Appendix

LAMPIRAN -1
PROSEDUR ANALISA
Universitas Sumatera Utara
LAMPIRAN -1A
PROSEDUR ANALISA WARNA LOVIBOND
1. Tujuan
Metode ini menentukan warna dengan membandingkan cahaya yang dipancarkan
melalui kedalaman tertentu dari lemak, minyak atau asam lemak terhadap warna
cahaya asal dari sumber yang sama, dipancarkan melalui standart.
2. Batasan
Dapat digunakan untuk minyak-minyak hewan, tumbuh-tumbuhan dan asam
lemak
3. Peralatan
3.1. Lovibond Tintometer Model E AF 900
3.2. Lighting cabinet, two 60 watt pearls lamps
3.3. Color racks, consisting of red, yellow, blue, and neutral
Racks with color reading as follow Red : 0.1-0.9; 1.0-9.0; 10.0-70.0
Yellow
: 0.1-0.9; 1.0-9.0; 10.0-70.0
Blue
: 0.1-0.9; 1.0-9.0; 10.0-04.0
Neutral
: 0.1-0.9; 1.0-3.0
3.4. Glass cell, made of optical glass, 1" and 5.25"
4. Bahan-bahan:
None Applicable
5. Langkah kerja
5.1. Cairkan contoh 100 C diatas titik leleh jika masih padat dan saring jika perlu
untuk menghilangkan pengotor padat
5.2. Tuangkan contoh yang tersedia secukupnya ke dalam sel bersih dan kering
5.3. Tempatkan sel yang mengandung contoh kedalam pemegang sel secara
benar.
5.4. Setelah penutupan ruang sel, segera tentukan warna contoh. Mula-mula
digunakan rak warna kuning 10 terhadap merah 1.
5.5. Atur sampai perbandingan warna yang akurat dicapai, tanpa perlu
mempertahankan ratio 10 kuning terhadap 1 merah dan gunakan angka biru
atau netral yang rendah untuk memperoleh perbandingan, tapi tidak lebih
dari 9.0 biru atau 3.0 netral
5.6. Mencatat ukuran cell dan pembacaan warna merah, kuning, biru atau netral
pada pembentukan perbandingan warna.
5.7. Hasil dinyatakan dalam bentuk seperti dibawah ini :
5.7.1. Pembacaan angka merah, kuning, dan biru atau netral diperlukan
untuk memperoleh perbandingan
5.7.2. Panjang sell yang digunakan
5.8. Pengukuran warna diambil pada satu panjang sel tidak boleh dipakai untuk
menghitung nilai warna untuk panjang sell yang lain.
5.9. Sebaiknya ketajaman (kejelasan) warna tidak pernah lebih besar dari 20 total
lovibond color
6. Rujukan
AOCS Ce 13e-92
LAMPIRAN -1B
PROSEDUR PEMBUATAN METYL ESTER ASAM LEMAK.
1. Tujuan
Metil ester dari asam lemak dan minyak dipisahkan dan ditentukan secara
kuantitatif dengan GLC menggunakan packed column tertentu atau asam lemak
langsung dipisah dan ditentukan secara kuantitatif dengan GLC menggunakan
capillary column tertentu.
2. Batasan
Metode ini berlaku untuk asam lemak dan minyak nabati yang mempunyai atom
karbon 6 sampai 20 setelah dirubah menjadi ester untuk packed atau langsung
asam lemak untuk capillary column.
3. Peralatan
3.1. Analytical balance
3.2. Block heater
3.3. Thermometer
3.4. Screw vial, 5 ml
4. Bahan-bahan
4.1. BF 3 = methanol solution, reagent grade
4.2. Sodium chlorida saturated solution
4.3. Solvent, n-hexane, reagent grade
4.4. Methanol, reagent grade
4.5. NaOH 0.5 N in methanol

Larutkan 20 +0.05 g, reagent grade NaOH dalam 1 L metanol
5. Langkah kerja
5.1. Determination carbon chain for fats and oils
5.1.1
Timbang sampel sekitar 0.02 gram kedalam vial 5 ml yang tertutup
5.1.2
Tambahkan 2 ml 0.05N NaOH metanol, dan panaskan didalam blok

pemanas pada suhu yang diatur 68+ 10C selama 10 menit.
5.1.3
Tambahkan 2 ml larutan reagen BF 3 metanol, dan panaskan didalam

blok pemanas pada suhu yang diatur 68+ 10C selama 15 menit
5.1.4
Keluarkan dari blok pemanas dan didinginkan pada suhu ruangan
5.1.5
Tambahkan 2 ml heksan dan 1 ml larutan NaCl jenuh, kocok dan

biarkan selama 1 menit, sekarang larutan heksan siap di injeksikan.
5.2. Determination carbon chain ini pack column

5.2.1. Timbang sampel sekitar 0.02 ml gram kedalam vial 5 ml yang
tertutup.
5.2.2. Tambahkan 2 ml larutkan reagen BF 3 metanol, dan panaskan didalam
blok pemanas pada suhu yang diatur 68 + 10C selama 15 menit
5.2.3. Keluarkan dari blok pemanas dan dinginkan pada suhu ruangan.
5.2.4. Tambahkan 2 ml heksan dan 1 ml larutan NaCl jenuh, kocok dan
biarkan selama 2 menit, sekarang larutan heksan siap untuk di
injeksikan.
5.3. Determination carbon chain ini capillary column
5.3.1. Timbang sampel sekitar 0.02 gram kedalam vial 5 ml yang tertutup
5.3.2. Tambahkan 2 ml heksan dan kocok, jika sampel tidak larut panaskan
beberapa menit untuk melarutkannya.
5.3.3. Sekarang larutan heksan siap untuk di injeksikan.
6. Rujukan
AOCS CE2-66
LAMPIRAN -1C.
PROSEDUR ANALISA KOMPOSISI ASAM LEMAK
1. Tujuan
Metil ester dari asam lemak dipisahkan dan ditentukan secara kuantitatif dengan
GLC menggunakan packed colomn tertentu asam lemak langsung dipisah dan
ditentukan secara kuantitatif dengan GLC menggunakan capillary coloumn
tertentu.
2. Batasan
Metode ini berlaku untuk asam lemak dan minyak nabati yang mempunyai atom
karbon 6 sampai 20 setelah dirubah menjadi metil ester untuk packed column
atau langsung asam lemak untuk capillary column.
3. Peralatan
3.1. Syringe, 10 1
3.2. Shimadzu Gas chromatograph, GC-14B
3.2.1. Injector Insert glass type, splitless mode
3.2.2. Detector Flame Ionization detector, range 102
3.2.3. Columns
For methyl esters of fatty acid- GP 10% SP 216 PS on 100/120
Supelcoport.
Supelco Cat. No. 1-1879, square Loop
For fatty acids :

-
HP-FFAP, Cross linked polyethylene glycol-TPA phase

15 m x 0.53 mm x 1.0 m, Hawlett Packard Part No. 19095F 123
Coloum Glass, 20% DEGS Chromosorb WHP on 60/80

Temp. Max 2000C, P/N 221-14368-31/7G (3.2-3.1), Lenght 3 M
Coloum Stainless, GP 10% SP-216-PS on 100/120 Supelcoport

Temp. Max 2000C, Lenght 2 M
Flow rate of Gas :

Gases
Packed Kpa
Nitrogen
90
Hydrogen
60
Air
50
Temperature
Programs Injector, 0C
Detector0C
Samples
Column, 0C
Initial temp, 0C
Initial time, min.
Program rate, 0C/min
Final temp. 0C
Final time, min
Capilllary KPa
40
55
30
Packed
220
230
CPO
C 12 PKO
RBD PS
C 18
120
140
100
0
0
0
10
10
10
190
190
190
15
15
15
Capillary
230
250
C 8 -C 10
C 8, C 18
C 16 -C 18
170
0
10
190
8
100
0
10
230
5
3.3. Recording system, Chromatopac C-R6A

Attenuation, mV/full scale
Width
Slope, V/min
70 max
Drift
Minimum Area, Count
1000 max
TDBL
Chart speed, mm/min
3.4. Screw cap vial, 5 ml

3.5. Analytical balance, 0.0001 g accuracy
4. Bahan-bahan
4.1. Solvent,n-hexane, reagent grade
4.2. Carries gas, nitrogen with ultra high purity (UHP)

4.3. Hydrogen, Ultra high purity
4.4. Air, industrial grade, free from oil and moisture
5. Langkah Kerja
5.1. Preparation sample
5.1.1. Methyl ester
5.1.1.1.Penyediaan metil ester merujuk pada lampiran 6
5.1.2. Fatty Acid
5.1.2.1.Timbang sampel sekitar 0.02 gram kedalam vial 5 ml yang
bertutup.
5.1.2.2.Tambahkan 2 ml heksan dan kocok, jika sampel tidak larut
panaskan beberapa menit untuk melarutkannya.
5.2. Prosedur
5.2.1. Pilih keadaan yang optimal dari sistem GC dan file Chromatopact
untuk sampel yang tepat
5.2.2. Dengan menggunakan, injeksikan 1 kedalam kolom, dan start GC.
5.2.3. Identifikasikan puncak-puncak dari kromatogram, menggunakan
kromatogram standar sebagai petunjuk.
5.3. Perhitungan
ACi x FCi x 100
Calculation : % Ci = Sum (FCi x ACi
Dimana
% Ci
= Kandungan rantai karbon i dalam % berat
ACi
= Area rantai karbon i
FCi
= Faktor respons rantai karbon i
Sum (ACixFCi) = jumlah dari FCi x Aci
6. Rujukan
6.1. User Manual, Shimadzu Chromatopac C R6A & C-R8A
6.2. User Manual, Shimadzu Chromatograph GC 14B
7. Informasi-informasi lain yang dibutuhkan

1.1. Packed column hanya sesuai untuk metil ester
1.2. HP-FFAP untuk C8C10 Fatty Acid
LAMPIRAN -1D
PEMBUATAN LARUTAN STANDAR NATRIUM TIOSULFAT (NA 2 S 2 O 3 )
1. Tujuan
Cara ini menunjukkan pembuatan dan membakukan larutan natrium tiosulfat
secara kuantitatif.
2. Batasan
Hanya dapat digunalan untuk larutan Natrium Thiosulfat
3. Peralatan
3.1. Analytical balance, 0.0001 g accuracy
3.2. Burrete, accurately calibrate 50 ml
3.3. Cylinder glass, 25 ml, 100 ml
3.4. Reagent bottle, 5000 ml
3.5. Volumetric pipette, 5 ml
3.6. Erlenmeyer flask, 300 ml
3.7. Volumetric dispenser 20 ml
4. Bahan-bahan
4.1. CO 2 free distilled water
Didihkan air suling selama 20 menit dan dinginkan dengan penutup untuk
mencegah penyerapan CO 2 .
4.2. Potasium Iodium solution, 15%
Larutkan 150 gram Kalium Iodium ke dalam 1000 ml air suling
4.3. Starch Indicator, 1%
Larutkan 1 gram serbuk starch ke dalam 100 ml air suling yang panas dan
dinginkan.
4.4. Standart primer kalium dikromat 0.1 N
4.5. Larutkan 2.4518 gram yang telah dikeringkan dan dinginkan dalam labu ukur
500 ml dengan air destilat dan terakan sampai tanda batas dan simpan dalam
botol gelap.
5. Langkah Kerja
5.1. Preparation of Sodium solution, 0.1N & 0.01N
Larutkan dalam 124,5 + 0.1 gr Natrium thisulfat ke dalam air suling dan
larutkan hingga 5 L.
5.2. Sodium Thiosulfate Standardization 0.1N
Pipet 25 ml larutan kalium dichromat ke dalam erlenmeyer 300 ml,
tambahkan 5 ml asam klorida pekat, 20 ml larutan kalium iodida dan aduk.
Diamkan selama 5 menit, dan kemudian tambahkan 100 ml air suling. Titrasi
dengan larutan natrium thiosulfat, aduk sampai warna kuning pucat.
Tambahkan 1-2 ml indikator starch dan lanjutkan titrasi secara perlahan
hingga warna biru benar benar tak kelihatan.
5.3. Sodium Thiosulfat Standardization
5.4. Encerkan 100 ml larutan N 2 S 2 O 3 0,1N ke dalam 1000 ml labu ukur dengan
air destillat dan terakan sampai tanda batas.
Untuk standarisasi, pipet 2 ml larutan kalium dichromat ke dalam erlenmeyer
300 ml . Tambahkan 5 ml asam klorida pekat, 20 ml larutan kalium iodium
dan aduk. Diamkan selama 5 menit, dan kemudian tambahkan 100 ml air
suling. Titrasi dengan larutan natrium thiosulfat, aduk sampai warna kuning
pucat. Tambahkan 1-2 ml indikator starch dan lanjutkan titrasi secara
perlahan hingga warna biru benar-benar tak kelihatan.
5.5. Perhitungan
20.394 x wt of K 2 Cr 2 O 7 x fp
ml of Na 2 S 2 O 3
Normality of Na 2 SO 2 O 3 =
6. Rujukan
AOCS Official Method Tg 1-64.
LAMPIRAN -1E
PEMBUATAN LARUTAN STANDAR WIJS
1. Tujuan
Prosedur ini menggambarkan pembuatan larutan wijs dari iodine monochlorida
2. Batasan
Cara ini hanya digunakan untuk membuat larutan wijs dari iodine monochlorida
komersil.
3. Peralatan
3.1. Cylinder glass, 100, 1000 ml
3.2. Erlenmeyer flask, 500 ml
3.3. Filter paper
3.4. Magnetic stirrer
3.5. Reagent bottle, 5000 ml, amber
3.6. Volumentric pippete, 10 ml
4. Bahan-bahan
4.1. Acetic acid glacial
4.2. Distilled water

4.3. Iodine monochloride
4.4. Potasium Iodida Solution, 15%
4.5. Cyclo hexane
4.6. Starch indikator
4.7. Sodium thiodulfate solution, 0.1N
4.8. Sulfuric acid, 2%
5. Langkah kerja
5.1. Stock solution :
Tambahkan 317 +0.1 g iodine monochloride ke 1 L asam asetat glasial, aduk
hingga larut selanjutnya saring dengan kertas saring whatman 41H atau
sejenisnya ke botol yang bersih dan kering. Saring dengan segera untuk
mencegah terjadinya kontaminasi terhadap air dan simpan di tempat yang
sejuk. Buang larutan bila terbentuk endapan.
5.2. Wijs Solution :
Dengan menggunakan glas ukur tuangkan 117.0 + 0.1 ml larutan stock ke
botol 5 L yang telah terisi asam asetat, kemudian aduk hingga merata.
5.3. Wijs standardization
Menentukan perbandingan I/Cl yang mana harus dalam batas 1.10 + 0.1
seperti prosedur berikut :
5.3.1. Iodine content :
Tuangkan 150 ml larutan chroline jenuh ke dalam erlenmeyer 500 ml,
dan tambahkan beberapa butir butiran kaca.
5.3.2. Pipet 5 ml larutan wijs ke dalam larutan erlenmeyer yang telah berisi
chlorine jenuh, aduk dan panaskan hingga mendidih.
5.3.3. Didihkan dengan cepat selama 10 menit, dinginkan dan tambahkan 30
ml asam sulfat 2% dan 15 ml larutan iodida.
5.3.4. Aduk dengan baik dan segera titrasi dengan larutan natrium thiosulfat
0.1N dengan starch sebagai indikator.
5.4. Total Halogen Content
5.4.1. Tuangkan 150 ml air destillat yang baru mendidih ke erlenmeyer 500
ml yang bersih dan kering.
5.4.2. Tambahkan 15 ml larutan kalium iodida 15%

5.4.3. Pipet 20 ml larutan Wijs ke dalam erlenmeyer tersebut, aduk hingga
homogen
5.4.4. Titrasi dengan natrium tiosulfat 0.2N dengan starch sebagai indikator.
5.5. Perhitungan :
Halogen ratio :
Dimana :
2A
3B 2A
A = Volumen natrium thiosulfat untuk menitrasi kandungan

iodine
B = Volume natrium thiosulfat untuk menitrasi kandungan
halogen total.
6. Rujukan
AOCS Official Method Tg 1-64
LAMPIRAN -1F
PROSEDUR ANALISA BILANGAN IODIUM
1. Tujuan
Bilangan iodine adalah suatu ukuran ketidakjenuhan dari minyak industri dan
turunnya dan dinyatakan dalamistilah gram iodin terserap setiap 100 gram contoh
(% iodine terserap).
2. Batasan
Dapat digunakan untuk minyak-minyak industri dan turunnya, seperti minyak
kering alami atau buatan dan asam lemaknya.
3. Peralatan
3.1. Analytical balance, accurate up to 0.0001 gr
3.2. Burrete or Automatic piston burrete with stirrer, 50 ml
3.3. Erlenmeyer flask with stopper, 250 to 300 ml
3.4. Volumetric dispenser, 30 ml, 1 ml adjustabilty
3.5. Volumetric pippete, 15,25 ml
3.6. Graduate cylinder, 100 ml
4. Bahan-bahan
4.1. Sodium Thiosulfate Solution. 0,1N
Merujuk ke pada lampiran 8
4.2. Wijs Solution
Merujuk pada lampiran 9
4.3. Pottasium Iodida Solution, 15%
Larutkan 150 g kalium Iodida dalam 1000 ml air demin
4.4. Starch indicator solution
Buat pasta 1 gram starch dengan sedikit air dingin. Tambahkan sambil
diaduk dengan 100 ml air mendidih.
4.5. Sikloheksana sebagai pengganti karbon tetraklorida seperti rekomendasi
5. Langkah Kerja
5.1. Cairkan sampel jika masih padat dan timbang seperti berikut ini : (catatan 7).
Sample
Caprylic, Capric Aicd,
Lauric Acid, Myristic
Acid, TPSA,
Hydrogenated, TPSA,
DPSA, RGSA, Stearic
65%
Weight,g
5 + 0.5
Sample
Weight,g
CPKO, SPKOFA
0.70-1.00
RBDPS, SRBDPSFA
0.40-0.60
CPS, SCPSA and Oleic Acid
0.30-0.50
CPO, SPOFA
0.10-0.20
5.2. Tambahkan 10 ml Sikloheksana, pipet 15 ml larutan Wijs dalam labu yang

mengandung contoh dan aduk dengan baik
5.3. Buat dan lakukan penentuan blanko sekaligus sama dengan contoh.
5.4. Simpan labu-labu di dalam tempat gelap selama 30 menit pada suhu 25 + 50C
5.5. Pindahkan labu ke penyimpanan, tambahkan 10 ml larutan Kl, 100 ml air
suling.
5.6. Titrasi dengan larutan 0.1N Na 2 S 2 O 3 , penambahannya secara bertahap dan
dengan pengadukan yang kuat dan tetap sampai warna kuning hampir
lenyap. Tambahkan 1-2 larutan indikator kanji dan lanjutkan titrasi sampai
warna biru lenyap seketika.
5.7. Perhitungan :
Iodine value, gI 2 /100g
Where :
( Vb Vs) x N x 12.69
=
W
Vb
= ml Na 2 S 2 O 3 0.1 dipakai pada titrasi blanko
Vs
= ml Na 2 S 2 O 3 0.1 dipakai pada titrasi contoh
= Normalitas Na 2 S 2 O 3
= Gram contoh
6. Rujukan
AOCS Official Method Tg 1-64

7.1. Larutan Wijs harus lebih 100-150% terhadap jumlah terserap
7.2. Untuk Oleic acid, menggunakan 25 ml larutan Wijs, 20 ml Cyclohexane dan

20 ml larutan Kl 15%
LAMPIRAN -1G
PROSEDUR ANALISA HEAT STABILITY
1. Tujuan
Metode ini mengukur stabilitas warna dari asam lemak (fatty acid) setelah
pemanasan dalam kondisi analisa khusus.
2. Batasan
Berlaku untuk semua fatty acid normal
3. Peralatan
Oil batch
Mixer
Thermometer
Tubes Thermal Resistance
Filter paper
Colorimeter
4. Bahan-bahan
4.1. Sulfuric Acid (corrosive material)
5. Langkah Kerja
5.1. Pembuatan larutan khusus Asam sulfat 1 : 1
Masukkan 1 bagian asam sulfat ke dalam 1 bagian air dengan hati hati,
jangan
sampai terbalik.
5.2. Perlakuan Sampel
Jika sampel yang diuji tidak cair pada suhu ruangan, cairkan dengan
pemanasan
di water batch sampai suhu tidak lebih dari 10 oC di atas titer sampel.
5.3. Perlakuan Peralatan

5.3.1. Pastikan sebelum oil batch digunakan, sudah diverifikasi dahulu suhunya
dengan menggunakan thermometer standar.
5.3.2.
Tabung harus dicuci bersih dengan asam sulfat (1:1), kemudian dibilas
dengan air distillat dan dikeringkan.
5.4. Cara Kerja

5.4.1. Set wadah minyak ke suhu 205 + 2 oC dan jaga suhu dalam kisaran khusus
ini.
5.4.2. Isi tabung yang bersih dan kering hingga kedalaman 12.7 cm dengan
sampel dan masukkan dalam wadah minyak.
5.4.3. Atur volume di dalam wadah minyak hingga ketinggian 14 cm dari bagian
bawah gelas tabung. Bila meletakkan beberapa tabung gelas di dalam oil
batch, suhunya tidak turun lebih dari 5 oC di bawah suhu minimum oil
batch dan waktu untuk menaikkan suhu menjadi 205 oC tidak lebih dari 5
menit.
5.4.4. Atur waktu 60 menit untuk samplel yang memiliki bilangan iodium di atas
15 atau atur 120 menit jika sampel memiliki bilangan iodium lebih kecil
atau sama dengan 15.
5.4.5. Pindahkan tabung dari oil batch dan lihat warna menggunakan AOCS
official Method Td 1a - 65 atau Lovibond Color.
6. Rujukan
AOCS Official Method Td 3a-64

Kebersihan glassware sangat penting. Metode yang disarankan dibersihkan
dengan detergent dan dibilas dengan asam sulfat. Larutan dikromat jangan
dilakukan.
LAMPIRAN -2A
Tabel L1. Mutu Umpan Hidrogenated Splitted Crude Stearic Acid
(HSRBDPSFA).
No
Item Analisa
Color 51/4, R/Y
Komposisi (% berat):
Bilangan Iodium (IV) Umpan, g /

100 g
0,7
0,6
5,8/44,4
4,9/42,1
Asam laurat, C 12
0,1
0,1
Asam miristat, C 14
1,3
1,3
Asam palmitat, C 16
59,5
56,8
Asam stearat, C 18
38.6
41,3
Asam oleat, C 18-1
Asam linoleat, C 18-2
Asam arachidat, C 20
0,4
0,4
Unknown, Unk
0,1
0,1
Sumber : PT. Flora Sawita Chemindo, 2008
LAMPIRAN -2B
Tabel L2. Hasil Perhitungan Nilai Rata-rata Warna Distillat Asam Stearat Berbasis
RBDPS.
No
Kecepatan
Bilangan
Alir
Iodium (IV)
Umpan,
Umpan,
ton/jam
g/ 100 g
0,7
5,5
0,6
0,7
5,75
0,6
0,7
6,00
0,6
Warna R DAS
Suhu Bottom
MD,
C0
Warna Y DAS
R
R-1
R-2
Rata -
Y
Y-1
Y-2
rata
Rata
- rata
218
0,1
0,1
0,1
0,7
0,7
0,7
220
0,1
0,1
0,1
0,7
0,7
0,7
222
0,1
0,1
0,1
0,7
0,7
0,7
218
0,1
0,1
0,1
0,7
0,7
0,7
220
0,1
0,1
0,1
0,7
0,7
0,7
222
0,1
0,1
0,1
0,7
0,7
0,7
218
0,1
0,1
0,1
0,7
0,7
0,7
220
0,1
0,1
0,1
0,7
0,7
0,7
222
0,1
0,1
0,1
0,7
0,7
0,7
218
0,1
0,1
0,1
0,7
0,7
0,7
220
0,1
0,1
0,1
0,7
0,7
0,7
222
0,1
0,1
0,1
0,7
0,7
0,7
218
0,1
0,1
0,1
0,7
0,7
0,7
220
0,1
0,1
0,1
0,7
0,7
0,7
222
0,1
0,1
0,1
0,7
0,7
0,7
218
0,1
0,1
0,1
0,7
0,7
0,7
220
0,1
0,1
0,1
0,7
0,7
0,7
222
0,1
0,1
0,1
0,7
0,7
0,7
Keterangan : R = Red ; Y = Yellow ; R = harga rata rata R-1 dan R-2; Y Rata rata
= harga rata rata Y-1 dan Y-2 sesuai simbol Warna Lovibond
234
LAMPIRAN -2C
Tabel L3. Rata-rata Heat Stability dan Produksi Fraksi Ringan dan Distillat Asam
Stearat (DAS) dari RBDPS.
Kecepatan
No
Alir
Umpan,
(ton/jam)
Bilangan
Iodium
(IV)
Umpan,
g/100 g
0,7
1
0,7
H/S - 2
H/S
LE
DAS
kg/jam
kg/jam
MD,
C0
218
0,4
3,8
0,4
4,1
0,40
3,95
82,73
4923,75
220
0,4
4,8
0,5
5,2
0,45
5.00
93,25
4937,25
222
0,5
5,4
0,5
5,8
0,50
5,60
98,55
4967,51
218
0,3
3,7
0.3
3,8
0,30
3,75
95,125
4925,05
220
0,3
4,8
0,4
5,0
0,35
4,90
95,58
4936,85
222
0,4
5,2
0,4
5,3
0,40
5,25
91,40
4949,8
218
0,4
3,9
0,5
4,0
0,45
3,95
86,25
5146,00
220
0,5
4,9
0,5
5,3
0,50
5,10
98,33
5161,50
222
0,6
5,4
0,5
5,8
0,55
5,60
102,93
5194,00
218
0,4
4,0
0,4
3,8
0,40
3,95
99,30
5150,00
220
0,4
4,9
0,5
5,1
0,45
5,00
100,06
5161,25
222
0,5
5,3
0,5
5,4
0,50
5,35
100,65
5196,00
218
0,5
4,0
0,5
4,2
0,50
4,10
90,30
5370,60
220
0,6
5,0
0,6
5,3
0,55
5,15
99,60
5385,90
222
0,6
5,8
0,6
6.0
0,60
5,90
83,70
5435.65
218
0,5
4,0
0,4
4,1
0,45
4,05
103,20
5377,20
220
0,5
4,9
0,5
5,2
0,50
5,05
103,80
5386,30
222
0,6
5,4
0,5
5,5
0,55
5,45
105,30
5444,70
5,75
0,6
0,7
3
H/S 1
Bottom
5,50
0,6
Suhu
6,00
0,6
Keterangan : H/S = heat stability ; R = red ; Y = yellow ; H/S = heat stability rata rata.
LAMPIRAN -2D
Tabel L4. Hasil Perhitungan Rata - rata Respon Yield Destillat LE, AS dan Residue serta Distillat -2.
Kec. Alir
No
Umpan,
ton/jam
Yield Fraksi Ringan (LE)

IV Umpan,
g/ 100 g
0,7
5,50
0,6
0,7
5,75
0,6
0,7
6,00
0,6
Yield Distillat Asam Stearat
Yield Residue
Yield Dist -2
Suhu B MD
0
LE-1
LE-2
LE
DAS-1
DAS-2
DAS
Res-1
Res-2
Res
(Dest-2)-1
(Dist-2)-2
Dist-2
kg/jam
kg/jam
kg/jam
kg/jam
kg/jam
kg/jam
kg/jam
kg/jam
kg/jam
kg/jam
kg/jam
kg/jam
218
96,750
94,00
95,375
4922,50
4925,,00
4923.75
283,00
285,00
284,00
198,52
196,00
197,26
220
95,150
96,10
95,625
4936,50
4938,00
4937,25
280,00
281,00
280,50
188,85
184,90
186.75
222
99,00
98,00
98,500
4965,015
4970,00
4967,51
277,00
278,00
277,50
158,99
154,00
156,49
218
82,50
83,00
82,750
4924,00
4926,10
4925,05
280,60
277,00
278,80
212,90
214,90
213,90
220
93,50
93,00
93,250
4937,50
4936,20
4936,85
275,50
276,00
275,75
194,00
194,80
194.40
222
95,40
97,10
96,250
4970,50
4969,10
4969,80
274,00
275,00
274,50
160,10
158,80
159,45
218
100,80
97,80
99,300
5143,40
5148,60
5146,00
297,30
299,40
298,35
208,50
204,20
206,35
220
99,48
100,63
100,055
5161,20
5161,80
5161,50
292,67
293,00
292,835
196,65
194,57
195,70
222
102,35
103,50
102,925
5192,30
5195,70
5194,00
287,50
289,80
288,50
167,85
161,00
164,425
218
85,70
86,80
86,250
5148,00
5152,00
5150,00
293,30
291,50
292,40
223,00
219,70
221,35
220
94,88
97,17
96,025
5161,78
5160,63
5161,25
288,50
288,80
288,65
204,84
203,40
204,12
222
100,10
101,20
110,150
5196,30
5195,70
5196,00
284,05
286,35
285,20
169,55
166,75
168,15
218
105,00
101,40
103,200
5368,20
5373,00
5370,60
308,00
309,00
308,50
218,80
216,60
217,70
220
103,20
104,44
103,800
5385,60
5386,20
5385,90
304,20
305,40
304,80
207,80
204,00
205,90
222
107,40
109,20
108,300
5435,10
5436,20
5435.65
301,20
302,40
301,80
156,30
152,20
154,25
218
90,15
90,60
90,375
5372,40
5382,00
5377,20
303,00
302,5
302,75
234,60
225,40
230,00
220
98,40
100,80
99,600
5385,00
5388,00
5386,30
300,60
301,80
301,20
216,00
209,40
212,70
222
104,40
106,20
105,300
5444,20
5445,20
5444,70
297,00
298,20
297,60
152,60
152,20
152,40
LAMPIRAN -2E
Tabel L5. Hasil Perhitungan Rata-rata Bilangan Iodium (IV) Distillat Asam
Stearat Berbasis RBDPS.
Kecepatan
No
Alir Umpan,
ton/jam
Bilangan
Iodium (IV)
Umpan,
g/ 100 g
0,7
5,5
0,6
0,7
2
5,75
0,6
0,7
3
6,00
0,6
Bilangan Iodium (IV) DAS
Suhu
IV Rata -
Bottom MD,
IV 1
IV 2
C0
gr/100 gr
gr/100 gr
218
0.15
0,15
0.150
220
0.15
0,17
0.160
222
0,17
0,17
0,170
218
0.14
0,15
0.145
220
0,16
0.15
0.155
222
0,16
0.16
0.160
218
0.16
0,16
0.160
220
0,17
0,17
0,170
222
0,17
0,17
0,170
218
0,16
0,15
0.155
220
0.16
0,17
0.165
222
0,17
0.16
0.165
218
0,16
0.17
0.165
220
0.18
0,17
0.175
222
0,18
0,18
0,180
218
0,16
0.16
0,160
220
0,17
0.17
0,170
222
0,18
0.17
0.175
rata
gr/100 gr
LAMPIRAN -2F
Tabel L6. Hasil Perhitungan Rata - Rata Bilangan Asam Residue Berbasis
RBDPS.
Kecepatan Alir
No
Umpan,
ton/jam
Bilangan
Iodium (IV)
Umpan,
100 g
0,7
1
5,5
0,6
0,7
2
5,75
0,6
0,7
3
6,00
0,6
g/
Bilangan Asam (AV) Residue
Suhu
Bottom MD,
AV 1,
AV 2,
AV Rata - rata,
218
33,5
36,5
35,00
220
25,8
28,0
26,90
222
25,5
27,5
26,50
218
28,3
27,8
28,05
220
23,9
24,5
24,20
222
23,6
25,1
24,30
218
33,6
36,4
35,00
220
26,0
27,6
26,80
222
25,0
27,5
26,25
218
28,5
27,8
28,15
220
24,5
24,8
24,65
222
24,0
24,8
24,40
218
34,0
37,0
35,50
220
26,5
27,5
27,00
222
25,8
27,8
26,80
218
28,2
28,0
28,10
220
25,0
24.5
24.75
222
23,80
24,6
24,20
C0
Keterangan : AV = Acid Value (Bilangan Asam) dalam mg KOH/gram
LAMPIRAN -2G
Tabel L7. Perbandingan Mutu Distillat Asam Stearat (berbasis RBDPS) Hasil
Optimasi
Mutu DAS
Sebelum
Optimasi (*)
0,10,2R/0,70,9Y
Mutu DAS
Sesudah
Optimasi
0,5-0,8R/67,5Y
0,55R/5,45
Y
0,15 - 0,24
0,175
total
keduanya
1,0 %
maks
< 1,0
total
keduanya
0,30 %
maks
C 16 , asam palmitat
56 - 63
In specs
59,00
C 18 , asam stearat
37 42
Sering <
37.0
40,25
< 1,0
total
keduanya
0,45 %
No
Parameter Mutu
Warna (Colour) 5 ,
Lovibond
Heat Stability (H/S)5 ,

Lovibond
Bilangan Iodium (IV), gr/100

gr
Komposisi, % berat :
C 12 , asam laurat
C 14 , asam miristat
C 20 , asam arachidat
Unk
Standar
Mutu
DAS
0,1R/
0,8Y maks
0,6
R/6,0Y
maks
0,20 maks
total
keduanya
1,0 %
maks
0.1/0.7
LAMPIRAN 3A
General Linear Model: Yield AS versus F Umpan, IV Umpan, Suhu B MD
Factor
F Umpan
IV Umpan
Suhu B MD
Type
fixed
fixed
fixed
Levels
3
2
3
Values
5.50, 5.75, 6.00
0.6, 0.7
218, 220, 222
Analysis of Variance for Yield AS, using Adjusted SS for Tests

Source
P
F Umpan
0.000
IV Umpan
0.004
Suhu B MD
0.000
F Umpan*IV Umpan
0.105
F Umpan*Suhu B MD
0.000
IV Umpan*Suhu B MD
0.081
F Umpan*IV Umpan*Suhu B MD
0.681
Error
Total
S = 2.49864
R-Sq = 99.99%
DF
Seq SS
Adj SS
Adj MS
1251684
1251684
625842
100243.94
70
70
70
11.25
17999
17999
9000
1441.52
32
32
16
2.56
793
793
198
31.74
36
36
18
2.90
14
14
0.58
18
35
112
1270741
112
R-Sq(adj) = 99.98%
Unusual Observations for Yield AS

Obs
31
32
Yield AS
5372.40
5382.00
Fit
5377.20
5377.20
SE Fit
1.77
1.77
Residual
-4.80
4.80
St Resid
-2.72 R
2.72 R
R denotes an observation with a large standardized residual.
LAMPIRAN -3B
One-way ANOVA: Yield AS_0.6 versus F Umpan_0.6
Source
F Umpan_0.6
Error
Total
S = 25.65
Level
5.50
5.75
6.00
N
6
6
6
DF
2
15
17
SS
631841
9870
641711
MS
315920
658
R-Sq = 98.46%
Mean
4943.9
5169.1
5402.8
StDev
20.8
21.5
32.9
F
480.10
P
0.000
R-Sq(adj) = 98.26%
Individual 95% CIs For Mean Based on

Pooled StDev
--+---------+---------+---------+------(-*)
(-*)
(*-)
--+---------+---------+---------+------4950
5100
5250
5400
Pooled StDev = 25.7
Fisher 95% Individual Confidence Intervals

All Pairwise Comparisons among Levels of F Umpan_0.6
Simultaneous confidence level = 88.31%
F Umpan_0.6 = 5.50 subtracted from:

F Umpan_0.6
5.75
6.00
Lower
193.60
427.33
Center
225.17
458.90
Upper
256.74
490.47
---+---------+---------+---------+-----(*-)
(-*-)
---+---------+---------+---------+------200
0
200
400

F Umpan_0.6
6.00
Lower
202.16
Center
233.73
Upper
265.30
---+---------+---------+---------+-----(-*)
---+---------+---------+---------+------200
0
200
400
LAMPIRAN -3C
MTB > Oneway 'Yield AS_0.7' 'F Umpan_0.7';
SUBC>
Fisher 5.
One-way ANOVA: Yield AS_0.7 versus F Umpan_0.7

Source
F Umpan_0.7
Error
Total
S = 24.61
Level
5.50
5.75
6.00
N
6
6
6
DF
2
15
17
SS
619875
9085
628960
MS
309937
606
R-Sq = 98.56%
Mean
4942.8
5167.2
5397.4
StDev
20.1
22.0
30.5
F
511.75
P
0.000
R-Sq(adj) = 98.36%

Pooled StDev
--+---------+---------+---------+------(-*)
(*-)
(-*)
--+---------+---------+---------+------4950
5100
5250
5400
Pooled StDev = 24.6


F Umpan_0.7
---5.75
6.00
*)
Lower
Center
Upper
194.05
424.26
224.33
454.55
254.62
484.83
---+---------+---------+---------+-(*-)
(---+---------+---------+---------+--
----200
200
400

F Umpan_0.7
---6.00
Lower
Center
Upper
199.93
230.21
260.50
---+---------+---------+---------+-(-*)
---+---------+---------+---------+-----200
200
400
LAMPIRAN -3D
One-way ANOVA: Yield AS_5.50 versus IV Umpan_5.50
Source
IV Umpan_5.50
Error
Total
S = 20.45
Level
0.6
0.7
N
6
6
DF
1
10
11
SS
3
4181
4184
MS
3
418
R-Sq = 0.08%
Mean
4943.9
4942.8
StDev
20.8
20.1
F
0.01
P
0.930
R-Sq(adj) = 0.00%

Pooled StDev
------+---------+---------+---------+--(------------------*-----------------)
(------------------*-----------------)
------+---------+---------+---------+--4930
4940
4950
4960
Pooled StDev = 20.4

All Pairwise Comparisons among Levels of IV Umpan_5.50
IV Umpan_5.50 = 0.6 subtracted from:

IV Umpan_5.50
---+0.7
)
Lower
Center
Upper
--------+---------+---------+------
-27.37
-1.06
25.24
(----------------*------------------------+---------+---------+------
---+-15
15
30
LAMPIRAN -3E
Source
IV Umpan_5.75
Error
Total
S = 21.75
Level
0.6
0.7
N
6
6
DF
1
10
11
SS
11
4731
4741
R-Sq = 0.23%
Mean
5169.1
5167.2
StDev
21.5
22.0
MS
11
473
F
0.02
P
0.883
R-Sq(adj) = 0.00%

Pooled StDev
-+---------+---------+---------+-------(----------------*---------------)
(----------------*---------------)
-+---------+---------+---------+-------5148
5160
5172
5184
Pooled StDev = 21.8


IV Umpan_5.75
0.7
Lower
-29.88
Center
-1.90
Upper
26.08
IV Umpan_5.75
0.7
+---------+---------+---------+--------(------------------*-----------------)
+---------+---------+---------+---------30
-15
0
15
MTB > Oneway 'Yield AS_6.00' 'IV Umpan_6.00';

SUBC>
Fisher 5.
LAMPIRAN -3F
Source
IV Umpan_6.00
Error
Total
S = 31.69
Level
0.6
0.7
N
6
6
DF
1
10
11
SS
88
10044
10132
R-Sq = 0.87%
Mean
5402.8
5397.4
StDev
32.9
30.5
MS
88
1004
F
0.09
P
0.773
R-Sq(adj) = 0.00%

Pooled StDev
-----+---------+---------+---------+---(-----------------*-----------------)
(-----------------*-----------------)
-----+---------+---------+---------+---5376
5392
5408
5424
Pooled StDev = 31.7


IV Umpan_6.00
---+0.7
Lower
Center
Upper
--------+---------+---------+------
-46.19
-5.42
35.35
(---------------*---------------)
--------+---------+---------+------
---+-25
25
50
LAMPIRAN -3G
MTB > Oneway 'Yield AS_218' 'F Umpan_218';
SUBC>
Fisher 5.
One-way ANOVA: Yield AS_218 versus F Umpan_218

Source
F Umpan_218
Error
Total
S = 4.024
Level
5.50
5.75
6.00
N
4
4
4
DF
2
9
11
SS
404104.0
145.7
404249.7
MS
202052.0
16.2
R-Sq = 99.96%
Mean
4924.40
5148.00
5373.90
StDev
1.53
3.54
5.81
F
12480.91
P
0.000
R-Sq(adj) = 99.96%
Individual 95% CIs For Mean Based on Pooled

StDev
+---------+---------+---------+--------*)
*
(*
+---------+---------+---------+--------4920
5040
5160
5280
Pooled StDev = 4.02

All Pairwise Comparisons among Levels of F Umpan_218
F Umpan_218 = 5.50 subtracted from:

F Umpan_218
----5.75
6.00
*)
Lower
Center
Upper
217.16
443.06
223.60
449.50
230.04
455.94
--+---------+---------+---------+-*)
--+---------+---------+---------+------200
200
400

F Umpan_218
----6.00
Lower
Center
Upper
--+---------+---------+---------+--
219.46
225.90
232.34
*)
--+---------+---------+---------+--
-----200
200
400
LAMPIRAN -3H
SUBC>
Fisher 5.

Source
F Umpan_220
Error
Total
DF
2
9
11
S = 0.9486
R-Sq = 100.00%
Level
5.50
5.75
6.00
N
4
4
4
SS
403471.6
8.1
403479.7
Mean
4937.05
5161.35
5386.20
StDev
0.84
0.56
1.30
MS
201735.8
0.9
F
224198.66
P
0.000
R-Sq(adj) = 100.00%

Pooled StDev
---------+---------+---------+---------+
*)
*
*
---------+---------+---------+---------+
5040
5160
5280
5400
Pooled StDev = 0.95


F Umpan_220
5.75
6.00
Lower
222.785
447.633
Center
224.303
449.150
Upper
225.820
450.667
F Umpan_220
5.75
6.00
-+---------+---------+---------+-------*
*)
-+---------+---------+---------+--------200
0
200
400

F Umpan_220
6.00
Lower
223.330
Center
224.847
Upper
226.365
F Umpan_220
6.00
-+---------+---------+---------+-------*
-+---------+---------+---------+--------200
0
200
400
LAMPIRAN -3I
SUBC>
Fisher 5.

Source
F Umpan_222
Error
Total
S = 3.521
Level
5.50
5.75
6.00
N
4
4
4
DF
2
9
11
SS
444900.8
111.6
445012.4
MS
222450.4
12.4
R-Sq = 99.97%
Mean
4968.65
5195.00
5440.18
StDev
2.49
1.82
5.26
F
17943.69
P
0.000
R-Sq(adj) = 99.97%

Pooled StDev
------+---------+---------+---------+--*
*
*)
------+---------+---------+---------+--5040
5160
5280
5400
Pooled StDev = 3.52


F Umpan_222
---5.75
6.00
(*
Lower
Center
Upper
220.72
465.89
226.35
471.52
231.98
477.15
---+---------+---------+---------+-*)
---+---------+---------+---------+-----200
200
400

F Umpan_222
---6.00
Lower
Center
Upper
---+---------+---------+---------+--
239.54
245.17
250.80
*)
---+---------+---------+---------+--
----200
200
400
LAMPIRAN -3J
Results for: Worksheet 3
MTB > Oneway 'Yield AS_5.50' 'Suhu B MD_5.50';
SUBC>
Fisher 5.
One-way ANOVA: Yield AS_5.50 versus Suhu B MD_5.50

Source
Suhu B MD_5.50
Error
Total
S = 1.758
Level
218
220
222
N
4
4
4
DF
2
9
11
SS
4156.29
27.81
4184.10
R-Sq = 99.34%
Mean
4924.40
4937.05
4968.65
StDev
1.53
0.84
2.49
MS
2078.14
3.09
F
672.52
P
0.000
R-Sq(adj) = 99.19%

Pooled StDev
--------+---------+---------+---------+(*)
(*-)
(*-)
--------+---------+---------+---------+4935
4950
4965
4980
Pooled StDev = 1.76

All Pairwise Comparisons among Levels of Suhu B MD_5.50
Suhu B MD_5.50 = 218 subtracted from:

Suhu B
MD_5.50
220
222
Lower
9.838
41.442
Center
12.650
44.254
Upper
15.462
47.066
----+---------+---------+---------+----(*)
(*)
----+---------+---------+---------+-----25
0
25
50

Suhu B
MD_5.50
222
Lower
28.792
Center
31.604
Upper
34.416
----+---------+---------+---------+----(*)
----+---------+---------+---------+-----25
0
25
50
LAMPIRAN -3K
SUBC>
Fisher 5.

Source
Suhu B MD_5.75
Error
Total
S = 2.318
Level
218
220
222
N
4
4
4
DF
2
9
11
SS
4693.13
48.35
4741.48
R-Sq = 98.98%
Mean
5148.00
5161.35
5195.00
StDev
3.54
0.56
1.82
MS
2346.56
5.37
F
436.76
P
0.000
R-Sq(adj) = 98.75%

StDev
+---------+---------+---------+--------(-*-)
(-*-)
(*-)
+---------+---------+---------+--------5145
5160
5175
5190
Pooled StDev = 2.32


Suhu B
MD_5.75
220
222
Lower
9.645
43.295
Center
13.352
47.003
Upper
17.060
50.710
-----+---------+---------+---------+---(*-)
(-*)
-----+---------+---------+---------+----25
0
25
50

Suhu B
MD_5.75
222
Lower
29.942
Center
33.650
Upper
37.358
-----+---------+---------+---------+---(*-)
-----+---------+---------+---------+----25
0
25
50
LAMPIRAN -3L
SUBC>
Fisher 5.

Source
Suhu B MD_6.00
Error
Total
S = 4.585
Level
218
220
222
N
4
4
4
DF
2
9
11
SS
9942.6
189.2
10131.8
R-Sq = 98.13%
Mean
5373.90
5386.20
5440.18
StDev
5.81
1.30
5.26
MS
4971.3
21.0
F
236.47
P
0.000
R-Sq(adj) = 97.72%

Pooled StDev
------+---------+---------+---------+--(--*--)
(-*--)
(--*--)
------+---------+---------+---------+--5380
5400
5420
5440
Pooled StDev = 4.59


Suhu B
MD_6.00
220
222
Lower
4.966
58.941
Center
12.300
66.275
Upper
19.634
73.609
--------+---------+---------+---------+(--*-)
(-*-)
--------+---------+---------+---------+-35
0
35
70

Suhu B
MD_6.00
222
Lower
46.641
Center
53.975
Upper
61.309
--------+---------+---------+---------+(-*--)
--------+---------+---------+---------+-35
0
35
70
LAMPIRAN -3M
SUBC>
Fisher 5.

Source
Suhu B MD_0.6
Error
Total
S = 205.3
Level
218
220
222
N
6
6
6
DF
2
15
17
SS
9322
632389
641711
R-Sq = 1.45%
Mean
5150.8
5161.5
5203.5
StDev
202.2
201.1
212.5
MS
4661
42159
F
0.11
P
0.896
R-Sq(adj) = 0.00%

Pooled StDev
------+---------+---------+---------+--(--------------*--------------)
(--------------*--------------)
(--------------*--------------)
------+---------+---------+---------+--5040
5160
5280
5400
Pooled StDev = 205.3


Suhu B
MD_0.6
220
222
Lower
-241.9
-199.9
Center
10.8
52.8
Upper
263.4
305.4
--------+---------+---------+---------+(---------------*--------------)
(--------------*---------------)
--------+---------+---------+---------+-160
0
160
320

Suhu B
MD_0.6
222
Lower
-210.7
Center
42.0
Upper
294.7
--------+---------+---------+---------+(---------------*--------------)
--------+---------+---------+---------+-160
0
160
320
LAMPIRAN -3N
SUBC>
Fisher 5.

Source
Suhu B MD_0.7
Error
Total
S = 203.3
Level
218
220
222
N
6
6
6
DF
2
15
17
SS
8714
620246
628960
R-Sq = 1.39%
Mean
5146.8
5161.6
5199.1
StDev
199.9
200.6
209.4
MS
4357
41350
F
0.11
P
0.901
R-Sq(adj) = 0.00%

Pooled StDev
------+---------+---------+---------+--(--------------*--------------)
(--------------*--------------)
(-------------*--------------)
------+---------+---------+---------+--5040
5160
5280
5400


Suhu B
MD_0.7
220
222
Lower
-235.5
-198.0
Center
14.8
52.3
Upper
265.0
302.5
---------+---------+---------+---------+
(----------------*----------------)
(---------------*----------------)
---------+---------+---------+---------+
-150
0
150
300

Suhu B
MD_0.7
222
Lower
-212.7
Center
37.5
Upper
287.7
---------+---------+---------+---------+
(----------------*---------------)
---------+---------+---------+---------+
-150
0
150
300
LAMPIRAN -3O
MTB > Oneway 'Yield AS_218' 'IV Umpan_218';
SUBC>
Fisher 5.
One-way ANOVA: Yield AS_218 versus IV Umpan_218

Source
IV Umpan_218
Error
Total
S = 201.0
Level
0.6
0.7
N
6
6
DF
1
10
11
SS
47
404203
404250
R-Sq = 0.01%
Mean
5150.8
5146.8
StDev
202.2
199.9
MS
47
40420
F
0.00
P
0.973
R-Sq(adj) = 0.00%

Pooled StDev
----+---------+---------+---------+----(-----------------*-----------------)
(------------------*-----------------)
----+---------+---------+---------+----5000
5100
5200
5300

All Pairwise Comparisons among Levels of IV Umpan_218
IV Umpan_218 = 0.6 subtracted from:

IV Umpan_218
--+0.7
Lower
Center
Upper
--------+---------+---------+-------
-262.6
-4.0
254.7
(-----------------*----------------)
--------+---------+---------+-------
--+-150
150
300
LAMPIRAN -3P
SUBC>
Fisher 5.

Source
IV Umpan_220
Error
Total
S = 200.9
Level
0.6
0.7
N
6
6
DF
1
10
11
SS
0
403480
403480
R-Sq = 0.00%
Mean
5161.5
5161.6
StDev
201.1
200.6
MS
0
40348
F
0.00
P
1.000
R-Sq(adj) = 0.00%

Pooled StDev
--+---------+---------+---------+------(-----------------*-----------------)
(-----------------*-----------------)
--+---------+---------+---------+------5000
5100
5200
5300


IV Umpan_220
-+-0.7
Lower
Center
Upper
-------+---------+---------+--------
-258.4
0.0
258.4
(----------------*----------------)
-------+---------+---------+--------
-+--150
150
300
LAMPIRAN -3Q
SUBC>
Fisher 5.

Source
IV Umpan_222
Error
Total
S = 210.9
Level
0.6
0.7
N
6
6
DF
1
10
11
SS
59
444953
445012
R-Sq = 0.01%
Mean
5203.5
5199.1
StDev
212.5
209.4
MS
59
44495
F
0.00
P
0.972
R-Sq(adj) = 0.00%

Pooled StDev
---------+---------+---------+---------+
(------------------*-------------------)
(------------------*------------------)
---------+---------+---------+---------+
5100
5200
5300
5400


IV Umpan_222
--+0.7
)
Lower
Center
Upper
--------+---------+---------+-------
-275.8
-4.4
266.9
(-----------------*-----------------
--------+---------+---------+--------+-150
150
300
MTB > Save "C:\Program Files\MINITAB 14\Data\MINITAB.MPJ.26";
SUBC>
Project;
SUBC>
Replace.
5/10/2009 5:57:13 PM
LAMPIRAN -4A
7/13/2009 9:33:10 PM
Welcome to Minitab, press F1 for help.
General Linear Model: IV DAS versus F Umpan, IV Umpan, Suhu B MD

Factor
F Umpan
IV Umpan
Suhu B MD
Type
fixed
fixed
fixed
Levels
3
2
3
Values
5.50, 5.75, 6.00
0.6, 0.7
218, 220, 222
Analysis of Variance for IV DAS, using Adjusted SS for Tests

Source
P
F Umpan
0.000
IV Umpan
0.010
Suhu B MD
0.000
F Umpan*IV Umpan
0.920
F Umpan*Suhu B MD
0.679
IV Umpan*Suhu B MD
0.920
0.986
Error
Total
DF
Seq SS
Adj SS
Adj MS
0.0012056
0.0012056
0.0006028
18.08
0.0002778
0.0002778
0.0002778
8.33
0.0012722
0.0012722
0.0006361
19.08
0.0000056
0.0000056
0.0000028
0.08
0.0000778
0.0000778
0.0000194
0.58
0.0000056
0.0000056
0.0000028
0.08
0.0000111
0.0000111
0.0000028
0.08
18
35
0.0006000
0.0034556
0.0006000
0.0000333
S = 0.00577350
R-Sq = 82.64%
R-Sq(adj) = 66.24%
LAMPIRAN -4B
One-way ANOVA: IV DAS_0.6 versus F Umpan_0.6
Source
F Umpan_0.6
Error
Total
S = 0.007746
Level
5.50
5.75
6.00
N
6
6
6
DF
2
15
17
SS
0.0006778
0.0009000
0.0015778
MS
0.0003389
0.0000600
R-Sq = 42.96%
Mean
0.15333
0.16167
0.16833
StDev
0.00816
0.00753
0.00753
F
5.65
P
0.015
R-Sq(adj) = 35.35%

Pooled StDev
-------+---------+---------+---------+-(--------*-------)
(-------*--------)
(-------*--------)
-------+---------+---------+---------+-0.1520
0.1600
0.1680
0.1760


F Umpan_0.6
5.75
6.00
Lower
-0.001199
0.005468
Center
0.008333
0.015000
Upper
0.017865
0.024532
F Umpan_0.6
5.75
6.00
---+---------+---------+---------+-----(-------*-------)
(------*-------)
---+---------+---------+---------+------0.012
0.000
0.012
0.024

F Umpan_0.6
6.00
Lower
-0.002865
F Umpan_0.6
6.00
---+---------+---------+---------+-----(-------*------)
---+---------+---------+---------+------0.012
0.000
0.012
0.024
Center
0.006667
Upper
0.016199
LAMPIRAN -4C
One-way ANOVA: IV DAS_0.7 versus F Umpan_0.7
Source
F Umpan_0.7
Error
Total
S = 0.008433
Level
5.50
5.75
6.00
N
6
6
6
DF
2
15
17
SS
0.0005333
0.0010667
0.0016000
MS
0.0002667
0.0000711
R-Sq = 33.33%
Mean
0.16000
0.16667
0.17333
StDev
0.01095
0.00516
0.00816
F
3.75
P
0.048
R-Sq(adj) = 24.44%

StDev
---------+---------+---------+---------+
(--------*--------)
(--------*---------)
(---------*--------)
---------+---------+---------+---------+
0.1600
0.1680
0.1760
0.1840


F Umpan_0.7
5.75
6.00
Lower
-0.003711
0.002956
Center
0.006667
0.013333
Upper
0.017044
0.023711
F Umpan_0.7
5.75
6.00
----+---------+---------+---------+----(--------*-------)
(--------*--------)
----+---------+---------+---------+-----0.012
0.000
0.012
0.024

F Umpan_0.7
6.00
Lower
-0.003711
Center
0.006667
Upper
0.017044
F Umpan_0.7
6.00
----+---------+---------+---------+----(--------*-------)
----+---------+---------+---------+-----0.012
0.000
0.012
0.024
LAMPIRAN -4D
One-way ANOVA: IV DAS_5.50 versus IV Umpan_5.50
Source
IV Umpan_5.50
Error
Total
DF
1
10
11
S = 0.009661
R-Sq = 12.50%
Level
0.6
0.7
N
6
6
Mean
0.15333
0.16000
SS
0.0001333
0.0009333
0.0010667
StDev
0.00816
0.01095
MS
0.0001333
0.0000933
F
1.43
P
0.260
R-Sq(adj) = 3.75%

Pooled StDev
----+---------+---------+---------+----(------------*------------)
(------------*-----------)
----+---------+---------+---------+----0.1470
0.1540
0.1610
0.1680


IV Umpan_5.50
0.7
Lower
-0.005761
Center
0.006667
Upper
0.019095
IV Umpan_5.50
0.7
------+---------+---------+---------+--(--------------*---------------)
------+---------+---------+---------+---0.0080
0.0000
0.0080
0.0160
LAMPIRAN -4E
Source
IV Umpan_5.75
Error
Total
DF
1
10
11
S = 0.006455
R-Sq = 15.25%
Level
0.6
0.7
N
6
6
Mean
0.16167
0.16667
SS
0.0000750
0.0004167
0.0004917
StDev
0.00753
0.00516
MS
0.0000750
0.0000417
F
1.80
P
0.209
R-Sq(adj) = 6.78%

Pooled StDev
--------+---------+---------+---------+(----------*-----------)
(----------*-----------)
--------+---------+---------+---------+0.1600
0.1650
0.1700
0.1750


IV Umpan_5.75
0.7
Lower
-0.003304
Center
0.005000
Upper
0.013304
IV Umpan_5.75
0.7
----+---------+---------+---------+----(-------------*-------------)
----+---------+---------+---------+-----0.0060
0.0000
0.0060
0.0120
LAMPIRAN -4F
Source
IV Umpan_6.00
Error
Total
DF
1
10
11
S = 0.007853
R-Sq = 10.84%
Level
0.6
0.7
N
6
6
Mean
0.16833
0.17333
SS
0.0000750
0.0006167
0.0006917
StDev
0.00753
0.00816
MS
0.0000750
0.0000617
F
1.22
P
0.296
R-Sq(adj) = 1.93%

Pooled StDev
--------+---------+---------+---------+(--------------*-------------)
(--------------*-------------)
--------+---------+---------+---------+0.1650
0.1700
0.1750
0.1800


IV Umpan_6.00
0.7
Lower
-0.005102
Center
0.005000
Upper
0.015102
IV Umpan_6.00
0.7
----+---------+---------+---------+----(-------------*--------------)
----+---------+---------+---------+-----0.0070
0.0000
0.0070
0.0140
LAMPIRAN -4G
One-way ANOVA: IV DAS_218 versus F Umpan_218
Source
F Umpan_218
Error
Total
S = 0.005
Level
5.50
5.75
6.00
N
4
4
4
DF
2
9
11
SS
0.0004667
0.0002250
0.0006917
R-Sq = 67.47%
Mean
0.14750
0.15750
0.16250
StDev
0.00500
0.00500
0.00500
MS
0.0002333
0.0000250
F
9.33
P
0.006
R-Sq(adj) = 60.24%

Pooled StDev
-------+---------+---------+---------+-(-------*-------)
(-------*-------)
(-------*-------)
-------+---------+---------+---------+-0.1470
0.1540
0.1610
0.1680


F Umpan_218
5.75
6.00
Lower
0.002002
0.007002
Center
0.010000
0.015000
Upper
0.017998
0.022998
F Umpan_218
5.75
6.00
---+---------+---------+---------+-----(-------*-------)
(-------*-------)
---+---------+---------+---------+------0.010
0.000
0.010
0.020

F Umpan_218
6.00
Lower
-0.002998
F Umpan_218
6.00
---+---------+---------+---------+-----(-------*-------)
---+---------+---------+---------+------0.010
0.000
0.010
0.020
Center
0.005000
Upper
0.012998
LAMPIRAN -4H
Source
F Umpan_220
Error
Total
S = 0.006872
Level
5.50
5.75
6.00
N
4
4
4
DF
2
9
11
SS
0.0004667
0.0004250
0.0008917
MS
0.0002333
0.0000472
R-Sq = 52.34%
Mean
0.15750
0.16750
0.17250
StDev
0.00957
0.00500
0.00500
F
4.94
P
0.036
R-Sq(adj) = 41.74%

Pooled StDev
---+---------+---------+---------+-----(---------*---------)
(--------*---------)
(---------*--------)
---+---------+---------+---------+-----0.1520
0.1600
0.1680
0.1760


F Umpan_220
5.75
6.00
Lower
-0.000992
0.004008
Center
0.010000
0.015000
Upper
0.020992
0.025992
F Umpan_220
5.75
6.00
---+---------+---------+---------+-----(--------*--------)
(---------*--------)
---+---------+---------+---------+------0.012
0.000
0.012
0.024

F Umpan_220
6.00
Lower
-0.005992
Center
0.005000
F Umpan_220
6.00
---+---------+---------+---------+-----(--------*--------)
---+---------+---------+---------+------0.012
0.000
0.012
0.024
Upper
0.015992
LAMPIRAN -4I
Source
F Umpan_222
Error
Total
S = 0.005270
Level
5.50
5.75
6.00
N
4
4
4
DF
2
9
11
SS
0.0003500
0.0002500
0.0006000
MS
0.0001750
0.0000278
R-Sq = 58.33%
Mean
0.16500
0.16750
0.17750
StDev
0.00577
0.00500
0.00500
F
6.30
P
0.019
R-Sq(adj) = 49.07%

Pooled StDev
---+---------+---------+---------+-----(--------*-------)
(-------*--------)
(--------*-------)
---+---------+---------+---------+------
0.1610
0.1680
0.1750
0.1820


F Umpan_222
5.75
6.00
Lower
-0.005931
0.004069
Center
0.002500
0.012500
Upper
0.010931
0.020931
F Umpan_222
5.75
6.00
--------+---------+---------+---------+(--------*-------)
(-------*--------)
--------+---------+---------+---------+-0.010
0.000
0.010
0.020

F Umpan_222
6.00
Lower
0.001569
Center
0.010000
Upper
0.018431
F Umpan_222
6.00
--------+---------+---------+---------+(-------*-------)
--------+---------+---------+---------+-0.010
0.000
0.010
0.020
LAMPIRAN -4J
One-way ANOVA: IV DAS_5.50 versus Suhu B MD_5.50
Source
Suhu B MD_5.50
Error
Total
S = 0.007071
DF
2
9
11
SS
0.0006167
0.0004500
0.0010667
R-Sq = 57.81%
MS
0.0003083
0.0000500
F
6.17
P
0.021
R-Sq(adj) = 48.44%

Pooled StDev
Level
218
220
222
N
4
4
4
Mean
0.14750
0.15750
0.16500
StDev
0.00500
0.00957
0.00577
+---------+---------+---------+--------(------*-------)
(------*-------)
(-------*-------)
+---------+---------+---------+--------0.140
0.150
0.160
0.170


Suhu B
MD_5.50
220
222
Suhu B
MD_5.50
220
222
Lower
-0.001311
0.006189
Center
0.010000
0.017500
Upper
0.021311
0.028811
------+---------+---------+---------+--(--------*---------)
(---------*--------)
------+---------+---------+---------+---0.012
0.000
0.012
0.024

Suhu B
MD_5.50
222
Suhu B
MD_5.50
222
Lower
-0.003811
Center
0.007500
Upper
0.018811
------+---------+---------+---------+--(--------*---------)
------+---------+---------+---------+---0.012
0.000
0.012
0.024
LAMPIRAN -4K
Source
Suhu B MD_5.75
Error
Total
S = 0.005
DF
2
9
11
SS
0.0002667
0.0002250
0.0004917
R-Sq = 54.24%
MS
0.0001333
0.0000250
F
5.33
P
0.030
R-Sq(adj) = 44.07%

Pooled StDev
Level
218
220
222
N
4
4
4
Mean
0.15750
0.16750
0.16750
StDev
0.00500
0.00500
0.00500
-------+---------+---------+---------+-(---------*--------)
(--------*---------)
(--------*---------)
-------+---------+---------+---------+-0.1560
0.1620
0.1680
0.1740


Suhu B
MD_5.75
220
222
Suhu B
MD_5.75
220
222
Lower
0.002002
0.002002
Center
0.010000
0.010000
Upper
0.017998
0.017998
-+---------+---------+---------+-------(----------*-----------)
(----------*-----------)
-+---------+---------+---------+--------0.0070
0.0000
0.0070
0.0140

Suhu B
MD_5.75
222
Suhu B
MD_5.75
222
Lower
-0.007998
Center
0.000000
Upper
0.007998
-+---------+---------+---------+-------(----------*----------)
-+---------+---------+---------+--------0.0070
0.0000
0.0070
0.0140
LAMPIRAN -4L
Source
Suhu B MD_6.00
Error
Total
S = 0.005
DF
2
9
11
SS
0.0004667
0.0002250
0.0006917
R-Sq = 67.47%
MS
0.0002333
0.0000250
F
9.33
P
0.006
R-Sq(adj) = 60.24%
Level
218
220
222
N
4
4
4
Mean
0.16250
0.17250
0.17750
StDev
0.00500
0.00500
0.00500

Pooled StDev
------+---------+---------+---------+--(-------*-------)
(-------*--------)
(--------*-------)
------+---------+---------+---------+--0.1610
0.1680
0.1750
0.1820


Suhu B
MD_6.00
+-----220
222
--)
Lower
Center
Upper
0.002002
0.007002
0.010000
0.015000
0.017998
0.022998
---+---------+---------+--------(-------*-------)
(-------*-------+---------+---------+---------
+------0.010
0.000
0.010
0.020

Suhu B
MD_6.00
222
Suhu B
MD_6.00
222
Lower
-0.002998
Center
0.005000
Upper
0.012998
---+---------+---------+---------+-----(-------*-------)
---+---------+---------+---------+------0.010
0.000
0.010
0.020
LAMPIRAN -4M
Source
DF
SS
MS
Suhu B MD_0.6
Error
Total
2
15
17
S = 0.008165
R-Sq = 36.62%
Level
218
220
222
N
6
6
6
Mean
0.15333
0.16333
0.16667
0.0005778
0.0010000
0.0015778
StDev
0.00816
0.00816
0.00816
0.0002889
0.0000667
4.33
0.033
R-Sq(adj) = 28.17%

Pooled StDev
-+---------+---------+---------+-------(---------*---------)
(---------*---------)
(---------*---------)
-+---------+---------+---------+-------0.1470
0.1540
0.1610
0.1680


Suhu B
MD_0.6
Lower
+-----220
-0.000048
222
0.003286
--)
Center
Upper
0.010000
0.013333
0.020048
0.023381
---+---------+---------+--------(---------*---------)
(---------*---------+---------+---------+---------
+------0.010
0.000
0.010
0.020

Suhu B
MD_0.6
Lower
+-----222
-0.006714
Center
Upper
---+---------+---------+---------
0.003333
0.013381
(---------*---------)
---+---------+---------+---------
+------0.010
0.000
0.010
0.020
LAMPIRAN -4N
Source
Suhu B MD_0.7
Error
Total
DF
2
15
17
S = 0.007746
R-Sq = 43.75%
Level
218
220
222
N
6
6
6
Mean
0.15833
0.16833
0.17333
SS
0.0007000
0.0009000
0.0016000
StDev
0.00753
0.00983
0.00516
MS
0.0003500
0.0000600
F
5.83
P
0.013
R-Sq(adj) = 36.25%

Pooled StDev
-+---------+---------+---------+-------(--------*-------)
(-------*--------)
(--------*-------)
-+---------+---------+---------+-------0.1520
0.1600
0.1680
0.1760


Suhu B
MD_0.7
+---220
)
222
-----)
Lower
Center
Upper
-----+---------+---------+---------
0.000468
0.010000
0.019532
(---------*---------
0.005468
0.015000
0.024532
(---------*--------+---------+---------+---------
+----0.010
0.000
0.010
0.020

Suhu B
MD_0.7
-+---222
Lower
Center
Upper
-----+---------+---------+--------
-0.004532
0.005000
0.014532
(---------*---------)
-----+---------+---------+--------
-+----0.010
0.000
0.010
0.020
LAMPIRAN -4O
One-way ANOVA: IV DAS_218 versus IV Umpan_218
Source
IV Umpan_218
Error
Total
S = 0.007853
Level
0.6
0.7
N
6
6
DF
1
10
11
SS
0.0000750
0.0006167
0.0006917
MS
0.0000750
0.0000617
R-Sq = 10.84%
Mean
0.15333
0.15833
StDev
0.00816
0.00753
F
1.22
P
0.296
R-Sq(adj) = 1.93%

Pooled StDev
--------+---------+---------+---------+(--------------*-------------)
(--------------*-------------)
--------+---------+---------+---------+0.1500
0.1550
0.1600
0.1650


IV Umpan_218
0.7
Lower
-0.005102
Center
0.005000
Upper
0.015102
IV Umpan_218
0.7
----+---------+---------+---------+----(-------------*--------------)
----+---------+---------+---------+-----0.0070
0.0000
0.0070
0.0140
LAMPIRAN -4P
Source
IV Umpan_220
Error
Total
S = 0.009037
Level
0.6
0.7
N
6
6
DF
1
10
11
SS
0.0000750
0.0008167
0.0008917
R-Sq = 8.41%
Mean
0.16333
0.16833
StDev
0.00816
0.00983
MS
0.0000750
0.0000817
F
0.92
P
0.360
R-Sq(adj) = 0.00%

Pooled StDev
-+---------+---------+---------+-------(------------*-------------)
(-------------*------------)
-+---------+---------+---------+-------0.1560
0.1620
0.1680
0.1740


IV Umpan_220
0.7
Lower
-0.006625
Center
0.005000
IV Umpan_220
0.7
-----+---------+---------+---------+---(-------------*--------------)
-----+---------+---------+---------+----0.0080
0.0000
0.0080
0.0160
Upper
0.016625
LAMPIRAN -4Q
Source
IV Umpan_222
Error
Total
S = 0.006831
Level
0.6
0.7
N
6
6
DF
1
10
11
SS
0.0001333
0.0004667
0.0006000
MS
0.0001333
0.0000467
R-Sq = 22.22%
Mean
0.16667
0.17333
StDev
0.00816
0.00516
F
2.86
P
0.122
R-Sq(adj) = 14.44%

StDev
---------+---------+---------+---------+
(-----------*------------)
(------------*-----------)
---------+---------+---------+---------+
0.1650
0.1700
0.1750
0.1800


IV Umpan_222
0.7
Lower
-0.002121
Center
0.006667
Upper
0.015455
IV Umpan_222
0.7
---+---------+---------+---------+-----(------------*-----------)
---+---------+---------+---------+------0.0070
0.0000
0.0070
0.0140
7/14/2009 5:49:26 AM
LAMPIRAN 5A
7/29/2009 8:24:37 AM
General Linear Model: HS DAS, Red versus F Umpan, IV Umpan, Suhu B

MD
Factor
F Umpan
IV Umpan
Suhu B MD
Type
fixed
fixed
fixed
Levels
3
2
3
Values
5.50, 5.75, 6.00
0.6, 0.7
218, 220, 222
Analysis of Variance for HS DAS, Red, using Adjusted SS for Tests

Source
P
F Umpan
0.000
IV Umpan
0.000
Suhu B MD
0.000
F Umpan*IV Umpan
0.387
F Umpan*Suhu B MD
0.964
IV Umpan*Suhu B MD
0.868
0.964
Error
Total
S = 0.0440959
DF
Seq SS
Adj SS
Adj MS
0.107222
0.107222
0.053611
27.57
0.046944
0.046944
0.046944
24.14
0.060556
0.060556
0.030278
15.57
0.003889
0.003889
0.001944
1.00
0.001111
0.001111
0.000278
0.14
0.000556
0.000556
0.000278
0.14
0.001111
0.001111
0.000278
0.14
18
35
0.035000
0.256389
0.035000
0.001944
R-Sq = 86.35%
R-Sq(adj) = 73.46%
LAMPIRAN 5B
One-way ANOVA: HS DAS, Red_0.6 versus F Umpan_0.6
Source
F Umpan_0.6
Error
Total
S = 0.05774
Level
5.50
5.75
6.00
N
6
6
6
DF
2
15
17
SS
0.07000
0.05000
0.12000
MS
0.03500
0.00333
R-Sq = 58.33%
Mean
0.35000
0.45000
0.50000
StDev
0.05477
0.05477
0.06325
F
10.50
P
0.001
R-Sq(adj) = 52.78%

Pooled StDev
-------+---------+---------+---------+-(------*------)
(------*------)
(------*-------)
-------+---------+---------+---------+-0.350
0.420
0.490
0.560


F Umpan_0.6
5.75
6.00
Lower
0.02895
0.07895
F Umpan_0.6
5.75
6.00
--+---------+---------+---------+------(------*------)
(------*------)
--+---------+---------+---------+-------0.10
0.00
0.10
0.20
Center
0.10000
0.15000
Upper
0.17105
0.22105

F Umpan_0.6
6.00
Lower
-0.02105
Center
0.05000
Upper
0.12105
F Umpan_0.6
6.00
--+---------+---------+---------+------(------*------)
--+---------+---------+---------+-------0.10
0.00
0.10
0.20
LAMPIRAN 5C
One-way ANOVA: HS DAS, Red_0.7 versus F Umpan_0.7
Source
F Umpan_0.7
Error
Total
S = 0.05676
Level
5.50
5.75
6.00
N
6
6
6
DF
2
15
17
SS
0.04111
0.04833
0.08944
MS
0.02056
0.00322
R-Sq = 45.96%
Mean
0.45000
0.50000
0.56667
StDev
0.05477
0.06325
0.05164
F
6.38
P
0.010
R-Sq(adj) = 38.76%

Pooled StDev
---+---------+---------+---------+-----(-------*-------)
(-------*--------)
(-------*--------)
---+---------+---------+---------+-----0.420
0.480
0.540
0.600


F Umpan_0.7
5.75
6.00
Lower
-0.01985
0.04681
Center
0.05000
0.11667
Upper
0.11985
0.18652
F Umpan_0.7
5.75
6.00
----+---------+---------+---------+----(------*------)
(------*------)
----+---------+---------+---------+-----0.10
0.00
0.10
0.20

F Umpan_0.7
Lower
Center
Upper
6.00
-0.00319
0.06667
0.13652
F Umpan_0.7
6.00
----+---------+---------+---------+----(------*------)
----+---------+---------+---------+-----0.10
0.00
0.10
0.20
LAMPIRAN 5D
One-way ANOVA: HS DAS, Red_5.50 versus IV Umpan_5.50
Source
IV Umpan_5.50
Error
Total
S = 0.05477
Level
0.6
0.7
N
6
6
DF
1
10
11
SS
0.03000
0.03000
0.06000
R-Sq = 50.00%
Mean
0.35000
0.45000
StDev
0.05477
0.05477
MS
0.03000
0.00300
F
10.00
P
0.010
R-Sq(adj) = 45.00%

StDev
+---------+---------+---------+--------(---------*---------)
(---------*---------)
+---------+---------+---------+--------0.300
0.350
0.400
0.450


IV Umpan_5.50
0.7
Lower
0.02954
Center
0.10000
Upper
0.17046
IV Umpan_5.50
0.7
+---------+---------+---------+--------(---------*---------)
+---------+---------+---------+---------0.070
0.000
0.070
0.140
LAMPIRAN 5D
Source
IV Umpan_5.75
Error
Total
S = 0.05916
Level
0.6
0.7
N
6
6
DF
1
10
11
SS
0.00750
0.03500
0.04250
R-Sq = 17.65%
Mean
0.45000
0.50000
StDev
0.05477
0.06325
MS
0.00750
0.00350
F
2.14
P
0.174
R-Sq(adj) = 9.41%

Pooled StDev
-+---------+---------+---------+-------(-------------*------------)
(------------*------------)
-+---------+---------+---------+-------0.400
0.440
0.480
0.520


IV Umpan_5.75
0.7
Lower
-0.02611
Center
0.05000
Upper
0.12611
IV Umpan_5.75
0.7
---+---------+---------+---------+-----(-----------*------------)
---+---------+---------+---------+------0.060
0.000
0.060
0.120
LAMPIRAN 5E
Source
IV Umpan_6.00
Error
Total
S = 0.05774
Level
0.6
0.7
N
6
6
DF
1
10
11
SS
0.01333
0.03333
0.04667
R-Sq = 28.57%
Mean
0.50000
0.56667
StDev
0.06325
0.05164
MS
0.01333
0.00333
F
4.00
P
0.073
R-Sq(adj) = 21.43%

Pooled StDev
-+---------+---------+---------+-------(----------*----------)
(---------*----------)
-+---------+---------+---------+-------0.450
0.500
0.550
0.600


IV Umpan_6.00
0.7
Lower
-0.00760
Center
0.06667
Upper
0.14094
IV Umpan_6.00
0.7
--+---------+---------+---------+------(-----------*-----------)
--+---------+---------+---------+-------0.060
0.000
0.060
0.120
LAMPIRAN 5F
One-way ANOVA: HS DAS, Red_218 versus F Umpan_218
Source
F Umpan_218
Error
Total
S = 0.05270
Level
5.50
5.75
6.00
N
4
4
4
DF
2
9
11
SS
0.03167
0.02500
0.05667
MS
0.01583
0.00278
R-Sq = 55.88%
Mean
0.35000
0.42500
0.47500
StDev
0.05774
0.05000
0.05000
F
5.70
P
0.025
R-Sq(adj) = 46.08%

Pooled StDev
---------+---------+---------+---------+
(--------*--------)
(--------*-------)
(--------*-------)
---------+---------+---------+---------+
0.350
0.420
0.490
0.560


F Umpan_218
5.75
6.00
Lower
-0.00931
0.04069
Center
0.07500
0.12500
Upper
0.15931
0.20931
F Umpan_218
5.75
---+---------+---------+---------+-----(--------*-------)
6.00
(-------*--------)
---+---------+---------+---------+------0.10
0.00
0.10
0.20

F Umpan_218
6.00
Lower
-0.03431
F Umpan_218
6.00
---+---------+---------+---------+-----(-------*-------)
---+---------+---------+---------+------0.10
0.00
0.10
0.20
Center
0.05000
Upper
0.13431
LAMPIRAN 5G
Source
F Umpan_220
Error
Total
S = 0.06455
Level
5.50
5.75
6.00
N
4
4
4
DF
2
9
11
SS
0.04500
0.03750
0.08250
MS
0.02250
0.00417
R-Sq = 54.55%
Mean
0.40000
0.47500
0.55000
StDev
0.08165
0.05000
0.05774
F
5.40
P
0.029
R-Sq(adj) = 44.44%

Pooled StDev
---------+---------+---------+---------+
(--------*--------)
(--------*---------)
(--------*--------)
---------+---------+---------+---------+
0.400
0.480
0.560
0.640


F Umpan_220
5.75
6.00
Lower
-0.02825
0.04675
Center
0.07500
0.15000
Upper
0.17825
0.25325
F Umpan_220
5.75
6.00
-----+---------+---------+---------+---(-------*--------)
(--------*-------)
-----+---------+---------+---------+----0.12
0.00
0.12
0.24

F Umpan_220
6.00
Lower
-0.02825
Center
0.07500
Upper
0.17825
F Umpan_220
6.00
-----+---------+---------+---------+---(-------*--------)
-----+---------+---------+---------+----0.12
0.00
0.12
0.24
LAMPIRAN 5H
Source
F Umpan_222
Error
Total
S = 0.05270
Level
5.50
5.75
6.00
N
4
4
4
DF
2
9
11
SS
0.03167
0.02500
0.05667
MS
0.01583
0.00278
R-Sq = 55.88%
Mean
0.45000
0.52500
0.57500
StDev
0.05774
0.05000
0.05000
F
5.70
P
0.025
R-Sq(adj) = 46.08%

Pooled StDev
----+---------+---------+---------+----(-------*--------)
(--------*--------)
(-------*--------)
----+---------+---------+---------+----0.420
0.490
0.560
0.630


F Umpan_222
5.75
6.00
Lower
-0.00931
0.04069
Center
0.07500
0.12500
Upper
0.15931
0.20931
F Umpan_222
---+---------+---------+---------+------
5.75
6.00
(--------*-------)
(-------*--------)
---+---------+---------+---------+------0.10
0.00
0.10
0.20

F Umpan_222
6.00
Lower
-0.03431
Center
0.05000
Upper
0.13431
F Umpan_222
6.00
---+---------+---------+---------+-----(-------*-------)
---+---------+---------+---------+------0.10
0.00
0.10
0.20
LAMPIRAN 5I
One-way ANOVA: HS DAS, Red_5.50 versus Suhu B MD_5.50
Source
Suhu B MD_5.50
Error
Total
S = 0.06667
Level
218
220
222
N
4
4
4
DF
2
9
11
SS
0.02000
0.04000
0.06000
R-Sq = 33.33%
Mean
0.35000
0.40000
0.45000
StDev
0.05774
0.08165
0.05774
MS
0.01000
0.00444
F
2.25
P
0.161
R-Sq(adj) = 18.52%

Pooled StDev
-+---------+---------+---------+-------(----------*----------)
(----------*----------)
(---------*----------)
-+---------+---------+---------+-------0.280
0.350
0.420
0.490


Suhu B
MD_5.50
+--220
222
-)
Lower
Center
Upper
------+---------+---------+---------
-0.05664
-0.00664
0.05000
0.10000
0.15664
0.20664
(----------*----------)
(----------*--------------+---------+---------+---------
+---0.10
0.00
0.10
0.20

Suhu B
MD_5.50
+--222
Lower
Center
Upper
------+---------+---------+---------
-0.05664
0.05000
0.15664
(----------*----------)
------+---------+---------+---------
+---0.10
0.00
0.10
0.20
LAMPIRAN 5J
Source
Suhu B MD_5.75
Error
Total
S = 0.05
Level
218
220
222
N
4
4
4
DF
2
9
11
SS
0.02000
0.02250
0.04250
R-Sq = 47.06%
Mean
0.42500
0.47500
0.52500
StDev
0.05000
0.05000
0.05000
MS
0.01000
0.00250
F
4.00
P
0.057
R-Sq(adj) = 35.29%

Pooled StDev
---------+---------+---------+---------+
(---------*--------)
(--------*---------)
(---------*--------)
---------+---------+---------+---------+
0.420
0.480
0.540
0.600


Suhu B
MD_5.75
+--220
222
--)
Lower
Center
Upper
------+---------+---------+---------
-0.02998
0.02002
0.05000
0.10000
0.12998
0.17998
(---------*---------)
(--------*------------+---------+---------+---------
+---0.080
0.000
0.080
0.160

Suhu B
MD_5.75
+--222
Lower
Center
Upper
------+---------+---------+---------
-0.02998
0.05000
0.12998
(---------*---------)
------+---------+---------+---------
+---0.080
0.000
0.080
0.160
LAMPIRAN 5K
Source
Suhu B MD_6.00
Error
Total
S = 0.05270
Level
218
220
222
N
4
4
4
DF
2
9
11
SS
0.02167
0.02500
0.04667
R-Sq = 46.43%
Mean
0.47500
0.55000
0.57500
StDev
0.05000
0.05774
0.05000
MS
0.01083
0.00278
F
3.90
P
0.060
R-Sq(adj) = 34.52%

Pooled StDev
-+---------+---------+---------+-------(---------*---------)
(---------*---------)
(---------*---------)
-+---------+---------+---------+-------0.420
0.480
0.540
0.600


Suhu B
MD_6.00
---220
222
-)
Lower
Center
Upper
----+---------+---------+---------+-
-0.00931
0.01569
0.07500
0.10000
0.15931
0.18431
(---------*----------)
(---------*------------+---------+---------+---------+-
----0.080
0.000
0.080
0.160

Suhu B
MD_6.00
---222
Lower
Center
Upper
----+---------+---------+---------+-
-0.05931
0.02500
0.10931
(---------*----------)
----+---------+---------+---------+-
----0.080
0.000
0.080
0.160
LAMPIRAN 5L
Source
Suhu B MD_0.6
Error
Total
S = 0.07746
Level
218
220
222
N
6
6
6
DF
2
15
17
SS
0.03000
0.09000
0.12000
R-Sq = 25.00%
Mean
0.38333
0.43333
0.48333
StDev
0.07528
0.08165
0.07528
MS
0.01500
0.00600
F
2.50
P
0.116
R-Sq(adj) = 15.00%

Pooled StDev
-------+---------+---------+---------+-(----------*----------)
(----------*----------)
(-----------*----------)
-------+---------+---------+---------+-0.360
0.420
0.480
0.540


Suhu B
MD_0.6
--220
222
Lower
Center
Upper
-----+---------+---------+---------+-
-0.04532
0.00468
0.05000
0.10000
0.14532
0.19532
(---------*---------)
(---------*---------)
-----+---------+---------+---------+-
---0.10
0.00
0.10
0.20

Suhu B
MD_0.6
--222
Lower
Center
Upper
-----+---------+---------+---------+-
-0.04532
0.05000
0.14532
(---------*---------)
-----+---------+---------+---------+-
---0.10
0.00
0.10
0.20
LAMPIRAN 5M
Source
Suhu B MD_0.7
Error
Total
S = 0.06236
DF
2
15
17
SS
0.03111
0.05833
0.08944
R-Sq = 34.78%
MS
0.01556
0.00389
F
4.00
P
0.041
R-Sq(adj) = 26.09%
Level
218
220
222
N
6
6
6
Mean
0.45000
0.51667
0.55000
StDev
0.05477
0.07528
0.05477
Pooled StDev
----+---------+---------+---------+----(--------*--------)
(--------*--------)
(--------*--------)
----+---------+---------+---------+----0.600
0.420
0.480
0.540


Suhu B
MD_0.7
--220
222
Lower
Center
Upper
----+---------+---------+---------+--
-0.01007
0.02326
0.06667
0.10000
0.14341
0.17674
(--------*---------)
(--------*---------)
----+---------+---------+---------+--
---0.080
0.000
0.080
0.160

Suhu B
MD_0.7
--222
Lower
Center
Upper
----+---------+---------+---------+--
-0.04341
0.03333
0.11007
(--------*---------)
----+---------+---------+---------+--
---0.080
0.000
0.080
0.160
LAMPIRAN 5O
One-way ANOVA: HS DAS, Red_218 versus IV Umpan_218
Source
IV Umpan_218
DF
1
SS
0.01333
MS
0.01333
F
3.08
P
0.110
Error
Total
10
11
S = 0.06583
R-Sq = 23.53%
Level
0.6
0.7
N
6
6
Mean
0.38333
0.45000
0.04333
0.05667
StDev
0.07528
0.05477
0.00433
R-Sq(adj) = 15.88%

Pooled StDev
-----+---------+---------+---------+---(-----------*-----------)
(-----------*-----------)
-----+---------+---------+---------+---0.500
0.350
0.400
0.450


IV Umpan_218
0.7
Lower
-0.01802
Center
0.06667
Upper
0.15135
IV Umpan_218
0.7
----+---------+---------+---------+----(-------------*-------------)
----+---------+---------+---------+-----0.060
0.000
0.060
0.120
LAMPIRAN 5P
Source
IV Umpan_220
DF
1
SS
0.02083
MS
0.02083
F
3.38
P
0.096
Error
Total
10
11
S = 0.07853
R-Sq = 25.25%
Level
0.6
0.7
N
6
6
Mean
0.43333
0.51667
0.06167
0.08250
StDev
0.08165
0.07528
0.00617
R-Sq(adj) = 17.78%

Pooled StDev
+---------+---------+---------+--------(-----------*-----------)
(-----------*-----------)
+---------+---------+---------+--------0.360
0.420
0.480
0.540


IV Umpan_220
0.7
Lower
-0.01769
Center
0.08333
Upper
0.18435
IV Umpan_220
0.7
---+---------+---------+---------+-----(-----------*------------)
---+---------+---------+---------+------0.080
0.000
0.080
0.160
LAMPIRAN 5Q
Source
IV Umpan_222
Error
Total
DF
1
10
11
S = 0.06583
R-Sq = 23.53%
Level
0.6
0.7
N
6
6
Mean
0.48333
0.55000
SS
0.01333
0.04333
0.05667
StDev
0.07528
0.05477
MS
0.01333
0.00433
F
3.08
P
0.110
R-Sq(adj) = 15.88%

Pooled StDev
-----+---------+---------+---------+---(-----------*-----------)
(-----------*-----------)
-----+---------+---------+---------+---0.450
0.500
0.550
0.600


IV Umpan_222
0.7
Lower
-0.01802
Center
0.06667
Upper
0.15135
IV Umpan_222
0.7
----+---------+---------+---------+----(-------------*-------------)
----+---------+---------+---------+-----0.060
0.000
0.060
0.120
8/2/2009 8:41:36 AM
LAMPIRAN -6A
5/8/2009 6:04:08 AM
General Linear Model: HS AS Yellow versus F Umpan, IV Umpan, Suhu B
MD
Factor
F Umpan
IV Umpan
Suhu B MD
Type
fixed
fixed
fixed
Levels
3
2
3
Values
5.50, 5.75, 6.00
0.6, 0.7
218, 220, 222
Analysis of Variance for HS AS Yellow, using Adjusted SS for Tests

Source
P
F Umpan
0.034
IV Umpan
0.007
Suhu B MD
0.000
F Umpan*IV Umpan
0.837
F Umpan*Suhu B MD
0.942
IV Umpan*Suhu B MD
0.175
0.946
Error
Total
S = 0.180278
DF
Seq SS
Adj SS
Adj MS
0.26722
0.26722
0.13361
4.11
0.30250
0.30250
0.30250
9.31
15.58389
15.58389
7.79194
239.75
0.01167
0.01167
0.00583
0.18
0.02444
0.02444
0.00611
0.19
0.12500
0.12500
0.06250
1.92
0.02333
0.02333
0.00583
0.18
18
35
0.58500
16.92306
0.58500
0.03250
R-Sq = 96.54%
R-Sq(adj) = 93.28%
LAMPIRAN -6B
5/8/2009 10:38:31 AM
One-way ANOVA: HS AS Yellow_0.6 versus F Umpan_0.6
Source
F Umpan_0.6
Error
Total
DF
2
15
17
S = 0.6813
R-Sq = 1.99%
Level
5.50
5.75
6.00
N
6
6
6
SS
0.141
6.963
7.104
Mean
4.6333
4.7500
4.8500
MS
0.071
0.464
StDev
0.7062
0.6834
0.6535
F
0.15
P
0.860
R-Sq(adj) = 0.00%

Pooled StDev
---------+---------+---------+---------+
(--------------*--------------)
(--------------*--------------)
(--------------*--------------)
---------+---------+---------+---------+
4.40
4.80
5.20
5.60


F Umpan_0.6
--+
5.75
-)
6.00
---)
Lower
Center
Upper
---------+---------+---------+-------
-0.7218
0.1167
0.9551
(---------------*---------------
-0.6218
0.2167
1.0551
(---------------*---------------------+---------+---------+-------
--+
-0.50
0.00
0.50
1.00

F Umpan_0.6
--+
6.00
-)
Lower
Center
Upper
---------+---------+---------+-------
-0.7385
0.1000
0.9385
(----------------*-----------------------+---------+---------+-------
--+
-0.50
0.00
0.50
1.00
LAMPIRAN -6C
5/8/2009 10:38:31 AM
One-way ANOVA: HS DAS Yellow_0.7 versus F Umpan_0.7
Source
F Umpan_0.7
Error
Total
DF
2
15
17
S = 0.7907
R-Sq = 1.45%
Level
5.50
5.75
6.00
N
6
6
6
Mean
4.8500
4.8833
5.0500
SS
0.138
9.378
9.516
MS
0.069
0.625
StDev
0.7740
0.7782
0.8191
F
0.11
P
0.896
R-Sq(adj) = 0.00%

Pooled StDev
------+---------+---------+---------+--(----------------*----------------)
(----------------*----------------)
(----------------*----------------)
------+---------+---------+---------+--4.40
4.80
5.20
5.60


F Umpan_0.7
--+
5.75
6.00
--)
Lower
Center
Upper
---------+---------+---------+-------
-0.9397
-0.7730
0.0333
0.2000
1.0064
1.1730
(----------------*---------------)
(---------------*----------------------+---------+---------+-------
--+
-0.60
0.00
0.60
1.20
F Umpan_0.7
--+
6.00
-)
Lower
Center
Upper
---------+---------+---------+-------
-0.8064
0.1667
1.1397
(---------------*----------------------+---------+---------+-------
--+
-0.60
0.00
0.60
1.20
LAMPIRAN -6D
5/27/2009 10:40:11 AM
One-way ANOVA: HS AS Yellow_5.50 versus IV Umpan_5.50
Source
IV Umpan_5.50
Error
Total
S = 0.7408
Level
0.6
0.7
N
6
6
DF
1
10
11
SS
0.141
5.488
5.629
R-Sq = 2.50%
Mean
4.6333
4.8500
StDev
0.7062
0.7740
MS
0.141
0.549
F
0.26
P
0.623
R-Sq(adj) = 0.00%

Pooled StDev
-+---------+---------+---------+-------(----------------*----------------)
(----------------*----------------)
-+---------+---------+---------+-------4.00
4.40
4.80
5.20


IV Umpan_5.50
0.7
Lower
-0.7364
IV Umpan_5.50
0.7
------+---------+---------+---------+--(---------------*--------------)
Center
0.2167
Upper
1.1697
------+---------+---------+---------+---0.60
0.00
0.60
1.20
MTB > Oneway 'HS AS Yellow_5.75' 'IV Umpan_5.75';
SUBC>
Fisher 5.
LAMPIRAN -6E
5/27/2009 10:40:11 AM
Source
IV Umpan_5.75
Error
Total
S = 0.7323
Level
0.6
0.7
N
6
6
DF
1
10
11
SS
0.053
5.363
5.417
R-Sq = 0.98%
Mean
4.7500
4.8833
StDev
0.6834
0.7782
MS
0.053
0.536
F
0.10
P
0.759
R-Sq(adj) = 0.00%

Pooled StDev
--------+---------+---------+---------+(----------------*---------------)
(----------------*----------------)
--------+---------+---------+---------+4.40
4.80
5.20
5.60


IV Umpan_5.75
0.7
Lower
-0.8088
Center
0.1333
Upper
1.0754
IV Umpan_5.75
------+---------+---------+---------+---
0.7
(--------------*---------------)
------+---------+---------+---------+---0.60
0.00
0.60
1.20
LAMPIRAN -6F
5/27/2009 10:40:11 AM
Source
IV Umpan_6.00
Error
Total
S = 0.7409
Level
0.6
0.7
N
6
6
DF
1
10
11
SS
0.120
5.490
5.610
R-Sq = 2.14%
Mean
4.8500
5.0500
StDev
0.6535
0.8191
MS
0.120
0.549
F
0.22
P
0.650
R-Sq(adj) = 0.00%

Pooled StDev
------+---------+---------+---------+--(----------------*----------------)
(----------------*----------------)
------+---------+---------+---------+--4.40
4.80
5.20
5.60


IV Umpan_6.00
0.7
Lower
-0.7532
Center
0.2000
Upper
1.1532
IV Umpan_6.00
0.7
------+---------+---------+---------+--(---------------*---------------)
------+---------+---------+---------+---0.60
0.00
0.60
1.20
LAMPIRAN -6G
5/27/2009 10:40:11 AM
One-way ANOVA: HS AS Yellow_218 versus F Umpan_218
Source
F Umpan_218
Error
Total
DF
2
9
11
S = 0.1269
R-Sq = 42.00%
Level
5.50
5.75
6.00
N
4
4
4
Mean
3.8500
3.9250
4.0750
SS
0.1050
0.1450
0.2500
StDev
0.1732
0.0957
0.0957
MS
0.0525
0.0161
F
3.26
P
0.086
R-Sq(adj) = 29.11%

Pooled StDev
---+---------+---------+---------+-----(---------*--------)
(---------*--------)
(---------*--------)
---+---------+---------+---------+-----3.75
3.90
4.05
4.20

F Umpan_218
---+5.75
6.00
----)
Lower
Center
Upper
--------+---------+---------+------
-0.1280
0.0220
0.0750
0.2250
0.2780
0.4280
(---------*---------)
(---------*------------+---------+---------+------
---+-0.20
0.00
0.20
0.40

F Umpan_218
---+6.00
-)
Lower
Center
Upper
--------+---------+---------+------
-0.0530
0.1500
0.3530
(---------*----------------+---------+---------+------
---+-0.20
0.00
0.20
0.40
LAMPIRAN -6H
5/27/2009 10:40:11 AM
MTB > Oneway 'HS AS Yellow_220' 'F Umpan_220';
SUBC>
Fisher 5.

Source
F Umpan_220
Error
Total
DF
2
9
11
S = 0.1886
R-Sq = 12.73%
Level
5.50
5.75
6.00
N
4
4
4
Mean
4.9500
5.0500
5.1000
SS
0.0467
0.3200
0.3667
StDev
0.1915
0.1915
0.1826
MS
0.0233
0.0356
F
0.66
P
0.542
R-Sq(adj) = 0.00%

Pooled StDev
----+---------+---------+---------+----(-------------*-------------)
(--------------*-------------)
(-------------*-------------)
----+---------+---------+---------+----4.80
4.95
5.10
5.25


F Umpan_220
+----5.75
6.00
Lower
Center
Upper
----+---------+---------+---------
-0.2016
-0.1516
0.1000
0.1500
0.4016
0.4516
(-----------*-----------)
(-----------*-----------)
----+---------+---------+---------
+-----0.25
0.00
0.25
0.50

F Umpan_220
+----6.00
Lower
Center
Upper
----+---------+---------+---------
-0.2516
0.0500
0.3516
(-----------*-----------)
----+---------+---------+---------
+-----0.25
0.00
0.25
0.50
LAMPIRAN -6I
5/27/2009 10:40:11 AM
MTB > Oneway 'HS AS Yellow_222' 'F Umpan_222';
SUBC>
Fisher 5.

Source
F Umpan_222
Error
Total
DF
2
9
11
S = 0.2544
R-Sq = 19.38%
Level
5.50
5.75
6.00
N
4
4
4
Mean
5.4250
5.4750
5.6750
SS
0.1400
0.5825
0.7225
StDev
0.2630
0.2217
0.2754
MS
0.0700
0.0647
F
1.08
P
0.379
R-Sq(adj) = 1.46%

Pooled StDev
-----+---------+---------+---------+---(-----------*-----------)
(-----------*-----------)
(-----------*-----------)
-----+---------+---------+---------+---5.25
5.50
5.75
6.00


F Umpan_222
--+-5.75
6.00
-)
Lower
Center
Upper
-------+---------+---------+-------
-0.3569
-0.1569
0.0500
0.2500
0.4569
0.6569
(----------*-----------)
(----------*----------------+---------+---------+-------
--+--0.35
0.00
0.35
0.70

F Umpan_222
--+-6.00
Lower
Center
Upper
-------+---------+---------+-------
-0.2069
0.2000
0.6069
(-----------*----------)
-------+---------+---------+-------
--+--0.35
0.00
0.35
0.70
LAMPIRAN -6J
MTB > Oneway 'HS AS Yellow_5.50' 'Suhu B MD_5.50';
SUBC>
Fisher 5.
One-way ANOVA: HS AS Yellow_5.50 versus Suhu B MD_5.50

Source
Suhu B MD_5.50
Error
Total
S = 0.2128
Level
218
220
222
N
4
4
4
DF
2
9
11
SS
5.2217
0.4075
5.6292
R-Sq = 92.76%
Mean
3.8500
4.9500
5.4250
StDev
0.1732
0.1915
0.2630
MS
2.6108
0.0453
F
57.66
P
0.000
R-Sq(adj) = 91.15%

Pooled StDev
+---------+---------+---------+--------(---*---)
(----*---)
(---*---)
+---------+---------+---------+--------3.60
4.20
4.80
5.40


Suhu B
MD_5.50
220
222
)
Lower
Center
Upper
--+---------+---------+---------+------
0.7596
1.2346
1.1000
1.5750
1.4404
1.9154
(----*----)
(---*-----+---------+---------+---------+------
-0.70
0.00
0.70
1.40

Suhu B
MD_5.50
222
Lower
Center
Upper
--+---------+---------+---------+------
0.1346
0.4750
0.8154
(----*----)
--+---------+---------+---------+------
-0.70
0.00
0.70
1.40
LAMPIRAN -6K
SUBC>
Fisher 5.

Source
Suhu B MD_5.75
Error
Total
S = 0.1780
Level
DF
2
9
11
SS
5.1317
0.2850
5.4167
R-Sq = 94.74%
Mean
StDev
MS
2.5658
0.0317
F
81.03
P
0.000
R-Sq(adj) = 93.57%

Pooled StDev
------+---------+---------+---------+---
218
220
222
4
4
4
3.9250
5.0500
5.4750
0.0957
0.1915
0.2217
(----*---)
(---*---)
(---*----)
------+---------+---------+---------+--5.50
4.00
4.50
5.00


Suhu B
MD_5.75
--220
222
Lower
Center
Upper
+---------+---------+---------+------
0.8404
1.2654
1.1250
1.5500
1.4096
1.8346
(---*---)
(---*---)
+---------+---------+---------+------
---0.70
0.00
0.70
1.40

Suhu B
MD_5.75
--222
Lower
Center
Upper
+---------+---------+---------+------
0.1404
0.4250
0.7096
(---*---)
+---------+---------+---------+------
---0.70
0.00
0.70
1.40
LAMPIRAN -6L
SUBC>
Fisher 5.

Source
Suhu B MD_6.00
Error
Total
S = 0.1986
DF
2
9
11
SS
5.2550
0.3550
5.6100
R-Sq = 93.67%
MS
2.6275
0.0394
F
66.61
P
0.000
R-Sq(adj) = 92.27%
Level
218
220
222
N
4
4
4
Mean
4.0750
5.1000
5.6750
StDev
0.0957
0.1826
0.2754

Pooled StDev
------+---------+---------+---------+--(---*---)
(---*---)
(---*--)
------+---------+---------+---------+--5.40
6.00
4.20
4.80


Suhu B
MD_6.00
-220
222
Lower
Center
Upper
-+---------+---------+---------+------
0.7073
1.2823
1.0250
1.6000
1.3427
1.9177
(---*---)
(---*---)
-+---------+---------+---------+------
--0.80
0.00
0.80
1.60

Suhu B
MD_6.00
-222
Lower
Center
Upper
-+---------+---------+---------+------
0.2573
0.5750
0.8927
(---*---)
-+---------+---------+---------+------
--0.80
0.00
0.80
1.60
LAMPIRAN -6M
5/8/2009 6:04:08 AM
SUBC>
Fisher 5.

Source
Suhu B MD_0.6
Error
Total
S = 0.1374
Level
218
220
222
N
6
6
6
DF
2
15
17
SS
6.8211
0.2833
7.1044
MS
3.4106
0.0189
R-Sq = 96.01%
Mean
3.9000
4.9833
5.3500
StDev
0.1549
0.1472
0.1049
F
180.56
P
0.000
R-Sq(adj) = 95.48%

Pooled StDev
----+---------+---------+---------+----(-*-)
(--*-)
(-*-)
----+---------+---------+---------+----4.00
4.50
5.00
5.50


Suhu B
MD_0.6
220
222
Lower
0.9142
1.2809
Center
1.0833
1.4500
Upper
1.2525
1.6191
---------+---------+---------+---------+
(--*--)
(--*--)
---------+---------+---------+---------+
0.00
0.60
1.20
1.80

Suhu B
MD_0.6
222
Lower
0.1975
Center
0.3667
Upper
0.5358
---------+---------+---------+---------+
(--*--)
---------+---------+---------+---------+
0.00
0.60
1.20
1.80
LAMPIRAN -6N
5/8/2009 6:04:08 AM
SUBC>
Fisher 5.

Source
Suhu B MD_0.7
Error
Total
S = 0.2047
Level
218
220
222
N
6
6
6
DF
2
15
17
SS
8.8878
0.6283
9.5161
MS
4.4439
0.0419
R-Sq = 93.40%
Mean
4.0000
5.0833
5.7000
StDev
0.1414
0.2137
0.2449
F
106.09
P
0.000
R-Sq(adj) = 92.52%

Pooled StDev
------+---------+---------+---------+--(--*--)
(--*--)
(--*--)
------+---------+---------+---------+--4.20
4.80
5.40
6.00


Suhu B
MD_0.7
220
222
Lower
Center
Upper
-+---------+---------+---------+-------
0.8315
1.4481
1.0833
1.7000
1.3352
1.9519
(---*--)
(--*--)
-+---------+---------+---------+-------
-0.80
0.00
0.80
1.60

Suhu B
MD_0.7
222
Lower
Center
Upper
-+---------+---------+---------+-------
0.3648
0.6167
0.8685
(--*--)
-+---------+---------+---------+-------
-0.80
0.00
0.80
1.60
LAMPIRAN -6O
7/10/2009 7:46:39 AM

Retrieving project from file: 'C:\Program Files\MINITAB
14\Data\MINITAB.MPJ.23'
MTB > Unstack ( 'IV Umpan' 'HS AS Yellow');
SUBC>
Subscripts 'Suhu B MD';
SUBC>
NewWS;
SUBC>
VarNames.

MTB > Oneway 'HS AS Yellow_218' 'IV Umpan_218';
SUBC>
Fisher 5.
One-way ANOVA: HS AS Yellow_218 versus IV Umpan_218

Source
IV Umpan_218
Error
Total
S = 0.1483
Level
0.6
0.7
N
6
6
DF
1
10
11
SS
0.0300
0.2200
0.2500
MS
0.0300
0.0220
R-Sq = 12.00%
Mean
3.9000
4.0000
StDev
0.1549
0.1414
F
1.36
P
0.270
R-Sq(adj) = 3.20%

Pooled StDev
---+---------+---------+---------+-----(------------*------------)
(------------*------------)
---+---------+---------+---------+-----3.80
3.90
4.00
4.10


IV Umpan_218
+-----0.7
Lower
Center
Upper
---+---------+---------+---------
-0.0908
0.1000
0.2908
(------------*-----------)
---+---------+---------+---------
+------0.15
0.00
0.15
0.30
LAMPIRAN -6P
SUBC>
Fisher 5.

Source
IV Umpan_220
Error
Total
S = 0.1835
Level
0.6
0.7
N
6
6
DF
1
10
11
SS
0.0300
0.3367
0.3667
R-Sq = 8.18%
Mean
4.9833
5.0833
StDev
0.1472
0.2137
MS
0.0300
0.0337
F
0.89
P
0.367
R-Sq(adj) = 0.00%

Pooled StDev
---------+---------+---------+---------+
(-------------*-------------)
(-------------*-------------)
---------+---------+---------+---------+
4.92
5.04
5.16
5.28


IV Umpan_220
--+--0.7
----)
Lower
Center
Upper
------+---------+---------+-------
-0.1360
0.1000
0.3360
(---------------*---------------+---------+---------+-------
--+---0.15
0.00
0.15
0.30
LAMPIRAN -6Q
SUBC>
Fisher 5.

Source
IV Umpan_222
Error
Total
S = 0.1884
Level
0.6
0.7
N
6
6
DF
1
10
11
SS
0.3675
0.3550
0.7225
MS
0.3675
0.0355
R-Sq = 50.87%
Mean
5.3500
5.7000
StDev
0.1049
0.2449
F
10.35
P
0.009
R-Sq(adj) = 45.95%

Pooled StDev
-+---------+---------+---------+-------(--------*-------)
(--------*--------)
-+---------+---------+---------+-------5.20
5.40
5.60
5.80


IV Umpan_222
0.7
Lower
0.1076
Center
0.3500
Upper
0.5924
IV Umpan_222
0.7
+---------+---------+---------+--------(---------*---------)
+---------+---------+---------+---------0.25
0.00
0.25
0.50

SUBC>
Project;
SUBC>
Replace.
Saving file as: 'C:\Program Files\MINITAB 14\Data\MINITAB.MPJ.23'
Existing file replaced.
SUBC>
Project;
SUBC>
Replace.
7/10/2009 8:31:46 PM
LAMPIRAN 7A
8/17/2009 6:22:32 PM
General Linear Model: AV Residue versus F Umpan, IV Umpan, Suhu BMD

Factor
F Umpan
IV Umpan
Suhu BMD
Type
fixed
fixed
fixed
Levels
3
2
3
Values
5.50, 5.75, 6.00
0.6, 0.7
218, 220, 222
Analysis of Variance for AV Residue, using Adjusted SS for Tests

Source
F Umpan
IV Umpan
Suhu BMD
F Umpan*IV Umpan
F Umpan*Suhu BMD
IV Umpan*Suhu BMD
F Umpan*IV Umpan*Suhu BMD
Error
Total
S = 1.21906
DF
2
1
2
2
4
2
4
18
35
R-Sq = 94.69%
Seq SS
0.344
135.334
294.976
0.341
0.101
45.802
0.288
26.750
503.936
Adj SS
0.344
135.334
294.976
0.341
0.101
45.802
0.288
26.750
Adj MS
0.172
135.334
147.488
0.170
0.025
22.901
0.072
1.486
F
0.12
91.07
99.24
0.11
0.02
15.41
0.05
P
0.891
0.000
0.000
0.892
0.999
0.000
0.995
R-Sq(adj) = 89.68%
LAMPIRAN 7B
One-way ANOVA: AV Residue_0.6 versus F Umpan_0.6
Source
F Umpan_0.6
Error
Total
S = 1.948
Level
5.50
5.75
6.00
N
6
6
6
DF
2
15
17
SS
0.13
56.94
57.07
MS
0.06
3.80
R-Sq = 0.23%
Mean
25.533
25.733
25.683
StDev
2.023
1.908
1.913
F
0.02
P
0.983
R-Sq(adj) = 0.00%

Pooled StDev
--+---------+---------+---------+------(----------------*----------------)
(----------------*----------------)
(----------------*----------------)
--+---------+---------+---------+------24.0
25.0
26.0
27.0


F Umpan_0.6
+--5.75
6.00
Lower
Center
Upper
------+---------+---------+---------
-2.197
-2.247
0.200
0.150
2.597
2.547
(---------------*---------------)
(---------------*---------------)
------+---------+---------+---------
+---1.5
0.0
1.5
3.0

F Umpan_0.6
+--6.00
Lower
Center
Upper
------+---------+---------+---------
-2.447
-0.050
2.347
(---------------*---------------)
------+---------+---------+---------
+---1.5
0.0
1.5
3.0
LAMPIRAN 7C
One-way ANOVA: AV Residue_0.7 versus F Umpan_0.7
Source
F Umpan_0.7
Error
Total
S = 4.553
Level
5.50
5.75
6.00
N
6
6
6
DF
2
15
17
SS
0.6
311.0
311.5
R-Sq = 0.18%
Mean
29.467
29.350
29.767
StDev
4.493
4.569
4.597
MS
0.3
20.7
F
0.01
P
0.987
R-Sq(adj) = 0.00%

Pooled StDev
--------+---------+---------+---------+(---------------*---------------)
(--------------*---------------)
(---------------*---------------)
--------+---------+---------+---------+27.5
30.0
32.5
35.0


F Umpan_0.7
+-5.75
6.00
Lower
Center
Upper
-------+---------+---------+---------
-5.720
-5.303
-0.117
0.300
5.487
5.903
(---------------*---------------)
(---------------*---------------)
-------+---------+---------+---------
+--3.5
0.0
3.5
7.0

F Umpan_0.7
+--
Lower
Center
Upper
-------+---------+---------+---------
6.00
-5.187
0.417
6.020
(---------------*---------------)
-------+---------+---------+---------
+--3.5
0.0
3.5
7.0
LAMPIRAN 7D
One-way ANOVA: AV Residue_5.50 versus IV Umpan_5.50
Source
IV Umpan_5.50
Error
Total
S = 3.484
Level
0.6
0.7
N
6
6
DF
1
10
11
SS
46.4
121.4
167.8
MS
46.4
12.1
R-Sq = 27.66%
Mean
25.533
29.467
StDev
2.023
4.493
F
3.82
P
0.079
R-Sq(adj) = 20.43%

Pooled StDev
-----+---------+---------+---------+---(---------*----------)
(---------*----------)
-----+---------+---------+---------+---24.0
27.0
30.0
33.0


IV Umpan_5.50
----0.7
--)
Lower
Center
Upper
---+---------+---------+---------+-
-0.549
3.933
8.415
(------------*----------
---+---------+---------+---------+-----3.5
0.0
3.5
7.0
LAMPIRAN 7E
Source
IV Umpan_5.75
Error
Total
S = 3.501
DF
1
10
11
SS
39.2
122.6
161.8
MS
39.2
12.3
R-Sq = 24.25%
F
3.20
P
0.104
R-Sq(adj) = 16.67%

StDev
Level
0.6
0.7
N
6
6
Mean
25.733
29.350
StDev
1.908
4.569
+---------+---------+---------+--------(------------*------------)
(-----------*------------)
+---------+---------+---------+--------22.5
25.0
27.5
30.0


IV Umpan_5.75
----0.7
-)
Lower
Center
Upper
---+---------+---------+---------+-
-0.887
3.617
8.121
(------------*-----------
---+---------+---------+---------+-----3.5
0.0
3.5
7.0
LAMPIRAN 7F
Source
IV Umpan_6.00
Error
Total
S = 3.521
Level
0.6
0.7
N
6
6
DF
1
10
11
SS
50.0
123.9
174.0
MS
50.0
12.4
R-Sq = 28.75%
Mean
25.683
29.767
StDev
1.913
4.597
F
4.04
P
0.072
R-Sq(adj) = 21.63%

Pooled StDev
-----+---------+---------+---------+---(----------*---------)
(---------*----------)
-----+---------+---------+---------+---24.0
27.0
30.0
33.0

IV Umpan_6.00
----0.7
---)
Lower
Center
Upper
---+---------+---------+---------+-
-0.446
4.083
8.612
(------------*-----------+---------+---------+---------+-
-----3.5
0.0
3.5
7.0
LAMPIRAN 7G
One-way ANOVA: AV Residue_218 versus F Umpan_218
Source
F Umpan_218
Error
Total
S = 4.260
Level
5.50
5.75
6.00
N
4
4
4
DF
2
9
11
SS
0.2
163.3
163.5
R-Sq = 0.11%
MS
0.1
18.1
Mean
31.525
31.575
31.800
StDev
4.200
4.127
4.445
F
0.00
P
0.995
R-Sq(adj) = 0.00%

Pooled StDev
---+---------+---------+---------+-----(------------------*------------------)
(------------------*-------------------)
(------------------*------------------)
---+---------+---------+---------+-----27.5
30.0
32.5
35.0


F Umpan_218
-+5.75
6.00
Lower
Center
Upper
--------+---------+---------+--------
-6.764
-6.539
0.050
0.275
6.864
7.089
(----------------*----------------)
(----------------*----------------)
--------+---------+---------+--------
-+-4.0
0.0
4.0
8.0

F Umpan_218
-+6.00
Lower
Center
Upper
--------+---------+---------+--------
-6.589
0.225
7.039
(----------------*----------------)
--------+---------+---------+--------
-+-4.0
0.0
4.0
8.0
LAMPIRAN 7H
Source
F Umpan_220
Error
Total
S = 1.547
Level
5.50
5.75
6.00
N
4
4
4
DF
2
9
11
SS
0.21
21.53
21.74
MS
0.11
2.39
R-Sq = 0.97%
Mean
25.550
25.725
25.875
StDev
1.816
1.408
1.377
F
0.04
P
0.957
R-Sq(adj) = 0.00%

Pooled StDev
--+---------+---------+---------+------(----------------*-----------------)
(----------------*-----------------)
(-----------------*----------------)
--+---------+---------+---------+------24.0
25.0
26.0
27.0


F Umpan_220
+-5.75
6.00
Lower
Center
Upper
-------+---------+---------+---------
-2.299
-2.149
0.175
0.325
2.649
2.799
(---------------*----------------)
(---------------*----------------)
-------+---------+---------+---------
+--1.5
0.0
1.5
3.0

F Umpan_220
+-6.00
Lower
Center
Upper
-------+---------+---------+---------
-2.324
0.150
2.624
(---------------*---------------)
-------+---------+---------+---------
+--1.5
0.0
1.5
3.0
LAMPIRAN 7I
Source
F Umpan_222
Error
Total
S = 1.623
DF
2
9
11
SS
0.06
23.69
23.76
MS
0.03
2.63
R-Sq = 0.26%
F
0.01
P
0.988
R-Sq(adj) = 0.00%
Level
5.50
5.75
6.00
N
4
4
4
Mean
25.425
25.325
25.500
StDev
1.607
1.513
1.740
Pooled StDev
-----+---------+---------+---------+---(-----------------*------------------)
(-----------------*------------------)
(-----------------*-----------------)
-----+---------+---------+---------+---24.0
25.0
26.0
27.0


F Umpan_222
-+5.75
6.00
Lower
Center
Upper
--------+---------+---------+--------
-2.695
-2.520
-0.100
0.075
2.495
2.670
(----------------*-----------------)
(----------------*-----------------)
--------+---------+---------+--------
-+-1.5
0.0
1.5
3.0

F Umpan_222
-+6.00
Lower
Center
Upper
--------+---------+---------+--------
-2.420
0.175
2.770
(----------------*----------------)
--------+---------+---------+--------
-+-1.5
0.0
1.5
3.0
LAMPIRAN 7J
One-way ANOVA: AV Residue_5.50 versus Suhu BMD_5.50
Source
Suhu BMD_5.50
Error
Total
S = 2.800
Level
218
220
222
N
4
4
4
DF
2
9
11
SS
97.24
70.56
167.80
R-Sq = 57.95%
Mean
31.525
25.550
25.425
StDev
4.200
1.816
1.607
MS
48.62
7.84
F
6.20
P
0.020
R-Sq(adj) = 48.60%

Pooled StDev
------+---------+---------+---------+--(--------*--------)
(--------*--------)
(--------*--------)
------+---------+---------+---------+--24.5
28.0
31.5
35.0

All Pairwise Comparisons among Levels of Suhu BMD_5.50
Suhu BMD_5.50 = 218 subtracted from:

Suhu
BMD_5.50
-220
222
Lower
Center
Upper
------+---------+---------+---------+-
-10.454
-10.579
-5.975
-6.100
-1.496
-1.621
(----------*----------)
(----------*----------)
------+---------+---------+---------+-
--8.0
-4.0
0.0
4.0

Suhu
BMD_5.50
222
Lower
-4.604
Center
-0.125
Upper
4.354
------+---------+---------+---------+--(-----------*----------)
------+---------+---------+---------+---8.0
-4.0
0.0
4.0
LAMPIRAN 7K

Source
Suhu BMD_5.75
Error
Total
S = 2.665
Level
218
220
222
N
4
4
4
DF
2
9
11
SS
97.93
63.90
161.83
R-Sq = 60.51%
Mean
31.575
25.725
25.325
StDev
4.127
1.408
1.513
MS
48.96
7.10
F
6.90
P
0.015
R-Sq(adj) = 51.74%

Pooled StDev
------+---------+---------+---------+--(-------*--------)
(--------*-------)
(-------*--------)
------+---------+---------+---------+--24.5
28.0
31.5
35.0


Suhu
BMD_5.75
-220
222
Lower
Center
Upper
------+---------+---------+---------+-
-10.112
-10.512
-5.850
-6.250
-1.588
-1.988
(---------*----------)
(---------*----------)
------+---------+---------+---------+-
--8.0
-4.0
0.0
4.0

Suhu
BMD_5.75
222
Lower
-4.662
Center
-0.400
Upper
3.862
------+---------+---------+---------+--(----------*----------)
------+---------+---------+---------+---8.0
-4.0
0.0
4.0
LAMPIRAN 7L
Source
Suhu BMD_6.00
Error
Total
S = 2.868
Level
218
220
222
N
4
4
4
DF
2
9
11
SS
99.91
74.05
173.96
R-Sq = 57.43%
Mean
31.800
25.875
25.500
StDev
4.445
1.377
1.740
MS
49.96
8.23
F
6.07
P
0.021
R-Sq(adj) = 47.98%

Pooled StDev
------+---------+---------+---------+--(--------*--------)
(--------*--------)
(--------*--------)
------+---------+---------+---------+--24.5
28.0
31.5
35.0


Suhu
BMD_6.00
+-220
222
Lower
Center
Upper
-------+---------+---------+---------
-10.513
-10.888
-5.925
-6.300
-1.337
-1.712
(----------*-----------)
(----------*-----------)
-------+---------+---------+---------
+--8.0
-4.0
0.0
4.0

Suhu
BMD_6.00
222
Lower
-4.963
Center
-0.375
Upper
4.213
-------+---------+---------+---------+-(----------*-----------)
-------+---------+---------+---------+--8.0
-4.0
0.0
4.0
LAMPIRAN 7M
Source
Suhu BMD_0.6
Error
Total
S = 0.4398
Level
218
220
222
N
6
6
6
DF
2
15
17
SS
54.163
2.902
57.065
MS
27.082
0.193
R-Sq = 94.92%
Mean
28.100
24.533
24.317
StDev
0.283
0.372
0.601
F
140.00
P
0.000
R-Sq(adj) = 94.24%

Pooled StDev
-+---------+---------+---------+-------(--*--)
(--*---)
(---*--)
-+---------+---------+---------+-------24.0
25.2
26.4
27.6


Suhu
BMD_0.6
--+
220
222
Lower
Center
Upper
---------+---------+---------+-------
-4.1079
-4.3246
-3.5667
-3.7833
-3.0254
-3.2421
(--*---)
(---*--)
---------+---------+---------+-------
--+
-3.0
-1.5
0.0
1.5

Suhu
BMD_0.6
-+
222
Lower
Center
Upper
---------+---------+---------+--------
-0.7579
-0.2167
0.3246
(---*--)
---------+---------+---------+--------
-+
-3.0
-1.5
0.0
1.5
LAMPIRAN 7N
Source
Suhu BMD_0.7
Error
Total
S = 1.289
Level
218
220
222
N
6
6
6
DF
2
15
17
SS
286.61
24.92
311.54
MS
143.31
1.66
R-Sq = 92.00%
Mean
35.167
26.900
26.517
StDev
1.628
0.921
1.219
F
86.25
P
0.000
R-Sq(adj) = 90.93%

Pooled StDev
-----+---------+---------+---------+---(---*---)
(---*--)
(--*---)
-----+---------+---------+---------+---27.0
30.0
33.0
36.0


Suhu
BMD_0.7
+
220
222
Lower
Center
Upper
---------+---------+---------+---------
-9.853
-10.236
-8.267
-8.650
-6.680
-7.064
(---*----)
(---*----)
---------+---------+---------+---------
+
-7.0
-3.5
0.0
3.5

Suhu
BMD_0.7
222
Lower
-1.970
Center
-0.383
Upper
1.203
---------+---------+---------+---------+
(----*---)
---------+---------+---------+---------+
-7.0
-3.5
0.0
3.5
LAMPIRAN 7O
One-way ANOVA: AV Residue_218 versus IV Umpan_218
Source
IV Umpan_218
Error
Total
S = 1.168
Level
0.6
0.7
N
6
6
DF
1
10
11
SS
149.81
13.65
163.47
MS
149.81
1.37
R-Sq = 91.65%
Mean
28.100
35.167
StDev
0.283
1.628
F
109.73
P
0.000
R-Sq(adj) = 90.81%

Pooled StDev
--+---------+---------+---------+------(---*----)
(----*---)
--+---------+---------+---------+------27.5
30.0
32.5
35.0


IV Umpan_218
--0.7
Lower
Center
Upper
-----+---------+---------+---------+-
5.564
7.067
8.570
(----*----)
-----+---------+---------+---------+-
--0.0
3.0
6.0
9.0
LAMPIRAN 7P
Source
IV Umpan_220
Error
Total
S = 0.7024
Level
0.6
0.7
N
6
6
DF
1
10
11
SS
16.803
4.933
21.737
MS
16.803
0.493
R-Sq = 77.30%
Mean
24.533
26.900
StDev
0.372
0.921
F
34.06
P
0.000
R-Sq(adj) = 75.03%

Pooled StDev
-+---------+---------+---------+-------(-----*------)
(-----*-----)
-+---------+---------+---------+-------24.0
25.0
26.0
27.0


IV Umpan_220
---+0.7
)
Lower
Center
Upper
--------+---------+---------+------
1.4631
2.3667
3.2702
(-------*-------------+---------+---------+------
---+0.0
1.2
2.4
3.6
LAMPIRAN 7Q
Source
IV Umpan_222
Error
Total
S = 0.9611
Level
0.6
0.7
N
6
6
DF
1
10
11
SS
14.520
9.237
23.757
MS
14.520
0.924
R-Sq = 61.12%
Mean
24.317
26.517
StDev
0.601
1.219
F
15.72
P
0.003
R-Sq(adj) = 57.23%

Pooled StDev
------+---------+---------+---------+--(--------*--------)
(--------*--------)
------+---------+---------+---------+--24.0
25.0
26.0
27.0


IV Umpan_222
0.7
Lower
0.9637
Center
2.2000
Upper
3.4363
IV Umpan_222
0.7
+---------+---------+---------+--------(---------*----------)
+---------+---------+---------+---------1.2
0.0
1.2
2.4
LAMPIRAN 8A
12/18/2009 11:03:21 PM
General Linear Model: Res Yield versus F Umpan, IV Umpan, Suhu MD

Factor
F Umpan
IV Umpan
Suhu MD
Type
fixed
fixed
fixed
Levels
3
2
3
Values
5.50, 5.75, 6.00
0.6, 0.7
218, 220, 222
Analysis of Variance for Res Yield, using Adjusted SS for Tests

Source
F Umpan
IV Umpan
Suhu MD
F Umpan*IV Umpan
F Umpan*Suhu MD
IV Umpan*Suhu MD
F Umpan*IV Umpan*Suhu MD
Error
Total
S = 1.12607
DF
2
1
2
2
4
2
4
18
35
R-Sq = 99.43%
Seq SS
3534.34
178.53
261.07
0.08
11.89
6.85
1.61
22.82
4017.21
Adj SS
3534.34
178.53
261.07
0.08
11.89
6.85
1.61
22.82
Adj MS
1767.17
178.53
130.54
0.04
2.97
3.43
0.40
1.27
F
1393.64
140.80
102.94
0.03
2.35
2.70
0.32
P
0.000
0.000
0.000
0.967
0.094
0.094
0.862
R-Sq(adj) = 98.90%
Unusual Observations for Res Yield

Obs
7
8
Res Yield
280.600
277.000
Fit
278.800
278.800
SE Fit
0.796
0.796
Residual
1.800
-1.800
St Resid
2.26 R
-2.26 R
R denotes an observation with a large standardized residual.
LAMPIRAN 8B
One-way ANOVA: Res Yield_0.6 versus F Umpan_0.6
Source
F Umpan_0.6
Error
Total
S = 2.737
Level
5.50
5.75
6.00
N
6
6
6
DF
2
15
17
SS
1752.48
112.34
1864.83
MS
876.24
7.49
R-Sq = 93.98%
Mean
276.35
288.75
300.52
StDev
2.31
3.35
2.43
F
117.00
P
0.000
R-Sq(adj) = 93.17%

Pooled StDev
--------+---------+---------+---------+(--*--)
(--*--)
(--*--)
--------+---------+---------+---------+280.0
288.0
296.0
304.0
Pooled StDev = 2.74


F Umpan_0.6
----
Lower
Center
Upper
---+---------+---------+---------+--
5.75
6.00
)
9.032
20.799
12.400
24.167
15.768
27.534
(-*--)
(--*----+---------+---------+---------+--
----12
12
24

F Umpan_0.6
--6.00
Lower
Center
Upper
---+---------+---------+---------+---
8.399
11.767
15.134
(--*--)
---+---------+---------+---------+---
---12
12
24
LAMPIRAN 8C
One-way ANOVA: Res Yield_0.7 versus F Umpan_0.7
Source
F Umpan_0.7
Error
Total
S = 3.577
Level
5.50
5.75
6.00
N
6
6
6
DF
2
15
17
SS
1781.9
191.9
1973.8
MS
891.0
12.8
R-Sq = 90.28%
Mean
280.67
293.28
305.03
StDev
3.01
4.46
3.07
F
69.64
P
0.000
R-Sq(adj) = 88.98%

Pooled StDev
---+---------+---------+---------+-----(---*---)
(---*--)
(---*---)
---+---------+---------+---------+-----280.0
288.0
296.0
304.0
Pooled StDev = 3.58

F Umpan_0.7
---5.75
6.00
-)
Lower
Center
Upper
8.210
19.965
12.612
24.367
17.013
28.768
---+---------+---------+---------+-(---*--)
(--*----+---------+---------+---------+--
----12
12
24

F Umpan_0.7
--6.00
Lower
Center
Upper
---+---------+---------+---------+---
7.353
11.755
16.157
(---*--)
---+---------+---------+---------+---
---12
12
24
LAMPIRAN 8D
One-way ANOVA: Res Yield_5.50 versus IV Umpan_5.50
Source
IV Umpan_5.50
Error
Total
S = 2.683
Level
0.6
0.7
N
6
6
DF
1
10
11
SS
55.90
72.01
127.91
R-Sq = 43.70%
Mean
276.35
280.67
StDev
2.31
3.01
MS
55.90
7.20
F
7.76
P
0.019
R-Sq(adj) = 38.07%

Pooled StDev
----+---------+---------+---------+----(--------*---------)
(---------*--------)
----+---------+---------+---------+----275.0
277.5
280.0
282.5
Pooled StDev = 2.68


IV Umpan_5.50
----0.7
---)
Lower
Center
Upper
--+---------+---------+---------+--
0.865
4.317
7.769
(----------*---------+---------+---------+---------+--
-----3.0
0.0
3.0
6.0
LAMPIRAN 8E
Source
IV Umpan_5.75
Error
Total
S = 3.947
Level
0.6
0.7
N
6
6
DF
1
10
11
SS
61.5
155.8
217.3
MS
61.5
15.6
R-Sq = 28.31%
Mean
288.75
293.28
StDev
3.35
4.46
F
3.95
P
0.075
R-Sq(adj) = 21.14%

Pooled StDev
---------+---------+---------+---------+
(-----------*----------)
(-----------*-----------)
---------+---------+---------+---------+
288.0
291.0
294.0
297.0
Pooled StDev = 3.95


IV Umpan_5.75
----0.7
--)
Lower
Center
Upper
---+---------+---------+---------+-
-0.549
4.528
9.605
(-----------*------------+---------+---------+---------+-
-----4.0
0.0
4.0
8.0
LAMPIRAN 8F
Source
IV Umpan_6.00
Error
Total
S = 2.766
Level
0.6
0.7
N
6
6
DF
1
10
11
SS
61.20
76.48
137.68
R-Sq = 44.45%
Mean
300.52
305.03
StDev
2.43
3.07
MS
61.20
7.65
F
8.00
P
0.018
R-Sq(adj) = 38.90%

Pooled StDev
--------+---------+---------+---------+(---------*---------)
(---------*---------)
--------+---------+---------+---------+300.0
302.5
305.0
307.5
Pooled StDev = 2.77


IV Umpan_6.00
----0.7
----)
Lower
Center
Upper
--+---------+---------+---------+--
0.959
4.517
8.074
(-----------*--------+---------+---------+---------+--
-----3.0
0.0
3.0
6.0
LAMPIRAN 8G
One-way ANOVA: Res Yield_218 versus F Umpan_218
Source
F Umpan_218
Error
Total
S = 3.471
Level
5.50
5.75
N
4
4
DF
2
9
11
SS
1183.0
108.4
1291.4
MS
591.5
12.0
R-Sq = 91.60%
Mean
281.40
295.38
StDev
3.44
3.62
F
49.09
P
0.000
R-Sq(adj) = 89.74%

Pooled StDev
---+---------+---------+---------+-----(---*---)
(---*---)
6.00
305.63
3.35
(---*---)
---+---------+---------+---------+-----300
310
280
290
Pooled StDev = 3.47


F Umpan_218
---5.75
6.00
--)
Lower
Center
Upper
---+---------+---------+---------+--
8.423
18.673
13.975
24.225
19.527
29.777
(----*---)
(---*----+---------+---------+---------+--
----12
12
24

F Umpan_218
--6.00
Lower
Center
Upper
---+---------+---------+---------+---
4.698
10.250
15.802
(----*---)
---+---------+---------+---------+---
---12
12
24
LAMPIRAN 8H
Source
F Umpan_220
Error
Total
S = 2.477
Level
DF
2
9
11
SS
1237.62
55.20
1292.82
MS
618.81
6.13
R-Sq = 95.73%
Mean
StDev
F
100.89
P
0.000
R-Sq(adj) = 94.78%

Pooled StDev
------+---------+---------+---------+---
5.50
5.75
6.00
4
4
4
278.13
290.74
303.00
2.78
2.42
2.19
(---*--)
(--*---)
(---*--)
------+---------+---------+---------+--280.0
288.0
296.0
304.0
Pooled StDev = 2.48


F Umpan_220
---5.75
6.00
*--)
Lower
Center
Upper
8.656
20.913
12.618
24.875
16.579
28.837
----+---------+---------+---------+(---*--)
(------+---------+---------+---------+-
----12
12
24

F Umpan_220
--6.00
Lower
Center
Upper
----+---------+---------+---------+--
8.296
12.257
16.219
(--*---)
----+---------+---------+---------+--
---12
12
24
LAMPIRAN 8I
Source
F Umpan_222
Error
Total
DF
2
9
11
SS
1125.66
46.27
1171.93
MS
562.83
5.14
F
109.47
P
0.000
S = 2.267
Level
5.50
5.75
6.00
N
4
4
4
R-Sq = 96.05%
Mean
276.00
286.93
299.70
StDev
1.83
2.39
2.52
R-Sq(adj) = 95.17%

Pooled StDev
--------+---------+---------+---------+(--*--)
(---*--)
(---*--)
--------+---------+---------+---------+304.0
280.0
288.0
296.0
Pooled StDev = 2.27


F Umpan_222
---5.75
6.00
-)
Lower
Center
Upper
7.298
20.073
10.925
23.700
14.552
27.327
----+---------+---------+---------+(--*--)
(--*----+---------+---------+---------+-
----12
12
24

F Umpan_222
--6.00
Lower
Center
Upper
----+---------+---------+---------+--
9.148
12.775
16.402
(--*--)
----+---------+---------+---------+--
---12
12
24
LAMPIRAN 8J
One-way ANOVA: Res Yield_5.50 versus Suhu MD_5.50
Source
Suhu MD_5.50
Error
Total
S = 2.763
DF
2
9
11
SS
59.20
68.71
127.91
MS
29.60
7.63
R-Sq = 46.28%
F
3.88
P
0.061
R-Sq(adj) = 34.35%

StDev
Level
218
220
222
N
4
4
4
Mean
281.40
278.13
276.00
StDev
3.44
2.78
1.83
+---------+---------+---------+--------(---------*---------)
(---------*----------)
(---------*---------)
+---------+---------+---------+--------273.0
276.0
279.0
282.0
Pooled StDev = 2.76

All Pairwise Comparisons among Levels of Suhu MD_5.50
Suhu MD_5.50 = 218 subtracted from:

Suhu
MD_5.50
---220
222
Lower
Center
Upper
+---------+---------+---------+-----
-7.695
-9.820
-3.275
-5.400
1.145
-0.980
(-------*--------)
(--------*--------)
+---------+---------+---------+-----
----10.0
-5.0
0.0
5.0

Suhu
MD_5.50
--222
Lower
Center
Upper
+---------+---------+---------+------
-6.545
-2.125
2.295
(--------*--------)
+---------+---------+---------+------
---10.0
-5.0
0.0
5.0
LAMPIRAN 8K

Source
Suhu MD_5.75
Error
Total
S = 2.868
Level
218
220
222
N
4
4
4
DF
2
9
11
SS
143.25
74.03
217.28
MS
71.62
8.23
R-Sq = 65.93%
Mean
295.38
290.74
286.93
StDev
3.62
2.42
2.39
F
8.71
P
0.008
R-Sq(adj) = 58.36%

StDev
-+---------+---------+---------+-------(-------*--------)
(-------*-------)
(-------*-------)
-+---------+---------+---------+-------284.0
288.0
292.0
296.0
Pooled StDev = 2.87


Suhu
MD_5.75
--220
222
Lower
Center
Upper
--+---------+---------+---------+----
-9.220
-13.038
-4.632
-8.450
-0.045
-3.862
(------*-------)
(-------*-------)
--+---------+---------+---------+----
---12.0
-6.0
0.0
6.0

Suhu
MD_5.75
222
Lower
Center
Upper
--+---------+---------+---------+------
-8.405
-3.818
0.770
(-------*------)
--+---------+---------+---------+------
-12.0
-6.0
0.0
6.0
LAMPIRAN 8L
Source
Suhu MD_6.00
Error
Total
S = 2.732
Level
218
220
222
N
4
4
4
DF
2
9
11
SS
70.52
67.17
137.68
MS
35.26
7.46
R-Sq = 51.22%
Mean
305.63
303.00
299.70
StDev
3.35
2.19
2.52
F
4.72
P
0.040
R-Sq(adj) = 40.37%

Pooled StDev
---+---------+---------+---------+-----(--------*--------)
(--------*--------)
(--------*--------)
---+---------+---------+---------+-----297.5
301.0
304.5
308.0
Pooled StDev = 2.73


Suhu
MD_6.00
---220
222
Lower
Center
Upper
-+---------+---------+---------+----
-6.995
-10.295
-2.625
-5.925
1.745
-1.555
(--------*-------)
(--------*--------)
-+---------+---------+---------+----
----10.0
-5.0
0.0
5.0

Suhu
MD_6.00
-222
Lower
Center
Upper
-+---------+---------+---------+------
-7.670
-3.300
1.070
(-------*--------)
-+---------+---------+---------+------
--10.0
-5.0
0.0
5.0
LAMPIRAN 8M
Source
Suhu MD_0.6
Error
Total
S = 10.87
Level
218
220
222
N
6
6
6
DF
2
15
17
SS
92
1772
1865
MS
46
118
R-Sq = 4.96%
Mean
291.32
288.53
285.77
StDev
10.82
11.39
10.38
F
0.39
P
0.683
R-Sq(adj) = 0.00%

Pooled StDev
-----+---------+---------+---------+---(------------*-------------)
(------------*-------------)
(------------*-------------)
-----+---------+---------+---------+---280.0
287.0
294.0
301.0


Suhu
MD_0.6
220
222
Lower
-16.16
-18.93
Center
-2.78
-5.55
Upper
10.59
7.83
---------+---------+---------+---------+
(------------*-------------)
(------------*-------------)
---------+---------+---------+---------+
-10
0
10
20

Suhu
MD_0.6
222
Lower
-16.14
Center
-2.77
Upper
10.61
---------+---------+---------+---------+
(------------*-------------)
---------+---------+---------+---------+
-10
0
10
20
LAMPIRAN 8N
Source
Suhu MD_0.7
Error
Total
S = 10.95
DF
2
15
17
SS
176
1798
1974
MS
88
120
R-Sq = 8.89%
F
0.73
P
0.497
R-Sq(adj) = 0.00%

StDev
Level
218
220
222
N
6
6
6
Mean
296.95
292.71
289.32
StDev
11.05
10.88
10.92
+---------+---------+---------+--------(------------*-------------)
(------------*-------------)
(------------*-------------)
+---------+---------+---------+--------280.0
287.0
294.0
301.0


Suhu
MD_0.7
220
222
Lower
-17.71
-21.11
Center
-4.24
-7.63
Upper
9.24
5.84
-+---------+---------+---------+-------(-------------*------------)
(------------*-------------)
-+---------+---------+---------+--------20
-10
0
10

Suhu
MD_0.7
222
Lower
-16.87
Center
-3.40
Upper
10.08
-+---------+---------+---------+-------(-------------*------------)
-+---------+---------+---------+--------20
-10
0
10
LAMPIRAN 8O
One-way ANOVA: Res Yield_218 versus IV Umpan_218
Source
IV Umpan_218
Error
Total
S = 10.94
Level
0.6
0.7
N
6
6
DF
1
10
11
SS
95
1196
1291
MS
95
120
R-Sq = 7.37%
Mean
291.32
296.95
StDev
10.82
11.05
F
0.80
P
0.393
R-Sq(adj) = 0.00%

Pooled StDev
--------+---------+---------+---------+(-------------*-------------)
(-------------*-------------)
--------+---------+---------+---------+287.0
294.0
301.0
308.0


IV Umpan_218
--0.7
Lower
Center
Upper
----+---------+---------+---------+--
-8.44
5.63
19.70
(-------------*-------------)
----+---------+---------+---------+--
---10
10
20
LAMPIRAN 8P
Source
IV Umpan_220
Error
Total
S = 11.14
Level
0.6
0.7
N
6
6
DF
1
10
11
SS
52
1240
1293
MS
52
124
R-Sq = 4.05%
Mean
288.53
292.71
StDev
11.39
10.88
F
0.42
P
0.530
R-Sq(adj) = 0.00%

Pooled StDev
--+---------+---------+---------+------(-------------*--------------)
(-------------*--------------)
--+---------+---------+---------+------280.0
287.0
294.0
301.0


IV Umpan_220
---0.7
Lower
Center
Upper
----+---------+---------+---------+-
-10.15
4.18
18.51
(-------------*--------------)
----+---------+---------+---------+-
----10
10
20
LAMPIRAN 8Q
Source
IV Umpan_222
Error
Total
S = 10.65
DF
1
10
11
SS
38
1134
1172
MS
38
113
R-Sq = 3.23%
F
0.33
P
0.576
R-Sq(adj) = 0.00%

StDev
Level
0.6
0.7
N
6
6
Mean
285.77
289.32
StDev
10.38
10.92
+---------+---------+---------+--------(---------------*---------------)
(---------------*---------------)
+---------+---------+---------+--------276.0
282.0
288.0
294.0


IV Umpan_222
-+-0.7
---)
Lower
Center
Upper
-------+---------+---------+--------
-10.15
3.55
17.25
(----------------*--------------------+---------+---------+--------
-+--8.0
0.0
8.0
16.0
12/19/2009 11:02:00 PM
LAMPIRAN -9A
PENGOLAHAN DATA SPC

Tabel L8. Tabel SPC Yield DAS.
Pengukuran
Sub
Range
STD
BKA
BKB
0.02
90.806
90.781
0.14
90.806
90.781
0.05
0.01
90.806
90.781
0.02
90.836
90.751
0.05
0.04
90.806
90.781
0.02
90.836
90.751
0.03
0.05
0.01
90.806
90.781
0.02
90.836
90.751
0.04
0.05
0.02
90.806
90.781
0.02
90.836
90.751
0.02
0.05
0.01
90.806
90.781
0.02
90.836
90.751
90.794
0.06
0.05
0.03
90.806
90.781
0.02
90.836
90.751
90.794
0.09
0.05
0.05
90.806
90.781
0.02
90.836
90.751
X1
X2
DEV
Grup
X1
X2
X3
X4
90.78
90.77
90.81
90.78
90.785
90.794
0.03
0.05
91.00
90.74
90.73
90.72
90.798
90.794
0.28
0.05
90.80
90.80
90.78
90.80
90.795
90.794
0.02
90.79
90.73
90.83
90.80
90.788
90.794
0.03
90.78
90.79
90.80
90.81
90.795
90.794
90.77
90.78
90.81
90.80
90.790
90.794
90.78
90.80
90.79
90.80
90.793
90.794
90.83
90.80
90.77
90.79
90.798
90.87
90.78
90.77
90.78
90.800
BKA
BKB
0.02
90.836
90.751
0.02
90.836
90.751
10
90.78
90.79
90.78
90.83
90.795
90.794
0.05
0.05
0.02
90.806
90.781
0.02
90.836
90.751
11
90.81
90.79
90.78
90.80
90.795
90.794
0.03
0.05
0.01
90.806
90.781
0.02
90.836
90.751
12
90.77
90.80
90.81
90.80
90.795
90.794
0.04
0.05
0.02
90.806
90.781
0.02
90.836
90.751
13
90.80
90.80
90.79
90.80
90.798
90.794
0.01
0.05
0.00
90.806
90.781
0.02
90.836
90.751
14
90.79
90.78
90.79
90.80
90.790
90.794
0.01
0.05
0.01
90.806
90.781
0.02
90.836
90.751
15
90.76
90.80
90.80
90.82
90.795
90.794
0.06
0.05
0.03
90.806
90.781
0.02
90.836
90.751
16
90.80
90.81
90.76
90.84
90.803
90.794
0.08
0.05
0.03
90.806
90.781
0.02
90.836
90.751
17
90.81
90.76
90.78
90.80
90.788
90.794
0.05
0.05
0.02
90.806
90.781
0.02
90.836
90.751
18
90.80
90.78
90.79
90.80
90.793
90.794
0.02
0.05
0.01
90.806
90.781
0.02
90.836
90.751
19
90.80
90.79
90.78
90.80
90.793
90.794
0.02
0.05
0.01
90.806
90.781
0.02
90.836
90.751
20
90.80
90.80
90.80
90.78
90.795
90.794
0.02
0.05
0.01
90.806
90.781
0.02
90.836
90.751
21
90.80
90.77
90.78
90.79
90.785
90.794
0.03
0.05
0.01
90.806
90.781
0.02
90.836
90.751
22
90.80
90.79
90.77
90.80
90.790
90.794
0.03
0.05
0.01
90.806
90.781
0.02
90.836
90.751
23
90.78
90.78
90.81
90.81
90.795
90.794
0.03
0.05
0.02
90.806
90.781
0.02
90.836
90.751
24
90.83
90.79
90.80
90.77
90.798
90.794
0.06
0.05
0.03
90.806
90.781
0.02
90.836
90.751
25
90.79
90.79
90.79
90.80
90.793
90.794
0.01
0.05
0.00
90.806
90.781
0.02
90.836
90.751
Untuk X SPC :
Untuk S SPC :
X1= 2269.8 R = 1.15
S = 0.57
X2 = 90.7935 R = 0.05
S = 0.02
n=4
A1 = 1.88
A2 = 0,279
BKA = X2 + A2R = 90.806
BKA = X2 + A1S = 90.836
BKB = X2 A2R = 90.781
BKA = X2 A1S = 90.751
LAMPIRAN -9B
PENGOLAHAN DATA SPC

Tabel L9. Data SPC Bilangan Iodium DAS
Pengukuran
Sub
Grup
X1
X2
X3
Range
X4
X1
X2
STD
R
BKA
BKB
DEV
BKA
BKB
0.18
0.18
0.17
0.17
0.175
0.1741
0.01
0.01
0.01
0.178
0.170
0.01
0.188
0.161
0.17
0.17
0.18
0.18
0.175
0.1741
0.01
0.01
0.01
0.178
0.170
0.01
0.188
0.161
0.18
0.17
0.17
0.18
0.175
0.1741
0.01
0.01
0.01
0.178
0.170
0.01
0.188
0.161
0.17
0.16
0.18
0.18
0.173
0.1741
0.02
0.01
0.01
0.178
0.170
0.01
0.188
0.161
0.18
0.16
0.18
0.18
0.175
0.1741
0.02
0.01
0.01
0.178
0.170
0.01
0.188
0.161
0.18
0.18
0.17
0.17
0.175
0.1741
0.01
0.01
0.01
0.178
0.170
0.01
0.188
0.161
0.18
0.17
0.18
0.17
0.175
0.1741
0.01
0.01
0.01
0.178
0.170
0.01
0.188
0.161
0.18
0.17
0.17
0.17
0.173
0.1741
0.01
0.01
0.00
0.178
0.170
0.01
0.188
0.161
0.17
0.17
0.17
0.18
0.173
0.1741
0.01
0.01
0.00
0.178
0.170
0.01
0.188
0.161
10
0.17
0.17
0.18
0.18
0.175
0.1741
0.01
0.01
0.01
0.178
0.170
0.01
0.188
0.161
11
0.17
0.18
0.17
0.18
0.175
0.1741
0.01
0.01
0.01
0.178
0.170
0.01
0.188
0.161
12
0.18
0.17
0.17
0.17
0.173
0.1741
0.01
0.01
0.00
0.178
0.170
0.01
0.188
0.161
13
0.17
0.17
0.18
0.18
0.175
0.1741
0.01
0.01
0.01
0.178
0.170
0.01
0.188
0.161
14
0.17
0.17
0.18
0.17
0.173
0.1741
0.01
0.01
0.00
0.178
0.170
0.01
0.188
0.161
15
0.18
0.18
0.16
0.18
0.175
0.1741
0.02
0.01
0.01
0.178
0.170
0.01
0.188
0.161
16
0.18
0.18
0.17
0.16
0.173
0.1741
0.02
0.01
0.01
0.178
0.170
0.01
0.188
0.161
17
0.18
0.17
0.16
0.18
0.173
0.1741
0.01
0.01
0.01
0.178
0.170
0.01
0.188
0.161
18
0.17
0.18
0.17
0.17
0.173
0.1741
0.01
0.01
0.00
0.178
0.170
0.01
0.188
0.161
19
0.18
0.18
0.18
0.16
0.175
0.1741
0.02
0.01
0.01
0.178
0.170
0.01
0.188
0.161
20
0.16
0.18
0.18
0.18
0.175
0.1741
0.02
0.01
0.01
0.178
0.170
0.01
0.188
0.161
21
0.17
0.18
0.18
0.16
0.173
0.1741
0.02
0.01
0.01
0.178
0.170
0.01
0.188
0.161
22
0.18
0.18
0.17
0.18
0.178
0.1741
0.01
0.01
0.00
0.178
0.170
0.01
0.188
0.161
23
0.18
0.17
0.18
0.17
0.175
0.1741
0.01
0.01
0.01
0.178
0.170
0.01
0.188
0.161
24
0.16
0.18
0.18
0.18
0.175
0.1741
0.02
0.01
0.01
0.178
0.170
0.01
0.188
0.161
25
0.18
0.16
0.17
0.18
0.173
0.1741
0.02
0.01
0.01
0.178
0.170
0.01
0.188
0.161
Untuk X SPC :
Untuk S SPC :
X1= 4.4
R = 0.3
S = 0.18
X2 = 0.174
R = 0.01
S = 0.01
n=4
A2 = 0,279
A1 = 1.88
BKA = X2 + A2R = 0.178
BKA = X2 + A1S = 0.188
BKB = X2 A2R = 0.170
BKA = X2 A1S = 0.161
LAMPIRAN - 9C
PENGOLAHAN DATA SPC

Tabel L10. Data SPC Heat StabilityRed DAS
Pengukuran
Sub
Grup
X1
Range
X2
X3
X4
X1
X2
STD
R
BKA
BKB
DEV
BKA
BKB
0.5
0.5
0.6
0.6
0.550
0.558
0.100
0.096
0.06
0.585
0.531
0.055
0.662
0.454
0.6
0.5
0.6
0.5
0.550
0.558
0.100
0.096
0.06
0.585
0.531
0.055
0.662
0.454
0.6
0.5
0.6
0.5
0.550
0.558
0.100
0.096
0.06
0.585
0.531
0.055
0.662
0.454
0.5
0.6
0.5
0.6
0.550
0.558
0.100
0.096
0.06
0.585
0.531
0.055
0.662
0.454
0.6
0.5
0.6
0.5
0.550
0.558
0.100
0.096
0.06
0.585
0.531
0.055
0.662
0.454
0.6
0.5
0.6
0.5
0.550
0.558
0.100
0.096
0.06
0.585
0.531
0.055
0.662
0.454
0.6
0.5
0.6
0.6
0.575
0.558
0.100
0.096
0.05
0.585
0.531
0.055
0.662
0.454
0.6
0.5
0.6
0.6
0.575
0.558
0.100
0.096
0.05
0.585
0.531
0.055
0.662
0.454
0.6
0.5
0.5
0.6
0.550
0.558
0.100
0.096
0.06
0.585
0.531
0.055
0.662
0.454
10
0.5
0.6
0.5
0.6
0.550
0.558
0.100
0.096
0.06
0.585
0.531
0.055
0.662
0.454
11
0.5
0.5
0.6
0.6
0.550
0.558
0.100
0.096
0.06
0.585
0.531
0.055
0.662
0.454
12
0.6
0.5
0.5
0.6
0.550
0.558
0.100
0.096
0.06
0.585
0.531
0.055
0.662
0.454
13
0.6
0.5
0.6
0.5
0.550
0.558
0.100
0.096
0.06
0.585
0.531
0.055
0.662
0.454
14
0.6
0.5
0.6
0.6
0.575
0.558
0.100
0.096
0.05
0.585
0.531
0.055
0.662
0.454
15
0.6
0.5
0.6
0.6
0.575
0.558
0.100
0.096
0.05
0.585
0.531
0.055
0.662
0.454
16
0.6
0.5
0.6
0.5
0.550
0.558
0.100
0.096
0.06
0.585
0.531
0.055
0.662
0.454
17
0.5
0.6
0.6
0.6
0.575
0.558
0.100
0.096
0.05
0.585
0.531
0.055
0.662
0.454
18
0.5
0.6
0.5
0.6
0.550
0.558
0.100
0.096
0.06
0.585
0.531
0.055
0.662
0.454
19
0.5
0.6
0.5
0.6
0.550
0.558
0.100
0.096
0.06
0.585
0.531
0.055
0.662
0.454
20
0.5
0.6
0.6
0.6
0.575
0.558
0.000
0.096
0.05
0.585
0.531
0.055
0.662
0.454
21
0.6
0.6
0.6
0.5
0.575
0.558
0.100
0.096
0.05
0.585
0.531
0.055
0.662
0.454
22
0.6
0.6
0.5
0.6
0.575
0.558
0.100
0.096
0.05
0.585
0.531
0.055
0.662
0.454
23
0.6
0.5
0.5
0.6
0.550
0.558
0.100
0.096
0.06
0.585
0.531
0.055
0.662
0.454
24
0.6
0.5
0.6
0.5
0.550
0.558
0.100
0.096
0.06
0.585
0.531
0.055
0.662
0.454
25
0.6
0.6
0.5
0.5
0.550
0.558
0.100
0.096
0.06
0.585
0.531
0.055
0.662
0.454
Untuk X SPC :
Untuk S SPC :
X1= 14.0
R = 2.4
S = 1.38
X2 = 0.558
R = 0.096
S = 0.06
n=4
A2 = 0,279
A1 = 1.88
BKA = X2 + A2R = 0.585
BKA = X2 + A1S = 0.662
BKB = X2 A2R = 0.531
BKA = X2 A1S = 0.454
LAMPIRAN -9D
PENGOLAHAN DATA SPC

Tabel L11. Data SPC Heat Stability Yellow DAS
Pengukuran
Sub
Range
STD
BKA
BKB
BKA
BKB
0.10
5.47
5.37
0.10
5.47
5.37
0.09
5.585
5.257
0.09
5.585
0.18
0.10
5.47
5.257
5.37
0.09
5.585
0.20
0.18
0.08
5.257
5.47
5.37
0.09
5.585
5.421
0.20
0.18
5.257
0.10
5.47
5.37
0.09
5.585
5.425
5.421
0.20
5.257
0.18
0.10
5.47
5.37
0.09
5.585
5.4
5.400
5.421
5.257
0.20
0.18
0.08
5.47
5.37
0.09
5.585
5.257
5.4
5.4
5.450
5.3
5.4
5.425
5.421
0.10
0.18
0.06
5.47
5.37
0.09
5.585
5.257
5.421
0.20
0.18
0.10
5.47
5.37
0.09
5.585
5.4
5.4
5.5
5.257
5.450
5.421
0.10
0.18
0.06
5.47
5.37
0.09
5.585
5.257
5.3
5.5
5.5
5.5
5.5
5.4
5.5
5.450
5.421
0.20
0.18
0.10
5.47
5.37
0.09
5.585
5.257
5.3
5.425
5.421
0.20
0.18
0.10
5.47
5.37
0.09
5.585
13
5.5
5.3
5.257
5.5
5.5
5.450
5.421
0.20
0.18
0.10
5.47
5.37
0.09
5.585
14
5.4
5.257
5.4
5.4
5.5
5.425
5.421
0.10
0.18
0.05
5.47
5.37
0.09
5.585
15
5.257
5.5
5.3
5.5
5.4
5.425
5.421
0.20
0.18
0.10
5.47
5.37
0.09
5.585
5.257
16
5.5
5.3
5.4
5.4
5.400
5.421
0.20
0.18
0.08
5.47
5.37
0.09
5.585
5.257
17
5.5
5.5
5.3
5.3
5.400
5.421
0.20
0.18
0.12
5.47
5.37
0.09
5.585
5.257
18
5.4
5.4
5.5
5.3
5.400
5.421
0.20
0.18
0.08
5.47
5.37
0.09
5.585
5.257
19
5.3
5.5
5.4
5.4
5.400
5.421
0.20
0.18
0.08
5.47
5.37
0.09
5.585
5.257
20
5.3
5.4
5.5
5.4
5.400
5.421
0.20
0.18
0.08
5.47
5.37
0.09
5.585
5.257
Grup
X1
X2
DEV
X1
X2
X3
X4
5.3
5.4
5.5
5.5
5.425
5.421
0.20
0.18
5.5
5.5
5.4
5.3
5.425
5.421
0.10
0.18
5.4
5.5
5.5
5.3
5.425
5.421
0.20
5.3
5.4
5.4
5.5
5.400
5.421
5.5
5.5
5.3
5.4
5.425
5.3
5.4
5.5
5.5
5.4
5.3
5.5
5.5
5.5
5.5
5.5
10
5.5
11
12
21
5.3
5.4
5.6
5.4
5.425
5.421
0.20
0.18
0.13
5.47
5.37
0.09
5.585
5.257
22
5.3
5.4
5.5
5.4
5.400
5.421
0.20
0.18
0.08
5.47
5.37
0.09
5.585
5.257
23
5.4
5.4
5.4
5.5
5.425
5.421
0.10
0.18
0.05
5.47
5.37
0.09
5.585
5.257
24
5.5
5.5
5.5
5.3
5.450
5.421
0.20
0.18
0.10
5.47
5.37
0.09
5.585
5.257
25
5.4
5.5
5.3
5.4
5.400
5.421
0.20
0.18
0.08
5.47
5.37
0.09
5.585
5.257
Untuk X SPC :
Untuk S SPC :
X1= 135.5
R = 4.5
S = 2.18
X2 = 5.421
R = 0.18
S = 0.09
n=4
A2 = 0,279
A1 = 1.88
BKA = X2 + A2R = 5.471
BKA = X2 + A1S = 5.585
BKB = X2 A2R = 5.371
BKA = X2 A1S = 5.257
LAMPIRAN -9E
PENGOLAHAN DATA SPC

Tabel L12. Data SPC Bilangan Asam Residue.
Pengukuran
Sub
Grup
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
X1
X2
X3
24.6
0
24.6
0
24.7
0
24.5
0
24.6
0
24.6
0
24.5
0
24.6
0
24.6
0
24.6
0
24.6
0
24.6
0
24.7
0
24.6
0
24.7
0
24.7
0
24.6
0
24.5
0
24.7
0
24.7
0
24.6
0
24.7
0
24.6
0
24.7
0
24.6
0
24.6
0
24.7
0
24.7
0
24.7
0
24.6
0
24.7
0
24.7
0
24.7
0
24.7
0
24.7
0
24.7
0
24.6
0
24.7
0
24.5
0
24.7
0
24.8
0
24.6
0
24.7
0
24.5
0
24.8
0
24.6
0
24.7
0
24.5
0
24.6
0
24.5
0
24.6
0
X4
X1
X2
Rang
e
R
STD
R
BKA
BKB
DEV
BKA
BKB
24.70
24.625
24.650
0.10
0.13
0.10
24.687
24.613
0.07
24.785
24.515
24.70
24.675
24.650
0.10
0.13
0.05
24.687
24.613
0.07
24.785
24.515
24.70
24.675
24.650
0.10
0.13
0.05
24.687
24.613
0.07
24.785
24.515
24.70
24.625
24.650
0.10
0.13
0.10
24.687
24.613
0.07
24.785
24.515
24.70
24.625
24.650
0.20
0.13
0.10
24.687
24.613
0.07
24.785
24.515
24.60
24.625
24.650
0.10
0.13
0.05
24.687
24.613
0.07
24.785
24.515
24.50
24.625
24.650
0.30
0.13
0.15
24.687
24.613
0.07
24.785
24.515
24.80
24.650
24.650
0.20
0.13
0.10
24.687
24.613
0.07
24.785
24.515
24.60
24.625
24.650
0.10
0.13
0.05
24.687
24.613
0.07
24.785
24.515
24.80
24.650
24.650
0.20
0.13
0.13
24.687
24.613
0.07
24.785
24.515
24.60
24.675
24.650
0.10
0.13
0.10
24.687
24.613
0.07
24.785
24.515
24.70
24.650
24.650
0.10
0.13
0.06
24.687
24.613
0.07
24.785
24.515
24.70
24.675
24.650
0.10
0.13
0.05
24.687
24.613
0.07
24.785
24.515
24.70
24.625
24.650
0.20
0.13
0.10
24.687
24.613
0.07
24.785
24.515
24.70
24.675
24.650
0.10
0.13
0.05
24.687
24.613
0.07
24.785
24.515
24.80
24.675
24.650
0.30
0.13
0.13
24.687
24.613
0.07
24.785
24.515
24.60
24.625
24.650
0.10
0.13
0.05
24.687
24.613
0.07
24.785
24.515
18
19
20
21
22
23
24
25
24.6
0
24.6
0
24.7
0
24.7
0
24.7
0
24.6
0
24.7
0
24.6
0
24.6
0
24.6
0
24.7
0
24.7
0
24.6
0
24.7
0
24.7
0
24.6
0
24.6
0
24.6
0
24.6
0
24.7
0
24.7
0
24.7
0
24.6
0
24.6
0
24.70
24.625
24.650
0.10
0.13
0.05
24.687
24.613
0.07
24.785
24.515
24.70
24.625
24.650
0.10
0.13
0.05
24.687
24.613
0.07
24.785
24.515
24.70
24.675
24.650
0.10
0.13
0.05
24.687
24.613
0.07
24.785
24.515
24.60
24.675
24.650
0.10
0.13
0.05
24.687
24.613
0.07
24.785
24.515
24.70
24.675
24.650
0.10
0.13
0.05
24.687
24.613
0.07
24.785
24.515
24.70
24.675
24.650
0.10
0.13
0.05
24.687
24.613
0.07
24.785
24.515
24.70
24.675
24.650
0.10
0.13
0.05
24.687
24.613
0.07
24.785
24.515
24.70
24.625
24.650
0.10
0.13
0.05
24.687
24.613
0.07
24.785
24.515
Untuk X SPC :
Untuk S SPC :
X1= 616.3
R = 3.3
S = 1.79
X2 = 24.65
R = 0.13
S = 0.07
n=4
A2 = 0,279
A1 = 1.88
BKA = X2 + A2R = 24.687
BKA = X2 + A1S = 24.785
BKB = X2 A2R = 24.613
BKA = X2 A1S = 24.515
LAMPIRAN -9F
PENGOLAHAN DATA SPC

Tabel L13. Data SPCYield Residue.
Pengukuran
Sub
Grup
X1
X2
X3
Range
X4
X1
X2
STD
R
BKA
BKB
DEV
BKA
BKB
4.96
4.95
4.97
4.97
4.963
4.965
0.01
0.01
0.01
4.969
4.961
0.01
4.979
4.952
4.96
4.97
4.97
4.97
4.968
4.965
0.01
0.01
0.00
4.969
4.961
0.01
4.979
4.952
4.97
4.97
4.96
4.97
4.968
4.965
0.01
0.01
0.00
4.969
4.961
0.01
4.979
4.952
4.95
4.96
4.97
4.97
4.963
4.965
0.01
0.01
0.01
4.969
4.961
0.01
4.979
4.952
4.96
4.97
4.95
4.97
4.963
4.965
0.02
0.01
0.01
4.969
4.961
0.01
4.979
4.952
4.96
4.96
4.97
4.96
4.963
4.965
0.01
0.01
0.01
4.969
4.961
0.01
4.979
4.952
4.95
4.97
4.98
4.95
4.963
4.965
0.03
0.01
0.02
4.969
4.961
0.01
4.979
4.952
4.96
4.96
4.96
4.98
4.965
4.965
0.02
0.01
0.01
4.969
4.961
0.01
4.979
4.952
4.96
4.96
4.97
4.96
4.963
4.965
0.01
0.01
0.00
4.969
4.961
0.01
4.979
4.952
10
4.96
4.97
4.95
4.98
4.965
4.965
0.02
0.01
0.01
4.969
4.961
0.01
4.979
4.952
11
4.96
4.97
4.98
4.96
4.968
4.965
0.01
0.01
0.01
4.969
4.961
0.01
4.979
4.952
12
4.96
4.97
4.96
4.97
4.965
4.965
0.01
0.01
0.01
4.969
4.961
0.01
4.979
4.952
13
4.97
4.96
4.97
4.97
4.968
4.965
0.01
0.01
0.00
4.969
4.961
0.01
4.979
4.952
14
4.96
4.97
4.95
4.97
4.963
4.965
0.02
0.01
0.01
4.969
4.961
0.01
4.979
4.952
15
4.97
4.97
4.96
4.97
4.968
4.965
0.01
0.01
0.00
4.969
4.961
0.01
4.979
4.952
116
16
4.97
4.97
4.95
4.98
4.968
4.965
0.03
0.01
0.01
4.969
4.961
0.01
4.979
4.952
17
4.96
4.97
4.96
4.96
4.963
4.965
0.01
0.01
0.00
4.969
4.961
0.01
4.979
4.952
18
4.96
4.96
4.96
4.97
4.963
4.965
0.01
0.01
0.00
4.969
4.961
0.01
4.979
4.952
19
4.96
4.96
4.96
4.97
4.963
4.965
0.01
0.01
0.00
4.969
4.961
0.01
4.979
4.952
20
4.97
4.97
4.96
4.97
4.968
4.965
0.01
0.01
0.00
4.969
4.961
0.01
4.979
4.952
4.952
21
4.97
4.97
4.97
4.96
4.968
4.965
0.01
0.01
0.00
4.969
4.961
0.01
4.979
22
4.97
4.96
4.97
4.97
4.968
4.965
0.01
0.01
0.00
4.969
4.961
0.01
4.979
4.952
23
4.96
4.97
4.97
4.97
4.968
4.965
0.01
0.01
0.00
4.969
4.961
0.01
4.979
4.952
24
4.97
4.97
4.96
4.97
4.968
4.965
0.01
0.01
0.00
4.969
4.961
0.01
4.979
4.952
25
4.96
4.96
4.96
4.97
4.963
4.965
0.01
0.01
0.00
4.969
4.961
0.01
4.979
4.952
Untuk X SPC :
Untuk S SPC :
X1= 124.1
R = 0.3
S = 0.18
X2 = 4.965
R = 0.01
S = 0.01
n=4
A2 = 0,279
A1 = 1.88
BKA = X2 + A2R = 4.969
BKA = X2 + A1S = 4.979
BKB = X2 A2R = 4.961
BKA = X2 A1S = 4.952

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LAMPIRAN -1

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: 0.1-0.9; 1.0-9.0; 10.0-70.0

: 0.1-0.9; 1.0-9.0; 10.0-04.0

3.4. Glass cell, made of optical glass, 1" and 5.25"

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4.5. NaOH 0.5 N in methanol

Timbang sampel sekitar 0.02 gram kedalam vial 5 ml yang tertutup

Tambahkan 2 ml 0.05N NaOH metanol, dan panaskan didalam blok

Tambahkan 2 ml larutan reagen BF 3 metanol, dan panaskan didalam

Keluarkan dari blok pemanas dan didinginkan pada suhu ruangan

Tambahkan 2 ml heksan dan 1 ml larutan NaCl jenuh, kocok dan

5.2. Determination carbon chain ini pack column

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For fatty acids :

HP-FFAP, Cross linked polyethylene glycol-TPA phase

Coloum Glass, 20% DEGS Chromosorb WHP on 60/80

Coloum Stainless, GP 10% SP-216-PS on 100/120 Supelcoport

Flow rate of Gas :

3.3. Recording system, Chromatopac C-R6A

Minimum Area, Count

Chart speed, mm/min

3.4. Screw cap vial, 5 ml

4.2. Carries gas, nitrogen with ultra high purity (UHP)

= Kandungan rantai karbon i dalam % berat

= Area rantai karbon i

= Faktor respons rantai karbon i

Sum (ACixFCi) = jumlah dari FCi x Aci

7. Informasi-informasi lain yang dibutuhkan

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4.2. Distilled water

5.4.2. Tambahkan 15 ml larutan kalium iodida 15%

A = Volumen natrium thiosulfat untuk menitrasi kandungan

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CPS, SCPSA and Oleic Acid

5.2. Tambahkan 10 ml Sikloheksana, pipet 15 ml larutan Wijs dalam labu yang

= ml Na 2 S 2 O 3 0.1 dipakai pada titrasi blanko

= ml Na 2 S 2 O 3 0.1 dipakai pada titrasi contoh

7. Informasi-informasi lain yang dibutuhkan

7.2. Untuk Oleic acid, menggunakan 25 ml larutan Wijs, 20 ml Cyclohexane dan

5.3. Perlakuan Peralatan

5.4. Cara Kerja

7. Informasi-informasi lain yang dibutuhkan

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Color 51/4, R/Y

Bilangan Iodium (IV) Umpan, g /

Asam oleat, C 18-1

Asam linoleat, C 18-2

Sumber : PT. Flora Sawita Chemindo, 2008

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Yield Fraksi Ringan (LE)

Yield Distillat Asam Stearat

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Bilangan Iodium (IV) DAS

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Bilangan Asam (AV) Residue

Keterangan : AV = Acid Value (Bilangan Asam) dalam mg KOH/gram

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Heat Stability (H/S)5 ,