Py] wee JOURNAL OF CHROMATOGRAPHY LIBRARY — volume 44 analytical artifacts GC, MS, HPLC, TLC and PC Brian S. Middleditch Depanmen of Boctenia ard Biya! Soknces, Usvesty of Heuston, "4800 Carew Roos, Howton. TX77008, USA = ELsevier ‘Amsterdam —Oxtord— New York—Tekyo 1989 1 smucrec 33F nernnaenmmeaty. senescence rauoma cour anrne. Newvou Wwrouen Ft con 1808 Free ee cogs Re, ae AE Bn smvouserssee teserea No a of benny pind, en ree ey ot ‘umes my fom br an ane, soto rece, poe weeny Seaman nett prev upactgussin st use See Ser ber BF ‘ixitne engcon PO Bor, 1050 samen, Teheran Sgr nes een ia Ta pent tn ng nth ar ‘Sonconttn srw romcper ape the patan ey osm eA At SEs at ad ace mt esa ae no owaentty au Oy ait ayy aa wo pean oper ‘isi cineca hem pin ero spoigh avrg male pan a cifoe nhl ned ans, ont ‘RetpBlecon oe rt conte pre oder be ay 8 ce 0 Dedixartn arm raet roy menace ‘Ths oo pr on ie ee D220) Popped # % 3 3 g 3 3 3 g x % g‘BRAMRAARARRRAAERESEEEAARAEE SEA HARARARRAARRRRRRARARRRRRRRRARRRER dhianl TE RRAAAARRARARAGEARAERABBAAARAR SRE ANLRA NRA LLRRBRRRUAARRAADARART High bat Ik i HauSRASRAISAIARAHAARRAREAI RE Ses BIgELESDasESereCK ERE Rr ER eRAgsEoOssoS il tl iat AA RRRRARRARRRAARBRRRAREAG8253222557 588A BABHRANBARREHARARRERRARBAREFEE A / BEDRBABRBARERMRRR GG GUeEaa OO TEEES TS 293 288 aSSATTONITTTIGOE TIESSRSSRBSRRRREREB! BREREEES sgngaueRengeess eeeee.asaaananuNsaasRRanccnancee: EREEERGRAHRARNBAURARSAASERER! eet i \ ‘gegUSUSSESRESTAERRTTTIELITAS SSS OSATTTTTLTNNNT NA TETEESITTTETLEE iH ii wRRERSE SERSinane SON Terma 2 ebb and Mares eda data uasaaee see BERR ESS SESERDERARERRARERERAREARIIT AQRIISA ITI AREAS HOSSERSSSDISAABRASAIAABOELELERLERRARAREREETTPREFACE From lie ad gouged ln gt beaies Singh go ban ae ie Maye god Lord eer ns ‘Anyi cerns shold, perhaps, nly hs wana Com rye tae ‘Pareto fom Marphy'e Caw. Pw sa reriabe plore o piled problems Beare Se ve std experienced mat lke ow saya cere SEG st Sedan lag twa, comers a ee os |Fis'elode epson a canlog of he tubers orn analy nur 3 hee Compan ose ne em ‘hist ie le welt on pce wis, Howee:stol te rosa © ‘ue soe nda ef be types of rte wh com 1+ raise a ria may mas nd can each ot see, a stupor ilae tc ey Soden rari pai conan fo {im ea ru be py of sea no sna wed Sengdeuget fom tps toe + Acetate ns mee apa et ite end of erin i SSC a tat Bg Sed Wy doe as "onsen ae Am lege x esr yi cece i Screed ek SSR ea RB ra chained ‘Tica con pot fom bur msaiesties ins eaead ede ree Sloat ky ne males, seed ingue eerdcas ea slvens sued he enroute acd wo ober pada Ye ‘tee Etc smart to pobish he fadgs ‘Coarse Pasty ese an Mies ners of Hoon ggnauaysgdaygadeexeeseuuaaanaa dae ee dane ERSINTRODUCTION Bethlehem ve et Egon Bose hc rm re see rg Seataegate Uleterc peer ek maa ee IepcsNarataaTiar sche emmene pool Os ci Tite ACETALDEHYDE C2840 (49 “The comsnn are of te substance gan. Inn cae i aceon. For some {niet chokr ef name spent ile Soret ary sce ee a seve fergcnysued synonyms. The molar feral nd moleui eigen ie Fgh of te Te For ine onveienee of mas spatreacopts he sleeula weight ‘esis om th mga ori nigh oh st st re exh een, Reeaiseide is Ox Bhs (ot) stones: Now ta he mie weigh of he tos ‘Bondan oops of cleric 35,0 ht mayen clonae (CHSC) ssa 8 Inoecle weight of 12+ 2) +238) "Be Mass Spectrom { ‘Specra were recorded in th u's abort obtained tom he pbs erature ‘Allott seta vere obvaed by cleston panto, wih a econ energy of ‘ev. Soa tented ha some of the pera donate oe wih me vas ‘10 com masa fo so emanate see compound ree re a Structure owe Teeny sein empl ee“ rey YF musePT 2 Mudaedoh [Chemical Absracs Service Indexing Information eet re sc i epee it Eectece nes Soe eigen pet ay SESS wreseaud ty ae le ena ‘Stadt abana des not mater wher an auto a fers oath [Seog amen Genet amet Shoes aan seer meme creche SSS eee Merck Index Releence “The Mer nde an xe Ky tote eure. referee ven he Teh lane rsd for sees wc ea x vous Te Nish Eft hs gorparin vm sh tenes i molec weigh eer or he anvenee of mas steps. Synonyms ‘iunfomupte tat mo cei ave mie ones. Seve pause meni te Suncnalee spat of tomezcate overhears pu ie ala | ‘Sends to deo bs name wert fet oitem. The Coie Rtas EEfieeusses yen foment or ee of ceed ey se is ‘yen wih he pba een ces ex. Ermine ean en ea Fri Ree =ERaeene AnalytlealArifocts barr mora ere of et ade! fed, ‘SARS i iety ceed” Stine” a massacre aad tata ‘Stspmund io milnaedegradacon during Krage, 0 his wil menoned fhe bev Pager ecoce a made ts Cems apples ty Ath Chemis Co. meee Shee i oo ofthe few companies whe fen eiphend we revel he EEShst ato aan ner snes ns eieprtctenert intr ait te ‘eae tere eer tates SS eee Specra of Derivatives i L ese of eis daquenty encountered, so aon pera ae semetnet [ved och nebyl ents Osmebyloune why xy nd met ‘eng spropie Tae rayne eaves ch forte wi ah ‘ea eed eal Sergi ape ws wih ecomsrng aE Gas ee te spat ae and me Forni awd Be eset rose Rte as ein cosceoncig ht en ply it dering hfomasn ‘rownispcoral ster age mnspeas nem ‘Compe era ones se provide, oh ee il ve a pod incl of ‘ecient 3 phlexoe or cng Ratings mare fungal Inthe more Foran obcr ari to be Bed by eaiy an Serve 9 Sedat marl encie + Middteditch Indexing : ee in pest” ines, wih eins deed Mourn Bae Rae “There also Molecular Forrla thr, nd Subject ingees, The ste inde Fantalscompretensie. oma te nemo of nonopaph of ert, A ABIETIC ACID CapH3002 (302) Pr 05 so 100 150 302 200, 250 300 350 een, (CAS: LPhenaubrenectonle ad, 12.4494. 610, 10adeeh ol Atdney ‘Aman aty Li (hata dba, S110). rel Aediogty Mer index: Mas spcrom: NBS 4827, Aas 1909 ‘743-Abietadion 18 sel, (1 {LSB fn. 1000)-123.440-4 5.610.108 Dees Tyson dey. ey phonandeneatacye ei, 1 Uponidenteae see See pea pores. resin ai common encoun in wood produ espe raper nd devon6 Midateich oui te xed hs st ol poor uty andes evidence a ene ogrdalen Homer's s sia pupa arved ty ehding thee, Resin acs wok ‘eco be sayed nthe ce sitet he pres hcccararat ‘pe wer mic apnea devecenon mite cried. es ‘Sear sy cep ec Mas spect fmt set CH (310, NBS 4, les 191": rs 4 i 50 100 150 239 | \, 18) 200 250 300 350 See oi: RACs /ETALDEHYDE cx, 4), TP laa so 100 150 crycHo (cas: Aah 5-0-0) Mera: 31 Masser: NBS 3978, is 12 Analytical Arifacts 7 ‘esi adhe, ld, tana Ey ye cnt stm rely ie eee 1) Se cc ans nena ethan nd Wace Ree iaelly cane fain oa (ng) wi me mle She SINGS), 2k of hae aera chee) nd gh te ‘ese rine of wi tes semper tn er area deed oars een “as etal, 1981; Exhsson et a, 1 cess ecgee pba ee a ee regia geo cept ter eo ‘Wik Shey ac deter ecb tee concn he wa frat of wea fo ancl, Hoe Bielefeld end wath pron wi amy cop ey Acs can conde wi 6 eyeliner teiycsonsintins ‘ui eran oysters earbes et ae Sept 191). Dl ie Lor Teer hence hes pgthacne ss oe igen Seater ae Acsuldind cn scone wi dane price pty Lares ass specu of atch Oty orine [HNO CF, NBS fz so 100 150 eal: Cmonoroeu, DIEM TER, DIMETHOMANE, EMAL EEE, ACTA ‘Sistine one Pagal sono Puivono Scenes Teno SoCuNO. nes, TemaoRO canoes- OO tas spectrum of he NA-dimthy ernative of acetamide [CaHgNO (7) NBS 6, Ye crim of he NAc [catyxo ACETAMIDE CaHSNO (59) ** 59 hs 7 A 50 100 150 50 00 150 Formas spatnam of 0 -suinethysyceaie sete enty fr that compound (CHSCONH, See alto: ACETONITRILE, N,0-BIS(TRIMETHVLSILYL)ACETAMIDE, N{TRIMETHYL= CAS: Acai [6035-5] SEACH Mernde 35 mt NK i ene nem ‘ina tnt te eR spaiety cer actin eee En iaeana Apne rt spt er vee cet NOE wo ys |” 50 100 150 5 3 : & 3 i CeHyNO3 (151) os 151 1 1. so 100 150 ‘CAS: Acta 1-4hydroxypheny- (108-902) Merktnder 39 Mas specu: NBS 467# Resin index: 1687 Arey ta 1985) Aten eal Acs, cg, ¢- Anon Aspe ihesaminapsenel, NAcetypaninopievl, pAceyainopbstl Ai Fait Ayton, Aine io Aporie:RPAF” Beruf, Biches, Cap (Ciel, Chnoayne, Dar, Data gee, Doe, Dolipae, Dymadon, Eola Ene,10 Middledich nn, a Fn i a et i haeayeeaaie. pipet saphena Sein L2aenp, Conese, Lona er ome tn a ‘Analytical Artifacts iran ofthe Wises) deriv Mase (255), BS 498 uw of sextaminepben ICiaasNO2Sin sa et Pi Tener, CO eb cine fa os Ps rien Vaan. Vale nse ene tii ee eps ese : vpn wie arta ety oie wich mye ih te J ‘pipe Seip aia 97). x x esau be tebe enaineten OU) NBS 47 180 7 ws woe 280 295 L 200 250 360 wo 0 * ee 8 j State: ptenonmerniscenc Ac, PHECCETEY unm cof vine eter ingen NOS|C2).NOS wot ACETANILIDE, ' es |! wpe CaHtyNO (135) a | a 4 135 30 100 150 i 1 2s 3° 100 oy PaNCo.cHy (AS: Asien 10844) Merk 200 250 300 350 Mas specu: NBS 4087" Retin inde: 1362 (Arya 1985)Rn Middtedivch al frien wing cies. Whe ti yaa aire o i ao nave meron eo serial patearanaag wie reest rtd mx anv 98 90,10 30min argon). Unde Fee eyo aematy iy cram and ie egrdanon POON GEESE en reeten ones tad ese _ eesti oe ateteeiscnh ace ig Meciatahishemnieancemnormane = See cio: 0 -BtrRBCM SELYUNCETAMBE,NTRENETEYSYUACETAMIDE ACETIC ACID CaH402 (60) ye iso 0 100 150, cao cont paras te Sa ptt) tneeaityeitcmes Yr epee eet eae ae acne asec Inmet where a loa marae male alain fo resents of volt ais, ‘cose ay te pal ebvene vase Gee, 17? Since cay easy onde see a tise hat cers canine Eihamuitiye case ou ect, sons Geena moO Me yaaa ee & pret npc al ing ngs, oa eased etal in- aiconning cco ap reetvisetier ftiyeces el moorpmiensrpesenmne of ra) tasters Teed pate ge amawesc t al sen cl 197). Analytical Artifacts B so 100 150 See ale AceraL Dano, CoocesTescL, DIETHYL Fn, ETHYLENE GLYCOL DIACE- $ave GLoES, PALDUTC A, Tene ARIINCIS, -TETRADECENE ACETIC ANHYDRIDE CaM 05 (102) as 1 (102) 50 100 150, xeon Ch hoon ia soon Ate jecoz fot sentence Setar hearse Se lt: N-ACETYL2 YOO FYRIDYLACETIC AC, PREDMidétedtch Genrer C3860 74) ACETONE las 50 100 150 HOCH,CO.CH (CAS: 2Propanons, Hhyrxy (116096) Merk dex: 56 Mass pect: NBS 22, Alas 75,61" yroxyacetone, 1 Hydny 2 propane ‘Acetokwas pore ms contamina in acetone which had been manofactsa fo ‘ne halowsha ca, 19160 Se ae ACETONE ACETONE CaHte0 (58) 50 100 150 cHCO.CH (CAS: 2-Proparane (67-6411 Merck Index 58 Mass spec: NES 3980, As 28,2, 3%, Speier and Spiele (173) Analytical Arifacts, 1s inet al, Dine kwne, PKenpopane Met tne, Prosi ether Repo ss conan net eer (Ene and Spelt, 1982), ont (1976) ‘eeu to dct acetone in Malick ecient EEE iB Sic Alte contere leg wi alesis woo! Acstore was, Soecver und wte preset ms coertaton 0.00% ste 200 ie eid Toole ise need ener 0g of abyarusmagestr sl, ered ‘Saeed 1000 fd by evapsucntnder nuropen ct war eating pate. Tis, (Sins scene was iosaced ding e Gong aneencenaca sep fe cncetaon [i esl! wesyee coe oas 200 pi Nona were proved forte soe etn netiyene aie before flan Acs among te exopnous capone of the human xy oils (Labows Pais ‘Acsvene femaee sa soul a ene, Evens (1987) has ole Pat tone may fea hom veiled epee i i se cri ut aise nanece res earn reetae {iar and 130 ened. by em be reeved fice rom ae op $637) idiia eer cucnonteeuw man can aoe ‘hse ep rsd shold be Cscatedfesuey” The Mere dex nice Oat soe Riana yee oma deeteen een So Stiagesew eee cee se oe eet areca Sars Sacer aes ah ap Bitte Woesacirene vetatonem bie Egiciagyawctmmetie sate Sane ae HRI Sumo mats moamant toes cect errs aA ceeded twee te sna ce, wie Lau Pe (8) te Epadeere amie mennae sens Semaneamone ‘Una rode scree wa fon corn dictoe seal, uy pte ety (eigen ee aro a -Acctone which had been manvfctarel rom cnn was own conan act, bt siren at ete aot ee, ny rhea ee ety isn Pena Tt pad oleimaiecrs balioac, ‘Aes (1970 eyed tat a boro grade sven contained tg noclale fie wherest en rly! eagen Gace actors ete’ Yes uh O01 gfe The ‘lures ofthe reo samples of sre weet Eve ‘econ ca pers wih amines to race Sti bess (renter and rant Sprawl meses pyc) se,16 Middledivch sr rouse eon ect satan . Mas ecto of cone O-ethyoine(CH:NO 7, NBS AEE Analytical Artifacts ” ite (22.6 pra, snd scion (002-8 ppm) (Kakemcto and Mayan, $e ao: ACEtA MIDE. N - scar st YUACEEAMIDE,BUTYLATED HYDROXY ‘rowan waits anon SUCeORTEE NEN 1 x Baht er li | {ACETOPHENONE Exo aan ann : 30 100 180 [8 Seco: CETL, ACETYLENE AXLLARY YLATEES,RUTANONE CHOLESTEROL, Sart cree cone bmtwt Menucate Dene ee BEE - Rare DONOR Rete BUEHMUMSNMBROL DCT RI {LATE DonAlaus, ETRANGL, ETHYLENG OLYOO DINCETATE SOEHDRORE, MEST L l Suman etic Seve mm a fe nne ennatsounote Mmmsrvanie Oeste ‘ce, Fee, none nce TM A 30 100 150 Proc AS: Enero ey 18.8621 ACETONITRILE CHiN GH nero, hem 98.862 Mer ne 6, oy Masset NESS, 778° Rein i: WS (Any etal, 185) ‘Aevesicnon, Aceytberase, Baroy mei, Hyon, Met phy kme, |-Fhenyethwnne, Phenyl meant Ketone mm nwt steno a estan pot Tras OC (Les an Wan, 0 so 100 150 Ie rote when teen wed oe ead a rena a AOE, Folia dtu 8). Te poke sf acpecne guna a et yen Eger iemni tals eve sie pac uaa tlspn resp) Soc ora hat AS: pes 150581 Seat yea ep oe Mert nde o 140 Acetophenone ass peso NS, As, Spr an Spee (93) - fassane pees neti yt, Mane cb, Mey oh USAF : 3 iS ae oa + 3.30 Arsinpriy in 0 sess Sh 1972) : : : 3B lori cece in vin gsi nae aes 840 pm, : $ : fou oan 3 ppok oclontesee OBES peas ola: seta yore18 Middlediich ‘Acetepenene lar exresed in irons pecan (6x Semi) ‘Analytical Artifacts 1» pecan of mayer of acer cd CSHNOs (131), NBS 40754 “Tex experiments wer complied 1 sme eet ye fact ta sh Tes ls Tighe of topes tan ant Te so ‘See i: TOU ARTIFACTS «6 : 2 1 131 "ACETOXYDIMETHOXANE, Cattn404 074) ACETONE so 100 150 “pe mates etl omen tte Rat A ‘Mas specrum of timehyiy ernie of amu ‘ae wd cosy te ecnrega spies ites ch i (NOS (180, BS Somewhat ee Wooues WO. Seca: DOEMOXASE _ i 16514 ‘ACETURIC ACID CalHNOs (117) i ACETURIC AC 1 Lass) TT. so 100 150 iss Sees ACEC ACD n 1 Ww ACETYLACETONE + r CsH4s02 (100) so 100 150 ‘cHJCONHCH,CO.OM = cas: Crng Nace 158.2481 © Meck inter 75 ® 100 Mas perm NBS HT" permit ai, Ace anintte Wie. Acete, eee anon = ee 150 Eero steve herein cHyco.cH,co.cHy CAS: 24 Rat vesdna tea mgd san ops ate lowing pe of aces fine (23.5.6) sess rsp ia a ae enone Finer ACS G39 EROS Fp, Arce crm sto REO yf eA al aie x troup toes St ty low sted wah Reo ings Ong ab 1976 as speceu: NES 407 as 240° Acne Doce20 + Miadtedich Acesuestone was eed ate mance repose fan tectonic afer sci, = a ars tar shew fo pte Soke Sesh yer aan chen oe Saw 18 _ N-ACETYL-1,2-DIHYDRO-2-PYRIDYL- ‘KcenIC ACID ColiyNO5 (181) 50 '? 181 30 100 150 oc, isnt rin ES vin gt" (ac neat vestments nwt pet er ete tt ces a a ReRAS mattmee nae ‘perene os yaa of encytn (compound sled from cereal mame itereed teagan cu ican Solent! oe Get cmiaetecyamn fanvcot Pep abate seed 1 Sta rato, sie orotate, bes place when wiorontic hue Peerage ion. ‘Seat: ACC ANDRO. PYRIDINE. TRFLUOROACETYLATION ARTEACTS Analytical Arifcts a ACETYLENE, ca eH) so 100 150 HoacH CCAS: Bye 4862} Mercknder: 4 Mas spe NES 3877, Ais 2° Bain Ismmaeed asa soln store, Ever (1987) ta ord that cee ‘heron sce Ass gs te cate poredacepine By ‘iblirtonGt-S1°) teas [wedi dy eons with oxygen sors (i {cr Ths pacar was conde ely wy sr cua of eye sce Tad ten named iy my mete evaatng exposes had crore ring the rae ‘tercjune Woe aboraa ‘Acein among te contmiaut tt cts from Tefen FP bags (Lonremsne aL, fagglne ame us 930 See al: ACETONE, TEEN FEPCONTANDAANTS N-ACETYLTOLUENE- (CAS: Acta 4 syn) (2720068.7) _No-Tejsenyseaice ‘A. minor metiolte (6 in rat 2% in ac) of tohene--slonaide, an ip in ‘Setharn "Ths meabote was Werte as met Serve, Tome By oman, SULFONAMIDE — CyHy4NO38 (213)Midleditch Analytical Arifocs 3 vegeta i, eget te saengmentaemra mits ania ca = Eonaaoer | vee pat gerne tae ‘eae Pa [ 200 250 300 350 2 . L See en we eae a pcooausen on | padeonenen Le thee 200 280 300 350 | cast 2s-Popwericwtontic sid, Hayy) tay ser 7-507) “Set aba: SACEMARIN, TOLUERE SULFERANIDE CapHts40 (402) CETYL TRIBUTYL CITRATE v9 50 100 150 Mace specam: NBS 3122" Reta index: 2253 (Ramsey el, 195). ew 122 pope eye, Cf Tint Det ‘A pli component evi wd Ara 97) eve sped maces ert cna sa hh ay cnc ese ‘Sitar The pate were arr as en pore 8 Fp Corp tots mart fo af ty ei) (eyes, BYR Sale cncearsan athe me ach aoe re, 1D Ay eg ‘ray maces wages a fire ene an A TY Seyi: cx RCD, URE L200 CONTAINS TARAme Middteditch Crating0s (318) ACETYL TRIETHYL CITRATE — cxf “Teco S123 gmat Gen) i ay enn 23 peatoneniiyen ATE, pt any 9-ACRIDINECARBOXALDEHYDE C1aHigxo G07) _ CAS:9-Accnecatraeyde (885.284) Dyce joe 101 Combats eater sepue eammge 9 igs coreg OV ta eat Saaiscn S30 gsc BT) ‘ACRIDONE CisHyNO (95) 167 \ I 50 100 150 135] Analytical Artifacts 2s coo (CAS: (10 Acriione 158-950 Mas specu NBS 114" Accdnene,8-Aciinone, 9. Acros, 10) Acton Aflac deve foc the aay f pinay ad scenery aati aries yi faye chemaouragy ca be peared fy reacon i chy ne ise re aurea ae) tscniJaion Oe Meco ly nin ates Urine oposite manag opeoee cee RE Simbeer al 19). Anempe once plo he Booey Scodaing fected twit spate ee ele cones of otioomacandceto anion elcciec ed Bi et ADENINE CsHtsNs (135) is i s sa 108, so 160 150 or i CCAS: HF Pun Gann (7324-5 Merkede: 12 Masses: NES 4086" ‘Adenio. ¢Arinopusive 6-Anioo Uf poe, 6 Anio-V- pve, 6 Ani Spring, LeDRyco-Simtrpurine, SoD 6 ningun: Levees, Vas bs Many ap seat os cen elie reps tom bood bark peor! ‘equ or ool neeled tbe vc ft ay ha er as# 4 1" eset vt hunts ey, ty scree ymusrne ee z Soe coe eeaeecaceam gions BoM aaratenmeere tne Sia waren caret Hine Sainte oui to anys by as amszy etal (1980) reper fat fe alenine was mot amenable Sromacr ‘See cs: EXPIRED BLOOD CONTAMINANTS 9-PHESL ADENINE oe ADIPIMIDE. —C¢HyNO2 (127) poor Won agen neta 8 seeenpctrece cee artnet Cue 8 wencwenen ADRENALINE BUTYL ETHER Cy3HarNOs (239) J aa so 100 150 Analytical Arias ” 29 , 200 250 300 350 mo, Naot, (CAS. Fyne 1 -bao3y 24cm) DOT) Mas span: Forest ea 1910)" 4-Day 2(meyaninetylprcaecst ‘Te: of mukiple ses dsig paper chromatography of cxeebolarines was ‘rela ey 58 yap varie ot 57 tower ure rt oe ‘lass stig wee polis fr ese sp were dsconerea. Fares era (19%) lenlaedte cherry roar and wes pats wi eet ‘ten rat of ain bel, te ol was eed by ms ‘peso nd ote ech as enn a ADVENTITIOUS TRIMETHYLSILYLATION Rerasaeaty deetira esheets asin Bear ed etre te en ee tt eee cuts cota meme sane Beate ‘Siuenne oft cnhion edie tore hopes AFLATOXIN EXPOSURE- 6 = iddtedich Analytical Arfcte » AIR LEAKS : “ [Aires wa contua bem formas specs. They tend ae he ese [Ste source and efi noone, wl ey wy a arn owas. A Sve ek nigh onde mere even um kot We ave aceon ceed ‘Bemus pec of enone to ronson therm Sane Tons hare of ak nt mi 14 4 oF), 16(0° 0029.17 0" ECG) 20 ch, 2 yh Se (One. 0 (Ar) sn (COW Sle ok Spl, 173), Oi tine mass pnts Oc e asf compas nd de ‘hn ms mais) wl ete wage ea fr cen ro ea fiancee. Te wily bea pat ove «6 (eqroming Aro we Ghee id speacdyOk an nasa wes Pelt ‘Leak dawn way be cle any of seve lve Ie ea ssl enough low {he Rnment ete en re ean fan ie ue spore om 4 (CHICO") ray pret woe spt whan lec e eakAL ay eer A Tar sks. Leaks of ordi ee mr woul. Ths be meee Grong sue tanec my be pose > stan, apposh omens fr apa) sok ‘ebarl sree dense: ‘Stactaee 58 cnet copia clans amas specrone wing alk ‘arundel sea ye by tang Ror ugh ss et ‘Seralng he conecter" Ths speach analogs that ployee) Vea eat ‘Bene Ca lose es) avec fhenatparh ped vid ‘hres ene helre ron oc even caer of ak Sl eer ‘Parmen umsthie50 ihe mba ere armen hse 6 ela ALKAPTONURIA ARTIFACTS Allon sa dso of pam lala re neat ic which homegente sede nigh come gee. evel ot ae ‘then isa songedting spent wih he craton of tan reine, ‘Ehydowyndalccee 8, ran, abet (Ko, 989), ALLENE, CH (40) 30 100 150 No-00H, CAS: 12 pain 53-490 ass pec: NES3974 At 89 A posi connie slope Vanier 642 and 3 serpents (a@is Wii e)necagees a Se ee {est he tubs epattd alee ose, in Sn cms SPs at fen eon spe. See at: BuoopcauscronDeves SE ALLICIN Cellye0Sz (162) CHe-CHCH,SO.SCH.CHACH, (CAS: 2-opee Lunatic i, $2 proper exer IS39.86 6] Merkin 245 ‘Tio? oper sulle ai Salyer 1p te undead contin gai eits te ono ot. A knowlege cok wll thayeteuihs pric ene er ar lew etaneee ore Tneeeese fi inary ansermatn lvs bers be ee ans, whch ce ili Cta=CH.CHSO CHCHIOH)COOH) to produce aici Ii ales ich ‘porte forte favor of gar, Ca ol catty sam Sis crs ees Beep wheres reel dal cine Since secrecy shoul nt hat ete rate fem pol ebaied fy tea nnn co tes ‘ne smc ard anvomttspoperie fc rene Pro (Deh, ‘Alii undergoes debyraion dain gas chromatography to afer two tomate Seine wnk en sang arom peli ea Apron ard lies abr tal, yf ee PONS ME sie30 iadledich “Ain wa found by Moca (1986) ne lloingcongeperaonsin vty of ‘a praca erbe bls (4-62 megan honey (4 ROR) EN 2 te pat ics ace ne Gee tan gael em aa tontatc cath Es Fue mar tte Nias Mase EEN uatin Se pmcesine ie ALLYL ISOTHIOCYANATE Cass 09) lat 33 conceit cost os vena venom Sn Ane ee sus aminenen nao aie eh at aes ealed Popegtsctnoeynne Retsin, Symes must ol Volele ‘ale mast ‘a ischiocyanate she odorous cestiert of Mack rtd seas, Kewell ‘Aah atiocana Sen ang theyll of ae frm subj who ha {Crowned ned coming lrg amb tse, See ae: Sava a [ALUMINUM FOIL CONTAMINANTS “mm eer pegs sesh hx laces ry ai ore ty coe Cit eared a rene er mee rao OY Sea ca a os oem | } i Analyical Arifacts a AMBERLITE XAD-2 ‘ete pti inex yee tm aoe ean eee et pe ettanmeyeoe ey ae eee cee a A asst delgitenee, 2) pease kp Seay Fels atten) omens, copie Gee aches Soh Seen res annSleN GC cartes tates ‘eprnaed orm aie oy et te ieee connate ‘ipegente mentees cee etegs TCopah dhyebave (13 pn cinyfenzene © pon) iybyehane (6.7 ppm, ey analog Sg ance rosin ieee Bch son prods egecurered when Amberite XAD-? i expoued 0 nite one eck adda Gy le al pute dey psa, inet “Genayltene ack direnesyheaee Middedich Analytical Arijocts B AMBERLITE XAD-4 AMBERSORB XE-348 Merk er 38 A nceplr ropbic ln extange resi: sree dveybn cops. pris eect in hi rein cde bey (100 pen, 13. (014) tenn {oe (H0 pp), 1 -ipberithane 3 ppm), ati £3 meee (0 eat debtor, (or?) eboapbtane (10 pp) eysyrene O70 Fees netpten Orne, epee GAIL 2) ‘enarlee Spire peered ane Sp a, BE ue sa ang, ‘Scott a. (1988) have mpgs ha soe of tee mpaities a fore dng he [putin armani sy of Ante SADU Thee of to en {Sry temic cna rented gee casa emp ‘Blk et a (158) conelued hit Abete XAD- was to eal comand 0 be Slater uo ees omer Se ol BONY, DOERR BEXZENE 1 DUMENLETHANE, LET. Neniineske KEmiyit pase abet EDVENAAMTALENE ENN ~ SRne, METNLRIMIEL, Meng NDENE MEMOUNAENTIALENE, ETM STYRENE NAMUIMALENE, STLBENE, STYRENE, TOL eXTLENE AMBERSORE XE-340 ‘A nonpaay, mysrogbotc lon excharge resin: exbonaceous compestion smi 6 aij abate Contaminants extracted from this sesin incl petcen (or phen), [Satire telatcszpen tpt, Opa came” fee ey mein ce mation eh, to?) ‘Segoe sa ona dasa ea lo (18) cone tt Ameria XE 340 was o tev coined be Sch forbe ace nays of panes fom Ye. ‘Se alu: ANTURACENE, BEXZDP.UORANTHENE, BENZOIDINAPHTHOTHIOPNENE, BISARPaiti,PLLoganTcne, FuoRane, Mer iMENYL< MENON LENE NNT#ROSODIMETYLANING, PIENANTHRENE, PHEXVLSAPHTHALENE, AMINO ACID ANALYSIS We hie plo of metas wif etna of nin nee port ote aos el mae Se lens eso hve ewe We precede sy date lr ec ce eed i eae ‘Bs drenstopapy ef ron amine sei ernst re rblem, These le yh cera sno Sx char hn, AMINO ACID CONTAMINATION ad ct (1972) mre a nde oes fs ad carina rere whe tga aces craps of tcc een ‘avi og Dat dled wa coed 610s ca neve oad a Se comapinu cle envy ene cet fl who ca ‘Chi feowedty copia riming wid ipl dated ae, Hyg aie archematgrapie pats wich ick wih Sanne yee ele sete poeu Middleditch Analytical Artifacts 35 sc ait prepare by ation of iso, the use of DL supplement low-ethonine soybean-bese infant aan hamish geet ei FE rsa fin eo new pine spent 2 from microbial contamination (Hamilton and receiving these forrut 3-AMINOBENZ[d]ISOTHIAZOLE ’ 1,1-DIOXIDE C7H6N202S (182) HI 182 od fo ty Cul 6, CAS: 1,2-Benzisothiazol-3-amine 1,1-dioxide [7668-28-2] ‘Mass spectrum: Renwick (1978)* An impurty in xetarin, The compound is xcoed ‘unchanged in rat urine (Renwick, See also: SACCHARIN AMINOBENZOPHENONES ibe, se drs mayogur when they ae hed Ang Solon andr enviar for aher metodo eas, Indeed has boy pone) that some benzadiazepines become desalkyatedio the corresponding primary henones during cid hydrolysis (Verwelj and 6 Bruyne, 1983). found in paints with ceria ay remboles accumulate in high eta me pete ain aS. '36 > Middteach Analytica Arifacts ” 7 4-AMINODIPHENYE SULFONE, CrattyiNOxs @3) ro { om 250 CAS: Renan, ya) 7019.14} 200 5 500 sso -rentaen Meriine r coe ibs of por, AMINOPROPIOPHENONES. sek nt Sn 4) ive lee eae ws pass mig iit nit tmp 2s rag rman tet dear Sokersainsm can acvwagie Prin, tment mee snd taney eae fee ————— saa ran = roe ps cesraopphy A roe iotes ‘ton peo siping a seanetaae he Eps ‘Srearogap ayes Soh eats ae, however ‘acu to |1-AMINOPYRENE 9 189 so 100 150 (CAS: 1 yer 16066731 Mas pecrors Swesmu 1982)" Anioprene $Arinopece LNinopyrne decomposes dng sss by combined gus cromatography ~ ase ‘Spee ia pot otainely Meath ah aninpyrene has bony monsraed tal sega spn ie he OCHS ana ee a a ‘Begs pecrorece, a wells nt pe cerssoprph alam Senn coe ‘Seals: NTRATED REMATIC HYDROCARBONS es AMMONIA, HN 7) eee 7 30 100 150 iy (CAS: Ammonia (1658-41-7) Mer nex: 500F Middtedich ‘Mass spectrin: NBS 1 Ais 1* omed when tense titans ie ened inthe pence of sts ste (Corkins ra 198). ‘See eto: AMEN ACE CONTAMINANTS, THOEANOX, UREN ‘AMMONIUM CARBAMATE, CHN202 (78) NH{CO.ONH {CAS: Caramel, nncanennks (111-70) Merk nde: 518 “Ammonium anintornt, Anise of moni cbonste cmd when te nsec tito te in the presene of sinks sc (Crk ear 198) ‘See aso: TNC oe AMMONIUM CHLORIDE HACIN (53) Analytical Artifacts 2 (AS: Beane, (pponyrreby (382145) Anylbenyonite, Bey any xe, Ben pentyl eer ‘An impuy detect in bey a pane by Novo and Novos 1979) See ali: BENEML BUTYL METIALATE . AMYL BENZYL PHTHALATE oc" oon ‘CAS: 12 Rereetioxyi ai ety penne ese (1240. Av inpy detected in ey ul pas by Novo an Novsndov8 (1879. Se ooo: BREE BUTYL THALATE CapH2204 26) AMYLENE, Cato 70) Niect ‘CAS: Ammnam erie 12125429] Merck Kader: 522 amos, Sal ammonia, Ametlor, Ammoseric, Aeonium mute, Drammen, ‘Sarna “ene fend can ih boast eee cane ce win ape a2 fe PCE a gestae for vm appease, 1977) ‘See aso: HEXANESAIYLDISEAZANE ARTS oe ‘AMYL BENZYL ETHER C12Hx0 (178) CcHy(cHascheocHPn ES \ 70 so 100 150 (ory}.0-cHeHy (CAS: 2 Bee, 2a [13-35] Merck ner 635 Mas specu NBS 16, Ais 62, 64 Bary, 2-Methy2ene, Trimehleyene ie a preset in Bde nt Jackson “ted in cl Napa RE Sea hor meyer os Ge ‘“m- 0 Middledisch ‘See bo: CaLoRoron, MEINE CHLONDE. ANILIDE. DERIVATIVES ‘Storch carbonyls may become mie evi by ween wh iit me Geet ye chee eC Cres when St BODE Set a nen fn ne hw when be erdon cont wt Analytical Artifacts a ‘Mass pecram of Wiis atne [CllaNSig (37), NBS AB") 7 50 100 150 peo "fe comes ne for ferme which decongones we allo ‘Sor rnmnide pon werent wth cyl cde acetate (Une 97). a Cetin ANILINE HN (93) or 1 ad 200 250 ‘300 350 See als CAPROLACTAN NV DDAETHVLANSLNE METHYIHENYLAMENE beck vo Cats vena saeco ast pret temt aos renee Anincteozee, Arinoptn, Arie oi Benadan Biv ol C1. 76000, C1 oxidion fe Cyan Ryan NCL CUN736, Phare Repo ior pty incapeactan (Caen ta, 1981). Formas set of hme che ery or metybenyie. Formas gece of -ietalie se heey fr hat ssa. ANISOLE Cog es os 78 so 100 150 Procty (AS: Benen, methoxy 1004631 Mec ae: 694 Mas perm: NES 401, As 337° een index 915 (Ary et a, 585 Medxyteszene Mt pen bey, enytmedyebera Middledich Fomed ding oncokne tytn of ay ad sing inane hy oxi, pred ete toed ot etn ard was gree Tt Pe eh Pleat a stem (Waans ad Halper 8} ANTHRACENE, Crattao 178) 76 ‘\ Analytical Aries a ANTIFOAMING EMULSION ‘anol eta (966) consis encountered wo eas in chvoraogans cine! dng ‘Ao gs Chromaogroi salar of he Favor fection of series cencetatd ral ‘lad experent iacsed har they derived rom a arifesing emulsion, bt he Fees werent Gaerne. Antfcem AF eben ol earer been wed by Peta. (9c dang te as ehemaopagie sas of sersed concerted ik, Bot 10 ‘eal penser ned “See lo: ED CAPROATE, ETE. CAPRYLATE, Ene OBWTHATE, ETH. OLEATE, Eni pears enivs marcos Er Sannare Eine. VARA, so 100 150 OO ch sos ct vase NO 0" cnn: aay bye pain Qs onic epee neni rt Ee at nt Pre 8 Rosman area Saas Sebi See io: AMBERGOND XE 40, LUNAR SAMPLE, PHENANTHRESE a ANTICAKING AGENT ee ee ‘Auch Cheri Co, wets sodium chlarse wit a race amount of a wide ‘Baking agen Ovinch nd , 587 See las SoDRMEILORIDE ARACHIDIC ACID CapHtaq02 12) as 73 50 100 150 200 250 300 350 (Gs(OHpyCHgCOOH CAS: cos eid 1906305), Mec nde: 96 as spectra: NBS 2363" Anco Repo a consent of ler paper Reber al 1970.7 ‘Maidleditch Mas spetru f ety ahi CHO, 02, NBS 412 As 1985+ a 87 so 100 150 so 109 150 200 250 300 350 34 400 450 500 50 Analytical Arifacts 6 See alo: RTER PAPER CONTAMINANTS ARTIFACT or ARTEFACT? Bat sping re accep, and here 0 rer meng capers of ont tothe preted speling- Compact sec: of vars tees (se Sey aes ted inca arses eta oopl wed fs nes ra fe SAB) Database Artitact Artest gic, 2% Boe Seca wd Fite ats 3 { Bee pecer e 4 ‘bse Se Evtermere face % 1 ceeecmwrry mersionl Faron Aoss gf Necopopea ed fame 2 : papal demand 2 3 Rite Ate a i et mr oe “Ta he spelng “Arlt” has een wd hong bok, ARYL PHOSPHATE OILS See abe: SwernPa seat ASPARTIC ACID C4HaNO4 (133) 6 °8 S70 { 135 Se woeencouancoct cas ramen ven ve 0" came man ent ay esters of erifworoscettes ae fequetly ex as derivatives forthe analysis of nlp tere aa eat ee eae Fee ate ree eee soa aie ct Stn ca foe an ccna OaIEAD nnn asin co J a [20 138 180 ‘so 100 150 Analytical Arifocts a (CAS: Beni sh, 2c) [0-78-21 Merk ne 8 Mas spectre NBS S00" ett index: 1308 (Ae ta 1985) . ‘Acetyl, Aces ala, Ace, Aetogte, Aes. Acti ai, Acton, ‘$c enone act vactonpbetasc a, >(Acelony)berae aa. Aca, Ae i pli secon, Aig, Ave Apne fs A Ep ln ema Roo Say Spe, Sct ese vy utenti ie sree anette emit Busmes fone eae canoes Rene eu teneiria ce numntte ams issigerintnege mentee © aa Seciammrtemersensammel, tte gee tpe teres i iit eete tae aren Gee sp ak mecca ite ne snare ae Bes ieee ere iam en cae ee DEAS Geel nee ee RA ere A fs ee aed ea Securit cen nearness ApS hoi Angee Grad-sae aca muacn an Eocene ge ee nen a fs eat tin ies me eet ee Soo cache meaner Saba Ge Ge eer ane BS ceri ghes eine Oe oh a (Ere en Nee fie Sec ta are ‘ae beer ea rents ide hice Mai cane! Nee ome ge rain PAC Paige Re 6, Pete, Fem, Perl Peo, enteric nm poet ieee scaurrehoe inmate ee as Hoot rele eaueeate cae SEL Sgheiaa aa Wagener mete Ee es ire ree ora oa Se is oe oe PRE: Foloyae, Trtacgese. Yrncopi, Tamines, Tig, Tec, ‘engi ad at ‘cpp an do orth ra the restce af her cents body Mus. ‘28 forex bt he rico of ponagandivrs , Middedich se an ain ep ee nag tn geaaiteemetaaenoanerg ect Mas spectra of pita ey eer [C198 NBS 1090" =a, 4 T so 100 150 Mas specu spa ety eer [04S 52) NBS 17724 a 135] 210 22 200 250 300 380 See aie: ROSTAGLASONSA RB. Analytical Artifacts eo “Te catechol xrogens (2 and tydronesuogen, such as 2.nydroxyestacil, ‘Bien Sapien) ae peasy pape nn Serine omied presence of sole Shor sae ge wee? Solan sae as en enplye ant mininie s of hy ony endtociegi ayaa aa 9) teeter ier ge it aera adseanhines SS aaSs eee eau oruinomenrace AXILLARY VOLATILES Broo compound ected anor haan aly vlads sete, ene, GyFenenes, buyled Hydrant, tuyaed tyrxychae,chiortert, ded [Bisa ciple, tata rel ime, opp! msn Egypt cideemoa Wosee, mistylen” melee chicaée, phere, ‘evn tee, een, sof xyes Gatoes ay 9 See ala: ACeTONE, BEWZENE, BUTYL ATED HYOAOKYAWSOLE, BUTYLATED HYDROXY. ‘TovvENe, CrLororon, DierHve MALATE, Envi encent, 2ETHVL-T- [HEKANOL SOPHOPYL LAURATE,SOPOPYL MARCARATE, LOPROPYL MYRISTATE, ISOPROPYL PALNITATE,OPRGPYL PENTADECAMOATE; LOPROPYL STEARATE. Isormorvt TRIDECANOATE,LIMONERE, MESTYLENE, METINLENE CHLORIDE, [NAPITALEME, TETRACHLOROETHVLENE, TOLUENE, THICHLOROSTHYLENE, vans RVLENE p KVLENE AZOBENZENE Ca2HyoN2 (182) AUTOXIDATION ‘oxen gs hula facto be unde analysis of bikes 2 ean ‘Sentate sac in supe hich me red wder faeries pera, 1B) este ae comon aontatcn roc of neurat pe ‘sean les cet and 3 ett a pa ‘Sete abte fom te eh otis eyed and eo, 981), 7 so 100 150 Pieten: F, Middledich CAS: Diane, ier) Merck Index: 917 ‘Mas specu: NES 4931, Midi tl 9810" ‘Reset ines 1586 Rams ta, 1880) [Azobenade, Asean, Azbibenaee, Azan, Aare, BeamenesRenene, BzeRSfune Ophenyinaee Die ie, ENT 14611, NCECODS26 -Digheniyrzedecompases Gung ws omc afd anbenene (ia rasa B Bo BBO CpHygNO G73) i ‘CAS: Onazle,25.tist pes 49 2085-8-2 Retton nex: 3710 Rams ta, 1980) 2 By tipo), 25-8 pes) nae, 2S DHE ‘A stain eget Rare, 1980, BROT “Com CCAS: Benzoazoe, 22-25 shighenedinniAS4(0.1 ive [128-645] en nex: 2745,5750 (Rasy ea, 1950) CagHtagX2028 (430) 2.5.Bia- tert-butyl. 2-denzoxszalyihi {ip niophene, 22-25 Thiophene Anion reagent which fend no ‘een i of S750 ad ner ‘a0, haga pk witha sistracnes nee‘aiteich Analytical Arfact 53 [BEHENIC ACID Catly0s G40) 394 a 5 3° ay 3 T + 200 250 300 so J a Sect: PTR raven cena 3° 100 150 BENZALDEHYDE HO (106) Pe 3 3! 200 20 300 30 cttycrasoHCOOH 4 4 30 CAS: Docosanoic acid [112-85-6) we i ‘Merck Index: 1023 Peo walocenres a atcisne AS: vata 000-7 eon Me no 154 Reo cen the pp Reg 197 nt eal, 9 Masepecas BS 018 Ase 1,31 ‘Mass spectrum of methyl behenate {CzsHqs0; (354), NBS 495, Atlas 2024*): ° " een nya an NC, 191), 96a, 158) 7 ‘Alon iil een Ait send, Ariel if anon, s 7 ‘erect at Saba as An np nec bey ay pty Nev Nowa (9). J Bey i apn af Te Ln Wie 10, = iW edt spe minal elisa so 100 150 Felimat sales (Petz ea Bere may sm syne when sci coring at hocaton fed ere sconce frac Rusa es) eon Pride ncomerade Mupenclieni Gaga scmlog = Pheryaceoe, an ant forme ding he mays of ampetarne newbies, can ‘do be eran i hence (bechet an AL Sana 12)Middtedich Fas pec of eral O-meilosine (HNO (38), NBS 35°F so 100 150 Set ao: BEAT. BUTYL ATALATE, PHENYLACETONE, STYRENE, TENAK ARTIFACTS BENZENE Colts (78) BENZENE 7 yl gc 8 a 268 ox 07 209) oe sehr cam. pen am aang FoI Ga poesia eee ga imecedio™ Foon ease ‘eae maybe pda om lhe ven ane i ening tat can pes ie Tenax vest Pelizat ang Kron (988) Gemonstaed hat Fukelecabexent is convene! Pgbensee donne et cea nen hoe ohio ih par a Hise Sete rostral, 30 ve “en ‘enzene was ppaeniy employed toc hpi conan wed or be caper ‘cies al Celea bu fever deed dre De sala. Moree, Pgs ce an seen Sa ie, se, es ae Sa Tn Sng te naw rae ross of teraee- Tse Of oD eget pried nc oe nari “See eto: AXILLARY VOLATILES, CARBON DISULFIDE, CHAECOAL, CYCLOHEXANE, eleeatzene, Crcvoretani, ruses, Hevane, 2MMETYERUTANE, SASiEEyeeteace, Mermn2¥el ores ane, 2 MEnHYLreNTaNE, METI MET Bacon ccLonertarnut, SOLVENT IM/URITIES, TNA ARTIFACTS, ‘facta TOLENE mw RYLENE oRWLNG POOLS nn (CAS: Benne [71-43-2) As ve cor Mas: ‘NBs 3967, Alas 10,101, 1, Speer and Spier (1978), Mile: Sabet 0380 Rete nex 64 (Heydar aed Mom, 19618) canner, Bens, Berge, Benen, Bcarbret of hydrogen, Carbon ol, Coal Coane, Bere oe stn Maar teas Sse ewe, Pen ‘ie rte, Pyrotee Repred san npr inte owing nes tne a cmap es a pms oe Spe pp) Cie ‘Sink io. ‘Bene naman be expen comport fhe aan sir wales (bows et i) putes epned in grades of Benzene eas 2ettrane OOS. A, se eee I pm), hreaypenane (0095-01 PPM hexane ESS (AS: 21-Bensnisale 2 oe, 13 hyo ($8.38) Merc dex: 100, eigen MB, AOMB, ASME, 13-Diye 2 errialoe. 2Mesa- SORE ear {aero oe metic amt omy ase,‘6 ‘Miaaledich BENZ{é\ISOTHIAZOLE 1,1-DIOXIDE CyHgNO2S (167) 0 [ TS iy9 ve so 100 150 co estén vemnmoea cue repaint ama BENZ(d)ISOTHIAZOLINE 1,1-DIOXIDE Cy HtyNO2S (169) ire 3 | | Ll cso) 3° 100 150 & (CAS: 12-Bensseile, 231, -oxie 36163} Mas spect: Sic ea 1976)" sna cs » 2h ae foieyattt moan 7 ena (oaastya rete compet er seat ‘85 unconjugated and 40% conjugated; rat 15%). om Mass pect of ety Serve o terezie | oie (CN (0) Keown ans asta oe ‘cies FenaOs Te hes ad Mas: spectrum of tinuihysiyl derivative of bezdlsthiszeline 1.1-dion [ejtighOst Es Reick aa Wins TR a I 50 100 150 2a 200 250 300 350 Sea: SAECHARON,2-SULFAMOYI BEDI ACD, 2 SUFAMOYLRENZYL ALCOHOL, Coolie (282) wu Sin Reporte sa commit in Arter XE40 esi Haan Panga, 1982),Middedich “rere are several isomers of benenfcehene, nai benvolelacepenayne, Fa aera enw ifuoraniee, tenon, bers |Woray. enol ucrahene, Mevafezysee axe fee. Atelpats who rely sly x00 are a eqn cont angus between ese Hemet. ‘See cue: AMDERSORS XEMO C8603 (122) jos 22 so 100 150 Prco.o4 (CAS: Bensole acid (6585.0) Merk nex: 198 ‘Mass spectrum; NBS ASH, Alas 500, S02" ete index: 1160 Ae ea, 1985) ‘Benzenecaroxyic ai, Crbsybenzene, Days, Penleibony i, Phenyl: Rema ea Recser BA newer, Temples eri aden roo ee Mi OR Pe a egal i chy is pnd! hen yee is cole oo Tenax ap for SRE) Sine bene ele td Kros,196) i would no Be enexpeed 1 rd Sette Sain theses, 0 Benes acid has a been eptea aderaaon prods of Amberite XADS2Biowsh Bear ao oa race hse hs pased (aan ca, 381 ‘ig common species of aca have ben an ysl perc iw bee ek wich co reap came wi tone bers ane Se wl ca Tee canteen i ur rac fei Fee te pees cl bers be woe bt ae Series fond arene va pein. ‘Analyicl Artifacts » as spectrum of rah henast CDs (139, NBS 31, As, 691693, 694 135 7 wo 1 | Pa owe sx ge cine. 69 re 7 2 oe Sel; Aste #TEXAD 2, BEXZALDIDE, TENAX ARTEACTS _— JENZO[BINAPHTHOTHIOPHENE, Crete 23) so 100 150 200 250 300 350o = Midedich Analytical Artifacts or CMe ed 10) Romer 27. hn-nten Ee Cee oe tee 58) Mas spec of tenure Osnethyxine CHgNO 1), NBS 13904 CAS: Reng 2-86) 7 135 st era: SIM ts ss ph iio ‘Reported as contaminant in Amberoed XE-340 resin (Hunt ae! Pangaro, 1582). a, 1 See also: AMBERSORB XE-340 * 100) 150 BENZOPHENONE CysH 90 (182) rs n ve a0 zo m0 30 Seeoe Towers 50 119; _ BENZO[a]PYRENE, Captl2 252) co 4: ea de 1968 ec ns: a: BS 2A 3 Peas 161 aay 18) 4 = v09 wo sr ie ene yee Oude lankamey a rested een bee ny ening coed seadeSeancpadlsek cu tiene ey” Dome eatin eda nt a cain coerce tetamae sestjper fi hatyaene Retour ntacongtece Geen, atlatert Bipatteckartnaten ase xe mo we ws (ere Iden 8563), Benrptenone 6 f2-dnytony 4.r. Middlediich (CAS: Benollpyree 150324] ero Inder: 1106 Mas spect: NBS 486, Alas 1756, Meech et a 19 44 Benaopicen, -tenropyrene, 67-Deazopyrne, 34-Benpyten, Beazyrent, Set Betophne 3 Abenepyone,Benllpyree, OP, SA-BP, BO? Benaseyrene collet rom certains om ers ep pcepeily in ae ee ondsig in Ve ee See aio: CUMEEONS BENZOTHIAZOLE C7HNS (035) iss 30 100 150 ca (CAS: Beran (95.1691 Mere inde 111 Mass spectrom: NBS 38, As 677° Retin index: 198 eye and MG, 19818) Besenlfonazste, Benaizse,©-2857, Thin arate, USAFEK-4812 Ferret and Fanagan (1973) oud tt benzoic fom rt bing conan Fer ney fae Sud They ntl at epost were common Anatyticel Arifocts 6 aur pening teers aos ois mals fob concn A ter pring er et Wa eal ith gop (Se ae art a 8 ee Fe sr) satan mk beso 9. sa ed el ee 8 anes cere mi (rede 13 end mil a aenndFamgss En 4-BENZOY-6-CHLORO-3,4-DIHYDRO-I-METHYL, (QUINOXALINONE, CreHlisCiN: a 50 100 150 300 250 300 350 Soy tom Mas spectrum Sade a yn er Kea (709° age of siazepam 45.epoie, ns rarer GSS ERS gna “Seve ome sn aos remncurty Ser aa: DUZEDAMMiddiedtch Analytical Arifacts 6 BENZYL ALCOHOL rH,0 108) BENZYL, BENZOATE Cuti203 @12) 708 es 31 30 100 150 30 100 130 enon sks, AS: Eee 01 Meni 130 212 penne, A IT So erin de: 146 Rata, 180 105A ea 5) 200 750 300 wo ena dc, Benet, eo cl thyenene Peso Prcocctaen ‘Fen Feenyinetancl, ene alcbol Toten CAS: Benzoic acid, phenylmethyl ester [120-514] -Aninpcy eect int hl ialaby Nevec nt Noe 7%. seen ae eu sto an deaines hve teen sili ncaa sch separa {Pe sa Hanan 197 Bown a 1 chan 9A Cape cea Dl as stplaa spe metic pong, Psat pie mero ee lca spas oc el ing, Paco of pose omens eta cose rey igh tees ey acd Soe ey ee epi se et fepuin Bowen e195) Ben lol is formed by tyes of NNleclten.0-benalsoure and Bente expt reg ese ata ‘Mas spe of bale rime eter COS (180, NBS 910%) BT To 135 50 100 150 See: BENEYL BUTYL ATALATE, DENY ETHER, EPA Mas spectrum: NBS 442, At 1510151 ‘ASeabio,Ascabil Benyinte, Boreal tency exer, Benz leche benoic een Benzyecserenrbonye Benzyl, Beny!Poyiinen: Cocker Nese, inmate Seahnes, ante Vera" eae ‘An imputy detec i ey ty pial by Nowa and Novsadrs (1979) See alo: BEXOVL WR¥L THALATE“ Miadledck Oe BENZYL BUTYL ETHER CuHye0 (164) BeNzyL BUTYE ee 164 50 100 150 PRCH:OCH(CHe)2CHs CCAS: Benzene (btoxyey [588 7-0) ‘Mass spectrum: NBS 670" (Guaoeymety benzene ‘an ipury dsc bray ty pial by Nov nd Noveston (197 See alto: BENE. BUTYL PHITIALATE BENZYL BUTYL PHTHALATE CygHt2004 12) rs ior 1 L 50 160 150 206 312 200 250 300 350 Analytical Arfcts o np CAS 12 Benireicubonicald ean buyer 85687] Mass sper: Midleich eal. 58° Reteton nex: 2327 Ramsey e198), 2909 (Ane ea, 1985) Ben ig pti deme, Bu Dery pte, NCLCSSTS, Paatin! BB, Sine oleate baci {apenas inet a Bare si rd Croty (1996 repre that "evra nnchlrnated sents of USP ot Sepa gchar enone eas eir eo oie sir memceem aaa eave spanner aerate ae ena ciate eee {Suareteieig fet, dod day te ol eng ef ese tw psi was eS Apis in ent ay elas decry Nos a Never (97 eas tol enn eal ten! pal, beach, byt a tea beet, ember clin, cyt bay peat, Dena cary ale en eb pte, tempat, tual, yt tezoate, ty yl ivi, ‘lara pin, ciel pale, er a Boal ne saber lonee ‘See lo: Ny REN ETH, AMY HENEYL ETHALATE, BXTALDENYOE, BENZYL ‘Accom, Bexeve HENzoATE, BeNave BUTYL Iv, BEV co.OnDE, BENZYL ‘Reeve mistacaré, Bovey. Wom. REALATE, BENGYL ISOBUTYL PaTMALATE Nebxzvurniatimibe, BUTYL aLconOL, BUTYL GENZOATE, BUTYL ETHYE ‘ReTMALATE, N BUTYLPTHALDMDE: AMY PHTHALATE DENEVE PATHALATE, Biron rite boa. milan, DonSA ETHAN W ERMAN BENZYL BUTYL SEBACATE Catts204 648) PhCHzO,OC{CH2\xCO.OCH.{CH.)-CHy ‘CAS: Deere ai ay phenynty 12288364) Reto nn 2130 Ray 3, 1980)co . Middteditch aap sete , Alesis. Asie ten an acne ws cin ne eae ad acca acy BO). “t See: DIENT. SEMCATE, DIRUTY. SEBACATE BENZYL CHLORIDE CHyC (126) 126 50 100 150 Prowse (CAS: ene, oro) 1004.7) Merc ae 136 as specu NBS 460, AS, 304 (Cerone erzae, Chloophenytnetan, 0-Chorooen,c-Chertluene, ‘NerGiee0” rope ‘Aa pty detec nbs apa by Nowe nd Noveadrd 197), Seeoio: Ber wu LATS, POPENE OX BENZYL HEXYL PHTHALATE oc e000 (CAS: 12 Bennet ai eal penne ser 7217047.91 ‘A inpty dtcesin ten tl pla by Nowe se Noes (199) Se co: BEE. BUT. LATE CatHi2dO4 G40) Analytical Artifacts 0 BENZYL ISOAMYL PHTHALATE ce oon erence, 00cKps (CAS: 1 2-Bamenedtbsyi 3 ety phenyl er 7270-46 ‘An purty detected i bey ty pase by Nove: and Novas 197. See aba: Bexev. sureLMeTALATE CaeHi2204 826) BENZYL ISOBUTYL PHTHALATE co.cenenen, Cron (CAS: 12 tenet: ai 2ety rogy ey eter (7270-4. ‘An ipa eee in benzyl by Nowe and Now (197) See aio: BEML MU. ALTE CrsHi294 G12) N-BENZYLPHTHALIMIDE, Ch cine cn npr 10014 ‘An purty deserted in bey type by Nowe ed Nenad (1579. See aie: BENZYL BUTYL TALE CastuiNO2 @37) eeuoreeaMiddlediich BICYCLOHEXYL CiaHar (166) AnalyicalArifacts ” Mas pce: NBS 180 66,1762 176,164 ‘A isptatere ner asp) as en egret a conan a Anesats ‘Selves Gan ng, 9) See ct: ANDERSON XE0 BIOLOGICAL VARIABILITY = bent BOS O-O eylaber 1192511 Mass specu: NBS 79, Als 1080, 1051, Mieco West 979" Cytoheryeytobexne, Dielaenyt ‘An imporityercouriered in “silent” grade yeohenne, This impurity my ‘paren ents fenrnmeral ares since cores Wi Wedeeane co OSS ps cuca oes idle nd Wes. 173) cast See eso: CYCLOHEXANE BILE ACIDS aie wee si ieee eae nate em Sots heme cae gether see he bree oemmnccr atone Seale ca au samc enoe Ee a BINAPHTHALENE CapHis (54) ‘CAS. 1,1 binaphaene (6043-5), 1.2-bioaphsene (4525-76-02: arhinlene feta Toten wonder how lnm eve anv mening cones rome te of esomemerstha hey ptr ce bay fe Deeg bechemscal shoal ‘Ss among mice lan ved tein which have en aed onc homopeneus Se! wer ‘cycled contre perpen ifiea. Da what set pop” Oly ‘recy whee nthe pes alt vn no pe re Seinen fr sn cengeial eae eds Yrg (Uh camped teisaningreview oldie pring ths ce BIPHENYL, Cialis ast) [se 50 160 150 Pen (AS19252 ern 305 ast specrom: NBS 418, Alas 7,928" ttn intr: 1389 (Racy a, 166), (Hee and Mori, 562) ‘enzne, phen Lenenere, Pear X, Phere erent port agaconamint in Anbee XAD 2s KAD eins cera 69 ie orognct ic opal 3 pon Auorape we tcomsnnan iw nese NES (tia ay 5B Ht nd Pra, 198)2 Midtedueh Ben! was encutered ance eles cep y bean uncondiined Pop (Ql tenm Ge a aavemn of snge (Las nd Walls, igh ised as angina x cu dt nao it pled oe cg ‘REDS Saye stannic See ali AMBERLITE XAD2, AMOEALITE XAD-4, AnHERSORE XE-SH0, LUNAR ‘Shu, RocaPa OxbAOw TENA ARTOACTS o-BIPHENYLAMINE, Crotty N (169) res _ oxi encour tconcanaaons sb 25 32 pp in commercial cen ee (fetal 7, Seco: DENMAN Analytical Arifacts n HENYLAMINE CrttN (69) [es etl a 50 160 150 O., CAS: 1.1 -Biheny-aie(2-67-] Mercedes 123 as spcur: NBS 4272" ‘Aminaiphny,p Aiotiptenl & Anipdigtny. pAninedptey, Biphe Soke Ratinnuliflent Pena Rea me ” ‘Ao purty neue concerns gh 855 pin cornea pay Amine repute (Sulece ay 1 Mean : Steal: DeHESLAMI BIS(4-BENZOYL-S-HYDROXY.2-METHOXY- ‘PHENYL)METHANE CapHtasO¢ (468) a, rites by mas secon a6 m seve shea adv ext fom a bp cpa cospestan See fom4 Middleditch eS BIS[2-(2-BUTOXYETHOXY)ETHYL] "ADIPATE. CatieaOs (434) ere aOR LO YooKYeH,0.0%1eHy.cODeKCH,oOLCHOOYCH ON, CAS: Henares a i2-@-brrstbonye eer [141-173] Retction index: 255 Rams 18) Buoxyehonety ape, aorta ite A latices Ranaey ta, 1980, ee BIS@2-BUTOXYETHYL) PHTHALATE, Crlts006 (366) x LF wo ae eae coe oa poyoE4 (CAS: 1 2Denzeietoyi si s?-btnyety ese (117835) Mass sperm NBS 2856+ Reseion inden: 2850 Ramey el, 980) Abi rfc * Bec poe ens Melos Sa Dt aa oe het A lastizer Ramsey eta 198, i 1S(2-BUTOXYETHYL) SEBACATE CaaHtea0¢ (402) CHe(CHesoH0CH-CH,0.0C(0H4)00 0CH,CH_OCHACH CH, AS Da ai, icy er) eee: 270 (Ramey, 1980) Raoetytehcae (bane ta Asie Ramsey ea, 1980, ee 'S(2,3-DIBROMOPROPYL) PHOSPHATE. C_H;,Brq0aP (494) (Che cH6%0H,0),P0.08 AS: 1-Ropancl, 23 iene, yd pape 542259) 2S bien opeteng op i ape edn is Per ein chi’ Seep abo ES Fe tS ear a acre re See ato srenannse Ts. BIS@-ETHOXYETHYL) ADIPATE Cratta6¢ 290) (CHsCHeOCH_CtH,0.00,0H,),CO.OCH,CHZOCH,CH ‘CAS: Henaesioi ai, is(athonyey eter 108-444} Retain inde: 1880 Rasy al, 1980), 124 (Aste el, 1985) Piedoxreeyp atte, oxy ade76 Middtedicch A plsicerRansey cal, 1960, . BIS(-ETHOXYETHYL) PHTHALATE coe eoceyayoa4e, (CAS: 12-emeneicoryic a, bf? hoe ese 9) Rexoron ine: 215 Ramsey ea 1960, 2103 ey et 1855) Dieter pee, Boney pba plaice (Ramsey ea, 1980, Cretta20¢ (10) BIS(2-ETHOXYETHYL) SEBACATE Crate ¢ 846) (GHsCH,0CHCH.0.00(CH,),00.0CH,CH,0CHLCH, (CAS: Deen i, Hs?eexyey ee 24102, Reunion inde: 2270 Rare ea, 580) Dieta shes, Phosyetylsetoewe A plaice Ramsey, 1580, ——— BIS@-ETHYLHEXYL) ADIPATE Ca2Hla204 (370) ———evecred» a 57 129 so 100 150 Analytical Arete ” 4 370 ae 250 so 350 Pale sCH4CHsCHLCH.D.OC(CHs,CO.CCHLOHCHCHy Csr AS: ennai mi a yey e823. sc NSS, peer Spe (57) trond 281 Ramey a, 190) ‘Ait 2EH. ix? hy ben hexane sid, Bisoiex DOA D2 een DOR Menoer DOA NET ESS ter DOA ee POM st ‘pie as nd Cie 1985), Peo owl he) fw! wrong in aia 135-15°C for 9 mes has Somat trae ea ape tt encountered ace ccs of aos wage cg al an Marvel ea (973) eponed that bey easy ree ee en vind he cap of cen: tots vie ene at gee CT sa Me creme 5 a NHR eh OT ot BIS@-ETHYLHEXYL) ISOPHTHALATE coches angensien mo (CAS: 13-Bermneetort a BA eyeny exer 197.993) Rano ince: 2790 (Ramsey, 1560) Pi2 thers inpehae, Dicey ope, DOM Aplaiiner Ray ta, 1960, Caalts504 090)8 Middtedtch BIS(2-ETHYLHEXYL) PHTHALATE Co4Htye4 (390) has 167 oly so 100 150 278 7 f 200 250 300 350 300 400 430 500 350 pes co en OOOO, na (CAS: 12 Bereneticaexye al Bs? Besy eter 1171.7) Merk aden 1248 Mass sperm: NBS SOS, Safe and Hating (173), Sp Matick ea (981) Reser ince: 2507 amay a, 860) tod Spier 1975). Analytical Arifecss 9 Be styber | 2beneicunr lat, ifthe) 12 benzene eso Bel i Cond SS Sede ae ans Dibefocol pinay bor, Eoyhesiansices Eotbent tomes hae Fite seiner OOF throer 68 fatter DOR: RI CSET teeta lb antoo Alt Pc su icy ees Pacis PIS, Sed Sa Tres DO, Vee i Wea 1S Abigale, ln employe in vac pr ci Skane and Cosy (1990 pod th ever contacted soles of US or Ge ce equated bce ac nl ben os a pale “Te solvens nr or dened tert wa aed a dose aaah {San ctu of glam bss appl otenve te palace Hower TOO Shieh nc et enya ple Pe tray ae ‘gotlening Ser Inee, he Gail tae of sling of hese ted ples ws ‘Eiemiee ote 23 oes et ap cd net a 7 fe Seep att car te pice ina a iy omen EE sec enact eh ane BGonr Ofte hc ate yca Set evog ata carom aanetotes fre Eee RUC haie ts er reae eeeen Sco sire races SSaahSecrmanre ia gs emia rig nt cei ye Sos ie aeuesee tis tuemmnent ater enn raat yen = Sorbent etc n iaeing EE one acme oe tock aa ‘Te poy (ay cnet) fom Ree 2 rom hie eo st made has bee opened to covtin beni pane (ces Macy 7). Wee od ce (9) ‘gedit hate acs te Hd temp) ag Sores ark Pent alr oe rr eb ply vinci) tgs ay ten SIE OS me petay eben eo eke ee ood or srial Fate ong raninkn of iodo pane ones (Anonyoous 197 Ching ta Tob Inswerusslutons tne her fd conto sey ble a is Ip pro Sab Tea incre Fabben hyn pine aby ae pa Be coven persue of hen aaa elie yt dee ‘cm onan tom be lrisen cone eee guna Manes0 Middledich allectd ty be Apa 12 strats 31 months afer th Sorveye ling and even ‘euenad expose te ears of te Lara sas oas sufi crgae ‘Sle epic (Gost Clary, 197). “ey repos of chemi Fae non det By ben) [tale ep dependnt pen he solvent ployee mage stan {Einjte! in bine: Nehanol sous have sored pea ony 2 Soe be ‘Sue Gined wheat dslie was employed Peo nal Pad, “Te aia anatomic agent cspyramide coches wits i 2cthythey) pba (Ea ps cemaoprahy ov SEC, tos ust be keto eve ‘oan wie ater sch ge dene fom pase Hood tgs (Dube ism, Bis@-ety then pane x meabolnd to Zethylheylhyoge pala by fsb (Genin a 9 ‘Seg alm: Buon couLEcToN DEVICES, CONTAMINATED HEAGESTS, DAZOMETHANE, Bioctre nmacete Eniawot, MEnOeNtan- Lol, RENTAL HYDROGEN Paar Exo 000 CavTabass, FER PAPER CONTAMDANTS LUNAR Shatruts,ButHALATE Rahs, PRIMALIC ACID, SODIUM CHLOMDE, SOXBLET ‘Pans, PIS@-ETHYLHEXYL) SEBACATE Cane 426) ras » We lta. ” 100 we ao wo avo =o Analytical Ariacte sr 0 ao eae ae can orenaono ccm coceH CHO CHAD css eatin ‘ent serena At a9 sew yh in igntgean ans tealerer mazes Pte erin ps Sc eee ee po evagrain compre (2p fe orm. The ceraminart was ot peat ‘read certo uate al 1970, See aos Cen 1 1S(4-ETHYLPHENYL)ETHANE, CisHta2 @38) WAT TL, epoed asa cant in Amtrie XAD2 en a cece 026 pat Fg, me Sect: AMRERLTENAD28 Middle BIS(2. METHOXYETHYL) PHTHALATE oe ‘co ocyenoe%, (CAS: 12-Benzeedicaoxfi ai bis-nehcajey/) ser 17-25] Rexaion dex: 1940 (Ramsey ta 1980) Dintoxyey pale ‘Aplascizer (Rasey ec, 180). Crattys6 (282) BIS(METHYLTHIO)ETHANE CaltyoS2 (12) Ter 122 ttf 50 160 150 (ChySCHeCHASCHs CCAS: Ethane 12-bit) [658-18 81 as specram: NBS AS, Ais 98° 12. Bimethyimerepoytane Eeregten nine ior hued ee of aes (aie See al: CEO, BIS(METHYLTHIO)METHANE CHySp (108) CchySCH2SCHs Analytical Arete 8 CAS: Meare, bey in) 1618-264) er aden 1253 Biinethyimercy)etne, Meyneirethysie) Fmd when tbe insect hitnox ished nthe pres f sans sel Cares {182} Th compoard eprbeforthe chars or fe hie le Jeu iahghcrcortnn veers ar eal pepe usa See aio: NOON BIS(METHYLTHIO)METHYL tert-BUTYL KETONE CoHg082 (192), (CtisS)-cHCO.C(CHals (CAS: 2Baanone 3 .imety1 sme 139195250) 33. Dimey metho? ane Farmed ten escent Coie Sean Racea BISOFLEX 1001 ‘iii eps ich afr mip eats oe cmap any BIS(S.S-TRIMETHYLHEXYL) PHTHALATE. CyeHq20q (418) cc SOLEMN RIE), ‘coceeHenyE eI, (AS: 12.Benonibon ic mi 3,5 imehyexy eae 628-608) Disonenyl pia_ a + idétedtch Fenny ti tg hen cma a far (ate tsd Mock 9 1N,0-BIS(TRIMETHYLSILYL)ACETAMIDE CyHy4NOSip (203) jar 75 ne 100 150 203 200 250 +300 350 (CHSCLOSHCHS)F-NSYCH)s ‘CAS: ani ei, methyl tines eer 1016 50.81 Mas specume NBS 1218" Bsa ca wets eer, ie By einem shear. Crime yea Majer prt n W.0-is ney Daceamice ae Hint ay ctaise FE ee en lage (he) pig go a coi we ‘Smcyinl nd onan rah 172) -Aecanie is ehyobss roa of NO edited Se aloe ACETAMIDE. ACETONITRLE STFA ADDETION PRODUCTS, HEXAMETICA DESK Tena MSL AMOI CTADENNOSLML RCETAMDE Analyical Arifoets a BLENDER CONTAMINANTS ays oe (172 mend he re et 3 Bar mie ‘Spicer wih Teltm pai "hey noted a Tew ens ‘Bais anis ets fohat ofa ber ake. ‘eed verl nes for dea 12 mies each ie else mene ea aes See alee ELON CONTANNANTS BLOOD-ALCOHOL DETERMINATION ‘aii tured ig el dering eam iy cre BLOOD COLLECTION DEVICES Plane sings and ube ae otros sources of plainer and cher comarinans, ‘any of vouch rte wh arlene he lod Many authors refer © bod colle devices by te col of tes stopper. The {eloving clos are enplajed by Besos Dison ret Vacenies tes scctereertae ete cee a ‘Serna a spe bn oper ud co aiane = ‘Seas ser ocr toast eas Soper eeMidiledich rasgyeensass & Slit ape ase pere nmin Yacve Yawn ii 4 i & i ‘a soppersctep these mich ae brown, orangelreen o ellow ate now fe of etyetyh pos “The jr contains amy last Tone Rosser and Bogner (1970 "ene sn pale es Mie and Dickson, Fiat ted cclcace wm a pase ne (eee! an wise eo cleced fom eee ns EN aia pas conan od ced usng ewe ets Gefen tun! pra sd may Site usae be tacdeneae -Aetersisifcct contaminant 2 butonyetiy)phespae (Pay, 1974 Mis ‘SDS ote rand vem, 199) Cer onan which mere ot ee at tere hey were repre ray SSesSSIESaFienonue: Pay ea (197) enced we: wh ha bee ran Rta (oD No ean wen ange cape var acled exacted ah Eiesaen’ Sec eoormpanty oh corcesraed exe afford ode MASE ‘wih nee ‘arya (193) fear at ood cole in Voce tubes consiing gti Bah Gat eae ssa say wh feb metre a, aia nm tsrence ate, Ts mea Anelyticat Anifacts 7 150.3% vy) and mane (50 pen wh, They suggested ht he hydrogen was aby Feel a ee tae octet me a ‘Eel ft snd Wn 00ponbed a pct nar pect of several ut dacs tubes (B-D No. 6432, 6433, “tbs conned Hyde fms 2), vee (10, % oe i 3h mehane ls 10, suspen 29, Sa ie Sane ora Gi 0), peopne ean se fe 50, ad es (Gi S64) Ts ctnarirants nee eeceuntedinaonscore coed Veooest {FobeSU ana" Tate tubes The average hydrogen concentration was 80 FP in ‘acute 13 toe an een 30 pin Vers TOD aes Twas eed Tht vo pics doe fom tescane cong rater aa fom hee by (te abe Uren ea (190) hove ome ut loved soppeed EDTA coming ‘Yocusoe 6476 bes yen 04-10 of een ence, td that te EDTA ‘Shon GL) iy contin a cf exten enone The ext note etre ‘ik Gacrmaten of he ctonytemogit cue Ha. This ober can Be ‘mind ie aes are opened ee od cleo ers aya coin inn wat deccse Yee conan egestas uaa "Pace cormaminane col be eve by wasn wah wae oF epee i rn pc el rn trees ae at Bogie eae eek ceectatay Serre scoped iemntiyrist re tace SSeeicen irom Retina tc saamamenen ata schema ceoncerecen a EGSG SUSE ttitveve ic irs peamagiome tect ofc Basa cceier ieee mage omraas teat pene etaeae ter eat each ae betbeon hs ow rey cna pate om ia Vase he. Petje loo collin devices ae appre zeae for some proces. Pei C1 pred er no rece mh rag aes we {mneatay for andconvas rsx when ep Var el ers tes a employed ‘An agueaus ext of BD serum separatr bes was found t onan at let ten mpoand arnbed by mas spect 85 Citta Cito Ghd Shrine! uo Sido ch sue ito Sato ‘Te comin vo esi ey ge ih te pee ete SESSaoe Steet reweraer tetas SOS GEES CNS och aceakt cancion mao38 * Mideteinch (etnicen report fed conan whic colaes wih mphaqestne on GVET Groen ea 179) See als: ACETYL. TRIBUTYL CRATE, ALLENE, CARBON MONOMIDE, BUTYL FiniaLate, HybRooEN, 7-@ Hvoxos erHviwexcavFojweNzoTmazous, Marna 2 Meriva ert 6 ers BUTYL, PHELALATE ASTIN, PROPANE, PROTED DDD. ica BLUE FLUORESCENCE, Atworinaare fren any by bia ye chromate gay tnd hye comet 8 fe eon ps abun ma fi (ve un th ‘SmgutArperglte porsncus NER 999 au lords tue Fuaresem Spots Wh ss eo of anny weer tn eee ty ‘Eeseey tte a cece aca econyeetyctonymceaperic ‘Sian! Scone An heat slvent sje er Og ‘Retro ins meng wba na geese Ait cn ty Pe (18) en i fm cos eh ta St Retar Uhl Fated i bat of sbi warts oe ‘kre wae. Ts enty went Geerioe, bet mv atenave say bse ope layer irornogrpy was reaped “Ser ios TRRCLAYERHBOMATOCRAPIEY RETEACTS BORON TRIFLUORIDE ETHERATE. C4H1gBF30 (142) (cH0H),08F5 ‘CAS: Born, itor onthe CF) 10968-] Merc en 1336 Baron furs tent, Bree hose ty eer, ay eter oro tere complex ‘Ths eget dens a esa ofa vio, canbe eid oe ccm (Girl ara rown: 19. King and (1977) warn apa the oe of bron ‘Scone bese wane whe ces wand he ode oe co. Begon ifort nderges mn ram rin with fceterl 24.28 poi to els Seo and p-ydony.Saigman Sere (atkavaet 1971 Analyicat Aries 8 BOTTLE CAPS He ocd {he psi dics sed oe ese ae fr be packaging of gh pry ade solvents. ‘Tage were roby mae Teen, pte a do ‘oil was ‘Machete hwo orto aden Th ache wa found ob len at ‘rg sents td append ob mapsabl rrp uy aoa escae ‘Gliroch ts 654 moL) it some barnes of tore. Bode sdsenve and tiene ‘der a ec ong an apa Macarena ‘Se ol RESIS AC, SLICA GEL CONTAMNANTS, SQUALENE, TERN, TOLUENE BROMINATED DIBENZOFURANS 6 tiydvony 245.245 Rexawercipheny ecomposes drag gs cromatgrapty on STONE clea n tibiae w sted to easier: Wh Son ‘Sggesee that enon sols be exereed woanevertrorinaed erature Se ened cing ata (Gare ea, 177. See lo: 6VERONY-24.5.2 45 HEXABROMOBIIEN BROMODICHLOROMETHANE. CHBeCI, (162) a 4, 4 127 4162) 30 100 150 Heel, CCAS: Mebure,bomodktlo. (1527-41 Mas psu: NBS 626, A 1026, nica ta (196) Dichertramarsahre he presence of sin eli in ore ater an ed 9 he a ‘loth sch av homeowner x elo, tor aadidéleditch Bo Mi F xomocioreetne dung sarge, the malyiscnns be conte rom Bi ae te te wry macs wath arene eh tio mon (ase nd tee, 197) cus chaive slain tough sar acre carbon ae Gey co 180 ‘See aso: CARMEN TETRACHLORIDE, CHARCOAL, CHLORINE, CHLOROFORM. DEROMO™ Sieenemune ‘passage of concerted foes boos Analytical Artifacts a BUTANONE. C40 (72) as BSTFA ADDITION PRODUCTS 1973) pone eto fH 0-etuinetiyspisturoaceanie (41% ai re a nd rene fr oe Put flo 8 ae tata ceama ce iruiserone ae imir cecsauneo peta, oes ta le raat Ape Stfbe mei Sm tee San nounanmsoname Chig(CHa}o8(OH}2 came) vane tien veers torent ett ene” eam mnemonics so 100 150 H00.0H,CHs AS.2-Buanne (785331 ec ne 5845 ‘as Speco: NS 39, as 66,65, 70,71,73, Sper at pee(1975) uan.2ene, ay met eo, eco, MEK, Mey aoe, Maye Are Feondin ined psi yctagin ty Eloman nd Kase (1980 ‘Acetoe which had ben manufactured fom cumere was found to contain 2-btnone (iaikowstat a 9Tea ‘Anes (1$70) repo aa supe bray rate 2-bamnne cored 139.6 mg SRR He nate he tre oes en e Set ln: ACETONE, CHOLESTEREL, LAMINATED PASTICFOOD PACKAGING BUTENES Cally (56) an Whkins (19853) opened at tenes wer peat in scone canted Vou tod ead aecgeal ter * See lie: BLoob COLLECTION DEVICES 2Q-BUTOXYETHOXY)ETHYL ACETATE — CygHz904 (204) (CHj00.0CHgCH/OCH_CHOCHCH) Cty (CAS: Bang, 2-2 twonjetboxy) eee 1247-4)2 Middtedich Boylextint sre : Deed int aside (Sse, 1981), This stance was rnd bend top ao he sae was tert htt or re Sweaty? pro 2.RUTOXYETHYL OLEATE Cagttag03 382) CCH(CH,Y/CHACHICHCO.0CHCH_OCHAICH,).CHs (CAS: 9.onateemoic ad 2,2 gore ese 100.397) plaice which tors mite ps hostage peaks Rams ea, 180) N-BUTYLACETAMIDE CéHhyyNO (115) Bo Ss 2 ns 30 100 150 (CHSCONHCHICHOHs (CAS: Acti, tay 1119.8.9) Mas specu: NBS 457" Repo asa minr impurity incl (Carvin et a, 181) Ser alos CIROLACTAM Analytical Arifocts 98 BUTYL ALCOHOL CaHt190 74) BT 55 14 50 100 150 OhisOHehacHOH (CAS; 1 Buel (71.363), Mer nde: 1513 Mas spect: NBS 23, As 2 85, 8, Speer an Spier (1973) Butea, CCS 203, 1 Hydrate, Mellon, Propylene ‘A imgry dete obey pale by Novant Nowak C1979) Mass secwu of ay ele methyl ee (Hy OSi 46), NBS 15) rs ra jy 41 46 30 100 150a Midatedtch Anlyicel Aric 95 secBUTYL ALCOHOL Calti90 78) fereBUTYL ALCOHOL Cata90 (74) as is 31 wl yee Ly ol ca so 100 150 so 100 150 CH,CHCHONIOH (cri)4cOH (cas: 2 tan 789221 CAS:2 ropa 2 net 15-650) Merk In: 114 Merk nex 1515 ‘Mas spectra: NBS 23, Aa, 5,87, Stele and Spee (1973) “eBury alcool, Buyer hate, OCS 301, Edy ety bio, 2 Hyco, Set cdptextinel SA “aot bas ten found it conection of 051% in reagent rade whores Giese eta, 1°71. Mass specram e-bay hol ety eer C308 (6), NBS 415° 7: Slias iz, a3 ill | 14s 30 100 v0 Set at THONROEHUDE ‘Mass spectrum: NES 3986, Ate 83, 84,25, 86%, Spill ad Spiele (1975) er Butapo, Baal Balter, 1.1-Dintylednc, 2 Meth ropa ‘Siocon peeaeel ™ men Reported stables in 7 of 22 samples of etna grade 11.)-vihlroetane amepeb faetere witmes e aeaee en tere Bury alechol is formed wen te irsecse hos is ested in the presence of ‘ties sel Cans ra 19D. Mass specu of et tty sol ety tes Ith (146), NBS 433": 7scs 5 Middleditch Analytical Artifacts 7 BUTYLAMINE, CaltiN 13) BUTYLATED HYDROXYANISOLE CuH 1602 (180) BS re 7 Pago = a ey » 100 ms = 100 1 CHg{CHaCHNHg 8: nai O79) on Meter t6 Mas specu: NBS 3985, Alas 77 Retin inex 909 (Arye, 1985) Amine Mono teaming, Nene Rezrted aint impurity inept (Cais et 181. se pecmum of methyl derrtve of tuyanie [CS (8 NBS 384) ae 87 50 100 150 Se line CAROLACTAM CAS: Phenol (L,-imeetiy} 4 mary (250165) Merck ner: 1520 Mass specu: NBS, Alas 1230, Kosta (1581) Rexeion nde: 162 (Rasy ea, 1980) _utaecioe 12, BIA. .-Disetlety)-netonytena, bar, partion LF ‘Aa aint mise oferty mehorypteol an er bay -+etoxyphenak Buylaed nero avon the expiroscomgnens of he hora yoikie daewsaa bm “7 [oS errors recom Sesion lan ind 23 abaya £-metenyipeny cb ‘See also: AXRLARY VOLATILES, 22° DINYDRONY-S5-DMETHOXY-3,3-Dbtert BUD, 73 Dier SUTY WORORY £3 ONMETNENEIEO ETERMiddteduch BUTYLATED HYDROXYTOLUENE CisHae0 220) eee oo J %0 100 150 J [205 220 200 0 30 x0 One. Qe tH), CAS: Phenol 2-i-netylety) 4nd (128-570) Merk nde: 1521 as pct: NBS 45, As 1553 1564, Spacers een index: 1690 (Ray 21850) “Asuancioe 8, BIT, Bi | inet -+-netyiptenl, Bay rorlane, SE ai Bite! Sma ae Oetorney bp ewok 6 eer ay SA et teres 33 beer b-eoyrayre, BEDI merece Draes higlp menyyiech, rapa ool, oat CP. cere ep riieel NCCE Ferber, Psex , Susee Seine SME Pon eeu BT Tope 0 Vs nits aint. Used a a serie io Burk a Jackson “ise nl tig 5 aang a ences ch may bea Bgh 250 Teyeratran Renita see roy cae ara uniber e floing pois 3 ae T cyanviyl tea, eelohenere (OU), deb] eer oreenedin Fable fann (6.009%), Zedge! (90 ppm, medley betyosctene ple and Spite (1973 Ende Analytical Artfact 9 (apaamamnacten sys 10) mere usabirensirop ae ut rama cee pagans spb ccancend hs eacoiaeta eayteaer pe ace nuncio ece yams 97H an accom fOr pps Remberea08 71) ‘yen Ha et (197) fund yee tyrone song be vies oft Wipe ahte! Wongawoussanaer monic et hyenas ms rptio te psa aaman snaty Ward tl 96) BobyRosscces Goa = PryedRndonrolee i ong te expen component of he aan iy Fea aewseras 7. Sunk et a (174) fund buy hye in water which ad psd ho Ba ten ett a sued a compan ws sabi sed eppecracing omarion “Te analy of pheno nonin in rutin sb Da Ager chro ‘BhaedSpecrncopy was evloed by Aes (970. He encountered mefowce fom riesgo Sw dor pa ‘Sued to ave os problems A saslactery rota Was Filogteene See alr: ACETONITRILE, AXILLARY VOLATILES, CHLOROFORM, CYCLOMEKENE, Better uve Quon Mette, Distr. en, PLTER PAPER CONTAN: Nass Sava, TettonyoROrURAN eeie were Tov tenyed BUTYLATION ARTIFACTS (Cacao and Kogan (197) have repos ta tra soul be sd for ‘fe brla of ein a reve eve the fomaton of extaneus ps CNOA rates sed tuned ofan te emg of Somat Fo ret catey maker scatee TE chao be Type wi Eile bling HC suo resced be exraneas pea tbe bana HET Bk100 = Miditeitch BUTYL BENZOATE Cunt? (178) 23 178 50 100 150 PHO.OCHICH) CHa (CAS: Bran yee 1136-60-71 Mere nde 1525 Mas specu: NS 4513, As 1207 Aa putty dts in bey bay pha by ove and Novsaon (1979). See ao: BuoevL BUTYL LALA BUTYL BUTYRATE CyHty602 (144) se [Tl a 4s 14a so 100 150 (CHycH_CH4CO.OCHA( CHC (CAS: Bota ac yee (108.21-7), Mas spectrum: NBS 394, Aas 79, 80 nBuytniuenode, Bayt tute Septoria pene raf cot on Fe Sei (Roe al 1981). = ome Analytical Artifacts wor Serle Crexenxane pelert-BUTYLCATECHOL C19He0g (166 50 100 150 mse (CAS:1 2 Benne (1, cimedyety 98.2931 ‘yar uae er Bayete pr Babin Diey Mas spexram: NBS 69, Aas 108, 186+ Used by Alch Chemical Ca anni ine flowing products: Sty iene 2. nottortene,4tatrostycene, gopren (100 pen), mets leelpeniatene dimer {Gi pr, acretytsyrne (18 pp). styrene 0" ppc), tay ethos Gop ed Pnaplpyine (UIE) Qadiani EN See lo: SOREN, e:METIV STYRENE, STYRENE tert BUTYL CHLOROACETATE CgHxC102 (150) cic,co.00(cH), CCAS: Acti ch choo, 1 dete ese 107.59-5) Merck nde 1536 (Cros cl erty ete, Crone i 1d tyeser one ah. 197) funder ay orate in wer which ha psd ews etn i They nea ep hyo sat102 Middledich ter BUTYLDIMETHYLSILYL ESTER HYDROLYSIS “amet produce he erty devs of arbor acs wig nent es rapa kw we rs nia we us oitd vats e ees riven ‘trol sin as SET eating ade Pecase ofa ay of he kaze Le ee ttre fom the eoosoe. Ths problem vas coy Sem ene gy asng ryaine x her acd savenges, owen, eae: Fequeboarh yt Cor nin enact Fe ep mana and were sae frre han a wee fer extaion #0 ‘Erin ately 1989). BUTYL EPOXYSTEARATE Ca2H4203 (54) ay eye, omen yeneo ceo, CAS: Ocean ony tes [1068521 ayl 9, 0eponyoctidecarote, Buy 9 10- Midateiuch Avalyica rifts 10s 7 BUTYL ISOBUTYL PHTHALATE Cietiz204 278) B00 eH, ] (236) 20 250 300 350 yen, Sei: DUTY. REALATE,LQUD PETOLATM {tert BUTYL HYDROPEROXIDE C4Hl002 90) (cttygc008 (CAS: ySpeed, dimethyl (1581-2) ee nde 1543 Cine TBH, 1 Dineiyetytdoperite Sg by Asics hes ie com von Mec nd Za tert BUTYLHYDROQUINONE CroHa02 (166) (AS: Bemanetel, 241 imei 1968.33.01 244-4 tenet, TBHQ Used by Ach Chesca Co, an iti in lb... 2.44(1M SHS ‘ne GO pp lech ad Zt 1987). icant ers all Foerster ote ‘Se Eat co hn rng. ea (CAS: 12 Benmredicboxye at buy 2-medylpopylese[TII-S-5 A placer eset Esha eam Eade 198, ‘See ls EXTRACTO COUMRCONTAREUNTS BUTYL ISODECYL PHTHALATE Oe. a ees ewan inden: 1950 Raney, 1980) ‘Alas Raraey a, 198). CanHs104 (362) fer-BUTYL METHYL SULFIDE c ; Css (104) a 104 50 100 150 (C¥a)90SCHy (CAS: Pope, 22 (ney) (6163640)F108 Midaledich 2 Mey onahytniogonsce epee he ce tor hui eps nen Cats See aio: HaoeANOX oo ter BUTYL, METHYLTHIOMETHYL KETONE, ‘er BUTYLOXIME (CunHsNOS (217) aomeee (CHg)s0(CH2SCH)-NOO(CHa)s CCAS.2-Buanone 33-dimeg {met ti) 0(1.- (221) eee NaS) (CtiahsC(CHeSCHy)-NOCH,SCHy (CAS:2 Baanone, 33th ney), meyer (67? 60-7) 33 imate) 2uanoe 0 netyomedryoxine Fomed wen he nsec tofnos shee inthe presence of wiles ste (Cras eras). Seon: TEAK tert: BUTYL METHYLTHIOMETHYL KETONE ‘OXIME CyHysNOS (161) ee (Cts (CH2SCH)-NOH CAS: 2-Dasone, 33nd (mebyhi)oxie 8195825 3.Dimety metic) barn oxine Foret ten dees fos tee te pct sane te Cl See alo OEANOX BUTYL OCTYL FUMARATE Creti2g4 284) ‘CHy(CHCH0.00.CH-CHCO.OCHACH,},CHy CCAS: 2-Buendii aC), by oy eer 6530-453, ‘Assy plaice epored a a consent of war which ad owed ro oben esata.) * BUTYL OLEATE CaaHta202 (538) CCHy(CH,);CHACHICH,J6CH,CO OCHHA(CHCHMiddtedich (CAS: 9-Osndeceni el, bane 102-77-81 : ‘pin we atc site nsdn commer ase, BUTYL-PBD CraHl2N20 (354) cou CCAS, 13,4-Oxadigoe, 2(1,1-bphengl--y5-6-(0.-Simethyethyphen AS ae phen vey Reteton index 3342 (Rasy ea 1960) 2G-ipente seer [einen ‘A scintlation eget which maybe encourtere rng ss ehorogrphic sales Geaary a erg) 1 onal 211.1 -Biphr ats ptert-BUTYLPHENOL, CxoHt140 (150) iss 3 107 e 50 160 150 cron, Anca Arcs 109 CAS: Pel (1 -SinetebyD- B84} Meck er 157 ase spesmome NBS 458° er bays, Buen, (1. Dit etyebeoo Hytrany er bey benene a sip a ws ia ped Seg ck {Sb ei en Seog sar ie mo oe cf ety eile of pier (Cuth0 (160, NaS 67, ss ean te pser-baylana (ied (14) co 164 so 100 150 4-tert BUTYLPHENYL SALICYLATE t. (CAS: Bene ai, 2x, (1. ty pbenyese [7.18 3) Merkin: 1588 drei aie (ity by pees, Saye ae perry Cr7Hig03 270) Aliph sbsrber ui foad wrapigs iy nwa how (<0.1).FP io Muttich N-BUTYLPHTHALIMIDE Crm con nes dont ‘An impurity detected in bes bul pala by Nor and Neves (1979) See obo: BENE BUTYL ATHALATE Cy2H13NO> (203) BUTYLPHTHALYL BUTYL GLYCOLATE —CygH2,0¢ (336) vs ee | oa oe CHE, cosayenen, (CAS: 12-Derenictonyi ni, boxy 2-oey tty exer 1570-1 ‘Mas spectrin: NES 2619" osteo x eg a i jk eee ‘Analytical Artifacts mw ‘Alain ict may migrate from pacaging msi io fot (io and Bhar. SENSE Hue a 8) entemesea tpt tay pole ng he nays ple aps Seed ho was cea ‘Buy! buy jena has ten cpcuree in poling Hie bing in Paelonepprans isresbolaed wo gcolypnalae Oseger nt Rui, 1970. See alin LYCOLYLPETHALATE , BUTYL STEARATE CaaHge02 G40) Bo Sue Se a so 100 150 257 340 200 20 300 ‘350 (CHis(C) gC Hg CO.OCHaI OHCs CAS: Onatenne bay ese [12395-] Mera 1862 as ectom: NBS 4951, Alas 1972, 1914 Rees ines 157, 2362 (Rasy a, 1980) Reyteratecnose Api ih ar eas ning sconce a12 + Midteitch BUTYRIC ACID Caie02 8) [so % | 20 so 100 150 (CHyCH,CH,CO OH (cas: Bae ai [10752-4) Mec ae 1565 Mas pect: NS 4, As 156, 161, 162" Reto ine: 1309 Ae a, 1985) usc i Bure, Eyl ci opancartonybe a Prey ait ac ett pers catia rt re ya ey Mas secu fet hay (CO (102), NBS 9, Alas 272, 2774 [= 14 2 Lb a toe a w00 150 tgs of OS (ONS rs | 145, a (160) A 100 0 c CAFFEINE CaltyN402 154) 67 109 4] 30 100 150 e Oy (CAS: Paine 26 ine 3.7 yo 1.3.7 ety 198.0821 Mer ae 1605 as specu: S491, Ai 13 Rew de: 110 (Ady 1,195) Coie, 37-Daye 13,7 ined surge 246 ore, Goin, Sl NOB Tho Th 17 Fy 26 nope 1 meetin: ‘Analnos igus consti ob and rb since iti pect a ys inks, ‘Salado andes A utero rrpesrpen as ek ean calc See ato Tazo CALCIUM CARBONATE CCa0 (100) caC03, Middledsch (CAS: Cwteic acl [471-311 Merk ade: 1628 ‘Aront, Aptone, Argue, Clee, lal, El wie, exons, Litopable Jeon tS ferised ance, ae, ae, Whig, ‘sed by Aldich Chemical Cot sabe abl cloreormae and 4-mahonynzyt ‘hn (Milde Zs, 19. a CALCIUM LEVULINATE CyaHy4Ca0g 270) ————————IE (cHj00.0H,C,00 01-08 CCAS: emai um i 59-6401 Merk 165 Leni sams ¢ Oxopeni sda a “he ie of tins to wh clin ena a en aise sins eine Bust dhpaety easton ee sures wee wo sae Fe ee rete ae tydrnyre so tectve, oP Fema tha ico) Kem ca, 97 ee CAMBENDAZOLE, CyaHty4N4O28 (02) VT 50 100 150 Analytical Artifacts dS aie [a8 302 T | 200 250 300 350" coc, ‘CAS: Came acid (2a tenia. methyl ester fern S03) mm mh Venta Mek ne: 1708 Mass spectrom: NBS 26+ ela Roveam Canbene, Cane, ie, eopnscaronaniathbend- Mae" Rajoposcctontsaco’ larhentmnzs, nop 26a oly S-berinsdzokenearae MISS, Novzae, Novibe, 2. Pao} Reni eappy coer [2-6 Tiss) i brad Slam asker i Feiler ecer CAMPESTATRIENE CagHtag (380) 2A Nedykesaene eponed asa consist of fhe Snorer wasnt specif Le Sivetmranon Remterg ea, See ls FLTERPAFER CERTAMIRANTS6 ~ Midatedich 2-CAMPESTENE CagHlag (384) joe 50 100 150 1s 350 200 250 300 350 sea 400 450 ‘500 ‘S50 (CAS: Enon. 2 ene 5 (5938124) 4Matyt:2tcenene Mas specie Fagan ea (178) Fagan eta (1970 eciet canpetne pd steep nn yi. They ‘SEER S ie npn we oc pond sepia fe corepneg Anabyical Arefacs 7 ser es vag tox hey were poly fond by sila Pocasticagc afccae oftempwaee” = NY Somat See ab: 2-Sr0sTIME CAMPHOR CreHi60 152) a p08 6 152 ‘90 100 150 costing 8 van vee A tei eet go 85 deers pee ear ee ‘agrees eee sees one sce enna Any, i oa pet tity vous Midatedich Analytical Artfcts 19 CAPRIC ACID CyoH2903 (172) a { at 1 280 250 300 350 oy 129 wl bu a al | ‘7 30 See aio: PNET ACD 100 150 ChiylcraycHsC0.08 CAPROAMIDE, CgttysNO (115) CAS: Deano nid 3485 = Merck Index 1735 Mase sperm: NS 27, Als 153 Dect aid Daca Neos 10, Nacsa ait 4 La us gression ak coc Spom | Be eo wo as speci of met cpr CMO, (189), NBS 240, Aas 123,126, 12864; | CHCHSCH-CO.NH, = (As: Heit (08-04) Messen NBS 162" 8 ajc inca (Cnvin e181) ah | L ‘6 Sea: CARELACTAM 0 100 0 1 as pec wim ef arc C031 2), NBS 161" {] cAPRotc Aci Caity203 (116) Ta a | % tls | og 50 100 150mw 120 Midietich CHiy(CHaCH,CO.OH (CAS: Hesaoie ai [142-621 “ Merck ade 1734 Mas spectra NS 168, As 23,428" ‘Revation inex: 28, 199A a 1585) Balt a, Cronies Hex aR a, ‘Severe species of cera characters of winry wat infections pra cape at ‘Girseneeal 979) ree of mat expe LOH, NES TAs $9, 56, 55, 7 8 2 4 30 50 100 150 Nas specu funy eserofcapoiaci (HO (18), NBS O16" is n| 173 wl. Le 50 100 150 ‘Analytical Artifacts ‘“ ‘CAPROIC ALDEHYDE CeH1120 (100) [#55 Li 100 50 100 150 (ry(cHayoH-CHO (CAS: Heal 1662511 Meh ae 785 Mas geo: NBS 4007, Alas 255,256,257 Coponeye, opealeye, Capri, Hexaihy, Hexaal Sreagtizten eT cs ene og pci ‘Soci presi ees aang asf ein of yt acted wih ler Ms specu of -metyonie fcepee ah (12, NBS 259°: ie Lda ae 50 100 150Ei ute Analytical Arifacts Bs (CAPROLACTAM, CeHiniNO (113) CAPRYLIC ACID Cgltye02 (148) 5s 3 eo 30) a 84 1 . 4 4 144 50 100 150 50 100 150 rors, (Hai CHe)soH-C0.08 how caster) Merck oder 1739 (CAS: 24 Anepin-2one, exer (105-602) Merck nde 1736 Mass specours NBS 145% “Aminocaproic neti, 6-Aminchexanoic aid lactam, 6-Caprolaciam, e-Caprolactar, SrCaprclenm, Cyclohexanone bookie, Hex repn2 ne, Hest BoC cam, PReohexamedyieremine, NCLCSDnG, Onshore Majo impure ical hae ben pod asi, xeoamide tae Maker ages op ie cane pie ce aoe era ceca tuple, cycerenyanine athe ienebay amDe, ‘Eiepi an ccytopbnmne (oars a, 181). ‘Se lt: ADIPMIDE, ANON V-BUTYLACETAMIDE, BUTYLAMINE, CAPROAMIDE, Salita Greuoniskv save, N-CVCLONEXYLIDENEDUTYEAMINE, 1O- eetape Ieovatenababe, 6 METH S-VALEMOLACTAM, OCTARYOROPTEN- ‘xan, Vata as specu NBS 36, As TH? Hienecatooiic atl, Neo Pe 0, Os sei Onici Oye epret sacnmmina nih aii erent ah 2 25 pr sagem MoS agree of et ai ts 8, NES A, A 99, 0 ~ ® dat L198 SO qe neon 101 AS 50 100 150‘Analyilal Artifacts 2s Arey Ox 8 th be Meng Nc Se Cae reece mere Tice cameras aaa x sae ees ae seas ‘ =e aitaieBCtschroactyina) toyeheene 1 ccatonae NT Sis ae ra Va ptegain eaten ecto gw 700 we we 0 sect: Paseneee SOeTaT Tana EE (CARBARYL Cy2HyyNO2 (201) CAPTAN, CyHfgClyn0,S 299) aa 79 Ws “~ \ Bs Hy wo ., 1-1 ° wo 1m 7 soo 20 we 3 se 200 250 300 350 * sec, CAS: i ecindole-1 (2H) Alone, 3.47.Ptetytr-2{(iclormehyehiol- fis} Mera: 745 Mas specs NBS 812° eteton nex: 200 (Thmpon ea, 17: Ramey 1960) (CAS: 1a eterna (6325-2) Merkle: 1766 Mas specu: NBS 1183*| Rexaton inden: 1490 (Anya 985) 2ofun, am, Coin, Ca, Cutan, Cat 0, Caos 7, Cu ia, Canidern, Compound 744, Cag Sein, Deaper, Dear, ENT 29369, Eeoas evista | prod Nadya rice este {S80 Lan ear Metis eapaglewtunone, CNSR oe { ewvoePs Match ‘e-Nopii Nomethcabante, OMS 29. Pra, Earn, Sees, Sete, Serie, Sen Sk fart Ue 7, Unio Csi 144 aims, (198) have desc peclem wi ie gas eromatgrapcHetfaton He te eecherea te ea taba tn the marerbery exc hd ee tan ce (eave prin) cl 21, whaas on aun spl of ae ceive reton ie 6 A. Howey Oe ass pect Ounce the ait a anew aruraia cheno mas eo wer ct ated tine conespnding spec of aur carta. was seated a tbe [Eager rotten ine oe extna pk ruled from ovelading of te gas orator aici ‘CARBENDAZIM ‘CoHgN302 (191) Lo pine +t 30 100 150 3 A aweoaos (CAS: Cabri ald 1 bensiniazo2 ner 1060-21-71 Mere nex: 171 Mas spect NBS 4379" ‘BAS 340, BAS 67054, Davin, BCM, 2Benainidaolcartamic sid mel exer, Ti bensntieah2 plume se medi ester, BMC, Cavtencaale, CTR 6669, ‘Bernal Ho Hat, ki 2(Mebosyeato io bruise Met benz [dicate Me 1i-bimiguol2 3k nee ecm Tc ey {iseesteemenpermur. Assan ting enon tenner Settee arma rGeun mmcars egainie fet epeewtieaararenta esas iSite cep ea toes otal ie ee ‘hints 80 had hrofor, 10 Benen sas beta, Eanes st 0° a we aeeretent a 10, NO Pe SOETaatig ee eteomacgrphy 180", and carendaim was formed inthe co Analytical Arifocs a source fa mas pecrmettopering a 180° (Chia and Doors, 1974) ‘SERS ANS ATMS SheaBcataonoteatentcm. NES CARBITOL CoHt1a05 (139 as 39 n pth 134 50 100 150 CChyCH,OCH,CHOCH-CHLOH ‘cas: Bhan, 2-@eborytory) (11900 Me ae 12 as ec: NBS 258" cael cent yin nn ce, ia ee Ae Beh onan Eotyig eas 2-2 iboyedbony ae, Ey ce Patras, Solved el Cari sed sa sven oc ety, and my appear in gs chem of Srey aia rope et manner Pry a ans. 1978) as spectra of inet derivate oer {C051 205, NBS 1256" ro 4 J so 100 150we ~ Middedtch Anclyical Aries 19 206 200 250 300 350 Steal: (PEmoreTeR ACEC ACD 200 250 300 350 Se is EXTRACTION COUNEUCONTANRANTS 1a-CARBOMETHOXY.20-(2'(oASOPROPYL- PHENYL)-ETHYL)-1,30-DIMETHYL- CYCLOHEXANE, C20Hl3002 (302) ‘too ese ea, 13 diy 212 ¢L-ey le CAS: Splenmectont a 13 dneby 2123-1 etyey ey 13-DineibyL2.(28 matey pbenyeyeyloeranecatonybe ait ‘A conan po in nrc by Ent (980, Tis compound is ectaiyreieelo berms ne) Eases. 0580. secu of ety ese of e-cetathny-2e(2-m-sopopy ey 19.30- Sean os ONO NRS UR wt satd 50 100 150 CARBON BLACK ‘seme te oon ck wt etn ud oar opac ‘yarcartos (tres guranes tayaes, at io conpeuds) Subsequent exrac ‘Uni limanophe et ved erg eed eae Ye ee arp andmaphlenedevivves (raphy SSaEio peony fae readme he opie wan sas poops ee ‘Shand (Puch ale) “Te Merk Inde 1792] provi ual scour of te vcs amorous carters CARBON DIOXIDE - con ay a 02 (CAS: Cuber oid [124389] Mas spect NES 3978, As 11° ‘Cun id as Conic sydd, Catone, Dry ee Formed utenti ince fannie in the pros of sles eel (Cotas east)Oe aaa’ See al: DHOFANOX —_— CARBON DISULFIDE C82 (76) Vee i 50 100 150 82 CAS: Carton ile (115-0) Merck Index: 1795 ‘Mass spectrum: NBS 24, as 9, Spiel ard Spieler (1973) ‘Caron bislfe, Con bse, Carbon dsnhite, Carbon ude, Dihncrbnic ‘Sipe, NOTODD1, uhecwbinsahydie, Weevkox ape angie lous te seems es nd (gy apectopmonee ple OF Feet 85 Lp ids Okada 1970, nd ye foley reso hee aa er Ce soe compan 2 pb nian fae 5 po) a0 1S ‘Bae (pis and Ord ‘See alae: BENZENE, TOE CARBON MONOXIDE co as) ES so 100 150 co Analytical Artifacts 13 CCAS: Carbon mosoxie(630-08-0) Merc nds: 197 ‘Mas sperm: NBS 3977, as 3" ‘carbon menoore, Cute oxide Lavender stopered EDTA. containing Vacotans tubes (No, 6496) nave ben found to ‘ln cron mooie. Tose tube! ae nsstabl fr colecting ood for say is Stes femepiobn one ules te abst peed toe se Veeman et 1981. Carton monoid s formed when te nsec hota etd inthe presence of ‘Sint el (Cokin a 983), See la: BLOOD COLLECTION DEVICES THHOFANOK —_— ‘CARBON TETRACHLORIDE cy 152) CARBON TETRACHLORIDE rr 77 eg 2 ul i || say so 100 150 ecu CAs: Meher 1628-1 ene: 199 Mag ccc NS 7, An 59, pea Spine (97), a Beninform, Caton, Carbon chloe, ENT 4705, Fos, re 10, Halon 104, Nine eon Necatrina Nestee Peetiononehane, Techoronehare ‘Arps (1970) repre th sll agent grade carton erchlrie conned 0.23 Seon teh oo Oe The CCuten teraelonide nas teen found ‘Setboretyine Gleher ea 97D, ‘The presence of residual chlorine in clated water can ad to the prodacion of ToGESRIS shah in cand ee ca "rer at concentration of 05% in reagent grade1 Middteatch borchoromsane dung porge, fhe wus cinot be conc romp it ‘Stogmened hat esl bese emoved by acon aha eae ch ‘8 soda eu Budde an Eicher 179), Pasage of comenrate squtous clin solitons tough anor activated exon Mtr eben erode (Sey etal 381) ‘$4 uo: BROMODICHLOROMETHANE, CHARCOAL, CHLORINE, CXLOBOFORM, BistoncertonosetAve, TUCHLORDETLENE Analyical Artifacts 133 (1.234-Temtyer-67-snytroy 3.souralncaronye wd 5 eo “oral oecurtng anino ac” rom seeds of he egune Mucana tone ele us Ts "ws ebb form by eran bree Bap ome bes a tral om enamine ens ene ea, ine See a: FORMALDEHYDE, TETRARYOROSOCUNOLNES CARVACROL, CioHtig0 (180) CARBONYL SULFIDE Cos (60) 1s co 2 150 deh It 30 100 150 30 120 150 once cw (CAS: Caton oie (463.581) ‘Mas seem: NBS 298, Ate 35° Caren oxmtie orp te ieee isos heel ne pra of sas st (Ce See cise OFAN L-CARBOXY-6,7-DINYDROXY-1.2, ‘TETRAHYDROISOQUINOLINE. CAS: SHsouinlingcabonylic sid, 123terahyéo-6 7-4inytrony-, (S) bani CipHtaNOg (209) (CAS: Phas 2th (09.752) Mer nder: 1855 Mas specu: NBS 419, Als 95 Anion, 2p Cymenol, 2 Hydroxy p-cymene, pop cea, Tema, 2 Me pane Sint eachyeaypiosl ema me MN Catan found undergo deraaon ude sii condins nator eave Simones a Set: Crea134 Midaleditch Analytical Arifacts 135 CARZENIDE CHyNO4S (201) H (CAS: Benois (anon 1384101 Mer nde 1858 4¢Aminoson nmi si, Beno wip sultans, pCuoxstenenelonanise, ‘ita p Sultmoytenoe a, p Samos 2p Sulfocaronenok 28 A comtarinainschain See alas Scene 200 250 300 350 410 | 400 450 500 350 Se alas FER PAPER CONTANDRANTS 7 CETYL ALCOHOL, CieHta40 (242) EROTIC ACID Coelts202 (396) ‘CHy(CH)2s0H:COOH TS] 69) 3 or (CAS: Heacoramie a 1505-465.71 mn Repo as consent fer poperRenber ea, 197) ‘Mas secmum of retest (C40 (410, NBS 588, a 2173 > tbo to ra 67 143 | tl (242) 50 100 150 200 250 300 350 (CH(CHa)dOHzOH (CAS: 1 Hexadean 6653-524) Merkin: 983136 > Middtedch Mas spre NBS 46, At 1713, 1714 715%, vo Ua eta 1971), Bil Bol Pil aes Report sa cosine fle pger(Remberg et a 1971; en Unmet, 971) ak sine cobs alec, A) > Mase of wines derivative of ey esta (Ci F08i (14), NBS Yep recon vis ow, rs 103 298 wa 200 250 300 350 ‘See alias EXTRACTION CLINGS COSTAMEUSTS,PLTER PAPER CONTAMANTS (CHAMELEONS ‘Wachcatfordengig uses eae ames. Acantonsry te: Acoupiof ye ao on ofthe protest the Universi of Houson tkvisin sation ‘Sherine Tunas Conposdon of feces wed bythe Cay t eepdaage ‘dics car Tete Se gare re ola Kren, tune whch reopened ar ynnymn fr 4 siir.o.ced neo the Envtonmeil Poesia Agency's “Pry Sage faleichc 181, ser i et hare Coney ac ung ‘etic for whch he Evie rowan Agcy ba imped eget ie {changes ne eee st called the Hoon fice of he mulecare and Sratrmtd mac kKease was nie. a Syeonym for ddaivo ae 8 nl , ° t00 150 50 100 180, 293 200 250 300 350168, + “Middteditch les! pecan of Dexsl-3006C cared yin: : re aati 30 10 150 207 200 250 300 350 1 ae 480 300 350 A samen pea fr clam eet Caton, QV, OF-10, QF, SE, 'SF-50, XE-640) has also been provided by Spiteer and Spteller (1973). e ‘Scale DECAMETHYLCYCLOPENTASILOKAN, HEXAMETHYLCYCLOTRSTLORANE, ‘Stoxwus Analyical Arifacs 16 upper was war ofthe problem andreplcad hen with another (wont Bo, Batt Toei ote carina te om Sets eas sec ‘ow ean you avo prodens with canine agen? By he single expe of See ee af ely deny noe tr ten See ae BSCE PRTUALATS COPPER cu (63) cu (CAS: Copper 740-508} Mera: 2491 ‘Ach Chemical Co. npoy capers atta te fing produc a0 2. fedStensege, chorsindomstane, {chor -odopropane, and ey! idoactae ‘Riles ae Zs, 187). Se a: POO BEARDS AND LAC. SPOTS COTININE CroHt12N20 076) CONTAMINATED REAGENTS ‘King na (1977 warm ha,“ tly vows ose Daeg pr Sa Cages appear nay aero gre oes nas gre sare ay act sb wrong seins. Asan exe, 1 ee pets apes tle of peneucropepln ed found fs wey co te chee fhsted Stuctashesvilycntuminaed ota elteoacec 2 “Ap reucawle ‘aeey ot 7 reagents tga avule vhs conarraon sd some ot ning way ena Be re wr” using ee 17081 prada ox of 4 Otley PASI theft bay comand wb Bee chybey pamae he 100 150 ‘CAS: 2.Pyrotinone, mel S3-psnS)- 486566 Mee ex: 2532 ‘Mas sect NBS 4302"170 Midaleteh ete indee: 1678 (Arey et a 1989) 1 MedyL 5.6 prion, ¥ Meyt2-G pS pymtiene CCotsce a major meal of ricesig and cn be wed to monitor compliance wit ‘Siting Genes propa If coonine to be massed ai however, he ait ‘Sem fc tased wit exe co remove cote hich mapht have derive em amo ‘here topo sake (ky and Wotan 1985), COUMARIN eee 0 150 (CAS: 241-1 Benzopyan ne P1645} Merk ine: 2543 Col4g02 (146) ‘Mas spectra: NES 4183" Retetion ner 1418 (dey a, 1885) 1 2-Benzopyrone, Counasin, ci o-Coumssia acid lone, Coun aye, aan Pipdvoenmunte sé cone opdroxjemam atone, 20X12. ‘npn, Tena became ‘Acinamor he ofr inked ben was ce to the Pour wd in ts peptone ‘ASE RIng sop ees ideaied ex eumarn whic Served fom coer eed ‘Belin Flu wits cfkocor conned 2636 ppm tuna, wide De coun eT of clover seeds wat 096-1 2%. The sete also cena the locos of Sy Ci, hich ny be convened to couman by ayerejs Gung, wocacing (ry eal, 978). Analytical Artifacts m o-CRESOL, CrHg0 (108) joe 50 100 150 os. or CAS: Pens, 2-mety (95.487) Mec nde: 2566 Mass spectrom: NBS 4021, ASS 35,338" exon nde: 1040 (Arey ea, 1865) ‘Cree aio Hydraxyole, 2 Mattel Junk eta (1974) found o-cresa in water which had pase nog & polyng Chr) ie, and tegened ha wae ber ade tobe plyes. Mas sperm of ety desiatv of cl {CaO (122), NBS 4053* jizz Mii, 50 100 150m ._ Middleditch Serta tne oct NEE Analytical Artifacts trans2.Dotenal, Cresent, Cron, Cronica, P-Methylecrleia, ‘oppose adore! ee js res ‘Identified as an impurity in the antimicrobial agent dimethoxane (Woolfson and Woodside, ‘eo ‘es | | See Doerr spt it 50 100 150 ‘CROTONIC ACID CaHeOr (86) CRESYL DIPHENYL PHOSPHATE Cig 1704P (340) i" [Ps e * 50 100, 150, Cia ire mayen erycaeoneoor _Amajor contenant repored in dicresyl phenyl phosphate (Ramsey et, 1980). (CAS: 2-Butenoic aid E3724-65-0) festa baer nem nets ne CROTONALDEHYDE, CaHigO (70) [ar so 100 150 cHycHcHCHO (AS: 2. 6170303), Merc ae: 285 acs seceum: NBS 16, Alas, 59" Mas spectra: NBS 2, As 137,138 rans? buenle sc o-Crotnie 2, wars-Cotonke a 3-Methyaeic a Bledyaoyte aid Std ernie ‘Goi ai atten repre a mip in reagent rate ty ct Pea cote ena sn cote le elon vine seperti gemini onic Serie anc aes tatkup ihe conser iran dilinan (Comper Mas spec of ethyl ester fete (C3403 (10), NBS, Alas 245° J es 41 100m4 Miaitedtch Analytical Artifacts 175 ele: PPL ACETATE * (CUMENE Coz (120) “CRYSTALLIZABLE CHLOROPHYLL” ros a Seneonih Tne ies eases we elite ore Cachan eas ve Sand th fi Gera ry oe en Sharan ory Ay aber nai ond where eum etn te fare of erp heey. Whar Wilner chimed wo have crysalised Botinipctede deine ease ih mamendn ne ‘arog was m tad hat the plan pigmerts were call cOMer ane. The feud had begun. Iwas Tew vers The Establishes. tn i second Maser’ PaaS Gh) tases addy ntl te prenonenenefsceste seen on apt $e ny ac ier oie is when cng mean eer cto igre troup Soe ee Woo ea hl Free Be wer were Sper Kd Ansedars teen, Dt ce aa PEE Al ove Nal ‘Fee suspe mehodsogy wich wish uncom nd he ws tn Ost (iS tetanatet sa) Altea beeen wich od cone, wd roman ices chs ie were eng na Bes abo aia Fanon Marner ha notrett inset sin sate su be aed ie Frents,poute cathe creare fhe werk td deed resus. Tt Srreaskedvicewty a 100) Poessor Le Marcwa of Cracow Ualveriy wre that Tawet's whole pod vas snlaly wong, ar the scaled cyacoraie ce naar Stands emetic sing sent te hptl erdomer ot Het a 1512 at Wares conceal est ts edt suo tit twas Wile’ wo was eared Reel Po Byler. ocure of [E1013 for hs Cocovery. By a ime German ors wee aporaching Wars and ‘etc hcocon baa, Hews i ksh and deo 31 whe ag P'Treteaimgee of by Jovna fortwo deca brome ere ls ean aan hemi, Hs rc ey wn ech ‘ne smltncoa elon of opens emeex mixes 10 50 100 150 PRCHICHe (CAS: Benz, Lm) 5828) Merkin: 2605, Mas spec 4089, Alas 83,48, 486% Como, opropytenzine, propyl, (Metter, 2-Penygopene CCunen has teen denied contaminant n sctne maroc fom come ina il i carat se ccm ge ect nape chy gl, Te ayes waamered wwe wire Epes hy elec oth Gliese Sed in 2a-Gmsmrenprepne. he Seamed repr’ bal tpprey fren manufac fem aoe twat ‘mardi he tere erie ef ebb Be {SRC se merc ST mene core (Sih 58, See abo: ResTONE,ETHVLENECLYCOL CUPRIC CHLORIDE CHLORINATION ‘leita et a. 197 have deserved he he conversion of 3epry thy [iene (or extn prodct fans) fo (E)-chion 2 ety rtnaeye nthe sre feo enbene The won cndons were ve se posilly {tina srr epnses Sen, pra, conse, N-CYANO ARTIFACTS Metylene clarke may te contaminated wid eanogn clerige, which reacts wid ‘rary an secondary tes weld Neyo aac. “Ths ine176 ‘Middtedich when xt fom anes slo was cone beara i Seipioe tlon hanln cea ‘See i: Crasocen cmtcni, Men. EE CLONE CYANOGEN CHLORIDE cCIN (61) ier ‘cen ‘CAS: Cynapen clr (06-74) Merc atx 268 Maspecrunc NBS 10, AeA (Cre aie, Conon Metylee corde may te conaizated with ay ediy es cya Ereraronsfigh Lega ints tate of ‘wasnt toad incr enchae, aruder io See alin 1. CHAO ARTIFACTS METILENE CORDS ( locebne Pane, CYCLOHEXADIENE, Celis (80) 5:19 Gara Tad A ON A tre 8. 8 Acta re rt pt ype opt ei ‘eee ere rete cee SEAS aee eva aihanneae une fedeccraneue tmarmen Anolytical Artifacts a7 CYCLOHEXANE CoH ise 4 joa 50 100 150 Oo (CAS: Cyelterane 1102-7 esc er: 2717 Mas pee: NES 3901 Ala 125,127, 129, pier snd Spell (1973) exon nen 681 Heydanek and McG, 19813) erahyrobenzee, Heanetylene Hesaoptbene x contrat in Maligchrote Nonograe mettyne cari eon ee gael ee, Sree lr sire. te, ee eae 60 (023 pr specucprownetc pe Fs gp and Okc el he ate pend (8 po sua ee (3 pry gore Ze eat ela "Cilahorne has beck wed sabre eetyine Dan 8 (Se ere ieee ce et eee on Sis See ana ct gy oral et fala @ jn) ay pine gia) nd we poss ‘ eerste tr ile ings” pate cites ‘SEs 15539 mp tonote waae “Pc souce cP Soo wast aeee nace or rom tee oie SSLASE emavaré, Donen rmiatate,buocrY, MUnALATE, HEPTACOSANE, Pitrcocane Menriuane ert ontbe, NOwCOsANE,GeTACOSANE, PENTACOSANE, SEVEN" INvuRITIES, TETRACOSANE, TOLUENE, TRIACONTANE, TRIBUTYC srt (CYCLOHEXANONE CeHt190 98) 2 | ‘ at dd | By 100 150 AS: Cycabearane 108.981) Merckx 2720, Mass pera: NBS 4008, Alas 23,224, 227° exon inde: 885 (Aiea, 1985) ‘Azae, Hexaton, Hye O, Ketcenametyene, Natene, NCLCSS005, Pine ene, ‘nein tone Seton sempeyed in he mata pai nd may ea aru in Sees apenas dpebeen Camera oa Qos eaten Wins’ tau cee eC eal tls oa respaenr ote PC herp Paeed isi uod nel luge The eyshexznoe cone se sein, 3% ‘iio and Ringe soak sre foc 2.5 we ext te 25.159 mg Whe Re enienaen of eychexanone a euicngdet cleus exmese (ACD) ad ong ‘ai, Sitough fr shoal be Posed at tar compe fess spect Were otaied orth uo ef eacheranne ine cnet he a. Analytical Artifacts ” ypoberanene ay be fone cringe heralded of ie uncer vacuo 3 25 ret and Neva, 1979). Thy ed orcomctt sn neta of eae Ins ben mpaned ia cyohesanone it mio crit ohms rns aki nd stich 1971, wile ks tnceaion ke ipmesrychvoed in be ue abe ‘der un amen (aise a 97a) ipa where bee rine wat gunned wi cjcanre, vce: eaae iaa dead ee e Stor eign re ccc MN IS I ee as seco cf eon dative coc CHhsNO (12, NBS ar eS a so 100 150 See so: CAPMOLACTAM, CYCLONEXEE, LYSE CYCLOHEXENE Callao (62) 34 7 e 4 50 100 150 O AS: Cycoheren (1108-81 Mer nde: 2721 Mas spectra: NBS 3999, Alla 113, Speleran Spee 1973) Rexeton index: 70 (Any ea, 1985)180 * Middtedich 1234-Teaiydobenene . Use 9 rfc sd asa fo “ied in hs” rade met ere thirde” Bitionlboe song pcs ee wn lr at lesa exraced ah eae re Ober Bayo etlorogelobeene, ethnsral jelcrsanene, echoes oe, ‘Pipe andZeyelnerePoe ebin l 57) Adc Chemic Co. ses aye rnb sabi ethene ech fd Zaks 98 Cerne my eet Tee aie a om mn ama ‘lense aioe tes osc Bunch a (079) danced eenonen 2 re fiuung such experiments, while eliza and Kost (1984) ner found tat [PRlgkacoesoe nas omer [lea (ul corey dane tlotetees [iglohioyeetare cones) and CD WO Some. “See oso: BEXZENE, BUTYLATED HYDROXYTOLUENE 2-CHLoROCYCLOUEXANOL, ‘Siclorezananer Crecotanore, 2 CYCLowRE 1, CHCLOISREN ONE, Dre.oROCCLONEANE METOVENE = : natal t foo iS (CAS: 2Cyeohenen a 22673} Mas specram: NBS 72" Cycehesen 3-3 Reparaaaconamrt in pope Soc hls (Nowiket, 179) Analytical Arias 1a Mas scr water eyeene 1H YCS 10) NBS i 170 aL it so 100 150 Secale: Sonaernomuss 2-CYCLOHEXEN-1-ONE C60 06) cy ded ot so 100 150 Reyne asa contamintin pape Sorbet ities Nowicketa 157). {Cyc ay be ferme hen one pad ag Ten GC eae Ai cpbeacs evs ppd anc esa 3S e See al SNOUT DOMBLES,THUAK ARTACTSMidateditch Analytical Arifacts 183 Mag pecan f dime diva of yah nie (AHN (127) NBS 238, As “CYCLOHEXYLAMINE Coty 09) seh ea 5s 1 4s ” jt i 4 30 100 150 so 10 180 Seeks: CAPRELACTAM o-CYCLOHEXYLANILINE Cig 075) | cache as feces 203 17s Mas seca: NBS 406 As 2° Reon ine 917 nyt 1985) J -——ineyelcbenane, Aninchbyrtene CHA, Hanning 50 100 150 Aor import in eat (Cherish ct, 1981. as spectrum of may irate of eclobenpamin (Cris (13). NBS 46 he ‘is Sb apecum appre srt Sou rm ‘CAS: Berman, 2yeceay 806-19) Ns spectrum NES E36* 1 up oye, Cyeesyereine ‘Avec cmc perros of 555 pi als omnia phe so 100 150 ‘tite peo cee y Sa er ak OOD, Sec: Deane18 + Midétedich “Analytical Artifacts 1s p-CYCLOHEXYLANILINE, Cutty 75) CYCLOHEXYL ISOBUTYL PHTHALATE ——_Cigl¥404 (04) vs 50 109 150 OO CCAS: Bensening, ytoten 607058) ae sesame NBS 6 ‘yeh, 4 Ceryeenanine “pov mp eco wae concn none of scone phy: Paras examied by Sut 8 977 See ae: DOMES ‘N-CYCLOHEXYLIDENEBUTYLAMINE CyoHigh (153) CHKONDEN, (CAS: Busine, Meycabergiene (6407992) Ncyehbesyine peaine Amir npc in cage (Carwin ea 881), ‘See cise: CAPROLACTAM oe (CAS: 12 Benes 2 eyabnyt 2 mehypey ester 1534-008) ‘A plsicns whic tots e 10 pls wich als ee peta dfn ont cope ‘EBiiptieaiee geomet ob sani, SEE ee RACED) ang pene Camey oo, OH. ‘Sei: ICYCLONEXYLASTALATE, DISOBLTY. PTIALATE cane RoOCT PAA Oot cena ty ter -Aplascies whic fot wo pats ding en ems, wih een ine APES yaaa icy sa. Ca2H 3204 (360) CYCLOHEXYL TRIDECYL PHTHALATE ——CzyHq204 (430) oc re Reto index: 2518 (Rare a 1980) ‘A plas Raman a 1980,fe Middledich AnabyicalArifocts 187 (CYCLOPENTANE C5Hyo (70) CYCLOSTEROID ARTIFACTS “ps eo ai i 2 liquid ahr bein upon by cor serene” fe cad Sa 0 SEER ccs, dieu r SERS ae en lace by wong ah O1 M haere a, einai aed - SRO Dre ach chamie emt eet Bs wo we FEE Pass aalta eta emae oe Qo cso) ear sec NSA rm ae a ef pe certs fer ro et a I Seem se Seeing petiabrtan Sig eatin ote ro: as ero "tierencs compound (19 ppm), sclaon ale {Bupprs ahd 1S grade 1p (ide and Ora, 197. See lio: BENZENE, TOLUENE oe (CYCLOPROPANE FATTY ACIDS ee ‘Reaction of bora icridenetanel wih dst err a open ppd feng 10 set Fan ce eee Co30% scr (3 mina, C17 O14 ae? pane, ad Ojo ater smite. Mow eal th Ys of S100, ae O10. at sana arora tihlonefmetaral the metas =m (Bintaevi fad Thompooe, 1971 Bran cal 1972). “See cso: METHOXYLATION ARTIFACTS, METHYLATION ARTIFACTS CYSTEIC ACID CH ,NOSS (169) HOLOCCHINH,JCHSOgH CCAS: Aine, 3: 113100828) Merendex 2716 ‘Ari -slorpialai, 3 Suonine Anita ruc feystine seating, When hoy trie employed he ‘Sip fonction ofan aby metal me psec a nah as 36 fe cysteine maybe convenes o eye S00, The eneiae i rized 0 Oe ‘sin, 570) See ae Crete CYSTINE Colhi2N20482 (240) HO OcoHIOHeSECHECHNHICO.OK casscysine 165931 Merc nen 27 Bian Peto dele, BE-Damino AF Geant de, SSPE ORE lar ea Forney sro inal soins ie. Oita oe eve ‘Sn ieee pom op hearse ste ‘eteminatos of bah compound (Frank and Seeger, 1985). ee188 See len: Abn ACD CONTAMINATION, CYSTEC ACID 24-D CpH6COs (220) jez so 100 150 220 200 250 300 350 (CAS: Aewte ai (24 crepe) 9475.71 Meridex: 2790 ‘Mas spesrare NES 481° sg, ne, tes feb Ce Cn ie Sore i ebeamnerat ir ae eee Reha 8 ieee a ke ene ree Foe oe eed Siete Sar itn ene tea Seer Sires Bidens ora ccs190 Middledich Weed Ap Buy, Weotar, Weedar6s, Weed-B-Gen, Weeder, Weedone, Weedoee LV, ‘Weed Rhu, Wonder Bar side may corsn 1.55 of 240 as. an input, ‘cortamiution toms nels win 2.-dchloopreol woul ed wo e predation of 2D" The saeea eBoy tro a ed shen, 197 Mass spectrum of met ser Of24. [CY03 (24), NBS ATE: ars 17s 199) ° 50 100 150 199 asa L 200 250 300 350 ee DAIDZEIN Casts (58) Analytical Artifacts 11 Mas pcoumot trina iva on CaO 098 Semen eral, (19840)"1: ——_ 200 250 300 350 p58 385 400 450 500 550 ‘See ae BOFLAVONES AAD LERANS CCAS: 4H Benopyrantene, Tyron 344-nyronypeny)- 1686-68) Merk ide: 294 «4. 2-ngonysoavone,7-Hytroy 3-4 ydrorypheny) 4H-Ltenopyran- tone 1 phytocarogen of dietary crigin encoumere during the analysis of human use Godman eta 9840. DAPSONE C2HraN 2038 (248) 7 jos 65 50 100 150192 + itiddtediach reas 200 250 300 330 OS (CAS: Benznamine, ufos (0.08 0) Merck ee 808 Mas spec: NBS 4637" Ramon index: 280 (Aya 1589) ‘Anidv 11 976 Avolfon, Avon, BEC t-aniopteny) sun, Crys ide ADS Si Pa Panels, 4-Day ‘sit ign len Dibner: yore, Car, OS, Danas PUSS set AT 96, nlitelee C,NCLCUTTTS 7 Siora Slane, {Stipes 4€ulonne Same, mca 8 UB pattem wire mpd Pedtcidipcot lee ese impemes donoreantinae oe ai iihwaaene wortuyaion of trido-tani one (tea nt SERPS dheg) ana rater oie oe aalgnos eave fp ‘nev ahycbye produ othe cog (Vaden ete Seal 4 AMINCDNHENY.SULFONE,24°-DIAMINOIEMENYL STLENE Analytical Artifcts 193, __ pe"DDD CrattiyCls C8) re 165, 50 100 150 By | 318 + 200 250 300 350 y CCAS: Bene, L422 iceety ident clr: (72481 Merk de 3084 Mas pecan: NBS AS, Safa tinge (1973), Md et 198) Reto ner: 720 (Arey ea, 1985) L1-Big clovophen}2.2-dtlerotne, Bicone) 22-Sehevontane, 2 Baby chlropery -aclerectane 22 Bat DL deh, ‘oo, Dele a napedlocperitane i Dawa AC py hve Dictoriphenykichlaneslane 1c ichoryieneisl chore. Sen hie era pen eee ielone ae, Fearne eg ta Be a Nc Ric, SS Roane: TBE, p71, Tanchierodphen ane ‘Areal ofpp DDT, te major easier cis DO. DDD may be famed ing te aayiefpp“DOT by gas bemtogphy. Tit ‘tr nd Gbatr USES" Sten aie pet raion ha cs ven yO ‘lama employed serach 23% he pp"DET injected may ele as pg-DOD. ere seem pa ie band for DDD, cicus bm e Gerdespm Middledich ace in deine sytem of thes cromazograph, Te probe is avoided ifs ‘ee amr rie Conse 9 oR ar Sickie i Me ned conan te le eof Bay pine tn cameron of py" DOT 07. DDD (Bus and GIT Oman Coto, 15g av epg tented Pa Sree column shoo te compacts oe Ble. ‘See alu: CHAMELEONS, DDT, METAL COUNS, THIN-LAYER CIOMATOGRAHY Analytical Artifacts 195 Abo fog DOT, ih praetor DOT enews a Agiassoa: birt amaabe ole anceps dg Meme (og DOD). (1977) ave ep a op"DDE meres withthe ie rapa Tieden weber sec we ‘SinGins wee obuned on «pk eon coed Wi 13% OVT wd L988 Qt ee ‘onanSE SO caplycolnn Siaces Sees: OT op-DDE Calla, C1 ppDDE CralisCle G1) 176 176 \ ' | 30 100 150 so 100 150 ae | ab) "| 316, + 4 + 200 250 300 350 200 250 300 350 hy CAS: Benzene, chloro 222 chloe A-hlrphen eben (324 82-6) Mass specu: NBS 2402 Resection inden: 2070 (Ayes 1985) Log Middiedtch Anatytical Artifacte 27 aoe 220 217 216. 200 250 300 350 200 250 300 350 comp 0% come: CH, 6 Henco.0n (CAS: 25-¢yclheatene- one, 26-6, lity -(7922-2) Mas semen: NBS 1429" 2B Ldinetyehy2 Seycbeaiene Lone Toe tir 26ers tbe is oiled eters ee ‘ster tr he elton beeen hese wo sbsanes nai compe ‘Thecomerion af ens to tesrgunoe pocedrim sil sdinen, tt tere Pomorie sige, anny eam, Thun nace fom Soe Sta te sentence toped sendy 050 pm OF {low ie edna imei onset! S aa cap of Mem, The er ‘ast aed eps ee an crm oper Avid i 981) See ai: 2 Dien SURE 2,6-DI-ter!sBUTY LBENZOQUINONE, 4(CARBOXYMETHYL) METHIDE. C1720 (276) 175 189) 50 100 150 ‘CAS: Propane acid, 3.5 imehylethy) on0-25 DICHLOROBENZENE Catach ca) 23 nye epee = Agere enti app ot ine vd 17, Sea: toousnmes mt pote DIBUTYLTIN DILAURATE CaatlgOuSn (2) % 100 150 cranny cuCneOUO ES, oyeryayeod (CAS: Surana ay onododeeyDoryl- 1723857) Mer nde 3000 Buyers, Davanes, DBTL. Dibuybisaucyioxyin, Dibuybis(I-oxodo- (eons, Diy a, Slit D2, Ti rl ae, isa ‘seb inthe rua of ovina). Necanenblew analysis by fschrormopeary Ramsey ca 190. 44'-DICHLOROAZOBENZENE CAS: Disses, att chlorpteny (1602002) Bistehloophey inne Hydealyl of ehlornate phorylmie erin alfrts caries wich my ‘er? euyrttartoranons me ernest sce Crore eRe ROGUE Sintec cmd font cas eres CipHigCtaN2 250) (CAS: tener, Lt elore(10646-7] Mas spect NBS 4129, Al 17, BB, Miche (181)¢ Reve nr: 1023 (Arey 1985) Dieoide. | itlrohenzanesp ieorbenzl, NCL.CSI955, Pui, Parcs: {a Paral uh rtemene, aterten arom, Frans Penge Pawan PDB PCB, Sasecior ‘When Hin et a. (1973) iti p cirberone among he volts of ole Ret, Sey seed ha wt poboblya eto dacetptsen produ Se pee tee er dais woe phen Deaaiome Wek ed wo ce irk de (Cele ts 197) detected a dkclrchenzos In haan beth, an sugered it i ‘Sve rm dthrteroee wedi cae form ner ste 6 te vos ‘efoekngy experinens to stale composioe ped ae a contains ae lowing ype of —_ Soest epg are ater Gereade eo a aro marae asap of cancenraod umes oie sealons rough gual iva Mra ilrobenaee (Sep a, 8) = ten «Secs: ACETONITRILE, CHARCOAL, THA ARTIACTS' 230 Midteich Ania Arifocts ou 444"-DICHLOROBENZOPHENONE C1s¥igCh0 @50) DICHLOROBENZYL TRICHLOROPHENYL omens ee ETHER CratiCis0 88) r3 1 i mn i 4 | 4 0 100 150 1 ee 30 100 139 : 354 200 750 300 350 200 750 300 350 aspect Sate 905% Aconenntl ec pate 24 cla wh may le : Aguada ease ato eae (AS medonone, chamgtny 803821 Maseru: NEST" 2,}DICHLOROBUTANE Cally id lope octane, DBF, DCB py Dilachenepeone a Mych (29 mete of pg-DDT, te maj ent wal DDT, tah 197) mea ot Der eae rar oie phragm es SSSI cps inharan sopreume ichrtrzptnen may efor og th mas te side fl coos re ee ese ae 0 Lawl | ea Gtalk ak 170. im 18. 50 100 Seeao:bOT wo CH.cHOLCHELCHs (CAS: Bae, 25. 1581-57-71 ass geciom: NBS 20, las 27, 528°22 ~ Midledich aanganeiocmme md O82 ae famed shen eoze SESE ah ano ney ge a ped oh TGC Cape ‘Zoran bane bunch and Pecan 1979) ‘feces ofthe to heroes evry ene Seen: TN ARTEACTS ee DICHLOROCYCLOHEXANE CotlyoChe (12) ee Nas spect NBS 47,416,156 seven merc dhoreyeabeanes ens Two of tem may be raced frm cy Sooner Star coming cote i sapled ug Tener rin (Bench and per aN ea a Kin Ss), Peli and Kc 986) monroe Piles cemeneg wi ieberane cong sary. Dihlrcyclobenane may be fomed when led water spls ae extrac with ‘edn ee whe Sued with lone (Daa 1988) Seale: CYCMEXENE, METIVLESE CHLORIDE, THXAK ARTIS Analytical Artifacts 233 amen (1967) deste the we of 2-chlretyl esters. a dsutves or the sof rca hn wy Sentence SEDER evades were pegared by racson wih 2eneanol-2-CHero- age de fom Eats Chel roc ented ape Sea riage usec wpe algae DICHLORODIFLUOROMETHANE cn; (120) es an | a2 f'-DICHLORODIETHYL ETHER CaligCh0 (142) ee 6s Se essen tine vance na nF tena ye 8) psicerputaseearna aso he PSs iyfeicle eet gone Begs eae Sip keg ctegrtpey ESSE ohana raat casa) so 100 150 cre ‘CAS: Neth, ein 175.784 Mercer: 3088 as spec: NES 7, Misc a (1980 Alsen ype 2 Aron Dire cmetng, Ee CF 2. inn 12. ARSC Neon fe te ts pn 12 Geneon (ito, eee BSS Et tad Pega anceps ds may be preserved by 8 eesing athe which vos, act comet wth ered ya erg nes Ecibclikuefcnare Cnet mo Kit (977 bave Geox sl Gioia: ‘Tere news ena is aos meen26 Mudatedich Analyieal Artifacts 235 sym-DICHLOROMETHYL ETHER C2HAChO (114) 7 i so 100 150 cich,och,c! CAS: Methane, nse. [2.88.1 Mera edo: 3085 me) Mass spect: NES A093, Aas 368, Mieldich to 98D [BCME. Hischloromety eer, Bi: CME, Chlo{chrameibor methane, Cer aoa ee ep eerdiscin! ede, Dinenyrt-satresber Mochi ‘Bet er Oxpaccsoebe) Dichromedy eters bon repre a ax uy inthe chlrrety ing ae ‘Bitty meyer Cloud Ral el tal (1970 le ha ym es maybe food wih bf ‘hou C01 & rencon of fraucny nd Ryorogen cere nos a. Toman ‘2. (v1 Rather onentpset ne wasions betwen falda cre ‘ebsinney fc acer CichOC OCD an Saher iis6cllE Seon, a § fokon ite tom Cec lO (SPSS) Soa tat be ayes es ach as CUS PRO 2 Giro" ol 983) se py cea ls gelesen ne oma Disa as rer fuel song ele ram bane pore Becta tne ergo cyan my saree sso ‘Dereon eer Stung sd Wh Se ieee PROPANE LOHR and pm hooey eer have snot ene eco as citnageptic ec neon SED eee 2,6-DICHLOROPHENOL CgHtyCh,0 (162) (CAS: Penal, 265 iho (67.465. ‘2fDiherophenl was epee by Berges (197) to be asx romonsf e oes ‘5. miner american) hs ral ee ha ie ra esc re ce ‘any hort pews ae wed ashes. Howeve, one fe ference tks Ser rl prc ox ‘ether tone compen a dae sada A Tce eet we date cul ery ws we ‘Zheng bat sen es, eee heh be pron vn grew he fps ted a ‘rhe fal ay meee hae nie Mra. Sever i {Ge caprimest and nro ntmepie: ote we nes, tanga meta ‘ae ng uly ge geno ecg gen ont, Seealio: Mennnecr.oDe N-@.5-DICHLOROPHENYL)-3-1SOPROPYL-24-DIOXO- {MIDAZOLIDINE-L-CARBOXAMIDE. Cy3Hi,3C1N303 (329)236 “Middleditch Analytical Artifacts 237 329 200 250 300 +350 oO ban, CAS: 1nkzolincrboxaite, 1-035 elropheny) medley} 2s. feesrasay Mas spec: Coke et ah (9)" redone (3 dcrpteny) N toy 2. doxsniaralg | atone, Gee ye Fue on he a Raa te tbe oop are eee a eet [Rigid ae tasesy sec esi er nthe sien, Coke {GiSd ts sana vans of rode chat (or ear aried speak ot {Enger racagn tin by gue ranaoyeagte wpa within mites of Sade Oe ‘ard Adan sly he po np mae. es yey ra rs cy te ey on pte nna akip Sonepat ti Sbnae an veme rng ea DICHLOROPROPENE each (10 sage of cacti agus crn ens rghit con Hock Seecperas Semana a Seeake: UsCoA. DICHLOROSTYRENE. CHCl: (172) “ere emegatson eeean ago Saeraaeserrererahion rotor ree SEGicrib manana eae See abe STRENE, TOXAK ARTIACTS bod eb ft te - x (CAS: Bernat, 26 cleo (9805} Mas speenur: NBS 4480" ALSO, Als, Baran, CDNA, DCNA 2(Dichlore--siomiln,26-Dihoro-+ ‘ivcbenzeumie, Dol RIGS, Resa, Ut Dir compton crore clus mal of copes cr ales geet rehire nt gut an (tod eve, ght. 238 Middledich icon shoul necked wit be iste ichlaran Me Indes 30382 See lie: METAL COMES ee DICRESYL PHENYL PHOSPHATE, CapHligO4P (354) ‘CAS: Phosphoric aber henge [2646-73-1 “Two dees pen ae peset concen of 142% and 15.2% i cet ea Hag cecaon of 3 me fered! Fygel CE ee ora has conan reper ces) pny Psp Oe er ete wl ney oma Rae) ey 190). ‘Se alu: CRESVL IPE PHOSPHATE, TUCRESYL PHOSPHATE DICYCLOHEXYL ADIPATE OnnnminenO) ‘CAS: Henne i cyclen ener 9699-01 Reteon index: 2282 (Racy ta 1980) (yet ate Aplus Crslts904 10) Analytical Anifacts 239 NN-DICYCLOHEXYL-3-PENTYLAMINE ore set by Abie Chemical Cn o saline 2 {ineysyDehonrehyl hie 128) (Sfiathiten and ins, 88, CHiN @st) DICYCLOHEXYL PHTHALATE CagHia60s (330) rae Latah 50 100 150 (330) DICYCLOHEXYL OXALATE OneO (CAS: Bhan, pln er 162062-6, etevos index: 1860 (Ramsey 1980) Cyckbeny rata Alas, Crattz204 250) 200 250 300 380 Oo (CAS: 2 enero i decease 8661-7 Mae pec: NBS 2548, As 180" Renn inte: 2461 (Raye, 1980)240 Midateditch este pala : ‘Alaina a ia 158). Sith a Blane (197) ne gg SeSSehee paiSeg macotnde major inpurtyineyahery by peli (Rasy 1,190). NN-DICYCLOHEXYLUREA On, CisHasN20 (224) (CAS: Ure igen (2387-23-21 a sf derazaon estos leben which set ‘2 love wo og ewriatoe sue foes foes (val, Eh Fulereal 913: Gati Nites snd Sob 1975) DIDECYL ADIPATE Cagltsy4 (426) {Cly(CHpleCH0.00(CH,),CO.OCHOM,}ECHy (CAS: Herne acid ie ser 105.975 Rewtion index: 2905 Ramsey 31980) Aplasicoee DIDECYL PHTHALATE CagtlasOa (440) ‘Seven isan ee pales ar ued spa (Aas an Gian, 1969, DIETHYL ADIPATE CroHy904 202) (CHsCH-0.00(0H)C0.00H,Ct%, (OAS: Hennes wid, tyes [81-284] Analytical Artifacts 2a ‘Renton index: 949 Rasy et, 98), 134 (Arey ta 1985) inate Apts DIETHYLAMINE, CaN 03) 58 1 so 100 150 (crore (CAS: name, ty (1009-71 Mer nde 3090 Mas specu: NBS 2, Als 6 DEN, Dietaning MEykethnanioe iain forma a prt ira ain epg (mes Alcplarve eke Pie von ene See cue W NEROOOETLANINE DIETHYLBENZENE CrpHag (134) ‘CAS: Bere, ey 15340-1741 Mas spec NBS 302 Aas 653, 658 669,67. 672 Repanedssa contamina i Abe XAD2 esi ta cocenrain of 102 ppm. Aer [fiat cium ee cnr at al pT Ot ‘wnt empyedin be Wenn tes 80 fon Pere aay ‘See ct: AMBERLITEAD 2 FORAPAK ONDATION22 ‘Miadtedteh ee DIETHYL CARBONATE CsHy003 (118) DIETHYL CARBONATE Ce as o ro) so 100 150 GHCHJOCO.OOH CH ‘CAS. Cai a ity ser 105-581 Merkle 3727 Mas specu: NS 18, Aa 50" Dis, inca fermi rye, Ey eon, Eta pie (96) pane ety caert was forme when ea app ca ee ertectans once be nore cnc Ve enol pena ‘Ser la: CLOMOFORM,EDIANOL, EALESERS, URETHAN DIETHYL ETHER Catt 7 DETHYL EMER BT so 3) 7a so 100 150 CH_CHOCH ECs (CAS: Bane, L-exbi 6029-7) Merk nde: 3751 Mase specu: NBS 3986, Als 4, 86+ Analytical Arifocts ms _Anestsiceer,Anebesa eer, Aes her, Di exe, Ee, Eboxyethane, ‘Siptemer yone |e Owtiebane Seven obey, Sle ber Borin Jckon ie as” ety ether cnn 2 ers taped byron (sadeh rd Za 1987, 2.6<)ert iene {est he pps Aton) tne sob edt sn ‘er unit ety abe i set fer be exrason of aqueous samp, aad ‘yes act a ean ean, forme a ey acta vail fered abe and Ree 1967. Sop ena ers eevee ‘ASeubee pace ae gh roy eek canon 0 mph Te cot Soncen jet ete is cease cere dng he deeriatin of Mood bol ees ‘SRE eh sea te lr ng te supe (Cry, 197). Passage of concensed aguas cla sons dough granular acted ean wd ety cer (Soe ete 18D. Seto: CEPALDEHYDE, ACE ACD, ACETONE, BUTYATEDIDROXYTOLLENE, ‘Slane 2 Draerr BrUsoL, EasoL, Ev ACETATE, POYLCALLATE, DIETHYL ETHOXYSUCCINATE, CxoHigOs 218) ry0H:0.06OH_CHLOCH,CHICO.OEHECH (AS: Sune i bay ay ene 1796100) onset courered when eiaol-stabiln chloferm wat wid wo extn maple sy Fost eth ash lamin, wos nenion cto ‘ic ab ad edmal pce 1) Seeclt: CHLOROFORM, DUEL MALATE, ErHANGL, ETTLESTERS2 Middedich DIETHYL FUMARATE Cel i204 (172) a7 99 72) so 100 150 couenoccp wicooayen, (CAS: 2 Butea act (6) ity ser (625514) asset: NBS 78, Ass 167, 1168" Retro ex: 1160 Heyer and McGann, 18) epi marae Encountered ven ethanol stblized crofrm vas used rexract maple yp ‘Ryton oda far od el anal (pe ta, 18). DIETHYL KETONE, CsHty90 66) a [s7 6 so 100 150 (CrgCHCOCH CH (CAS:3-Penaine 962.) Merc index: 3106 ‘Mas spectra: NBS 3992, Aas 141,146 MS DIETHYL MALATE CeHt140s (190) (CHCH-0,00CH,CH(OHICO.OCH,CHs (CAS: Bune ci ony ty est 7384123 Encountered when tara-ubized eherforn was vse fo extract maple Sip. Foil arene pod of ma ab ant eal pee 1969) DIETHYL OXALATE Ceth1004 (146) ae Ss 14 so 100 (CH,CH,0.0000.00H,0H, CCAS: Boards, ety eser 5521) (148) 150' 6 Middledtch Merc ae: 3110 Mass peer NBS 4125, Als 820,522" Retention index: 540 (Arie, 1985) Diet etaneone Edy one Encountered when chal stat eMeroforn was used to enact maple STH ogee ee clo crac act acaba oi produc and ean pice a, 19697 a DIETHYL PHTHALATE, Cra 404 22) eee ras Ww 50 100 150 222 nabicolArifoces ur scenes i, te gi tm ce sep es Api has dG, 49), Sn enna 97) hw mene at SEY Ta fove Rahal hg Gna ese an Remneta ope Snt te osha 17) ale hes (Go tinea fo ti at ity phate a among te exogenous components ofthe human ally voles (Gated, 197) Diet ple as en eps eatin pact Anite XAD 2 raph Seip eat a Rep anni he ity pase sed odaanae ene sa ave fund his corsa spe ‘ices sted by etanlearacion att of hy tae wig a ays st aways nnn of certain Sari an bored aud vient om ‘rated texas maple sop. ws sped ur twas area pric fea TGC aese cutee pode) and ethan (pi ea, 190) See cu: ACETONE, ANMERLIE XAD2, ANTLARY VOLATILES, CHLOROFORY, Secret: Banos Ev. txt, EgrmAacTiow GOLA CONTAMIATS, Fibcave Memancn, Menbvunircriowbe Suu MSMLES DIETHYL SEBACATE Cragg 58) 200 250 300 350 co = civsmramoetantermn vas Mas spect: NBS 4521, Alas 1569, 157, Milica 981 Retesion index: 1568 (Ramsey es, 1660), 1559 (Heyéarek and MeCarin, 1981), HSot (Arey ta 1985) (CF,CH_0.,004CH}400 00H ‘CAS: Deanne si ethylene (110-407) enon inde: 146 (Ramsey, 1980, 145 (Ay ta 198) ‘Biatex DES, Diet decane, Dit teen, ty she Aplaiae8 + Middeditcs >? ‘ls-DIETHYLSTILBESTROL, Crittay02 (268) ey ” (CAS: Phenol, 44412 Shy -eenediy i (2 (2610587) AE 2DethyLAZedenesiyiphenal crt er opt ner seletben annft sa cera rer donee et tmieratas Pomc ‘tay actly Be dpe fran he rans omer schon, Ruben (1970) Same tennis erences Sy ee oe aetna SiyDtstewonearade. The tus pc bo bones ay hepeaelose a a fa 200 ina ds cooks wc ities, ek erie fe sonra red eo 60 aha TO, eases nen trp tea Sousa ea are ets Fe cetera esas Seay coon fa Ur mona yen ae oreoeeienale sername Seer epee DIETHYLSTILBESTROL MONOMETHYL, ETHER ‘CigHta20> 282) .e%, Analytical Arifcts 2409 (CAS: Penal 4-2 methonypheny cen (777260.6) Merc ex 5161 39% Diet metoxy ates, (By ‘Spubtonygheny-+p metorypheny suns Meso ‘A eur mist o€ 230% of he ifr 73-70% of he rans fn of his seni fomed rapidly when dotved In ity cer, win 1S mie ‘when Gaslved in chloterm Sas orto shu Sectesosthrofeqlbes fgpate she ag aes equa ne ecru ied lr ‘Fae cfoqibaion of oa eae ane (lar 1, ey bteeypbenot, DIETHYL 2,2,3,3-TETRAMETHYLBUTANE- 14DIOATE Ci2H2204 230) (gCH00.O(CHg:CICH3),CO.OCH:CH (CAS: Baresi cl, raed ity eer 567-543] esti an psy nie cages Uohaeson an he, 170. See aos QoMRATE 1,3-DIGLYCERIDES peste arac 2a my tea rt ae ae ts eg ae ret rae eattoeana tonne iets ae iireiidgemcen at acgsat faeries osu aetieivahfasianes algheedes sean cel a sgiecciprencipiastnha ieioeeemaae See al TUGLYCERDES250 Middtedtch Analytical Artifacts 2st DIHEPTYL PHTHALATE concngeyieh, ors ‘CAS: 12- Benenson ai, hey ester 3608213) Retin inden: 2800 Rae 1580) eo eae Aplastic, Cra¥ty404 862) DIHEXYL MALEATE, CeHaag (88) vecooayennen, OOCKEHy CCAS: 2 Buena 2), ies] este 16064588) Rezo index: 2116 Rasy, 1; Ay ta, 1985) Dixy Apia, ee DIHEXYL PHTHALATE CagHlse4 (334) eee a ve fos rae 1 ssa 200 250 300 350 oe ‘coceeH EN, (CAS: 12 Berenice der ete (875-3) ase spectra: NBS 4537 ery stale siigsivaxraagerearer sere Seat: PLTER PAPER COREASENASTS DIHYDROABIETIC ACID Captts202 (308) KO, AS: mace 123A S848 10 eden A Sayre ta aeakewhiesr ata Abo 0c sei. 78 Dybn wt (tea tba Bf On ‘henecarmeye a 3 kapopy SP podooup 3-0-5. Arend commonly eco in wos! pods espe paper an etersa0 ney nie 90:01 NS, rn fn Middedich NBS 2441, Ekman and im Luu pod Lim Pane eee eee sna mac a ciinoe a " cissbtnnst cients ma chusigniiyony bones eee atennee teeeyclnmtrim secs {Retain ofa dink They st rane of mctlipndn ee aes keane re it ee ofS epee SEG), Su 48), 309 (98), 308 ash 27 GH), LOR) (Ober a si tig ay See alo: 2 HDRORY-1S-OXOATRACTYLANA-CARBGHYLATE Anabyical Artifacts 253 2,3-DIHYDROBENZ[d)ISOTHIAZOLE 1,L-DIOXIDE, CrHyNO,S (169) co. (CAS: 23-Diydroben{aotianl, ote 996.1631 ‘Anion saa, Remick nl Bll OSD aye se mein a. ie ied era tar pred ern ap Pl fae a Ue mcclstamned nee Sarno ae Go sence Zasktlemnt ae pak wei thane Pees ial Seiler hl i) aa act emboli tracy Montes sige Mea Conus ees, Seat: SACCIAIUN. 2 SULFAMOYLBEN 2 ACD, 2 SULFAMOVLSESEYL ALCOHOL DIHYDROCONIFERYL ALCOHOL, CroH 140s 1182) Puen (CAS: Beene yon: 3athony [2305.13.71 ‘Hyde 3 methnytemenprops using dy of ms fave Fp th (196) fun that he peak to ‘Byatt ae oe a cea: 9 net Bs once us compu wes ered ne pcin pt ong See rodent acumisnd ol mst Fong pe24 Middtedich nT DIHYDROISOPIMARIC ACID CaoHts202 (204) oOo 30 00 150 ee 25 304 200 250 300 350 7 ‘CAS; 1 Pherantivenceabo i act, 7h 12.3 Aan 5 678.1008 oteeayeo SASpelmeng Te latap tba iOaa} (3605-365) iar sei, 15,16 Dye acl, (1, 4b 70.1000) ‘ERRUISSTIRAR fa iloedeeyie aa-gimehy poem ‘ony aides 1 maoypedoen eS oi ‘resin ac commonyeebaneredin wood profusely pope an eterno. Analytical Artifacts 255 Mas seo of ey yinpimar (CHO (18) NBS 235: 21 so 100 150 318 200 250 300 350 See RESO ACIS DIHYDROPALUSTRIC ACID Ca9H202 G04) met, Yoon AS; | Mrannrenecaone cd, 12.4486. 8910 Detect A SRS TRAST eae a (Madara... 05678910. Dadecye- Adi. eee sauna ea me - ‘Ars acid commonly entered wool pods especialy pend eee, Farmacepcmum of ety ibrar, seth ey fr ty yep, ‘Sele: METH. DORYDROPALLSTRATE,RESI ACIDS * eeasorsct256 * Midatedvch Analytical Arifacts 27 DINYDROPIMARIC ACID CasHin02 02) y-DIHYDROXYCHALCONE Cstia03 240) ey ey Noor By 100 150 AS marae i) 2 A S679 5 ‘he meny Rca toto 5) Ba (Rada .78 0) 2.344S57.9008 Daeg 487 Hasty aden a Arenas ncren od meio ea an es L Ma cf pia Cie 18, NBS 209" a zo sho ~ 91 105 121 pas r 78 ett 14 300 200 250 Seat: METS. DANDROSOROARATE, RESIN ACIS DIHYDROXYABIETYL PHTHALATE ster that may mite or packaging mits to fod (ho and Blame, 7 ‘CAS: 2.Propert-one 15: nyonrpen360046-1) Mas spec For tal (1973) 13-BisAydroapbeny-2 open one ii meet oa a cei ply oe cmp wich oles poly err whe ime oP ae va SES Trliunranoe haere eae "8 Middtedich Analyical Arifocs 259 2,2!-DINYDROXY-5,5'-DIMETHOXY- ‘33)-Di-ter-BUTYLBIPHENYL CazHs004 358) 2,2! DIHYDROXY-5,5'-DIMETHOXY- 34-Di-vertBUTYLBIPHENYL CaaHso04 (358) co | BT y 4 | | Ly 1 il ath tte 14+ 3° v0 150 0 100 150 ase | 358 | i 20 30 380 200 250 300 350 ‘ om cy, oo Sey, cas ,-Blpbeny 22h 3-1 metyeiy S seo OTE) as ecm: Mo Maga 173° 4.3L.) dime) Siete}? il inydrony $5 ditony 33h 1s ford hen ages 2 OS so aang wake pice sees sEhtan eee ean perry Mas, 9). Ts miner ay SRES cena e Mente sa Re gear rere (0973) appa be earainted wi waits See al: vn Doren nO cites een ON ‘eg seontanartans amen wpm wean given et ee See reel eine mimi {ands fc cmcan yada. a See ei: BUTYLATED PEROXIDE260 , Middtedch DISOAMYL PHTHALATE cee CONE CCAS: 12 Renamer lt, BeS-mehyay ener [15505] Reon ne: 1853 Ramsay ta 1980) ey pane amyl pale CagHl2404 (306) Aptis, DIISOBUTYL ADIPATE CraHl 604 (258) rs 18s 37 50 00 150 (258) 200 250 300 380 (CitggCHHCH0.00(0H1C0.00H;CHICHe CCAS: Heed bites roy ener 41-048 ‘Mas seta: NBS 1897, At 1785" Rew nde: 160 (ay 8198) oy ape Analytical Artifacts 261 ‘Aplus. DIISOBUTYL AZELATE CipH3204 00) hi s7 50 100 150 2 ] (300) 200 250 300 350 (cHslacHe#:0.00;¢H,}.00.OCHCHICH)e (CAS: None el, B-etpopy eer (105.805 Mas specu: NBS 2286, Aas 1906 webu ‘A plate (ts and Gia, 198). DIISOBUTYLENE CFs (112) (CH3),COH:CICH) CH (CAS: Peon, 244srimethyt 25167708) Dishes, 24.4 Trimahy penton Diotulene bas ten ound at a concentration of O02 in a "tye The mace sect cnis waco of me 11, a peak a me 59 nd oes irs of 1, 6 0 97. No relasvesboncates wee repel fr hens lene eea, 197)22 Middiedich Se lo: RIC OROETINUNE ‘Anatytical Ariifacts 263 DUSOBUTYL TEREPHTHALATE CxeH2204 278) DISOBUTYL PHTHALATE C1eH2204 278) feledieahada arian 5 149 167° ra 36 187 ! 50 100 150 30 109 150 P= 4 23 | am 00 om 2 250 300 350 4 200260), 200 20 300 350 i | oc cOEHENC HHO, CCAS: L2-eneneiaoaye i, bist popy ese (495) ‘Mas spectrum: NBS 4745, as 2850, 1851, Speer and Spee (1973) Reeion inden: 1863 Ray ta 198,153 (Arty 1985) expe MIB, bry pale ‘A plainer (Aa and Gis, 1989), Sito aed Blea 13) have supped tha plas (Aas ant Gin, 1985) compre nage at Stay migra rom pct mars Seaman a Beemer oven Caer 1972) 0f pope Some mbes Nowe a {G57 Ecacaeclors (ese, 1990) ab of wane wich ha Bowed voug) ia es Gea, 18 ‘Amajocontninat in plone tle Raney eta 1980, See lo: CHCLOPENYL BOBUTYL PITHALATE, SONILET TIRES ‘CAS: 4 Bezneicaory a 2 mehypopyl es 1898-1) ‘Mass perm: NBS 21, Ais 180 Ree inde: 1972 Rasy ay 1980) eta repalze Apatite DUSODECYL ADIPATE. CagHiso4 (426) CaO. 0C(CHe) 60.004 aHa, (AS: eran isodecyl ese [27178160] een inde: 745 Rasy ea, 1980)264 . ‘Middleditch ‘wee pare : i . DISODECYL PHTHALATE CopHlasOs (446) Analytical Ariifacts Rezo index 244 Arye, 1585) toc aie {5p ich rs mare peak ue a remap amy 8g 2.0 an. (CAS: 12 Benatar ai, deel este 6761-400) Reweon inde: 2511 (Ramsey 1980) ues hae ‘Aplus tar may mit fo aking aia od (Sho ae Bune, 19FD Reporte contamina: sie ac pe an) al, 0D Seto: S008. SOOTY PATHALATE DISOHEPTYL PHTHALATE On om coatoeemnem deed aen ‘step phase ‘piste we ats iets pn hoppy any ta. Cals, 4 (362) DISOOCTYL ADIPATE Ca2He204 (370) (Hs70 OC CH40.0Cg Hyp ‘CAS: Hernia sony ene (1390865) DISOOCTYL MALEATE CapHtseOe (340) pe0.06)4, nbeo cep, ‘CAS: 2-Buenedio sl 2) Weyer ener 2-165] tency ate ‘Alger which attoris mati pak po scrappy Rams DIISOOCTYL PHTHALATE CoaHls204 290) ras so 100 150 200 250 300 350266 Middledich ann eer eer coats Con. cine tn 26) concn pn 97 vnesssiegea ona I sc me nt pene a ns rare neem ca "ue fom oc ro fd tka nd Blame 1973). $380) i mean ey phale Rarey ea 1980) DIISOOCTYL SEBACATE CapHts04 (426) CeH4s70.0C CHal—C0.00oHsr CAS: Deana isnot eer 27214500) ey state “ which for hil peaks pon gs ehromatography Rasy a ‘shor Analytical Artifacts 267 DISOPROPYL DISULFIDE Col xgS2 (150) as 108 150 Pa 160 150 (ChgzcHsscH(cral AS-D 1-253.) as pcr NBS 45s HP Binet, 25 Din tteane ‘A SisPSAe "Ghee ih Sade Lehn ae eres ctr an menace ras ‘Sud ater by Muppet (070), The Yet met ween tse ih ln pee snl CaS (Gtenmt Or 9) Serotec Nan S DISOPROPYL KETONE CHO (114) ae na so 160 150 (CH) -cHCO.CHCHe AS Penman, 2m (65.8001 as pec: NBS OS, 49"268 ‘Middledich 2A Dine Speman . isopropyl ketone has ben coord as 2 comaminan i atone manufactured rom, comer a Mas spc of O-methyoime of spropy etn {Ca yNO (43) NBS 386" “Analytical Artifacts 268 wea ‘A ete for Ps ed tenis py ip, Lraa 9160 pp we an sree {pgaess marine einen ve ys aur be orm opimaey po were ented bik (Sins, 197 1a ud tal ane ane seswseroe \6-DIISOPROPYLNAPHTHALENE CusHtan 212) 78 so 100 150 oF 212 200 250 300 350 oe ‘CAS: Naghbene, 25 b-etedyD- AIST] Mas eco: Sun (1977 DIKETOPIPERAZINES The condenetion fo camino ed, with elimination of v0 malas of water {Bi fomton of ice ey erie foraton os umopperazine (barb, 197, Se ai: LPROLYLA-YOROSCRROLE. DIMETHOXANE CeHy404 0174) ogo! (CAS: 13.Dioan do) 26-inatiyh ate 28.002} Merkin: 3016 Acconhoine, 6 Actoy2/dinety insane, DOOM, 24-Dinethy 1 éian- ‘fSerm, 6 Dine dona! scetse, Da, Gard DAN rs nhs nici gn lade acted ctmaehyd, a aon (Skahocan(woatsan snd woul 10 = Se los ACETALDESYDE, ACSTONOMETIOXANE. CHAMELEON, CROTORALDERYDE270 Miadiedic 3,4DIMETHOXYACETOPHENONE CyoH1205 (180) so 100 150 2.0% 5 My cistanon sean 900) von ve mame tmecoorcoe nte. rapes en coarse mains See so: Sommzrrenazs —— DIMETHYL ADIPATE Callne04 (179) —_K_ ca 145 174 50 100 150 (CHyO.00(CH,),C0.0CHs Analytical Arifacts a (AS Henao ai. ciety ese (2753.0) Masse: NBS 294, a 117,174, 1195¢ een index: 1203 Rar ta, 1980), 1213 Arey 1985) soviee : : sce ee TaN DIMETHYLANILINE catan a2 AMOUMETRYLANTLINE atin 07) v2 > pats] % wee ere iene Amey 881 venta vers HRS i Ala Hae ay 7S Mai (1973), Spleller and Spiteller (1973) = « = Reon index: 1052 Aaya, 1985) NA-Dinaybemesmie,Dimebypteylaine, N-Dinesbenranie ‘Ayres of metho ng sienna sie get a ira) Geo ney aon of utes cmnavs mentolis, dpa: ‘pda ied fry a canbe eee by jesing mse of sabia 3nd ‘Soul shoe of ity anivar hye. The acon und gost, {de nag appu obs hazards ban daze. See: wam > Middleek DIMETHYLBENZALDEHYDE CoBin10 (134) ™ arms cd) os ten ep depen pdt SARE TASTE od pad tame a) ‘Sees nse XAD2 DIMETHYLBENZOIC ACID CoHl1202 (150) ‘A dinates wi (ane: ot specifi) hasbeen repo aa depron ‘eaimelle EAD. top wa spas ne ‘Set los AMBERLITEXAD2 = vb Lt Soon moKncige eas bene 183) a Mas specoum: NBS £087" BDMA, Bonita, WN Diayhencneetamine ea Dimetra os fhe few ; ‘ona or tenes. yet achomumscen dee. Gees wi Wats fain on Canwest ne cece Vniznbetylanine ov Aprea LA pial mace of WV -sinebensyuin Beastie FF lanerchange sn pepe om a Snsy aly smirk (Gnagh Desc Joexchngr on pr myrrh (Gow As afodng& ase postive Analytical Artifacts ay See aoe NTROSAMIME ANALY, M NFROSODITHYLAMONE.N-NETROSODIPROPYL- Se DIMETHYLBIPHENYL, CiaHya (182) EgeeLg Sietag Ame Maa cin er 0 ome int ‘pit ne Sena Gate Pages, 1 See au: AMBERLITEXAD? DIMETHYL CYANURATE, ren TT Te, cA 13st eb 8 ‘arpa wten te cide htrox isbeed inthe psec of snes el (Cores ana * See alo Tagen CsHyN303 (157) DIMETHYLCYCLOHEXYL PHTHALATE ——_CaaH¥3904 (358)om Middlediteh Analytical Artifacts (275 DIMETHYLDIFLUOROSILANE CaHGF2Si 06) NN-DIMETHYLFORMAMIDE, C3HyNO 73) er ps 98 1 i so 100 150 50 100 150 (cHanSife HOONCH CAS: Sine iodine 353.6621 (CAS: Foal, MA neg (6612.2) Mark nde 5237 Mer ner 3237 Maz spec: NBS 62° Nase spectra 3985, a 76, Spieler an Sper (197) iene yin Dinh hermanie, DMF, DFA, NSCSS6,U-224 “The pence of dimethydfaoasre, i amu 8c a 0.14 mf ama A by pod of ation esztins erpoyng NN dinety oma i areas APU baedtoteanfomeator cf ory scones el tee (dp 197) These apni afr inet Horamie ty yeas Gang {ed forearbons” (Conk, 1979) (QE)-3,7-DIMETHYL-7-ETHOKY-2- ‘OCTENOIC ACID CraHia203 214) (CHigeC(OCH CHa) CHLCH_CHO{OHs)-CHCO.OH as ten fn to ander ander ae cnitos oto! QE Seay Sony Scena Hs Rare eal 98. ‘See auo:CrHaL. Stooge onde we Andee 197) ‘prolapse cee eee aera ea vei uti ae ae Cine ote erm {SiEtdy ls contain dot clk pa ce pas srices oe actin Sia btelataatiane 9h tection ects age toc et ea See: )N-Doaenn FORMAN DALAM. ACETAL BY-PRODUCTS, HEXAMETIL- DISLAzANE ARTEACT, MEAN. FORMANGDE ARTEACTS ‘NN-DIMETHYLFORMAMIDE DIALKYL ACETAL BY- ‘PRODUCTS, aire anne eis peeasol ad saan amr ps eaegen ae ve Sa past a tty ne pee fe Rncieraciiae stents incising, BT) ov el 7 eid sneer ci i yo Wowtc of Ni Omatylonnie cll ar wth ase meine276 + Middtedech of imetee to afer cinetytigonethyene deivaine. Abo, Bint {Cimaie dil scr rete ni nro ford the Conepeediogdiabosy ‘Ceblinis No wer Gest mee proved See abe: NE-DOUETIL FORMAMIDE DIMETHYL FUMARATE DECOMPOSITION “ses nd Bachar (1969 have pd ha una dros compan ‘Egge dacoumgony ctsspoaes gern °C Thee ptt eel See ct: MeL Analytical Artifacts ced N.N-DIMETHYL-W.(METHYLAMINO- ‘CARBONYLJUREA. CsHyaN302 (45) CCHANHCO.W(CHICONHCHs (CAS: nidsitborie mie, HV? ney [160021 2 Toney nt, ANN Teta, 1.2 Tethyliniodiaroni Forge wt rece ston he te sc tel (Caine See ale ODER DIMETHYL ISOPHTHALATE C4994 (194) 5,6-DIMETHYL-S-NORBORNEN-ex0-2-0L CyH140 (138) res isa so 100 150 20 (CAS: 13 Renan a diet eer 1459.93-4 as pec: 191, As 1348, 1849 Reso ine: 1488 (Ramey ea 198) pli, 50 100 150 A Mas speci: Keedamet a (1580) ‘36-Dimety ts saromen. co-lead arg nly fhe lea oil of Aes ‘Solas yee ain pode ag ass Racket 1980) Sec ate Sar