Chemical Engineering Department

EXPERIMENT NO.

ABSORPTION

ABSORPTION
1
ABSORPTION

Chemical Engineering Department

AIM : when It is contacte with atm. air in a pac!e col"mn. APPARATUS : Pac!e col"mn# Recei$er %las!# Blower# B"rette# Pipette. MATERIAL : Conc. &'SO(# atm. air# ).* N NaO&# Phenolphthalein as an in icator. THEORY : It is an operation in which a gaseo"s mi+t"re is contacte with a s"ita,le li-"i which issol$e one or more component o. the gaseo"s mi+t"re lea$ing other component as it is. The li-"i "se .or the a,sorption is !nown as inert gas. In this e+periment concentrate & 'SO( is "se to a,sor, the mi+t"re .rom air. &ere Con. &'SO( is !nown as sol$ent an moist"re present in atm. Air is a,sor,e ,/ concentrate &'SO( 0sol$ent1. PROCEDURE: *. Arrange the clean appatat"s as shown in .igher. '. Ta!e * ml. sample o. Concentrate &'SO( an .in it2s Normalit/. 3. %ill the ."nnel with con. &'SO(. (. Start &'SO( .rom the pac!e col"mn an start ,lower a air s"ppl/ to col"mn. 4. 5hen all the aci .rom the ."nnel is collecte in recei$er# stop air s"ppl/. 6. Ta!e * ml. sample o. aci .rom the recei$er .las! an .in its Normalit/. PROCEDURE FOR ANALYSIS : Ta!e * ml. o. aci ,/ $ol"metric pipette into '4) ml. $ol"me .las!. A the water to the mar! an prepare '4) ml. il"te aci . Titrare this sol"tion with ).* N NaO&.

ABSORPTION

Chemical Engineering Department

OBSERVATION TABLE : sr no. amount o norma(&t* !."n NAo# o r$%u&r$' or '&(ut$ a)&' "!ML. o '&(ut$ a)&' norma(&t* o sam+($ ,M (&tr$

CALCU.ATION : ". Norma(&t* : N"V" / N0V0

0. 1m-L&t$r : 1m-L&t$r / Norma(&t* o $2tra)t$' 3E%. 4t o H0SO5

RESULT 6 CONCLUSION : -

ABSORPTION