Đồ Án Thiết Kế Hệ Thống Chưng Cất Nước ..

Chung taygn Natte ~ Axit axetio GUWD: Hguyén Van Lye LOIMS DAU Khoa hoe ky thugt ngay cdng phat trign va edag v6iné MA nhu clu ngay cing cao vé 46 tinh khiét cia cic sin pham. Vi thé, cic phutsng phap ning cao d® tinh khiét udm lun due cai tién va Adi mdi dé ngay cang hoan thién hun, nhut i: c6 de, hip thu, chung ft, trich ly. Tay theo dic tinh yéu edu etia sin phim ma ta c6 si la chon phuting phép phi hyp. BOi vi he Nude ~ Axit axetic Ia 2 ef tit tan Lin ho’n toan, ta phai ding phuting phip chung eat dé nang cao 46 tinh kh. BO dn mOn hoc Qué trinh va Thiet bi 18 mot mon hoe mang tinh tng hop trong qué tinh hoc tip cia céc k¥ suf Cong nghé Héa hoc tong lai. Mén hoc gip sinh vién gidi quyét nhiém vu tinh toxin cu thé vé: quy trinh cOng nghé, két eifu, gid thanh cia mot thiét bi trong sin xudt héa chit thye phdm. Day la bube dau tien dé sinh vign van dung nhimng kién thife 48 hoc ciia nhiéu mdn hoe vao ‘quyét nhang véin 42 ky thudt thy t€ mot cach tng hop. Nhiém vu cia Bé dn nay Ia thigt ké he thdng chumg edt Nude — Axit axetic e6 ning sudt 1a 3000 kg/h, ndng 40 nhap ligu a 30% Kh6i lung, néng a6 sin phim dinh 1a 95,5% kh6i luting, nbng 46 sin phdm day 1 0.5% kh6i luting, Sit dung hoi d&t c6 p suit 2,Sat Trang 1Chung taygn Natte ~ Axit axetio GUWD: Hguyén Van Lye GIGI THIEU LLY THUVET VE CHUNG Cit: 1, Khai nigun: CChumg et la qua tinh ding dé téch efe et eda mat hn hop Tag can nh hin hp kh Wing thanh eéc ex ut eng biet dya vo dO bay heii Khéc nhau eda cae eff wt trong hén hop (nghTa fa khi 6 cag mét abiét 46, dp sudt hoi bio hda cla céc edu ti khiéc shaw) Thay vi dua vao trong hn hgp mot pha méi 4é tgo nén sy tiép xuic gidta hai pha nhut trong qui tinh hp thu hoic nha khi, trong qua trinh chumg ct pha mdi duige tao nén bling su bc hoi hode ngung tu Trong tring hgp dén gidn nhit, chung cit va c6 die khéng khde gi nhau, wy nit gta hai gud trinh nay c6 mét ranh gidi co ban la trong qué trinh chyng edt dung méi va chat tan d&u bay hoi (nghia la cdc ett déu hin dign trong cit hai pha nhimg voi IG hdc nhau), edn trong qué tinh 66 die thy chi e6 dung mdi bay hoi edn chat tan khong bay hi Ki chung eit ta tha duge nhigw cau ut va thing thi bao mhigu cut sé th dese bay hia sin phdm, Néu xét hg dan gid chi 6 2 cu iF th ta thu dug 2 sn phim: + Sin phim dinh chi yéu gdm edi tit €6 46 bay hot ldn va mot phi it 6 6 bay hai bé, + Sin phiim iy chil yu 26m edu tt e6 46 bay hot be va mOt phan Ht teu tt e6 46 bay hoi lon ai vdi hg Nude Axit axetic th * Sdn phim dinh chil yéu Ia nude, # Sin phim day chi y6u 1a axitaxeti. tu tt 2. Cie pluttng phiip eluing ett: 2.1, Phan loai theo ap suit im vie = Ap suite haip = Ap suse duong - Ap suat cao 2.2, Phiin loai theo nguyén Iy lam vige: = Chimg eat don gin = Ching bing hai nude tre tie = Chimg eat 2.3, Phan loai theo phutsng php cfip ahiét 6 day thap: = Cp nhige nye tie = Cap nhige gidn tiép Vay: d6i voi hé Nude ~ Axit axetic, chon phutmng phép chung eft ién tue ep nhigt sidn tiép bang néi dun ¢ ap suat thwng. Trang 2Chung taygn Natte ~ Axit axetio GUWD: Hguyén Van Lye 3. Thiet bi ehuiny edit: ‘Trong sin xuat thufing ding nhiéu Jogi thigt bj khée nhav dé tién hanh chung eft, Tuy nnhién yéu céu ca ban chung cia ede thiét bi van ging nhau nghia la dién tich bé mat tip xe pha phai In, diéu may phy thude vao mite dO phan tin ea mot haw chat nay Vo Tt chat kia, Néu pha khi phan tin vao pha lng ta e6 ede loai thap mim, néu pha long phan tin vio pha khi ta e6 thap chém, thip phun,.. G dy ta khao st 2 loai thuéing diing [a thip ‘mam va thép chém, = Thip mm: than thip hinh try, thing diing phia trong o6 gin efic mam 6 eu tao khée nhau, én d6 pha Ing va pha hoi duge cho tiép xic voi nhau. Tay theo cau {90 cia ia, ta 06: = Thép méim chép : tren mm b6 tri e6 chép dang tron, xupap, chi. = Dap mém xuyén 16: trén mim c6 nhiéw 18 hay ranh + Thip chém Ghdp dém): thdp hinh try, gém nhigu bite ni voi nhaw bang mat bich hay han. Vat chém due cho vao thép theo mét trong hai phuong phép: x€p ngdu nhign hay xép the te. So sinh wu nhutge Giém ela ese loai thip Thép chem Thép mim xuyén 16 Thap mam chép_ ~ Gu to Kha don gin, Tri Ie womg dS tip. | - Khé dn din, we {7 Ted lye thé. ry - Higu suit kha cao, = Higu suit cao. Keay | Lam vigedsev8i chit ting em | yen nev dang dém edu os p= p cia chat lbng. Do o6 higu ing thanh > higu | - Khong fim vige due ~ C6 td ye Wn ‘suat truyén khoi thatp, Voi chat Wing bin. = Tiéu Wn ohiéu = BO én dinh khong cao, khé van |-Kétedu kha phite tap. | vat ne, ket cfu Nhuge | hinh. phge tap. diém | - Do 6 higu ving thank —> khi ting nang suit thi higu tng thank tang > kh6 tang nang sus = Thigt bj khd nang né. Vay; ta sit dung thép mam xuyén 15 dé chung cat hé Nudie ~ Axit axetic. Trang 3Chung taygn Natte ~ Axit axetio GUWD: Hguyén Van Lye I. G1OL THIED $6 BO VE NGUYEN LIEU = 1. Axil axe LLL. Tinh bat Axil axetic ndng chay & 16,6°C, diém s0i 118°C, hn hgp trong nue vi moi ty Ie Trong qué tinh hén hgp vai nutde €6 sif co thé tich, vBi ty trong eye dai, chita 73% axit axetic (D : 1,078 va 1,0553 46% vai axit thudin Khi€d. Neudi ta khéng thé suy ra dude ham long axit axctic trong nude tif ty trong cia nd, ngoai trt 46% vai cdc ham Ingng dui 43%. Tinh an mon kim loai + Axit axetic an mon sit + NhOm bj din man bd axit loang, n6 dé khang (t d6i vd axit axetic die va thudn khiét Béng va chi bi An mon béi axit axetic véi suf hign dign cia kh6ng kh = Thige va mOt 6 logi thép nikel ~ erom dé khiing t61 A6i vi axit axetic. Axit axetic thuiin khiét cdn goi lt axit glaxial bdi vi no dB dang dong dae ket nude dé 8 dudi 17°C, dude digu ché chit yéu bing sy’ oxy héa di voi andehi Khong mau sfc, vi chua, tan trong nue va edn etylic. shu axetic. 1.2, Bidu che? Axitaxetic duge didu che bing each: 1) Oxy héa ob atic tde déi vi cén etylic dé bign shanh andekit axetic, la mt giai doan rung gian. Su oxy héa kéo dai s2 sidp tue oxy héa andehit axetic thank axit axetic. CHCHO + "4 0; = CH;COOH CsHsOH + 0; = CHsCOOH + H.0 2) Oxy ha andehit axetic duage 1go thank bing eich idng hop tt acetylen. Sv oxy héa andehit due tign hinh bing khi Wi voi su hign dig Naudi ta thao tic trong andehit axetic @ nhigt d6 gin 80°C Aé ngdin chin swt peroxit, Higu suat dat 95 ~ 98% so vdi ly thuyét. Neu ta dat dutge nh thé ra ‘au khi ché axit axetic Ket tinh duige, CH,CHO +140, Coban axel 80°C oH COOH 3) Tong hop di ti cén metylie va Cachon oxit Higu susie 06 thé dat 50 — 60% so vai ly thuyét bing cdc 66 dinh cachon oxit ren cn metylic qua xtc tie Nhigt d6 tir 200 ~ 500°C. ap suit 100 - 200atm: CH.OH + CO» CHsCOOH vai sif hign dién ctia metaphotphit hode photpho ~ vonframat kim logi 2 va 3 héa tr (ching han sit, coban). da coban axetat thanh a8 ding 1.3, Ung dung: Axit axetic Ri m6 axit quan trong nhiit trong ede Togi axit htu ed, Axit axetie dm due rt nhiéu img dung vi n6 18 loai axit hitu e¢ ré tién nhdt. N6 due ding dé ché tao rt hig hgp chat va ester. Neudn teu thy chil yu eda axit axetic Ri Lam déim an (dam an chuia 4,5% axit axetic). = Lam dong dic nha mi cao su. Trang 4Chung luygn Nuthe ~ Axit axetio GOHD: Hgnyin Van Lye chit déo to sqi xenluloza axetat — lim phim dinh khéng nhay lita. = Lam chat nhya kétdinh polyvinyl axetat, + Lam cic phim mau, diye phim, nude hoa ting hop. = Axctat thém ding lim chat cin mau (mordant trong nghé nhuém) = Phan 1dn cfc ester axetat déu la ede dung mbi, thi du: izoamyl axetat hda tan due nhiéu loai ahufa xenluloza. 2. Dutte: Trong diéu kign binh thuting: nude Ta chit lng khong mau, khong mii, khong vi nnhuing khdi nude day sé ¢6 miu xanh nat. Khi héa rin n6 6 thé tn tai d dang 5 dang tinh thé kha nhav. Tinh chat vat Wy = Khoi hnyng phan tt: 18 g/mol Khoi hnmg rigng de? > 1 g/ml = Nhiged6 néng chiy —: 0'C + Nhigt 49 s6i 100°C NuGe Rt hyp chat chigm phan Ion tn trai dat (3/4 dign tich tr4i At 1A mde biEn) va rift cn thiét cho su sting. Nude la dung moi phiin eve manh, e6 kha ning hod tan nhieu chat va 1a dung moi re quan trong trong KY thudt héa hoe: Chuong 2 QUY TRINH CONG NGHE Chi thich esic ki higu trong qui trinh: 1. Bén chita nguyén liu. 2 Bom, 3. Bén exo vi 4. Thigt bi trao di nhigt vi sn phim dink, 5. Thigt bj dun s6i dang nhép lig 6. Bay hoi 7. Linu hong ké. 8. Nhigt ke: 9. Thap chung eff. 10, ‘Thigt bi nung ty sin phim din, 11, Apké 12. Thigt bi dun s6i day thép. 13, Thigt bi kam ngui sin phim day, 14. Bén chita sin phim day. 15. Bén chita sin phiim dinh Trang 5Chung luyén Nutte - Axit axetic GOHD: Nauyin Van Lye Hén hop Nude ~ Axit axetic ¢6 ndng 40 nutde 30% (theo phan Khoi htgng), nhigt a khoding 27°C tai binh chita nguyen ligu (1) diige bm (2) bum len bn cao vj (3). TH 46 hig dita dén thigt bi trao di nhiét vai sin phim dinh (4). San a6, hn hap duige gia nhi€t En nhi€t 46 s6i trong thi€t bj dun soi dng nhap ligu (5), 1i due da vaio thap chumng e&t (9) 8 dia nhap ligu. ‘Trén dia nhdp ligu, chit lng duvge teOn vei phan Ing tit doan luyén cia thap chay xuGng. Trong thap, hoi di tt dui lén gip chat ling tt tren xudng. G diy, c6 si tiép xtic Va tra 46; gita hai pha voi nhau., Pha 1éng chuyén dng trong phin chung cane xuGng dudi cang gidm ndng d6 céc eau tt d€ bay hoi vi di bi pha hdi tao nén tit néi dun (12) i cud cau ti dB bay hoi, Nhigt d6 cng len trén cing tha’p, nén khi hei di qua ede da tt dui len th edu tt €6 mhigt d6 Oi cao Ia axit axetic sé ngung ty Iai, cuGi edng ten dinh thdp ta thu duge hdn hap c6 edu tt mde chiém nhigu nhs (c6 néng dé 95,5% phiin khdi hngng). Hoi nay di vao thiét bi ngutng ty (10) va dutge ngting ty hodn to2n. Mot phiin chat ling nguing tw duige trao di nbigt voi dong nhap ligu trong thiét bi (4) (sau khi qua bn cao vi). Phin cdn Jai cia chat ling ngung tu duge hoan vu vé thap 6 dia ing. MOt phan cu ti c6 nhigt d@ s0i thp dirge Ge hoi, edn Ini effu tt e6 nhigt dQ SO; cao trong chat 1dng ney cng ting. Cudi cing, 0 day thip ta thu duige hin hgp lng haw hét 12 ede eau ti kh6 bay hi (axit axctic). Hdn hop King 8 diy 6 néng 46 nude 1a 0,55 phan khéi Iueng, edn lai I awit axetic, Dung dich lng @ day di ra khéi thép vio ndi dun (12). Trong néi dun dung dich long mot phi sé bée hai cung cap Iai cho thap dé tiép tue lam vige, phan cdn Iai ra khdi ndi dun di qua thi€t bj Kim ngudi sin phim dy (13), duge lam ngudi dén 35°C , edi duige dra qua bén chita sin phiim dy (14). He théng lim vige lién tye cho ra sin phim dinh 1a miGe, sau khi trao d6i ahiét voi dong nhap ligu e6 nhigt 46 35°C va dhtge thai bé. Sn phim day Id axit axetic dude git li Feany 7Chuing luygn Natée ~ Axit axetie GOHD: Nauyin Van Lye CAN BANG VAT CHAT CAC THONG 86 BAN DAU: Chon loai thap 18 thip mam xuyen 16 Khi chimg luyén dung dich axit axetic thi eu tt d& bay het fd nut. fi /Axit axctic: CH,COOH = M,, = 60 (e/ mol) franco 8/m Nang sudt nlp ligu: Gp= 3000 (kg/h) = Néng d9 nhip ligu: xp= 30% (kg mide kg hn hop) + Néng d9 sin phim dinh: xn = 95.5% (ke nude! kg hn hap) = Néng 49 sin phiim diy: xw = 0,5% (kg muée/ kg hn hop) = Ap suilt hoi d6t: Py = 2,5at * Chon: ¥ Nhigt 66 nhap ligus tev = 27°C Y Nhigt d6 sin phim dy sau khi Iam ngudi: tue = 35°C Y Nhigt 46 dong nude lanh di vio: ty = 27°C Y Nhigt 66 dong mude lanh di ra: te = 43°C ¥ Trang thai nhdp ligu 1 trang thai long s6i # Che ky bids Gr, F:susit ugg nhgp ligu tinh theo kg/h, kmoVh Gp, D: suit nung sn phdm dinh tinh theo kg/h, kmol/h Gwy,.W: suit gg sin phdm day tinh theo kg/h, kmoV/h wii SAK xi, xi ndng d6 phéin mol, phan kh6i Iugng cia cf 1. XA€ DINK SUAT LUONG SAN DRAM DINE va SAN DRAM DAY THU BUG Bun gin tgp 30-05 3090 = 931.579 (kg/h) 55-05 1068.42 (kg/h) Trang 8Chung luyén Nutte - Axit axetic GOHD: Nauyin Van Lye Mm. XAC DINE TESO HOAN LUU LAM VIEC = 1, Déna dé phén mot: 03 18 = 0,588 (mot nude! mot hn hop) os, 1-03 18” 60 0,005 bt {mol mude/ mol hon sms ans = 4016 (mot nude mot nd gp) 18 60 TOES Tapas 79.986 (mol murder mot HB bp) 18 60) 2. Suit bere wot tay di eva dina nbeiy tidus 230m Kw _ 098606 0.01647 T Xp Ky 058824 —0,01647 3. Tisd hodn tu tim viées 1 09 08 07 06 05 04 03 02 Ou 0 0 01 02 03 04 05 06 07 08 09 1 finh 1: D6 thi edn bing pha ctia hé Nude ~ Avi axetie Frany 9Chung luyén Nutte - Axit axetic GOHD: Nauyin Van Lye Dya vio hinh 1 = ye" 098606 ~ 0,705 Yr—Xp 0,705 0.58824 Ti SG hodn uu Lam vige: R= 1,3Rqin + 0.3 = 3,429 Ti s@ hodn liu ti thi 407 IV. XAC DINE SUAT LUONG MOL CUA CKO DONE DEA = Coi Iu Iugng mol cia ee dng pha di trong mdi doyn thap (chung v2 Tuyen) Ia khong asi 4, Dad dial thé: i L tu L Vi tai dinh thap néng 6 phan mol cia nue trong pha Ing va pha hoi bing nhav. = Kh6i lugng cia pha ho va pha léng tai dinh thay a bng nha: Muro = Mun = Xp. My + (1 ~ xp). M=0,986. 18+ (1 ~ 0,986). 60 = 18.585 (kg/mol) Sut lung kh6i lung ela dong hai tai dinh thé: Guy = (R-H1)Gp = (3,429 + 1). 931,579 = 4126,142 (ky) Suat lugng mol ea dong hoi tai dinh tip rp = Ge. = 41265182 _ 952,099 (kmoth) Mio 18,585 Suit lugng khéi lugng eta dong hodn hvu: G,=RGp= 3.429. 931,579 Sut iugng mol aia dong hoan leu: 2. Tai mim nip lieu: Khoi gg mol eda dng nhap lieu Mp= xp. My + (I~ xp). Ma = 0,588. 18 + (1 ~ 0,588). 60 = 35,294 (kg/kmol) Suit iuwgng mol cia dong ahip lieu: Frang 10Chung luyén Nutte - Axit axetic GOHD: Nauyin Van Lye = Ge 3000 256,885 (kot) M, 35294 Va: np=L= 171,885 (kmolh) Wea L + F= 171,885 + 256,885 10 = 222,009 (kot) 28,770 (kmol/h) 3. Tai diy thip: w Vi tai day thip ndng 46 phn mol ela nuit rong pha Ing va pha hai bling nhau. = Khoi lung eda pha hi va pha Ting tai dy tip 1a Dang nhaw Maw = Mow = xu. My + (I — xw). My = 0,016. 18 + (1 0.016). 60 = 59,308 (kg/mol) Sut iugng mol cia dong sin phém day: wee Gv _ 2086421 _ 34 576 (emorn) Myy 59308 VA: ney =n" Le = 128,770 (kmoVh) ‘nyw = Nhe = Mw = 222,009 (kot) Trang 11Chuing luygn Natée ~ Axit axetie GOHD: Nauyin Van Lye TINH THIET BI CHiNH (Thap mam xuyén 15) Dhutong trink duiing lawn vige Phin luyén: me x+ Xo - 3429 _, , 0986 - x = 0,774x + 0,223, +1 R41 342041 342941 Phin chumg: y=R+f x4 I-f = 342941696, , 1-696 , ggg Rel GI 342941 *” 342941 = 1,157 ~ 0,003 1 BUONE KIN TRAD s 4. Dein ayn: 1.1, Khdi lung riéng trung binh eta pha I6ng trong phin luyén: ‘Néng 46 phiin mol trung binh eta pha long trong phan luyén: 186 + 0,58 a Dia vao hinh 2 => Nhiét d6 trung binh ciia pha lng trong phn luyén: ee) Néng 46 phiin kh lung trung binh eta pha lng trong luyén: Ry +%, 0955+ aoe 2 ‘Tra bing 1.249, trang 310, [5] = Khoi lang rieng cia nude & 101,4°C: pyr = 957,364 (kg/m’) ‘Tra bing 1.2, trang 9, [5] = Khoi lung riéng cia anit axetic 3 101.4°C: pa = 955.480 (kg/m) Ap dung trong cOng thife (1.2) trang 5, [5]: 1% 1k, 0628 | 1-0628 Pu Pu Pa, 957.364” 955,480 0,787 {mol nude! mol hn hop) 101 628 (kg nude/ kg hn hop) = 0,001 => pu, = 956,661 (kg/m") 1.2, Khoi ung ring trung blah cia pha hoi tong phd luyén: Néng 46 trung binh ea pha hoi trong phiin Iuyén yu = 0,7 74x, + 0,223 = 0832 Defa vao hinh 2 = Nhigt 45 trung binh eta pha hoi tong phiin luyén: Ty, = 101,6 (°C) Khai Ifgng mol trung binh cia pha hei trong phan luyén Ma = yu. My + (I~ yi). My = 0,832. 18 + (I ~ 0,832). 60 = 25,054 (kg/kmol) Khoi higng riéng trang binh cia pha hai trong phan luyén: Trang 12Chuing luygn Natée ~ Axit axetie GOHD: Nguyen Van Lye ou = PM = _P25084 9.515 gin’) ~*(101,6+ 273) 73 118 16 m4 nz 110 108 106 102 100 CT Hinh 2: Gidn dé T— x.y etla h@ Nude ~ Axit axetic Frang 13Chuing luygn Natée ~ Axit axetie GOHD: Nauyin Van Lye 13, Tinh.vén.t6e pha hoi di trong phan Iuyén: Tra bang IXa, trang 169, [6] => Vai duting kinh thép trong khoaing 1.4 = 1,6 (m) thi hosing eich mam Ta: Ah = 400 (mm) = Ot (m) ‘Tra d6 thj 6.2, trang 286, [4] => C = 0,057 ‘Van t6e pha hai di trong phiin luyén o,-¢ Pu, Ven .953 (mm/s) LA, Tinh duting kinh phn luyén: Sut iugng mol cia pha hei trong phiin luyén: nn Sut ugg thé teh ea pha hai wong phan luyen 222,009 (kmol/h) 24 009 x 224 101,64 273) Ay RT, _ 222.009 55 «(101.6 +273) = 1,895 (m’/s) On 3600 P 3600 x1 en Duting kinh phin nygn: 6, = /22m = [41895 _ 112 (my Vr,” Vrxi9ss 2. Dein eluing: Tinh tosin twtsng tf nh phi luyén => ta 66 bang két qui sau: Tuc | pwc | pac_| Were | pre 0.302 | 0.153 | 107.4 | 952,924 | 944,680 | 0,001 | 945.928 | Tne | Muc | pac | oc | Que |e 0347 | 109 [4541s] 1.449 | 1.456] 1,933) 1,300 16 thé I’y dutng kinh cila ton thép 1a dudng kinh cia phiin chumg. Chon theo chuin = 6 = 1.4 (m) (pha hgp vai diéu kign 6 = 1.4 + 1.6m) Két ludn: dying kinh thap Ia @ = 1.4 (m), ‘Van tc pha hai trong phin chung va phdn luyén theo thie té: =p 2193. as640v9 .231 (mis) Frang 14Chuing luygn Natée ~ Axit axetie GOHD: Nguyen Van Lye © of 023 tS HOB Hinh 3: 86’ mam ls thuyét Frang 15Chung luyén Nutte - Axit axetic GOHD: Nauyin Van Lye . CHIEU CAO THAD 4. Dlein tayén: Dya vao hinh 3 => So mam ly thayét phan luyén: ny, = 19 Ll. Tinh hig suit mim: Tai nhigt d6 trung binh cia pha hoi trong phan luyén Tin. = 1O1.6°C + Tra bang 1.250, trang 312, [5] => Ap suit hoi bao hoa cila nite Py. = 1,09668 at = $806,060 (mmilg) ‘© Tra hinh XXL, trang 466, [4] => Ap sudt hoi bao hoa eilaaxit axetic Pa, = 150 (mmltg) Nén: a, = Pat = 806.060 _ 5 374 Pa 150 Tai mbit 46 tung binh cia pha King trong phan lnyén Tu, = 101.4°C hi + Tea bing 1.104, trang 96, [5] = B6 nbd cia nude ja, = 0,2808 (€P) + Dang toan dé 1.18, trang 99, [51 => D6 nhdt eva axitaxetie wa = 0.42 (P) 6 nhdt eta hdn hop long: Haj = Xlgus + xg (cong thie (1.12), trang 84, (51) Nén: Igy = 0,787. 1a0,2808 + (1 ~ 0,787)1g0,42 = -0,514 = 1, = 0,306 (cP) > ayu.= 64d ‘Tra hinh 6.4, trang 287, [4] = Fy = 0.42 Vi thap c6 duting kinh 1dn; 6 = 1.4m> 0.9m = phai higu chinh Iai gid ti Ey ‘Tra biinh 6.5, trang 258, [4] = A= 0,14 Nén: Eq, = Ey(1 + A) = 0479 1.2. Tinh si mém thye t€ phiin tuyén: 86 mam thye: ng, = 2 39,683 = 40 2. Dhiin elu: ‘Tinh todn widng ty abut phin luygn => ta €6 bing két qua sau: me | Pwe [Pac | ae [we [xe | gue | we 14 [106,632] 190 | 5,614 | 0.2632 | 039 | -0.461 | 0.346 acne | Ee Ecc [mc | mcquy ton 1944 | 04 | 0,456 | 30,702 31 3. Chitin cao tip: SO mam thye t€ ciia todn thép: my = nay + Mac = 40+ 31 = 71 Chigu cao than thap: Hog = (My -1)Ah + 1 = 29 (m) Chon day (np) clip tiéu chun o6 * 25 = y= 0.25. 14 = 0.35 (m) Frang 16Chung luyén Nutte - Axit axetic GOHD: Nauyin Van Lye Chon chit cao g@: hy = SOmm = 0.05 (m) Chiu cao day (np): Hay = thy = 0.4 (m) Kétludn: Chiu cao toan thép: H = Hig + 2Huy =29 + 2.0.4 = 29.8 (m) mm. Tee LY THAD 1. Cin tao mam tds Chon thap mam xuyén 18 o6 Sng ehay chuyén vor: + Ti€idign usdo bing 8% ign ch mam. + During kink 15: dy 003 (my, + Chigw cao 20 chiy tn: hyy = 50mm = 0,05 (m). © ign tich eda 2 ban nguyét bhng 20% dign sich mam, + Li bet theo hin ye giée dB, + Khoving cach gita 2 tam 16 bing 7mm. = Mam duge fam bing thép khong gi XISHIOT. $6 15 teén 1 mam: os 4) } 17422,222 03, Goi a fi s6hinh lye gide Ap dung cong thite (V.139), trang 48, (6]: N = 3a(a+1) +1 Giaii pang tinh be 2 => a = 75,706 = 76 = N = 17557 (18) S616 trén duding chéo: b= 2a + 1 = 153 (18) 2. Ded lute etia dia kkhd: Ap dung cong thie (IX.140), trang 194, [6]: AP, él voi dia o6 tit dign tudo bang 8% dign tich mam thi & = 1,82 2.1. Phin tuyé Van te hoi qua W: 0, = — = 15,392 (im/s) 8% 008 15392.0815 Nén: APu = 182 75.724 (Nim?) 2.2. Phin cat Van te hai qua WB: a'g= Se = 1256, 8% ~ 008 15,696 (m/s) Nén: APye= 182 24,829 (Nim*) 3. Tri le do site eng bi mats ‘Vi dia £6 dvting kinh 18 > Imm 40 = Ap dung cOng thie (IX.142), trang 194, [6]: aP, = ——4°_ Sect i a : rel: 13d, +0,08d 5, 3.1, Phan luyen: Frang 17Chung luyén Nutte - Axit axetic GOHD: Nauyin Van Lye Tai nhigt 46 trung binh cia pha ling trong phin lnyén Tu = 101.4°C thi + Tra bing 1.249, trang 310, [5] = Sife cing bé mat ctia nue ow: = 0,585756 (Nim) # Tra baing 1.242, trang 300, [5] => Sife cing bé mat cia axit a4. = 0.019674 (N/m) Ap dung cong thute (1.76), trang 299, [5]; = 1.1 6 oe Ne: oy, = 2585756 0.019675 «4619 ex) 10585756 + 0.019674 Chota: AP, =——4*9019__ 19. 519 am?) 13 0,003 + 0,08 x 0,003 3.2. Phin ching: Tinh to‘in tong ty nhu phiin luyén => ta e6 bang két qui sau ove | owe | oe | Apac 0.573996 | 0.019134 | 0,019 | 18.988 4. Teds late thiiy tink do ehait tng trén dia tao ra: Ap dung c6ng thife trang 285, [4]:AP, = 1.3hyKp.z Valis hy = hyo + hy on-(ass] Trong a6: = Lyn: chigu dai eda g@ chdy tin, m = K= pup. : ty 36 giita khoi Ingng rigng cht ling bot va khdi vung riéng eta chit long, lay gan bing 05. | ge mM Pe Tinh chiéu dai go chdy eran suit Iuging thé tich eta pha ling, m'A, a _ 20% 2a- sina = 025 Frang 18Chung luyén Nutte - Axit axetic GOHD: Nauyin Van Lye Dang phép kip = «= 1,626753345 (Rad) sin 1926753345 Nén: Ly = sin 017 (m) 4.1, Phan tuyen: Kh6i gag mol trung, My +M, cia pha ling tong phan luyéa: 8,58: Mu= = 26,940 (ky/kmol) 2 2 Susftlugng mol eiia pha King trong phdn luy@n: nu = L= 171,885 (kmol/h) Sudt huang thé dich cba pha long tong phan luyén: uy = BivMu _171885%26940 _ 60134 (np) Pu 956,661 0134 185%1017 «05 Chota: AP = 1.3(heo + ANLIKpug ‘3.(0.05 + 0.01269). 0.5. 956,661. 9,81 = 382,396 (Nh Nén: Ahy = = 0,01269 (m) 42. Phin chung Tinh tosin twsng tf nhu phan luyén => ta 66 bang két qui sau {mic [Que [tne [apie {47.301 [0.00357 | 0.02432 | 448.261 J. Fina este tuts we eta thitp: Téng td lye cba 1 mim wong phan Iuygn cba thap Ia APL = APut + AP. + AP. = 175.724 + 19,519 + 382,39 Téng trd lye cia | mim trong phin chung cia thap La: APC = AP yc + APac + AP = 324,829 + 18,988 + 448,261 ‘Kiém tra hoat dong cia mam: Kim tra igi khoiing cach mam Ah = 577,638 (Nim) = 792,078 (Nh 4m dim bao cho diéu kign hoat déng binh tung ota thap: Ah > 1s 2 rue Voi cae mam trong phan chung trd lve thus life qua 1_mam ln hon trd Ie thuy Ive eta AP. 792.078 rmam trong phan layén, ta 06: 18 = 0,154 Puck 945928918 = Didu kign teén duge théa. = Kiém tra tinh dng nha cia hoat dong cia mam. Tinh van te t6i thigu qua IS ea pha hii Vain di dé cho ese 16 trén mam déu hoat eesti Rd Scat ng: vnin= 0,67 |8PcHIc. ~ 9 67, [981945 928 «(0.05 + 002852) _ 19 935 < 15,696 rc fi 1821449 => Cac 16 trén mamdéu hoat ding. Kétludn Téng trd luc thiy Ine eta thap: Frang 19Chung luyén Nutte - Axit axetic GOHD: Nauyin Van Lye AP = ng. AP, + nycAPc = 40, 577,638 + 31, 792,078 = 47659,953 (Nim?) 6. Kido tea nyiip tut ki thiip hoat déng: Khoiing céch gitta 2 mam: Ah = 400 mm). BO qua s¥ tao bot trong dng chy chuyén, chigu cao myc chat King trong dng chiy chuyén ela mam xuyén [6 due xie dinh theo biéu thite (8.20), trang 120, [2] hy=h +A, +AP-+hy ——, (mm.chit Ing) Trong a6: = Iigs: chigu eao g@ chdy tran (mm) = Ahy :chigu cao lop chit ling trén mam (mm). AP: tng ted hye eta | mam (mm.chat ng). ‘= hy + tn that thy Ie do dong ling chi tit dng chay chuyén vio mam, duge xe inh theo bigu thife (5.10), trang 115, [2]: hy -o128{ 2) _(mm.chit ling) = Qc: tu higng eda chat King (mh), = Sy: tigt dign gitta Gng chdy chuyén va mam, Sa=0,8 . San = 0.8. = 1.4? = 1,232 (mr) Dé thip khong bi ngdp Int khi hogt dOng thi: has zan = 200 (mm) 6.1, Phin luyén: = Ay =0,01269. 1000 = 12,69 (mm) 517.638 999 -_ 577.638 + APL= 1000 = 577.658.1999 = 61,550 (mm.chit long) Pue 956,661 981 : i 0329{ Oi a9 ers (0,002 (mm.chat long) \ 100%1,232 Nén: ha. = 50+ 12,69 + 61,550 + 0,0002 = 124,237 (mm) < 200 (mm) Vay: Khi hoat d6ng thi mam phin luyén sé khong bj ngap Iut 6.2, Phiin chung: Aye = 0,02432. 1000 = 24,32 (mm) . 192.078 __ 1999 = 85,357 (meh ling) (0,00357 x 3600 \* it le Nén: hoc = 50 + 24,32 + 85,357 + 0,0014 = 159,676 (mm) < 200 (mm) Vay: Khi hoat dGng thi mim 6 phn chung sé khong bi ngap tut. Kéi ludn: Khi hoat d0ng thap s khOng bi ngGip Int Frang 20Chung luyén Nutte - Axit axetic GOHD: Nauyin Van Lye ef pay Tip 1. Dhan thé: Vi ihap hogt dng & 4p su tadng nen ta thie ke thd Hin try bhng phucng php han hd quang dign, kigu han gigp méi 2 pha. Than thép duye ghép véi nhau bang ede m6 hep bich. Vi thip hogt dGng 6 nhigt 6 eno (>100°C) nén ta phii boe e&ch nbigt cho thi. bé dim bio chit hugng cia sin phim va kh nang an mon cla axit axetic &i vai thigt bi. ta chon thie bj than thap Id thép Khong wi ma X1SHIOT. LLL. Cie thdng s6 edn tra va chon phue-vu che qua tin inh tin: + Nhigtdé tinh todn: (= gus + 20°C = 117.6 + 20= 137.6 °C) + Apsuat tinh todn: vi thip hoat d9ng 3 ap suit thuding hoi Ingng rigng trung binh cla pha ling tong toRn thé Pus +Pc _ 956,614 945.928 fee 2 Nén: P= pigll = 951,295. 9,81. 29,8 + 47659,953 v 151,295 (kg/m) 125759,532 (Nim) 326 (Nim?) +H s6'bd sung do an mon héa hoe eila mii truimg: Vi méi dng axit 66 tinh &n mon va thd gian sit dung thit bj 18 trong 20 nam = Cy=1.2=2(mm) + Une.sudt cho phép tu chudn: Vi vat ligu la XISH10T = [9] = 140 (N/mm*)— (Hinh 1.1, trang 18, (7]) + Hesé'higuehink Vi thigt bi c6 be ldp ech ahigt > = 0.95 (trang 26, (7}) = Cing sud cho phép: [6] = [o1" = 133 (N/mm) a eareeieai sa Vi sit dung phucsng phip han hé quang dign, kiéu han giip moi 2 pha (Bang XIILS, trang 362, (61) 1.2, Tinh bé day: Ta c6: ly, = 133. .0,95= 387,863 >25 P9326 =s 4P 0002 805 = S' + C, = 1,805 +2 105 (mm) * cp, — 2133095 Quy tron theo chudin: S=4 (mm) (Bang XIIL9, trang 364, [6]) Bé day t6i thi€u: Spin =4 (mm) (Bang 5.1, trang 128, [7]) => Bé day S thda diéu kign. 1.3, Kiém tra 46 bén: + <0 = 4? 0,1. 0,001 <0,1 (thea) 1400 Frang 21Chung luyén Nutte - Axit axetic GOHD: Nauyin Van Lye Nén: [P]= 2S}@(S=C,) _ 2%133%0,95%(4 2) _ 9 369 5 p= 0,326 (thoa) b+(S-C,) 1400 + (4—2) Két udu: $= 4 (mm) 2, Diu oa mip: lh. Chon day va nap c6 dang hinh ellip tiéu chudin, e6 g3, lam bing thép X18H10T Chon bé day day va np bing voi bé day than thap: S =4 (mm), Kigm tra didu kign: AoinS-C), 5 R,+(S-C,) Trong dé: D)= 6 Vi day va nép 06 hinhellip i6u chun voi = 0.25 Ri =D, = Diu kign teén dutge théa nhue da kiém tra 6 phdn than thé, Két ludn: Kich thude cia day va nip: = Daring kinh trong: D, = @ = 1400 (mm) = hy=350 (mm) = Chiu cao gi: gy = 50 (mm) + BE day:S=4 (mm Dign tich b& mat trong: Stent .35 (m*) (Bang XTII.10, trang 382, 161) Vv. BE DAY Mim ater i : bea den ie NhiBLd6 tinh ton: t= tous = 117.6. CO) : {nh todin: P = Py s+ Peo Chon bé day 20 chiy trim la 3mm. Thé tich cdia a3 chay tran: V = 1,017. (50 + 50 +400 — 20). 3. 10°° = 0.00146 (m’) ‘Tra bing XIL7, trang 313, [6] = Khoi lugng riéng ela thép XISHIOT la xin Khoi Inng go chay tran: m= Vpxisinor = 11,572 (kg) 7900 (kg/m) Ap suit do ga chiy tran tac dung lén mam tron: P,, aaa 73,147 (Nim*) 4 Khoi lung rigng cia chit long tai day thap: prw = 927,309 (ky/m") Ap svat tly dink Praens = puwethgo+ Alc) 927,309. 9,81. (0,05 + 0,02432) Frang 22Chung luyén Nutte - Axit axetic GOHD: Nauyin Van Lye 676,059 (Nim* => P= 73,747 + 676,059 49,806 (Nim .0007 (Nim?) » mestts, 5s bs Athos etal eats Vi moi trudng axit 06 tinh an mn va thd gian sif dung thigt bj 1a trong 20 nam = C,=1.2=2(mm) + Gng sudt cho phép titu chudn: Vi vit ligu la XISHIOT = [a = 141 (Nim?) (Hinh 1.1, trang 18, (71) + He sd‘higuchinh: =| (trang 26, 171) + Ung sudt cho phép: (0) =» [ol = 141 (Nim) 99824 (Nimm*) (Bang 2.12, trang 45, (7]) + He sé‘Poisson: w= 0,33 (Bang XIL7, trang 313, (6]) os71 + Hi sé'diéu chink: oy 2. Tinh bé day: D6 voi bin won de ngam kep ch&t theo chu vi 3P(D Ung susit eve dai d ving chu vi 6, (ey (Cong thite 6.36, trang 100, [8}) 16 Boi vi ban c6 YC 1B: Guy, = 22 =(3) <{ol eos ep | 3? — ~4q9 [3% 0.0007 949 (mm oN YT 16lol9, Viexi4ixos71 Nen:$ +C,=3,849 (mm) Chon S = 5 (mm) Kiém tra diéu kién bit Bo véng eye dai d tim: W, = x (Cong thite 6.38, trang 100, [8]) pat 649,D, Voi: D, )_ 3 PRI > Wy, Oy 649,ES' 16" Dé dim bio diéu kiga bén thi: Wo< 2S wna Ww, = 2, 0000727001033") 16" 0571 «199824%5 => Bé day S da chon théa didu kién. Vay: S =5 (mm) Frang 23Chuing luygn Natée ~ Axit axetie GOHD: Nauyin Van Lye VE BICK GHED THAN ~ BAY va NAD Mat bich 18 bd phan quan trong ding dé ndt c phiin cia thigt bj eding nhu n6i exe phan khae vi thi€t bi. Céc loai mat bich thudng sit dung, = Bich lién: fa b6 phiin néi lién vai thigt bi (han, diic va ren). Loai bich ny chi yeu ding thiét bi Kim vige voi ép sust thap va dp suit trang binh. Bich urdo: chii yéu ding n6i dng din lam vige 6 nhiét 46 cao, dé néi eae bd bing kim loai mau va hop kim cia ching, dc bigt la khi cén lim mat bich bing vat ligu bbén hon thigt bi. + Bich ren: chi yu ding cho thiét bj lm vige 8 ap suat cao. ‘Chon bich duge ghép thin, diy va np Kim bang thép CT3, cifu tao etia bich la bich lin khdng 66, at ‘Tra biing X111.27, trang 417, (6, tng vi D, == 1400 (mm) va dp suse inh rosin P= 0,326 (Nimm*) = chon bich c6 ede thong s sau: Bu Jong D, D Dy D, D, b a z (am) (cai) 1400 | 1550[ 1500] 1460] 1413 35 24 40 Tra bang IX.5, trang 170, [6], vdi Ah = 400 (mm) = khodng each gitta 2 mat bich la 200mm va s6 mam gitta 2 mat bich Ia 5. = 86 mat bich cin ding dé ghép 1a: (15 +1).2 Khoiing cfch giita 2 mt bich theo thife 8! Akay 1,933 (m) D6 kin ctia méi ghép bich chi yeu do vat dém quyét dinh, Dém lim bling ede vat Higu imém hdn so vdi vat ligu bfch. Khi xiét bu long, dém bi bign dang va dién day lén cde chd ad ghé tren bé mat etia bich. Vay, dé dim bao 46 kin cho thiét bi ta chon dém Ia day amiting, ¢6 bé day la 3¢mm), Trang 24Chung luyén Nutte - Axit axetic GOHD: Nauyin Van Lye va. CHAN DO THAD tro ‘Tra bing XIL7, trang 313, [6] = Khoi Iugng riéng eda thap CT3 8: pers Khoi hvyng cia mot bich ghép than: mmacaaenase = $(D*-D," Pen = 4 850 kg/m’) 14°)0038 47850 = 95.486 ih) Kh6i hrgng cia mot mam: 100% — 8% — 10% )P sss:n07 = ,005.0,82.7900 Mom = =D, ges, 9,861 (kg) als Khoi lgng eta than tha mgan = 5(D'eeD') Haan Pris 7 p } (1,408? -1,47 }29.7900 = 4042,054 (kg) Khoi Ingng eta day (nip) thap: asin) = Ské ae Dass» Printer = 2,35 «0,004 . 7900 = Kh6i Iygng eta toan tha: m= 32 mich grpshin 71 Mois + Medin +2 Mayas 26 (ke) = 10786.231 (kg) 2. Finh chin do thip: Chon chan d@: thap dude 43 trén béin chan, Vat ligu lam chin 40 thdp 1a thép CTs, & Theo dy hitb 0 a P _mg _ 10805694 «9,81 645.10" (N) Tai trong cho phép trén mot chan: Gy 4 4 Be dim bilo dé an ton cho thiét bi, ta chon: G.= 4.10°(N) ‘Tra bing XIIL35, trang 437, [6] = chon chan do o6 cae thong s6 sau: L B Bi | Be H h . 1 a 260 | 200 | 225 | 330 [| 400 | 225 | 16 | 100 | 27 Frang 25Chung luyén Nutte - Axit axetic GOHD: Nauyin Van Lye ‘Thé tich mot chain 48: Verano ~ (384. 16. 330, 2 + 260. 16. 200). 10° = 0,005 (m°) Khoi lung m@t chin 40: Messe go= Versa se. Pers= 38,363 (ke) Vin. TAL TREO THAD Chon tai reo: tai treo duge g&n tren thin thip dé gitt cho thap khi hj dao dOng trong dieu kign ngoai edn ‘Chon vat ligu Him tai treo ft thép CT Ta chon bin tai treo, tai trong cho phép trén mot tai treo: G, = G, 10°(N). 2 A rs \ a 4 Nat t a WAZA Y a alle ‘Tra biing XIIL.36, trang 438, [6] = chon tai treo o6 exec thong $6 sau. L B By H s 1 a a 190 | 160 | 170 | 280 | 1 | 80 | 25 30 Khdi lugng mat tai treo: Masco Tra bang XI.37, trang 439, (61 = Chon tim l6t tai treo bling thép CT3 e6 ec théng s6 sau: + Chigu dai tim lot: H * Chigu rong tm lot: B = Be day tim Thé tich mot fm I6t tai treo: Vain c= Khoi hing mot tim I6t ta treo: Mn 5 (ke) 160. 320. 8. 10° = 0,001 (m*) pers= 9.244 (kg) Trang 26Chuing luygn Muito — Ait axetio GOWD: Nyuyin Van Lye ng din ting due n6i vi hit bi bhng mi ghép dl ‘rong hiét bi ny, asi dung m6 ghép thao do. DSi vai msi she thio dfs, agit ta fam dogn Sng nd, d6 a oan Gang ng 6 mat bic hay ren dé nb v6 ing + Logi c6 mt bich tuting ding vi ng 66 diiag kinh d > 10rum, + Loai ren chil yéu ding vi ng 06 duting kinh dS 10mm, ddi khie6 thé ding wi d 32mm, Ging din dg tam hing thép XISHIOT. due lam bing thép CT fu tg0 cia bich Lb 1 Guy uluiv tidus Nbigt d@ cba chét ling shdp ligu y= 103.4 CC) Tai nhigt do nay th # Khdi ugng riéng cia nude: py = 955,884 (kg/m") * Khéi luyng riéng cba axit: pa = 951,880 (kg/m') Nén: 1-31-32 0 0,001 = py = 953,078 (kg/m’) PrP Pa 980.392 "99802 ‘Chon loai dng néi cm siu vaio thiét bi. Chon vn te chit ing trong Ging 3 8 v= 0,2 (ol). ‘Duting kinh trong ciia dng noi: (a £3000 fo duge hoe khéng théo dug, liga khong ef. = [8G | 43000 = 0.075 cm) = 75 com = apa, ~ V3600%953,078% xx et ea = Chon dng 66 D, = 80 (mm) ‘Tra bing XII1.26, trang 409, [6] Buin y | em |e | oo | oo | on Libba oy w we] ws] iso] eleChung luyga Nutie — Axit axetie GOWD: Hguyén Van Lue 2. Ong hoi édiah thie: Nhiét 46 cia pha hoi tai dinh thap 1a tay = 100,1 (°C). Khéi hugng riéng cla pha hoi tai dinh thap: PMyo ___1x18,585 RT 224 1 99,14273) mm Chon van téc hoi ra khoi dinh thép 1a vp = 120 (mis). Dudng kinh trong cla ng néii: [4G _ [__4eai2eraz 3600p 5152 9 \ 3600% 0,607 x x 120 = Chon Ging e6 D, = 150 (mm), ra = 0,607 (kg/m’) D, ).142 (mm) = 142 (mm) ‘Tra bang XIIL32, trang 434, (6] = Chiéu dai doan dng n6i l= 130 (mm). ‘Tra bing XIIL26, trang 409, [6] => Cc thing s6 ella bich ting véi P = 0.326 (Nimm*) 13 Bu long D, D, D Ds. D, b & Z (um) (cai) 150 | 159 [| 260 | 225 | 202 | 20 16 8 3. Ong hose liu: Nhiét d6 ctia chat Ing hon hvu li tho = 100,1 °C) Tai mhigt 49 nay th = Kh6i hiyng rigng ctia nude: p = Khoi htm ri Nén:; 1 =>. + Pin Py Pa 958,326” 957820 Chon loai Ging ndi cam su vio thigt bi. Chon van te chit ling trong dng n6i 18 vi» = 0.2 (avs) utdng kinh trong cia dng néi: p= | 4S = [43194568 HOOP, yy \ H60O%9SEB03% 2x02 = Chon ding e6 Dy = 80 (mm). ‘Tra bing XTI1.26, trang 409, [6] = Che thong s6 ctia bich ting vai P = 0,326 (N/mm?) la 958,326 (kg/m) 957,820 (kg/m') 0,001 = pun = 958,303 (ke/m") = 0,077 (m) = 77 (mm) Bu ling po | om | > | om | o |e pee (am) ‘cai 80 was] 150] 8] is] 16) NNhigt d6 cia pha hai tai dinh thap fi tuw = 117.6 (°C) Chon van te hai vio day thap vw = 120 (rl). Frang 28Chuing luygn Natée ~ Axit axetie GOHD: Nauyin Van Lye uting kinh trong cia ding n6 #1764273) 0,145 (m) = 145 (mm) 1 3600Pa 3600 % 1% 3120 = Chon ding e6 Dy = 150 (mm). ‘Tra bing XIIL32, trang 434, [6] => Chidu dai doan dng noi |= 130 (mm), ‘Tra bing XIH.26, trang 409, (6] = Cée thong s6 etia bich ttng voi P = 0.326 (N/mm?) Ia Bu Jon, Dy D, D Ds. D, bh rt e (am) (cai) 150 | 159 [| 260 | 225 [ 202 | 20 16 8 5. Ong dén ling oto ndi dun: Nhigt d@ ciia chat ling tai dy thép 1 tow = 117,1. (°C) Tai nhigt dd nay tht = Khoi Iniyng ring ctia nutée: py = 945,391 (ky/m') + Khoi luting rigng cia axit: pa = 927,220 (kg/m’) nen, 1 - 3a, !=8w 00005, 1= 00005 Pw Px Pa 945,391” 927,220 Chon van wWe chit ling tong Sng n6i 8 Yew = 1 (av) uting kinh trong ciia ding n6 AmyyMyy __ [4 256885x59308 36009, V7” V 3600 927,309 x 1 = Chon ding 66 D, = 80 (ram) Tra biing XIIL32, trang 434, [6] => Chiu dai doan dng noi l= 110 (mm), ‘Tra bing XII1.26, trang 409, [6] = Che thong S6 ctia bich ting vi P = 0.326 (N/mm?) Ia 1,001 => prw = 927.309 (kg/m) n, 10976 (an) = 76 (earn) Bu Jon ds Zz (mm) (cai) 80 sol iss] 150] 128 18 16 4 Dy D, D Ds. D, h 6. Ong dein Leng ca kbd on Chon van t6e chit ling trong dng n6i 18 vw Busing kinh trong cia dng n 4Gw (36009, 2” V3600%927309 x nx015 => Chon ding e6 Dy = 80 (mm). Tra bing XIIL.32, trang 434, [6] => Chiu dai doan dng noi l= 110 (mm), ‘Tra bing XI11.26, trang 409, (6] > Cée thong s6 ea bich tng v6i P= 0,326 (Nimm’) 1 dun: 15 (ans), 073 (mn) = 73 (mem) Frany 29Chung luyén Nutte - Axit axetic GOHD: Nauyin Van Lye Bu Jong ds Zz (um) (cai) 80 sol iss] 150] 128 18 16 4 Dy D, D Ds. D, h KhGi luyng mae bch ghép Sing din Lng als woneanee= F0 =D, bipers == (0185? - 0,08"): 0,018 7850 = 3,088 (ke) Khoi lugng m6t bich ghép dng din hoi: (0.260° - 0,150" )x 0,02 7850= 5,561 (kg) ime scne= £(0°~D2 5 = xX. LOD CACH SHIT s Trong qué tfinh hoat dng ciia thap, do thdp tie xtic v6i khOng khi nén abiét lwgng tn that ra mai trang xung quanh ngay cing In. BE thip hoat dng én dinh, éting vai cae thong s6 di thigt ké, ta phai tng din hing hoi dét gia nhigt cho ndi dun dé thép kh6ng bi ngudi (nhit la sin phéim dinh, dnh hung dén higu suit elia thép). Khi d6, chi phi cho hoi d6t sé ting. Dé thap khong bj ngugi ma khong ting chi phi hoi 46, ta thiét ke lop quan than thd, Chon vat ligu céch nhigt cho than thép Ia amiang o6 b8 day 18 5, ‘Tra bang 28, trang 416, [4]: Hé s6 din ohiét cia amiting 1a iy = Nhiét lugng t6n that ra m6i trudng xung quanb: Qu = 0,05.Q5= 0,05.265,148 = 452734,492 (kI/h) = 125759,581 (W) Nhi€t tdi mat mat rieng: Qe Be (ty ta) Beat, (Wim?) Hh nhigt bao. 151 (Wim.K). Gn Trong a6: = ty emhigt 06 eiia lop each nhigt tip xtie Voi be mat ngodi eda tha. ta mhigt 49 ciia lp cach mhigt tiép xiie vai khong kh, + Aty:higu sO nhigt 46 gitta hai hé mat cia Ip cach hig Dé am toa ta lity Aty = Mtmae = tay ~ Chon us = 27°C = At = fy: dign tich bé mat trung binh cia thap (ké ca Ip each nhigt), m?, fy = nDyHl +P a + Pat Sis +75. 4 m(De+ Saint 5)H ‘Ta 06 phiting tinh: FRM 0004 +8,)298 oRi91 1 1a08+8,) "8, € 98,1918, = 1,404 + 3, > 8, =0,01445 (m) = 14,45 (mm) Frang 30Chuing luygn Natée ~ Axit axetie GOHD: Nauyin Van Lye Vay: chon 8, = 15 (mm). “Thé tich vat ligu cach nhigt cin ding: v (D.+ 2San+ 6,).5, = m.(1,4 + 2, 0,004 +0,015).0,015. 29.8 TINH THIET BI PHU 1 THIET PE BUN S01 BAY THAD s Chon thigt bi dun s6i day thap Ia ndi dun Ketl. Gng truyén nhigt dutge lam bang thép XI8HIGT, kich thie ding 38 x 3 + ining kinh ngodi: dy = 38 (mm) = 0,038 (mm) + BE day Ging: 6= 3 (mm) = 0.003 (mm) 18 hol mie 6 2,Sat di trong ding 38 x 3. Tra bing 1.251, trang 314, [5] + Nhigt h6a his 189500 (ike) + Nig d9 SOi: ty,9% b= 12625 CC) Dang sin phim tai day e6 nig Tre khi vo n6i dun (ng): ts + Sau Khi dutge dun si (hot 17,1 CC) 17.6 CC) 1. Suit lieing ht mide ein ditnae Can bing mht cho toin thép: Qa + Grhrs = (R41) Goro + Gols + Gwhns + Qn Gil sit Qa = 0,05Qu = 0,95Qa= (R+1) Gory + Gotlos ~ hrs) + Gw(hws ~ hes) hrs = crtes = [Xyey HUE )e Ites hws = ewetws = [Kyey +0 Kw )ey Its, f#hps = entos =[Xp¢y +1-Xpe, Ios o1D= Katy HRI la’c nq Xp = 0,986 = ts = 100,1°C Frang 31Chung luyén Nutte - Axit axetic GOHD: Nauyin Van Lye 1.1, Nhigtdung rigng: ‘Tra bang 1.249, trang 310, [5] = Nhigt dung rigng cla nude & 100,1°C = 4,22013 (ki/kg.K) = Nhiet dung riéng ea nude 0 103,4°C = 4.22442 (ki/kg.K) = Nhiét dung riéng ciia mye 8 117,1°C = 4,24507 (kirkg.K) Tra bing 1.154, trang 172, [5] = Nhigt dung rigng ea axit axetic 6 100,1°C = 2,430525 (kikg.K) => Nhigt dung riéng ciia axit axetic 6 103.4°C = 2,44785(kU/kg.K) = Nhigt dung riéng cia axit axctic 6 117.1°C = 2.519775 (ki/kg.K) 1.2, Enthalpy: ss hys = (0,3. 4,22442 + 0,7. 2.44785). 103.4 = 308,217 (ki/kg) ‘© hws = (0,005. 4,24507 + 0,995. 2,519775). 117,1 = 296,076 (ki/kg) f¢hps = (0,955. 4.22013 + 0,045. 2.430525). 100,1 = 414,374 (ki/kg) 13, Nhigtn6a hei Tra bang 1.250, trang 312, [5] = Nhigt héa hoi eda mde & 100,1" Ding tosn dé 1.65, trang 255, 15] = Nhigt héa hoi ca axit axetic 3 100,1°C = ‘Tra bing 1.251, trang 314, [5] = Nhigt héa hoi eda nude 62.5 at = 189.5 (ki/kg) Nén: rp = 0,955. 259,76 + 0,045. 418,6 = 2176,908 (kW/kg) = ry = 2250,76 (kl/kg) 100 (Keal/kg) = 418.6 (kl/kg) 1.4, Tinh lung hai nude cin ding: hit lugng cn cung ep: RENGp fy +Go (lags Hyg) + Gy (lys —h HEHEHE Os Nei ding hai mide bao hia (Khong ehita sim) d& cap nhigt thi: Qa= Gyo. hyo Q 2. Tiéw sd whiét dé trang tink Chon kidu truyén nhigt ngwse chiéu, nén: le 19054689,833 (kI/h) Vay: Gyo = 22 =4135,506 (kgm) (12625 -117,1) -(126,25~117,6) Bg OS a6as=1Td 8AM RD 12625-1176 theo cing thite ahi d6i vai twsng phang: (Wie?K)Chung luyén Nutte - Axit axetic GOHD: Nauyin Van Lye Vai = cg: he sO etip nhigt cla hoi a6t (W/m?.K). = ashe s6 ep nhigt cia sin phim day (Wim) = Shes mhigt trd qua thanh Gg va Kop cia, 3.1, Nhigt ti qua thanh dng va I6p edu tact : * (Wien 3, y a Trong a6: + tar inhige d6 ea vich tgp xtc vai ho At (trong Sng). °C + to inhigt dd cia vich tgp xtc vai sin phim dy (ngodi Sng). °C BE day thanh ding: &,= 0,003 (mm) + He s6 dfn nhigt ca thép khong gi: 4 = 16,3 (WimK) (Bang XIL, trang 313, (61) = Nhigt td I6p bain trong Sng: r1 = 1/5800 (m".K/W) (Bang 31, trang 419, [4]) trd lop cau ngoai Sng: r:=1/5800 (m*K/W) 5.289,10° (m2. K/W) Nen: Ee 3.2, Xde dinh he s6 eifp nhigt cla dang sin phidm day ngoai Sng: Ap dung cdng thife (V.89), trang 26, [6] erate Nhiét 46 s6i trung bin ciia dng sin phim & ngoai dng: = 11735 (C) => Ts = 117,35 +273 = 390.35 (K) ‘Tai mhigt 49 s6i tung bin thi = Khoi lung riéng cia pha hoi trong dong sin phim 3 ngoai dng: y= PM = bess sae RT, (117354273) 273 = Khoi hnmg rigng ciia mute: py =945,1935 (ke/m’) (Bang 1.249, trang 310, [5]) Khoi ung rigng cia axit: px = 926,77 (kg/m) (Bang 1.2, trang 9, [5]) 1_Xw ,1-Xw 0,005, 1-0,005 Nen: 1a %w 427 %w _ 00005, 10,005. DP Px Pa 945,935" 926.77 #6 nhot cita mfBe: py = 2.43.10" (N.s/m*) (Bang 1.249, trang 310, [5]) = DO nhdt cia axit: 44 = 3,60.10% (N.s/m’) (Bang 1.104, trang 91, [5]) Nén: Ig = xwlgqiy + (1 ~ xw)lgua = 0.016 1g(2.43.10%) + (1 -0,016)1g03,60.10°) 487 = = 3,577.10" (Nim?) = He s6 din nhigt cia nude: Aw = 0.68547 (WimK) (Bang 1.249, trang 310, [S}) = He s6 dfn ohigt cia axit: Aa = 0.15153 (WimK) (Bang 1.130, trang 134, [5]) Ap dung e6ng thite (1.33), trang 123, [S)) 0,001 = p= 926,860 (kg/m) Frang 33Chung luyén Nutte - Axit axetic GOHD: Nauyin Van Lye A= hy. Xw +t Aad - wy) — 0,72 wal] - Xw)Coy~ ha) = 0,152 (WhmK) = Nhigt dung rigng cia nic: ey = 4245,495 (WkgK) (Bang 1.249, trang 310, [5]) = Nhigt dung ring ctia axit: ca = 2521,0875 (/kgK) (Bang 1.154, trang 172, [S]) Nén: €= eK y +64. (1 = Ky) = 2529,7095 (kk) + Sife cding bé mat cia made: oy = 0,5542 (Nim) (Bing 1.249, trang 310, [5]) Site caing b& mat ea axit: 0 = 0,0182385 (Nim) (Baing 1.242, trang 300, [S]) Nen: 6 = 2% = 0.018 (Nim) + Nhigt hoa hai ciia nite: ry = 2214420 (I/kg) (Bang 1.250, trang 312, [5]) # Nhigt hoa hot cla axit: r= 606460,6 (kg) (Tos 48 1.65, trang 285, 15]) Nén:r=AyRq +t (I > fy) = 415800,397 (U/kg) 3.3, Xe dinh hé s6 elp nbigt cla hai dét wong ding: : {npied Ap dung edng thie (3.65), trang 120, [4]: «., = 0,725| Pe. —_ Vist, -twdy Dang phép ldp: chon ty) = 126,1961412¢°C) Nhigt a9 trang bioh ciia mang nucle ngung 14: y= % (ty + b1) = 126,223 CC) Tai mhi€t a6 nay th * KhGi lung riéng cia nude: py = 937,935 (kein) # BO nhdt cia nude: py = 2.25.10" (N.slm") + He s6 din nbige cba mute: 2 =0,686 (Wim) Nén: dy = 45649,776 (Wink) 2 a= Hay ~ ty) = 2458 642 (Wi Gi = Ga = 2458,642 (Wimn*) (xem nhigt tdi mst mat 18 Khong dang KE) tar GBR = 124.896 (°C) 325,828 (W/m'K) (v6i q= q) 5 (t2 ~ ts) = 2458,641 (Wim’) sai sb 100% = 0,00004% < 59% (tha) KEL ludn: ty = 126,19614 12°C va ty2= 124,896°C 3.4, Xe dinh he sé tmuyén nhie: i 276,252 (Wim’K) see + 5.289.107 + 45649,776 325,828 4. Bé mat teunén ahiet: BE mat truyén nhigt duge xée dinh theo phudng tinh trayén nhigt: 9054689,833.1000__ 494-970 (a2) K.At,, 3600«276,252 «8,898 5. Cin tao thiét bis Frang 34Chung luyén Nutte - Axit axetic GOHD: Nauyin Van Lye Chon s& 6ng truyén nhigt: n= 1657 (ng). Ong duge b6 tri theo hinh luc gite déu, Chigu dai Sng truyén nhige: L = ss 5,616 (m) = chon L= 6 (m) 2 Tra bang VIL trang 48, [6] = S6 Gag trén diving chéo:b = 47 (ng) Tra bing trang 21, [3] => Bue Ging: t= 48 (mm) = 0,048 (m) Ap dung cong thife (V.140), trang 49, [6]: = Buring kinh trong ella thigt bi: D = 1(b-1) + 4d, = 36 (m) . THIET EE LAM NOUOH SAN PRAM BAY = Chon thiét bj lam ngudi sin phim day la thigt bi trayén ahigt Gag Kéng Gag. Gng trayén nhigt due lam bang thép XISHIOT: = Kich thutte dng trong: 38 x 3 = Kich thuve dng ngoai: 57x 3 Chon: = Nue Kim lanh di trong Gng trong vdi nhigt d} vao ty = 27°C va nhigt dO rate = 43°C + Sin phdm day di trong Ging ngoai vai nhiet AO vao tws = L17.1°C va nhigt 46 ra to 35°C. CA bing nhigt: Q = Gw(hvs ~ hive) = Ge (tne ~ by) Nhigt dung riéng eta nttée 0 35°C = 4,178 (ki/kg.K) Nhigt dung rigng cia axit 6 35°C = 2.0735 (ki/kg.K) én: hnwn = (0,005. 4,178 + 0,995. 2.0735). 35 = 72,940788 (kI/kg) ‘Tra bing 1.250, p312, ST 1 = Enthalpy ctia nugde 6 27°C = hy = 113,13 (kikg) = Enthalpy eiia nude 0 43°C = he = 180,17 (kikg) Lugng nhigt trao d6i: Q = Gris ~ he) = 461537,184 (KI) = 6884,505 (kg/h) Susi luong nude edn dang: G, = 2, blew sf mhiét dd trang fink: Chon kiéu tuyén nbigt nguac chiéu, nen = 43)-@5—27) = 29,695 (K), B. Web sé truyén nbiéts He s6 truyén nhigt K dude tinh theo cong thie: Frang 35Chung luyén Nutte - Axit axetic GOHD: Nauyin Van Lye W/m?) Voi = Gg: hg sO ctip nhigt cia dong mide Ignh (Wim?.K), + ay :he sO edp nhigt cia dong sin phim diy (W/m?.K). re: nhigt rd qua thanh Gng va Iép cu. 3.1, Xe dinh he s6 eafp nhigt cla nude trong dng: Kich thude eiia dng trong: = Dutdng kink ngoai BG diy Ging: 6,= 3 (mm) = 0,003 (m) = Busing kinh trong: dy = 0,032 (m) Nhigt 46 trang binh ciia dong nue trong ding: ty = % (ty + te) = 35 CC). Tai niet dO nay th: Kh6i luting ring ciia nude: py = 994 (kg/m) BO hat cia nue: vy = 7.23.10" (m/s) He 86 din nhigt cia mde: Ay = 0,626 (WitmK) = Chun so Prandtl: Pra = 4.9 Vaan te nude di wong ding, 8 (am) = 0,038 (mm) v,=— 4G. -_4 6884505 ___ 9 399 (mys), 3600p,nd; 3600% 994% nx 0,03 Chuan sé Reynolds Re, = Nabe: = 23820082 _ 195877,980 > 10": che 6 chiy ri v, 728.10 Ap dung cong thnte (3.27), trang 110, [4] > cdng thite xae dinh chusin sof Nusselt: 0,021.6, Re? Pro Pres ‘Trong a6: £1 ~ he s6 tinh dén Anh hurdng ella he sO eaip nhigt theo ty 1é gida chigu dai Lva dating kinh d eta 6g. ‘Tra bing 3.1, trang 110, [4] = chon = | 7 N nhigt cia nude trong Ging: Oy = 3.2, Nhigt ti qua thanh Sng va I6p edu: = = (Wim). Trong a6: = tay imhigt d6 cia wich tig xite vai sin phim day (trong éng trong), # tuo !mhige dé cila veh tig xi Vai nude lanb (agoai Sng trong), °C & jena 2, Frang 36Chung luyén Nutte - Axit axetic GOHD: Nauyin Van Lye + BG day thanh Ging: 6 = 0,003 (m) HG 86 dfn nhigt cba thep khing gi: A= 16,3 (WhmK) = Nhigt td lop bin trong Sng: 7 = 1/5000 (m?.K/W) + Nhigt td lop eu ngoai Sng: 2=1/5800 (mm KW) Nén: Bi: = 5,565.10° (m7K/W) 3.3, Xéc dinh hé s6 cap nhiét cia dang sin phim day ngoai cng: ich thuGe cia dng ngoai = Dating kink ngoai: D, = $7 (mm) = 0.057 (m) = BG day Ging: 6,= 3 (mm) = 0,003 (m) Dating kink trong: Dy, = 0.051 (m) Nhigt d@ trung binh cita dong sin phiim diy ngoai ding: tw = ¥4 (tws + twn) = 76.05 (°C). Tai mhigt d6 nay th = Khoi hngng rigng cia nude: p = Khoi yng rigng Nén: 1. %w ,!"%w P Py Py 97417 985.5425 = BO nhdt cia mtBe: py = 3.73.10" (Ns?) = DO nhdt cia axit: sq = 4.75.10 (N.s/m’) Nén: Igu = xwlgq + (1 ~ xw)lgua = 0.016.1g3.73.10%) + (1 -0,016)1g(4.75.10°) 325 = w= 4,734.10" (N.sim?) He s6 din nhigt eda nude: Ay = 0,672 (Wik) HG sé dfn nhigt cia axit: 4 =0,161 (WimK) Nén: A =Ay. Xw+ Ra(1 = Xw) 0,72 XwAl = xwi(hy- hal = Nhigt dung rigng cia nude: ey =4191,84 (/kgK) = Nhigt dung rigng ctia mide: e4 = 2294,4725 UikgK) Nen. 2303,959 (kek) 974,17 (kg/m?) 985.5425 (kg/m) = 0,001 = p = 985,485 (kg/m) 161 (WimK) NEw tea (I> Ky. Ap dung edng thite(V.5), trang 12, [6]: Pr Vin tc cia dong sin phim day ngoai dng 4G 4<2068.421 3600px(D; =d2) — 3600* 985.485 xx x(0.05T 0,038") aiing kinh tueing dating: dhe = Dy-~ dy = 0,051 ~ 0,038 = 0,013 (m) Chuiin s Reynolds _Wdgp _ 0,642 0,013 985485 _ yh 4,734.10 Ap dung cong thite (3.27), trang 110, [4] > c6ng thite xéc dinh chudin s6 Nusselt 0,642 (avs) Re 17362,792 > 10°: ehé 9 chay r6i Nay oat, Rede” 2) Trong d6: e; ~ he s6 tinh én nh hiding ctia he s6 ep nhiet theo ty Ie giita chiéu dai L va diting kinh d ciia dng. ‘Tra bing 3.1, trang 110, [4] = chon & Frang 37Chung luyén Nutte - Axit axetic GOHD: Nauyin Van Lye uy. He s6 efi ahiet ca ddng sin phim dy ngoai ding: ow = ~Y Ding phép lap: chon tw Tai nhigt 9 nay th DO what eila mde: py = 5.12.10" (Ns?) BO nhdtciia axit: ua = 7.51.10" (N.sim?) Nén: Igy = xwlgn + (I ~ xw)lgua = 0.016.125.12.10") + 1 -0.016)1g(7.51.109) 127 => ww = 7,460.10" (N.sim?) = He s6 din nhigt cia nue: Ay = 0.652 (Wik) He s6 alin ahigt ca axit: Ax =0,165 (W/mK) Nén: Awi =A. kw Aa] = Xw)= 0,72 xw(l = XW) = Nhigt dung riéng cia mde: ey = 4178 (kgK) + Nhigt dung ring ella ne: ca = 2176,834 (Ike) Nen: ews 2186840 (kak) 4.361476 (°C) 0,165 (W/mK) NEw +4. (I= Ey) Syittws Ap dung edng thite (V.38), trang 12, [6]: Pryy = “S" 860 Nen: Nuw = 107,074 = cy = 1329,497 (W/mK) ov (to — fy) = 28834,837 (Wim) = c= qw = 28834,837 (Wim?) (xem nhigt tii mat mat 18 khOng ding ké) 3 tea = tei GEH= 38316 CO) = Pry = 4.509 Nin = 44512 = 09 = 8695,774 (Wim?) = gy = Oy (tw2 ~ ty) = 28834,837 (Wim*) Saw Kiém tra sai so: | 100% = 0,000001% < 5% (théa) Kit ludn: ty = 54,361476°C va t 8,316°C 3.4, Xée dinh hé sf uy nhiss 702,432 (Wim'K) pee 5565.10 + I 3005,774 1329,497 4 Bé mat teuyén ubiét BE mat teuyén nhige duge xée dinh theo phuting tinh trayén nhigt: Q 461537,184 1000 _ 6 146 fn?) Kat, 3600%702,432%29,695 5. Olin tao thiét bi: Frang 38Chung luyén Nutte - Axit axetic GOHD: Nauyin Van Lye Chiéu dai Sng truyén mhige: L = 55,899 (m) = chon L = 57 (m) a,+4 2 781,250 > 50 => «= 1: thda Kiém tra; = 5 0032 Két ludn: Thiét bj im ngudi sin phidm day Ia ehigt bj ruyén ni chigu dai ng trayn nhigt L = 57 (m), chia thanh 19 diy, mi dy 3m. Ging Weng dng voi Chon thiét bi ngung ty vé ~ dng loai TH, dat nm ngang. Ong truyén nhigt dutge Kim biing thép XISHIOT, kich thue Ong 38 x 3: = Dating kink ngoai: dy = 38 (mm) = 0,038 (m) = BG day Ging: 6,= 3 (mm) = 0,003 (m) = Dafng kink trong: dy = 0,032 (mm) Chon: = Nute lam lanh di trong dng voi nl = Dang hi tai dinh di ngoai ng vai nhiét 46 nguing tu taping = 100,1 °C) 1, Suit cong nutic lam tanh edn drwy : Can bling nhit: Qy Nén: Qu =(R+ Dt Lugng nude edn ding: 2. Diéw sé whiét dé trang bink + Chon kiéu truyén nhigt neue chiéu, nén: 7) = (100,1=43) _ re = 64.771 (KD. "100,143 3. Te a6 trayén He 6 wuyén nhigt K due. theo cng thie: k= cum +E, 4 Vai ay hg 86 cfip nhigt cia dong nude tanh (W/m?K). dong 1 bg 86 ealp nbigt cdi dong hoi ngung tu (Wim?.K), Frang 39Chuing luyen Nutie - Ait axetic: GOWD: Nguyen Van Lye = ie mhigt rd qua thanh Gng va Idp eu, 3.1, Xae dinh he s6 ed{p nhige cila nude di trong éng Nhigt d6 tcung binh cia dong nvide trong Sng: = ¥2 (ty + te) = 35 °C). Tai nhigt 46 nay th Khoi inmg riéng cia nutte: py = 994 (ka/m") + BG nhat cia nude: vy = 7.23.10" (m’/s) + He s6 din nhigt ca nude: Ay = 0,626 (Wik), Chon van te nude di trong Sng:vs= | (rvs) 3 8ssngs n= Oe 4 SSBEBISH kgs 3600p, ndzv, 3600x994 "x0, ‘Tra baing V.IL, trang 48, 6] => chon n= 61 (Sng) = Van te thu t cia mde trong Sng: 46, 4 133983,158 3600p,nzd? ~ 3600x994 x 61x «0,032 Chuan s6 Reynolds re, ~Nalle 07630082 v, 723:10 Ap dung cong thife (3.27), trang 110, [4] = céng thie xac dinh chudin s6 Nusselt: 0,021.5,.Re! Pr “{B) = 0,163 (m/s. :3779,509 > 10": ché dé chay roi Nu, Trong 46: 1 ~ hé s6 tinh dén Anh hudng ctia hé s6 efip nhigt theo ty 1é gidta chiéu dai L va ding kinh d ciia dng. Tra baing 3.1, trang 110, [4] => chon ¢; He s6 eflp nhigt cia mute di trong Sng trong: On 3.2, Nhigt ti qua thanh Sng va Ip e4 -(W/m?), Trong d6: tur imhigt d6 cia vieh tip xi V4 hei gus # G2 mhigt d6 eta véeh tid xi Vor nue lan, °C BG day thanh dng: 8, 0,003 (mm) = He s6 din nhigt ca thép khong gi: 4 = 16,3 (Wink) = Nhi¢t tr lop ban trong Gg: r, = 1/5000 (m= K/W) = Nhigt td lop eau ngoai Sng: r2=1/5800 (m"K/W) Nen: Si = 5,565.10 (m°.K/W) Trang 40Chung luyén Nutte - Axit axetic GOHD: Nauyin Van Lye 3.3. Xée dinh hé sO efip nbigt cia hai nguing tu ngodi dng Didu kign: = Ngung ty hot bao hoa = Kh6ng chita khong khi khong ngung. = Hoi ngung tu 6 mat ngoai sng = Mang chét ngumg ty chay ting. = Ong nim ngang. Ap dung cong thife (3.68), trang 120, [4] B ng damn chige nim ngang thi: 5 emt 1d, ‘Tra biing V.IT trang 48, [6] = v6i s6/ ding n = 61 th sO Ging teen dudng chéo cia hinh 6canh Ris b=9 Tra hinh V.20, trang 30, [6] = hé s6 phy thude vdo eich b6 ti dng va s6 Sng trong smi day thing ditng Ia cq) = 0,62 (vi xép xen ké va s6 Ging trong mbi day thing ditng la 9) = He sf eaip nhigt trung binh ciia chiim Ong: caging = eats = 0,624 Dang phép lap: chon tw: = 89,915675 CC) Nhigt d6 trung binh ciia mang chat ngung ty: ty = M4 (tmp + ts) = 95,008 (°C) ‘Tai mhigt 6 nay thi = Khoi hing riéng cia nude: p Wg cia axit: pa 0955 961,795 (kg/m) 963,741 (kg/m') 0,001 => p = 961,882 (kg/m) © BG mhdt cia nude: py = 2.97.10 (N.s/m’ + BO nhdt cia axit: y= 485.104 (N.simn’) Nén: Ig. = xolgpy + (1 ~ xo)lgha = 0.986.1g(2.97.10°) + (1 = 0.986)1g(4.85.10°) 524 = p= 2,990.10" (Nsim’) # He s6 din abigt cba nude: dx = 0,681 (WhmK) + H8 s6'din abigt cia axits hy = 0,156 (WimK) Nén: h=hy. Xp+ Ral Xp) 0,72 Xp. - Xp\(N~ ha) = 0,641 (WimK) = Nhigt ngimg ty cia dong hot: r= rp = 2176,908 (kiPkg) = 2176908 (Irkg) Nén: en = 10559,531 (Whar'k) > Ungne = 6546,909 (Wit?K) = doaine = Uosne (tge~ tw) = 66675,849 (Wier) = 4)= Gosia = 66675,849 (Wa) (xem nhige ti malt mit 1 khOng ding ké) tei 42m = 52,813 CC) = Pry = 3.393 > Nu, = 191,340 3743,093 (Wim?K) ia U2 — &) = 66675,863 (Wim? Trang 41Chung luyén Nutte - Axit axetic GOHD: Nauyin Van Lye 100% = - 0,00002% < 5% (théa) ooo Kétludn: ty = 89, 915675°C va tya= 52,813°C 3.4, Xée dinh hé s6 truyeén nhigs k-—| 7 (024,207 (Wim"K) t+ 5565.10 +! _ 66675,863 66675849 4. Be mat trumén ahiéts Bé mat truyén nhige due xée dinh theo phuemng tinh truyén nhig Qu 8982230.9821000 97 611 Kat, 3600%1024,207% 68,777 tao thiét bis 1 truyén nhigt 1 (Ging). Ong duge b6 wi theo F L= — 5 -= 50607 (m) = chon L= 6 (m) inh Iue gide du Chigu dai Sng truyén a $6 Gg tén dudng chéo: b= 9 ng) Tra bing trang 21, [3] => Bude dng: t= 48 (mm) = 0,048 (m) Ap dung edng thite (V.140), trang 4, (6) = Duting kioh trong eta thik bf: D = WbeL) + 4, 36 (mn) IV. THIET £1 TRAO DEL NHIET G14 DONG NHAD LIEU va Sin HAM DINE = Chon thist bi tro déi nhigt gitta dong nhap ligu va sin phdm dinh [a thigt bi teayén nhigt ng Ing dng. Ong trayén nhiet duc lam bang thép X1S8HIOT: = -Kich thutie6ng trong: 38 x 3 = Kich thtve dng ngoai: 57x 3 Chon: = Dang nhip ligu di trong Ging trong vai nhiét d6 vao try Sin phém dink di trong dng ngoai véi nhigt 46 va0 tos = 35°C. FC, }00,1°C va mhiét 46 ra to, 4. Uhiét dé din va cia ding nbip lieu + Can bing nhigt: Q = Gr(hin ~ hry) = Gothos ~ hex) Tai nigt d6 27°C thi: = Nhigt dung riéng cia mutde: ew = 4,178 (kivkgK) # Nhigt dung riéng ctia née; cx = 2,031 (ki/keK) = hwy = crtey = [%pey +(1-%y Jey Ite = 72,230 (Keg) Tai mhigt d0 35°C tht Trang 42Chung luyén Nutte - Axit axetic GOHD: Nauyin Van Lye = Whigt dung rigng etia nude: ¢, # Nhigt dung riéng cia axit: eq Roly +R Iq tow Nén: Q = Goflhos ~ hon) = 461537,184 (ki/h) 178 (ki/kg.K) 2.0735 (ka/kg.K) 42,915 (kkg) hye = 2 hyp = 156,525 (8 mG tes (amg) Ding phép lap => tx = 56,2134 °C) ecanasiaree aa Chon kigu truyén nbigt nguée chidu, ay, = 11004 = 36,2134) = 85-27) a 100, 2134 La 35-27 1,083 (K), 3. Heb sé truén nbiée + He s6 truyén nhigt K due tinh theo cong thie: Voi ap: hé sO efip ahigt cia dong nlp Tigu trong ding (Wim?-K), = ao:hé s6 ep nhigt eda dong sin phiim dinh ngoai 6ng (Wim?.K). = Die whigt ud qua Wid dug va Wp eau. 3.1, Xée dinh hé 86 eifp nhigt ela dong nhdp lieu trong Sng: Kich thude ella dng trong: uring kinh ngoai d, = 38 (mm) = 0,038 (m) BE day ding: 8.= 3 (mm) = 0,003 (m) + Paring kinh tong: dy = 0.032 (im) Nhigt d6 trang binh cia dng ahip liGu trong Sing: te = (tev + tx) = 41,6067 (°C). ‘Tai nhigt 46 nay thi ing riéng cia mide: Khoi ining riéng cia axit: py New: += 385 o3 Pr Py Pa 994525 * 1025,152 + BO mhdt cia me: py = 635.10 (Ns/m) + BO nhgt cia axit: 4 = 8.82.10" (N.sim’) Nén: Igue= xrlgqts + (1 ~ XPlgHa = 0,588.1g(6,35.10") + (1 -0,588)lg(8,82.10°) 3,138 = pp = 7,273.10" (N.sien?) He s6 dfn nit cia nude: Ay = 0,636 (WimK) + HG sé din abit cia axit: a = 0,168 (WimK) Nén:fe= in. e+ RAL = X= 0,72 xe = x09an~ Pad = Nhigt dung riéng cia nutéc: ey = 4178 (kek) 991,525 (kg/m!) 1025,152 (kg/m’) 1001 = pr = 1014,827 (kg/m) 237 (Wik) Trang 43Chung luyén Nutte - Axit axetic GOHD: Nauyin Van Lye + Nhigt dung riéng cia nse: Nén: ¢r= eX + 64. (I> Xp 729,417 (kg) 303,959 (kg) Ap dung cong thiée (V.35), trang 12, [6]: Pr, ‘Van téc cda dong sin phim déy di trong éng: 4G 43000 3600pxd, 3600x1014 827 x 20,032" Chudn s6 Reynolds ve 021 (mis) HORN 0.032 OU82T _ 45588,056 > 10° sche’ d6 chit ri Ms 7223.10 Ap dung cong thifc (3.27), trang 110, [4] = eng thite xc dinh chuiin s6 Nusselt: Rey Nuy = 0,021.5).Re?? Pr’ {®) Pr, ‘Trong 6: ¢; ~ he s6 tinh dén anh hung ciia hé s6 cap nhigt theo ty Ié gia chiéu dai L va dung kinh d cia Sng. ‘Tra biing 3.1, trang 110, [4] = chon &) Nuyhp He s6 cfp nhigt cia dong nhp ligu trong Sng: 3.2, Nhigt ti qua thanh Sng va Ip edu fate wim’), Trong dé: = tor rmhigt d6 cia véich tie xtie vai sin phdm dinh, °C = too mhigt d6 cia vich tie xc voi dong nhap ligu, °C tht ‘= Nhit ted Ip cau ngoai Gng: rs =1/5800 (m°.K/W) Nén: Y= 5,289.10" (m?°.KW) 3.3, Xde dinh hé s6 ci{p nhiét cila dng sin phdm dinh ngoai Gng: Kich thude cba dng ngori + During kinh ngodi: D, = 57 (mm) = 0.057 (m) = Be day dng: (mm) = 0,003 (m) + Duting kink trong: Dy = 0.051 (m) Nhigt d@ trung binh ciia ding sin phim inh ngodi Sng: tp = M4 (tos + tox) = 67.55 (°C). Tai mhigt do thi: © Khoi lutyng rigng ciia nutBe: py = 979.123 (kg/m') = Khoi ling rigng cba axit: py = 995,3175 (kg/m) Trang 44Chung luyén Nutte - Axit axetic GOHD: Nauyin Van Lye _ Xp _ 0.955, 1-0,955 Po Py Px 9794123 995,317: © BO mhdt cia mute: py = 4.16.10" (N.sim*) © BO mhdt eiia axit: jrq = 5,94.10% (N.s/m*) Nén: Igo = Xplauy + (1 — x)lgpia = 0,986.1g(4,16.10%) + (1 -0,986)1g(5,94.10") 379 => pip = 4,182.10 (N.sim’) + He s din nhiét ciia mide: Ay = 0,666 (W/mK) © HG s6 din nhiét cia axit: 24 = 0,162 (WimK) Nén: Ap =2y. Xp + Ral Xp)~ 072 Xp Xp)(An~ Aa) = 0,627 (WimK) = Whigt dung rigng eiia nube; cy = 4185,04 (keK) + Nhigt dung rigng cia nude: cx = 2248,1475 (ikeK) Nén: cy =n Xp +0. (I~ Xp) = 4097.88 (IkeK) Nen: = 0,001 => po = 979.840 (kg/m) Ap dung cong thite(V.35), trang 12, [6]: Pr, = 242 =2,732 ‘Van te ciia dong sin phém dinh ngoai éng: 4931579 F) ~ 3600 x979.840 x nx (0051 0,038) During kinh twong ducing: che = Dir — dn = 0,051 — 0,038 = 0,013 (m) Chudn s6 Reynolds VodaPy _ 0.291 0,013«979,840 By 4182.10" = 2300 < Re < 10000 => Ché a chay qua do. Ap dung cong thife (V.44), trang 16, (6] = cong thie xée dink chusin s6 Nusselt Ruy =K,.t, ng? (Be Pras) Trong ds: = 61 — he sO tinh dn Anh hudng eda he $6 exp niet theo ty Ie gia chigu dai L va during kinh d cia Sing, ‘Tra bing 3.1, trang 110, [4] => chon e; = ko— he s6'phu thude vio Re ‘Tra bing trang 16, [6] => k, 0,291 (amis) = 851,772 19,683 He s6 ef’p nhigt cia dng sin phim dinh ngoai Gng: a = Diing phép lap: chon ty, = 59,24484523 (°C) Tai mhigt d6 may thi © BG mhdt cia mute: py = 4.76.10" (N.s/m*) © BO mhot ea axit: jl, = 7.07.10" (N.sim?) Nen: Iguys = xplauis + (1 ~ xo)lgita = 0,986 1g(4.76.10%) + (1 -0,986)1g(7,07.10") 320 => pws = 4,782.10" (N.sim’) He sO dln nhigt cia nude: Ay = 0,658 (WimK) = He s6 din ahigtciia axit: 2 = 0,164 (Wim) Nén: Awi= An. Xo+2a(1 - Xp) 0,72 xp(1- xp)(Aw- Aa) = 0,621 (WimK) Trang 45Chung luyén Nutte - Axit axetic GOHD: Nauyin Van Lye + Nhigt dung riéng cia ne: . # Nhigt dung riéng cia nude: ¢4 Nen:ew = ent, +e4-(1 = Xp 182,245 (kg) 202,960 (kg) 4093177 kg) Ap dung edng thite (V.35), trang 12, [6]: Pry, Sutin 154 Nen: Nup= 44,115 = thy = 2128,781 (Wim?) (ty ~ tw) = 17679,884 (Wim?) go= 17679,854 (Wim?) (xem nhigt tdi mét mat a khOng dang ké) 10.10 (Naf?) 91.10 (Nasi?) = DG whdt ca axit: wa Nén: Iguw2 = xelgun + (1 ~ xe)lgua = 0,588.1g(6,50.10%) + (1 - 0,588)1g(7.91.10°) 195 = pa = 6,388.10" (N.s/m") He s6 din ahigt cia nude: Ay = 0,647 (WimK) © He sO din nhigt cia axit: 24 = 0,166 (WimK), Nén: Awa = An. xe+ ACL ~ Xe) 0.72 xR(1- xe)(in-h Nhigt dung rigng clin nue: ey = 4178 (WikgK) © Nhigt dung riéng ciia nutde: cq = 2152,935 (I/keK) Nén: cw2= en, +4. (I~ Xp) = 2760454 Wkgk) 1.237 (WimK) Ap dung e6ng thite (V.35), trang 12, [6]: Pry Nén: Nup = 287.590 => ap= 213,269 (Wim?K) = ge= ay (ty2~ te) = 17679,854 (Wim?) Kiém tra sai sé = 041 sop = 00000018 «586 (nda) ae Két lug: ty = 59,24484523°C va ty: = 49,894°C_ 3.4, Xde dinh hé s6 truyén nhiét: ke neat att nt 5289.10" 3133200 2038781 4. Bé mit teuyén uhiéls BE mat teuyén nhige due xAc dinh theo phuting tinh truyén niet Q 2528848601000 __ 69 ( Kat, 3600681481 21,083 Trang 46Chung luyén Nutte - Axit axetic GOHD: Nauyin Van Lye 5. Clin tan thie biz Chigu dai Sng teuyén nhigts L = 44,465 (mn) => chon L = 45 (m) 45 a, 00032 Ket ludn: Thiet bj tao A6i nhigt gia dine nhp Tigu va sin phim dinh RL diet bi truyén nhigt Sng King Ong voi chigu dai dng truyén nhigt L = 45 (m), chia thanh 15 day, mdi day 3m, Kiém tra 406,250 > 50 = = 1: thda Vv. THIET EI DUN SOI ‘Chon thigt bi dun sOi dong nhdp ligu Ii thiét bi truyén nhigt Sng Ing dng. Gng tray€n nhigt dutge lam bang thép X18HIOT: = Kich thtde ding trong: 38 x 3 = Kich thuite dng ngoai: 57 x3 Chon: = Dong nhap ligu di trong Sing trong véi nhigt 49 va0 ty = tre 6 rat 103.4°C. + Hoi ngumg tw di trong dng ngoai es ap sudt 25a: Y- NhiGt h6a hoi: fy, f= 2189500 (kg) 56,2134°C va nhigt Y Nhigt 9 891: ty, 26,25 (°C) 1. Suit lung hei dét en ding + Can bang nhige: Nén: Q= Grllrs~ hee Lugng hoi d6t cin dng: G, = 2= 207,845 (keh) 2. Hiéu sé whiét dé trung binh : Chon kiéu truyén nbigt nguge chigu, nén (126.25 ~56.2134) ~ (126.25 ~103.4) Ate = 42,128 (K) 12625-1034 3. The s6 truén wbiet + He s6 wuydn nhigt K due tinh theo céng thie: Trang 47Chung luyén Nutte - Axit axetic GOHD: Nauyin Van Lye AWim?.K) Voi + Ge: hé sO ctip nhigt ca dong nhip Higu tong dng (W/mK), = cy she 36 ep nhit iia hoi ddt ngoai Sng (W/mK), ree mhigt r8 qua thanh Gng va Ip cau, 3.1, Xée dinh hé sO cap nhiét cia ding nhip ligu trong Ong: Kich thude cia Gng trong: = Dating kink ngoai: dy = 38 (mm) = 0,038 (m) BG day Ging: 6,= 3 (mm) = 0,003 (m) Daring kinh trong: dh = 0,032 (m) Nhigt 6 trung Dinh ea dong nhap ligu trong Sng: te = % (tv + te) = 79,8067 (°C. Tai nhigt d6 nay thi: hing riéng cia mide: Khoi hiyng rigng cia axit: py Xp IHK, 3 971,916 (kg/m) 981,222 (kg/m') 3 0,001 = pr = 978412 (kg/m) 971,916 | 981,222 #6 nhat cita mfBe: py = 356.10" (Nim?) + BO nhdt cia axit: 44 = 5.61.10 (Nasim’) Nén: Igqie= xelguy + (1 ~ xpdigqa = 0,588.1g(3,56.10°) + (1 -0,588)lg(5.61.10%) 367 = wr = 4,294.10" (N.sim?) He s6 dfn nhigt eda nue: Ay = 0,675 (WimK) = He s6 din nhigt cia axit: 4a = 0,160 (W/mK) Nén: p= dy. Xe+ Ral - Xy)— 0,72 Xp(L~ XpMn- Aa) = 0.237 (WimK) = Nhigt dung riéng cia nude: ey = 4194,845 (J/kgK) + Nhigt dung ring eila nite: cx = 2314,947 (IikeK) Nén: ce = eX, +4. (1 ~ Xp) =2878.916 Wikgk) Ap dung cong thife (V.35), trang 12, [6]: Pr, = Vaan t6e cia ding nhap ligu di trong Sng: 4G, 43000 * 3600pxd;, — 3600978412 x xx0,032" Chuiin sf Reynolds Yed,Pe _ 105900329784 Me 1294.10 Ap dung cong thite (3.27), trang 110, [4] > cOng thite xdc dinh chudin s Nusselt 1,059 (avis) Rey = 77226,631 > 10* : ché' 46 chily roi Nuy =0,021.5,.Red# Pree { Phe Pr Trong 46: ; ~ hé sO tinh dén anh hudng eiia hé s6 ep nhigt theo ty é gita chidu dai L va duting kinh d ea dig. Frang 48Chung luyén Nutte - Axit axetic GOHD: Nauyin Van Lye ‘Tra bing 3.1, trang 110, [4] = chon c) ip nhigt eva ding nhép ligu di wong Sng trong: c= 3.2. Nhigt tdi qua thinh Sng va ldp céu : t - Swim’). So vm. a Trong a6: # tr nhigtdg ea véch tig xiie voi hai abt, °C tar mig dg cia wich tig xife vai dong ahip ligu, °C & Sona By, +B day thanh ding: & = 0,003 (=m) + He s6 din abigt cia thép Khong gk: 4 = 16.3 (Wink) + Nhigt wd I6p eu tong 6ng:r1 = 1/5800 (m= K/W) © Nhiét trd ldp cdu ngoai Ging: r;=1/5800 (m".K/W) Nén: Dr, = 5,289.10 (m7. KW) 3.3, Xéc dinh hé s6 céfp nhiét cila hoi ngung tu ngoai dng. Kich the eva Sng ngoi + ating kinh ngoai: D, = 57 (mm) = 0,057 (m) + BE day Ging: = 3 (mm) = 0,008 (rm) + Dating kinh trong: Dy, =0.051 (m) Ap dung cong thite (3.65), trang 120, [4]: «., =0.7254) Litt, tw, Dang phép lap: chon t Nhigt d6 trang bin ci Tai nhigt 6 nay thi © Khéi lutung rigng ctia nutéc: py = 939,1646791 (ke/m*) BG ahde cia nude: jy = 2,28.104 (N.s/e") He s6 dfn nhigt cia muc: Ay = 0,686 (Wien) Nén: a = 15945,030 (Wink) 11 (6 ~ fy) = 48110,923 (Wim) qs =48110,923 (Wim*) (xem nhigt tai mat mat ld khong dang ke) > faa = ts - GB = 97,788 CO) Tai nhigt 49 nay tht = 6 nhdteila mBe: py = 2.87.10" (N.sin*) BO nhdt cia axit: 49 = 4.71.10 (N.sim*) Nén: lgpina = xrlgh + (1 ~ xelgha = 0,588.g(2,87.104) + (1 -0,588)1g(47 1.10") = 3454 = pry = 3,519.10" (Nsim’) He s6 fin nhigt cia nue: Ay = 0,682 (WimK) He s6 din nhigt ea axit: 4a =0,156 (WimK) Nén: Aya = Aw. e+ 2a(L~ Xe) — 0,72 xp(1- xp)(Ry~ Aa) = 0.234 (W/mK) * -Nhigt dung rigng cia mite: cy = 4220,461 (J/kg) 23,232701 (°C) mang mide nguing tu: ty =" (ty + tw) = 124,7413505 °C) = 4Chung luyén Nutte - Axit axetic GOHD: Nauyin Van Lye + Nhigt dung riéng cia nse: Nén: ewa= ey + 64 (I~ Xy) 417,391 (kg) 2958,312 WkgK) Ap dung cong thife (V.35), trang 12, [6]: Pry: Nén: Nup= 361,817 = ap = 2675,614 (Wim?) > qe= a (ta fe) = 48110,909 (Wim?) ‘Kiém tra sai sé: _fnal c Két lugn: ty) = 123,232701°C va t, 100% = 0,00003% < 5% (tha) 97,798 3.4, Xde dinh he s6ruyén nhige L 2675,614 + 5,289.10 +15945,030 = 1035,907 (Wii 4. Bé mat truyén ahiét Bé mat truyén nhiét duge xéc dinh theo phyong trinh truyén nhiét: Q__485077,0841000 Kat,” 3600-1021 5. Chin tao thiét bi + Chiu dai Ging truyén mhige: L = = 26,343 (m) = chon =27(m) 2272 943,75 > 50> 4 = Ithba 0.032 Kéi ludn: Thiét bi tea0 Ai nhit gia ddng nh§p ligu va sin phim dinh 1a thist bi truyén nhigt dng 16ng ng vdi chigu dai Gng truyén nhigt L = 27 (m), chia thanh 9 dy, mdi day 3m. vi BON CAO VEE 1. Féin tit dudng éng déne Chon 6g din o6 duting kinh trong Ii dy = 80 (mm) ‘Tra bang IL15, trang 381, [5] = Bd nham cia Gng: 6 = 0,2 (mm) = 0,0002 (m) (in mon it) Tén that dudng Sng din: hy = [athe é (my 2g Trong 46: #2) :he sO ma sit tong duving dng Frang 50Chung luyén Nutte - Axit axetic GOHD: Nauyin Van Lye 30(m). 1 08(m), 4000 : che’ chi «6 Chudn sé Reynolds khi bit ddu xudt hién vdng nham: Re, = 220(d\/e)"" = 186097,342 Vi Reg < Reg < Rey = ch d0 chay r6i tng vai khu vye qui 40. Ap dung cong thi (1.64), trang 379, [51 = 01 {140 $12) <0029 1.3. Xe dinh Sng he 36 tdn that cue bo ® Chiadh Tra bing 11.16, trang 382, [5]: Chon dang Sng wn cong 90" 66 ban inh R v6i Rid = 2h Sur an) = O15. Butiing dng 06 6 ch8 6 = &, = 0,15. 6= 0.9 * Van ‘Tra bing 9.5, trang 94, [1]: Chon van elu v6i d9 mé hoa tod thi Bs iy = 10. ang ding c6 2 van ct = Fyn = 10.2 = 20 % Linu hang k€ = 8; = 0 (coi nhur khong ding ké) 4% Va than : &xip= 1 Nen: DEn = G+ Guat 19 Frang 51Chung luyén Nutte - Axit axetic GOHD: Nauyin Van Lye ons So +219 | eT 08° °° 2x98 Vay: by \047 (am) 2. Téu thet dudng dng din trong thiét bi trav déi nbiét qida ding nhio hy m 2 = Trong a5: da :he sO'ma sat trong dung dng, es chidu dai dudng dng din, ly = 45¢m). = do: duting kinh Ong din, do = de = Yer: tOng he s6 t6n that eye bd. + vor van te dong nhap ligu trong ding din 032(m). 2.1, Van we dong nhdp lieu trong Sng din :v2= 1,021 (avs) 2.2, Xée din hé s6 ma sit trong dung dng Chuan s6 Reynolds : Re: = 45588,056 > 4000: ché a6 chay réi 6 nhém: e = 0,002 Chusin so Reynolds gid han-Reps = 6(dv/e)"” = 1982,191 Chun s6 Reynolds khi bat du xudt hign ving nham: Rey = 220(dy/e)" = 66383,120 Vi Regi < Re} < Rey = ché d6 chay roi tng voi khu vie qua 4. « , 100)" Re, Ap dung cong thie (1.64), trang 379, [5]: 42=04 {140 0022 2.3, Xde dinh tng hé s6't6n tht cuc bo ® ChaU ‘Tra bing 9.5, trang 94, [1]: 7 Buing ng o6 (15 — 1) = 14 ch U > Eu = 22. 14 = 308. ® botthu ‘Tra baing HL16, trang 382, [8]: Khi C6 1 chd dot thu = Esersna 1 = 0,458 % Dorms ‘Tra bing 11.16, trang 382, [5]: Khi C6 1 ch5 d6t md = Ey n92= 0,708 Sur + Goon 2 + Gaoe me 2= 31,966 45 10217 Vay: h, ={0.022—?_ + 31,966 3.316 im arb (omm gg 388 gs 36 Frang 52Chung luyén Nutte - Axit axetic GOHD: Nauyin Van Lye eu va sin phiim dink: 1 vie hye [a, 2426, |S om A ( 1g ys (m) ‘Trong a6: = a :hé sma sit trong dung dng = Is: chidu dai dung dng din, f= 27(m). dutng kinh Ging dn, ds = dy = 0.032(m) © Yes: tOng ng s6 tn that eve bd. vs: van te dong nhap ligu trong ding din 3.1, Van ue dong nhdp lieu wong dng din :va= 1,059 (avs) 3.2, Xae dinh he s6 ma sit trong dung Gng : Chuiin s Reynolds : Re: = 77226,631 > 4000: che d6 chay ni 16 ham: ¢ = 0,002 Chuiin s Reynolds gidi han: Reg = 6(€s/e)"7 = 1982191 Chusin so Reynolds khi bit du xudt hign ving nham: Res = 220(di/e)"" = 66383.120 Vi Re > Rey = ché 46 chi #63 ting vi ving nham. Ap dung eéng thite (11.64), trang 379, [5]: hs = 0,032 [114+ 2)e04,/2F 3.3. Xde diah wing he sé win that cue bd * chev ‘Tra bing 9.5, trang 94, [1]: Gu» «1 Bunting Sng c6 (9 ~ 1) =8 cht U = fe2 = 2,2. 8= 17.6 ® Docthu Tra bing 11.16, trang 382, [5]: Khi & C6 1 eh6 dt thu = Eterm = 0.458 4 Dorma ‘Tra bing 11.16, trang 382, [5]: Khi C6 1 chi Abt md = Ea 493= 0,708 Nén: Dé = Gin Banca 3 + Sav nd 27 Vay: hy 227 18.7 fay: by =| 0032505718. 6 2x981 4. Chiéu ea bin eno vi: Chon = Mat cit (1-1) 1d mat thosing chit Wng trong bén cao vi, = Mat ct (2-2) la mat edt tai vi tri nhap lig thap. Ap dung phuténg tinh Bernoulli cho (1-1) va (2-2): Frang 53Chung luyén Nutte - Axit axetic GOHD: Nauyin Van Lye BR,» Pre 28 nent Trong a6: + 24:48 cao mat thosng (1-1) so v6i mat dt, hay xem nit ft chiéu cao bén ca0 vi Hi + 72:0 cao mat thosng (2-2) so voi mtd, ha én vi ti nh ligu: sin + y+ (Oye — DAN + 04 14 +04 + (31 - 1904+ 05 = 13,3 (m) = Py: dp sudt tai mat thong (1-1), chon P; = | at=9,81.10* (N/m?) ap suit igi mat thoang @-2) Xem AP=Py~ Py = mg .APL = 40.577,638 + vs van We tai mat thosng (1-1), xem v4 # vps vin we tai vi wf nhgp liu, v2= ve = 0,167 (m/s). + Dhaes:t6ng tn inst wong dng cr 1-1) dein (2-2) Dhy.a= hit hat hy= 6,002 xem nhur la ehigu cao wt mac dt Vay: Chiéw cao bin cao vit Ho 992,665 © 2x981 21,676 (m) Chon Ha, = 25 (m), VE. BOM: 1. Dang sucits Nhigt d9 dong nhdp liu Ia te= 27°C, Tai mhigt 49 may thi + Khoi lung rieng ea nude: py = 996,42 (k/m’) © Khoi luting rigng cia axit: pr = 1040.65 (kg/m*) Nien: 1a 3e Se 03, 108 _ 9901 = pe = 1026,974 (kg/m) Pr Py Px 99642” 1040.6 + BO nndt cia made: jy = 8.56.10" (Nim?) = BO mhdt cla axit: pla = 1.18.10" (Nisin) Nén: Igue= xrlguy + (1 ~ xelgu = 0.588.1g8,56.10") + (1 -0,588)Ig(1.18.10°) OLL = pr = 9,753.10" (N.sfm") Sulit hugng thé tch ela ddng nhdp ligu di trong Sng: 9, =n 3000 Py 1026978 Vay: chon bom 6 ning st 2,921 (m'/hy Frany 54Chung luyén Nutte - Axit axetic GOHD: Nauyin Van Lye 2. Cét ip: Chon Mgt ct (1-1) 8 mu thosng chit tng trong b6n chia nguyen igu. = Mat cét (2-2) la mat thoaing chit long trong bén cao vi Ap dung phusng tinh Bernoulli cho (1-1) va @-2) + ee tyane 4 adh pee De pre’ 2g Trong a6: = 71:6 cao mat thosing (1-1) so vai mat dat, chon 2, + 23 d9 cao mit thodng 2-2) so voi mat di, 2 = He = Pi: dp suat tai mat thodng (1-1), chon P; = | at, © Pp: dp suaft tai mat thoding (2-2), chon P;= | at + vyvn! vn eta mst thosng (11) va@-2), xem v + Shas tng en tht wong dng (1-1) an 2-2) = Hy: 06t dp cia bom. n+ 2.1, Tinh sGng tr ue trong Sng Chon duiing kinh wong cia Sng hit va Gng day bng nhau: de = 50 (mm) ‘Tra bang ILS, trang 381, [5] => DO nhiim ca Sng: & = 0.2 (mm) = 0,0002 (m) Can moa it) Téng td lye trong dng hit va Ong dy Dna =[attle Trong d6: Ay: chidu dai dng htt Chigu cao hit cia bom: Tra bing 1134, trang 441, [5] = hy = => Chon h = 6 Gm) +: chidu dai dng diy, chon ly =20 (m) Dy: téng tén that cuc bo trong Sng hit. ey: tng tn that euc bd trong ding dy 2 hg s6 ma sat trong Gag hit va Gng diy. vv: van te dong nhap ligu trong ding hit va Sng dy (m/s) 40, = __43____ 9.494 amis) 3600nd, ~ 3600% nx 0/080 3 (m) 4 Xéic dinh he s6'ma sit wong dng hit va Sng dy Chusin s6 Reynolds Voth py _ 0424 0.05 «1026, ir 9,753.10 Chuan sé Reynolds tdi han: Reyy = 6(dy/e)"” = 301,065, Chudin s6 Reynolds khi bait du xust hign vang nhaim: Rey = 220(dy/e)"* = 109674 381 Vi Regs < Rer < Rey ché dp chay r6i tng vai khu vue qus 09, 14 = 22344,356 > 4000 : ché 46 chiy 16 Frang 55Chung luyén Nutte - Axit axetic GOHD: Nauyin Van Lye {146 ® Xéc dinh tng tn that cuc b6 trong ding hit + Ché win cong ‘Tra baing 11.16, trang 382, [5]: Chon dang Sng usin cong 90” e6 bain kinh R voi Rid 2 Uh Sar can = OS. Ong hiit 06 2 chd udin => & =0,15.2=0,3 © Van ‘Tra bing 95, trang 94, [1]: Ong hit e6 1 van chu = Ey Ap dung eéng thife (11.64), trang 379, [5]: 3) = 0032 Re, thon van edu v6i d9 mé hon toa th Ey (5 10 * Ché udn cong : Tra bang I1.16, trang 382, [5]: Chon dang Gag udn cong 90" ¢6 ban kinh R voi Rid 2th Ei a= 0.15. Ong day 06 4 chd w6n = = + Von ‘Tra bing 95, trang 94, [1]: Chon van ek vid md hod oan thi Ga cay = 10 Ong day o6 1 van edu > B= 10 * Vio bdn cao vi y= 1 Nén: LE = Sur + St Sev = 116 620 Vay: Dhaa={0.032 tr Dnaa( oor ces +103 +116) 2.2, Tinh e@t ép cia bom: Hy = (22~ 23) + Dhn.2 = 25~ 1) +0353 4.353 (mn) 3. Cig suits Chon higu suat cia bom: n= 0.8 QuHyppg _ 3%24.353 1026, 3600.n, 360008 = 255.572 (W) = 0.343 (Hp). Kéiludn: Dé dim bio thap hoat dng lién tue ta chon 2 bam li tim loai XM, e6: Cong suse the t€ eda bom: Np =' = Nang sudt: Qy= 3 (m'/h) = Cot ap: Hy = 24,353 (m) = Cong suit: Ny = 0,343 (Hp) Trang 56Chung laygn Nuibe ~ Axit axetio GOHD: Nauyin Van Lye eins 6> AN TOAN va TU DONG HOA AN TOAN LAO BONE = lain nd: Tit ci cdc chit ling du c6 kha ning bay hoi va nhigt d6 bay hoi phy thude vio nhigt 46 si cia n6. Su chay khi nio eting xay ra trong pha hii va tén bé mat thosing cia chat Jong. Sau khi dX bay hoi thi sy chay va e&e yéu 6 anh hung d&n gus tink déu gi6ng nh sur chéy ota of, kh. Kha ning chéy eda chit ling o6 thé x4e dinh bing c&e thong s6 Khe nhaw abu nhigt 4 bang chdy, nhige 46 bée chdy, nhigt 9 ay bec chay ho¥e gidi han né, ahung hay ding hai née 49 bung chdy. Chit Ibng cng dB chay tht nhigt d6 bing chay cing th'p va nhigt 0 bde chay cang gan nhiet dO bang cha Axitaxetic It chit o6 nhigt d@ boc chay la 35°C & dp suit khi quyé LLL, Nhimng nguyén nhan gay chay né tne tgp: Nhettabié, moe dim chay xust hign ein 66 3 ye tt: 46 1 ehat chiy, chat oxy ha voi 1§ le xée dinh gita chiing vai mdi bat ehéy, MBi bat chay trong thy t€ cing rt phong phi n ting phéng dign giita cac dim may c6 tich dién trai dtu hod gitta dim may voi mat AXt, Dign Sp gita dim may voi mat dt 6 thé dat hang triéu hay hang tram trigu von, Nhigt 46 do sét dainh rat cao, hing chue nghin 6, vist qua xa nhigt d6 ty bat chdy cia ede chit chay duige Trang 57Chung luyén Nutte - Axit axetic GOHD: Nauyin Van Lye Hign twang tinh dién: tinh dign sinh ra do sy ma sit gia cae vat thé, Hign anyng nay ri hay gp khi bom r6t (thao, nap) e4e chat King nat ede chat King e6 chia nhimng hop chat 6 eye niu xang, du... Hign tuting tinh dign tao ra mot lép dién tich kép trai du Khi dign ap gia cae lép dién tich dat (Gi mot gid ti nhat dinh s€ phat sinh tia lita dien va ety chay, MBéi chay cing e6 thé sinh ra do hé quang dign, do chap mach dién, do déng cu dao dign. Nang lugng gidi phong ra cia céc rung hp trén thuting dii dé gay chay nhiéu hon hap. Tia lita dign 18 mdi kh ph bien rong moi Tinh vye sit dung dig, Tia Wika c6 thé sinh ra do ma sit, va dap gia cae vat rin Trong céng nghiép hay ding céc thigt bi c6 nhigt o6 nhigt dd cao, a6 1a ede mBi bat chay thing xuyén nh 10 d6t, 10 nung; ede thiét bi nay hay si? dung ede nhién 1igu ahut than, sin phim du mé, ca loai khi chéy ty nhién, nhin tao; do dé néu thiét bj ho ma KhOng phat hign duye dé xt ly kip thoi sé gy chay nd nguy hiém. i khi chay né xdy ra do A bén eta thiét bi khong dim bao, ching han dip suft trong binh khi nén 6 thé gay né néu nhut 46 bén cia binh khong dim bao. Trong sin xudit néu nhigt d6 gia nhigt cia mot chat chay ndo ds Idn hon nhigt a bing chay eting gay ra chay, n6, MOt s6 chat khi tip xiie vai mugde nh eacbua canxi (CaC) gay chay nd; nhiéu chit khi tie xiie v6i ngon lita trin hay tan lita rit d& gay chay nd, ching han nhu thue n6 clorat kali (KCIOs).. Nhiéu khi chay né xay ra do ngwai sin xudt thao tic khOng diing quy tinh, ching han dang chilt d& chay d& nhém Io gay chay, khOng thy hién ding trinh tw thao tac. ing nguyén nhan chay né rat da dang tr thiét KE, cOng nehé, quin ly, thanh tra, kiém tra trong sin xudt 1.2, Cie bién php phdng ching chay né: a) Ngon lita trdn oi khi ngu ta vin sit dung ngon hia trin (khOng che chain kin) dé chumg eat cc chit Ing dé chay. Nhtng vy chy nd thudng xuyén xiy ra voi ede thiet bj kiéu nay 1a bing chiing vé stf nguy hiém cia ching. Mot mat, nguy od chay né e6 thé xust hign trong qui trinh r6t nap chat ing hod do thiét bi chita chit Iéng khOng kin. Mat khéc c6 nguy e li hai chung edit bée Léa va King xuding phia dui tiép xt vai hi. Khi lim vige vai ngon lif trin phai thuing xuyén kiém tra d6 kin cila cdc Ong din kh (hoge hoi) bing eéch dang dung dich cia chit e6 bot (nhut dung dich x& phdng) phét len cfc ché cén kiém tra aé phat hign xem khi (hod hai) e6 10 ri ra ngoai khong. Chi duge thye hign cde cong vige han hoje cde cng vige 66 sit dung ngon lita tein trong nhing day chuyén sin xudt e6 neuy higm chay nd néu dude su déng ¥ va cho phép cila ep thém quyén bang van bin chinh thc, ddng thai phai thue hién ede bién phap phong chong chdy nd thich hyp. Trong ting hap edn thiét pha e6 agi eitu hia trve tai hd. b) Hoar déng ciia xe, mdv cd ding ca dién: Hoat dong cia cée xe, may 6 chay bang ding eo dién phai duvse quy dinh de bigt Cae xe, may ndy khong dude hoat dOng tong Khu vwe nguy hiém va név hoat ding gin 45 thi phi git? mOt khong eich an toan 12 10m (46i vdi khu vue e6 Khi dé chéy th Frang 58Chung luyén Nutte - Axit axetic GOHD: Nauyin Van Lye khoding eich an tofin fi 20m). Nhitng khu ve nguy hiém 6 day 18 nbitng khu v¥e 66 kha ning xudt hign hén hyp d& chéy né gitta khi, hoi hose byi v6i khong khi, vi dy hing khu vue kho e6 chét dB chay nd, nhitng khu vic c6 thao tic pha trn, rt, nap céc Kht va chat JWng dé chay n6. Déi voi nhiing Khu vite chi lwu git Iugng nhd Kh hoa cht Wng dé chay (vi dy 10 binh Kh c@ nh) thi khéng e@n gilt khoding efich an toan (én, Xung quanh ede khu vye 6 nguy hiém chéy né phi e6 bién caah bao did vi te dB gy, ©) Heie thud’ Id, bdt diém, dé hte: Lénh ciim hit thude la phai due tuan thi tyét di trong cae khu ve ¢6 nguy hiém chay né. Mat khée en quy dinh nhitng noi dude phép hut thude Ia va néu e6 aigu kign th bg tri cde phng duige phép hit thude Id. Vige khOng e6 hoe c6 quit it cae phong Auge phép hit thude li e6 thé din dén sif vi pham Jénh cfm hiit thude vi nhitng hiiu qua rst ning Ce hainh dng bat diém, d0t Ka 1g Phai due e&im hodn toa. d) Cac thiét bi didn: Trong nhiing khu vue o6 nguy hiém né, cae thiét bi din phi duge thiét ké lip dat sao cho: = Nhiét d6 cao nhat eiia cde phan thiét bi dién ludn thi‘p hon nhiét 46 bing chay cia hn hop nguy hig, = Cac bé phan c6 phat ra tia Na dign déu due bao vé che chin. ©) Caécnguén edy téc nhdn chdy khde: = Tia fa do hn dign, mai hode va dip. = Tinh aiga = Cic kh va hai 66 nbidt 46 bang chy tp es thé s€ bec chdy Ki gap ec vat thé + Cae phiin img ta nbigt o6 thé t@ nén ngudn tic ahin dét ning va gay chéy nguy higm néu nhigt d6 phan ting ting qué cao. 2. An todn dieu: 2.1, Cée nguyén nhan gay ra tai nan dién Tai nga dign gidt xay ra khi co thé con ngui tp xtle Vi 2 dign dign thé khée nhaw high cho mot dong dign chay qua eo thé. C6 thé xay ra ce tinh using sa 8) Cham vio 2 ddy dién trong mang din: Di vdi mang dién 3 pha néu cing cham vo 2 day néng co thé sé chiu mot dién 4p dy, néu cham vao I day néng va 1 daly ngudi cd thé sé chiu dién dp pha. Dign dp day e6 gid tri bling 1,73 lin dign 4p pha nén mife d6 nguy hiém cling cao hon. b) Cham mét ddy néng trong mang 3 pha trung sinh néi dt (mang sao, Néiu ea thé khong cach dign vai dat sé ehiu mot di€n sp pha. ©) Cham mbt ddy ning trong mang 3 pha trung tinh Khong ndi dd (mang tam gid Frany 59Chung luyén Nutte - Axit axetic GOHD: Nauyin Van Lye Deng dign qua co thé phy thude gid tj dign trd rd va dign dung ky sinh eta mang. ) Ro. dién ra v6 thie bi V6 thiet bi dong co... thing khOng mang dién, Khi chat hung cach dign gidm hay day din dign cia thigt bi cham v6 s& Kam v6 thigt bi mang dign (twdng ty nhut mot day 1néng trong mang dién), néu ngudi cham vaio v6 thiGt bi sé bi dign gidt. ©) Dodien dp bude o phing dién cao dp: 2) Dod quang: 2.2. Cac bign phap kp thudt dé phong tai nan dién = Noi dat bio vé. ~ Noi dat trung tinh (con got la not Khong). = N6i dang thé. = Ding dign dp tha - Bign &p céch ly + Cit dign bio ve. = Cich dién. - Nain chan va che chin, Te dGng héa la mot vain dB rt quan trong trong sin xudt igm nhiin cng va cho ning suat ca0 hot Trong he thong chung eit Nude ~ Axit axetic nay, ta en phai ty dOng hoa trong cde khau sao: + Nhap lig. = Hoan Iu, = Cung edp hei dét va mde lam lanh éng thai phai o6 h@ théng an toan, tf dong déng ngit khi cd ste xly ra. n nay. N6 sé gitip tit TINH KINH TE = Luyng thép X18HIOT edn ding: My = Tiga tia + 2ai(aip)= 730,671 (kg) Lung thep CTS cin ding M. 32mecrasiaae* 4.2. mycnshp ng +22. Mac sre gta $4. moranan +t 4. Mai geo 4 Mai 322,338 (ke) # $6 bulong edn ding n= 16,40+4.4 42,8 =672 (cdi) + Chigu dai ong 38 x 3mm: Ly = 1657.6 +57 +61. 6 +45 +27 = 10437 (m) Frany 60Chuing luygn Natée ~ Axit axetie GOHD: Nauyin Van Lye Sng 57 x 3mm: [= 57-445 +27 = 129 (m) + Chiéu dai dng 80mm: Chon tng chi dun, dng din King ra khdi ndi dun va nhigt 30m. 10+ 30 = 60 (mm) = Chiéu dai dag 150mm: Chon téng chiéu dai Sng hoi 8 dinh thap va dng hoi 6 day ai Sng hoan ha, ng din King vio ndi ing din sin phim dinh vao thiét bi trao di = Chigu dai dng SOmm: Chon tng chiéu dai Sng chay tran va Sng xd dy tirbén cao vi fi 50m. Ls=2.6+20-4 50 =82 (m) + Kinh quan sat: during kinh 1a 180mm, day 20mm s==.0,1 4 0.025 ( Chon 2 kinh quan sit =>$ = 2. 0,025 = 0,051 (mn?) = Bom ly tim: chon 2 barn ly im = Ny = 2. 0,343 = = Cait inox 38 x 3mm: n = (18 + 14 +8).2 = 80 (cai) Cit inox 57 x 3mm: n = (18 + 14 +8).2 = 80 (ei) 1,685 (Hp) Vat ligu So Wigng Don gid | Thanh tién (@) Thép XISHL0T 730,671 (kg)| 50000 (@ikg) | __386533562 Thép CT 332,338 (kg)| 10000 (kg) 33223379 Bulong 672 (cai) | __5000 (aiediy 3360000 ‘Vat ligu eich nhigt 1,998 (m') | 4000000 (am) 7993230 [Suztin atm 10437 (m) 50000 (d/m) 521850000 ag dn 57 x 3m 129 (m)|_100000 cam) 12900000 Ong 80min “0 en) | 100000 (any “6000000 Ong 150mm, 10m) 100000 (afm) 1000000 Gng 50mm 82m) | _100000 (am) 200000 Kinh quan sit 10,051 (m*)| 250000 ¢a/m’) 12723 Bam ly tim (0,685 (Hp) | 700000 (a/H1p) 479626 Ap ké ty dong 1 (edi) | 600000 (aed) ‘600000 Nhigt ké dign td tw ghi 3 (esi) | 200000 (ave) «600000 Lau lugng ké (> 50mm) 2 (cai) | 1500000 (Aveai) 3000000 ‘Van inox SOmim S (edi) | 150000 (Alea) 7750000 ‘Van inox s0mm 6 (esi) | 150000 (aveaiy ‘900000 acco inox SOmm (csi) | 150000 (aveaiy 750000 Racco inox 80mm 2 (cai) | 150000 (ave) 300000 Cit inox 38 x 3mm 80(cai) | 15000 (ares) 1200000 Cit nox 57x 3mm 80 (cai) | 30000 (aieaiy 2400000 Cit inox 80mm 14 (cai) | 30000 Caled) 420000 Cit inox 150mm 3 cai) | 30000 (avesiy ‘90000 Cait inox 50mm 10 (esi) | 30000 (a/eaiy 300000 Trang 61Chung luyén Nutte - Axit axetic GOHD: Nauyin Van Lye Tinox 50 3(eii)] 30000 (edi 90000 ‘Tong chi phi vit tit 992.952.521 Vay tng chi phi vara 1 d8ng. Xem tién c6ng ché to bing 200% tién v9t Vay: t@ng chi phi la 3 déng, LOI KET Voi he théing chumg edt Nude ~ Axit axetic diing thap mam xuyén 18 nh da thigt ke ta thy bén canh ning mu dim etng edn eG nhiGu nhutge diém. Thiet bi e6 wu diém 1 ining sudt va higu sudt cao nhumg thiét bi edn rat eng kénh, di hdi phai e6 suf van hanh Yai d6 chinh xe cao. Bén canh d, khi vin hank thiét bi nay ta cing phai het site cha ¥ 4n vin a an toan lao dong 4€ tranh moi nbi ro 66 thE xay ra, gdy thigt hai vé neu va FAD LIEU THAM KHAO UL. Trin Hang Dang - Neuyén Vain Lue - Hoang Minh Nam — Vai Bé Minh, “Qué tinh va Thiét bi trong Céng Neh? Héa Hoe ~ Tap 1, Quyén 2: Phan riéng bing Khi ang, ite ty tim, bom, quat, may nén. Tink he thing dung dng”, Nha xvit bin Dai hoe Quée gia TpHCM, 1997, 203tr. [2]. Vo Van Bang - Va Ba Minh, “Qué rink va Thiet bi trong Cong Nghe Héa Hoc ~ Tép 3: Truyén Kh6i", Nha xudt bin Bai hoe Quée gia TpHCM, 2004, 388tr. [3]. Pham Van Bon - Nguyén Dinh Tho, “Qué trinh va Thiet bi trong Cong Nghe Hoa Hoc ~ Tap 5: Qué tinh va Thiét bj Truyén Nhigt*, Nha xudt bin Bai hoc Quée gia ‘TpHCM, 2002, 3720. Frang 62Chung luyén Nutte - Axit axetic GOHD: Nauyin Van Lye (4) (31 (ol. a. (3) o. Pham Van Bén - Va Bé Minh - Hoang Minh Nam, “Qué trinh va Thiet bi trong Cong Nghé Héa Hoe ~ Tap 10: Vi dw va Bai tp”, Nha xuiit bin Bai hoc Quée gia TpHCM, 468%r. ‘Tap thé tae gid, “Sd ray Qua trinh va Thigh bi Cong nghé Héa chat ~ Tap 1°, Nna xuit bin Khoa hoe KY thuat Ha N6i, 1999, 626tr, Tap thé tae gid, “S6 ray Qué trink va Thigi bi Cong nghé Héa chdt ~ Tap 2", Nra xuft bin Khoa hoc Kj thugt Ha N6i, 1999, 447t, HG Lé Vien, “Thi ké' va Tinh ton céic thiét bi héa chai”, Nha xust bain Khoa hoe va Ky thug, HA Noi, 1978, 286tr. Naguydin Minh Tuyén, “Co s0 Tinh ton May va Thiet bi Ha cht ~ Thue phaim”, Nid xuft bin Khoa hoc va KF thugt, Ha Noi, 1984, 134tr ‘Trén Hitu Qué, “Ve AF shudt og khi ~ Tép 1", Nhd xudt bin Dai hoe va Giso due chuyén nghigp, 1991, 160tr. [10 Pham Dinh Tri, “380 phuong thie diéu ché vd sing dung hoa hoe trong sdn wud va bi sing”, Nhi xust bin TpHCM, 1988, 144. [ILNguyBn ThE Dat, “Khoa hoe AF thudt bdo hb tao ddng vd mdr 56 vdin dé v8 moi trudng”, Nha xuit ban Khoa hoc va K¥ thuat, Ha Noi, 2005, 283tr. [12LeThE Nghia, “KF shudt an todn trong sdn xudi va sit dung hda chat *, Nha xudt bin Khoa hoe Ky thudt, 2000, 299tr. Frang 63

Đồ Án Thiết Kế Hệ Thống Chưng Cất Nước ..

Transféré par

Informations du document

Copyright

Formats disponibles

Partager ce document

Partager ou intégrer le document

Options de partage

Avez-vous trouvé ce document utile ?

Ce contenu est-il inapproprié ?

Droits d'auteur :

Formats disponibles

Đồ Án Thiết Kế Hệ Thống Chưng Cất Nước ..

Transféré par

Droits d'auteur :

Formats disponibles

Vous aimerez peut-être aussi