ENSAYOS DE REPETIBILIDAD DEL MATERIAL VOLUMTRICO

Instrumento
Tipo
Capacidad, mL
Termmetro
Fluidez
Termmetro
Nube
Termmetro
PFE
Termmetro Viscosmetro
Termmetro
Horno
110
Termmetro
GC-FID
80
Cronmetro
Fluidez
Cronmetro
PFE
Cronmetro Viscosmetro
Densmetro
Densmetro
Sensor de temperatura
Probeta
PFE
100
Balanza
Analtica
30
Balanza
Analtica
5
Balanza
Analtica
1
Balanza
Analtica
0.1
Balanza
Analtica
0.5
Balanza
Analtica
0.2
Balanza
Platillo externo
200
Titulador
Automtico
Baln
Aforado
500
Pipeta
Aforada
2
Baln
Aforado
50
Baln
Aforado
25
Baln
Aforado
10
Pipeta
Aforada
8
Pipeta
Aforada
5
Micropipeta
Aforada
1
Microjeringa Graduada
100
Cromatgrafo GC-FID
Cromatgrafo GC-FID
Cromatgrafo GC-FID
Cromatgrafo GC-FID
Cromatgrafo GC-FID
Cromatgrafo GC-FID
Cromatgrafo GC-FID
Cromatgrafo GC-FID

Resolucin
1
1
0.1
0.1
0.1
0.1
0.01
0.01
0.01
0.1
0.01
1
0.0001
0.0001
0.0001
0.0001
0.0001
0.0001
0.01
0.001

Clase

MeOH

A
I
I
I
I
I
I
II
A
A
A
A
A
A
A
A

1
1
1
1
1
1
1
1

FAME
MeOH
GLI
GLI
GLI
GLI
GLI
GLI

Tolerancia
1
1
0.1
0.1
0.1
0.1
0.01
0.01
0.01
0.1
0.01
0.5
0.0001
0.0001
0.0001
0.0001
0.0001
0.0001
0.01
0.001
0.25
0.01
0.06
0.04
0.04
0.02
0.015
0.008
1
1
1
1
1
1
1
1
1

N 1
N 2
14.8
14.8
14.8
14.8
274.9 277
40
40
109.2 109.3
110 112.2
5.01
5.11
5.01
5.11
660.4 660.9
875.8 875.8
14.99
15
99.67 99.42
30
30
4.999
5
1.001
1
0.1
0.1
0.5
0.5
0.2
0.2
200
200
4.998 5.007
499.4 499.4
2.027 2.016
49.86 49.93
24.93 25.05
9.925 9.828
7.93 7.948
4.988 4.928
1.01
1.03
99.9 100.4
9763 10091
251
260
102.4 78.45
336.7 292.3
65.28 65.32
511.8 492.1
161.7 146.3
122.3 121.1

N 3
15
15
277.6
40.02
109.1
112.2
4.93
4.93
660.9
875.8
15
98.75
30
5
1
0.1
0.501
0.2
200
5.008
498.7
2.015
49.93
24.98
9.839
7.954
4.931
1.02
99
10436
256
106.1
315
63.33
504
171.6
98.53

N 4
15
15

N 5
15
15

N 6
15
15

N 7
15
15

N 8
14.8
14.8

N 9
15
15

N 10
14.8
14.8

40.03
113.1
110.1
5.05
5.05
660.2
875.8
15
99.66
30
5
0.999
0.1
0.5
0.2
200
5.006
499.8
2.013
49.94
25.03
9.829
7.934
4.911
1.04
99.9
10150
266
101.8
318.1
65.8
496.8
149.2
100.6

40
107.1
108.3
5.07
5.07
660.3
875.8
14.99
99.26
30
5.001
1
0.1
0.5
0.2
200
5.002
499.7
2.02
49.91
25.01
9.852
7.942
4.926
1.01
100.2
10243
282
109.3
346.1
59
463.9
167.6
99.43

40.03
111.6
103.5
4.98
4.98
660.7
875.9
15
99.2
30
4.999
0.999
0.1
0.5
0.2
200
5.004
499.4
2.036
49.91
25.03
9.881
7.935
4.945
1.03
99.7
10214
326
102.5
305.7
65.8
504
181.1
124.7

40
109.9
111.2
4.92
4.92
660.1
875.7
14.99
99.34
30
5
1
0.1
0.5
0.2
200
5.002
499.5
2.021
50
24.99
9.879
7.965
4.906
1.05
101
10235
277

39.99
109.7
110.5
5.07
5.07
660.5
875.8
15
99.14
30
5
0.999
0.1
0.5
0.2
200
5.008
499.7
2.016
49.89
24.96
9.813
7.883
4.933
1.02
99.6
10085
276

39.98
109.6
111.8
5.03
5.03
660.4
875.8
14.99
99.03
30
5
1
0.1
0.5
0.2
200
5.008
499.5
2.007
49.89
25.04
9.814
7.907
4.943
1.06
100.5
10079
266

39.97
105.1
110.1
4.98
4.98
660.2
15
98.905
29.998
5.0004
1.0002
0.0999
0.4995
0.1999
200.01
5.0033
499.34
2.0172
49.967
25.004
9.8422
7.9141
4.9353
1.03
99.5
10102

Promedio
14.92
14.92
276.5
40.002
109.37
109.99
5.015
5.015
660.46
875.8
14.996
99.2354027
29.99865
5.00005
0.99983
0.09997
0.49986
0.19997
200.005
5.00470253
499.439841
2.01870437
49.9229705
25.0034291
9.85017295
7.93110216
4.93461042
1.03
99.97
10139.8
273.333333
100.091575
318.993208
64.0870383
495.452155
162.894322
111.084622

Desviacin estndar
0.103279556
0.103279556
1.417744688
0.019888579
2.181258556
2.577013776
0.062583278
0.062583278
0.287518115
0.05
0.005163978
0.30112565
0.00136565
0.000540062
0.000646443
6.74949E-05
0.000343835
6.74949E-05
0.005270463
0.003240212
0.30402034
0.007786503
0.041048469
0.038930639
0.03514915
0.024321194
0.022566701
0.016329932
0.573585216
171.7703894
22.23173408
10.9783627
19.76841878
2.656119178
16.85148358
13.37282128
12.75421822

N Datos
10
10
3
10
10
10
10
10
10
9
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
9
6
6
6
6
6
6

Grupo

U calibracin

Unidad
C
C
C
C
C
C
s
s
s
Kg/m3
C
mL
g
g
g
g
g
U=9,44781E-5 g+5,017e-6 g* Wi
g
U=0,010494 g+1,077e-5 g* Wig
mL
mL
mL
mL
mL
mL
mL
mL
mL
uL
Cap = % m/m MeOHrea
Cap = % m/m MeOHrea
Cap = % m/m MeOHrea
Cap = % m/m MeOHrea
Cap = % m/m MeOHrea
Cap = % m/m MeOHrea
Cap = % m/m MeOHrea
Cap = % m/m MeOHrea

METODO
Columna2
Columna3
Columna4
Fluidez
Nube
PFE
Visc
Contam
MeOH
Fluidez
PFE
Visc
Densidad, API
Densidad, API
PFE
Gli
Yodo, NAcido, Humedad, Contam, FAME, Gli
NAcido
Humedad, MeOH
FAME
Yodo
Contam
Yodo, NAcido, Humedad
NAcido
NAcido, MEOH
FAME
MeOH, Gli
MeOH, Gli
Gli
MeOH, FAME
MeOH, Gli
Gli
FAME
MeOH
Gli
Butanetriol 30uL
Gli
Tricaprin 30uL
Gli
Gli Punto 2 de la curva
Gli
Mono Punto 2 de la curva
Gli
Dig Punto 2 de la curva
Gli
Trig Punto 2 de la curva