Universidad Autnoma de Nuevo Len

Facultad de Ciencias Qumicas

Ingeniera Qumica

Laboratorio de Fisicoqumica II
Entrega: 18 de febrero del 2013

Prctica # 1 Equilibrio Lquido Slido

Diagrama Eutctico Simple

Sexto semestre

Daniella Nolasco Lpez

1569764

Grupo 3

Luis Carlos Flores Luna

1447626

Dra. Alcione Garca Gonzlez

Edith Priscila Muiz Cant

1487731

Equipo 1

Alan Enrique Jasso Ros

1486010

Ciudad Universitaria, San Nicols de los Garza.

Prctica # 1 Equilibrio Lquido Slido

Diagrama Eutctico Simple

OBJETIVO
Determinar prcticamente y con precisin el diagrama de equilibrio de fases lquido slido de una
mezcla binaria, mediante el mtodo de anlisis trmico.

DIAGRAMA DE FLUJO
Preparar 11 muestras de A y B de la siguiente manera:

A (g) 2.0 1.8 1.6 1.4 1.2 1 0.8 0.6 0.4 0.2 0
B (g) 0 0.2 0.4 0.6 0.8 1 1.2 1.4 1.6 1.8 2.0
Pese el vidrio de reloj y registre dicha masa.

Registre la cantidad exacta que pes.

Vaciar cada muestra en un tubo de ensayo de 13x 100 mm.

Pese el vidrio de reloj con la muestra que no logr transferir al tubo de ensayo.

Calentar en bao de agua hasta aproximadamente 96 C .

Colocar el tubo de ensayo en otro cuyo dimetro es de 35x 220 mm.

Pasar la muestra al sistema de enfriamiento.

Tomar lecturas de temperatura y tiempo, cada 15 segundos, hasta que la temperatura sea igual a 20C y sea
constante por lo menos durante 15 lecturas

Manejar los datos experimentales

FIN

DATOS EXPERIMENTALES
A: Difenilamina
B: Naftaleno
Peso vidrio de reloj (Mo): 38.456 g
Pesos Registrados en gramos
Muestra

A (g)

B (g)

A+B

Muestra + Vidrio de reloj (M1)

Residuos (MR)

1
2
3
4
5
6
7
8
9
10
11

2.0054
1.8019
1.5967
1.4052
1.2038
1.0186
0.7912
0.6063
0.4116
0.3177
0

0
0.2018
0.4071
0.6014
0.8014
1.0001
1.2118
1.4026
1.6012
1.8005
2.0066

2.0054
2.0037
2.0038
2.0066
2.0052
2.0187
2.003
2.0089
2.0128
2.1182
2.0066

40.4614
40.4597
40.4598
40.4626
40.4612
40.4747
40.459
40.4649
40.4688
40.5742
40.4626

0.0714
0.0507
0.0558
0.0696
0.0462
0.0587
0.089
0.0829
0.0758
0.0642
0.0546

Enfriamiento
Tinicial en todas las muestras es 96C
Muestra 1
MUESTRA 1
Tiempo
(s)

Temp.
(C)

Tiempo
(s)

Temp.
(C)

Tiempo
(s)

Temp.
(C)

Tiempo
(s)

Temp.
(C)

15
30
45
60
75
90
105
120
135

68
65
63
60
58
55
54
53
52

150
165
180
195
210
225
240
255
270

51
50
50
50
49
49
48
47
46

285
300
315
330
345
360
375
390
405

45
44
42
41
40
38
36
33
32

420
435
450
465
480
495
510
525
540

30
29
28
26
25
23
22
20
19

Muestra 2
MUESTRA 2
Tiempo
(s)

Temp.
(C)

Tiempo
(s)

Temp.
(C)

Tiempo
(s)

Temp.
(C)

Tiempo
(s)

Temp.
(C)

Tiempo
(s)

Temp.
(C)

15
30
45
60
75
90
105
120
135

40
39.1
38.8
38.5
37.2
36.6
36
35.5
34.8

150
165
180
195
210
225
240
255
270

34.3
33.5
33
32.5
31.9
31.2
30.7
30
29.3

285
300
315
330
345
360
375
390
405

29
28.5
28
27.6
27.3
27.1
27.1
26.9
26.6

420
435
450
465
480
495
510
525
540

26.5
26.3
26
25.5
25.2
24.8
24.5
24.1
23.8

555
570
585
600
615
630
645
660
675

23.2
22.8
22.1
21.6
21
20.5
20
20
19

Muestra 3
MUESTRA 3
Tiempo
(s)
15
30
45
60
75
90
105
120
135
150
165
180
195
210
225
240
255
270

Temp.
(C)
90
88
85
82
79
76.1
73
70.3
67.6
65.4
62.9
60.6
58.5
56.4
54.2
52.2
50.8
49.1

Tiempo
(s)
285
300
315
330
345
360
375
390
405
420
435
450
465
480
495
510
525
540

Temp.
(C)
47.5
45.8
44.4
43.1
41.5
40.4
39.5
38.8
38.4
37.9
37.5
37.4
37.2
37
36.6
35.5
34.6
34

Tiempo
(s)
555
570
585
600
615
630
645
660
675
690
705
720
735
750
765
780
795
810

Temp.
(C)
33.4
32.8
32.3
31.9
31.3
30.9
30.5
30.2
30
30
29.9
29.9
29.8
29.6
29.5
29.2
29
28.5

Tiempo
(s)
825
840
855
870
885
900
915
930
945
960
975
990
1005
1020
1035

Temp.
(C)
28.1
27.7
27.4
26.6
26.3
25.6
25
24.2
23.4
21.8
22.6
21.1
20.5
20
20

A partir de las siguientes muestras, slo se calent el tubo de ensayo pequeo 13mm x 100mm.
Muestra 4
MUESTRA 4
Tiempo
(s)
15
30
45
60
75
90
105
120
135
150
165
180
195
210
225
240
255
270

Temp.
(C)
90
81
79
76.2
73.6
70.2
66.8
65.5
62.8
60.6
58.6
56.5
54.6
52.5
50.5
49
47.3
45.7

Tiempo
(s)
285
300
315
330
345
360
375
390
405
420
435
450
465
480
495
510
525
540

Temp.
(C)
44.3
42.8
41.2
40
38.7
37.5
36.5
35.2
34
33
32.5
31.5
30.7
30.2
29.9
29.6
29.5
29.5

Tiempo
(s)
555
570
585
600
615
630
645
660
675
690
705
720
735
750
765
780
795
810

Temp.
(C)
29.5
29.4
30.5
30.5
30.5
30.57
31.2
31.1
31
31
30.9
30.7
30.6
30.5
30.5
30.3
28.3
27.5

Tiempo
(s)
825
840
855
870
885
900
915
930
945
960
975
990
1005
1020
1035

Temp.
(C)
27.1
26.7
26.5
26.2
25.8
25.3
24.6
23.6
22.5
22.1
21.4
20.7
20.3
20
20

Temp.
(C)
31.1
30.7
30.3
30
29.8
29.5
29.2
29
28.9
28.8

Tiempo
(s)
615
630
645
660
675
690
705
720
735
750

Temp.
(C)
28.4
27.6
27.5
27.1
27
26.6
26.1
25.6
25.2
24.5

Muestra 5
MUESTRA 5
Tiempo
(s)
15
30
45
60
75
90
105
120
135
150

Temp.
(C)
90
86
79
75
71
67.8
64.5
61.7
59.1
56.6

Tiempo
(s)
165
180
195
210
225
240
255
270
285
300

Temp.
(C)
54
53.4
50.4
48.4
46.3
44.6
43.2
41.8
40.6
39.6

Tiempo
(s)
315
330
345
360
375
390
405
420
435
450

Temp.
(C)
38.5
37.8
37
36
35.1
33.8
33.5
32.8
32.3
31.7

Tiempo
(s)
465
480
495
510
525
540
555
570
585
600

Tiempo
(s)
765
780
795
810
825
840
855
870
885

Temp.
(C)
24
23.6
23.2
22.6
22
21.4
21
20.3
20

Muestra 6
MUESTRA 6
Tiempo
(s)
15
30
45
60
75
90
105
120
135
150

Temp.
(C)
91
82
79
76.3
74
72.3
68.7
64.5
63.8
60.4

Tiempo
(s)
165
180
195
210
225
240
255
270
285
300

Temp.
(C)
55
53
52.3
51
50.4
47.7
46.2
44.5
43
41.7

Tiempo
(s)
315
330
345
360
375
390
405
420
435
450

Temp.
(C)
46.2
44.5
43
41.7
40.7
39.2
37.7
36.9
36
35.5

Tiempo
(s)
465
480
495
510
525
540
555
570
585
600

Temp.
(C)
34.8
34.3
33.8
33.2
32.5
31.9
31.2
21
30.6
30.4

Tiempo
(s)
615
630
645
660
675
690
705
720
735
750

Temp.
(C)
30.3
30
29.5
28.6
28.6
27.2
26.8
26.3
26
25.4

Tiempo
(s)
765
780
795
810
825
840
855

Temp.
(C)
25
24.3
23.5
22.5
21.8
20.6
20.1

Temp.
(C)
38.3
37.2
36.5
35.2
34.2
32.4
31.2
30
29.3
28.7

Tiempo
(s)
615
630
645
660
675
690
705
720
735
750

Temp.
(C)
28.6
28.5
28.5
28.5
28.3
28
28.4
27
26.5
26

Tiempo
(s)
765
780
795
810
825
840
855
870
885

Temp.
(C)
25.5
24.7
24
23.5
22.6
22
21.6
20
20

Muestra 7
MUESTRA 7
Tiempo
(s)
15
30
45
60
75
90
105
120
135
150

Temp.
(C)
80
77.2
74.5
72
69
66.5
64.7
63.3
62
61.2

Tiempo
(s)
165
180
195
210
225
240
255
270
285
300

Temp.
(C)
60.7
60
59
58.3
57.2
56.5
54.4
54
52.8
51.2

Tiempo
(s)
315
330
345
360
375
390
405
420
435
450

Temp.
(C)
49.7
48.3
47.1
46
44
43.2
42.1
41.9
40.4
39.4

Tiempo
(s)
465
480
495
510
525
540
555
570
585
600

A partir de las siguientes muestras, el tiempo se tom cada 5 segundos y hasta que llegara a
temperatura ambiente.
Muestra 8
MUESTRA 8
Tiempo
(s)

Temp.
(C)

Tiempo
(s)

Temp.
(C)

Tiempo
(s)

Temp.
(C)

Tiempo
(s)

Temp.
(C)

Tiempo
(s)

Temp.
(C)

Tiempo
(s)

Temp.
(C)

Tiempo
(s)

Temp.
(C)

5
10
15
20
25
30
35
40
45
50
55
60
65
70
75
80
85
90
95
100
105
110
115
120
125
130
135
140
145
150
155
160
165
170
175
180

94.5
91
88.4
86
84
82.7
81
79.8
78.5
77.5
76.3
75.1
74.2
73
72
71.2
70
69.1
68
67.5
66.5
65.5
64.5
64
63
62.2
61.5
61
60.3
59.5
59
58.2
57.9
57
56.6
55.7

185
190
195
200
205
210
215
220
225
230
235
240
245
250
255
260
265
270
275
280
285
290
295
300
305
310
315
320
325
330
335
340
345
350
355
360

54.5
54.5
54.3
54
53.7
53.5
53.4
53.3
53.1
52.9
52.5
52.4
52.3
52.5
52.4
52.3
51.5
51.4
51.2
50.8
50.5
50.2
49.9
49.5
49.2
48.9
48.7
48.4
48
47.5
47.3
47
46.7
46.4
46
45.7

365
370
375
380
385
390
395
400
405
410
415
420
425
430
435
440
445
450
455
460
465
470
475
480
485
490
495
500
505
510
515
520
525
530
535
540

45.4
45.1
44.8
44.5
44.3
44
43.7
43.5
42
41.8
41.6
41.4
42
41.5
41.1
41
40.6
40.4
40.1
39.9
39.5
39.4
39
38.9
38.6
38.4
38.2
38
37.9
37.6
37.4
37
37
36.4
36.5
36.2

545
550
555
560
565
570
575
580
585
590
595
600
605
610
615
620
625
630
635
640
645
650
655
660
665
670
675
680
685
690
695
700
705
710
715
720

36
35.9
35.7
35.5
35.4
35.1
34.9
34.8
34.5
34.4
34.1
34
33.8
33.6
33.5
33.4
33.1
33
32.8
32.6
32.5
32.4
32.2
32
32
31.8
31.6
31.5
31.5
31.4
31.2
31
31
30.9
30.6
30.5

725
730
735
740
745
750
755
760
765
770
775
780
785
790
795
800
805
810
815
820
825
830
835
840
845
850
855
860
865
870
875
880
885
890
895
900

30.4
30.4
30.2
30.1
30.1
30
30
29.9
29.9
29.8
29.8
29.8
29.7
29.5
29.5
29.5
29.4
29.4
29.4
29.4
29.4
29.3
29.3
29.3
29.3
29.3
29.4
29.4
29.4
29.5
29.5
29.5
29.6
29.6
29.6
29.7

905
910
915
920
925
930
935
940
945
950
955
960
965
970
975
980
985
990
995
1000
1005
1010
1015
1020
1025
1030
1035
1040
1045
1050
1055
1060
1065
1070
1075
1080

29.7
29.7
29.7
29.7
29.8
29.9
29.9
30
30
30
30
30
30
30
30
30
30
30.1
30.1
30.1
30.1
30
30
30
30
29.9
29.9
29.9
29.9
29.9
29.9
29.8
29.8
29.8
29.8
29.8

1085
1090
1095
1100
1105
1110
1115
1120
1125
1130
1135
1140
1145
1150
1155
1160
1165
1170
1175
1180
1185
1190
1195
1200
1205
1210
1215
1220
1225
1230
1235
1240
1245
1250
1255
1260

29.7
29.7
29.7
29.7
29.6
29.6
29.5
29.5
29.5
29.5
29.5
29.4
29.4
29.4
29.4
29.4
29.3
29.3
29.3
29.3
29.2
29.2
29.2
29.2
29.1
29.1
29
29
28.9
28.9
28.9
28.9
28.8
28.7
28.7
28.6

Continan datos de muestra 8

MUESTRA8
Tiempo
(s)

Temp.
(C)

Tiempo
(s)

Temp
(C)

Tiempo
(s)

1265
1270
1275
1280
1285
1290
1295
1300
1305
1310
1315
1320
1325
1330
1335
1340
1345
1350
1355
1360
1365
1370
1375
1380
1385
1390
1395
1400
1405
1410
1415
1420
1425
1430
1435
1440

28.6
28.6
28.4
28.3
28.3
28.3
28.3
28.3
28.3
28.2
28.1
28.1
28
28
28
27.9
27.8
27.7
27.6
27.6
27.5
27.4
27.4
27.3
27.2
27.1
27.1
27
26.9
26.9
26.8
26.8
26.8
26.6
26.6
26.5

1445
1450
1455
1460
1465
1470
1475
1480
1485
1490
1495
1500
1505
1510
1515
1520
1525
1530
1535
1540
1545
1550
1555
1560
1565
1570
1575
1580
1585
1590
1595
1600
1605
1610
1615
1620

26.4
26.4
26.4
26.4
26.3
26.1
26.1
26.1
26
26
26
25.9
25.8
25.8
25.8
25.8
25.7
25.6
25.5
25.5
25.4
25.4
25.4
25.3
25.3
25.1
25
25
25
24.9
24.8
24.8
24.8
24.7
24.6
24.6

1625
1630
1635
1640
1645
1650
1655
1660
1665
1670
1675
1680
1685
1690
1695
1700
1705
1710
1715
1720
1725
1730
1735
1740
1745
1750
1755
1760
1765
1770
1775
1780
1785
1790
1795
1800

Temp. Tiempo
(C)
(s)

24.5
24.5
24.5
24.4
24.4
24.4
24.3
24.3
24.2
24.2
24.2
24.1
24.1
24
24
24
24
24
24
23.9
23.9
23.9
23.8
23.8
23.8
23.8
23.7
23.7
23.7
23.6
23.6
23.6
23.6
23.6
23.5
23.5

1805
1810
1815
1820
1825
1830
1835
1840
1845
1850
1855
1860
1865
1870
1875
1880
1885
1890
1895
1900
1905
1910

Temp.
(C)

23.4
23.4
23.4
23.3
23.3
23.3
23.2
23.2
23.2
23.2
23.2
23.1
23.1
23
23
23
23
23
23
23
23
23

Muestra 9
MUESTRA 9
Tiempo Temp. Tiempo Temp. Tiempo Temp. Tiempo Temp. Tiempo Temp. Tiempo Temp. Tiempo Temp.
(s)
(C)
(s)
(C)
(s)
(C)
(s)
(C)
(s)
(C)
(s)
(C)
(s)
(C)
5
94.2
185
62
365
42
545
32.6
725
29.3
905
27.3
1085
29.3
10
91.3
190
61.3
370
41.6
550
32.5
730
29.3
910
27.3
1090
29.2
15
89.2
195
61
375
41.4
555
32.5
735
29.2
915
27.2
1095
29.2
20
87.1
200
60.5
380
41
560
32.1
740
29.1
920
27.1
1100
29.2
25
86
205
60
385
40.6
565
32
745
29.1
925
27.1
1105
29.2
30
84.6
210
59
390
40.3
570
31.8
750
29
930
27.1
1110
29.2
35
83.1
215
58.5
395
40
575
31.5
755
29
935
27.1
1115
29.2
40
82.5
220
58
400
39.6
580
31.2
760
29
940
27.1
1120
29.2
45
81
225
57.1
405
39
585
31
765
29
945
27.1
1125
29.2
50
80
230
56.5
410
38.5
590
30.6
770
28.8
950
27.5
1130
29.2
55
78.5
235
56
415
38.2
595
30.5
775
28.8
955
27.9
1135
29.2
60
77.5
240
55.2
420
38
600
30.4
780
28.7
960
28.5
1140
29.2
65
76.5
245
55
425
37.6
605
30.3
785
28.5
965
28.6
1145
29
70
74.5
250
54.5
430
37.4
610
30.4
790
28.5
970
28.6
1150
29
75
74
255
54
435
37.2
615
30.7
795
28.5
975
28.6
1155
29
80
73.5
260
53.3
440
37
620
31
800
28.5
980
28.6
1160
29
85
72.5
265
52.5
445
36.7
625
31
805
28.4
985
29
1165
29
90
71.5
270
51.2
450
36.5
630
31
810
28.3
990
29
1170
29
95
70.5
275
50.5
455
36.4
635
30.9
815
28.2
995
29.2
1175
29
100
69.5
280
49
460
35.5
640
30.8
820
28.2
1000
29.4
1180
29
105
69.1
285
48.5
465
35.4
645
30.7
825
28.1
1005
29.3
1185
29
110
68.5
290
48.1
470
35
650
30.7
830
28.1
1010
29.2
1190
29
115
68.1
295
47.5
475
34.6
655
30.5
835
28.1
1015
29.2
1195
29
120
68
300
47.2
480
34.5
660
30.5
840
28.1
1020
29.2
1200
29
125
67.5
305
46.6
485
34.3
665
30.4
845
28.1
1025
29.5
1205
29
130
67.1
310
46.3
490
34.1
670
30.3
850
28.1
1030
29.5
1210
29
135
67
315
46
495
34
675
30.2
855
28.1
1035
29.5
1215
29
140
65
320
45.5
500
33.7
680
30.1
860
28
1040
29.5
145
64.8
325
45
505
33.7
685
30
865
28
1045
29.5
150
64.6
330
44.5
510
33.7
690
29.8
870
28
1050
29.5
155
64.2
335
44.2
515
33.6
695
29.8
875
27.9
1055
29.5
160
64
340
44
520
33.5
700
29.8
880
27.6
1060
29.5
165
63.5
345
43.2
525
33.4
705
29.6
885
27.6
1065
29.5
170
63.1
350
43
530
33.1
710
29.5
890
27.5
1070
29.5
175
62.6
355
42.6
535
33
715
29.4
895
27.5
1075
29.4
180
62.3
360
42.3
540
32.9
720
29.4
900
27.4
1080
29.4

Muestra 10
MUESTRA 10
Tiempo
(s)
5

Temp.
(C)
95

Tiempo
(s)
185

Temp.
(C)
68.1

Tiempo
(s)
365

Temp.
(C)
53

Tiempo
(s)
545

Temp.
(C)
40.2

Tiempo
(s)
725

Temp.
(C)
33

Tiempo
(s)
905

Temp.
(C)
29

Tiempo
(s)
1085

Temp.
(C)
26.9

Tiempo
(s)
1265

Temp.
(C)
25.9

10

92

190

68

370

52.5

550

40

730

32.8

910

29

1090

26.9

1270

25.9

15

88

195

67.5

375

52.1

555

39.7

735

32.5

915

28.9

1095

26.9

1275

25.9

20

85

200

67.2

380

51.6

560

39.5

740

32.5

920

28.8

1100

26.8

1280

25.8

25

83

205

66.7

385

51.4

565

39.3

745

32.3

925

28.6

1105

26.8

1285

25.8

30

81

210

66.5

390

51.50.5

570

39

750

32.1

930

28.5

1110

26.7

1290

25.8

35

79.5

215

66.2

395

50.2

575

38.8

755

32

935

28.5

1115

26.7

1295

25.8

40

78.5

220

66

400

49.6

580

38.6

760

31.8

940

28.4

1120

26.6

1300

25.7

45

77.2

225

65.6

405

49.4

585

38.3

765

31.7

945

28.3

1125

26.6

1305

25.7

50

76

230

65.2

410

49

590

38.1

770

31.6

950

28.3

1130

26.6

1310

25.7

55

74

235

64.7

415

48.5

595

37.9

775

31.5

955

28.2

1135

26.5

1315

25.7

60

74

240

64

420

48.2

600

37.6

780

31.3

960

28.1

1140

26.5

1320

25.7

65

73.8

245

63.4

425

47.6

605

37.5

785

31.2

965

18.1

1145

26.5

1325

25.7

70

73.2

250

72.7

430

47.5

610

37.3

790

31.1

970

18.1

1150

26.5

1330

25.7

75

72.7

255

62.3

435

47.1

615

37

795

31

975

28

1155

26.5

1335

25.7

80

72.5

260

62

440

46.7

620

36.8

800

31

980

28

1160

26.5

1340

25.7

85

72

265

61.5

445

46.7

625

36.6

805

31

985

28

1165

26.4

1345

25.7

90

71.6

270

61

450

46.1

630

36.5

810

30.8

990

27.9

1170

26.4

1350

25.7

95

71.3

275

60.6

455

45.6

635

36.2

815

30.6

995

27.8

1175

26.4

1355

25.7

100

71.1

280

60

460

45.4

640

36

820

30.5

1000

27.8

1180

26.3

1360

25.7

105

71

285

59.6

465

45.1

645

35.8

825

30.5

1005

27.7

1185

26.3

1365

25.7

110

70.6

290

59.2

470

44.7

650

35.5

830

30.4

1010

27.6

1190

26.2

1370

25.7

115

70.5

295

59

475

44.5

655

35.3

835

30.3

1015

27.6

1195

26.2

1375

120

70.4

300

58.5

480

44.3

660

35.3

840

30.2

1020

27.5

1200

26.2

1380

125

70.4

305

58

485

44

665

35

845

30.1

1025

27.5

1205

26.2

1385

130

70.4

310

57.5

490

43.7

670

34.8

850

30

1030

27.4

1210

26.2

1390

135

70.4

315

57.1

495

43.2

675

34.6

855

29.8

1035

27.4

1215

26.1

1395

140

70.2

320

56.7

500

43

680

34.5

860

29.6

1040

27.3

1220

26.1

1400

145

70

325

56.3

505

42.5

685

34.3

865

29.6

1045

27.3

1225

26.1

1405

150

69.6

330

55.6

510

42.3

690

34.2

870

29.6

1050

27.2

1230

26.1

1410

155

69.5

335

55.5

515

42

695

34

875

29.5

1055

27.2

1235

26

1415

160

69.2

340

55

520

41.5

700

33.8

880

29.5

1060

27.2

1240

26

1420

165

69

345

54.6

525

41.2

705

33.8

885

29.4

1065

27.1

1245

26

1425

170

68.7

350

54.2

530

41

710

33.4

890

29.3

1070

27

1250

26

1430

175

68.6

355

53.7

535

40.7

715

33.2

895

29.2

1075

27

1255

26

1435

180

68.4

360

53.5

540

40.5

720

33.1

900

29.1

1080

27

1260

26

1440

Muestra 11
MUESTRA 11
Tiempo Temp. Tiempo
(s)
(C)
(s)
5
84
185
10
82.5
190
15
81.5
195
20
80
200
25
79.5
205
30
78.3
210
35
78.1
215
40
77.8
220
45
77.6
225
50
77.5
230
55
77.3
235
60
77.1
240
65
76.6
245
70
76.5
250
75
76.3
255
80
76.1
260
85
76
265
90
75.8
270
95
75.6
275
100
75.5
280
105
75.3
285
110
75.1
290
115
75
295
120
74.8
300
125
74.7
305
130
74.5
310
135
74.4
315
140
74.2
320
145
74
325
150
73.9
330
155
73.6
335
160
73.4
340
165
72.7
345
170
72.5
350
175
72.2
355
180
71.9
360

Temp.
(C)
70.9
70.3
69.9
69.5
69
68.6
68.1
67.4
66.8
66.3
65.6
65.2
64.6
64.3
63.7
63.2
62.8
62.4
61.9
61.3
60.6
60.2
60
59.6
59.2
58.9
58.5
58.1
57.6
57.2
56.9
56.6
56.3
56
55.6
55.4

Tiempo Temp. Tiempo Temp. Tiempo Temp. Tiempo Temp. Tiempo Temp.
(s)
(C)
(s)
(C)
(s)
(C)
(s)
(C)
(s)
(C)
365
55
545
45.1
725
39
905
35
1085
32.1
370
54.8
550
45
730
38.9
910
34.9
1090
32
375
54.5
555
44.7
735
38.7
915
34.8
1095
31.9
380
54.2
560
44.5
740
38.6
920
34.6
1100
31.9
385
53.9
565
44.4
745
38.5
925
34.5
1105
31.8
390
53.5
570
44.2
750
38.4
930
34.5
1110
31.8
395
53.3
575
44
755
38.3
935
34.4
1115
31.7
400
53.1
580
43.8
760
38.2
940
34.3
1120
31.6
405
52.8
585
43.6
765
38
945
34.2
1125
31.5
410
52.5
590
43.5
770
37.9
950
34.1
1130
31.5
415
52.2
595
43.3
775
37.8
955
34
1135
31.4
420
52
600
43.1
780
37.6
960
34
1140
31.3
425
51.7
605
42.9
785
37.6
965
33.9
1145
31.3
430
51.5
610
42.6
790
37.5
970
33.9
1150
31.2
435
51
615
42.5
795
37.4
975
33.7
1155
31.1
440
50.7
620
42.3
800
37.2
980
33.6
1160
31.1
445
50.4
625
42.1
805
37.1
985
33.6
1165
31
450
50.2
630
41.8
810
37
990
33.5
1170
31
455
50
635
41.6
815
37
995
33.4
1175
31
460
49.6
640
41.5
820
36.9
1000
33.4
1180
30.9
465
49.4
645
41.4
825
36.6
1005
33.2
1185
30.8
470
49.2
650
41.2
830
36.6
1010
33.1
1190
30.7
475
49
655
41
835
36.6
1015
33.1
1195
30.7
480
48.8
660
40.9
840
36.4
1020
33
1200
30.6
485
48.6
665
40.7
845
36.2
1025
32.9
1205
30.6
490
48.4
670
40.5
850
36
1030
32.8
1210
30.5
495
48.2
675
40.4
855
35.9
1035
32.6
1215
30.5
500
48
680
40.2
860
35.8
1040
32.6
1220
30.4
505
47.7
685
40
865
35.7
1045
32.6
1225
30.4
510
47.5
690
39.9
870
35.6
1050
32.5
1230
30.4
515
47.3
695
39.8
875
35.5
1055
32.5
1235
30.3
520
47.1
700
30.7
880
35.5
1060
32.5
1240
30.3
525
45.9
705
39.5
885
35.4
1065
32.4
1245
30.2
530
45.6
710
39.4
890
35.3
1070
32.3
1250
30.2
535
45.5
715
39.4
895
35.2
1075
32.2
1255
30.1
540
45.2
720
39.2
900
35.1
1080
32.2
1260
30.1

Continuacin datos de muestra 11

MUESTRA 11
Tiempo
(s)
1265
1270
1275
1280
1285
1290
1295
1300
1305
1310
1315
1320
1325
1330
1335
1340
1345
1350
1355
1360
1365
1370
1375
1380

Temp.
(C)
30
30
30
29.9
29.9
29.8
29.7
29.7
29.6
29.6
29.5
29.5
29.4
29.4
29.4
29.4
29.4
29.3
29.3
29.2
29.2
29.1
29
29

Tiempo
(s)
1385
1390
1395
1400
1405
1410
1415
1420
1425
1430
1435
1440
1445
1450
1455
1460
1465
1470
1475
1480
1485
1490
1495
1500

Temp.
(C)
28.9
28.9
28.8
28.8
28.7
27.7
27.7
28.7
28.6
28.6
28.6
28.6
28.6
28.5
28.5
28.5
28.4
28.4
28.4
28.3
28.3
28.3
28.3
28.3

Tiempo
(s)
1505
1510
1515
1520
1525
1530
1535
1540
1545
1550
1555
1560
1565
1570
1575
1580
1585
1590
1595
1600
1605
1610
1615
1620

Temp.
(C)
28.2
28.2
28.2
28.1
28.1
28.1
28.1
28
28
28
28
28
28
28
27.9
27.8
27.8
27.7
27.7
27.7
27.6
27.6
27.6
27.6

Tiempo
(s)
1625
1630
1635
1640
1645
1650
1655
1660
1665
1670
1675
1680
1685
1690
1695
1700
1705
1710
1715
1720
1725
1730
1735
1740

Temp.
(C)
27.6
27.6
27.6
27.6
27.6
27.6
27.5
27.5
27.4
27.4
27.3
27.3
27.3
27.3
27.3
27.3
27.3
27.3
27.3
27.3
27.3
27.3
27.3
27.3

BIBLIOGRAFA

Manual de laboratorio de Fisicoqumica II, 1 Edicin, Mxico 2012, pag.7-12.