Automation Process

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- - Aut omat i on Templ at e Fi l e - - cr eat ed: 5- DEC- 2003 09: 50: 18
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METHOD Pr ot on I S ADVANCED
HELP " Pr ot on 10 - > - 0. 5 ppm"
GROUP Pr ot on I S
EXPERI MENT Pr ot on I S
EXTENSI ON " _PROTON"
SAMPLE_I D " " r unt i me
COMMENT " " r unt i me
SLOT 0 r unt i me
SOLVENT " " r unt i me
TEMPERATURE 25[ dC] r unt i me OFF r unt i me
PROCESSI NG " ~GLOBAL_PROCESS_LI ST/ 1dh_nocl i p. l i st "
EXP_FI LE
" ~GLOBAL_EXPERI MENT/ 1d/ si ngl e_pul se. exp" DO
pr ocess : = " " ;
pr ocess_copy : = FALSE;
aut omat i c : = TRUE;
aut o_gai n : = TRUE;
spi n_st at e : = " SPI N ON" ;
scans : = 16;
END EXPERI MENT;
PRESENTATI ON
" ~GLOBAL_TEMPLATE/ par ams_r i ght _r unt i me_pr ot on. pmt " FOR
[ 1] Pr ot on@_1, NULL_BOX, NULL_BOX;
END GROUP;
END METHOD;
METHOD Pr esat ur at i on I S ADVANCED
HELP " Pr ot on " ,
" Pr esat ur at i on of t al l est peak"
GROUP Pr esat ur at i on I S
SLOT 0 r unt i me
EXP_FI LE
1
pr ocess : = " " ;
scans : = 16;
END EXPERI MENT;
EXPERI MENT Pr esat ur at i on I S
EXTENSI ON " _PRESATURATI ON"
SLOT 0 r unt i me
EXP_FI LE
" ~GLOBAL_EXPERI MENT/ 1d/ si ngl e_pul se_homo_gat ed. exp" DO
pr ocess : = " " ;
i r r _at t enuat or : = 35[ dB] ;
r el axat i on_del ay : = 3[ s] ;
scans : = 16;
TAKE hi ghest _peak ASSI GN_TO i r r _of f set FROM
Pr ot on;
END EXPERI MENT;
PRESENTATI ON
" ~GLOBAL_TEMPLATE/ pr esat ur at i on_r unt i me. pmt " FOR
[ 1] Pr ot on@_1, [ 2] Pr esat ur at i on@_1, NULL_BOX,
NULL_BOX;
END GROUP;
END METHOD;
METHOD Car bon I S ADVANCED
HELP " Car bon 200 - > - 5 ppm"
GROUP Car bon I S
EXPERI MENT Car bon I S
EXTENSI ON " _CARBON"
SLOT 0 r unt i me
PROCESSI NG " ~GLOBAL_PROCESS_LI ST/ 1dc_nocl i p. l i st "
EXP_FI LE
" ~GLOBAL_EXPERI MENT/ 1d/ si ngl e_pul se_dec. exp" DO
pr ocess : = " " ;
2
sn_r at i o : = 20;
scans : = 1024;
END EXPERI MENT;
PRESENTATI ON
" ~GLOBAL_TEMPLATE/ par ams_r i ght _r unt i me_car bon. pmt " FOR
[ 1] Car bon@_1, NULL_BOX, NULL_BOX;
END GROUP;
END METHOD;
METHOD Pr ot on_and_Car bon I S ADVANCED
HELP " Pr ot on 10 - > - 0. 5 ppm" ,
" Car bon 200 - > - 5 ppm"
GROUP Pr ot on_and_Car bon I S
SLOT 0 r unt i me
EXP_FI LE
pr ocess : = " " ;
scans : = 16;
END EXPERI MENT;
SLOT 0 r unt i me
EXP_FI LE
pr ocess : = " " ;
sn_r at i o : = 20;
scans : = 1024;
END EXPERI MENT;
3
PRESENTATI ON
PRESENTATI ON
END GROUP;
END METHOD;
METHOD Car bon_and_Dept _135 I S ADVANCED
HELP " Car bon" ,
" Dept 135"
GROUP Car bon_and_Dept _135 I S
SLOT 0 r unt i me
EXP_FI LE
pr ocess : = " " ;
sn_r at i o : = 20;
scans : = 1024;
END EXPERI MENT;
EXPERI MENT Dept 135 I S
EXTENSI ON " _DEPT135"
SLOT 0 r unt i me
EXP_FI LE " ~GLOBAL_EXPERI MENT/ 1d/ dept _dec. exp"
DO
pr ocess : = " " ;
sn_r at i o : = 20;
scans : = 1024;
sel ect i on_angl e : = 135[ deg] ;
END EXPERI MENT;
PRESENTATI ON " ~GLOBAL_TEMPLATE/ c13_dept 135
4
_r unt i me. pmt " FOR
[ 1] Car bon@_1, [ 2] Dept 135@_1, NULL_BOX, NULL_BOX;
END GROUP;
END METHOD;
METHOD Car bon_and_APT I S ADVANCED
HELP " Car bon" ,
" APT"
GROUP Car bon_and_APT I S
SLOT 0 r unt i me
EXP_FI LE
pr ocess : = " " ;
sn_r at i o : = 20;
scans : = 1024;
END EXPERI MENT;
EXPERI MENT APT I S
EXTENSI ON " _APT"
SLOT 0 r unt i me
EXP_FI LE " ~GLOBAL_EXPERI MENT/ 1d/ apt . exp" DO
pr ocess : = " " ;
sn_r at i o : = 20;
scans : = 1024;
END EXPERI MENT;
[ 1] Car bon@_1, [ 2] APT@_1, NULL_BOX, NULL_BOX;
END GROUP;
END METHOD;
5
METHOD Edi t ed_DEPT I S ADVANCED
HELP " Car bon" ,
" wi t h sub spect r a showi ng CH, CH2 and CH3' s"
GROUP Edi t ed_DEPT EXECUTE " dept _aut omat i on" I S
SLOT 0 r unt i me
EXP_FI LE
pr ocess : = " " ;
sn_r at i o : = 20;
scans : = 1024;
END EXPERI MENT;
SLOT 0 r unt i me
DO
pr ocess : = " " ;
scans : = 1024;
sn_r at i o : = 0;
TAKE " scans/ 2" ASSI GN_TO scans CONSTRAI N 8,
x_sweep,
x_of f set FROM Car bon;
END EXPERI MENT;
SLOT 0 r unt i me
DO
pr ocess : = " " ;
6
TAKE r ecvr _gai n,
scans FROM Dept 45;
END EXPERI MENT;
SLOT 0 r unt i me
DO
pr ocess : = " " ;
TAKE r ecvr _gai n,
scans FROM Dept 45;
END EXPERI MENT;
END GROUP;
END METHOD;
METHOD Pr ot on_and_COSY I S ADVANCED
HELP " Pr ot on 10 - > - 0. 5" ,
" COSY w/ hi gh r es. pr ot on spect r a"
GROUP Pr ot on_and_COSY I S
SLOT 0 r unt i me
EXP_FI LE
pr ocess : = " " ;
scans : = 16;
END EXPERI MENT;
EXPERI MENT Cosy I S
EXTENSI ON " _COSY"
SLOT 0 r unt i me
7
PROCESSI NG
" ~GLOBAL_PROCESS_LI ST/ 2d_cosy_abs. l i st "
EXP_FI LE " ~GLOBAL_EXPERI MENT/ cosy/ cosy. exp" DO
pr ocess : = " " ;
spi n_st at e : = " SPI N OFF" ;
x_poi nt s : = 512;
y_poi nt s : = 128;
scans : = 8;
TAKE cl i p,
x_sweep,
x_of f set ,
r ecvr _gai n FROM Pr ot on;
END EXPERI MENT;
PRESENTATI ON
PRESENTATI ON " ~GLOBAL_TEMPLATE/ cosy_r unt i me. pmt " FOR
[ 1] Cosy@_1, [ 2] Pr ot on@_1, [ 3] Pr ot on@_1, NULL_BOX,
NULL_BOX, NULL_BOX;
END GROUP;
END METHOD;
METHOD Pr ot on_and_DQF_COSY I S ADVANCED
HELP " Pr ot on 10 - > - 0. 5" ,
" DQF- COSY w/ hi gh r es. pr ot on spect r a"
GROUP Pr ot on_and_DQF_COSY I S
SLOT 0 r unt i me
EXP_FI LE
pr ocess : = " " ;
scans : = 16;
END EXPERI MENT;
EXPERI MENT DQF_Cosy I S
EXTENSI ON " _DQFCOSY"
8
SLOT 0 r unt i me
PROCESSI NG
EXP_FI LE
" ~GLOBAL_EXPERI MENT/ dqf _cosy/ dqf _cosy. exp" DO
pr ocess : = " " ;
x_poi nt s : = 512;
y_poi nt s : = 128;
scans : = 16;
TAKE cl i p,
x_sweep,
x_of f set ,
END EXPERI MENT;
PRESENTATI ON
[ 1] DQF_Cosy@_1, [ 2] Pr ot on@_1, [ 3] Pr ot on@_1,
NULL_BOX, NULL_BOX, NULL_BOX;
END GROUP;
END METHOD;
METHOD Pr ot on_and_NOESY I S ADVANCED
HELP " Pr ot on 10 - > - 0. 5 ppm" ,
" NOESY w/ hi gh r es. pr ot on spect r a"
GROUP Pr ot on_and_NOESY I S
SLOT 0 r unt i me
EXP_FI LE
pr ocess : = " " ;
scans : = 16;
END EXPERI MENT;
9
EXPERI MENT Noesy I S
EXTENSI ON " _NOESY"
SLOT 0 r unt i me
PROCESSI NG
EXP_FI LE " ~GLOBAL_EXPERI MENT/ noesy/ noesy. exp"
DO
pr ocess : = " " ;
x_poi nt s : = 512;
y_poi nt s : = 128;
mi x_t i me : = 0. 5[ s] ;
scans : = 8;
TAKE cl i p,
x_sweep,
x_of f set ,
END EXPERI MENT;
PRESENTATI ON
[ 1] Noesy@_1, [ 2] Pr ot on@_1, [ 3] Pr ot on@_1,
END GROUP;
END METHOD;
METHOD Pr ot on_and_HOHAHA I S ADVANCED
HELP " Pr ot on 10 - > - 0. 5 ppm" ,
" HOHAHA ( Tocsy) w/ hi gh r es. pr ot on spect r a"
GROUP Pr ot on_and_HOHAHA I S
SLOT 0 r unt i me
EXP_FI LE
pr ocess : = " " ;
10
scans : = 16;
END EXPERI MENT;
EXPERI MENT Hohaha I S
EXTENSI ON " _HOHAHA"
SLOT 0 r unt i me
PROCESSI NG
EXP_FI LE " ~GLOBAL_EXPERI MENT/ t ocsy/ hohaha. exp"
DO
pr ocess : = " " ;
x_poi nt s : = 512;
y_poi nt s : = 128;
spi n_l ock_t i me : = 50[ ms] ;
scans : = 8;
TAKE cl i p,
x_sweep,
x_of f set ,
END EXPERI MENT;
PRESENTATI ON
[ 1] Hohaha@_1, [ 2] Pr ot on@_1, [ 3] Pr ot on@_1,
END GROUP;
END METHOD;
METHOD 1H_13C_CH_cor r el at i on I S ADVANCED
HELP " Pr ot on 10 - > - 0. 5" ,
" Car bon 200 - > - 5" ,
" CH cor r el at i on w/ hi gh r es. Car bon and pr ot on
spect r a"
GROUP 1H_13C_CH_cor r el at i on I S
SLOT 0 r unt i me
11
EXP_FI LE
pr ocess : = " " ;
scans : = 16;
END EXPERI MENT;
SLOT 0 r unt i me
EXP_FI LE
pr ocess : = " " ;
sn_r at i o : = 20;
scans : = 1024;
END EXPERI MENT;
EXPERI MENT Chcor r el at i on I S
EXTENSI ON " _CHCORRELATI ON"
SLOT 0 r unt i me
PROCESSI NG " ~GLOBAL_PROCESS_LI ST/ 2d_ch_abs. l i st "
EXP_FI LE " ~GLOBAL_EXPERI MENT/ het cor / chshf . exp"
DO
pr ocess : = " " ;
x_poi nt s : = 1024;
y_poi nt s : = 128;
scans : = 8;
TAKE cl i p,
x_sweep ASSI GN_TO y_sweep,
x_of f set ASSI GN_TO y_of f set FROM Pr ot on;
TAKE cl i p,
x_sweep,
x_of f set ,
r ecvr _gai n FROM Car bon;
END EXPERI MENT;
[ 1] Chcor r el at i on@_1, [ 2] Car bon@_1, [ 3] Pr ot on@_1,
PRESENTATI ON
12
PRESENTATI ON
END GROUP;
END METHOD;
METHOD 1H_13C_CH_l ong_r ange_cor r I S ADVANCED
HELP " Pr ot on 10 - > - 0. 5 ppm" ,
" Car bon 200 - > - 5 ppm" ,
" FLOCK w/ hi gh r es. car bon and pr ot on spect r a"
GROUP 1H_13C_CH_l ong_r ange_cor r I S
SLOT 0 r unt i me
EXP_FI LE
pr ocess : = " " ;
scans : = 16;
END EXPERI MENT;
SLOT 0 r unt i me
EXP_FI LE
pr ocess : = " " ;
sn_r at i o : = 20;
scans : = 1024;
END EXPERI MENT;
EXPERI MENT Fl ock I S
EXTENSI ON " _FLOCK"
13
SLOT 0 r unt i me
EXP_FI LE " ~GLOBAL_EXPERI MENT/ het cor / f l ock. exp"
DO
pr ocess : = " " ;
x_poi nt s : = 1024;
y_poi nt s : = 64;
scans : = 128;
l ong_r ange_j : = 7[ Hz] ;
TAKE cl i p,
TAKE cl i p,
x_sweep,
x_of f set ,
END EXPERI MENT;
[ 1] Fl ock@_1, [ 2] Car bon@_1, [ 3] Pr ot on@_1,
PRESENTATI ON
PRESENTATI ON
END GROUP;
END METHOD;
METHOD Combi nat i on_1 I S ADVANCED
HELP " Pr ot on" ,
" Car bon" ,
" Dept 135" ,
" COSY w/ hi gh r es. pr ot on spect r a" ,
" CH cor r el at i on w/ hi gh r es. car bon and pr ot on
spect r a"
GROUP 1H_13C_COSY_CH_cor r I S
SLOT 0 r unt i me
14
EXP_FI LE
pr ocess : = " " ;
scans : = 16;
END EXPERI MENT;
SLOT 0 r unt i me
EXP_FI LE
pr ocess : = " " ;
sn_r at i o : = 20;
scans : = 1024;
END EXPERI MENT;
SLOT 0 r unt i me
DO
pr ocess : = " " ;
sn_r at i o : = 20;
scans : = 1024;
END EXPERI MENT;
EXPERI MENT Cosy I S
EXTENSI ON " _COSY"
SLOT 0 r unt i me
PROCESSI NG
EXP_FI LE " ~GLOBAL_EXPERI MENT/ cosy/ cosy. exp" DO
pr ocess : = " " ;
15
x_poi nt s : = 512;
y_poi nt s : = 128;
scans : = 8;
TAKE cl i p,
x_sweep,
x_of f set ,
END EXPERI MENT;
EXPERI MENT CHcor r el at i on I S
EXTENSI ON " _CHCORRELATI ON"
SLOT 0 r unt i me
EXP_FI LE " ~GLOBAL_EXPERI MENT/ het cor / chshf . exp"
DO
pr ocess : = " " ;
x_poi nt s : = 1024;
y_poi nt s : = 128;
scans : = 8;
TAKE cl i p,
TAKE cl i p,
x_sweep,
x_of f set ,
END EXPERI MENT;
PRESENTATI ON
[ 1] Car bon@_1, [ 2] Dept 135@_1, NULL_BOX, NULL_BOX;
[ 1] Cosy@_1, [ 2] Pr ot on@_1, [ 3] Pr ot on@_1, NULL_BOX,
NULL_BOX, NULL_BOX;
[ 1] CHcor r el at i on@_1, [ 2] Car bon@_1, [ 3] Pr ot on@_1,
END GROUP;
END METHOD;
16

Automation Process

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