Inversion of Sucrose 3rd Cycle

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Dr. Anbananthan / Mr. J P Tungare

Mr. Shete Abhijit Ashok
10.07.2009
Inversion of sucrose studies with IER technology. (3rd Cycle)
Objectives : Inversion of sucrose to glucose and fructose by using ion exchange resins.
Operating parameters :
Resin
Cation INDION 525
Anion INDION 860
Resin volume
300 mL
300 mL
Bed depth
820 mm
820 mm
Regeneration level
100 g/L
100 g/L
Regenerant volume
600 mL
600 mL
Regeneration time
45 5 min
45 5 min
Displacement by
MB water
MB water
Displacement volume
300 mL (To achieve pH 2)
600 mL
Rinse (Sweetening on)
2 BV 25.2 Brix sucrose solution at 2 BV/h flow rate
Initial pH
3.27
8.62
Initial Conductivity (s)
153.4
18.02
Service flow rate
2 BV/h
Results :
1) Collection of dilution solution before achieving initial brix at anion outlet
Volume
(mL)
Brix
Cation INDION 525

pH
Conductivity
Anion INDION 860

Brix
pH
Conductivity
100
55.0
3.08
86.3
25.0
8.69
24.3
200
56.4
2.92
77.2
25.4
8.57
15.9
300
58.0
3.05
72.2
30.0
8.00
5.41
400
58.0
2.88
68.9
33.4
7.18
1.39
500
58.4
2.80
62.5
53.0
6.75
0.61
600
58.4
2.92
60.8
56.0
6.68
0.39
700
59.0
2.95
64.4
57.0
6.52
0.31
800
58.2
3.00
64.0
58.0
6.43
0.29
Total Inlet sucrose solution:

1) Feed = 12.8 L of 58 Brix
2) Sweetening on = 1200 mL of 25.2 Brix
2) Service run after achieving initial brix at anion outlet
Volume
(BV)
Brix
Cation INDION 525

pH
Conductivity
Anion INDION 860

Brix
pH
Conductivity
59.4
3.03
63.7
59.4
6.48
0.22
60.0
2.94
59.3
59.2
6.13
0.26
60.0
2.94
62.3
60.0
6.06
0.24
59.0
2.84
64.1
58.8
5.95
0.23
59.0
2.89
64.9
60.0
5.86
0.25
59.0
2.86
61.4
59.2
5.31
0.21
59.6
3.04
61.4
59.2
5.32
0.21
59.6
3.13
52.1
59.6
5.47
0.20
59.4
2.84
63.2
59.0
5.50
0.23
10
59.0
2.88
62.1
59.4
5.43
0.25
11
59.0
2.83
62.1
59.8
5.46
0.23
12
59.0
2.85
63.8
59.0
5.33
0.25
13
58.8
2.88
64.5
59.4
5.48
0.26
14
59.0
2.88
65.9
59.2
5.50
0.25
15
59.8
2.80
62.0
59.2
5.20
0.26
16
59.0
2.91
63.8
60.0
5.44
0.20
17
58.4
2.94
65.0
59.0
5.50
0.24
18
59.0
2.84
64.7
60.0
5.43
0.24
19
58.8
2.89
64.9
59.0
5.42
0.24
20
59.4
2.88
62.2
60.0
5.14
0.26
21
58.0
2.78
68.6
59.6
5.16
0.28
22
59.8
2.69
64.8
59.8
5.45
0.26
23
58.8
2.75
64.9
59.4
5.26
0.23
24
59.4
2.67
60.9
59.6
5.21
0.26
25
58.6
2.71
65.3
59.8
5.22
0.25
26
58.8
2.75
66.0
60.0
4.78
0.25
27
58.2
2.76
67.9
59.8
5.28
0.25
28
59.5
2.56
65.7
60.2
5.16
0.33
29
59.2
2.77
66.7
60.2
5.16
0.26
30
59.2
2.73
65.8
60.6
5.15
0.26
Volume (BV)
Cation INDION 525
Anion INDION 860
31
59.2
2.76
64.5
60.6
5.15
0.26
32
58.8
2.52
70.2
60.8
5.17
0.28
33
59.8
2.76
64.4
59.4
5.41
0.23
34
60.8
2.82
54.7
60.2
5.40
0.30
35
60.0
2.94
50.6
61.0
5.26
0.27
36
59.8
3.03
47.8
60.2
5.30
0.29
37
59.6
2.98
42.8
60.0
5.36
0.25
38
59.5
2.96
41.9
59.5
5.56
0.29
39
60.0
3.06
37.0
60.0
5.11
0.25
40
59.5
2.94
36.6
60.0
5.12
0.22
41
59.5
3.07
32.7
60.5
5.26
0.29
42
59.0
3.31
32.9
60.0
5.34
0.22

Inversion of Sucrose 3rd Cycle

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Inversion of Sucrose 3rd Cycle

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To

Dr. Anbananthan / Mr. J P Tungare

Cation INDION 525

Anion INDION 860

300 mL (To achieve pH 2)

Rinse (Sweetening on)

2 BV 25.2 Brix sucrose solution at 2 BV/h flow rate

Initial Conductivity (s)

Service flow rate

Cation INDION 525

Anion INDION 860

Total Inlet sucrose solution:

2) Service run after achieving initial brix at anion outlet

Cation INDION 525

Anion INDION 860

Cation INDION 525

Anion INDION 860

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