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A hydrometer is an elongated glass bulb with a long, thin glass stem rising
from the top of the bulb. The bulb is hollow except for a plug of lead in the bottom.
If the bulb is inserted into a suspension, it will sink until the force of buoyancy is
just sufficient to balance the weight of the hydrometer. The hydrometer is designed
to sink into the suspension until the bulb is totally immersed, and the stem
protrudes above the surface of the suspension. Because the length of stem that
protrudes above the surface is a function of the density of the suspension, more of
the stem protrudes for denser suspensions. It is thus possible to calibrate the
hydrometer to read various densities. Soil hydrometers are typically calibrated to
read in g/ml or g/liter. Hence, an appropriate hydrometer can be inserted into a
suspension and a reading taken to obtain the average concentration of the solids in
the fluid displaced by the hydrometer. Because the hydrometer calibration is
affected by temperature and the specific gravity of solids, these factors will have to
be taken into account during the experiment.
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Time t = 0 Time t = t
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The velocity is expressed as the increasing depth of the hydrometer L in time t, or,
10 18η L L (cm )
D( mm) = =A (Eqn-2)
60 (γ s − γ w ) t t (min)
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where L1 is the distance between from top of the hydrometer bulb (the “0” mark) to
the solution surface mark. For example, suppose that the hydrometer reading of
zero is L1 = 10.5 cm. Now suppose that the hydrometer reads L1 = 2.3 cm for a 50
g/liter reading. The hydrometer reading is,
10.5 − 2.3
L1 (cm) = 10.5 − ( ) x (hydrometer reading )
50
L2 = 14 cm,
VB = volume of the hydrometer bulb = 67.0 cm2, and
AC = the cross-sectional area of the hydrometer cylinder = 27.8 cm2.
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Hydrometer Hydrometer
L (cm) L (cm)
Reading Reading
0 16.3 26 12.0
1 16.1 27 11.9
2 16.0 28 11.7
3 15.8 29 11.5
4 15.6 30 11.4
5 15.5 31 11.2
6 15.3 32 11.1
7 15.2 33 10.9
8 15.0 34 100.7
9 14.8 35 10.6
10 14.7 36 10.4
11 14.5 37 10.2
12 14.3 38 10.1
13 14.2 39 9.9
14 14.0 40 9.7
15 13.8 41 9.6
16 13.7 42 9.4
17 13.5 43 9.2
18 13.3 44 9.1
19 13.2 45 8.9
20 13.0 46 8.8
21 12.9 47 8.6
22 12.7 48 8.4
23 21.5 49 8.3
24 12.4 50 8.1
25 12.2 51 7.9
Table 1. The variation of L with the hydrometer reading for an ASTM 152-H
hydrometer.
To determine A for a soil with a specific gravity of the solids of Gs = 2.70 and with
the water in the solution at a temperature of 25ºC, the viscosity of water is,
This value can be confirmed from Table 2 that shows the variations of A with Gs and
the water temperature.
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Temperature
Gs
17 18 19 20 21 22 23
2.50 0.0149 0.0147 0.0145 0.0143 0.0141 0.014 0.0138
2.55 0.0146 0.0144 0.0143 0.0141 0.0139 0.0137 0.0136
2.60 0.0144 0.0142 0.014 0.0139 0.0137 0.0135 0.0134
2.65 0.0142 0.014 0.0138 0.0137 0.0135 0.0133 0.0132
2.70 0.014 0.0138 0.0136 0.0134 0.0133 0.0131 0.013
2.75 0.0138 0.0136 0.0134 0.0133 0.0131 0.0129 0.0128
2.80 0.0136 0.0134 0.0132 0.0131 0.0129 0.0128 0.0126
Temperature
Gs
24 25 26 27 28 29 30
2.50 0.0137 0.0135 0.0133 0.0132 0.013 0.0129 0.0128
2.55 0.0134 0.0133 0.0131 0.013 0.0128 0.0127 0.0126
2.60 0.0132 0.0131 0.0129 0.0128 0.0126 0.0125 0.0124
2.65 0.013 0.0129 0.0127 0.0126 0.0124 0.0123 0.0122
2.70 0.0128 0.0127 0.0125 0.0124 0.0123 0.0121 0.012
2.75 0.0126 0.0125 0.0124 0.0122 0.0121 0.012 0.0118
2.80 0.0125 0.0123 0.0122 0.012 0.0119 0.0118 0.0117
Table 2. The variation of the constant A with the specific gravity of solids Gs.
Finally, there are three corrections that need to be made: (1) a temperature of the
water FT, (2) a meniscus correction Fm, and (3) a zero correction Fz. These are as
follows,
2. The meniscus correction Fm is used with the upper level of the meniscus
reading. This correction is always positive.
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3. Zero correction Fz. Since a deflocculating agent is added to the soil distilled
water suspension for performing experiments, the zero reading is changed on
the hydrometer. This correction can be positive or negative.
Put the hydrometer in the cylinder of step 5. Record the reading, making sure to
use the top of the meniscus. This is the zero correction Fz, which can be positive
or negative. Also observe the meniscus correction Fm.
6) Using a spatula, thoroughly mix the soil prepared in step 3. Pour it into the
mixer cup. During this step, some soil will stick to the side of the beaker. Use
the plastic squeeze bottle to wash the remaining soil in the beaker into the
mixer cup.
7) Add distilled water to the cup to make it about 2/3 full, then mix for about 2
minutes with the mixer.
9) Pour the mix into the second 1000 cc graduated cylinder. Make sure that all
the soil solids are washed out of the mixer cup. Fill the graduated cylinder
with distilled water to bring the water level up to the 1000 cc mark.
Figure 8. The two 1000 cc graduated cylinders ready to start taking measurements.
12) Take hydrometer readings at cumulative times t = 0.25 min., 0.5 min., 1 min.,
and 2 min. Make sure to always read the top of the meniscus.
13) Take the hydrometer out after two minutes and put it into the constant
temperature cylinder next to it (step 5).
14) Take hydrometer readings at times t = 4 min., 8 min., 15 min., 30 min., 1
hour, 2 hours, 4 hours, 8 hours, 24 hours, and 48 hours. For each reading,
insert the hydrometer into the cylinder containing the soil suspension about
30 seconds before the reading is due. After the reading is taken, take the
hydrometer out and place it in the constant temperature cylinder from step
5.
15) Plot a grain size distribution graph on semi-log graph paper on excel with
percent finer on the log scale
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(4) Calculations.
Gs a
2.50 1.04
2.55 1.02
2.60 1.01
2.65 1.00
2.70 0.99
2.75 0.98
2.80 0.97
where Ws is the fry weight of soil used in the hydrometer analysis, and a is the
correction for the specific gravity
- Rcl = R + FM = 10.615
(11 −10 .115 )
- Using Table 1 & interpolating, L = 14 .5 + (14 .7 −14 .5) ⋅
(11 −10 ) = 14.677cm
30 (0.0911 x10 −4 )
- Using Eqn-4, A = = 0.01287
( 2.65 −1)
L
- Using Eqn-2, D = A ⋅ = 0.024653 mm
t
Environmental Conditions
Meniscus correction (Fm) = 0.5
zero correction (Fz) = 3
Temperature (t) = 22
Temperature Correction (Ft) = 0.65
a (From Table) = 0.99
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(5) Data.
Description of soil: Light brown silty sand
Hydrometer type: ASTM 151-H Specific gravity of solid, Gs = 2.65
Dry weight of soil, Ws = 50 g Temperature of test, T = 22.8 °C
Meniscus correction, FM = 0.5 Zero correction, FZ = +4
Temperature correction, FT = 0.85
Percent finer,
Time Hydrometer T (degree (a*Rcp)/50 *100 L D
FT Rcp Rcl A
(min) reading, R celsius) or (cm) (mm)
2*a*Rcp
0.25 10.125 22.8 0.85 6.975 13.95 10.625 14.675 0.01287 0.098605
0.5 10.12 22.8 0.85 6.97 13.94 10.62 14.676 0.069726
1 10.12 22.8 0.85 6.97 13.94 10.62 14.676 0.049304
2 10.12 22.8 0.85 6.97 13.94 10.62 14.676 0.034863
4 10.115 22.8 0.85 6.965 13.93 10.615 14.677 0.024653
8 10.1125 22.8 0.85 6.9625 13.925 10.6125 14.678 0.017432
15 10.11 22.8 0.85 6.96 13.92 10.61 14.678 0.012731
30 10.105 22.8 0.85 6.955 13.91 10.605 14.679 0.009003
1440 10.072 21.9 0.625 6.922 13.844 10.572 14.686 0.0013
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13.96
13.94
13.92
Percent finer
13.9
13.88
13.86
13.84
13.82
1 0.1 0.01 0.001
100
90
80
70
Percent Finer (%)
60
Sieve
50 Results
Hydrometer
40
Results
30
20
10
0
10 1 0.1 0.01 0.001
Grain Size, D (m m )
(6) Conclusions.
Hydrometer analysis allows geotechnical engineers to determine grain size
distribution in soil samples. Whereas sieve analysis can separate particle up to
0.038 mm with a No. 400 sieve, hydrometer analysis can distribute fine soil particles
up to a size of 0.001 mm.
There are many sources of error in this experiment. Human error in reading
and recording hydrometer readings and instrumental error are two sources of
error. Another source of error concerns the deflocculating agent and soil not
soaking for 8 to 12 hours in the beaker because of laboratory time constraints. In
addition, the rubber stopper was not applied to the graduated cylinder containing
the soil suspension neither shaken as instructed in step 10 of the procedure. This
prevented the thorough mixing of the soil with the water in the cylinder. The rough
insertion of the hydrometer adds error since it introduces disturbance to the soil
mix, causing turbulence. Moreover, the different size of grains in the sample
introduces error since the bigger particles will flocculate faster than the smaller
sizes and cause disturbance. Air bubbles floating on top of the liquid contributed to
some error as well in reading the meniscus. Lastly, only tap water with its
microscopic particles, rather than distilled water, was available at the laboratory at
time of experiment.
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(7) References.
1. Coduto, P. Donald. Geotechnical Engineering: Principles and Practices. New Jersey: Pearson
Education, Inc., 1999.
Data Sheet
Percent
finner,
Time Hydrometer a ⋅ Rcp
(min) reading, R R ×100 R L A D
50 (cm) (mm)
2 ⋅ a ⋅ Rcp