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....................................................... 1
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29 Istilah dan definisi.........................................................

..................................................... 1
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29 Cara uji.....................................................................
......................................................... 1
\par}{\phpg\posx2463\pvpg\posy3295\absw8550\absh4063 \sl-356 \f10 \fs18 \cf0 \fi
172 Prinsip.....................................................................
........................................................ 1
\par}{\phpg\posx2463\pvpg\posy3295\absw8550\absh4063 \sl-357 \f10 \fs18 \cf0 \fi
172 Bahan ......................................................................
....................................................... 2
\par}{\phpg\posx2463\pvpg\posy3295\absw8550\absh4063 \sl-356 \f10 \fs18 \cf0 \fi
172 Peralatan ..................................................................
...................................................... 2
\par}{\phpg\posx2463\pvpg\posy3295\absw8550\absh4063 \sl-357 \f10 \fs18 \cf0 \fi
172 Persiapan pengujian.........................................................
.............................................. 3
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172 Prosedur ...................................................................
...................................................... 3
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172 Perhitungan ................................................................
.................................................... 4
\par}{\phpg\posx2463\pvpg\posy3295\absw8550\absh4063 \sl-356 \f10 \fs18 \cf0 Jam
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............................. 5
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172 Jaminan mutu ...............................................................
.................................................. 5
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172 Pengendalian mutu...........................................................
.............................................. 5
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{\phpg\posx2118\pvpg\posy2580\absw8967\absh4276 \f10 \fs18 \cf0 \f10 \fs18 \cf0
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88 tentang
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{\phpg\posx2118\pvpg\posy3402\absw8950\absh636 \f10 \fs18 \cf0 \f10 \fs18 \cf0 M

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{\phpg\posx2118\pvpg\posy806\absw2082\absh207 \b \f10 \fs18 \cf0 \b \f10 \fs18 \
cf0 SNI 06-6989.22-2004 \par
}
{\phpg\posx2118\pvpg\posy1607\absw6257\absh770 \f10 \fs18 \cf0 \f10 \fs18 \cf0 a
) Reaksi oksidasi KMnO {\dn006 \fs11 4} dalam kondisi asam sebagai berikut :
\par}{\phpg\posx2118\pvpg\posy1607\absw6257\absh770 \sl-155 \par\f10 \fs18 \cf0
\fi807 2 KMnO {\dn006 \fs11 4} + 3 H {\dn006 \fs11 2}SO{\dn006 \fs11 4 }
\par}{\phpg\posx2118\pvpg\posy1607\absw6257\absh770 \sl-284 \f10 \fs18 \cf0 b)
Oksidasi KMnO4 dalam kondisi basa sebagai berikut : \par
}
{\phpg\posx5984\pvpg\posy1920\absw2556\absh277 \f10 \fs18 \cf0 \f10 \fs18 \cf0 2
MnSO {\dn006 \fs11 4} + K {\dn006 \fs11 2}SO{\dn006 \fs11 4} + 5 O{\dn00
6 \fs11 n }\par
}
{\phpg\posx2925\pvpg\posy2546\absw1644\absh228 \f10 \fs18 \cf0 \f10 \fs18 \cf0 2
KMnO{\dn006 \fs11 4} + H {\dn006 \fs11 2}O \par
}
{\phpg\posx5620\pvpg\posy2546\absw765\absh228 \f10 \fs18 \cf0 \f10 \fs18 \cf0 2
MnO{\dn006 \fs11 2 }\par
}
{\phpg\posx6486\pvpg\posy2546\absw2448\absh266 \f10 \fs18 \cf0 \f10 \fs18 \cf0 +
KOH + 3 O {\dn006 \fs11 n} + 3 H {\dn006 \fs11 2}O \par
}
{\phpg\posx2118\pvpg\posy2858\absw6158\absh207 \f10 \fs18 \cf0 \f10 \fs18 \cf0 c
) Zat organik dapat dioksidasi dengan reaksi sebagai berikut : \par
}
{\phpg\posx5266\pvpg\posy3173\absw1336\absh245 \f10 \fs18 \cf0 \f10 \fs18 \cf0 2
CO {\dn006 \fs11 2} + H {\dn006 \fs11 2}O \par
}
{\phpg\posx2128\pvpg\posy3649\absw342\absh207 \b \f10 \fs18 \cf0 \b \f10 \fs18 \
cf0 3.2 \par
}
{\phpg\posx2651\pvpg\posy3173\absw1490\absh636 \f10 \fs18 \cf0 \fi273 \f10 \fs18
\cf0 C {\dn006 \fs11 2}H {\dn006 \fs11 2}O + O{\dn006 \fs11 n }
\par}{\phpg\posx2651\pvpg\posy3173\absw1490\absh636 \sl-224 \par\f10 \fs18 \cf0
{\b Bahan }\par
}
{\phpg\posx2108\pvpg\posy4146\absw8991\absh2912 \b \f10 \fs18 \cf0 \fi29 \b \f10
\fs18 \cf0 3.2.1
Asam sulfat, H {\dn006 \fs11 2}SO{\dn006 \fs11 4} 8 N yan
g bebas zat organik
\par}{\phpg\posx2108\pvpg\posy4146\absw8991\absh2912 \sl-238 \par\b \f10 \fs18 \
cf0 {\b0 a)}{\b0
Pindahkan}{\b0 222}{\b0 mL}{\b0 H}{\b0\dn006 \fs11 2}{\
b0 SO }{\b0\dn006 \fs11 4}{\b0 pekat}{\b0 sedikit}{\b0 demi}{\b0 sedikit}{\
b0 ke}{\b0 dalam}{\b0 500}{\b0 mL}{\b0 air}{\b0 suling}{\b0 dalam }
\par}{\phpg\posx2108\pvpg\posy4146\absw8991\absh2912 \sl-208 \b \f10 \fs18 \cf0

\fi346 {\b0 gelas}{\b0 piala}{\b0 sambil}{\b0 didinginkan}{\b0 dan}{\b0 enc

erkan}{\b0 sampai}{\b0 1000}{\b0 mL}{\b0 dalam}{\b0 labu}{\b0 ukur}{\b0 1
000}{\b0 mL. }
\par}{\phpg\posx2108\pvpg\posy4146\absw8991\absh2912 \sl-171 \par\b \f10 \fs18 \
cf0 {\b0 b)}{\b0
Pindahkan}{\b0 kembali}{\b0 ke}{\b0 dalam}{\b0 gelas
}{\b0 piala}{\b0 dan}{\b0 tetesi}{\b0 dengan}{\b0 larutan}{\b0 KMnO}
{\b0\dn006 \fs11 4}{\b0 sampai }
\par}{\phpg\posx2108\pvpg\posy4146\absw8991\absh2912 \sl-209 \b \f10 \fs18 \cf0
\fi346 {\b0 berwarna}{\b0 merah}{\b0 muda. }
\par}{\phpg\posx2108\pvpg\posy4146\absw8991\absh2912 \sl-219 \b \f10 \fs18 \cf0
\fi3290 {\b0 \fs11 0 }
\par}{\phpg\posx2108\pvpg\posy4146\absw8991\absh2912 \sl-185 \b \f10 \fs18 \cf0
{\b0 c)}{\b0
Panaskan}{\b0 pada}{\b0 temperatur}{\b0 80}{\b0 C}{\b0
selama}{\b0 10}{\b0 menit,}{\b0 bila}{\b0 warna}{\b0 merah}{\b0 hila
ng}{\b0 selama }
\par}{\phpg\posx2108\pvpg\posy4146\absw8991\absh2912 \sl-265 \b \f10 \fs18 \cf0
\fi347 {\b0 pemanasan}{\b0 tambah}{\b0 kembali}{\b0 larutan}{\b0 KMnO }{\b0\
dn006 \fs11 4}{\b0 0,01}{\b0 N}{\b0 sampai}{\b0 warna}{\b0 merah}{\b0 mud
a}{\b0 stabil. }
\par}{\phpg\posx2108\pvpg\posy4146\absw8991\absh2912 \sl-224 \par\b \f10 \fs18 \
cf0 3.2.2
Kalium permanganat, KMnO4 0,1 N
\par}{\phpg\posx2108\pvpg\posy4146\absw8991\absh2912 \sl-252 \par\b \f10 \fs18 \
cf0 {\b0 Larutkan}{\b0 3,16}{\b0 g}{\b0 KMnO }{\b0\dn006 \fs11 4}{\b0 d
engan}{\b0 air}{\b0 suling}{\b0 dalam}{\b0 labu}{\b0 ukur}{\b0 1000}
{\b0 mL.}{\b0 Simpan}{\b0 dalam}{\b0 botol }
\par}{\phpg\posx2108\pvpg\posy4146\absw8991\absh2912 \sl-208 \b \f10 \fs18 \cf0
{\b0 gelap}{\b0 selama}{\b0 24}{\b0 jam}{\b0 sebelum}{\b0 digunakan. }\par
}
{\phpg\posx2118\pvpg\posy7628\absw530\absh207 \b \f10 \fs18 \cf0 \b \f10 \fs18 \
cf0 3.2.3 \par
}
{\phpg\posx2815\pvpg\posy7628\absw3710\absh235 \b \f10 \fs18 \cf0 \b \f10 \fs18
\cf0 Kalium permanganat, KMnO {\dn006 \fs11 4} 0,01 N \par
}
{\phpg\posx2118\pvpg\posy8105\absw8914\absh240 \f10 \fs18 \cf0 \f10 \fs18 \cf0 P
ipet 10 mL KMnO {\dn006 \fs11 4} 0,1 N masukkan ke dalam labu ukur 100 mL, tepa
tkan dengan air suling \par
}
{\phpg\posx2118\pvpg\posy8343\absw1808\absh207 \f10 \fs18 \cf0 \f10 \fs18 \cf0 s
ampai tanda tera. \par
}
{\phpg\posx2118\pvpg\posy8819\absw530\absh207 \b \f10 \fs18 \cf0 \b \f10 \fs18 \
cf0 3.2.4 \par
}
{\phpg\posx2816\pvpg\posy8819\absw3545\absh246 \b \f10 \fs18 \cf0 \b \f10 \fs18
\cf0 Asam oksalat, (COOH) {\dn006 \fs11 2}.2H {\dn006 \fs11 2}O 0,1 N \par
}
{\phpg\posx2118\pvpg\posy9295\absw8925\absh497 \f10 \fs18 \cf0 \f10 \fs18 \cf0 L
arutkan 6,302 g (COOH){\dn006 \fs11 2}.2H {\dn006 \fs11 2}O dalam 1000 m
L air suling atau larutkan 6,7 g natrium
\par}{\phpg\posx2118\pvpg\posy9295\absw8925\absh497 \sl-237 \f10 \fs18 \cf0 oksa
lat, (COONa){\dn006 \fs11 2}.2H {\dn006 \fs11 2}O dalam 25 mL H {\dn006 \fs11
2}SO {\dn006 \fs11 4} 6 N, dinginkan dan encerkan sampai 1000 mL \par
}
{\phpg\posx2118\pvpg\posy9770\absw1661\absh207 \f10 \fs18 \cf0 \f10 \fs18 \cf0 d
alam labu takar. \par
}
{\phpg\posx2118\pvpg\posy10247\absw530\absh207 \b \f10 \fs18 \cf0 \b \f10 \fs18
\cf0 3.2.5 \par
}

{\phpg\posx2816\pvpg\posy10247\absw2062\absh207 \b \f10 \fs18 \cf0 \b \f10 \fs18

\cf0 Asam oksalat 0,01 N \par
}
{\phpg\posx2118\pvpg\posy10723\absw8942\absh422 \f10 \fs18 \cf0 \f10 \fs18 \cf0
Pipet 10 mL larutan asam oksalat 0,1 N masukkan ke dalam labu ukur
100 mL, tepatkan
\par}{\phpg\posx2118\pvpg\posy10723\absw8942\absh422 \sl-238 \f10 \fs18 \cf0 den
gan air suling sampai tanda tera. \par
}
{\phpg\posx2118\pvpg\posy11437\absw530\absh636 \b \f10 \fs18 \cf0 \b \f10 \fs18
\cf0 3.2.6
\par}{\phpg\posx2118\pvpg\posy11437\absw530\absh636 \sl-238 \par\b \f10 \fs18 \c
f0 {\i 3.3 }\par
}
{\phpg\posx2646\pvpg\posy11437\absw3465\absh636 \b \f10 \fs18 \cf0 \fi169 \b \f1
0 \fs18 \cf0 Natrium oksalat (COONa)22H{\dn006 \fs11 2}O
\par}{\phpg\posx2646\pvpg\posy11437\absw3465\absh636 \sl-224 \par\b \f10 \fs18 \
cf0 Peralatan \par
}
{\phpg\posx2118\pvpg\posy12411\absw3446\absh2458 \f10 \fs18 \cf0 \f10 \fs18 \cf0
a) erlenmeyer 300 mL;
\par}{\phpg\posx2118\pvpg\posy12411\absw3446\absh2458 \sl-236 \f10 \fs18 \cf0 b)
labu ukur 1000 mL dan 100 mL;
\par}{\phpg\posx2118\pvpg\posy12411\absw3446\absh2458 \sl-238 \f10 \fs18 \cf0 {\
i c)}{\i
stop}{\i watch; }
\par}{\phpg\posx2118\pvpg\posy12411\absw3446\absh2458 \sl-237 \f10 \fs18 \cf0 d)
pemanas listrik;
\par}{\phpg\posx2118\pvpg\posy12411\absw3446\absh2458 \sl-238 \f10 \fs18 \cf0 e)
gelas ukur 5 mL;
\par}{\phpg\posx2118\pvpg\posy12411\absw3446\absh2458 \sl-237 \f10 \fs18 \cf0 f)
pipet ukur 10 mL dan 100 mL;
\par}{\phpg\posx2118\pvpg\posy12411\absw3446\absh2458 \sl-237 \f10 \fs18 \cf0 g)
gelas piala 1000 mL;
\par}{\phpg\posx2118\pvpg\posy12411\absw3446\absh2458 \sl-238 \f10 \fs18 \cf0 h)
buret 25 mL; dan
\par}{\phpg\posx2118\pvpg\posy12411\absw3446\absh2458 \sl-237 \f10 \fs18 \cf0 i)
termometer.
\par}{\phpg\posx2118\pvpg\posy12411\absw3446\absh2458 \sl-300 \par\f10 \fs18 \cf
0 {\b \fs16 2}{\b \fs16 dari}{\b \fs16 6 }\par
}
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{\phpg\posx8676\pvpg\posy806\absw2082\absh207 \b \f10 \fs18 \cf0 \b \f10 \fs18 \
cf0 SNI 06-6989.22-2004 \par
}
{\phpg\posx2118\pvpg\posy1607\absw342\absh207 \b \f10 \fs18 \cf0 \b \f10 \fs18 \
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{\phpg\posx2636\pvpg\posy1607\absw2172\absh207 \b \f10 \fs18 \cf0 \b \f10 \fs18
\cf0 Persiapan pengujian \par
}
{\phpg\posx2118\pvpg\posy2103\absw8977\absh2872 \f10 \fs18 \cf0 \f10 \fs18 \cf0
Penetapan larutan kalium permanganat, KMnO {\dn006 \fs11 4} 0,01 N dengan tahap
an sebagai berikut:

\par}{\phpg\posx2118\pvpg\posy2103\absw8977\absh2872 \sl-223 \par\f10 \fs18 \cf0

a)
Pipet 100 mL air suling secara duplo dan masukkan ke dalam labu erlenmey
er 300 mL,
\par}{\phpg\posx2118\pvpg\posy2103\absw8977\absh2872 \sl-144 \f10 \fs18 \cf0 \fi
2265 {\fs11 0 }
\par}{\phpg\posx2118\pvpg\posy2103\absw8977\absh2872 \sl-186 \f10 \fs18 \cf0 \fi
400 panaskan hingga 70 C.
\par}{\phpg\posx2118\pvpg\posy2103\absw8977\absh2872 \sl-170 \par\f10 \fs18 \cf0
b)
Tambahkan 5 mL H {\dn006 \fs11 2}SO {\dn006 \fs11 4} 8 N yang bebas zat
organik.
\par}{\phpg\posx2118\pvpg\posy2103\absw8977\absh2872 \sl-285 \f10 \fs18 \cf0 c)
Tambahkan 10 mL larutan baku asam oksalat 0,01 N menggunakan pipet volume.
\par}{\phpg\posx2118\pvpg\posy2103\absw8977\absh2872 \sl-311 \f10 \fs18 \cf0 d)
Titrasi dengan larutan kalium permanganat 0.01 N sampai warna merah muda dan
catat
\par}{\phpg\posx2118\pvpg\posy2103\absw8977\absh2872 \sl-238 \f10 \fs18 \cf0 \fi
400 volume pemakaian.
\par}{\phpg\posx2118\pvpg\posy2103\absw8977\absh2872 \sl-311 \f10 \fs18 \cf0 e)
Hitung normalitas larutan baku kalium permanganat dengan menggu
nakan rumus
\par}{\phpg\posx2118\pvpg\posy2103\absw8977\absh2872 \sl-238 \f10 \fs18 \cf0 \fi
400 sebagai berikut:
\par}{\phpg\posx2118\pvpg\posy2103\absw8977\absh2872 \sl-252 \par\f10 \fs18 \cf0
\fi1653 N{\dn006 \fs11 2} = V {\dn006 \fs11 1} x N{\dn006 \fs11 1 }\par
}
{\phpg\posx4439\pvpg\posy5261\absw226\absh224 \f10 \fs18 \cf0 \f10 \fs18 \cf0 V{
\dn006 \fs11 2 }\par
}
{\phpg\posx2517\pvpg\posy5499\absw1857\absh207 \f10 \fs18 \cf0 \f10 \fs18 \cf0 d
engan pengertian: \par
}
{\phpg\posx2517\pvpg\posy5813\absw246\absh1069 \f10 \fs18 \cf0 \f10 \fs18 \cf0 V
{\dn006 \fs11 1 }
\par}{\phpg\posx2517\pvpg\posy5813\absw246\absh1069 \sl-314 \f10 \fs18 \cf0 N{\d
n006 \fs11 1 }
\par}{\phpg\posx2517\pvpg\posy5813\absw246\absh1069 \sl-311 \f10 \fs18 \cf0 V{\d
n006 \fs11 2 }
\par}{\phpg\posx2517\pvpg\posy5813\absw246\absh1069 \sl-313 \f10 \fs18 \cf0 N{\d
n006 \fs11 2 }\par
}
{\phpg\posx2965\pvpg\posy5813\absw7433\absh1052 \f10 \fs18 \cf0 \f10 \fs18 \cf0
adalah mL larutan baku asam oksalat;
\par}{\phpg\posx2965\pvpg\posy5813\absw7433\absh1052 \sl-313 \f10 \fs18 \cf0 ada
lah normalitas larutan baku asam oksalat yang dipergunakan untuk titrasi;
\par}{\phpg\posx2965\pvpg\posy5813\absw7433\absh1052 \sl-313 \f10 \fs18 \cf0 ada
lah mL larutan baku kalium permanganat; dan
\par}{\phpg\posx2965\pvpg\posy5813\absw7433\absh1052 \sl-312 \f10 \fs18 \cf0 ada
lah normalitas larutan baku kalium permanganat yang tidak dicari. \par
}
{\phpg\posx2128\pvpg\posy7227\absw342\absh207 \b \f10 \fs18 \cf0 \b \f10 \fs18 \
cf0 3.5 \par
}
{\phpg\posx2651\pvpg\posy7227\absw1063\absh207 \b \f10 \fs18 \cf0 \b \f10 \fs18
\cf0 Prosedur \par
}
{\phpg\posx2118\pvpg\posy7725\absw8956\absh1910 \f10 \fs18 \cf0 \f10 \fs18 \cf0
Uji nilai permanganat dengan tahapan sebagai berikut:
\par}{\phpg\posx2118\pvpg\posy7725\absw8956\absh1910 \sl-238 \par\f10 \fs18 \cf0
a) Pipet 100 mL contoh uji masukkan ke dalam erlenmeyer 300 mL dan tambahkan
3 butir

\par}{\phpg\posx2118\pvpg\posy7725\absw8956\absh1910 \sl-237 \f10 \fs18 \cf0 \fi

337 batu didih.
\par}{\phpg\posx2118\pvpg\posy7725\absw8956\absh1910 \sl-313 \f10 \fs18 \cf0 b)
Tambahkan KMnO4 0,01 N beberapa tetes ke dalam contoh uji hingga t
erjadi warna
\par}{\phpg\posx2118\pvpg\posy7725\absw8956\absh1910 \sl-238 \f10 \fs18 \cf0 \fi
337 merah muda.
\par}{\phpg\posx2118\pvpg\posy7725\absw8956\absh1910 \sl-313 \f10 \fs18 \cf0 c)
Tambahkan 5 ml asam sulfat 8 N bebas zat organik.
\par}{\phpg\posx2118\pvpg\posy7725\absw8956\absh1910 \sl-313 \f10 \fs18 \cf0 d)
Panaskan di atas pemanas listrik pada suhu 105 C 2 C, bila terdapa
t bau H S, \par
}
{\phpg\posx7336\pvpg\posy9592\absw73\absh132 \f10 \fs11 \cf0 \f10 \fs11 \cf0 o \
par
}
{\phpg\posx8025\pvpg\posy9592\absw110\absh132 \f10 \fs11 \cf0 \f10 \fs11 \cf0 O
\par
}
{\phpg\posx10384\pvpg\posy9714\absw73\absh132 \f10 \fs11 \cf0 \f10 \fs11 \cf0 2
\par
}
{\phpg\posx2118\pvpg\posy9855\absw7169\absh1335 \f10 \fs18 \cf0 \fi337 \f10 \fs1
8 \cf0 pendidihan diteruskan beberapa menit.
\par}{\phpg\posx2118\pvpg\posy9855\absw7169\absh1335 \sl-171 \par\f10 \fs18 \cf0
e) Pipet 10 mL larutan baku KMnO {\dn006 \fs11 4} 0,01 N.
\par}{\phpg\posx2118\pvpg\posy9855\absw7169\absh1335 \sl-284 \f10 \fs18 \cf0 f)
Panaskan hingga mendidih selama 10 menit.
\par}{\phpg\posx2118\pvpg\posy9855\absw7169\absh1335 \sl-313 \f10 \fs18 \cf0 g)
Pipet 10 mL larutan baku asam oksalat 0,01 N.
\par}{\phpg\posx2118\pvpg\posy9855\absw7169\absh1335 \sl-313 \f10 \fs18 \cf0 h)
Titrasi dengan kalium permanganat 0,01 N hingga warna merah muda. \par
}
{\phpg\posx2118\pvpg\posy11422\absw140\absh488 \f10 \fs18 \cf0 \f10 \fs18 \cf0 i
)
\par}{\phpg\posx2118\pvpg\posy11422\absw140\absh488 \sl-312 \f10 \fs18 \cf0 j) \
par
}
{\phpg\posx2128\pvpg\posy12450\absw342\absh207 \b \f10 \fs18 \cf0 \b \f10 \fs18
\cf0 3.6 \par
}
{\phpg\posx2456\pvpg\posy11422\absw8515\absh1132 \f10 \fs18 \cf0 \f10 \fs18 \cf0
Catat volume pemakaian KMnO{\dn006 \fs11 4}.
\par}{\phpg\posx2456\pvpg\posy11422\absw8515\absh1132 \sl-284 \f10 \fs18 \cf0 Ap
abila pemakaian larutan baku kalium permanganat 0,01 N lebih dari 7 m
L, ulangi
\par}{\phpg\posx2456\pvpg\posy11422\absw8515\absh1132 \sl-238 \f10 \fs18 \cf0 pe
ngujian dengan cara mengencerkan contoh uji.
\par}{\phpg\posx2456\pvpg\posy11422\absw8515\absh1132 \sl-238 \par\f10 \fs18 \cf
0 \fi189 {\b Perhitungan }\par
}
{\phpg\posx2117\pvpg\posy12948\absw5249\absh880 \b \f10 \fs18 \cf0 \fi20 \b \f10
\fs18 \cf0 3.6.1 Nilai permanganat
\par}{\phpg\posx2117\pvpg\posy12948\absw5249\absh880 \sl-245 \par\b \f10 \fs18 \
cf0 \fi1843 {\b0 \f40 [}{\b0 (10}{\b0 -}{\b0 a)b}{\b0 -}{\b0 (10}{\b0 x}{\b
0 c)}{\b0 \f40 ]}{\b0 1}{\b0 x}{\b0 31,6}{\b0 x}{\b0 1000 }
\par}{\phpg\posx2117\pvpg\posy12948\absw5249\absh880 \sl-266 \b \f10 \fs18 \cf0
{\b0 KMnO }{\b0\dn006 \fs11 4}{\b0 mg/l}{\b0 = }\par
}
{\phpg\posx5284\pvpg\posy13915\absw146\absh207 \f10 \fs18 \cf0 \f10 \fs18 \cf0 d

\par
}
{\phpg\posx7667\pvpg\posy13676\absw251\absh207 \f10 \fs18 \cf0 \f10 \fs18 \cf0 x
f \par
}
{\phpg\posx2118\pvpg\posy14932\absw693\absh189 \b \f10 \fs16 \cf0 \b \f10 \fs16
\cf0 3 dari 6 \par
}
{\shp\shpfhdr0\shpbxpage\shpbypage\shpfblwtxt1\shpz0
\shpleft4168\shptop5253\shpright4845\shpbottom5253
{\*\shpinst {\sp{\sn shapeType}{\sv 20}}
{\sp{\sn fFlipH}{\sv 0}}{\sp{\sn fFlipV}{\sv 0}}
{\sp{\sn LineWidth}{\sv 14}}
{\sp{\sn fBehindDocument}{\sv 1}}{\sp{\sn lineColor}{\sv
65793}}}}
\sect\sectd\pard\plain
\pgwsxn12240\pghsxn15840
{\shp\shpfhdr0\shpbxpage\shpbypage\shpfblwtxt1\shpz0
\shpleft3751\shptop7462\shpright4722\shpbottom7464
{\*\shpinst {\sp{\sn shapeType}{\sv 20}}
{\sp{\sn fFlipH}{\sv 0}}{\sp{\sn fFlipV}{\sv 0}}
{\sp{\sn LineWidth}{\sv 14}}
{\sp{\sn fBehindDocument}{\sv 1}}{\sp{\sn lineColor}{\sv
65793}}}}
{\phpg\posx2118\pvpg\posy806\absw2082\absh207 \b \f10 \fs18 \cf0 \b \f10 \fs18 \
cf0 SNI 06-6989.22-2004 \par
}
{\phpg\posx2118\pvpg\posy1607\absw1857\absh207 \f10 \fs18 \cf0 \f10 \fs18 \cf0 d
engan pengertian: \par
}
{\phpg\posx2118\pvpg\posy1920\absw146\absh1335 \f10 \fs18 \cf0 \f10 \fs18 \cf0 a
\par}{\phpg\posx2118\pvpg\posy1920\absw146\absh1335 \sl-312 \f10 \fs18 \cf0 b
\par}{\phpg\posx2118\pvpg\posy1920\absw146\absh1335 \sl-314 \f10 \fs18 \cf0 c
\par}{\phpg\posx2118\pvpg\posy1920\absw146\absh1335 \sl-311 \f10 \fs18 \cf0 d
\par}{\phpg\posx2118\pvpg\posy1920\absw146\absh1335 \sl-314 \f10 \fs18 \cf0 f \p
ar
}
{\phpg\posx2626\pvpg\posy1920\absw5640\absh1335 \f10 \fs18 \cf0 \f10 \fs18 \cf0
adalah volume KMnO {\dn006 \fs11 4} 0,01 N yang dibutuhkan pada titrasi;
\par}{\phpg\posx2626\pvpg\posy1920\absw5640\absh1335 \sl-313 \f10 \fs18 \cf0 ada
lah normalitas KMnO {\dn006 \fs11 4} yang sebenarnya;
\par}{\phpg\posx2626\pvpg\posy1920\absw5640\absh1335 \sl-285 \f10 \fs18 \cf0 ada
lah normalitas asam oksalat;
\par}{\phpg\posx2626\pvpg\posy1920\absw5640\absh1335 \sl-311 \f10 \fs18 \cf0 ada
lah volume contoh; dan
\par}{\phpg\posx2626\pvpg\posy1920\absw5640\absh1335 \sl-314 \f10 \fs18 \cf0 ada
lah faktor pengenceran contoh uji. \par
}
{\phpg\posx2118\pvpg\posy3647\absw879\absh189 \f10 \fs17 \cf0 \f10 \fs17 \cf0 CA
TATAN \par
}
{\phpg\posx2118\pvpg\posy4103\absw530\absh207 \b \f10 \fs18 \cf0 \b \f10 \fs18 \
cf0 3.6.2 \par
}
{\phpg\posx3205\pvpg\posy3647\absw7054\absh231 \f10 \fs17 \cf0 \f10 \fs17 \cf0 A
pabila terdapat nitrit maka nilai KMnO{\dn006 \fs11 4} dikurangi 1,4 mg/L untuk
kadar nitrit 1 mg/L. \par
}
{\phpg\posx2816\pvpg\posy4103\absw4567\absh1097 \b \f10 \fs18 \cf0 \b \f10 \fs18
\cf0 Perhitungan{\i Relatif}{\i Percent}{\i Different} (RPD)
\par}{\phpg\posx2816\pvpg\posy4103\absw4567\absh1097 \sl-252 \par\b \f10 \fs18 \

cf0 \fi1334 {\b0 (X }{\b0\dn006 \fs11 1}{\b0 -}{\b0 X}{\b0\dn006 \fs11 2}{\b
0 ) }
\par}{\phpg\posx2816\pvpg\posy4103\absw4567\absh1097 \sl-208 \b \f10 \fs18 \cf0
\fi92 {\b0 RPD}{\b0
=}{\b0
----------------------}{\b0 x}{\b0 100}{\b0
% }
\par}{\phpg\posx2816\pvpg\posy4103\absw4567\absh1097 \sl-266 \b \f10 \fs18 \cf0
\fi1334 {\b0 (X}{\b0\dn006 \fs11 1}{\b0 -}{\b0 X}{\b0\dn006 \fs11 2}{\b0 )/2
}\par
}
{\phpg\posx2118\pvpg\posy5531\absw1857\absh207 \f10 \fs18 \cf0 \f10 \fs18 \cf0 d
engan pengertian: \par
}
{\phpg\posx2117\pvpg\posy5844\absw530\absh918 \f10 \fs18 \cf0 \f10 \fs18 \cf0 X{
\dn006 \fs11 1 }
\par}{\phpg\posx2117\pvpg\posy5844\absw530\absh918 \sl-314 \f10 \fs18 \cf0 X{\dn
006 \fs11 2 }
\par}{\phpg\posx2117\pvpg\posy5844\absw530\absh918 \sl-223 \par\f10 \fs18 \cf0 {
\b 3.6.3 }\par
}
{\phpg\posx2626\pvpg\posy5844\absw4488\absh1330 \f10 \fs18 \cf0 \f10 \fs18 \cf0
adalah hasil analisis pada penentuan pertama;
\par}{\phpg\posx2626\pvpg\posy5844\absw4488\absh1330 \sl-314 \f10 \fs18 \cf0 ada
lah hasil analisis pada penentuan kedua.
\par}{\phpg\posx2626\pvpg\posy5844\absw4488\absh1330 \sl-237 \par\f10 \fs18 \cf0
\fi189 {\b Perhitungan}{\b temu}{\b balik}{\b (}{\b\i recovery}{\b\i test}{
\b ) }
\par}{\phpg\posx2626\pvpg\posy5844\absw4488\absh1330 \sl-226 \par\f10 \fs18 \cf0
\fi1297 {\fs20 A}{\fs20 -}{\fs20 B }\par
}
{\phpg\posx2795\pvpg\posy7347\absw674\absh207 \f10 \fs18 \cf0 \f10 \fs18 \cf0 %
R = \par
}
{\phpg\posx4884\pvpg\posy7374\absw817\absh207 \f10 \fs18 \cf0 \f10 \fs18 \cf0 X
100% \par
}
{\phpg\posx4135\pvpg\posy7589\absw220\absh226 \f10 \fs20 \cf0 \f10 \fs20 \cf0 C
\par
}
{\phpg\posx2117\pvpg\posy8061\absw1857\absh207 \f10 \fs18 \cf0 \f10 \fs18 \cf0 d
engan pengertian: \par
}
{\phpg\posx2117\pvpg\posy8374\absw201\absh1053 \f10 \fs18 \cf0 \f10 \fs18 \cf0 R
\par}{\phpg\posx2117\pvpg\posy8374\absw201\absh1053 \sl-313 \f10 \fs18 \cf0 A
\par}{\phpg\posx2117\pvpg\posy8374\absw201\absh1053 \sl-313 \f10 \fs18 \cf0 B
\par}{\phpg\posx2117\pvpg\posy8374\absw201\absh1053 \sl-313 \f10 \fs18 \cf0 C \p
ar
}
{\phpg\posx4375\pvpg\posy8110\absw62\absh224 \f20 \fs20 \cf0 \f20 \fs20 \cf0 i \
par
}
{\phpg\posx2626\pvpg\posy8374\absw5612\absh1053 \f10 \fs18 \cf0 \f10 \fs18 \cf0
adalah{\i recovery} (%);
\par}{\phpg\posx2626\pvpg\posy8374\absw5612\absh1053 \sl-313 \f10 \fs18 \cf0 ada
lah kadar contoh uji yang di{\i spike} (mg/L);
\par}{\phpg\posx2626\pvpg\posy8374\absw5612\absh1053 \sl-313 \f10 \fs18 \cf0 ada
lah kadar contoh uji yang tidak di{\i spike} (mg/L); dan
\par}{\phpg\posx2626\pvpg\posy8374\absw5612\absh1053 \sl-313 \f10 \fs18 \cf0 ada
lah kadar standar yang diperoleh ({\i target}{\i value}) (mg/L). \par
}

{\phpg\posx2128\pvpg\posy9790\absw844\absh636 \f10 \fs18 \cf0 \f10 \fs18 \cf0 di

mana,
\par}{\phpg\posx2128\pvpg\posy9790\absw844\absh636 \sl-238 \par\f10 \fs18 \cf0 \
fi632 C \par
}
{\phpg\posx3026\pvpg\posy10267\absw165\absh207 \f10 \fs18 \cf0 \f10 \fs18 \cf0 =
\par
}
{\phpg\posx3520\pvpg\posy10200\absw525\absh421 \f10 \fs18 \cf0 \f10 \fs18 \cf0 Y
x Z
\par}{\phpg\posx3520\pvpg\posy10200\absw525\absh421 \sl-237 \f10 \fs18 \cf0 \fi1
75 V \par
}
{\phpg\posx2785\pvpg\posy10742\absw1857\absh207 \f10 \fs18 \cf0 \f10 \fs18 \cf0
dengan pengertian: \par
}
{\phpg\posx2795\pvpg\posy11056\absw165\absh771 \f10 \fs18 \cf0 \f10 \fs18 \cf0 Y
\par}{\phpg\posx2795\pvpg\posy11056\absw165\absh771 \sl-311 \f10 \fs18 \cf0 Z
\par}{\phpg\posx2795\pvpg\posy11056\absw165\absh771 \sl-314 \f10 \fs18 \cf0 V \p
ar
}
{\phpg\posx3303\pvpg\posy11056\absw5774\absh771 \f10 \fs18 \cf0 \f10 \fs18 \cf0
adalah volume standar yang ditambahkan (mL);
\par}{\phpg\posx3303\pvpg\posy11056\absw5774\absh771 \sl-170 \par\f10 \fs18 \cf0
adalah kadar standar KMnO {\dn006 \fs11 4} yang ditambahkan (mg/L); dan
\par}{\phpg\posx3303\pvpg\posy11056\absw5774\absh771 \sl-285 \f10 \fs18 \cf0 ada
lah volume akhir (mL). \par
}
{\phpg\posx2118\pvpg\posy12158\absw146\absh207 \b \f10 \fs18 \cf0 \b \f10 \fs18
\cf0 4 \par
}
{\phpg\posx2796\pvpg\posy12158\absw3981\absh207 \b \f10 \fs18 \cf0 \b \f10 \fs18
\cf0 Jaminan mutu dan pengendalian mutu \par
}
{\phpg\posx2118\pvpg\posy12634\absw5876\absh2257 \b \f10 \fs18 \cf0 \b \f10 \fs1
8 \cf0 4.1
Jaminan mutu
\par}{\phpg\posx2118\pvpg\posy12634\absw5876\absh2257 \sl-238 \par\b \f10 \fs18
\cf0 {\b0 a)}{\b0
Gunakan}{\b0 bahan}{\b0 kimia}{\b0 berkualitas}{\b0 mur
ni}{\b0 (p.a). }
\par}{\phpg\posx2118\pvpg\posy12634\absw5876\absh2257 \sl-237 \b \f10 \fs18 \cf0
{\b0 b)}{\b0
Gunakan}{\b0 alat}{\b0 gelas}{\b0 yang}{\b0 tidak}{\b0 ter
kontaminasi. }
\par}{\phpg\posx2118\pvpg\posy12634\absw5876\absh2257 \sl-253 \b \f10 \fs18 \cf0
{\b0 c)}{\b0
Gunakan}{\b0 air}{\b0 suling}{\b0 yang}{\b0 DHL}{\b0 nya}{
\b0 lebih}{\b0 kecil}{\b0 dari}{\b0 3}{\b0 \f40 }{\b0 mos. }
\par}{\phpg\posx2118\pvpg\posy12634\absw5876\absh2257 \sl-238 \b \f10 \fs18 \cf0
{\b0 d)}{\b0
Dikerjakan}{\b0 oleh}{\b0 analis}{\b0 yang}{\b0 kompeten. }
\par}{\phpg\posx2118\pvpg\posy12634\absw5876\absh2257 \sl-237 \b \f10 \fs18 \cf0
{\b0 e)}{\b0
Lakukan}{\b0 analisis}{\b0 segera}{\b0 setelah}{\b0 pengamb
ilan}{\b0 contoh}{\b0 uji. }
\par}{\phpg\posx2118\pvpg\posy12634\absw5876\absh2257 \sl-237 \b \f10 \fs18 \cf0
{\b0 f)}{\b0
Gunakan}{\b0 alat}{\b0 ukur}{\b0 yang}{\b0 terkalibrasi.
}
\par}{\phpg\posx2118\pvpg\posy12634\absw5876\absh2257 \sl-300 \par\b \f10 \fs18
\cf0 {\fs17 4}{\fs17 dari}{\fs17 6 }\par
}
{\shp\shpfhdr0\shpbxpage\shpbypage\shpfblwtxt1\shpz0
\shpleft3361\shptop10446\shpright3986\shpbottom10446
{\*\shpinst {\sp{\sn shapeType}{\sv 20}}

{\sp{\sn fFlipH}{\sv 0}}{\sp{\sn fFlipV}{\sv 0}}

{\sp{\sn LineWidth}{\sv 14}}
{\sp{\sn fBehindDocument}{\sv 1}}{\sp{\sn lineColor}{\sv
65793}}}}
\sect\sectd\pard\plain
\pgwsxn12240\pghsxn15840
{\phpg\posx8676\pvpg\posy806\absw2082\absh207 \b \f10 \fs18 \cf0 \b \f10 \fs18 \
cf0 SNI 06-6989.22-2004 \par
}
{\phpg\posx2118\pvpg\posy1607\absw342\absh207 \b \f10 \fs18 \cf0 \b \f10 \fs18 \
cf0 4.2 \par
}
{\phpg\posx2652\pvpg\posy1607\absw2037\absh207 \b \f10 \fs18 \cf0 \b \f10 \fs18
\cf0 Pengendalian mutu \par
}
{\phpg\posx2118\pvpg\posy2082\absw8885\absh918 \f10 \fs18 \cf0 \f10 \fs18 \cf0 a
) Lakukan analisis blangko untuk kontrol kontaminasi. Kadar khlo
rida dalam larutan
\par}{\phpg\posx2118\pvpg\posy2082\absw8885\absh918 \sl-238 \f10 \fs18 \cf0 \fi3
37 blangko harus lebih kecil daripada batas deteksi.
\par}{\phpg\posx2118\pvpg\posy2082\absw8885\absh918 \sl-311 \f10 \fs18 \cf0 b)
Lakukan analisis duplo untuk kontrol ketelitian analisis. Perbedaan pem
akaian larutan
\par}{\phpg\posx2118\pvpg\posy2082\absw8885\absh918 \sl-238 \f10 \fs18 \cf0 \fi3
38 kalium permanganate secara duplo tidak boleh lebih kecil dari 10%. \par
}
{\phpg\posx2118\pvpg\posy3585\absw146\absh207 \b \f10 \fs18 \cf0 \b \f10 \fs18 \
cf0 5 \par
}
{\phpg\posx2651\pvpg\posy3585\absw1440\absh207 \b \f10 \fs18 \cf0 \b \f10 \fs18
\cf0 Rekomendasi \par
}
{\phpg\posx2118\pvpg\posy4060\absw8954\absh2193 \f10 \fs18 \cf0 \f10 \fs18 \cf0
Kontrol akurasi
\par}{\phpg\posx2118\pvpg\posy4060\absw8954\absh2193 \sl-238 \par\f10 \fs18 \cf0
a) Analisis{\i blind}{\i sample. }
\par}{\phpg\posx2118\pvpg\posy4060\absw8954\absh2193 \sl-313 \f10 \fs18 \cf0 b)
Lakukan analisis{\i certified}{\i reference}{\i material}{\i (CRM)} untuk
kontrol akurasi.
\par}{\phpg\posx2118\pvpg\posy4060\absw8954\absh2193 \sl-314 \f10 \fs18 \cf0 c)
Kisaran persen balik adalah 85% sampai dengan 115% atau sesuai denga
n kriteria
\par}{\phpg\posx2118\pvpg\posy4060\absw8954\absh2193 \sl-237 \f10 \fs18 \cf0 \fi
338 dalam sertifikat CRM.
\par}{\phpg\posx2118\pvpg\posy4060\absw8954\absh2193 \sl-313 \f10 \fs18 \cf0 d)
Untuk kontrol gangguan matrik lakukan analisis{\i spike}{\i matrix} kisara
n persen temu balik
\par}{\phpg\posx2118\pvpg\posy4060\absw8954\absh2193 \sl-237 \f10 \fs18 \cf0 \fi
338 adalah 85% sampai dengan 115%.
\par}{\phpg\posx2118\pvpg\posy4060\absw8954\absh2193 \sl-314 \f10 \fs18 \cf0 e)
Buat kartu kendali{\i (control}{\i chart)} untuk akurasi analisis. \par
}
{\phpg\posx2118\pvpg\posy14932\absw693\absh189 \b \f10 \fs17 \cf0 \b \f10 \fs17
\cf0 5 dari 6 \par
}
\sect\sectd\pard\plain
\pgwsxn12240\pghsxn15840
{\phpg\posx2118\pvpg\posy806\absw2082\absh207 \b \f10 \fs18 \cf0 \b \f10 \fs18 \
cf0 SNI 06-6989.22-2004 \par
}
{\phpg\posx5764\pvpg\posy1607\absw1322\absh876 \b \f10 \fs20 \cf0 \b \f10 \fs20

\cf0 Lampiran A
\par}{\phpg\posx5764\pvpg\posy1607\absw1322\absh876 \sl-353 \b \f10 \fs20 \cf0 \
fi180 {\b0 \fs18 (normatif) }
\par}{\phpg\posx5764\pvpg\posy1607\absw1322\absh876 \sl-368 \b \f10 \fs20 \cf0 \
fi75 Pelaporan \par
}
{\phpg\posx2118\pvpg\posy3303\absw4394\absh207 \f10 \fs18 \cf0 \f10 \fs18 \cf0 C
atat pada buku kerja hal-hal sebagai berikut: \par
}
{\phpg\posx2118\pvpg\posy3779\absw228\absh2463 \f10 \fs18 \cf0 \f10 \fs18 \cf0 1
)
\par}{\phpg\posx2118\pvpg\posy3779\absw228\absh2463 \sl-314 \f10 \fs18 \cf0 2)
\par}{\phpg\posx2118\pvpg\posy3779\absw228\absh2463 \sl-311 \f10 \fs18 \cf0 3)
\par}{\phpg\posx2118\pvpg\posy3779\absw228\absh2463 \sl-314 \f10 \fs18 \cf0 4)
\par}{\phpg\posx2118\pvpg\posy3779\absw228\absh2463 \sl-313 \f10 \fs18 \cf0 5)
\par}{\phpg\posx2118\pvpg\posy3779\absw228\absh2463 \sl-313 \f10 \fs18 \cf0 6)
\par}{\phpg\posx2118\pvpg\posy3779\absw228\absh2463 \sl-313 \f10 \fs18 \cf0 7)
\par}{\phpg\posx2118\pvpg\posy3779\absw228\absh2463 \sl-313 \f10 \fs18 \cf0 8)
\par}{\phpg\posx2118\pvpg\posy3779\absw228\absh2463 \sl-313 \f10 \fs18 \cf0 9) \
par
}
{\phpg\posx2626\pvpg\posy3779\absw3038\absh2463 \f10 \fs18 \cf0 \f10 \fs18 \cf0
Parameter yang dianalisis.
\par}{\phpg\posx2626\pvpg\posy3779\absw3038\absh2463 \sl-314 \f10 \fs18 \cf0 Nam
a analis dan tanda tangan.
\par}{\phpg\posx2626\pvpg\posy3779\absw3038\absh2463 \sl-311 \f10 \fs18 \cf0 Tan
ggal analisis.
\par}{\phpg\posx2626\pvpg\posy3779\absw3038\absh2463 \sl-314 \f10 \fs18 \cf0 Rek
aman kurva kalibrasi.
\par}{\phpg\posx2626\pvpg\posy3779\absw3038\absh2463 \sl-313 \f10 \fs18 \cf0 Nom
or contoh uji.
\par}{\phpg\posx2626\pvpg\posy3779\absw3038\absh2463 \sl-313 \f10 \fs18 \cf0 Tan
ggal penerimaan contoh uji.
\par}{\phpg\posx2626\pvpg\posy3779\absw3038\absh2463 \sl-313 \f10 \fs18 \cf0 Bat
as deteksi.
\par}{\phpg\posx2626\pvpg\posy3779\absw3038\absh2463 \sl-313 \f10 \fs18 \cf0 Per
hitungan.
\par}{\phpg\posx2626\pvpg\posy3779\absw3038\absh2463 \sl-313 \f10 \fs18 \cf0 Has
il pengukuran duplo. \par
}
{\phpg\posx2118\pvpg\posy6598\absw4805\absh772 \f10 \fs18 \cf0 \f10 \fs18 \cf0 1
0)
Hasil pengukuran blanko.
\par}{\phpg\posx2118\pvpg\posy6598\absw4805\absh772 \sl-313 \f10 \fs18 \cf0 11)
Hasil pengukuran persen{\i recovery. }
\par}{\phpg\posx2118\pvpg\posy6598\absw4805\absh772 \sl-314 \f10 \fs18 \cf0 12)
Kadar angka permanganat dalam contoh uji. \par
}
{\phpg\posx2118\pvpg\posy14932\absw698\absh189 \b \f10 \fs17 \cf0 \b \f10 \fs17
\cf0 6 dari 6 \par
}
\sect\sectd\pard\plain
}