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Summary Report for GLC

Data
Compound

Peak
number

Area %

Cinnamon Bark Oil 0.5%

8.523

6.756

84.721

Cinnamon Leaf Oil 0.5%

Carvone 0.2%

Cinnamaldehyde 0.5%

Eugenol 0.5%

5.769

94.231

RT
1.2
5
2.5
9
4.8
6
4.7
5
8.6
5
1.4
5

100

1.916

98.084

2.447

97.553

2.6
7
4.8
2
4.7
8.6
3

Area
BC
912 01
723 01
9066
01
107 01
456 01
7448
01
7904
4338
01
4338
215 01
11006
01
11221
373 01
14870
01
15243

total

total

total

total

total

Calibration curve Data


Sample

R.T.

Peak Area

0.1% Cinnamaldehyde + 0.1%


Carvone (I.S.)

1.94

1745

Peak Area
Ratio
(PAR)
1.16

4.98
1.95

2032
1605

2.34

5.01
1.93

3757
1727

3.35

5
1.94

5788
1659

4.7

5.01
1.93

7804
1750

5.95

5.02

10407

0.2% Cinnamaldehyde + 0.1%


Carvone (I.S.)
0.3% Cinnamaldehyde + 0.1%
Carvone (I.S.)
0.4% Cinnamaldehyde + 0.1%
Carvone (I.S.)
0.5% Cinnamaldehyde + 0.1%
Carvone (I.S.)

Unknown Data

0.5% Cinnamon Bark Oil +


0.1% Carvone (I.S.)

1.34

156

1.65
1.93

522
1642

2.87
4.99

516
6462

Carvone
peak
Cinnamaldeh
yde peak

Discussion
Cinnamon Bark Oil 0.5% - Looking at the retention times for the cinnamon bark
oil I conclude that 84.721% of the compound is Cinnamaldehyde, 6.756% is
unknown and 8.523% is Carvone.
Cinnamon Leaf Oil 0.5% Looking at the retention times for cinnamon leaf oil I
conclude that 94.231% of the compound is Eugenol and 5.769% of the
compound is Cinnamaldehyde.

Using the data we can plot a calibration curve and we can compare the retention
times of the compound to identify our unknown percentage of Cinnamaldehyde
and our I.S.
0.5% Cinnamon Bark Oil + 0.1% Carvone (I.S.)
Retention Time 1.93 and 4.99 with 1642 and 6462 peak areas respectively, so
The Peak Area Ratio = 3.94
By using the calibration curve we can identify that the % Cinnamaldehyde in the
unknown is 0.34%.
Therefore in the cinnamon bark oil 0.5% it is 68% Cinnamaldehyde.