Académique Documents
Professionnel Documents
Culture Documents
-1
BERYLLIUM
"The Wonder Metal Which Performs Miracles"
INTRODUCTION
Beryllium may be taken as one of the best examples
to show how that many of the rarer elements which
were considered but laboratory curiosities only a few
short years ago are now the commonplace important
minerals today; and how that many of the other ele
ments considered rare today will be the common im
portant minerals of tomorrow and why prospectors of
today should learn something about them.
Only a few short years ago, in fact even as recent as
1942, beryllium was considered more or less a rare ele
ment; the production of the pure metal was so costly
it had but a few industrial uses; Beryl was the only
mineral used in its production; books on mineralogy
scarcely mentioned it; there was no simple test for its
. identification and prospectors did not bother to learn
anything about it.
With the outbreak of World War Two, beryllium sky
rocketed from a minor rare element to one of major im
portance. Today it is one of the most important, most
valuable and the most sought after in science and in
dustry, with the brightest future for expansion of all
the alloy metals.
As little as 2 per cent beryllium makes copper hard
as steel. It hardens and strengthens aluminum and
magnesium. Its alloys make non-magnetic instru
ments, non-sparking tools~ super stainless-steels, high
speed bearings and propellers for airplanes, and does
so many remarkable things that it has been rightly
and justly called "The Miracle Metal."
It is one of the necessary elements in the Atomic
Bomb as well as other war uses. Its future peacetime
as well as war uses are unlimited: alloyed with alum
inum or magnesium it will build the stronger and
lighter airplanes, automobiles, and the thousands of
other articles which make up our modern progressive
world. Mountains of beryllium ores will be needed!
These instructions will show you how to find them.
Value: The price of berryllium ore is based upon the
"unit," which is 200 pounds of ore containing 10 per
cent of beryllium oxide (BeO). The pre-war price up to
May 1942 was $3 per unit or $30 per ton for ore contain
ing 10 per cent BeO. Present price $40 per unit or $400
per ton for ore containing 10 per cent BeO, plus $40 for
each extra 1 per cent, thus an ore containing 14 per
cent BeO would be worth $560 per ton. These prices are
f.o.b. mines, in which case the buyer pays the freight.
Now for the first time in any book you can learn all
about beryllium: Its 18 known important minerals,
what they are, what they look like, where to prospect,
how and where to find them. Now for the first time an
easy Simple, quick and accurate test for their identific
ation. Our "Five Minute Beryllium Test" will show you
how to identify beryllium, if present, in any mineral in
5 minutes time; make 25 tests for less than 10c. Only a
few pieces of inexpensive equipment required. On
ly three mild chemicals needed, new discovery, no po
tassium cyanide or other rank poisons used. Anyone
can do it!
-2
PART ONE
BERYLLIUM
-3
r
Prospecting for Beryllium
FORMATION: While some beryllium minerals may
exist most anywhere or in any kind of rock, the most
likely formation is in Pegmatite, or in schist or gneiss
usually associated with the same. Pegmatite is a very
common formation, there being thousands of pegmatite
dikes scattered all over most of the United States.
These contain the greatest variety of valuable minerals
of all formations. In addition to the 18 beryllium min
erals, there are some 48 or more valuable minerals
which may be found in pegmatite, yet they are per
haps the least understood and least prospected, and
thus the most fertile field for the prospector who
knows his business. The 48 most important associate
minerals will be taken up in Part Two of these instruc
tions. But first let us understand something about peg·
matite itself; what it is, how to identify it, where to
dig.
WHAT IS PEGMATITE? Book on geology tell us "It
is very coarsely crystalline granite occuring in veins or
dikes cutting ordinary granite." This, however, is very
vague and indefinite; so let us say for our purposes
simply "Veins or dikes containing coarse quartz, feld
spar and mica," in,other words, wherever you find these
you start looking for the 18 beryllium and the other
48 or more associate minerals.
GEOLOGY: Pegmatite is Simply large or small
cracks in igneous or molten rocks, such as granite,
which have been filled with minerals forced up from
below in a molten state by heat and pressure, much
on the order of small elongated volcanoes which barely
reach the surface. This molten mass also contained
much water, with the following results:
First: As the surface cooled much the quickest it
forced the water to the uncooled portion below, and the
minerals followed the water; thus the surface may look
just like common "bull-quartz" showing little or no
mineralization, and so, generally, you must dig to find
the values in pegmatite; however, the values are usual
ly found fairly near the surface.
Second: The pressure being greater in the center
squeezed or forced the water, carrying the minerals to
one side or the other (or in some cases to both sides),
and thus,. this is the most logical place to dig, rather
than in the center.
Third: The outer lower portion, cooling slowly,
caused or allowed the various minerals to separate out
and collect in large or small individual masses; thus
we find quartz in large and small boulders, feldspar in
large or small individual masses, mica in large or
small books,. columbite or tantalite in large or small
nodules, beryl or other minerals in large or small cry
stals or masses, and so on.
Fourth: Due to the above we will generally find
one wall more or less a solid sheet or block of quartz
then the mineralized vein or zone, then the outer wall;
usually of some other material; many times this is
schist or gneiss, and this being softer and more porous
!he water carrying the minerals seeped or was forced
mto the same, and thus are sometimes also mineralized
and so should be prospected.
-4
BERYLLIUM MINERALS
5. BERYLLONITE: Beryllium-sodium-phosphorous.
Beryllium oxide 20 per cent. Specific gravity 3. Hard
ness 5.5 to 6. Crystal form: orthorhombic to platy.
Colors: white, colorless or pale-yellow. Transparent to
translucent to opaque, with brilliant vitreous luster.
Occurs: may be in large masses resembling quartz; or
in plates resembling white or yellow feldspar; or in
small particles scattered through the same; or in
gneiss, schist, or other associate minerals.
-5
6. EUCLASE: Beryllium-aluminum-silicate. 18 per
cent BeO, Specific gravity 3. Hardness 7.5. Colors: pale
green, pale-blue, white, colorless; vitreous to resinous
luster. Occurs: in pegmatite, or more common in chlor
ite schist. Looks like quartz.
7. HAMBERGITE. Beryllium-boron. 45 per cent
BeO. Specific gravity 3. Hardness 7.5. Colors: White,
pale-green, yellow; vitreous to resinous luster. Occurs
in pegmatite or elsewhere. May be mistaken for quartz
or common rock.
8. LEUCOPHANITE. Beryllium-flourine-calcium
silica. 14 per cent BeO. Specific gravity 3. Hardness 4.
Colors: white, yellow, pale-green,. vitreous luster; trans
parent to opaque. Occurs: in pegmatite or fluorspar,
for which it may be mistaken.
9. EPIDIDYMITE: Beryllium-sodium-silica. 14 per
cent BeO. Specific gravity 2.5. Hardness 6. Colors:
white or colorless; transparent to opaque; vitreous to
pearly luster_ Occurs: in pegmatite or elsewhere_ Looks
like quartz or white feldspar.
10. HELVITE: Beryllium-iron-manganese-sulphur
silicate. Beryllium oxide 14 per cent if pure; the pure
crystals more likely to carry near 14 per cent than is
beryl. Specific gravity 3 for pure crystals; if in iron
much heavier. Hardness 6 to 6.5. Crystal form: isomet
ric, tetragonal (resembles garnet). Colors: white, yel
low, green, brown, red. Transparent to opaque, with
vitreous to resinous luster. Occurs at Iron Mountain,
N. M. Is found in small crystals in streaks or masses
in magnetic iron. Likely mistaken for garnet.
NOTE: The large deposit of helvite discovered at
Iron Mountain, N. M., which it is said the government
spent $50,000 in developing, may better show the future
possibilities of milling low-grade beryllium ores. The
Bureau of Mines now indicate laboratory-tests show
promise of concentrating low-grade ores by froth flota
tion. May be future source.
11. DANALITE: Beryllium-iron-manganese-sulphur
and zinc. (Same as helvite except zinc). 14 per cent
BeO. Specific gravity 3.5. Hardness 5.5 to 6. Crystal
form, colors and occurrence, same as helvite. Likely
mistaken for garnet.
12. TRIMERITE: Beryllium-iron-manganese-cal
cium-silica. (No zinc or sulphur). 16 per cent BeO. Spe
cific gravity 3.5. Hardness 6 to 7. Colors: salmon-pink,
brown, gray, white, transparent to opaque; vitreous lus
ter. Crystal form, hexagonal. Occurs: same as helvite;
likely mistaken for garnet.
13. HERDERITE: Beryllium-flourine-calcium-phos_
phorous. 15 per cent BeO. Specific gravity 3. Hardness
5. Crystal form monoclinic. Colors: white, pale-green,
yellow. Transparent to opaque, with vitreous to resin
ous luster. Occurs: in crystal or granular masses, usual
ly in or near fluorspar, for which it is likely to be mis
taken. May be in pegmatite.
14. BERYLLIUM-SPAR: There is one record where
common feldspar has been mined and sold containing
12 per cent BeO. No doubt this is just common feldspar
impregnated with small crystals of phenacite or other
beryllium minerals. So watch feldspar for beryllium.
May be future source of beryllium.
-6
BERYLLIUM-YTTRIUM
-7
BERYLLJ UM GEM STONES
-8
PART TWO
Pegmatite Minerals
All the above may be found in pegmatite associated
with the 18 beryllium minerals; however, in classifying
them as pegmatite minerals we should understand the
following.
First: Some of these are considered strictly pegma·
tite minerals; this, however, does not mean that they
are never found in any other formation, or that you are
sure to find them every time you find pegmatite; it
simply means that pegmatite is generally the most
favorable formation.
Second: Others of these are not generally consider
ed as pegmatite minerals whatever, but as they do
quite often occur in pegmatite they are included as a
"tip" what to watch out for and to become acquainted
with them.
Third: Also remember, we do not include all min
erals which may occur in pegmatite: we cover only
those for which we have a simple test,. or which can be
identified by their physical properties, as explained in
the following pages.
-9
THE NEWER AND RARER MINERALS
Introduction
This is the age of the Alloy Metals. Many of the most
valuable of these are the newer and rarer minerals
which are generally less known, and which the average
prospector is walking over in the hills today and the
small mine owner is throwing upon the waste dump
unrecognized. Many of these are far more valuable
than the old standbys.
-10
THE RARER METALLIC MINERALS
-11
8. POLYCRASE: Columbium·tantalum-iron-urani
um. Variable percentages of each. Specific gravity 5.
Hardness 6. Colors: brownish-black to black. Occurs:
usually as nodules or as grains in pegmatite. Likely
mistaken for common rock.
9. WOHLERITE: Columbium-tantalum-calcium-sili
ca. Per cent variable. Specific gravity 5.5. Hardness 5.5.
Color: brown or light-yellow; vitreous luster. Looks like
common rock.
TITANIUM-Ti
THE ELEMENT: Lustrous white metal. Never found in
metallIc state in nature. Specific gravity 4.5; weighs
280 pounds per cubic foot. Melting point 1800 degrees
C. The oxide discovered in 1791; pure metal in 1910;
much used in making paint, welding rods,. etc. Value
pure metal $5 a pound. Identify: all ores by test 13.
10. RUTILE: Main are at present, Titanium oxide
60 per cent: Specific gravity 4. Hardness 6 to 6.5. Colors:
brown, red, yellowish, black. May be mistaken for rock
or iron.
11. ILMENITE: Titanium iron. Titanium oxide 31.6
per cent. Specific gravity 4.5 to 5. Hardness 5 to 6.
Lolors: Black, or brownish-black. Occurs: usually in
platy crystals in quartz; common in pegmatite. Looks
like common iron.
12. OCTAHEDRITE: Titanium dioxide. Titanium
60 per cent. Specific gravity 4. Hardness 5.5 to 6. Colors:
yellow, red, brown, black. Occurs in pegmatite. Looks
like iron.
13. TITANITE: Titanium-calcium-silicate. Titanium
oxide 40 per cent. Specific gravity 3.5. Hardness 5 to 5.5.
Colors: Gray, yellow, brown, black. Looks like com
mon rock.
14. BROOKITE: Titanium oxide. Per cent variable.
Specific gravity 4. Hardness 5.5 to 6. Colors: yellowish
red brown, black. Occurs: usually in cubical crystals
in pegmatite or elsewhere. Looks like rock; or if black,
like iron.
TIN-Sn
THE ELEMENT: A soft tin· white malleable metal.
Never found in metallic state in nature. Specific grav
ity 7.2; weighs 455 pounds per cubic foot. Melting point
231 degrees C. Known from ancient times. Very little
produced in the U. S. up until about 1942. Now several
quite large deposits known. No doubt others will now
be found with our "2 minute Tin Test"; prospectors are
walking over it today calling it "iron"! Value: present
price for ores $1 per pound for contained tin; thus a 50
per cent are now worth about $1,000 per ton. Identifica
tion: All ores by our quick Test No.4.
15. CASSITERITE: Tin oxide. Main are. Tin oxide
78.6 per cent. May be found in lode or placer; both oc
cur in fairly large quantities in New Mexico and sev
eral other states. Specific gravity 7. Hardness 6 to 7.
Colors: black, brown, red, yellow, green, white. Occurs:
usually in granite, pegmatite rhyolite etc. Looks like
common iron if dark colored; light colors look just like
common rock.
-12
16. STANNITE (Tin Pyrites): Tin-copper-iron-su}
phur. Tin oxide 27.5 per cent. Specific gravity 4.5.
Hardness 4. Colors: steel-gray bronzy. Occurs: in peg
matite or with copper ores. Likely mistaken for copper.
17. CYLINDRITE: Tin-lead· antimony. Percentage
variable. Specific gravity 5.5. Hardness 2.5 to 3. Color:
gray-black. Somewhat resembles stibnite or galena
and mistaken for the same. Occurs: massive in veins
or particles in rock.
BISMUTH-Bi
THE ELEMENT: A white brittle crystalline metal. May
be found in native state, but seldom. Specific gravity
9.78; weighs 612 pounds per cubic foot. Melting point
271 degrees C. (Can be melted in match flame). Much
used alloyed with tin or lead in low melting point com
pounds, such as for fuses, safety-plugs in boilers etc.
Also much in medicine etc. Value: pure metal around
$2.00 per pound; Ores depending on grade. Identifica
tion: all ores by Test 25.
18. NATIVE BISMUTH: Usually with some anti
mony sulphur, etc. Specific gravity 9.5 if pure, seldom
pure. Hardness 2 to 2.5. Colors: silver-white, but tar
nishes black. Occurs: usually granular as outer coating
on rocks, in veins with lead, silver, etc. Mistaken for
white or black iron.
19. BISMUTHINITE: Bismuth sulphide. Bismuth 81
per cent. Specific gravity 6.5. Hardness 2. Colors: lead·
gray to tin-white Nith yellow tarnish. Resembles white
iron when fresh broken. Occurs: usually massive or
fibrous.
20. BISMUTITE: Bismuth oxide. Bismuth 88 to 90
per cent. Specific gravity 6.5 to 7. Hardness 4 to 4.5.
Colors: white to greyish-yellow to green. Looks like
common rock.
21. BISMITE: (Bismuth ochre). Bismuth trioxide
89 per cent. Specific gravity 4.5. Hardness very soft,
crumbly, likely mistaken for dirt or clay. Occurs as an
earthy yellow powder.
22. URANOSPHAERITE: Bismuth·Uranium. Bis
muth oxide 42; Uranium oxide 57.7 per cent. Specific
gravity 6.5. Hardness 2.5. Colors: orange-red to brick
red, looks like rock.
23. TETRADYMITE: Bismuth-Tellurium. Bismuth
59; Tellurium 36 per cent. SpeCific gravity 7.5. Hard
ness 1.5 to 2. Color: tin-white but tarnishes black; like
ly mistaken for iron. Identity: Bismuth by Test 25;
Tellurium by Test 3.
URANIUM-U
THE ELEMENT: A white, hard and heavy metal. Nev
er found in metallic state in nature. Specific gravity
18.68; weighs 1,167 pounds per cubic foot. Melting point
1850 degrees C. Discovered 1789; first metal 1881, but
little used until after 1900. It is source of Radium, also
the atomic bomb. Value of ores depends upon grade.
Identification: All ores by Test 17.
-13
24. PITCHBLENDE (Urani.nite): Chief o~e of Ra
dium. Composition variable, usually contams some
lead, copper, rare earth or. ?ther e~ements. Per~entage
of uranium variable. SpecIfIc gravIty 9 to 9.7 If pure,
seldom pure. Hardness 5.5. Color, black with pitch
like luster; when freshly broken somewhat resembles
fresh broken cold tar, otherwise looks just like black
iron for which it is likely to be mistaken. Occurs: in
larg~ or small nodules, or as black particles in rock or
as black masses in veins in rock.
25. TORBERNITE: Uranium-copper-phosphorous.
Uranium oxide 61.2 per cent. Specific gravity 3.5. Hard
ness 2 to 2.5. Colors: various shades of green; likely
mistaken for low-grade copper. Occurs: usually in
thin tabular or micaceous form.
26. URANOPHANE: Uranium-calcium-silica. Per
cent variable. Specific gravity 4. Hardness 2 to 2.5.
Color: yellow, with vitreous luster: likely mistaken for
common rock. Occurs: groups or radiating or fibrous
crystals or masses.
27. AUTUNITE (Lime Uranite): Uranium-calcium
silicate. Percentage variable. Specific gravity 3.5. Hard
ness 2 to 2.5. Colors: lemon to sulphur-yellOW; likely
mistaken for Common rock. Occurs: usually in tabular
crystals.
28. GUMMITE: A silicate of uranium-lead-barium
calcium. Uranium trioxide 60 to 70 per cent. Specific
gravity 4. Hardness 2.5 to 4. Colors: yellow, orange,
red, brown, may be mistaken for common rock. Occurs:
platy or granular. Usually contains some pitchblende.
TUNGSTEN-W
THE ELEMENT: Name from German, Wolfram, thus
its symbol W. It is a hard brittle gray-black metal.
Never found in metalic state in nature. Specific gravity
19.3; weighs 1,193 pounds per cubic foot. Melting point
3370 degrees C. (highest of all metals). Much used in
lamp filaments, steel making, etc. Tungsten Carbide
one of hardest compounds known. Value: ores or con
centrates 65 per cent tungsten trioxide up to $2.00 per
pound. Identify: all ores by Test 3.
29. WOLFRAMITE: Tungsten-iron-manganese
(iron in excess of manganese). Tungsten trioxide 76.5
per cent. Specific gravity 7 to 7.5. Hardness 5 to 5.5.
Colors: black, grayish to brownish-black; likely mis
taken for iron. Occurs: massive, granular or platy form,
or in needle-like crystals.
30. HUBNERITE: Tungsten-manganese-iron (man
ganese excess of iron). Tungsten trioxide 75 per cent.
Specific gravity 7 to 7.5. Hardness 5 to 5.5. Colors: us
ually blackish-brown but in rare cases blue-black.
Likely to be mistaken for iron. Occurs: same as wol
framite; hard to distinguish between, but unnecessary
as test will tell if tungsten is present.
31. FERBERITE: Tungstate of iron. (Sometimes
manganese). Tungsten trioxide 76.3 per cent. Specific
gravity 7 to 7.5. Hardness 4.5 to 5. Colors: black to
brownish-black. Occurs: usually fine granular. Likely
mistaken for black iron.
14
32. SCHEELITE: Calcium tungstate. Tungsten triox
ide 80 per cent. Specific gravity 6. Hardness 4.5 to 5.
Colors: white, yellow, brownish, reddish, sometimes
greenish. Most likely mistaken for barite in color,
weight and hardness; or may be mistaken for quartz
or calcite if particles in rock. Occurs: as platy crystals,
massive or granular.
33. STOLZITE: Tungstate of lead. Tungsten triox
ide 51 per cent; lead 45 per cent. Specific gravity 8.
Hardness 3. Colors: yellowish grey, brown, red. Likely
mistaken for just lead ore.
34. TUNGSTITE: (Tungsten Ochre): Tungsten triox
ide 79 per cent. Specific gravity 5.5. Hardness 2.5 or
less. Colors: bright-yellow to brownish-yellow. Occurs
in earthy compact masses resembling hard clay.
MOLYBDENUM-Mo
-15
Miscellaneous Pegmatite Minerals
-16
DUKE'S
(Copyrighted)
INTRODUcrION
In "Beryllium-How and Where to Find It," we cover
15 of the more important known commercial beryllium
minerals or ores, and three most valuable Gem Stones.
The gem stones, we will find, always have the same
uniform characteristic physical properties such as col
or, hardness, etc., wherever found and thus may be
fairly accurately identified by their physical proper
ties alone. But in studying 15 commercial minerals we
find none of them possess any uniform characteristic
physical properties by which they may be identified:
that is they may look just like common rock, quartz,
iron ore, garnet or obsidian.
The above being true you may ask: "Then how do I
know WHEN to test for beryllium?" The answer is
You do not know! That is the object and purpose of
our test!-to find out! If you already knew it was
beryllium mineral there would be no object or reason
for testing it!
Here is the idea: Remember beryllium is a very
valuable element; you are playing for big stakes and
thus can afford to go to a little extra trouble to find
it-at least five minutes. After your solution is pre
pared it takes but about 5 minutes per test and costs
less than % cent each. In other words, you are gamb
ling five minutes time and % cent against a possible
fortune! So you simply proceed as follows:
First: Save up your rocks( numbered-where found)
until you have a number on hand-then test the
works regardless of what they may look like! Besides
the 15 listed, you may find a whole mountain of a new
mineral unknown at present! Not impossible! In fact,
the large deposit of Helvite found at Iron Mountain,
N. M., on which it is said the government has spent
$50,000 in developing, may be just such a deposit. Pro
spectors walked over this for years calling it "garnet!"
Second: The Helvite at Iron Mountain is not found
in large pure chunks or crystals as usually the case
with beryl, but consists of small crystals of helvite in
streaks or clusters in iron, thus a milling proposition to
separate the helvite and iron which has been worked
by froth flotation. No doubt the bulk of beryllium of
the future will be so obtained; by milling large de
posits of low grade ores, as now done with Molybden
um at Climax, Colo. This possibility should be kept in
mind in prospecting for beryllium.
Third: Known specimens, like physical properties,
are of value--if properly used: they will give some
idea what a certain mineral "might" look like, but do
not depend upon them entirely; your "big hit" may be
something which looks entirely different; one of the
other ores of which you have no sample, or an entirely
new one now unknown. Do not guess-make a test.
Only a chemical test will tell!
quantitativ~: This test may be made semi-quanti
tatIVe: The brIghter the blue the more beryllium pres
ent. By using the same amount of material and com
paring with one of known percentage, a fairly close es
timate of the percentage of the unknown may be ar
rived at. At least, poor, fair or good.
GENERAL INFORMATION
TEST EQUIPMENT
The following equipment is all that is needed. If you
now have our "Field Kit" for our "Quick Qualitative
Analysis" all you will need are the last eight articles.
1 Alcohol Lamp, about 2-ounce capacity best size.
1 Blowpipe for making fusions.
1 Small porcelain mortar and pestle; size 000 best
size.
3 Medicine droppers for handling solutions.
1 Metal holder for chinaware for making fusions.
1 Test tube %·inch by 4-inch for Quinalizarin Solu
tion.
1 Small porcelain dish for test solution (beryllium).
1 Small porcelain dish or spot plate for tests.
1 Small porcelain dish (if no spot plate) for "blank"
(can use piece of broken plate for quick tests).
1 Smallest amount Quinalizarin dye powder obtain
able.
1 ounce Borax Glass for making fusions.
1 Ounce Sodium Hydroxide for fusions (pellets best).
2 Small test tubes (2-inch x 14 ·inch best size) to
learn to distinguish beryllium from magnesium.
1 or more small pieces chinaware for fusions.
1 Sample Magnesium Ore for practice and compari
sons.
1 Sample Beryllium ore for practice and comparisons.
"BERYLLIUM TEST"
(Also for Magnesium)
METHOD OF PROCEDURE
NOTE: First read the previous instruction under "Gen.
eral information" over carefully, then proceed as fol·
lows: