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Data
Compound
Peak
number
Area %
8.523
6.756
84.721
Carvone 0.2%
Cinnamaldehyde 0.5%
Eugenol 0.5%
5.769
94.231
RT
1.2
5
2.5
9
4.8
6
4.7
5
8.6
5
1.4
5
100
1.916
98.084
2.447
97.553
2.6
7
4.8
2
4.7
8.6
3
Area
BC
912 01
723 01
9066
01
107 01
456 01
7448
01
7904
4338
01
4338
215 01
11006
01
11221
373 01
14870
01
15243
total
total
total
total
total
R.T.
Peak Area
1.94
1745
Peak Area
Ratio
(PAR)
1.16
4.98
1.95
2032
1605
2.34
5.01
1.93
3757
1727
3.35
5
1.94
5788
1659
4.7
5.01
1.93
7804
1750
5.95
5.02
10407
Unknown Data
1.34
156
1.65
1.93
522
1642
2.87
4.99
516
6462
Carvone
peak
Cinnamaldeh
yde peak
Discussion
Cinnamon Bark Oil 0.5% - Looking at the retention times for the cinnamon bark
oil I conclude that 84.721% of the compound is Cinnamaldehyde, 6.756% is
unknown and 8.523% is Carvone.
Cinnamon Leaf Oil 0.5% Looking at the retention times for cinnamon leaf oil I
conclude that 94.231% of the compound is Eugenol and 5.769% of the
compound is Cinnamaldehyde.
Using the data we can plot a calibration curve and we can compare the retention
times of the compound to identify our unknown percentage of Cinnamaldehyde
and our I.S.
0.5% Cinnamon Bark Oil + 0.1% Carvone (I.S.)
Retention Time 1.93 and 4.99 with 1642 and 6462 peak areas respectively, so
The Peak Area Ratio = 3.94
By using the calibration curve we can identify that the % Cinnamaldehyde in the
unknown is 0.34%.
Therefore in the cinnamon bark oil 0.5% it is 68% Cinnamaldehyde.