faa STL Era a 4955 Yarow Street ‘Arvada, CO 80002 Tel: 303 736.0100 Fax: 303.431 7171 wow ipe.com ANALYTICAL REPORT Project: A4TFCT940K3104401 STL Denver Lot #: D41280257 Doug Solon ASARCO PO Box 1111 FI Paso, TX 79999 STL DENVER Zh Patrick J. McEntee Project Manager October 8, 2004 [_escesinemionnens tein | sen et attTable Of Contents Standard Deliverables Report Contents Total Number of Pages Standard Deliverables The Cover Letter and the Report Cover page are considered integral Sec cnn ewer esi pe nt ar erecer i be 39 Table of Contents Case Narrative Executive Summary — Detection Highlights Methods Summary Method/Analyst Summary Lot Sample Summary Analytical Results QC Data Association Summary Chain-of-CustodyOt DALUL ST Case Narrative Enclosed is the report for five samples received at STL’s Denver laboratory on September 28, 2004. The results included in this report have been reviewed for compliance with STL’s Quality Assurance/Quality ‘Control (QA/QC) plan. The test results shown in this report meet all requirements of NELAC and any exceptions are noted below. This report may include data with reporting limits (RL) less than STL's standard reporting limit. These data and reporting limits are being used specifically to meet the needs of this project. Note that data are not customarily reported to these levels without qualifiers because they are inherently less reliable and potentially less defensible than the latest industry standards require. Dilution factors and footnotes have been provided to assist in the interpretation of the results. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of the method. STL utilizes USEPA approved methods in all analytical work. The samples presented in this report were analyzed for the parameters listed on the analytical methods summary page in accordance with the methods indicated. A stimmary of quality control parameters is provided below. This report shall not be reproduced except in full, without the written approval of the laboratory. Quality Control Summary for Lot D41280257 Sample Receiving > The cooler temperature upon receipt at the Denver laboratory was 5.8°C, The samples were received seven days after the collection date. > All sample containers were received in acceptable condition, Holding Times > The samples were analyzed outside holding times for Total Dissolved Solids (TDS). The samples Were received at the laboratory on the day of expiration and due to communication error the analysis was performed outside holding times. > All other analyses were analyzed within the required holding time. TCLP Metals Analysis, Methods SW846 6010B/6020 > The percent recoveries and RPD for the arsenic MS/MSD performed on sample D41280257-003 could not be calculated because the sample amount was four times greater than the spike amount ‘The method blank and LCS were in control. > No other anomalies were observed. General Chemistry > The pH sample duplicate performed on sample D41280257-001 was within control limits, > No anomalies were observed. All batch QC was in control.