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  • Experimental Procedure: o o o o o o o

    Transféré par

    Nicholas Cheong
    6 vues1 page
    A standard mixture containing 5% (v/v) each of benzene, cyclohexane, and toluene in diethyl ether is prepared in a 25 mL volumetric flask. The mixture is injected separately into a gas chromatography column to obtain standard chromatograms under suggested conditions of a nonpolar stationary phase, injection and detector temperatures of 250°C, carrier flow of 1 mL/min, and a temperature program ramping from 40°C to 170°C. The unknown sample is injected at 1000 μL using a syringe washed 3 times each with diethyl ether and the sample.

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    A standard mixture containing 5% (v/v) each of benzene, cyclohexane, and toluene in diethyl ether is prepared in a 25 mL volumetric flask. The mixture is injected separately into a gas chromatography column to obtain standard chromatograms under suggested conditions of a nonpolar stationary phase, injection and detector temperatures of 250°C, carrier flow of 1 mL/min, and a temperature program ramping from 40°C to 170°C. The unknown sample is injected at 1000 μL using a syringe washed 3 times each with diethyl ether and the sample.

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    © All Rights Reserved
    Téléchargez comme DOCX, PDF, TXT ou lisez en ligne sur Scribd
    Signaler comme contenu inapproprié
    6 vues1 page

    Experimental Procedure: o o o o o o o

    Transféré par

    Nicholas Cheong
    A standard mixture containing 5% (v/v) each of benzene, cyclohexane, and toluene in diethyl ether is prepared in a 25 mL volumetric flask. The mixture is injected separately into a gas chromatography column to obtain standard chromatograms under suggested conditions of a nonpolar stationary phase, injection and detector temperatures of 250°C, carrier flow of 1 mL/min, and a temperature program ramping from 40°C to 170°C. The unknown sample is injected at 1000 μL using a syringe washed 3 times each with diethyl ether and the sample.

    Droits d'auteur :

    © All Rights Reserved
    Téléchargez comme DOCX, PDF, TXT ou lisez en ligne sur Scribd
    Signaler comme contenu inapproprié
    sur 1

    Experimental Procedure

    1.

    25 mL volumetric flask is prepared for a mixture containing 5 (v / v % ) each of


    the benzene, cyclohexane and toluene in diethyl ether. Then, they are injected into
    the gas chromatography column seperately to obtain the standard chromotogram.

    2.
    The suggested chromatographic condition is stationary phase, nonpolar, injection
    temperature of 250 oC, detector temperature (250 oC),
    carrier flow of 1 mL/min, column temperature at 40 oC for 5 minutes, ramped
    to 60 oC with 2 oC/min and ramped
    to 170 oC with 10 oC/min which hold for
    5 minutes.
    3.
    The injection volume is fixed to 1000 mL and the syringe is washed for
    3 times with
    diethyl ether and 3 time with unknown sample and
    pumped 6 times for injection.

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