----------------------- Page 1----------------------F-06/02 ACCREDITATION Issue Date: 26/05/08 Rev. No: 05 DOCUMENT LAB 003 Testing Laboratory.

Accreditation Scope of Qarshi Research International (Pvt) Ltd. Hattar, Paki stan Permanent laboratory premises Materials/ Minimum Products tested Detection Limit X

Type of Tests/ Rang of Uncertainty Standard Properties Measurement of Specification/ measurement Measurement Techniques/ (where applicable) MU (+) Equipment

-Natural Health > 10 cfu / ml Supplement (1) -Food & Farm

used Aerobic Plate Counts > 10 cfu / ml Not applicable HPB Method MFHPB-18 October 2001

Product(2) (Health Products and Food Branch -Natural Health > 100 cfu / ml Supplement (1) -Food & Farm March 2002 Product(2) (Health Products and Food Branch Ottawa, Canada) Presence/Absence of Not applicable USP 28 <61> Salmonella Presence /Absence Ottawa, Canada) Yeast & Mould Counts > 100 cfu / ml Not applicable HPB Method MFHPB-22

Single viable

organism in 25 g/ 25 ml of analytical unit Single viable organism in 25 g/ 25 ml of analytical unit > 1 cfu / ml

2005

Presence/Absence of Not applicable USP 28 <61> E-coli 2005

Presence /Absence

Total Viable Plate Not applicable HPB Method Counts MFHPB-18 October 2001

> 1 cfu / ml

(Health Products and Food branch Soft drink, Water, Ottawa, Canada) Fruit Juices > 1.8 MPN / 100 ml Total Coliform Not applicable 1.8-1600 Official Method MFO-9 November 30, 1981 (Health Products and Food Branch Ottawa, Canada) Heterotrophic Colony > 1 cfu / ml Not applicable HPB Method Count 35 37 C MFHPB-18 Heterotrophic Colony > 1 cfu / ml Not applicable October 2001 Count 20 22 C (Health Products and Food branch Ottawa Canada) _____________ __________________________ Date Director Page 1 of 5 __

> 1 cfu / ml Water > 10 cfu / ml

----------------------- Page 2----------------------F-06/02 ACCREDITATION Issue Date: 26/05/08 Rev. No: 05 DOCUMENT LAB 003 Materials/ Minimum Products tested Detection Limit Type of Tests/ Rang of Uncertainty Standard Properties Measurement of Specification/ measurement Measurement Techniques/ (where applicable) MU (+) used Not applicable Water March 2002 Yeast & mould Counts > 10 cfu / ml (Health Products and Food branch Ottawa, Canada) Presence/Absence of Presence /Absence Not applicable USP <61> (USPStaphylococcus aureus 28), 2005 > 10 cfu / ml HPB Method MFHPB-22, Equipment

Single viable - Natural Health organism in Supplements (1) 25 g/ 25 ml of - Food & Farm analytical unit Products (2) Single viable - Pharmaceuticals organism in Articles (3) 25 g/ 25 ml of analytical unit Single Viable organism in

Presence/ Absence of Presence /Absence Not applicable USP <61> (USPPseudomonas 28), 2005 aeruginosa

Presence/ Absence of Presence /Absence Not applicable USP-28 <61>2005 Staphylococcus aureus

25 g /25 ml of Analytical Water unit Single Viable organism in aeruginosa 25g / 25 ml of analytical unit Food 10 /g Coliforms/ Not applicable E.coli Not applicable Coliforms VRB method > 10 /g Oxoid/ Merck Pour Plate SME >01 / 100ml Chromogenic Method Filtration Filtration Assembly SME Natural Health Supplements (1) 2.00 - Food & Farm Products (2) - Pharmaceutical RI=1.33 Articles (3) Brix = 10.0 0 Z =12.5 Concentrated Medicinal/ 1.0 Refreshing Syrups Polarity 0.22 Specific Gravity 0.04 (ASTM). Brix / Refractive Index USP 25 <831> RI 10.0-90.0 0.4 Method page 2071 0 Polarimeter Z 12.5-130 USP 25 <841> Sp 1.00-1.50 Gr Method page Ph measurement 0.06 Method based on 2.00-11.00 SW- 846, SW-846 & Method C-13 Presence/ Absence of Presence /Absence Not applicable USP-28 <61>2005 Pseudomonas

01 /100mL Water

2 g Natural Health

2071 LOD (Loss on Drying) At max 160 C USP 25 published 2 gm - 5 gm 0.39 g method (< 731>

Loss on Drying) Supplements (1) page # 2028 Papers

_____________ ___________________________ Date Director Page 2 of 5 ----------------------- Page 3----------------------F-06/02 ACCREDITATION Issue Date: 26/05/08 Rev. No: 05 DOCUMENT LAB 003 Materials/ Minimum Products tested Detection Limit Type of Tests/ Rang of Uncertainty Standard Properties Measurement of Specification/ measurement Measurement Techniques/ (where applicable) MU (+) used Disintegration Time > 1 min at USP 25 <701> 1.0 min 37 C, page 2010 Natural Health Wt. Per Tablets 100 mg Supplements (1) 0.20 mg USP 25 <1251> 150 mg -700 mg weighing on analytical balance Solid dosage forms 100 mg USP 25 <1216> Tablet friability 0.11 mg Page # 2255 > 100 mg Equipment

1 min

(Tablets) 8 N

Tablet hardness Method based on > 8 N 0.12 N equipment manual

PET Bottles, Glass Minimum 50 bottles ml

Brimful Capacity Density Method > 50 ml 0.62 ml Paper Grammage D 646-96 (2001)

2 2 80 mg / m Labels/ Paper 0.23 mg / m Grammage of - Natural Health 0.5 mg/L Supplements (1) 0.5 mg/L - Food & Farm Products (2) 0.5 mg/L - Pharmaceutical Articles (3) 0.1 mg/L - Water & Waste waters etc. 0.5 ppb ICCUMSA Sugar / Sucrose reading 15 at least ICUMSA Sugar / Sucrose reading 5 at least Sugars confectionaries, corn Syrups, cordials, distilled liquors, Non alcoholic > 0.1% 0.2 beverages, Milk & Acidity % Titration Method UV Visible Turbidity 0.88 5 - 1000 Spectrophotometer paper Elemental Analysis Ca 0.12 ppm FAAS Elemental Analysis Ni, 0.12 ppm FAAS Pb, Fe, Cu, Elemental Analysis Na 0.14 ppm FAAS Elemental analysis Cr, Mg, Cd, Zn, K, Mn 0.12 ppm FAAS Trace element Analysis 1.6 Sb, As, Hg FAAS & HVG > 0.5 mg/L > 0.5 mg/L > 0.5 mg/L > 0.1 mg/L > 0.5 ppb 2 Std. TM for > 80 mg/m

UV Visible Colorimetric analysis 0.1 Spectrophotometer

15 - 100

0.1% milk product, canned vegetables, food dressing, fruit & fruit products. Solid & Semisolid Soxhlet Apparatus Fat % 0.1% foods Method Food (cereals & cereal products. malt, Cocoa & Oven Drying Cocoa products, 0.1% cane, beet, raw & refined sugars or foods other than _____________ __________________________ Date Director Page 3 of 5 ----------------------- Page 4----------------------F-06/02 ACCREDITATION Issue Date: 26/05/08 Rev. No: 05 DOCUMENT LAB 003 Materials/ Minimum Products tested Detection Limit Type of Tests/ Uncertainty Properties of measurement Measurement (where applicable) MU (+) used acidic, Fruits & vegetables products)and animal or poultry feed Rang of Standard Measurement Specification/ Techniques/ Equipment __ Moisture % 0.4 % Method > 0.1 % 0.4 % > 0.1 %

Cereals & cereal products, milk & milk product, fruits and vegetables products, sugar & 0.1% sugar products, sea foods, bakery products, and animal of poultry feeds 5 mg/L 5 mg/L 5 mg/L 5 mg/L 5 mg/L Alkalinity 6.7mg/L Carbonates 1.1 mg/L Bi Carbonates 4.2 mg/L Total Hardness 4.1 mg/L Acidity 0.14 mg/L COD 8.8 mg/L Method Respirometric 0 ppm- 200 ppm Method Argentometric 5 mg/L Chloride (Cl ) 1.34 mg/L Method Water (drinking, 5 mg/L process) And Wastewater 5 mg/L TDS 2 mg/L TSS 3.0 mg/L Sulphate (SO ) 0.58 mg/L 4 Spectrophotometer UV-Visible >5 mg/L Gravimetric Method >5 mg/L Drying Method UV-Visible > 10 mg/L 10 mg/L > 5mg/L > 5 mg/L Titration Method >5 mg/L Titration Method >5 mg/L Titration Method >5 mg/L Titration Method >5 mg/L Titration Method Open Reflux >5 mg/L 5 mg/L Ash % 0.2 % method Muffle furnace > 0.1 %

0 ppm

BOD Not applicable

1 mg/L

Nitrates (NO ) 0.60 mg/L 3

> 1 mg/L Spectrophotometer UV-Visible

0.2 mg/L

Fluoride (F ) 0.58 mg/L Conductivity 1.66 mg/L Oil & Grease 6.8 mg/L

> 0.2 mg/L Spectrophotometer > 20 S Conductivity Meter Partition 2 mg/L Gravimetric Method

20 S

2 mg/L

Titration Determination of FFA in Method Crude & Fats & Oils 0.1% Refined oils 0.1 0.1% -50.0%

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ACCREDITATION Issue Date: 26/05/08 Rev. No: 05 DOCUMENT LAB 003 Materials/ Minimum Products tested Detection Limit Type of Tests/ Uncertainty Properties of measurement Measurement (where applicable) MU (+) used Rang of Standard Measurement Specification/ Techniques/ Equipment

(2.0-50.0) 0.5 Determination of Per Indirect Mili.equi.of Mili.equi.of Fats & Oils Peroxide/Kg Value (POV) Method Sample Of sample Oxides 1.0 % Titration Peroxide/Kg of

Sugar based Products (solid, Semisolids and Determination Liquid), 0.2 % Confectioner , Honey, 3.0 % Of Sugars Method Lane &Eynon 0.5 % -99.5 %

biscuits and Cookies etc. Beverages, Juices, Soft Drinks, 0.2 % Wines and Syrups etc. Liquid, solid, Semisolid 1.0 % Foods and

Determination Of Sodium 3.0% Benzoate Determination Of Crude 1.5 % Proteins Macro Kjeldhal 4.0 % - 25.0 % Method Extraction/ Titra 0.5 % -5.00 % tion Method

Feeds. Foods (that Contain fibrous Acid /Base Determination Materials)and 1.0% Animal or poultry Method feed 2% Of Crude Fiber 3.0% - 25.0 % Digestion

_____________ ____________________________ Date Director Page 5 of 5