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PROTONS
CHARLES
H.
BOWEN,
IR.
PRECESSION OF PROTONS
PRECESSION OF PROTONS
by
Charles H. Bowen, Jr.
ENGIN^.^RING EIECTHCNIC3
^>y
Monterey, California
This
wori<
is
accepted as fulfilling
the thesis
MASTER OF SCIENCE
IN
ENGINEERING ELECTRONICa
25283
PH5FAC5
This fHper describes the
of
device for
measuring the absolute values of, as well as mall changes in, the earth's
magnetic fieldo
The author's work on this device was accomplished at the Varian Assoc-
to hira in 1948,
to Dr. Martin Packard, the Director of Nuclear Spectroscopy at the laboratory, for his help and enttourageraent
o
li
TABLE OF CONTENTS
Page
Preface
Table of Contents List of Illustraticxis
ii
iii
V
1
Chapter 1
Chapter II
Introduction
Other types of Magnetometers
1. Dip Needles 2.
Earth Inductor
2
2
3 3
Station Magnetometer
of
Chapter III
Method
Attack
5
1, Theoretical Background
2, A
16
Chapter IV
Experimental Equipment
1. Polarizing Coils
2.
26
29
Receiving Coil
31
31 32
37
Narrow Band
7o Analoging Circuit
42
Chapter V
Chapter VI
Experimental Results
Conclusions
1. Possible Errors
44
46
46
iii
TABLE OF CONTENTS
Page
Appendix
48
57
Appendix II
Appendix III
Appendix IV Appendix V
58
59 86
8?
Bibliography
lY
LIST OF ILLUSTRATIONS
Fif^ure
Page
lo
2o
3.
8
9
4o
5o
Components of vector M
Proton resonance fcr ol molar solution of in water
30 MoC. R.F. Head
11
/^
r\
S04
12
6o 7o 8o 9.
14
15 17 19
lOo
19
11.
21
22
12
13
23
14.
Timing wheel
Polarizing coil circuit
Transient response of polarizing coil
2?.
15.
l6o
28
29
17.
Preamplifier
Q multiplier circuit
Photographs showing result on a hi^ Q circuit
Narrow band amplifier
cf
32
33
18 o
19 o
35 36
36
20o
LIST OF ILLUSTRATIONS
Figure
21,
22.
Page
One stage of binary circuit
38
39
AG 45
23 o 24 o
vi
CHAPTER
INTRODUCTION
The measurerBrib
of the
Icaig
bean of inter-
arvl
meter that measures the earth's field by measuring the free precession
(out of
50000
q) on
};
can be detected.
available for measuring the absolute value of the earth's magnetic field.
Further, changes of much less than h
frequency of
use
^ 1
10"^ gausa
CHAPTER II
m^
Naedlea
A balance
Changes in the
Jo
about 50000 Y^
Earth Inductor
This instrument is frequently used by magnetic observatories for
It consists
of a high speed rotating coil which generates a voltage for all orien-
tations exceot those for which its axis is parallel to that of the magnetic
3chmidt-Type Magnetometer
This device is widely used in magnetic prospecting.
It is similar
to the dip needle in that there are ooposing gravitational and magnetic
torques.
It
pivoted
but
even
This device
able reactor.
is
high permeability
If an alternat-
such that the earth's field can very nearly saturate it.
ing field, obtained from a coil, is superimposed on the earth's field the
core will saturate each cycle.
The phase cf each cycle at which satur-
Small changes of a
is
second.
T^rtiich
fieM
The
Station iMagnetometer
5ven a brief description of a station magnetometer would be too
McCorab,
The
one
wallad building with sawdust between one pair of walls and air between
the
equipment.
necessary.
Accuracy of better
to obtain.
CHAPTER III
METHOD OF ATTACK
1.
Theoretical Back/;round
An entirely new approach to the nagnetcmeter problepi was opened
Bloch,
Packard and Hansen (2) at Stanford and Purcell, Torey and Pound (8) at
Harvairl pioneered in this work.
follows.
The notation used follows that of Block (2) and Packard (7).
{zITv^b Planck's
the electron."
For the
nuclear magneton
njJii
However, careful measurements have shown that fcr the proton, since it
is not simply a spinning spherical shell of mass
The angular momentum and magnetic moments are ralat-^d by the gyro-
(This
is unrelated to ths
unit of magnetic
/^ -r5?
The vectcrs /(Aand (2^re either parallel, in which case
jis positive, or
anti-parallel and
is then negative
frequency.
strength Ho
^ ^ X
r:
uO
have jOquals
for protOTis,
Y^*
"^^^
ratio of
The fre-
^ Hi (^)
'
Total magnetization per unit volume
,
^<^
>-
'^/j'^
unit volume.
Further/*^ equals %/Tme re TCis the susceptibility, for the o -*" / / proton at roan temperature: / ^ x, X /
yd
=r
*/
>^
field
o)
The
polarizing field.
axis alon-^ the x axis, then we would have the setup shown in figure 2,
Figure 1,
Fitnire 2a
If ths coils oriented along the >^ axis are excited at a frequency
of
which has been processing about the polarizing field Ho, to absorb energy
from the source of R.F. voltage.
(The R.Fo field is termed the
H^^
field
Thus, as
long as no sample was present to be polarized, the R.Fo vectors have ccntponents alon^^ the x axis but
zero.
c exponents
adds to one or the other of the two rotating RoF. vectors depending on the
direction of rotation of
about the
z
A\
This vector,
,
/ij
is initially processing
angle
If
'
Figure
3<.
Ho, H|^
and M rectors
Howevsr, as the vector attempts to precesa about the field that is the
resultant of Ho and H^,
increases so that /^
at resonance, is rotating
in the xy plane and is in phase with one of the two RcFo vectors previous-
ly discussed.
il
A -
JL
'
-^
^^
->
along the
z axis,
If we assume that
uJo"
^^
^^
Uid
H;;<:
=r
2.
H,
Cos
u^ir
10
ccfi,
r s:a{
Figure 4.
Components of vector Mo
So that
and tgt
inrtien
^ equals
The
^ Ho
ill
(f>
equals 90
equals^.
negative in sign.
It is often easier to obtain resonance by havir^ a constant RoFo
frequency and start with a value of polarizing field that is near that
required for resonance.
field along the z axis with sweep coilu at an audio rate, the nuclear
monent /! can be made to pass thru the xy plane and, hence, resonance, at
an audio rate^
If, in addition to these coils already described, there is added
J^
receiving coil,
er coil by M
11
The transmitter coils, receiver coils, sample, plus certain matching networks are usually contained in an R,F, head called a probe
o
detected
usually
The
ment
shows an os-
*f
*i
ff~^
Figure 5.
ol'
12
One of the difficulties in realizing great accuracy vdth the magnetomet-^r operating in the 30 megacycle region is the
-d
difficulty of reading
has a waveform given
by Bloch as:
\4
T -^
Where
T,
and T^ are relaxation tine constants and other factors have The exact shape is difficult to determine,
Furthei;
The problem of
may exist in the field and because of the possibility of assymetry that may
exist in the wave shape due to a mixture of u and v "modes" as described
by Bloch. (1)
A common and very useful application of nuclear induction is in the
For example, the various proton lines of some substance such as ethyl al-
7<.
Mov-
ing to the right along the abscissa on the tape of figure 7 corresponds to
The sample being studied is placed in an R.Fo head which contains the
13
Figure 6.
lif
H
1
ri
1
c
1
c
\
oH
a^^ci^^
/*
6*"
nf*
//*'
f^
i^^ S,
Figure 7.
2.
is made
ileld strength
n by measuring frequency
60.
electron resonance
This possi-
bility, the use of electrcai resonance for low field measurement, was in-
t-
2000
could be obtained.
The material that follows will describe a new technique that utilizes
the free precession of protons in water to measure tha small magnetic field
of the
earth.
earth).
This polar-
field.
16
TZTTK^i
TTTU
"%
Figure 80
After
5 T,
exponentially decreasing amplitude, about the only magnetic field remaining, that of the earth.
will precess about the earth's field in the same way that it preHovaver, the frequency
equals
H on
17
Thus, for the 30 Mc probe discussed earlier, the field associated with
it was about 7000 gauss.
and the polarizing field, a snail signal of a few microvolts would be in-
is
then the amplitude of the signal induced in the receiving coil is reduced
but its frequency is unchanged.
18
1^
Figure 9.
^JJo^:^ r
my^^
1
cr
rf/
P/'C U*s\jp
^^f^'^h'
f^r
c^
t/r
H c
Figure 10
Since it
is
However,
the earth's magnetic field is homogeneous over a very large area and this
makes it possible to use quite large samples and thus obtain better signal
to noise ratios.
The polarizing coil should be capable
in series with the coil has been shown by Packard (7) to be:
V "ooen c ircuit N
A
^fp'A^^^i^'C^SU^t A/O""^
i/c/^^
=
=
= =
^
'^^ 3.U x 10
susceptibilityjtM =
//
Ho =
N =
^^'^
=
A^
K T
=
~ =
X 10~23 erg/gauss
Boltman's constant
291
The voltage across the capacitor shown in figure 11 which is the vol-
tage appli-^d to the grid of the first stage of the preamplifier is Q times
Voc.
^ -l^- where Q
i th Q of the
20
receiv<9r coil.
is:
Tu //
k1
Cc^^^^
'Lfcr
X
Figure 11.
Input to first stage of preamplifier,
hi^
Q is desirable.
Therefore,
it
is desirable to redui*
21
A shift of
25
corresponding to
Noise
^ equals
^/CTilwhe re
^L
If a
Figure. 12.
22
/f
^ t\l UJT
of the
was important that the signal not build up tor slowly for, if
be obtained.
is included as appendix I,
Feck
I.O
\i
fi-
/>
.z.
\
./
,i
-t
-y
/.o
"
^V^
^^
Figure 13.
Impressed on a circuit
23
The waveform shows that the transient condition caused by the high
Q circuit lasts only about one-tenth of a second which is not serious
since the total counting time expected to be available before the signal
is
sufficient amplitude and count the frequency with some device such as a
The HoPc y^U\. will count a 2 Kc audio freIt will count for 1 second of the signal
frequency with an uncertainty in the count of 1 cycle of the signal frequency which corresponds, for a one second count, to an uncertainty in
the earth's field of 25
J
o
the HoPo 52AA is to use the signal frequency, the 2 Kc, to gate on and
I
HcP. 52/fAo
In its normal use the gate would be kept open for 10 cycles
of the signal frequency during which 500 cycles of 100 Kc is counted with
tinue for much longer than 10 cycles of the signal frequency if accuracy
on the order of 1 ^ is to be obtained.
noise bursts that can occur and cause errors in the counting.
24
will decrease by a factor l/e each tins the range is doubled after reaching some S/N ratio that first causes some small error to exist in the
counting.
effects
This is the
one
time the range is doubled; the other a l/e decrease in accuracy each time
the range is doubled after reaching the critical S/N ratio.
The count
should always be continued to the critical value of S/N and to .567 of one time constsmt thereafter
This conclusion is justified in appendix II,
25
CHAPTBR IV
EXPERIMENTAL EQUIPM3JT
The following system components will be described:
1, 2,
3,
Polarizing coils
Receiving coil
Sample of 'water
h.
5.
Preamplifier
-\niplifier, Narrow
Band
6.
7o
Analoging circuit
lo
Polarizing coils
These two coils each consisted of 1200 turns of
/^18
vdre.
The D.C.
henry.
The
inside
It was
of a
sajTiple,
offl
The wheel rotated at 2 rpm which permitted one cycle of polarize and
A schematic
diagram of the
26
t'cfO
^' ^(^
(D
Figure 14.
Timing wheel
of the notch,
S]^
was closed o
caused
si
and S5 to close.,
mately 10 seconds, the power supply provided two amperes of current to the
polarizing coils and the water sample was thereby polarized.
tation
cf
As the ro-
the wheel continued, the microswitch arm dropped into the notch
to open.
causing
s-^
s^i^
R]_
(80,iH).
C2 was
^r. v^|
27
Fe
h- f
>
<
^^
Cvt
w^ tc/
l<
\
\
\
X->
YT
"d^i
\^
J
jrr\yyy'\
Co
.1
~yMy
v^
i>
\
\-
Figure 15.
Polirizirif;
coil circuit.
28
Pc/a
y^'r
yt
Cc
/ ^ (^
^/^
if)-se-
//^A
recU c
^i
c a
Figure 16,
The opening of Sr leaves the polarizing coils free to ring at the high
frequency but low amplitude deteniiined by the inductance of the coils and
their distributed capacitance.
See figure 16.
The voltage rises initi-
ally then decays for 2A raillisec(xids before the high frequency ringing
ccanmenceso
the polarizing coils induce large, unwanted signals in the receiving coil
which block the amplifying stages and cause ringing of the high Q circuits.
2.
Receiver coil
This coil was 4" long and had a 3.5" inside diameter.
It consisted
29
of 3500 turns of
)^26 ^dr^
The D,C.
polarizing coils it
is
cutoff so that the many small nuclear mom-^nts which combine to form the
tJius
Experience his shown that if cutoff is too rapid a smaller signal results.
This is tentatively accounted for by a fanning out of the nucl3ar moments
that combine to form K
with
a resultant
On cage 20 the equation for the maximum Wns voltage at the grid of the first stage of the preamplifier was given.
It depended on several
in the
coils and r'eceiving coil, the theoreticdj. value of maximum rms voltage to
be exoected at the grid of the first stage of the preamplifier is lo8
millivolts.
(The
saii^ple
sample.
30
An artificial
signal fron a signal generator was then introduced at the first grid of
the preamplifier and its amplitude at that point adjusted until the pre-
amplifier output as shown on the oscilloscope was the same as that obtained with the actual signal.
the signal from the actual sample of water produced a voltage of ,1 milli-
volt at the grid of the first stage of the preampliiler rather than the
used is for" a long cylLndrical sample which did not in fact exist.
si-Tial redaction can be caused
3.
Water sample
This was enclosed in a glass Jar that was fitted inside the receiving
The
1620
err,
Preamplifier
This devi'ie was placed near the transmitting and receiving coil.
It
v/as
ments and
3-t-
shown belowo
31
6-f
Jh-
'to\^
w
7*
C (lyyt^l
Fisrure 1'',
Preanplifier,,
Thus,
th'^
stages.
narrov-/
constructed.
The Q multiplier circuit consists of a cathode follower that has a
32
(i^'
yo^ Z.0
4AI<6'
1
7.
rAC"x
1}
zr
^7^K.
-L_.
ccipi/f
z'lco
.oH
orj
6BK,
'^
Figure 18o
Q multiplier circuit
33
io-?.,
Therefore,
by-
keeping the feedback also just sli.^htly less than one, the feedback can
be kept below a critical value that
i^rould
The
its 0.
_,
cycle
'.vith
resistor Rf all in
This
The rise
of
si.J^nal
supplied by
generator).
-A-as
The
found to be 57.
"-^ve
The second
to impressing a
Ki
There
a measurable rise
wouU
be expected.
frequency dial of
jn
34
Figure 19.
Photoc^raphs showing result of impressing a sine wave an a high Q circuit. (Continued on next page)
35
Firare
I'^o
This
next section.
B-K
Fl^mro
'?0o
6o
CSatin?;
2182 cycles.
The H.^o 524A rec^ired ,85 volts of input signal to trigger the first
squarinf^ and amplifying stages.
,85 volts would
positive rectangular pulses (shaped signal pulses) of about 30 volts amnlitude at oin one of the decade divider socket.
This decade divider then
supplies output pulses to pin 2 of tha same socket that are l/lO the frequency of the incoming
si^^i^ij.
.
<,
tive rectangular pulses into pin 1 were inverted and utiliiied to trigger
a binary'' gating counter.
provide
cuit was to reduce the last count error to a val.j9 equivalent to approxirrately
r,
change in the
eari:,h's
The schematic diagram of the binary circuit is shov*i on the next two
pages.
The binary scaling circuit consisted of 13 stages ^/^ich would actually
xs
37
N.
^
^
cm^
-_i
I
Figure 21
38
CD
>0
-.\.A
Fip;ur 22o
39
It was important that the counting not commence until 100 milli-
cf f
to be utilized.
The delay-
opposite side of the slowly rotatirg wheel from the polarizing coil micro-
switch o
cot
Figure 23,
Timing wheel,
AD
that it dropped into the notch 135 milliseconds after microswitch #1,
switch caused a relay to open and close that was connected to the reset of
the binary gating counter.
s^^
in draw-
When microswitch #2
was out of the notch, the 50000 ohm resistor was placed in series with
the grid resistor in one stage of each of the pairs of bistable circuits in the binary gating counter.
of the stages which had 50000 ohm introduced to become the "on" tube of
its pair.
52/A
counter limited
This out-
its output to 20 volts regardless of input signal amplitude. put when fed to the binary gating counter out of pin 1 of the
"Decade
Divider Socket" was not sufficient to trigger ths binary gating counter
provided s^ was open with the 50000 ohm in the grid lead of every other
stage.
tiire
that
microswitch #2 dropped into the notch did not start an erroneous count
When microswitch #2 dropped into the notch closing 35 and bypassing
the reset resistor, the binary gating counter was ready to receive input
signal pulses.
output pulse which would open the gate on the 100 Kc and start a count
on the HoP. 52/fA counting stages.
first output pulse would occur only after 4096 input sigial pulses and
additional pulses would follow spaced 4096 cycles of the input sigial frequency apart.
In order to cause the first input signal pulse to produce
41
introduced into the opposite stage of each pair than it would have been
normally.
count and /+O96 cycles later the count was stopped by the next pulseo
In order to determine tbs
ment, a Hewlett Packard low frequency standard of 1000 cycles was counted
for 8 seconds. The results showed the device to be accurate within the
is
Analoging circuit
For the data collected the precession frequency was counted and the
answer indicated on the lighted dials of the H.Po 524A counter.
For
scane
To this circuit
can be fed the same 100 Kc freouency that is counted by the HoPo 52AA
is
cycles occurring during a 2 second count will be about 200000 and the
actual number of cycles will differ from this sli^tly depending on the
exact frequency of precession.
counter capable
of
large number of times and when the 100 Kc is gated off will stop counting.
The count indicated at this time on the binary will detennine some refer-
ence numbero
42
six stages
43
CHAPTER V
aXPSRIMSNTAL RESULTS
Data were collect-^d far a plot
:^
magnetic field.
In general during the day data were collected for ten min(A total of 40 pieces of information was collected
c
Several
minutes when the indicated change in the earth's field was only
-j
"
Data taken starting at 0029 shows a drift in the earth's field of 3 Ifduring a ten minute period with a clear "trend" apparent in the data.
same type of trend is evident at other points in the datao
This
Data collected
between 0750 and 0820 is believed to have superimposed on the normal change
an effect
d'je
to th? arrival on the Varian parking lot of ab^ut 200 autoData were collected continuously and a total
It is also noted in the data that
at the end of the 24 hour cycle the readings indicated a return to the start-
An additional piece of information on equipment sensitivity was obtained by moving a 3 foot length iron pipe
feet distant
5
44
v'
-.
1.
TiAPT?:R VI
CONCLUSIONS
1,
Possible "Errors:
It is believed that changes in the earth's field of t
i
can be
c on fi.juration
The limitation is
imposed by the fact that the count is for only 2 seconds and the base
should be detectable.
Accuracy of course
creating the base
oscillator
frequency but with crystal controlled oscillators errors from this source
should be less than one part per million
o
source of error but with initial S/N ratios of 20 or 30/l, this is not a
problan unless long counts are attempted.
Accuracy with
field was achieved
^ T for
signal wave crosses the axis affects the accuracy of the count slightly.
2.
The orien-
tation of the coils need not be exact and the precession frequency is not
not operate as a rate of change instrument and does not require motion.
something
46
It could
47
APPKJiDIX
I
r
<t-
v<:-*)
Ot4
^OOAL SA5S
- P
J-.
i-
((,^Jl-)^,-^
T(s)
/5 ^.
^ ^-(3
>*
(^f ^)
48
-.-
X o)
<i
(
{.
(i
^)
c<>
cr
-f^^r/o^-0^
(r
ru)
c:
("s
^^J
t-
(';$'-
ps
i-
<l
-j:
is)
^
I.
t
-h
S^
( T
^?
'i
4~
'
^
/f
5
X-
+
<
i-^-^
/f
Zl
-SA
Ui^^)^^/^']L--'^''h')
U9
^4^ ^ ^ A j^
.-
- i
f^T ,- ^-^>
50
(^
--
(V
U^
(^ f
/
-
.> )(^ ^
i-jis)
0-i
u^
yy.^
N 'j y)
^;;>a-<<
/-^7^ /-i)"
(0
/.^-)
<'-v-^;^;^
(-
^-^>
("
f ^J) g
o.)
>^>
(-M-^)^i-s)"i-r^)
'Y)t
Ll-LM
r>0^'^^'^
-(*)
(( -^1-JY \-^)--h/S^)
U^O
51
r<^l<
/to'ic^
/"A
/^ecL i
pc.^-^
o(.
on e
ii
ku)
'
f-
Vii)
1^
(-
^o
s^>)
f
<^
e
><
V^ (- ^ f J
j^X-
^i
^^iif)
tVJ ^
f^/i
^ <.
(i_^')-)c-^' .;
;
52
^ei
-
(^i ^-.frf^)
i.11-
S<^
/
ilf
(JJ^r
fl-
C Ta H
/S
^^i
I
53
J.
M
-
o^
.-
(A-
^00
ci^ci
f^^^J
l/^< ^
T
o oo
^
-
Vo
K.
/-
>.?
^1'^
/^
/^r( K
f'
^0
ct
2.
t
j/.f)
I.
I
^
o
>
fv
^x-
^ ^0
54
"
-^
1/
3^^o
i:i.sL
-i* e-^
i"
f)-
>..!k'4x/oJ.to.g
1o
5$
>
-
5r4
r^
zi
OJ
\h)
3I
^^ -
|,
3>i^
jLfO
^0CaJ
^^
J J
t/
H^
- ^
l^*!*^
oUS
V<^
hei
^^ A^/W^^
(5
.i^i
--^
,H
'tscco^\dS
56
APPENDIX II
a/
r o -
l.o
,^-^4,7
57
APPENDIX III
1
2
3
819208
819208
819208
k
5
819208
819208
819209
6 7
819209
819209 819209
8
9
10
11
12
13
14
15
81Q209 819208
16
17
819208
819209
18
19
819209 819209
20
58
APPENDIX IV
3 I^iRCH
172B-38
1820-28
187710.6
187747 08
1933-43
2030-38
2129-39
2229-39
187754 08
18776lo7
187713c
187711cl
187712
2331-a
0029-39
0123-33
187708 08
187705 o
0215-25
0315-25
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BIBIJOGR/iPHY
1.
2.
Bloc'r,
Fo
V/.'V.
Physical Revisw 70
Physical Review 20
kSO
(1946)
474
(1946)
3.
Hay 1951
Simplified Q MulUoliftr P
130
Uo
Measurements of low magnetic fields using paramagnetic resonance Report prepared fcr University of California Rad lab P.O. #H-246$6 April 6, 1951
Magnetic Observdtor>' Manual UoSo Departrrert of Commerce Special PublicaUon 283 1952
1945
Method of nuclear induction 'thesis 3tanford
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