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Draft for Public Comment

Form 36 Version 6.1

DPC: 03/105152 DC
Head Office 389 Chiswick High Road London W4 4AL Telephone: +44(0)20 8996 9000 Fax: +44(0)20 8996 7001

Date: 28 March 2003 Origin: European

Latest date for receipt of comments: 2003.06.30


Responsible committee: Interested committees: PVE/15 Storage Tanks For The Petroleum Industry

Project no.: 2000/01081

Title:

Draft British Standard BS prEN 14620-5:2003 Design and manufacture of site built, vertical, cylindrical, flat- bottomed steel tanks for the storage of refrigerated, liquefied gases with operating temperatures between -5C and -165C Part 5: Testing, drying, purging and cool-down

Supersession information: If you are aware of a current national standard which may be affected, please notify the secretary (contact details below).

WARNING: THIS IS A DRAFT AND MUST NOT BE REGARDED OR USED AS A BRITISH STANDARD. THIS DRAFT IS NOT CURRENT BEYOND 2003.06.30. This draft is issued to allow comments from interested parties; all comments will be given consideration prior to publication. No acknowledgement will normally be sent. See overleaf for information on commenting. No copying is allowed, in any form, without prior written permission from BSI except as permitted under the Copyright, Designs and Patent Act 1988 or for circulation within a nominating organization for briefing purposes. Electronic circulation is limited to dissemination by e-mail within such an organization by committee members. Further copies of this draft may be purchased from BSI Customer Services, Tel: +44(0) 20 8996 9001 or email orders@bsi-global.com. British, International and foreign standards are also available from BSI Customer Services. British Standards on CD or Online are available from British Standards Publishing Sales Limited. Tel: 01344 404409 or email bsonline@techindex.co.uk. Information on the co-operating organizations represented on the committees referenced above may be obtained from the responsible committee secretary. Cross-references The British Standards which implement International or European publications referred to in this draft may be found via the British Standards Online Service on the BSI web site http://www.bsi-global.com.

Responsible Committee Secretary: Mr J E P Mortimer (BSI)

Direct tel: E-mail:

020 8996 7129 peter.mortimer@bsi-global.com

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Introduction This draft standard is based on European discussions in which the UK took an active part. Your comments on this draft are welcome and will assist in the preparation of the consequent British Standard. If no comments are received to the contrary, then the UK will approve this draft and implement it as a British Standard. Comment is particularly welcome on national, legislative or similar deviations that may be necessary. Even if this draft standard is not approved by the UK, if it receives the necessary support in Europe, the UK will be obliged to publish the official English Language text unchanged as a British Standard and to withdraw any conflicting standard. UK Vote Please indicate whether you consider the UK should submit a negative (with reasons) or positive vote on this draft. Submission The guidance given below is intended to ensure that all comments receive efficient and appropriate attention by the responsible BSI committee. Annotated drafts are not acceptable and will be rejected. All comments must be submitted, preferably electronically, to the Responsible Committee Secretary at the address given on the front cover. Comments should be compatible with Version 6.0 or Version 97 of Microsoft Word for Windows, if possible; otherwise comments in ASCII text format are acceptable. Any comments not submitted electronically should still adhere to these format requirements. All comments submitted should be presented as given in the example below. Further information on submitting comments and how to obtain a blank electronic version of a comment form are available from the BSI web site at: http://www.bsi-global.com/Standards+Development/Drafts/index.xalter
Date Document

National Committee

Clause/ subclause

Paragraph/ Figure/ Table

Type of comment (General/ technical/editorial) Editorial

COMMENTS

Proposed change

OBSERVATIONS OF THE SECRETARIAT

3.1

1st definition

Definition is ambiguous and needs clarifying.

Amend to read ... so that the mains connector to which no connection ...

6.4

Technical

The use of the UV Delete reference to UV photometer as an photometer. alternative cannot be supported as serious problems have been encountered in its use in the UK.

Microsoft and MS-DOS are registered trademarks, and Windows is a trademark of Microsoft Corporation.

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EUROPEAN STANDARD NORME EUROPENNE EUROPISCHE NORM


ICS

DRAFT prEN 14620-5

March 2003

English version

Design and manufacture of site built, vertical, cylindrical, flatbottomed steel tanks for the storage of refrigerated, liquefied gases with operating temperatures between -5C and -165C Part 5: Testing, drying, purging and cool-down
Conception et fabrication de rservoirs en acier fond plat, verticaux, cylindriques, construits sur site, destins au stockage des gaz rfrigrs, liqufis, dont les tempratures de service sont comprises entre - 5C et 165C - Partie 5: Essais, schage, inertage et mise en froid

This draft European Standard is submitted to CEN members for enquiry. It has been drawn up by the Technical Committee CEN/TC 265. If this draft becomes a European Standard, CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. This draft European Standard was established by CEN in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the Management Centre has the same status as the official versions. CEN members are the national standards bodies of Austria, Belgium, Czech Republic, Denmark, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Luxembourg, Malta, Netherlands, Norway, Portugal, Slovakia, Spain, Sweden, Switzerland and United Kingdom. Warning : This document is not a European Standard. It is distributed for review and comments. It is subject to change without notice and shall not be referred to as a European Standard.

EUROPEAN COMMITTEE FOR STANDARDIZATION COMIT EUROPEN DE NORMALISATION EUROPISCHES KOMITEE FR NORMUNG

Management Centre: rue de Stassart, 36

B-1050 Brussels

2003 CEN

All rights of exploitation in any form and by any means reserved worldwide for CEN national Members.

Ref. No. prEN 14620-5:2003 E

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prEN 14620-5:2003 (E)

Contents
Foreword ............................................................................................................................................................. 3 1 2 3 4 4.1 4.2 5 5.1 5.2 5.3
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Scope...................................................................................................................................................... 4 Normative references............................................................................................................................ 4 Terms and definitions ........................................................................................................................... 4 Hydrostatic and pneumatic testing ..................................................................................................... 4 Hydrostatic test ..................................................................................................................................... 4 Pneumatic test....................................................................................................................................... 7 Drying, purging and cool-down ........................................................................................................... 8 Drying ..................................................................................................................................................... 8 Purging ................................................................................................................................................... 9 Cool-down.............................................................................................................................................. 9

Annex A (informative) Cool-down of the tank................................................................................................ 10 Bibliography ..................................................................................................................................................... 11

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prEN 14620-5:2003 (E)

Foreword
This document (prEN 14620-5:2003) has been prepared by Technical Committee CEN/TC 265 "Site built metallic tanks for the storage of liquids", the secretariat of which is held by BSI. This document is currently submitted to the CEN Enquiry. This European Standard EN 14620 consists of the following parts: Part 1: General; Part 2: Metallic components; Part 3: Concrete components; Part 4: Insulation components; Part 5: Testing, drying, purging and cool-down.

The Annex A of this European Standard is informative

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prEN 14620-5:2003 (E)

Scope

This Part of EN 14620 specifies the requirements for testing, drying, purging and cool-down of the refrigerated liquefied gas storage tanks.

Normative references

This European Standard incorporates by dated or undated reference, provisions from other publications. These normative references are cited at the appropriate places in the text and the publications are listed hereafter. For dated references, subsequent amendments to or revisions of any of these publications apply to this European Standard only when incorporated in it by amendment or revision. For undated references the latest edition of the publication referred to applies. prEN 14620-1:2002 Specification for the design, construction and installation of site built, vertical, cylindrical, flat-bottomed steel tanks for the storage of refrigerated, liquefied gases with operating temperatures between 5 C and 165 C Part 1: General.

Terms and definitions

For the purposes of this part of this European Standard, the definitions given in prEN 14620-1 apply.

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4.1

Hydrostatic and pneumatic testing


Hydrostatic test
General

4.1.1

A hydrostatic test shall be carried out. The hydrostatic test shall demonstrate that: the tank is designed and constructed to contain the product (leakage test is not applicable for membrane tanks. The ammonia test shall be used to ensure membrane tightness); the foundation is able to support the tank contents. Test requirements for each type of tank

4.1.2

For the various tank types, the hydrostatic test shall be carried out in accordance with Table 1.

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prEN 14620-5:2003 (E)

Table 1 Hydrostatic test requirements Contents Single containment Tank (type II-III steels): Ammonia, butane, propane,
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Double containment Inner tank (type I-II steels): FH Outer tank (type I-II steels): FH Outer tank (pre-stressed conc): No test

Full containment Inner tank (type I-II steels): FH Outer tank (type I-II steels): FH Outer tank (pre-stressed conc): No test Inner tank (type IV steel): PH Outer tank steel (type IV steel): PH Outer tank (pre-stressed conc): No test

Membrane tank

FH

and propylene

Outer tank (pre-stressed conc): PH (see Note 2)

Tank (type IV steel): PH Ethane, ethylene LNG

Inner tank (type IV steel): PH Outer tank steel (type IV steel): PH Outer tank (pre-stressed conc): No test

Outer tank (pre-stressed conc): PH (see Note 2)

NOTE 1

FH means Full height hydrostatic test PH means Partial height hydrostatic test

NOTE 2 In the case of a membrane tank, the membrane cannot be hydrostatically tested. To ensure that the foundation is able to support the tank contents and the tank integrity is ensured, the concrete outer tank shall be hydrostatically tested before the insulation and membrane are installed. NOTE 3 Hydrostatic testing of the pre-stressed concrete outer tank is not required, see prEN 14620-3:2002, A.2.

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prEN 14620-5:2003 (E)

4.1.3

Additional requirements

The following additional requirements shall apply: for a full height hydrostatic test, the inner tank shall be filled to the maximum design liquid level. The same quantity of water shall be used for testing of the outer tank; for a partial height hydrostatic test of the inner tank, the test level shall be equal to 1.25 times the height of the maximum design liquid level multiplied by the density of the specified product to be stored. The same quantity of water contained shall be used for testing of the outer tank; the test level of a membrane tank shall be based on the partial hydrostatic test requirement indicated above; the hydrostatic test shall not be carried out until all welded accessories to the shell and the bottom of the tank are in place. Welding shall not be allowed after completion of the hydrostatic test; the contractor shall ensure that the quality of the water is such that no damage to the steel/concrete can occur. Conditions of implementation

4.1.4

Before the start of the test, the tank shall be cleaned. Any spatter and slag shall be removed from the welds, and all materials, objects or temporary installations used during its construction, shall also be removed. A pressure relief system shall be installed for the test of sufficient capacity in order that the internal positive and negative test pressures do not exceed those specified in the design. A water column gauge shall also be used to measure the pressure.
NOTE A corrosion inhibitor may be required.

4.1.5 4.1.5.1

Examination during filling Peripheral level check

Before filling, the following markers shall be installed on the outer surface of the tank: four markers for tanks with a diameter 10 m ; eight markers for tanks with a larger diameter.

Markers shall also be installed on the inner tank shell, in double and full containment tank systems, so that settlement of the inner tank can be monitored simultaneously with that of the outer tank. The markers shall be of such a type that they remain visible/usable after the tank is painted. The settlement of the tank shall be monitored during the filling and emptying of the tank. As a minimum, this shall be done when the tank is half full, a three-quarters full and full.

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prEN 14620-5:2003 (E)

4.1.5.2

Bottom surface level check

For tanks, where bottom differential settlements of more than 30 mm can be expected (e.g. tanks with raft foundation), provisions shall be provided so that the settlements in the centre of the tank can be monitored.
NOTE An inclinometer may be used.

4.1.6

Filling

The rate of filling shall be determined based on water/equipment availability and subsoil conditions. The full water load shall be maintained for at least 24 hours. During the test, a visual inspection of the shell welds for possible leakage shall be carried out. The anchors, if present, shall be adjusted. During the work, the observed settlements shall be compared with the predicted values. If differences occur, the geotechnical expert, involved in the foundation design, shall be consulted (see prEN 14620-1:2002, 7.1.10) and the purchaser shall be informed.

4.2
4.2.1

Pneumatic test
Pressure test

A pressure test shall be carried out at a test pressure equal to 1.25 times the design pressure of the tank.
Note: The test pressure shall be applied to the vapour space above the test water, except that in the case of a double wall tank with open-top inner tank, the inner tank may be completely or partially emptied of water before the pressure test.

The following actions shall be considered : --``,,```,``````,,,`,`,`,,`,,`,-`-`,,`,,`,`,,`---

pressure relief valves shall be installed, which shall have been adjusted to open at the test pressure, or provide a temporary pressure relief system to prevent the pressure exceeding the test pressure. The test pressure, when reached, shall be held for at least 30 minutes. Thereafter the test pressure shall be reduced to the design pressure; a soap solution test of all welded joints above the test water level shall be performed;
NOTE1 If the joint has previously been vacuum box tested, the soap solution test may be substituted by visual inspection.

Repairs shall not be made while the tank is under pressure;


NOTE 2 Repairs may be made later and vacuum box tested.

pressure shall be reduced and pressure relief valves shall be adjusted to open at the design pressure. The set pressure of the pressure relief valve shall be verified by pumping air into the vapour space.

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prEN 14620-5:2003 (E)

4.2.2

Negative pressure test

A negative pressure test shall be carried out at a pressure equal to the design internal negative pressure of the tank.
NOTE 1 A minimum holding time is not required. The test may be terminated as soon as the design internal negative pressure has been reached. NOTE 2 The negative pressure test should be carried out while there is still water in the tank. This will prevent possible uplift of the bottom and the thermal protection system (TPS).

The following actions shall be considered: vacuum relief valves shall be installed, which shall have been adjusted to open at the negative test pressure, or provide a temporary vacuum relief system to prevent the negative pressure exceeding negative test pressure; all openings shall be closed except those of the vacuum relief valves. The required negative pressure may be obtained by lowering the water level or by the use of an air-ejector; negative pressure shall be reduced and the vacuum relief valves shall be adjusted to open at the specified set pressure. The set pressure of the vacuum relief valve shall be verified by withdrawing water or using an air-ejector. Empty checks

4.2.3

After the tank has been emptied of water and is at atmospheric pressure, the following actions shall be considered: the anchorage, if provided, shall be re-checked for tightness against the hold-down brackets; air pressure, equal to the design pressure, shall be applied to the empty tank, and the anchorage, if provided, and the foundation shall be checked for uplift; the bottom shall be checked for abnormalities and all bottom welds shall be vacuum box tested; when bottom connections are fitted, all welds shall be inspected by 100% visual inspection and 100% dye penetrant or magnetic particle examination; when all the tests have been concluded, the tank shall be cleaned and dried.

5
5.1

Drying, purging and cool-down


Drying

In general, the tank contents shall be dried to a maximum dew point of 20 C.


NOTE When the annular space is filled with perlite powder, then a maximum dew point of 10 C can be tolerated for the annular space.

For the bottom insulation space(s) no requirements apply.

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prEN 14620-5:2003 (E)

5.2

Purging

The tank shall be purged before hydrocarbons are introduced. An inert gas shall be used.
NOTE In general, nitrogen is used.

Purging shall be carried out until the following oxygen concentrations are reached: 5 % for LPG tanks; 8 % for Ethylene tanks; 9.5 % for LNG tanks.

For the bottom insulation space(s) no requirement shall apply. At critical points, sample points shall be provided so that it can be demonstrated that the required purging is carried out.
NOTE 1 For full containment tanks, purging should be carried out from the inner tank to the annular space so that inward pressure on the inner tank is prevented. NOTE 2 The presence of an inert gas, e.g. nitrogen, during cool-down may result in sub-cooling of the steel below its design temperature e.g. butane tank to 45 C, propane tank to 70 C and LNG tank to 180 C. It is strongly recommended that this possible sub-cooling is prevented by the replacement of the nitrogen by warm product vapours prior to cool-down.

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5.3

Cool-down

Cool-down of the primary container shall be carried out in a controlled manner to prevent major temperature differences occurring during the cool-down. The temperature of the inner tank/membrane steel shall be monitored and be kept in a tolerable range.
NOTE For more details, see Annex A.

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prEN 14620-5:2003 (E)

Annex A (informative) Cool-down of the tank

Cool-down is usually carried out with liquefied gas. Cool-down procedure and the facilities should be designed carefully because it should prevent great temperature differences being generated in the steel plate, thus causing high stresses. These temperature stresses, in combination with mechanical stresses caused by bending, welding etc., may become so high that cracking will take place. This cannot be detected during the cool-down and leakage may be the result. The best option is to design a ring main at the top of the tank and to install spray nozzles on the ring main. On the wall of the tank and on the tank bottom skin thermocouples can be installed for temperature monitoring. This arrangement should be sized for the cool-down rate specified. For inner tanks, the following cool-down rates are typical: a target cool-down rate for the inner tank of 3 C/hr with a maximum of 5 C/hr; a maximum temperature difference between any two adjacent shell or bottom thermocouples of 30 C.

For membrane tanks the following cool-down rates are typical: a target cool-down rate for the membrane of 10 C/hr with a maximum of 15 C/hr; a maximum temperature difference between any two adjacent wall or bottom thermocouples of 50 C.

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Bibliography

prEN 14620-3:2002, Specification for the design, construction, and installation of site built, vertical, cylindrical, flat-bottomed steel tanks for the storage of refrigerated, liquefied gases with operating temperatures between 5 C and 165 C Part 3: Concrete components.

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