07

24.785

24.515

24.60

24.625

24.650

0.10

0.13

0.05

24.687

24.613

0.07

24.785

24.515

24.50

24.625

24.650

0.30

0.13

0.15

24.687

24.613

0.07

24.785

24.515

24.80

24.650

24.650

0.20

0.13

0.10

24.687

24.613

0.07

24.785

24.515

24.60

24.625

24.650

0.10

0.13

0.05

24.687

24.613

0.07

24.785

24.515

24.80

24.650

24.650

0.20

0.13

0.13

24.687

24.613

0.07

24.785

24.515

24.60

24.675

24.650

0.10

0.13

0.10

24.687

24.613

0.07

24.785

24.515

24.70

24.650

24.650

0.10

0.13

0.06

24.687

24.613

0.07

24.785

24.515

24.70

24.675

24.650

0.10

0.13

0.05

24.687

24.613

0.07

24.785

24.515

24.70

24.625

24.650

0.20

0.13

0.10

24.687

24.613

0.07

24.785

24.515

24.70

24.675

24.650

0.10

0.13

0.05

24.687

24.613

0.07

24.785

24.515

24.80

24.675

24.650

0.30

0.13

0.13

24.687

24.613

0.07

24.785

24.515

24.60

24.625

24.650

0.10

0.13

0.05

24.687

24.613

0.07

24.785

24.515

Universitas Sumatera Utara

18
19
20
21
22
23
24
25

24.6
0
24.6
0
24.7
0
24.7
0
24.7
0
24.6
0
24.7
0
24.6
0

24.6
0
24.6
0
24.7
0
24.7
0
24.6
0
24.7
0
24.7
0
24.6
0

24.6
0
24.6
0
24.6
0
24.7
0
24.7
0
24.7
0
24.6
0
24.6
0

24.70

24.625

24.650

0.10

0.13

0.05

24.687

24.613

0.07

24.785

24.515

24.70

24.625

24.650

0.10

0.13

0.05

24.687

24.613

0.07

24.785

24.515

24.70

24.675

24.650

0.10

0.13

0.05

24.687

24.613

0.07

24.785

24.515

24.60

24.675

24.650

0.10

0.13

0.05

24.687

24.613

0.07

24.785

24.515

24.70

24.675

24.650

0.10

0.13

0.05

24.687

24.613

0.07

24.785

24.515

24.70

24.675

24.650

0.10

0.13

0.05

24.687

24.613

0.07

24.785

24.515

24.70

24.675

24.650

0.10

0.13

0.05

24.687

24.613

0.07

24.785

24.515

24.70

24.625

24.650

0.10

0.13

0.05

24.687

24.613

0.07

24.785

24.515

Untuk X SPC :

Untuk S SPC :

X1= 616.3

R = 3.3

S = 1.79

X2 = 24.65

R = 0.13

S = 0.07

n=4

A2 = 0,279

A1 = 1.88

BKA = X2 + A2R = 24.687

BKA = X2 + A1S = 24.785

BKB = X2 A2R = 24.613

BKA = X2 A1S = 24.515

LAMPIRAN -9F

PENGOLAHAN DATA SPC


Tabel L13. Data SPCYield Residue.
Pengukuran

Sub
Grup

X1

X2

X3

Range
X4

X1

X2

STD
R

BKA

BKB

DEV

BKA

BKB

4.96

4.95

4.97

4.97

4.963

4.965

0.01

0.01

0.01

4.969

4.961

0.01

4.979

4.952

4.96

4.97

4.97

4.97

4.968

4.965

0.01

0.01

0.00

4.969

4.961

0.01

4.979

4.952

4.97

4.97

4.96

4.97

4.968

4.965

0.01

0.01

0.00

4.969

4.961

0.01

4.979

4.952

4.95

4.96

4.97

4.97

4.963

4.965

0.01

0.01

0.01

4.969

4.961

0.01

4.979

4.952

4.96

4.97

4.95

4.97

4.963

4.965

0.02

0.01

0.01

4.969

4.961

0.01

4.979

4.952

4.96

4.96

4.97

4.96

4.963

4.965

0.01

0.01

0.01

4.969

4.961

0.01

4.979

4.952

4.95

4.97

4.98

4.95

4.963

4.965

0.03

0.01

0.02

4.969

4.961

0.01

4.979

4.952

4.96

4.96

4.96

4.98

4.965

4.965

0.02

0.01

0.01

4.969

4.961

0.01

4.979

4.952

4.96

4.96

4.97

4.96

4.963

4.965

0.01

0.01

0.00

4.969

4.961

0.01

4.979

4.952

10

4.96

4.97

4.95

4.98

4.965

4.965

0.02

0.01

0.01

4.969

4.961

0.01

4.979

4.952

11

4.96

4.97

4.98

4.96

4.968

4.965

0.01

0.01

0.01

4.969

4.961

0.01

4.979

4.952

12

4.96

4.97

4.96

4.97

4.965

4.965

0.01

0.01

0.01

4.969

4.961

0.01

4.979

4.952

13

4.97

4.96

4.97

4.97

4.968

4.965

0.01

0.01

0.00

4.969

4.961

0.01

4.979

4.952

14

4.96

4.97

4.95

4.97

4.963

4.965

0.02

0.01

0.01

4.969

4.961

0.01

4.979

4.952

15

4.97

4.97

4.96

4.97

4.968

4.965

0.01

0.01

0.00

4.969

4.961

0.01

4.979

4.952

Universitas Sumatera Utara

116

16

4.97

4.97

4.95

4.98

4.968

4.965

0.03

0.01

0.01

4.969

4.961

0.01

4.979

4.952

17

4.96

4.97

4.96

4.96

4.963

4.965

0.01

0.01

0.00

4.969

4.961

0.01

4.979

4.952

18

4.96

4.96

4.96

4.97

4.963

4.965

0.01

0.01

0.00

4.969

4.961

0.01

4.979

4.952

19

4.96

4.96

4.96

4.97

4.963

4.965

0.01

0.01

0.00

4.969

4.961

0.01

4.979

4.952

20

4.97

4.97

4.96

4.97

4.968

4.965

0.01

0.01

0.00

4.969

4.961

0.01

4.979

4.952
4.952

21

4.97

4.97

4.97

4.96

4.968

4.965

0.01

0.01

0.00

4.969

4.961

0.01

4.979

22

4.97

4.96

4.97

4.97

4.968

4.965

0.01

0.01

0.00

4.969

4.961

0.01

4.979

4.952

23

4.96

4.97

4.97

4.97

4.968

4.965

0.01

0.01

0.00

4.969

4.961

0.01

4.979

4.952

24

4.97

4.97

4.96

4.97

4.968

4.965

0.01

0.01

0.00

4.969

4.961

0.01

4.979

4.952

25

4.96

4.96

4.96

4.97

4.963

4.965

0.01

0.01

0.00

4.969

4.961

0.01

4.979

4.952

Untuk X SPC :

Untuk S SPC :

X1= 124.1

R = 0.3

S = 0.18

X2 = 4.965

R = 0.01

S = 0.01

n=4

A2 = 0,279

A1 = 1.88

BKA = X2 + A2R = 4.969

BKA = X2 + A1S = 4.979

BKB = X2 A2R = 4.961

BKA = X2 A1S = 4.952

Universitas Sumatera Utara