Reference Manual: Alcolyzer Plus Beer

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Reference Manual
Alcolyzer Plus Beer
Beer Analyzing System
Firmware Version: V5.02.09

Reference Manual
Alcolyzer Plus Beer
Beer Analyzing System
Firmware Version: V5.02.09

Anton Paar GmbH assumes no liability for technical or printing errors or omissions in this document.
Nor is any liability assumed for damages resulting from information contained in the document.
Anton Paar GmbH reserves the right to content changes. This also extends to changes to delivery
volumes or any features of delivered parts.
All rights reserved (including translation). This document, or any part of it, may not be reproduced,
changed, copied, or distributed by means of electronic systems in any form (print, photocopy, microfilm
or any other process) without prior written permission by Anton Paar GmbH.
Trademarks, registered trademarks, trade names, etc. may be used in this manual without being marked
as such. They are the property of their respective owner.
Published by Anton Paar
Printed: Anton Paar, Austria
Copyright 2009 Anton Paar GmbH, Graz, Austria
Address: Anton Paar GmbH
Anton-Paar-Str. 20
A-8054 Graz / Austria Europe
Tel: +43 316 257-0
Fax: +43 316 257-257
E-Mail: info@anton-paar.com
Web: www.anton-paar.com
Date: 06.03.2009
Document number C27IB02M.fm
C27IB02 5
Contents
1 About the Reference Manual .......................................................................................................... 9
2 Safety Instructions........................................................................................................................... 9
2.1 General Safety Instructions ..................................................................................................... 9
3 About Alcolyzer Plus Beer............................................................................................................ 11
4 Testing the Supplied Parts............................................................................................................ 11
5 Putting into Operation................................................................................................................... 14
5.1 Installing the Instruments....................................................................................................... 14
5.2 Mounting the pH Electrode .................................................................................................... 16
5.2.1 Preparing and Mounting the pH Electrode "Hamilton Polilyte Lab" ........................ 16
5.2.2 Preparing and Mounting the pH Electrode "Orion model 91-63" ............................ 17
5.3 Mounting the Hoses without Option pH/Color........................................................................ 19
5.4 Mounting the Hoses with Option pH/Color............................................................................. 20
5.5 Completing the Installation .................................................................................................... 21
5.6 Connecting a Printer or PC.................................................................................................... 24
5.6.1 Connecting Alcolyzer Plus Beer to a Printer .......................................................... 24
5.6.2 Connecting Alcolyzer Plus Beer to a PC................................................................ 24
6 Functional Components................................................................................................................ 25
6.1 Display and Keypad............................................................................................................... 25
6.1.1 Display in the Measuring Mode.............................................................................. 25
6.1.2 Soft Keys in the Measuring Mode .......................................................................... 27
6.2 Rear View.............................................................................................................................. 28
7 General Instrument Settings......................................................................................................... 29
7.1 Setting the Display Contrast .................................................................................................. 29
7.2 Setting Date and Time........................................................................................................... 29
7.3 Configuring the Measuring System........................................................................................ 29
7.3.1 Setting the General Parameters............................................................................. 29
7.3.2 Defining the Peripheral Devices............................................................................. 30
7.3.3 Defining the Interface Settings ............................................................................... 30
7.4 Setting a Custom Function .................................................................................................... 30
7.4.1 Setting a User-Defined Ethanol Table (in %V/V) .................................................... 30
7.4.2 Setting a User-Defined Color Unit .......................................................................... 31
7.5 Selecting the Output Data...................................................................................................... 32
7.5.1 Selecting the Output Data for the Display .............................................................. 33
7.5.2 Selecting the Output Data for the Printer ............................................................... 33
7.5.3 Selecting the Output Data for the Data Memory..................................................... 33
7.6 Settings for the Sample Changer........................................................................................... 33
8 Setting the Measuring Methods.................................................................................................... 34
8.1 Description of the Measuring Methods .................................................................................. 34
8.2 Editing a Measuring Method.................................................................................................. 35
6 C27IB02
8.2.1 Editing a Predefined Method.................................................................................. 35
8.2.2 Editing a New Method ............................................................................................ 35
8.3 Selecting the Measuring Method ........................................................................................... 37
9 SOP (Standard Operating Procedure).......................................................................................... 38
10 Checking the Adjustment Validity................................................................................................ 41
10.1 Checking Procedure without Option pH/Color ....................................................................... 41
10.1.1 Performing a Checking Procedure with Water (0%V/V) ......................................... 41
10.1.2 Performing a Checking Procedure with a Water/Ethanol Solution of Known
Concentration ........................................................................................................................ 43
10.2 Checking Procedure with Option pH/Color ............................................................................ 44
10.2.1 Checking Procedure for the Measuring Parameter "alcohol" ................................. 44
10.2.2 Checking Procedure for the Measuring Parameter "pH"........................................ 44
10.2.3 Checking Procedure for the Measuring Parameter "color"..................................... 45
11 Adjusting the Instrument .............................................................................................................. 45
11.1 Adjustment without Option pH/Color...................................................................................... 45
11.1.1 Adjustment with Water (Zero Point)........................................................................ 46
11.1.2 Adjustment with a Water/Ethanol Solution of Known Alcohol Concentration ......... 48
11.2 Adjustment with Option pH/Color........................................................................................... 49
11.2.1 Adjustment Alcohol................................................................................................. 49
11.2.2 Adjustment Color.................................................................................................... 49
11.2.2.1 Adjustment with Water (Zero) ................................................................. 49
11.2.2.2 Adjustment with a Color Standard (Tartrazine) of Known Concentration 51
11.2.3 Adjustment pH........................................................................................................ 52
11.2.3.1 Automatic ................................................................................................ 53
11.2.3.2 Manual .................................................................................................... 54
11.2.3.3 Edit Buffer Data....................................................................................... 55
11.2.3.4 Sort Buffer Data ...................................................................................... 56
11.3 Density Adjustment................................................................................................................ 56
12 Measurement.................................................................................................................................. 58
12.1 Identifying the Sample and Assigning the Method................................................................. 59
12.1.1 Types of Sample Identification ............................................................................... 59
12.1.2 Sample Identification for "text + number" and "text"............................................... 60
12.1.3 Sample Identification for "list" and "# + list"............................................................ 60
12.1.3.1 Entering a Sample List ............................................................................ 60
12.1.3.2 Editing the Sample List during Operation................................................ 62
12.1.3.3 Deleting a Sample List ............................................................................ 62
12.2 Performing a Measurement without Option pH/Color ............................................................ 63
12.3 Performing a Measurement with Option pH/Color ................................................................. 64
12.4 Correcting Calculated Analysis Results................................................................................. 64
13 Data Memory .................................................................................................................................. 66
14 Cleaning Routines ......................................................................................................................... 67
14.1 Cleaning the Measuring Cells without Option pH/Color......................................................... 67
C27IB02 7
14.1.1 Between Series of Measurements on the Same Day............................................. 67
14.1.2 At the End of the Day ............................................................................................. 67
14.1.3 Once a Week.......................................................................................................... 68
14.2 Cleaning the Measuring Cells with Option pH/Color.............................................................. 69
14.2.1 Storing the pH Electrode ........................................................................................ 69
14.2.2 Between Series of Measurements on the Same Day............................................. 70
14.2.3 At the End of the Day ............................................................................................. 70
14.2.4 Once a Week.......................................................................................................... 71
14.3 Cleaning after Wort Measurements ....................................................................................... 72
14.4 Maintaining the pH Electrode................................................................................................. 72
14.4.1 Maintaining the Hamilton pH Electrode.................................................................. 72
14.4.2 Maintaining the Orion pH Electrode ....................................................................... 73
15 Menu Operation and Description ................................................................................................. 74
15.1 Menu Operation..................................................................................................................... 74
15.1.1 Operating the Soft Keys on the Instrument ............................................................ 74
15.1.2 Using an External PC Keyboard............................................................................. 75
15.1.3 Using a Bar Code Reader ...................................................................................... 75
15.2 Menu Description and Function............................................................................................. 76
15.2.1 "adjustment" ........................................................................................................... 76
15.2.1.1 "adjust alcohol"........................................................................................ 76
15.2.1.2 "adjust pH" .............................................................................................. 77
15.2.1.3 "adjust color" ........................................................................................... 77
15.2.2 "instrument settings"............................................................................................... 78
15.2.3 "method settings" ................................................................................................... 82
15.2.4 "user functions" ...................................................................................................... 83
15.2.5 "data memory" ........................................................................................................ 83
15.2.6 "utilities".................................................................................................................. 84
15.2.7 "parameter calculator" ............................................................................................ 90
15.2.8 "service mode" ....................................................................................................... 91
15.2.9 "auto sampler settings"........................................................................................... 91
15.3 Entering and Changing a Password ...................................................................................... 91
15.4 Installing a New Firmware Version ........................................................................................ 92
16 Calculations.................................................................................................................................... 93
17 Filling Samples with the SF-1 Sample Filling Unit...................................................................... 97
Appendix A: Degassing Beer Samples.......................................................................................... 98
Appendix B: Available Parameters ................................................................................................ 99
B.1 Method Parameters............................................................................................. 99
B.2 Printer Protocol Parameters.............................................................................. 101
Appendix C: Status and Error Messages .................................................................................... 102
C.1 Status/Error Messages for the Alcohol Measurement ....................................... 102
C.2 Status/Error Messages for the Color Measurement .......................................... 103
C.3 Status/Error Messages for the pH Measurement .............................................. 103
8 C27IB02
C.4 System Error Messages.................................................................................... 104
C.5 Other Messages................................................................................................ 104
Appendix D: Technical Data ......................................................................................................... 105
Appendix E: Interface Commands for Communication PC and Alcolyzer Plus Beer ............. 106
Appendix F: Configuration for Communication between DMA and Alcolyzer Plus Beer ...... 108
Appendix G: Firmware Versions .................................................................................................. 110
Appendix H: Wetted Parts............................................................................................................. 112
Appendix I: Material Safety Data Sheet for Tartrazine.............................................................. 113
Appendix J: Density/Concentration Table for Binary Aqueous Ethanol Solutions................ 115
Appendix K: Menu Tree................................................................................................................. 126
Index................................................................................................................................................... 128
1 About the Reference Manual
C27IB02 9
1 About the Reference Manual
This reference manual informs you about the installation and the safe handling
and use of the instrument. Make sure that the reference manual is easily
accessible to all personnel involved with the instrument. Pay special attention to
the safety instructions and warnings in the manual and on the instrument.
Symbols in this reference manual
This reference manual features the following symbols:
2 Safety Instructions
Read the reference manual at hand before using Alcolyzer Plus Beer.
Follow all hints and instructions contained in this reference manual to ensure
the correct use and safe functioning of Alcolyzer Plus Beer.
2.1 General Safety Instructions
Liability
The reference manual at hand does not claim to address all safety issues
associated with the use of the instrument and samples. It is your
responsibility to establish health and safety practices and determine the
applicability of regulatory limitations.
Anton Paar GmbH only warrants the proper functioning of Alcolyzer Plus
Beer if no adjustments have been made to the mechanics, electronics, and
firmware.
Only use Alcolyzer Plus Beer for the purpose described in this reference
manual. Anton Paar GmbH is not liable for damages caused by incorrect use
of Alcolyzer Plus Beer.
Caution:
This symbol calls attention to the risk of instrument damage or
measurement errors. Do not proceed until the indicated conditions for
averting this threat are fully understood and met.
Information:
This symbol calls attention to any additional information of use to the
operator.
2 Safety Instructions
10 C27IB02
Installation and use
Alcolyzer Plus Beer is not an explosion-proof instrument and therefore must
not be operated in areas with risk of explosion.
The installation procedure shall only be carried out by authorized personnel
who are familiar with the installation instructions.
Do not use any accessories or wearing parts other than those supplied or
approved by Anton Paar GmbH.
Make sure all operators are trained to use the instrument safely and correctly
before starting any applicable operations.
In case of damage or malfunction, do not continue operating Alcolyzer Plus
Beer. Do not operate the instrument under conditions which could result in
damage to goods and/or injuries and loss of life.
Check Alcolyzer Plus Beer for chemical resistance to the samples and
cleaning agents.
Maintenance and service
The results delivered by Alcolyzer Plus Beer not only depend on the correct
function of the instrument, but also on various other factors. We therefore
recommend to have the results checked (e.g. plausibility tested) by skilled
personnel before consequential actions are taken based on the results.
Service and repair procedures may only be carried out by authorized
personnel or by Anton Paar GmbH.
Disposal
Concerning the disposal of Alcolyzer Plus Beer, observe the legal
requirements in your country.
Precautions for highly flammable samples and cleaning agents
Observe and adhere to your national safety regulations for handling the
measured samples (e.g. use of safety goggles, gloves, respiratory protection
etc.).
Only store the minimum required amount of sample, cleaning agents and
other inflammable materials near the Alcolyzer Plus Beer.
Do not spill sample/cleaning agents or leave their containers uncovered.
Immediately remove spilled sample/cleaning agents.
Make sure that the setup location is sufficiently ventilated. The environment
of Alcolyzer Plus Beer must be kept free of inflammable gases and vapors.
3 About Alcolyzer Plus Beer
C27IB02 11
Connect Alcolyzer Plus Beer to the mains via a safety switch located at a
safe distance from the instrument. In an emergency, turn off the power using
this switch instead of the power switch on Alcolyzer Plus Beer.
Supply a fire extinction unit.
Ensure the sufficient supervision of Alcolyzer Plus Beer during operation.
3 About Alcolyzer Plus Beer
Alcolyzer Plus Beer is based on a highly accurate and patented NIR
spectrometer, which measures the alcohol content of beer in the concentration
range of 0 - 12%V/V.
Optionally, Alcolyzer Plus Beer can also be equipped with a color measurement
device and a pH measurement device. The color value (EBC or ASBC value) is
determined by the measurement of light absorption. For the pH measurement, an
electrode Hamilton (Polilyte Lab) or a measuring cell Orion (model 91-63) is used.
In combination with an Anton Paar density meter DMA 4500/5000 and a sample
changer SP-1m, the automatic determination of relevant beer parameters can be
achieved.
4 Testing the Supplied Parts
Alcolyzer Plus Beer was tested and packed carefully before shipment. However,
damage may occur during transport.
1. Keep the packaging material (box, foam piece, transport protection) for
possible returns and further questions from the transport and insurance
company.
2. Check the delivery for completion by comparing the supplied parts to those
noted in Table 4.1.
3. If a part is missing, contact your Anton Paar representative.
4. If a part is damaged, contact the transport company and your Anton Paar
representative.
12 C27IB02
Table 4.1: Supplied Parts
Symbol Pcs. Item/Spare Part Mat. No.
1 Alcolyzer Plus Beer (without option pH/color)
or
Alcolyzer Plus Beer
with option color + pH Hamilton or
with option color + pH Orion
8921
8921
9918
12167
1 Instruction manual
English or
German
including a CD with the reference manual
12665
12666
1 Power cable
USA:
UK:
Europe:
52656
61865
65146
1 Accessory kit 9860
2m Hose 3 x 5 silicone / 1m
Hose 1.6 x 3.2 Tygon / 1m
50814
67540
5 Syringe 5 mL / 1pc. 63130
2 Filling nozzle Luer Alcolyzer Plus / 1pc. 7046
2 Adapter Luer " UNF / 1pc. 64792
2 Male Luer plug / 1pc. 63865
C27IB02 13
3 Adapter Luer cone / 1pc. 63863
2 Filling nozzle fitting Alcolyzer Plus / 1pc. 10759
2 Filling nozzle UNF " Alcolyzer Plus / 1pc. 10758
2 Tube d=2.1, D=2.4, L=20 1.4571 / 1pc. 67982
1 Needle (only delivered with SF-1) / 1pc. 67394
3m Hose 2 x 4 silicone /1m
(only delivered with SF-1)
51273
1 Cable male 9 Pin / male 9 Pin / 1pc. 2359
1
(option)
Backup Card DMA 4500/5000 Alcolyzer for
firmware versions DMA V4.xxx or higher;
Alcolyzer V5.xx / 1pc.
23913
1 Waste vessel 500 mL 6210
1 Option color + pH Hamilton 9918
1 Electrode Hamilton pH = 0-14 0-80 9466
1 Option color + pH Orion 12167
1 Electrode Orion model 91-63 12555
5 Putting into Operation
14 C27IB02
5.1 Installing the Instruments
1. Put SP-1m into operation as described in the SP-1m instruction manual.
2. Connect the power cord of SP-1m to a power terminal with ground
connection.
3. Place the density meter on SP-1m.
4. Connect the connecting power cable (SP-1m accessory, Mat. No. 66178) to
the power outlet of SP-1m and the power outlet of the DMA.
5. Mount the filling nozzle fittings as described in the SP-1m instruction manual.
6. Place Alcolyzer Plus Beer on top of the density meter.
7. Connect the power cord of Alcolyzer Plus Beer to a power terminal with
ground connection.
Delivered with both
options color + pH
1 Connection cable type K1 BNC 1m 62521
1 Buffer solution pH=4.01 Hamilton (500 mL) 12554
1 Buffer solution pH=7.00 Hamilton (500 mL) 12556
1 pH storage solution 500 mL Hamilton 12632
1 Color adjustment set
Color standard approx. 50 EBC 2x50 mL
Ultra pure water 0.0 EBC 3x50 mL
12627
Information:
Alcolyzer Plus Beer does not require any special installation conditions.
Conditions in the installation area should be those in a typical laboratory.
To guarantee temperature stability, do not place Alcolyzer Plus Beer
- near a heater
- near an air conditioner
- in direct sunlight.
For air humidity restrictions see Appendix D.
Caution:
To ensure the correct functioning of the built-in ventilator, make sure the
airflow at the bottom and the rear of the instrument is not blocked.
C27IB02 15
8. Screw the filling nozzle fittings Alcolyzer Plus (accessory box) into the
openings of the measuring cell.
9. If the option pH/color is integrated, check that 2# Filling nozzle Luer
Alcolyzer Plus adapters are screwed into the openings of the pH measuring
cell (see Fig. 5 - 1).
Fig. 5 - 1 Mounting the adapters onto the pH measuring cell
10. Connect COM2 at the rear of Alcolyzer Plus Beer to COM1 at the rear of
DMA 4500/5000 using the connection cable (Mat. No. 2359).
11. If a printer is used, connect the printer interface cable to COM1 at the rear of
Alcolyzer Plus Beer.
12. Connect the interface cable of SP-1m to the S-Bus outlet of Alcolyzer Plus
Beer.
Caution:
Screw the adapters into the openings of the measuring cell hand-tight
(without using any tools). Otherwise, the connections between the adapters
and the measuring cell are not leak-tight and liquid may enter the electronics
and affect operation.
Caution:
Before switching on Alcolyzer Plus Beer, check that the given voltage and
frequency (AC100 to 240 V, 50 to 60 Hz) corresponds with the local mains
voltage and mains frequency. If large voltage fluctuations are to be
expected, the use of a constant voltage source (UPS) is recommended.
The non-fused earth conductor of the power cord must be connected to
earth.
16 C27IB02
5.2 Mounting the pH Electrode
5.2.1 Preparing and Mounting the pH Electrode "Hamilton
Polilyte Lab"
Preparing
1. Leave the pH electrode in an upright position for at least one hour.
2. Carefully remove the watering cap.
3. Flush the electrode with distilled water.
4. Check the inside of the electrode for unwanted air bubbles. Shaking the
electrode like a clinical thermometer will cause any bubbles to rise to the top.
Mounting
1. Loosen the protective tube by twisting it counterclockwise (see Fig. 5 - 2).
Fig. 5 - 2 Loosening the protective tube
2. Screw the connecting cable (Mat. No. 62521) to the rear end of the pH
electrode.
3. Connect the other end of the cable to the rear of Alcolyzer Plus Beer (see
Chapter 6.2).
4. Insert the pH electrode into the protective tube carefully until the end of the
electrode touches the bottom of the pH measuring cell.
5. Tighten the protective tube by turning it clockwise.
The pH electrode is fixed.
C27IB02 17
Fig. 5 - 3 pH electrode Hamilton
6. Check that both Filling nozzle Luer Alcolyzer Plus are screwed into the
openings of the pH measuring cell (see Fig. 5 - 1).
5.2.2 Preparing and Mounting the pH Electrode "Orion
model 91-63"
Preparing
1. Remove the protective shipping cap from the sensing element and save for
storage.
2. Clean any salt deposits from the exterior by rinsing with distilled water.
3. Uncover the filling hole and add filling solution to the electrode.
4. Place the pH electrode in the electrode holder and suspend in air for 15
minutes to thoroughly wet the reference junction.
5. Shake the electrode (like a clinical thermometer) to remove air bubbles.
6. Soak the electrode in pH electrode storage solution for one hour.
Information:
To maintain an adequate flow rate, the level of filling solution must always
be above the reference junction.
The filling hole must be open whenever the electrode is in use.
Caution:
Once the junction is wet, do not allow the electrode to dry out.
18 C27IB02
Mounting
1. Screw the connecting cable (Mat. No. 62521) to the rear end of the pH
electrode.
2. Connect the other end of the cable to the rear of Alcolyzer Plus Beer (see
Chapter 6.2).
3. Insert the pH electrode into the pH measuring cell carefully until the end of
the electrode touches the bottom of the pH measuring cell.
Fig. 5 - 4 pH electrode Orion
4. Tighten the knurled nut (see Fig. 5 - 4). The pH electrode is fixed.
5. Check that both Filling nozzle Luer Alcolyzer Plus are screwed into the
openings of the pH measuring cell (see Fig. 5 - 1).
Knurled nut
C27IB02 19
5.3 Mounting the Hoses without Option pH/Color
Fig. 5 - 5 Hose connections without option pH/color
1. Cut a piece of the silicone hose 3 x 5 mm (1) approx. 24 cm in length.
2. Connect one end of the hose to the air pump outlet of the DMA.
3. Connect the Adapter Luer cone to the other end of the hose.
4. Connect a Tygon hose (2) approx. 26 cm in length to the upper end of the
SP-1m needle and to the front adapter of the density meter.
5. Connect a Tygon hose (3) approx. 22 cm in length to the rear adapter of the
density meter and to the lower adapter of Alcolyzer Plus Beer.
6. Connect a Tygon hose (4) approx. 22 cm in length to the upper adapter of
7. Connect the tube, Mat. No. 67982, (5) to the other end of the hose.
8. Connect a silicone hose 2x4 mm (6) to the tube.
9. Lead the silicone hose via the peristaltic pump of SP-1m to a waste vessel.
10. The length of this hose can be selected according to the distance of the
waste vessel.
4 (T)
3 (T)
2 (T)
5 (Tube)
6 (S) to waste
6

1 (S)
(T) .... Tygon
(S) .... Silicone
20 C27IB02
5.4 Mounting the Hoses with Option pH/Color
Fig. 5 - 6 Hose connections with option pH/color
1. Connect an adapter Luer cone (1) to each opening of the pH measuring cell.
2. Cut a piece of the silicone hose 3 x 5 mm (2) approx. 24 cm in length.
3. Connect one end of the hose to the air pump outlet of the DMA.
4. Connect the adapter Luer cone to the other end of the hose.
5. Connect a Tygon hose (3) approx. 26 cm in length to the upper end of the
SP-1m needle and to the front adapter of the density meter.
6. Connect a Tygon hose (4) approx. 22 cm in length to the rear adapter of the
density meter and to the lower adapter of Alcolyzer Plus Beer.
7. Connect a Tygon hose (5) approx. 22 cm in length to the upper adapter of
8. Connect the tube, Mat. No. 67982, (6) to the other end of the hose.
9. Connect a silicone hose 2x4 mm (7) approx. 50 cm in length to the tube.
10. Lead the silicone hose via the peristaltic pump of SP-1m to the front adapter
of the pH measuring cell.
5 (T)
8 (S) to waste
3 (T)
6 Tube
7 (S)
4 (T)
2 (S)
1
(T) .... Tygon
(S) .... Silicone
to air
pump
C27IB02 21
11. Connect a 2x4 mm silicone hose (8) to the rear adapter of the pH measuring
cell.
12. Lead this hose to a waste vessel.
13. Select the length of this hose according to the distance of the waste vessel.
5.5 Completing the Installation
1. Turn on the SP-1m and the density meter and wait for the initialization of
both instruments to be completed.
2. Configure the DMA 4500/5000 according to Appendix F.
3. Turn on Alcolyzer Plus Beer using the power switch at the rear of the
instrument.
4. Select the menu instrument settings > device list and configure the device
list as follows (for details about operating the menu, see Chapter 15.1):
Caution:
Before switching on Alcolyzer Plus Beer, check that the given voltage and
frequency (AC 100 to 240 V, 50 to 60 Hz) corresponds with the local
mains voltage and mains frequency. If large voltage fluctuations are to be
expected, the use of a constant voltage source (UPS) is recommended.
The non-fused earth conductor of the power cord must be connected to
earth.
Information:
Once switched on, Alcolyzer Plus Beer performs a system check and an
attemperating procedure:
After transport, full stabilization of Alcolyzer Plus Beer might take up to
one day.
Usually Alcolyzer Plus Beer is ready for measurement after a start-up
period of one hour.
To guarantee an optimal temperature stability over a long time, always
leave the system switched on.
22 C27IB02
Fig. 5 - 7 Menu: instrument settings/device list
Now Alcolyzer Plus Beer initializes the communication between all
connected peripherals.
The COM2 interface of Alcolyzer Plus Beer is automatically configured
(connected to: PIB, baud rate: 9600, format: 8 bit No) and cannot be
changed unless density is set to not used.
If all devices are detected properly, the following message is displayed:
Fig. 5 - 8 Device check
5. If for a certain peripheral the message "offline" is displayed, check the
interface settings and/or connection of the corresponding connection cable
(see Appendix F).
INSTRUMENT SETTINGS
filling device
density
CO2
O2
SP-1m
device list
:
:
:
:
DMA xxxx series
not used
not used
DEVICE CHECK
filling unit
density
:
:
SP-1m
passed
C27IB02 23
Fig. 5 - 9 Device check failed
To repeat the device check, select device check.
To edit the device list, select change device list.
6. Set the control parameters for SP-1m in the menu auto sampler settings
(see Chapter 15.2.9).
To make sure that the measured sample is fully replaced with the next
sample, we recommend using the control parameter 1100 (100 seconds
filling time, approx. 30 mL sample). For further information, see the SP-1m
instruction manual.
Fig. 5 - 10 Measuring system: Alcolyzer Plus Beer Analyzing System
BUS ERROR
filling unit : offline
device check
20 sec
change device list
24 C27IB02
5.6 Connecting a Printer or PC
5.6.1 Connecting Alcolyzer Plus Beer to a Printer
Connect the printer cable (Mat. No. 64433) to the COM1 on the rear side of
Depending on the printer that you use, you can choose between 4 different printer
types for optimal communication between the connected printer and Alcolyzer
Plus.
Set the COM1 interface to the appropriate printer in the menu instrument
settings > COM1.
5.6.2 Connecting Alcolyzer Plus Beer to a PC
To transfer the measured results to a PC, connect the PC to Alcolyzer Plus Beer.
For further details, see Appendix F.
1. Connect the interface cable DMA-PC (Mat. No. 72979) to the PC and to
COM1 on the rear side of Alcolyzer Plus Beer.
2. If you use the Anton Paar software VisioLab for Alcolyzer, set the COM1
interface to VisioLab in the menu instrument settings > COM1.
3. If you use the Anton Paar software AP-SoftPrint, set the COM1 interface to
AP-SoftPrint in the menu instrument settings > COM1.
Printer type Holding time
after 1 line
End-of-line
character
Remarks
printer_1 800 msec LF CR after 40
characters
printer_2 1500 msec LF
printer_3 800 msec LF
printer_4 10 msec LF+CR
AP-SoftPrint 10 msec LF
6 Functional Components
C27IB02 25
6.1 Display and Keypad
After switching on, Alcolyzer Plus Beer performs a self-test and the initialization.
6.1.1 Display in the Measuring Mode
Fig. 6 - 1 Display after the end of the measurement
A ... Method
The selected method is displayed.
B ... Measuring status of the alcohol measurement
For details, see the reference manual, Appendix B.1.
C ... Time
D ... Sample name
E ... Measuring status of the color measurement
F ... Measuring status of the pH measurement
G ... Measuring status of the density measurement
The current status of the density measurement is displayed.
H ... Display area for measured values
I ... Information about the sample changer
J ... Soft keys
Information:
It may be necessary to adjust the contrast of the display with the black knob
"Display contrast" at the rear of the instrument.
BEER
valid
09:44:21
sample #
valid
valid
valid
SP-1m
%V/V
20 C
Beer3
c 7.4 EBC
pH 4.43
1.00521 g/cm
3
: stopped
A
B
C
D
E
F
G
H
I
J
26 C27IB02
Display of measured values:
The alcohol content is displayed in %V/V (2 trailing digits) at 20C (percent
volume per volume at the indicated temperature). If the measurement is not
finished, "....." is displayed. As long as the measurement is still in progress
("predetermined"), only one trailing digit is displayed. If the measuring result
is lower than -0.50%V/V or higher than 30.00%V/V, "low" or "high" is
displayed.
The color measurement is displayed in EBC or ASBC with one trailing digit
at 20C. If the measurement is not finished, "....." is displayed. As long as the
measurement is still in progress ("predetermined"), no trailing digit is
displayed. If the measuring result is lower than 0.5 EBC (-0.25 ASBC) or
higher than 130.0 EBC (66 ASBC), "low" or "high" is displayed.
The pH value is displayed in pH units (2 trailing digits) at 25C. If the
measurement is not finished, "....." is displayed.
Fig. 6 - 2 Display of further parameters
K ... Display area for calculated values
Selectable, calculated parameters are displayed in this area after pressing
the key (see Chapter 7.5).
BEER
valid
09:44:21
sample #
valid
valid
alcohol
p
Er
Ea
RDF
SP-1m
%V/V
20 C
Beer3
c 7.4 EBC
pH 4.43
3.86 %m/m
11.12 %m/m
3.59 %m/m
1.80 %m/m
68.95 %
: stopped
K
K
C27IB02 27
6.1.2 Soft Keys in the Measuring Mode
Toggle key:
To toggle between displays of measured and
calculated values
To enter the menu (the <Menu> key is
available)
Selects the measuring method.
Selects the main menu for various settings and
configurations. Access to the main menu can be
protected by a password.
Starts printing.
This soft key is only displayed when interface
COM1 or COM2 is configured for a printer in the
menu instrument settings.
Switches the air pump on.
Switches the air pump off.
Starts an automatic measuring process.
If a sample changer SP-1m is connected to
Alcolyzer Plus Beer and activated, the <Start> key
on Alcolyzer Plus Beer is not displayed. Start the
measurement with the <Start> key on the sample
changer.
Starts the next measurement.
To enter the sample identification.
Selects the list for the sample identification.
Confirms the changes.
Enters the SOP menu.
28 C27IB02
6.2 Rear View
Fig. 6 - 3 Rear view
A ... Cable of the pH electrode
B ... pH electrode
C ... "air pump inlet": Connection for a desiccator
D ... "pH / color Module": Connection for the pH electrode
E ... "COM2": Serial interface RS 232 for connecting a density meter or a
printer
F ... "Keyboard" Connection for a keyboard and/or bar code reader
G ... Power inlet
H ... Power switch
I ... "COM1": Serial interface RS 232 for connecting a computer or printer
J ... "S-Bus": Connection for a sample changer
K ... "Display contrast"
L ... Display contrast setting
M ... Cooling fins
A
B
C D E F G
I
J
K L
H
7 General Instrument Settings
C27IB02 29
7.1 Setting the Display Contrast
If necessary, adjust the display contrast with the "Display contrast" knob at the
rear of the instrument (see Chapter 6.2).
7.2 Setting Date and Time
Set date and time in the menu instrument settings > time or date using the soft
keys <>, <> or <>. Press <> to confirm the settings.
7.3 Configuring the Measuring System
1. Press and <Menu> to enter the main menu.
2. Select the menu instruments settings using the soft keys <> and <>.
Confirm with <>.
Fig. 7 - 4 Menu: instrument settings
7.3.1 Setting the General Parameters
Select the menu configuration to set general instrument settings.
Use the soft keys <>, <> and the key to select the parameter.
Press <> to confirm the settings.
Information:
For a detailed description of all setting options, see Chapter 15.2.2.
INSTRUMENT SETTINGS
device list
COM1
COM2
time
date
configuration
30 C27IB02
7.3.2 Defining the Peripheral Devices
Change to the menu instrument settings > device list to select the
connected peripherals like density meter, sample changer SP-1m or filling
device SF-1.
7.3.3 Defining the Interface Settings
Configure the two interfaces COM1 or COM2 for computer or printer in the
menu instrument settings.
7.4 Setting a Custom Function
You can define customized ethanol tables and color units.
7.4.1 Setting a User-Defined Ethanol Table (in %V/V)
If you want to use a different density/ethanol table than the OIML %V/V table, you
can edit a polynomial function (4th order) that calculates an ethanol value based
on your specific density/ethanol table.
Calculating the coefficients
The input value for the polynomial function is the ethanol %V/V value (c)
measured by Alcolyzer Plus Beer. The result of the calculation depends on the
entered coefficients according to the following formula.
Polynomial formula: Output (%V/V) = A0 + A1 x (c [%V/V]) + A2 x (c [%V/V])
2
+
A3 x (c [%V/V])
3
+ A4 x (c [%V/V])
4
The default values are the polynomial coefficients valid for the OIML %V/V table
(see Fig. 7 - 5).
Caution:
You can only use density/ethanol tables based on %V/V.
C27IB02 31
Fig. 7 - 5 Default setting of the polynomial coefficients
1. To calculate the coefficients, take the appropriate table (%V/V) that converts
the measured density into a corresponding ethanol value.
2. By using an appropriate mathematical program, you can calculate the
polynomial coefficients which are based on the table data.
Editing the user-defined ethanol table
1. Select the menu user functions > user defined ethanol table.
2. Enter the 5 polynomial coefficients (A0 to A4) as calculated.
Activating the user-defined ethanol table
1. At Alcolyzer Plus Beer, select the menu instrument settings >
configuration > calc. parameter.
2. Select CU V/V and press the <> key.
7.4.2 Setting a User-Defined Color Unit
If the color measurement according to EBC or ASBC is not desired, you can
define a user-defined color unit. This is done by correcting the EBC value c [EBC]
according to the formula shown in Fig. 7 - 6.
Editing the user-defined color unit
1. To enter the correction factor for the slope of the color measurement and the
offset, select the menu user functions > user defined color unit.
USER FUNCTIONS
user defined ethanol table
A0 : 9.982000e-01
A1 : - 1.520000e-03
A2 : + 1.924620e-05
A3 : - 1.461290e-07
A4 : - 4.574060e-09
+
Caution:
To obtain a correct alcohol adjustment of Alcolyzer Plus Beer, use the same
ethanol table in the DMA that you used for calculating the polynomial
coefficients (see Appendix F).
32 C27IB02
The following window is displayed:
Fig. 7 - 6 Menu: User functions/user defined color unit
2. Enter a slope value between 0 and 7.
Use the <> key to move the cursor.
Edit the highlighted number using the <> and <> keys.
Press <> to confirm the changes.
3. Enter an offset value between -10 and +10.
If not allowed values are entered, the slope is automatically set to 1.0 and
the offset to 00.0 after pressing <>.
Activating the user-defined color unit
1. Select the menu instrument settings > configuration > color unit.
2. Select CU and press the <> key.
7.5 Selecting the Output Data
When you select the parameters for display, printer and memory, you get a list
containing all parameters that are available for the predefined methods BEER,
CIDER, SOFT DRINK, WASH and MOLASSES (see Appendix B.1).
If you then select your appropriate measuring method, you get only the
parameters that are of importance for this very method.
Example: If you select the parameter p (original extract) [%Plato], this parameter
is only available in the methods BEER, WASH and MOLASSES.
USER FUNCTIONS
user defined color unit
c [CU] = .000 * c [EBC] + 00.00 1
C27IB02 33
7.5.1 Selecting the Output Data for the Display
Change to the menu utilities > display configuration.
Select up to 5 parameters using the soft keys <>, <> and the
key.
7.5.2 Selecting the Output Data for the Printer
You can select output data for the printer and save this selection in a printer
protocol. A printer protocol consists of a head and parameters. There are 4
factory-set printer protocols and 6 free printer protocols available.
Factory-set printer protocols:
- Printer protocol No. 6, used with BEER method
- Printer protocol No. 7, used with CIDER method
- Printer protocol No. 8, used with WASH and MOLASSES method
- Printer protocol No. 9, used with SOFT DRINK method.
For details of the settings, see Appendix B.2.
If required, you can change these pre-settings according to your demands.
To define or change a printer protocol, change to the menu utilities > output
configuration > printer protocol:
To activate/deactivate the parameters, use the key.
7.5.3 Selecting the Output Data for the Data Memory
Change to the menu utilities > output configuration > data memory.
You can activate up to 10 parameters to be stored in the data memory:
To activate/deactivate the parameters, use the key.
7.6 Settings for the Sample Changer
Enter the control parameter for SP-1m in the menu auto sampler settings
as described in the SP-1m instruction manual.
Information:
If data should be sent to a LIMS system, activate additionally the parameters
alcohol cond. and color cond.
8 Setting the Measuring Methods
34 C27IB02
This menu is only displayed if a sample changer is connected and configured
in the menu instrument settings > device list > filling device.
8.1 Description of the Measuring Methods
Alcolyzer Plus Beer provides 10 different methods:
Fig. 8 - 1 Menu: method settings
Method 1: BEER
Standard method for beers. This method can be used for almost all samples.
Method 2: CIDER
Method for ciders.
Method 3: SOFT DRINK
Method for alcohol-free beverages.
Method 4: WASH
Method for wash. Wash is an intermediate product of whisky production. It is an
alcohol containing liquid produced in the fermentation of worts by yeasts. The
alcohol content in wash varies between 7 and 10%vol.
Information:
We recommend setting the following filling times:
Without option pH/color: 80 seconds (sample changer parameter "1080").
With option pH/color: 100 seconds (sample changer parameter "1100").
METHOD SETTINGS
no. 1
no. 2
no. 3
no. 4
no. 5
no. 6
no. 7
no. 8
no. 9
no. 10
:
:
:
:
:
:
:
:
:
:
BEER
CIDER
SOFT DRINK
WASH
new method
MOLASSES
C27IB02 35
Method 5: MOLASSES
Method for molasses. Molasses is a honey-like, dark-brown sugar syrup which is
used as a fermentation raw material in the production of bioethanol. With this
method, you can determine the ethanol content of fermenting or ready-fermented
molasses.
Methods 6 to 10:
These methods are sample-specific and can be edited as described in Chapter
8.2.
8.2 Editing a Measuring Method
8.2.1 Editing a Predefined Method
You can edit the predefined methods "BEER", "CIDER", "SOFT DRINK", "WASH"
or "MOLASSES" to assign another printer protocol or enter a residual CO
2
content.
1. In the menu method settings, select one of the predefined methods and
confirm with <>.
2. In protocol no.:, you can select one of 10 printer protocols to assign it to the
selected method (For editing a printer protocol, see Chapter 7.5.2).
8.2.2 Editing a New Method
You can edit a new method to assign a special printer protocol (see Chapter 7.5.2)
or to enter a sample-specific alcohol correction factor (see Chapter 12.4). For the
types "BEER", "CIDER" and "SOFT DRINK", the residual CO
2
can be entered
1. Select a row between 6 and 10 in the menu method settings.
"new method" is displayed.
2. Confirm with <>.
3. Enter a name for the method and confirm the method name with <>.
Information:
If you measure fermenting molasses, we recommend to filtrate the sample
prior to measurement.
Information:
The menu item residual co2 is only used with PBA-B and the methods
"BEER", "CIDER" and "SOFT DRINK".
36 C27IB02
4. Select a type "BEER", "CIDER", "SOFT DRINK", "WASH" or "MOLASSES"
for the new method.
The type has to correspond with the sample to be measured.
5. If necessary, enter an offset between 0.99%vol and +0.99%vol (see
Chapter 12.4).
6. If necessary, enter a pH-offset between -0.99 and +0.99 in pH-deg. offset.
7. In protocol no.:, you can assign a printer protocol from 1 to 10 to the new
edited method.
For details about editing a printer protocol, see Chapter 7.5.2.
8. Press <> to confirm the settings.
Fig. 8 - 2 Menu: method settings/new method/name
EDIT METHOD no. 6
type
offset
pH-deg.offset
BEER :
:
:
+0.50 %V/V
name special beer :
protocol no.
residual co2
:
:
+0.50
05
0.00 g/l
Information:
The menu item residual co2 is only used with PBA-B and the methods
"BEER", "CIDER" and "SOFT DRINK".
C27IB02 37
8.3 Selecting the Measuring Method
1. Press the <Method> key in the measuring window.
Fig. 8 - 3 Selecting a method
2. Use the key to toggle between the different methods.
3. Select the appropriate method (e.g. "BEER") with the <> key.
The selected method is displayed in the left upper corner.
BEER
BEER
valid
09:44:21
valid
valid
method :
%V/V
20 C
c 7.4 EBC
pH 4.43
Information:
If you have assigned another method to a certain sample in the sample list,
this method instead of the selected method is used to measure the sample
(see Chapter 12.1.3.1).
9 SOP (Standard Operating Procedure)
38 C27IB02
To ensure that Alcolyzer Plus Beer gives correct results, check the adjustments
of the measured parameters regularly.
The integrated SOP (Standard Operating Procedure) allows you to perform an
automated control measurement of all measuring parameters as well as an
adjustment afterwards.
Carrying out the SOP
1. Select the menu utilities > SOP configuration and choose SOP #1 or
SOP #2.
"SOP #1" is defined as the "routine" SOP and contains the parameters water,
alcohol, pH1 and pH2.
2. Place the appropriate control solutions in the correct order into the sample
changer magazine (for preparing the control solutions, see Chapter 10).
The following control solutions are used for the SOP:
- Bi-distilled water to check the zero point of the alcohol and the color
adjustment
- A binary ethanol/water solution with an alcohol content of 8 to 12%V/V to
check the "known concentration" of the alcohol adjustment
- pH buffer pH 7.00 and
- pH buffer pH 4.01 to check the pH adjustment
3. Press the <SOP> key in the measuring window of Alcolyzer Plus Beer to
access the following menu:
Information:
The SOP can only be used in combination with a sample changer.
Information:
Carry out the "routine" SOP once a day. If desired, an additional SOP
(SOP #2) can be defined as an "extended" SOP with additional parameters
(e.g. color standard).
C27IB02 39
Fig. 9 - 1
Use the key to toggle between "SOP #1" and "SOP #2".
4. Press the <Cont> key to start the SOP.
5. Press the <Start> key on the sample changer.
The control solutions are measured automatically.
After the last measurement, the following window is displayed:
Fig. 9 - 2
6. If a measured value deviates significantly from the desired value, this value
can be readjusted now.
STANDARD OPERATING PROCEDURE #1
#1:
2:
3:
4:
#
#
#
water
alcohol
pH 1
pH 2
adjust ?
adjust ?
adjust ?
water
alcohol
pH 1
pH 2
SP-1m :
-0.01 %V/V
0.07
10.01
EBC
%V/V
4.02 pH
6.99 pH
stopped
adjust ?
10: 32: 54
40 C27IB02
7. Highlight the respective row "adjust?" and press the <> key (see Fig. 9 - 2).
8. Enter the desired value and press <>.
Fig. 9 - 3
The following window is displayed (in this example, the alcohol value has
been readjusted):
Fig. 9 - 4
Information:
The adjustment of the known concentration for the alcohol can only be
performed successfully if an accurate density meter and an appropriate
density/alcohol concentration table are available.
If the known concentration for the alcohol shall be adjusted, the alcohol
value measured by the DMA is displayed in a line below the SOP
parameters after pressing the <> key. This value can be taken directly
for the readjustment.
water
alcohol
pH 1
pH 2
adjust ?
adjust ?
adjust ?
10: 34: 27
-0.01 %V/V
0.07
10.01
EBC
%V/V
4.02 pH
6.99 pH
1 concentration: 0.05 %V/V
adjust ?
adjusted
adjust ?
water
alcohol
pH 1
pH 2
-0.01 %V/V
0.07
10.05
EBC
%V/V
4.02 pH
6.99 pH
adjust ?
10: 35: 16
10 Checking the Adjustment Validity
C27IB02 41
9. Finish the SOP by pressing the <Esc> key or the <Cont> key when all
parameters are readjusted.
If no SOP (see Chapter 9) is carried out, check the adjustments regularly as
described below.
10.1 Checking Procedure without Option pH/Color
Before each series of measurements, check the zero point using degassed,
bi-distilled water.
To check the validity of the slope of the adjustment, use a water/ethanol
solution of known concentration. Perform a slope check at least once every
week.
10.1.1 Performing a Checking Procedure with Water (0%V/V)
1. Boil fresh, bi-distilled water for several minutes to remove dissolved gas.
2. Fill a clean glass flask full with the boiled water and cover it.
3. Wait until the water has cooled down to 20 2C.
4. Clean the measuring cell as described in Chapter 14.
Information:
If one (or both) pH buffer deviates too much from the correct value, the
measured pH value and the measured temperature will be displayed in a
line below the SOP parameters after confirming the question "adjust ?".
The pH value can then be corrected according to the pH/temperature
table of the corresponding buffer.
The readjustment for the pH measurement is carried out for both
adjustment points simultaneously. Therefore, only one "adjust? is
displayed for both buffers.
Information:
For the color adjustment, it is only necessary to adjust the zero point with
bi-distilled water regularly.
If it is desired to check also the known concentration for the color
measurement (e.g. with a standard beer or color standard) this parameter
can be added to the SOP. If the known concentration for the color
measurement shall be adjusted, the color value of the color standard can
be entered in a line below the SOP parameters after pressing the <> key.
Color standards are available at Anton Paar. Contact your local distributor.
42 C27IB02
5. Fill a sample vial with degassed, bi-distilled water and put it into the
magazine of the sample changer.
7. Wait until the measuring status displays "valid".
8. If the displayed value is 0 0.03%V/V and is stable for a few minutes,
measurements can be performed.
9. If the displayed value is outside this concentration range, clean the
measuring cell and perform another control measurement.
10. If the measuring result is still out of range (0 0.03%V/V) perform a zero
point adjustment (see Chapter 11.1.1).
11. If "no sample" is displayed, clean the measuring cells according to Chapter
14.1.3 or Chapter 14.2.4 (with option pH/color).
12. Then perform an adjustment for the zero point and for the known
concentration.
Checking the validity of the density adjustment
1. As soon as the DMA gives a valid result (flashing display), check the density
reading.
2. If the result deviates more than 0.0001 g/cm
3
(DMA 4500) or 0.00005 g/cm
3
(DMA 5000) from the reference value (0.998203 g/cm
3
), perform a cleaning
procedure according to Chapter 14.
3. Repeat the checking procedure.
4. If the density result still exceeds the max. allowed deviation, perform an air/
water adjustment for the density meter (see Chapter 11.3).
Information:
If a density meter (DMA 4500, DMA 5000) is connected to Alcolyzer Plus
Beer, check also the validity of the density adjustment as described below.
C27IB02 43
10.1.2 Performing a Checking Procedure with a Water/
Ethanol Solution of Known Concentration
1. Prepare a water/ethanol solution with a concentration between 8 and
12%V/V.
2. Cover the flask and leave the solution for several hours at a temperature of
20 3C.
Before filling the measuring cell, the sample must be free of air bubbles.
3. Clean the measuring cell, if necessary (see Chapter 14).
4. Fill a sample vial with the water/ethanol solution and put it into the magazine
of the sample changer.
6. Wait until Alcolyzer Plus Beer and the DMA show "valid".
7. If the difference between the measuring values from Alcolyzer Plus Beer and
the DMA is less than 0.03%V/V and the results remain stable within this
range for a few minutes, the adjustment of Alcolyzer Plus Beer is correct.
8. If the displayed value is out of this range, clean the measuring cell and
perform another control measurement.
9. If the measuring result is still out of range, perform an adjustment using a
water/ethanol solution (see Chapter 11.1.2).
Information:
This measurement can only be performed successfully if an accurate density
meter and an appropriate density / alcohol concentration table is available.
Caution:
Only use high-proof ethanol without denaturant!
Information:
If Alcolyzer Plus Beer is used in combination with a DMA 4500/5000, the
alcohol concentration is directly displayed on the density meter.
44 C27IB02
10.2 Checking Procedure with Option pH/Color
10.2.1 Checking Procedure for the Measuring Parameter
"alcohol"
The checking procedure for the measuring parameter "alcohol" is performed as
described in Chapter 10.1.
10.2.2 Checking Procedure for the Measuring Parameter "pH"
Check the validity of the pH adjustment with buffers pH 7 and pH 4 once a day
(before starting the routine measurements).
Control measurement for buffer pH 7
1. Fill a sample vial with buffer pH 7 and place it in the sample changer
magazine.
After filling is completed, the measurement starts automatically.
3. Wait until the pH value is displayed in the measuring window ("valid").
This value is valid for 25C.
4. If the difference between the measured pH value and the set point is less
than 0.05 pH units, the pH adjustment is correct.
5. If the displayed value is out of this range, fill the pH measuring cell with the
same buffer and repeat the control measurement.
Caution:
Always use fresh pH buffers.
Information:
Instead of using the sample changer, one of the following filling procedures
can be used:
Disconnect the silicone hose that is plugged to the front adapter of the pH
measuring cell. Fill a 20 mL syringe with the buffer. Connect the syringe to
the front adapter of the pH measuring cell and fill in the buffer.
Or:
Remove the pH electrode from the pH measuring cell and immerse the
electrode into a vessel filled with pH buffer. Ensure that the buffer
temperature does not deviate significantly from the temperature in the pH
measuring cell as the temperature sensor for the pH measurement is
located in the pH measuring cell.
11 Adjusting the Instrument
C27IB02 45
6. If the displayed value is still out of range, perform an adjustment (see
Chapter 11.2.3).
Control measurement for buffer pH 4
The control measurement is performed in the same way as for buffer pH 7.
10.2.3 Checking Procedure for the Measuring Parameter
"color"
Checking procedure with water (0.0 EBC)
This procedure should preferably be performed together with the checking
procedure for 0% alcohol (see Chapter 10.1.1)
1. If the displayed value is 0 0.3 EBC (0 0.15 ASBC), measurements can be
performed.
2. If the displayed value is out of this range, clean the measuring cells and
repeat the control measurement.
3. If the measuring result is still out of range, perform a "zero" adjustment (see
Chapter 11.2.2).
11.1 Adjustment without Option pH/Color
Regular adjustments are performed with degassed bi-distilled water (0%V/V
alcohol, zero point).
Extended adjustments are performed with degassed bi-distilled water and a
water/ethanol solution of exactly known concentration in the range of 2 to
30 %V/V, preferably 8 to 12%V/V.
An extended adjustment is necessary if the checking procedure with a water/
ethanol solution of known concentration shows deviations of more than
0.03 %V/V from the reference value, even after correct zero point
adjustment.
Information:
During the first months, usually a drift of the color value of approx. 0.1 EBC
per day can be observed. This drift (in the positive direction) is a result of a
decreasing LED intensity.
46 C27IB02
If the adjustment of Alcolyzer Plus Beer is properly performed, it is sufficient
to check only the zero point before each series of measurements.
11.1.1 Adjustment with Water (Zero Point)
1. Boil fresh, bi-distilled water for several minutes to remove dissolved gas.
2. Fill a clean glass flask full with the boiled water and cover it.
3. Wait until the water has cooled down to approx. 20 2C.
4. Select Alcolyzer Plus Beer menu adjustment > adjust alcohol > zero.
5. Answer the question "Do you really want to adjust?" with <YES>.
If there is no bi-distilled water in the measuring system, press <S-Start> on
Alcolyzer Plus Beer. Then press the <Start> key on the sample changer.
The bi-distilled water is now filled into the measuring system by the sample
changer. After the filling procedure is completed, the adjustment procedure
starts automatically.
If bi-distilled water has already been filled into the measuring system, press
the <Start> key instead of the <S-Start> key to start the adjustment
procedure immediately.
6. Wait until the adjustment has been completed.
Information:
Before the adjustment, Alcolyzer Plus Beer has to be turned on for at least
one hour. However, after transport full stabilization of Alcolyzer Plus Beer
might take up to one day.
The ambient temperature should be stable to < 3C.
Caution:
Before starting the adjustment, ensure that the measuring cells are properly
cleaned (see Chapter 14).
C27IB02 47
Fig. 11 - 1 Successful adjustment
7. If the measurement value is stable to 0.02%V/V, the adjustment is
successful and "adjustment saved" is displayed (see Fig. 11 - 1).
Press <Cont> to confirm the adjustment.
Press the <Esc> key three times to return to the measuring window.
8. If "no stability - restart" is displayed after the adjustment, the required stability
of the measuring result could not be achieved. Problems during sample
filling (for example, air bubbles in the cell) could be the reason.
Clean the cells again and repeat the adjustment with bi-distilled water.
ADJUSTMENT ALCOHOL
S1 = 87.30 % of factory adjustment
adjustment 0.00 %V/V
adjustment saved
Information:
Additionally, the value S1 gives information about the measured signal
intensity of the current adjustment compared to the signal intensity at the
factory adjustment. This value decreases by-and-by due to ageing of the LED
and/or coating of the measuring cell.
If the S1 value is below 80%, clean the measuring cell thoroughly (see
Chapter 14) and repeat the zero adjustment. If the S1 value is still too low,
contact your Anton Paar representative.
Information:
After this adjustment we recommend performing the zero adjustment for the
optional color measurement because the bi-distilled water which is inside the
cells can be used for the zero adjustment of the color measurement.
48 C27IB02
11.1.2 Adjustment with a Water/Ethanol Solution of Known
Alcohol Concentration
1. Prepare a water/ethanol solution.
2. Cover the flask and leave the solution for several hours at 20 3C. Before
filling the measuring cell, the sample must be free of gas bubbles.
3. Select the Alcolyzer Plus Beer menu adjustment > adjust alcohol > known
concentration.
5. If there is no water/ethanol solution in the measuring system, press
<S-Start> on Alcolyzer Plus Beer.
The water/ethanol solution is now filled into the measuring system by the
sample changer. After the filling procedure is completed, the adjustment
procedure starts automatically.
If a DMA 4500/5000 is connected and configured properly (see Appendix F),
"DMA: measuring" is displayed on Alcolyzer Plus Beer. As soon as "DMA:
valid" is displayed, the alcohol concentration that comes from the DMA is
displayed in the first line of Alcolyzer Plus Beer display and can be used
directly as the "known concentration" value for the adjustment.
7. Press the <Cont> key to continue the adjustment.
8. Wait until the adjustment is finished.
Caution:
Only use high-proof ethanol without denaturant.
Information:
The concentration of the water/ethanol solution for the adjustment must be
between 2 and 30%V/V, preferably between 8 and 12%V/V alcohol.
Caution:
Information:
If a water/ethanol solution has already been filled into the measuring system,
press the <Start> key instead of the <S-Start> key.
C27IB02 49
9. If the measurement is stable to 0.02%V/V, the adjustment was successful
and "adjustment saved" is displayed.
10. If "adjustment failed" is displayed after the adjustment, the required stability
Clean the cells again and repeat the adjustment with a water/ethanol
solution.
11.2 Adjustment with Option pH/Color
11.2.1 Adjustment Alcohol
The adjustment for the measuring parameter "alcohol" is performed as described
in Chapter 11.1.
11.2.2 Adjustment Color
For the color adjustment, use the delivered color adjustment set.
11.2.2.1 Adjustment with Water (Zero)
1. Fill a clean sample vial with the delivered water standard (ultra pure water)
and place the vial in the sample magazine.
2. Select the menu adjustment > adjustment color > zero.
4. Press the <S-Start> key on Alcolyzer Plus Beer.
The ultra pure water is filled into the measuring system.
Information:
Alcohol solutions have a tendency to form gas bubbles. Handle the sample
with care.
Caution:
50 C27IB02
After the filling procedure is completed, the adjustment procedure starts
automatically.
Fig. 11 - 2 Successful adjustment
If the measurement value is stable, the adjustment is successful,
"adjustment saved" is displayed (see Fig. 11 - 2).
7. If "no stability - restart" is displayed after the adjustment, the required stability
Clean the cells again and repeat the adjustment with bi-distilled water.
ADJUSTMENT COLOR
S = 98.30 % of factory adjustment
adjustment 0.00 EBC
adjustment saved
Information:
Additionally, the value S gives information about the measured signal intensity
of the current adjustment compared to the signal intensity at the factory
adjustment. This value decreases by-and-by due to ageing of the LED and/or
coating of the measuring cell.
If the S value is below 80%, clean the measuring cell thoroughly (see Chapter
14) and repeat the zero adjustment. If the S value is still too low, contact your
Anton Paar representative.
Information:
After the color adjustment has been done properly, it is only necessary to
check the zero point adjustment with bi-distilled water regularly.
C27IB02 51
11.2.2.2 Adjustment with a Color Standard (Tartrazine) of Known
Concentration
1. Fill a sample vial with the delivered color standard (tartrazine) and place it in
the sample changer magazine.
2. Select the menu adjustment > adjust color > known concentration.
4. Press the <S-Start> key on Alcolyzer Plus Beer.
The standard is filled into the measuring cells.
6. Enter the EBC value of the delivered standard in the line "color".
7. Press the <Cont> key to continue with the adjustment.
9. If the measurement is stable, the adjustment was successful and
"adjustment saved" is displayed.
10. If "adjustment failed" is displayed after the adjustment, the required stability
Clean the cells again and repeat the adjustment with the color standard.
Information:
The concentration of the color standard for the adjustment must be between
1.00 and 60.00 EBC (0.50 to 30.48 ASBC), preferably at approx. 50.00 EBC
(25.40 ASBC).
Information:
After the color adjustment has been done properly, it is only necessary to
check the zero point adjustment with bi-distilled water regularly.
52 C27IB02
11.2.3 Adjustment pH
The adjustment of the pH electrode is performed with two buffers (pH 7 and pH 4).
(before starting the routine measurements). For details, see Chapters 9 and
10.2.2.
For the pH buffers "Hamilton Duracal" the buffer data (pH value depending on the
temperature) are integrated in Alcolyzer Plus Beer.
If the pH electrode is adjusted with these buffers, the correct buffer data are
selected automatically.
If you use a different buffer to "Hamilton Duracal", the buffer data (pH value
depending on the temperature) can be entered in the menu edit buffer data. If
the pH electrode is then adjusted with these buffers, the correct buffer data are
selected automatically.
Caution:
Always use fresh pH buffers.
Temperature (C) Buffer pH 7.00 Buffer pH 4.01
5 7.09 4.01
10 7.06 4.00
15 7.04 4.00
18 7.03 4.00
20 7.02 4.00
22 7.01 4.00
25 7.00 4.01
30 6.99 4.01
35 6.98 4.02
40 6.97 4.03
45 6.97 4.04
50 6.97 4.05
Information:
For the adjustment, the first buffer should be pH 7, the second buffer should
be pH 4.
C27IB02 53
11.2.3.1 Automatic
The adjustment is usually performed with "Hamilton Duracal" buffers. However,
the adjustment can be performed with other buffers. The data of these buffers
have to be entered in the menu edit buffer data. The edited buffers have to be
selected in the menu sort buffer data.
1. Select menu adjustment > adjust pH > automatic.
"clean pH sensor/expose to buffer 1" is displayed.
2. To fill buffer pH 7 in the measuring cells using the sample changer SP-1m,
press first the <S_Start> key on the Alcolyzer and then the <Start> key on
the sample changer.
3. After the filling procedure is completed, wait until the voltage and the pH
value is stable (also check if the pH value is plausible) before pressing the
<Start> key to start the adjustment.
"Standard 7.00" (or the name of your buffer) as well as a number (in row
"adjust") is displayed.
4. Press the <Cont> key.
The adjustment with the first buffer is finished.
5. Fill buffer pH 4 in the measuring cells and wait until the voltage and the pH
value is stable (also check if the pH value is plausible).
6. Then press the <Start> key to start the adjustment.
Information:
can be used:
the front adapter of the pH measuring cell and fill in the buffer. Use at least
15 mL buffer to make sure that the previous liquid in the pH measuring
cell is fully replaced.
Or:
Information:
If "no buffer saved" is displayed, the measured voltage deviates from the
stored tables (Hamilton or your own tables).
54 C27IB02
"Standard 4.01" (or the name of your buffer) is displayed. The adjustment is
finished. The voltages of the adjustment data (for the offset and the slope)
are displayed.
7. Press the <Cont> key to finish the adjustment.
11.2.3.2 Manual
The pH adjustment can also be performed manually. To do this, any buffer can be
used.
1. Select menu adjustment > adjust pH > manual.
2. To fill buffer pH 7 in the measuring cells using the sample changer SP-1m,
press first the <S_Start> key on the Alcolyzer and then the <Start> key on
the sample changer.
3. After the filling procedure is completed, wait until the voltage and the pH
value is stable (also check if the pH value is plausible) before pressing the
<Start> key to start the adjustment.
4. Enter the theoretical pH value of the buffer (pH value depending on the
current temperature) using either the <>, <>, <> keys or a keyboard.
5. Then press <>.
6. Wait until the adjustment with the first buffer is finished.
7. Then press the <Cont> key.
8. Fill buffer pH 4 in the measuring cells and wait until the voltage and the pH
value is stable (also check if the pH value is plausible).
9. Then press the <Start> key to start the adjustment.
Information:
can be used:
the front adapter of the pH measuring cell and fill in the buffer. Use at least
15 mL buffer to make sure that the previous liquid in the pH measuring
cell is fully replaced.
Or:
C27IB02 55
10. Enter the theoretical pH value of the buffer (pH value depending on the
current temperature) using either the <>, <>, <> keys or a keyboard.
11. Then press <>.
12. Wait until the adjustment with the second buffer is finished.
The voltages of the adjustment data (offset and slope) are displayed.
13. Press the <Cont> key to finish the adjustment.
11.2.3.3 Edit Buffer Data
If you use a different buffer to "Hamilton Duracal" for the adjustment, the buffer
data (pH value depending on the temperature) can be edited in this menu.
In the first two rows of the list the buffers "Hamilton Duracal" are predefined. The
data of these buffers are already programmed and cannot be edited.
The rows 3 10 are individually editable. For any buffer the buffer data can be
entered and stored using a certain name for the new edited buffer.
Entering buffer data
1. Select a row between 3 and 10 using the keys <> and <>.
"new buffer" appears on the display.
2. Press < > to enter the designation (e.g. "buffer pH 4") of the new buffer
using the <>, <>, <> keys or a keyboard.
3. Press the <> key.
Now the list can be entered (temperature and corresponding pH value).
4. Use the key to enter the data. Use the <> key to move the cursor.
Use the <> key to go to the next row. Press <> to save all entered data.
5. Answer the question "save new pH buffer?" with the <Cont> key.
Deleting buffer data
1. To delete a newly edited buffer, press the <Del> key.
2. Answer the question "really clear buffer data?" with <YES> and press the
<Cont> key.
Caution:
At least two pairs of temperature and corresponding pH value that enclose the
temperature, at which the pH is later measured, have to be entered.
56 C27IB02
11.2.3.4 Sort Buffer Data
If new edited buffers are stored in Alcolyzer Plus Beer (see Chapter 11.2.3.3),
these buffers can be selected to be used for the adjustment in this menu.
The buffers which are selected for the first two lines (no. 1 and no. 2) are used for
the adjustment. The first buffer should be buffer pH 7, the second buffer should
be buffer pH 4.
To move the appropriate buffers to line no. 1 and no. 2, perform the following
steps:
1. Select the buffer to be moved with the <> or <> keys.
2. Mark the selected buffer with the key. The key changes to .
3. The marked buffer can be moved to the appropriate line using the <> or
<> keys.
4. Press the key to release the marked buffer.
The key changes to . The buffer cannot be moved any longer.
11.3 Density Adjustment
If the connected density meter (DMA 4500, DMA 5000) needs to be re-adjusted
(see Chapter 10.1.1), perform the following steps:
1. Clean the measuring cells according to Chapter 14.1.2 (without option pH/
color) or Chapter 14.2 (with option pH/color).
2. To dry the measuring cells, fill a vial with highly concentrated ethanol (max.
96%) without denaturant.
3. Place the vial into the sample changer.
4. Select the Alcolyzer menu instrument settings > device list and set
density to not used. Confirm with <>.
5. Press the <Start> key on the sample changer to fill the highly concentrated
ethanol.
6. After filling is completed, press the <Stop> key on the sample changer.
7. Connect the air pump hose of the DMA to the needle of SP-1m.
8. Turn on the air pump of the DMA.
9. Open the pump lever of SP-1m and loosen the cartridge.
After 15 minutes the air pump will switch off automatically.
10. Remove the air pump hose from the needle and close the pump lever.
C27IB02 57
11. Perform an air/water adjustment as described in the DMA 4100/4500/5000
instruction manual (To fill the bi-distilled water into the measuring cells, press
the <Start> key on the SP-m).
12. When the density adjustment is finished, re-activate the communication
between Alcolyzer Plus Beer and DMA 4500/5000 by selecting the Alcolyzer
menu instrument settings > device list and setting density to DMA xxxx
series. Confirm with <>.
Information:
Before starting a new measurement, rinse the cells with an approx. 10%
ethanol/water solution (e.g. your alcohol adjustment solution) to decrease the
surface tension. This avoids air bubbles.
12 Measurement
58 C27IB02
12 Measurement
Press the <Sample#> key and enter a sample
identification and the appropriate method in the
sample list (see Chapter 12.1).
Fill the sample vials 3 mm below the rim with sample

and cover the vials.
Put the sample vials into the sample changer

magazine.
Press the <Start> key on the sample changer:

The sample from the first vial is automatically filled
into the measuring system and measured.
After the end of the measurement, the magazine

moves to the next vial. The next sample is filled and
measured.
After the last measurement, clean the measuring

cells (see Chapter 14).
If a pH electrode is connected, store it in a 3 molar

KCl solution (see Chapter 14.2.1).
12 Measurement
C27IB02 59
After initialization of Alcolyzer Plus Beer, measurements are continuously
performed. That means that the displayed measuring results are continuously
updated and can be printed at any time by pressing the <Print> soft key (no
automatic printout).
Start a new measurement by pressing the <Start> key on the sample
changer SP-1m.
As soon as the measurement is "valid", the protocol is printed automatically
(as long as the printer has been connected and configured properly, see also
Chapters 7.3.3 and 7.5.2). The measuring values flash.
The sample changer moves to the next position of the magazine and a new
measurement is started.
12.1 Identifying the Sample and Assigning the
Method
12.1.1 Types of Sample Identification
The type of sample identification can be selected in the menu utilities > sample
identification.
#+list (default):
This menu is only available if a sample changer is connected and activated. A list
of 24 individually selected numbers or texts can be entered. Additionally, the
position number of the sample changer vessel is displayed at the beginning of the
sample identification.
list:
This menu is only available if a sample changer is connected and activated. A list
of 24 individually selected numbers or texts can be entered.
Information:
The <Print> soft key is only displayed if connected to: printer_1 (or
printer_2/printer_3/printer_4/AP-SoftPrint/VisioLab) is selected in the
menu instrument settings > COM1 or COM2.
Information:
To obtain the calculation and printout of parameters (e.g. alcohol %m/m, SG
20/04,...), select calc. parameter OIML V/V (or CU V/V) in the menu
instrument settings > configuration. The density that is needed for the
calculations is directly transferred from the connected density meter.
12 Measurement
60 C27IB02
text + number:
The sample identification consists of text - consecutive number - text. The text
before and after the number can be up to 8 digits long. The consecutive number
is set once at the start and is then increased by one automatically at the beginning
of each new measurement.
text:
Sample identification using text. The text can be 20 digits long.
12.1.2 Sample Identification for "text + number" and "text"
1. Press the <Sample#> key in the measuring window.
2. Enter the sample identification using the <>, <> or <> keys and confirm
with <>. Optionally, the sample identification can be entered with a
keyboard or a bar code reader.
12.1.3 Sample Identification for "list" and "# + list"
12.1.3.1 Entering a Sample List
In the sample list, you can enter the sample identifications and you can
individually assign any measuring method (BEER, CIDER, SOFT DRINK, WASH,
MOLASSES or a new edited method) to each sample.
If no sample list has been entered before, immediately a list is displayed.
If a sample list was entered before, the following window is displayed:
Information:
The measuring method you define in the sample list overrides the method you
have selected in the measuring window (see Chapter 8.3). The used method
is shown on the display when the sample is measured.
12 Measurement
C27IB02 61
Fig. 12 - 1 Edit list
Select one of the options using the <> and <> keys. Press <> to confirm.
After confirming edit, the existing sample list can be edited.
After confirming new list, the existing list can be deleted. A new list appears
in which the new sample identifications can be entered.
2. To enter the sample identification, use the soft keys, a keyboard or barcode
reader.
a) Entering the sample identification with the soft keys:
Press <>.
Use the <> and <> keys to choose the characters.
Use the <> key to move the cursor.
Press <> to confirm the sample identification.
The cursor moves to the column "method".
Select the appropriate method using the key and press <>.
The cursor moves to the next line for entering the sample identification.
b) Entering the sample identification with a connected keyboard:
Enter the sample identification using the keyboard and press <>.
c) Entering the sample identification with a connected bar code reader:
Enter the sample identification using the bar code reader.
edit
new list
BEER
valid
09:44:21
valid
valid
SP-1m list :
%V/V
20 C
c 7.4 EBC
pH 4.43
12 Measurement
62 C27IB02
3. After editing the list, press the <Esc> key to return to the measuring window.
12.1.3.2 Editing the Sample List during Operation
The sample list can also be edited/changed during filling or measuring. This is
very convenient, especially if a sample identification has been entered incorrectly
or if an additional sample has been put into the magazine.
1. Press the <Sample#> key to edit the list.
2. Carry out the desired changes, confirm with <> and return to the measuring
window again by pressing <Esc>.
12.1.3.3 Deleting a Sample List
Manually
2. Use the <> key to select the line "new".
3. Press <>.
4. Answer the question "really discard sample list?" with <YES> and press
<Cont>.
Automatically
Select auto. new list in the menu utilities > sample identification >
SP-1m.
The sample list is automatically deleted when the sample magazine has
reached the zero position after a measuring cycle (see Chapter 15.2.6).
12 Measurement
C27IB02 63
12.2 Performing a Measurement without Option pH/
Color
1. Select the appropriate method (see Chapter 8.3).
2. Perform an SOP (see Chapter 9) or checking procedure (see Chapter 10.1).
3. Enter the sample identification (see Chapter 12.1).
4. Fill the sample into the sample vials.
5. Set the appropriate filling parameters in the menu sample changer
settings.
For the sample changer SP-1m we recommend using "1080" (80 seconds
filling time, approx. 20 mL sample).
6. Put the sample vials into the sample changer magazine.
The sample is filled into the measuring system and the measurement is
started automatically.
When the measurement is finished (condition: "valid"), a printout starts
automatically (if a printer is connected to COM 1 and configured properly).
The magazine automatically moves to the next position and a new
measurement is started.
Information:
The sample must be free of gas bubbles. Beers have to be degassed
before measurement (see Appendix A).
Thermostatting the sample before measurement (20 C) reduces the
measuring time.
Fill the vials at maximum to 3 mm below the rim.
Do not overfill the vials of the SP-1m since this will promote alcohol loss.
Cover the sample vials immediately to prevent alcohol loss.
Information:
During the filling procedure it is possible to press the <Stop> key on the
sample changer (e.g. if an incorrect sample has been filled). The <Cont> key
appears on the display of Alcolyzer Plus Beer.
If the <Cont> key is pressed, the current measurement is abandoned and the
display shows: "SP-1m: press START". A new measurement (with the next
sample) can be started.
Caution:
Clean the measuring cells when all measurements are finished (see Chapter
14.1). Do not leave sample in the cells as this results in deposits and
residues.
12 Measurement
64 C27IB02
12.3 Performing a Measurement with Option pH/
Color
Generally, the operation is the same as described in Chapter 12.2. At step 5, set
"1100" as the control parameter for the sample changer SP-1m in the menu auto
sampler settings. This corresponds to a filling time of 100 seconds. A sample
volume of 30 mL is recommended.
When using the option pH and color, the color measuring cell and the pH
measuring cell are filled automatically by the sample changer SP-1m, as well as
the density measuring cell of the DMA and the alcohol measuring cell of Alcolyzer
Plus Beer.
When the measurement is finished, the measured parameters alcohol [%V/V],
color [EBC or ASBC] and pH value are displayed and printed (if a printer is
connected).
12.4 Correcting Calculated Analysis Results
If the deviation between the alcohol content (alcohol %V/V) measured by the
Alcolyzer Plus and the reference value determined with the distillation method is
the same for different beer types, a valid correction factor for these beer types
can be entered. The correction factor uses addition to correct the alcohol content
value determined by the Alcolyzer Plus.
Examples:
Activating the alcohol correction factor
1. To enter the alcohol correction factor, set up a new method.
For setting up a new method, see Chapter 8.2.
2. Enter the correction factor as the offset value between -0.99%V/V and
+0.99%V/V.
Caution:
Clean the measuring cells, when all measurements are finished (see
Chapter 14.2). Do not leave sample in the cells as this results in deposits
and residues.
After the measurements, store the pH electrode in a 3 molar KCl solution
Alcolyzer Plus:
Distillation:
Correction factor:
alcohol %V/V = 5.41
alcohol %V/V = 5.29
= -0.12
Alcolyzer Plus:
Distillation:
Correction factor:
alcohol %V/V = 7.12
alcohol %V/V = 7.30
= +0.18
12 Measurement
C27IB02 65
After entering the correction factor, the alcohol value will be corrected for all
beer types measured with this new method.
3. For activating the measuring method, see Chapter 8.3.
4. To make sure that the appropriate offset is used, define the parameter offset
also for the printout (printer protocol/head).
For setting the output, see Chapter 7.5.2.
Examples of printouts of analysis data with and without correction:
Measurement: Not corrected Measurement: Corrected
------- A L C O L Y Z E R Plus -------
date : 2009-03-06
time : 11:42:38
sample no. : 0001
alcohol : 4.91 %V/V
offset : 0.00 %V/V
alcohol : 3.85 %m/m
density : 1.00543 g/cm3
p : 11.15 %m/m
Er : 3.65 %m/m
Ea : 1.86 %m/m
SG 20/20 : 1.00724
pH : 4.44 pH
color : 8.3 EBC
RDF : 68.58 %
ADF (m/m) : 83.33 %
Calories : 167.29 kJ/100 mL
--------------------------------------------------
------- A L C O L Y Z E R Plus -------
date : 2009-03-06
time : 11:48:49
sample no. : 0002
alcohol : 4.76 %V/V
offset : -0.15 %V/V
alcohol : 3.74 %m/m
density : 1.00543 g/cm3
p : 10.88 %m/m
Er : 3.60 %m/m
Ea : 1.86 %m/m
SG 20/20 : 1.00724
pH : 4.44 pH
color : 8.3 EBC
RDF : 68.23 %
ADF (m/m) : 82.93 %
Calories : 163.18 kJ/100 mL
--------------------------------------------------
13 Data Memory
66 C27IB02
13 Data Memory
The Alcolyzer Plus provides an integrated data memory for a maximum of 100
data sets.
The parameters that are stored have to be activated in the menu utilities >
output configuration > data memory (see Chapter 7.5.2).
Browsing the data memory
1. Select the menu data memory > browser to access the following window:
Fig. 13 - 1 Menu: data memory/browser
Press the key to go to the next data set.
Use the <> key to display the oldest data set.
Use the <> key to display the newest data set.
2. To display further parameters within the data set, press the <> key.
Fig. 13 - 2
DATA MEMORY
alcohol
alcohol
density
p
Er
1
2005-11-14 07:09:44
sample #
method
offset
:
:
:
05_special
BEER
0.00 %V/V
4.92 %V/V :
:
:
:
:
3.86 %m/m
1.00541 g/cm3
11.17 %Plato
3.65 %m/m
DATA MEMORY
Ea
pH
color
RDF
ADF (m/m)
1
2005-11-14 07:09:44
sample #
method
offset
:
:
:
05_special
BEER
0.00 %V/V
1.85 %m/m :
:
:
:
:
4.44 pH
8.2 EBC
68.64 %
83.41 %
14 Cleaning Routines
C27IB02 67
Use the key to toggle between the first and the second page of the
data set.
Use the <Print> key to print the data set.
3. Use the <Esc> key to go back one step in the menu.
It is now possible to browse between different data sets.
Deleting the data memory
1. Select the menu data memory > clear memory.
2. Press <>.
3. Answer the question "really clear data memory?" with <YES>.
The complete memory is deleted.
14.1 Cleaning the Measuring Cells without Option
pH/Color
Clean immediately after your measurements conclusion to avoid sample
residues in the measuring cells after a measurement cycle.
14.1.1 Between Series of Measurements on the Same Day
Fill the last vial of the magazine always with distilled water.
The distilled water can stay in the measuring cells until the next
measurements.
ethanol/water solution (e.g. your adjustment solution) to decrease the
14.1.2 At the End of the Day
1. As the last 5 samples, measure one vial of laboratory cleaner and four vials
of distilled water.
Information:
Suitable laboratory cleaners are e.g. Mucasol, Alconox, Tergazyme,
Extran and RBS 50 concentrate. Make sure to attend to the product
information concerning the cleaning agents concentration. E.g. Mucasol,
shall be used as a 3% solution, Alconox and Tergazyme as a 1% solution.
68 C27IB02
measurements.
14.1.3 Once a Week
Clean the measuring cells once a week (preferably before the weekend) with a
cleaner containing NaOCl (chlorine bleach) and NaOH (sodium hydroxide) or
KOH (potassium hydroxide). Make sure to attend to the product information
concerning the cleaning agents concentration.
Suitable cleaners containing NaOCl and NaOH (or KOH) are e.g.:
"Winepress Cleaner PM Membrane Presses", Cat. No. 409004, from Wigol
(www.wigol.de/en/index.htm).
"TM Desana" from Thonhauser (www.thonhauser.net/html/e/)
Alternatively, you can prepare a cleaner by yourself. Prepare an aqueous solution
of 0.5% NaOCl and 0.5% NaOH (or KOH).
1. As the last 5 samples, measure one vial of the above mentioned cleaner and
four vials of distilled water.
measurements.
Caution:
Do not let the cleaner soak in for more than 5 minutes.
The total NaOH (or KOH) and NaOCl concentration should not exceed
1 % in the applied dilution.
C27IB02 69
14.2 Cleaning the Measuring Cells with Option pH/
Color
Clean immediately after your measurements conclusion to avoid sample
residues in the measuring cells after a measurement cycle.
14.2.1 Storing the pH Electrode
Disconnect the pH electrode from the measuring system if
the system is cleaned with high-proof ethanol, concentrated NaOH or
concentrated laboratory cleaner
the system will not be used for a longer time.
If Alcolyzer Plus Beer is not used for more than one hour, the pH electrode must
be put into the storage solution (3M KCl):
1. Disconnect the silicone hose from the front adapter of the pH measuring cell
and place it into a waste vessel.
2. Fill a 20 mL syringe with storage solution, plug the syringe onto the front
adapter of the pH measuring cell and fill in the solution.
3. Leave the syringe plugged until new measurements are started
(see Fig. 14 - 1).
Fig. 14 - 1 Storing the Hamilton pH electrode
Caution:
The pH electrode must not be cleaned with high-proof ethanol, concentrated
NaOH or concentrated laboratory cleaner as it may destroy the electrode.
70 C27IB02
4. If you use an Orion pH electrode, attach the protection cap to the filling hole
of the electrode to avoid that the electrode solution dries out.
5. Before you start the next measurements, remove the protection cap again.
Fig. 14 - 2 Storing the Orion pH electrode
If Alcolyzer Plus Beer will not be used for more than 4 days, remove the pH
electrode and store it in a covered vial filled with storage solution.
14.2.2 Between Series of Measurements on the Same Day
Fill the last vial of the magazine always with distilled water.
measurements.
14.2.3 At the End of the Day
1. Measure two vials of distilled water.
2. Disconnect the pH electrode from the measuring system as described in
Chapter 14.2.1.
3. Measure one vial of laboratory cleaner and four vials of distilled water.
measurements.
C27IB02 71
14.2.4 Once a Week
Clean the measuring cells once a week (preferably before the weekend) with a
cleaner containing NaOCl (chlorine bleach) and NaOH (sodium hydroxide) or
KOH (potassium hydroxide). Make sure to attend to the product information
concerning the cleaning agents concentration.
Suitable cleaners containing NaOCl and NaOH (or KOH) are e.g.:
"Winepress Cleaner PM Membrane Presses", Cat. No. 409004, from Wigol
(www.wigol.de/en/index.htm).
"TM Desana" from Thonhauser (www.thonhauser.net/html/e/)
Alternatively, you can prepare a cleaner by yourself. Prepare an aqueous solution
of 0.5% NaOCl and 0.5% NaOH (or KOH).
1. Measure two vials of distilled water.
Chapter 14.2.1.
3. Measure one vial of the cleaner mentioned above and four vials of distilled
water.
measurements.
Caution:
Do not let the cleaner soak in for more than 5 minutes.
The total NaOH (or KOH) and NaOCl concentration should not exceed
1 % in the applied dilution.
72 C27IB02
14.3 Cleaning after Wort Measurements
After the last wort sample, perform an intensive cleaning procedure.
1. Rinse the measuring cells with at least 4 sample vials of warm water
(approx. 60 C).
Chapter 14.2.1.
3. Rinse the measuring cells with laboratory cleaner (see Chapter 14.1).
4. Rinse the measuring cells with 4 sample vials of distilled water and perform a
checking procedure according to Chapter 10.1.1.
5. If the checking procedure fails, clean the measuring cells (except for the pH
measuring cell!) with 1 vial filled with cleaner containing NaOCl (chlorine
bleach) and NaOH (sodium hydroxide) or KOH (potassium hydroxide)
(Chapter 14.2.4).
6. Rinse the cells with 4 vials of distilled water.
7. Fill in degassed, bi-distilled water and perform a checking procedure again
(Chapter 10.1.1).
measurements.
14.4 Maintaining the pH Electrode
(before starting the routine measurements). If necessary, perform a pH
adjustment. For details, see Chapters 9, 10.2.2 and 11.2.3.
Perform the following checking procedures once a week.
14.4.1 Maintaining the Hamilton pH Electrode
Inspect the electrode for scratches, cracks, salt crystal build-up or ceramic
diaphragms deposits.
Caution:
Do not pump in highly concentrated alcohol while wort is still in the measuring
cell. Always replace with distilled water.
C27IB02 73
Rinse off any salt build-up with distilled water.
Ceramic diaphragms: In the event of protein contamination, immerse the
electrode for several hours in 0.4% HCl + 5 g/L pepsin. If blackening of the
diaphragm is noted (due to silver compounds), immerse the electrode in
0.4% HCl + 76 g/L thiourea.
If the electrode gets dried out inadvertently for a short time, it can be placed
in storage solution overnight to regenerate it.
The life cycle of Hamilton pH electrode
The life cycle of electrodes is determined by the requirements as regards
response time, zero point and slope. Under favorable measurement conditions,
the life cycle may be 1 3 years at room temperature. Under unfavorable
conditions the life cycle can be also shorter. There is also a slight ageing factor
during storage.
Favorable conditions are:
Never let the electrode get dry out.
Never leave the electrode in distilled water or sample for a longer period of
time.
If the electrode is not in use (weekend, over night but also during the day
between the measurements) always place it in storage solution (3M KCl
solution) (see Chapter 14.2.1).
Avoid extended contact with acids, alkalis and alcohols.
14.4.2 Maintaining the Orion pH Electrode
Inspect the electrode for scratches, cracks, salt crystal build-up, or
membrane/junction deposits.
Rinse off any salt build-up with distilled water, and remove any membrane/
junction deposits as described in the Thermo Orion instruction manual.
Drain the reference chamber, flush it with fresh filling solution and refill the
chamber.
Caution:
For more detailed information on the safe use and maintenance of the pH
electrode, see the enclosed Hamilton instruction manual.
Caution:
For more detailed information on the safe use and maintenance of the pH
electrode, see the enclosed Thermo Orion instruction manual.
15 Menu Operation and Description
74 C27IB02
15.1 Menu Operation
To enter the main menu, press the key in the measuring window.
Then press the <Menu> key.
Fig. 15 - 1 Main menu
15.1.1 Operating the Soft Keys on the Instrument
Use the <> (UP) or <> (DOWN) keys to select a menu and press <> to
confirm.
To select from variable data in the submenus, use the key and
press <> to confirm.
To enter a number or a text, use the <> or <> keys and press <> to
confirm. Use the <> key to move the cursor.
<Esc> returns to the previous menu without any changes.
Confirm YES or NO with the <> key.
To return to the measuring mode, press <Esc> until the correct display
appears.
MAIN MENU
instrument settings
method settings
user functions
data memory
utilities
parameter calculator
service mode
auto sampler settings
adjustment
Information:
For an overview of the menu structure, see the menu tree in Appendix K.
C27IB02 75
15.1.2 Using an External PC Keyboard
If you often use menus in which alphanumeric inputs are required (e.g. sample
number) we recommend using an external keyboard.
1. Connect a standard German or US PS/2-PC keyboard to the keyboard plug
(PC/AT interface) at the rear of Alcolyzer Plus Beer. If necessary, use a plug
adapter from the PS/2 interface to the PC/AT interface.
2. Set the correct keyboard driver (German or US) in the menu instrument
settings > configuration.
Alphanumeric inputs (password or sample number) can be deleted using the
<del> key.
Using an external keyboard the desired numbers and letters can be entered
directly. After each input, the cursor is automatically moved to the next
position. When entering numbers the decimal point does not need to be
entered.
15.1.3 Using a Bar Code Reader
A bar code reader can be used to enter the sample identification.
The bar code reader has to be connected to the keyboard plug (PC/AT interface)
at the rear of Alcolyzer Plus Beer.
Information:
The keys <F1> to <F5> on the keyboard have the same function as the keys
<F1> to <F5> under the display of Alcolyzer Plus Beer. The cursor keys <>
and <> on the keyboard have the same function as the key on the
display of Alcolyzer Plus Beer.
Caution:
Connect the bar code reader before switching on Alcolyzer Plus Beer.
76 C27IB02
15.2 Menu Description and Function
15.2.1 "adjustment"

Fig. 15 - 2 Menu: adjustment
15.2.1.1 "adjust alcohol"
zero Zero point adjustment with water. For a
detailed description, see Chapter 11.1.1.
Do you really want to adjust?
NO Returns to menu adjustment.
YES Starts the adjustment.
known concentration Adjustment with a water/ethanol solution of
known alcohol concentration. For a detailed
description, see Chapter 11.1.2.
actual adjustment data The actual adjustment data are displayed and
can be printed out.
restore factory
adjustment
The alcohol adjustment is set to the factory
adjustment.
restore factory
adjustment?
NO Returns to menu adjustment alcohol.
YES The factory adjustment is set as actual
alcohol adjustment.
adjustment data
memory
All stored adjustment data can be displayed
and printed out.
ADJUSTMENT
adjust pH
adjust color
adjust alcohol
Only with option
pH/color
C27IB02 77
15.2.1.2 "adjust pH"
15.2.1.3 "adjust color"
automatic Automatic 2-point adjustment with integrated
buffer tables (see Chapter 11.2.3.1).
manual Manual 2-point adjustment (see Chapter
11.2.3.2).
edit buffer data New buffer tables can be entered (see
Chapter 11.2.3.3).
sort buffer data The buffer tables which shall be used for the
adjustment are selected (see Chapter
11.2.3.4).
actual adjustment data The actual measuring data of the pH
electrode as well as the last adjustment are
displayed and can be printed.
adjustment data
memory
and printed out.
zero Zero point adjustment with water. For a
detailed description, see Chapter 11.2.2.
known concentration Adjustment with a color standard of known
alcohol concentration. For a detailed
description, see Chapter 11.2.2.2.
actual adjustment data The actual adjustment data are displayed and
can be printed out.
restore factory
adjustment
The color adjustment is set to the factory
adjustment.
restore factory adjustment?
NO Returns to menu adjustment color.
YES The factory adjustment is set as actual color
adjustment.
adjustment data
memory
and printed out.
78 C27IB02
15.2.2 "instrument settings"
Fig. 15 - 3 Menu: instrument settings
configuration
calc. parameter If the density of the sample is known (to be
entered manually or transferred from a
connected DMA), the relevant sample
parameters can be calculated and the results
displayed or printed.
OIML V/V
(default)
This table is recommended for the majority of
all applications.
CU V/V If you have edited a user-defined ethanol
table (see Chapter 7.4.1), select CU V/V for
the calculations.
no No calculation of the parameter.
language The language for the printout can be
selected.
English
deutsch
Franais
Espaol
italiano
printer language The language can be selected.
English
deutsch
Franais
Espaol
italiano
country If the Alcolyzer Plus is used with the
language setting "English", the spelling
"color" or "colour" can be selected.
INSTRUMENT SETTINGS
device list
COM1
COM2
time
date
configuration
C27IB02 79
other Spelling: "color"
GB Spelling: "colour"
Ireland Spelling: "colour"
USA Spelling: "color"
keyboard type External keyboard with
German
(default)
German configuration
US US configuration.
color unit The unit for the color measurement can be
selected.
EBC
ASBC
CU User-defined color unit (see Chapter 7.4.2).
device list
filling device To activate/deactivate the communication
with a connected filling device.
no No filling device connected.
SP-1m
SF1
PFD Only used with PBA-B.
density To activate/deactivate the communication
with a connected DMA 4500/5000.
DMA
xxxx.series
not used
CO2 Only used with PBA-B: To activate/deactivate
the communication with a connected CO
2
meter.
CarboQC
not used
O2 Only used with PBA-B: To activate/deactivate
the communication with a connected O
2
meter.
OxyQC
not used
COM1 Interface configuration for the computer or
printer.
connected to
PC
printer_1
(default)
Has to be activated if the input buffer of the
printer has a high capacity (e.g. DH DP
1000). For details, refer to Chapter 5.6.1 and
the printer handbook.
80 C27IB02
printer_2 Has to be activated if the input buffer of the
printer has a low capacity (e.g. Citizen iDP-
560). Otherwise a loss of characters on the
printout may occur. For details, refer to
Chapter 5.6.1 and the printer handbook.
printer_3 If with setting "printer_1" or "printer_2" non-
defined empty rows are added in the outprint,
"printer_3" has to be activated. For details,
refer to Chapter 5.6.1 and the printer
handbook.
printer_4 If the printer has no automatic carriage
return, "printer_4" has to be activated. For
details, refer to Chapter 5.6.1 and the printer
handbook.
AP-SoftPrint For a faster data transfer when AP-SoftPrint
is used.
VisioLab For the data transfer when VisioLab for
Alcolyzer is used.
baud rate
300
600
1200
2400
4800
9600 (default)
19200
format
8 bit no
8 bit even
7 bit even
(default)
COM2 If a peripheral is activated at COM1, this
menu cannot be edited and "connected to:
PIB" is displayed.
connected to
printer has a high capacity (e.g. DH DP
1000). For details, refer to Chapter 5.6.1 and
the printer handbook.
printer has a low capacity (e.g. Citizen iDP-
560). Otherwise a loss of characters on the
printout may occur. For details, refer to
Chapter 5.6.1 and the printer handbook.
C27IB02 81
printer_3 If with setting "printer_1" or "printer_2" non-
defined empty rows are added in the outprint,
"printer_3" has to be activated. For details,
refer to Chapter 5.6.1 and the printer
handbook.
printer_4 If the printer has no automatic carriage
return, "printer_4" has to be activated. For
details, refer to Chapter 5.6.1 and the printer
handbook.
AP-SoftPrint For a faster data transfer when AP-SoftPrint
is used.
baud rate
300
600
1200
2400
4800
9600 (default)
19200
format
8 bit no
8 bit even
(default)
7 bit even
time Setting the time.
time
HH:DD
date Setting the date.
date
YYYY-MM-DD Year-Month-Day.
format Date format.
YYYY-MM-DD
(default)
DD.MM.YYYY
MM/DD/YYYY
sample filling unit This menu is only available if an SF-1 sample
filling unit is built-in. The parameters for the
sample filling unit SF-1 can be entered in this
menu.
filling time Time for filling the sample into the measuring
cell.
xxx sec.
filling type
forward
82 C27IB02
15.2.3 "method settings"
Fig. 15 - 4 Menu: method settings
for/backward If for/backward is selected the rotation
direction of the pump changes 3 times,
otherwise it moves forward.
turn on delay Time between pressing the <Start> key and
starting the rotation of the pump.
no. 1: BEER
no. 2:CIDER
no. 3: SOFT DRINK
no. 4: WASH
no. 5: MOLASSES
no. 6: new method
name Enter method name.
type Enter type of sample to be measured (BEER,
CIDER, SOFT DRINK, WASH or
MOLASSES).
offset Enter a product-specific offset in alcohol
%V/V.
pH-deg. offset Enter a pH-offset between -0.99 and +0.99.
protocol no.: Selection of the printer protocol (1-10) to be
used (see Chapter 8.2).
residual CO2: Only used in combination with a PBA-B to
enter the residual CO
2
content after
degassing.

no. 10: new method
name Enter method name.
METHOD SETTINGS
no. 1
no. 2
no. 3
no. 4
no. 5
no. 6
no. 7
no. 8
no. 9
no. 10
:
:
:
:
:
:
:
:
:
:
BEER
CIDER
SOFT DRINK
WASH
new method
MOLASSES
C27IB02 83
15.2.4 "user functions"
15.2.5 "data memory"
type Enter type of sample to be measured (BEER,
CIDER, SOFT DRINK, WASH or
MOLASSES).
offset Enter a product-specific offset in alcohol
%V/V.
pH-deg. offset Enter a pH-offset between -0.99 and +0.99.
protocol no.: Selection of the printer protocol (1-10) to be
used (see Chapter 8.2).
residual CO2: Only used in combination with a PBA-B to
enter the residual CO
2
content after
degassing.
user defined ethanol
table
Polynomial coefficients based on a user-
defined ethanol table can be entered to be
used for the parameter calculation (see
Chapter 7.4.1).
user defined color unit An offset and a slope can be defined if a color
measurement is used that differs from EBC
or ASBC (see Chapter 7.4.2).
browser To browse the stored data sets (see Chapter
13).
Each data set can be displayed and printed
out separately. The key displays the
oldest data set, the key displays the
newest data set. The key is used to
switch from the previous displayed data set to
the next one.
clear memory To delete all data sets (see Chapter 13).
really clear data memory?
YES
NO
84 C27IB02
15.2.6 "utilities"
Fig. 15 - 5 Menu: utilities
modify password The whole menu area can be protected from
unauthorized changes by using the password
function. For a detailed description, see
Chapter 15.3.
new password Input a password up to 10 digits long. The
password can be deleted by leaving the line
blank and pressing the <> key.
verify Enter the password again (control). The
password can be deleted by leaving the line
blank and pressing the <> key.
status Indicates whether the password is saved or
deleted.
sample identification Sets the type of sample identification to be
used.
SF1, PFD
text+number The sample identification consists of text -
consecutive number - text. The text before
and after the number can be up to 8 digits
long. The consecutive number is set once at
the start and is then increased by one
automatically at the beginning of each new
measurement.
text Sample identification using a text. The text
can be 20 digits long.
SP-1m
text+number See under SF1, PFD
text See under SF1, PFD
UTILITIES
sample identification
display configuration
output configuration
SOP configuration
default settings
firmware update
print configuration
modify password
C27IB02 85
list This menu is only available if a sample
changer is connected and activated. A list of
24 individually selected numbers or texts can
be entered (see Chapter 12.1.3). Each
position of the sample changer magazine is
linked with a unique number or text from the
list.
#+list This menu is only available if a sample
changer is connected and activated. A list of
24 individually selected numbers or texts can
be entered (see Chapter 12.1.3). Each
position of the sample changer magazine is
linked with a unique number or text from the
list. Additionally, the position number of the
sample changer vessel appears in front of the
sample identification.
SP-1m
manual new list The sample list has to be deleted manually.
auto. new list The sample list is automatically deleted when
the sample changer reaches the zero position
after the end of a measurement cycle.
display configuration At the end of the measurement, parameters
can be calculated and displayed. There are 4
lines available to display the calculated
parameters. In this menu, each line can be
allocated a parameter.
1: alcohol [%m/m]
2: p (original extract) [%Plato]
3: Er (real extract) [%m/m]
4: Ea (apparent extract) [%m/m]
5: ADF (m/m) (app. deg. of ferm.) [%]
output configuration In this menu the configuration of the printout
or protocol on the PC can be defined.
printer protocol
protocol no.: 1 (...
10)
10 different printer protocols can be defined
and assigned to different measuring
methods.
head 9 lines can be defined to print different
parameters. To each line one of the
parameters below can be assigned.
date (default)
time (default)
sample no. (default)
method
offset
86 C27IB02
temp. Alcolyzer
no
empty row
line
serial no.
parameter A maximum of 52 lines can be defined to print
different parameters. To each line one of the
parameters below can be assigned.
alcohol [%V/V]
alcohol cond.
density [g/cm
3
]
density cond.
pH (default)
pH cond.
color [EBC], [ASBC] or [CU] (default)
color cond.
alcohol (DMA) Alcohol content of a binary solution that has
been measured by the density meter. This
value is used to adjust the Alcolyzer Plus
(see Appendix E). The appropriate alcohol
table must be activated in the third line of the
DMA memory.
alcohol [%m/m]
(default)
Alcohol content in percentage by weight.
SG 20/04 Specific gravity of the sample.
SG 20/20
(default)
Specific gravity of the sample.
ASG Apparent specific gravity of the sample.
App.Density Apparent density of the sample.
SG alcohol Specific gravity of the alcohol.
SG extract Specific gravity of the extract.
Er [%m/m]
(default)
Real extract in [%m/m].
Er [g/100mL] Real extract in [g/100 mL].
Ea [%m/m]
(default)
Apparent extract in [%m/m].
Ea [g/100mL] Apparent extract in [g/100 mL].
p [%Plato]
(default)
Original extract in [%Plato].
p [g/100mL] Original extract in [g/100 mL].
RDF [%]
(default)
Real degree of fermentation in [%].
RDF (St) Real degree of fermentation in [%] according
to the standard formula.
C27IB02 87
RDF (US) Real degree of fermentation in [%] according
to the US formula.
ADF (m/m) [%]
(default)
Apparent degree of fermentation in [%] based
on %m/m.
ADF (g/100mL)
[%]
on g/100 mL.
Calories (S)
[kcal/kg]
Calories according to the Steiner formula in
[kcal/kg].
Calories [kcal/
kg]
Calories in [kcal/kg].
Calories [kcal/
100mL]
Calories in [kcal/100 mL].
Calories [kJ/
100mL] (default)
Calories in [kJ/100 mL].
Calories [kcal/
12oz]
Calories in [kcal/12oz].
PG Present gravity.
OG-BMP Original gravity according to the BMP
formula.
OG Original gravity.
SI Spirit indication.
EG Extract gravity.
DL Degrees lost.
Ratio E/A Ratio extract/alcohol.
alcohol-ASBC
[%m/m]
Alcohol content according to the ASBC
regulations in percentage by weight.
alcohol-IUPAC
[%m/m]
Alcohol content according to the IUPAC
Brix [Brix] Saccharose concentration in percentage by
weight. Only valid for measurements of
alcohol-free beverages in combination with
the "SOFT DRINK" method.
DMAxxxx #1 Any parameter which is activated at the 4th
position in the memory configuration of the
DMA 4500/5000.
DMA 4500/5000.
data memory A maximum of 15 parameters can be
activated and are stored in the memory.
alcohol [%V/V]
(default)
Alcohol content in percentage by volume.
condition alcohol Measuring status of the alcohol
measurement (e.g. "valid").
88 C27IB02
density [g/cm
3
]
(default)
True density measured by the connected
DMA.
condition density Measuring status of the density
measurement (e.g. "valid").
pH (default) pH value of the sample.
condition pH Measuring status of the pH measurement
(e.g. "valid").
color [EBC], [ASBC]
or [CU] (default)
Measuring result of the color measurement.
condition color Measuring status of the color measurement
(e.g. "valid").
alcohol [%m/m]
(default)
Alcohol content in percentage by weight.
alcohol (DMA) Alcohol content of a binary solution that has
been measured by the density meter. This
value is used to adjust the Alcolyzer Plus
(see Appendix E). The appropriate alcohol
table must be activated in the third line of the
DMA memory.
ASG Apparent specific gravity of the sample.
App.Density Apparent density of the sample.
SG alcohol Specific gravity of the alcohol.
SG extract Specific gravity of the extract.
Er [%m/m] (default) Real extract in [%m/m].
Er [g/100mL] Real extract in [g/100 mL].
Ea [%m/m] (default) Apparent extract in [%m/m].
Ea [g/100mL] Apparent extract in [g/100 mL].
p [%Plato] (default) Original extract in [%Plato].
p [g/100mL] Original extract in [g/100 mL].
RDF [%] (default) Real degree of fermentation in [%].
RDF (St) [%] Real degree of fermentation in [%] according
to the standard formula.
RDF (US) [%] Real degree of fermentation in [%] according
to the US formula.
ADF (m/m) [%]
(default)
on %m/m.
ADF (g/100mL) [%] Apparent degree of fermentation in [%] based
on g/100 mL.
Calories (S) [kcal/
kg]
Calories according to the Steiner formula in
[kcal/kg].
Calories [kcal/kg] Calories in [kcal/kg].
Calories [kcal/
100mL]
Calories in [kcal/100 mL].
C27IB02 89
Calories [kJ/100mL] Calories in [kJ/100 mL].
Calories [kcal/12oz] Calories in [kcal/12oz].
PG Present gravity.
OG-BMP Original gravity according to the BMP
formula.
OG Original gravity.
SI Spirit indication.
EG Extract gravity.
DL Degrees lost.
ratio E/A Ratio extract/alcohol.
alcohol - ASBC
[%m/m]
Alcohol content according to the ASBC
alcohol - IUPAC
[%m/m]
Alcohol content according to the IUPAC
Brix [Brix] Saccharose concentration in percentage by
weight. Only valid for measurements of
alcohol-free beverages in combination with
the "SOFT DRINK" method.
DMA 4500/5000.
DMA 4500/5000.
no
Information:
As soon as the memory configuration of the DMA has been changed, the data
memory of the Alcolyzer Plus is deleted ("DMA memory configuration
changed, data memory erased").
SOP configuration
SOP #1 Editing the SOP #1: The following measuring
parameters can be selected: water, alcohol,
color, pH 1, pH 2.
1: water
2: alcohol
3: pH 1
4: pH 2
5: ... 10: not
used
Not used, water, alcohol, color, pH 1 or pH 2
can be selected.
SOP #2 Editing the SOP #2: The following measuring
parameters can be selected: water, alcohol,
color, pH 1, pH 2.
90 C27IB02
15.2.7 "parameter calculator"
Fig. 15 - 6 Menu: parameter calculator
The "parameter calculator" function calculates relevant sample parameters from
the alcohol concentration and density value. The parameters can be printed or
transferred to a PC afterwards.
1: water
2: alcohol
3: ... 10: not
used
Not used, water, alcohol, color, pH 1 or pH 2
can be selected.
print configuration The instrument configuration is printed. This
menu is only available if a printer is
connected.
really print configuration?
NO
YES
default settings
really restore default settings?
NO Returns to menu utilities.
YES Selecting this function sets all instrument
settings to default values.
firmware update
really update firmware?
NO Returns to menu utilities.
YES The firmware update mode is started. (See
Chapter 15.4).
alcohol = Enter the alcohol content in %V/V.
density = Enter the density value in g/cm
3
.
PARAMETER CALCULATOR
alcohol
SG 20/04
SG 20/20
ASG
App. Density
SG alcohol
: 3.83 %m/m
: 1.00545
: 1.00723
: 1.00724
: 1.00438 g/cm3
: 0.99300
alcohol
density
= 04.88 %V/V
= 1.005420 g/cm3
C27IB02 91
The different beer parameters are calculated automatically.
15.2.8 "service mode"
In the service mode, the actual raw data of the measuring parameters alcohol and
color can be displayed and printed. This is of great importance for service
technicians checking for possible errors.
Fig. 15 - 7 Menu: service mode
By pressing the key, a password protected area is reached which is
only accessible to service technicians.
15.2.9 "auto sampler settings"
This menu is only available if a sample changer is connected and activated
in the menu instrument settings > device list.
To set the sample changer parameter, see the SP-1m instruction manual.
15.3 Entering and Changing a Password
The whole menu can be protected against unauthorized changes by using a
password.
Information:
The printout of the calculated parameters is defined by the activated method
(and the corresponding printer protocol).
valid
SERVICE MODE
c
S1
S2
S3
S4
= 3.77 %V/V
= 0.333663 V
= 0.345410 V
= 0.358604 V
= 0.362236 V
valid
pH
c
S1
= 4.83 pH / 0.1307 V / 25.75 C
= 49.02 EBC
= 0.069221 V
Information:
We recommend setting the following parameters:
- Without option pH/color: 1080
- With option pH/color: 1100
92 C27IB02
The password can be up to 10 digits long. Lower and upper case letters can
be used as well as numbers (a to z, A to Z, 0 to 9). Special characters are not
permitted.
Entering a new password
1. Enter the password in the menu utilities > modify password > new
password and confirm with <>.
2. Enter the password in the "verify" line.
3. Press <> to conclude this procedure.
If the password in the "new password" line is identical to the password in the
"verify" line, "status: saved" is displayed, otherwise "status: wrong".
Deleting a password
1. If the menu is protected by a password, this password has to be entered for
security reasons.
2. In line "new password", press the <> key without entering a password.
3. In line "verify", press the <> key without entering a password.
"status: deleted" is displayed.
15.4 Installing a New Firmware Version
A new firmware version can be loaded from the computer to the Alcolyzer Plus
via serial interface COM1. Detailed information is supplied with the firmware.
Information:
If you have forgotten your password, contact your local Anton Paar
representative.
16 Calculations
C27IB02 93
16 Calculations
All calculations are valid for 20C.
1. alcohol %V/V = alcohol content in percentage by volume
Alcohol %V/V is calculated using a specific function of the absorption
intensity of the NIR line of alcohol. The result is valid for 20C.
2. alcohol [%m/m] = alcohol content in percentage by weight
3. SG 20/04 = specific gravity of the sample
The sample density is either transferred from a connected density meter or
entered manually.
4. SG 20/20 = specific gravity of the sample
The sample density is either transferred from a connected density meter or
entered manually.
5. ASG = apparent specific gravity of the sample
6. App.Density = Apparent Density of the sample
7. SG alcohol = specific gravity of the alcohol
alcohol %m/m
alcohol %V/V
100% alcohol
sample
---------------------------------------------------------------------------- =
100%alcohol, (20 C)
0.78924 g/cm
3
=
SG 20/04

sample
water
4 C
------------------------
20 C
water, 4 C
0.999972 g/cm
3
= ( ) =
SG 20/20

sample
water
20 C
---------------------------
20 C
water, 20 C
0.998204 g/cm
3
= ( ) =
ASG
SG 20/04 0.0012
0.99703
------------------------------------------------- =
App.Density
8
sample, 20 C

air, 20 C
( )
8
air, 20 C
----------------------------------------------------------------------------- =
SG
alcohol

alcohol
water
------------------ =
16 Calculations
94 C27IB02
8. SG extract = specific gravity of the extract
The extract density is calculated according to the Tabari formula.
9. Er = real extract in [%m/m]
The real extract in %m/m is calculated from the extract density determined
by the Tabari formula using the Plato table.
10. Er = real extract in [g/100mL]
The real extract in mixed percent g/100mL is determined by:
11. Ea = apparent extract in [%m/m]
The apparent extract in % m/m is calculated from the sample using the Plato
table.
12. Ea = apparent extract in [g/100mL]]
The apparent extract in mixed percent g/100mL is determined by:
13. p = original extract in [%Plato]
14. p = original extract in [g/100mL]]
15. RDF = real degree of fermentation in [%]
16. RDF (St) = real degree of fermentation in [%] according to the standard
formula
SG
extract

extract
water
----------------- =
Er
wv
Er
ww
SG20/04 (Er
ww
) =
Ea
wv
Ea
ww
SG20/04 (Ea
ww
) =
p
ww alcohol %m/m 2.0665 Er + ( ) 100 [ ]
100 alcohol %m/m 1.0665 + ( )
---------------------------------------------------------------------------------------------------- =
p
wv
p
ww
SG20/04 (p
ww
) =
RDF
2.0665 alcohol %m/m
2.0665 alcohol %m/m Er +
--------------------------------------------------------------------------

100 =
RDF
p
ww
Er
p
ww
----------------------

100 =
16 Calculations
C27IB02 95
17. RDF (US) = real degree of fermentation in [%] according to the US
formula
18. ADF (m/m) = apparent degree of fermentation in [%] based on (%m/m)
19. ADF (g/100mL) = apparent degree of fermentation in [%]
based on g/100mL
20. Calories (S) = calories according to the Steiner formula in [kcal/kg]
21. Calories = calories in [kcal/kg]
22. Calories = calories in [kcal/100mL]
23. Calories = calories in [kJ/100mL]
24. Calories = calories in [kcal/12oz]
25. PG = present gravity
26. OG-BMP = original gravity according to the BMP formula
RDF
100 p
ww
Er ( )
p
ww
-------------------------------------------

1
1 0.005161 Er ( )
---------------------------------------------------

=
ADF
p
ww
Ea
p
ww
-----------------------

100 =
ADF
p
wv
Ea
p
wv
----------------------

100 =
kcal/kg (S) p
ww
36.4 =
kcal/kg 3.5 Er 7 alcohol %m/m + ( ) 10 =
kcal/100ml 3.5 Er 7 alcohol %m/m + ( )
sample
=
kJ/100ml 15 Er 29 alcohol %m/m + ( )
sample
=
kcal/12oz 6.9 alcohol %m/m 4 Er ( 0.11) + + [ ] SG
sample
3.55 =
PG SG
sample
1 ( ) 1000 =
OG-BMP p
ww
3.86098 p
ww
0.01435427 + ( ) =
16 Calculations
96 C27IB02
27. OG = original gravity according to the standard formula
28. SI = spirit indication
29. EG = extract gravity
30. DL = degrees lost
31. ratio E/A = ratio extract/alcohol
32. alcohol-ASBC = alcohol content according to the ASBC regulations in
percentage by weight [%m/m]
33. alcohol-IUPAC = alcohol content according to the IUPAC regulations in
percentage by weight [%m/m]
34. Color measurement: Conversion from EBC into ASBC
A0 =
A1 =
A2 =
A3 =
A4 =
A5 =
0.0080
4.30003
-2.048839E-1
1.8090493E-1
-7.3330484E-2
1.7587605E-2
A6 =
A7 =
A8 =
A9 =
A10=
-2.59916898E-3
2.374003555E-4
1.301128748E-5
3.91622006E-7
-4.973568E-9
OG EG DL + =
SI 1 SG
alcohol
( ) 1000 =
EG SG
extract
1 ( ) 1000 =
DL A
n
n = 0
10
SI ( )
n
=
ratio E/A
Er
alcohol %m/m
------------------------------------- =
alcohol-ASBC
alcohol %V/V
100 % alcohol
sample
--------------------------------------------------------------------------- =
alcohol-IUPAC
alcohol %V/V
100 % alcohol
sample
--------------------------------------------------------------------------- =
1 EBC 0.508 ASBC =
17 Filling Samples with the SF-1 Sample Filling Unit
C27IB02 97
17 Filling Samples with the SF-1 Sample
Filling Unit
Beside the standard filling procedure using the sample changer SP-1m, Alcolyzer
Plus Beer can also be filled using the integrated sample filling unit SF-1.
The SF-1 sample filling unit is an option for the Anton Paar Alcolyzer Plus.
The SF-1 sample filling unit fills the samples from a sample vial into the measuring
cells. After the measurement has been performed, the next sample is filled in
order to replace the previous one.
Fig. 17 - 1 Sample filling unit SF-1
Appendix A: Degassing Beer Samples
98 C27IB02
Appendix A: Degassing Beer Samples
Degas the beer samples according to the MEBAK-regulations
1
as follows:
1. Fill a 1 L glass flask one third full with beer.
The beer temperature should be between 20C and 25C.
2. Seal the flask with a glass stopper.
3. Shake the flask and release the pressure until there is no more built-up
pressure.
4. Filter the degassed beer through a folded paper filter and cover the funnel
with a watch glass immediately.
5. Fill the filtered beer into glass containers and seal them or analyze them
immediately.
6. Make sure that the sample containers are sealed and kept at a temperature
of approximately 20 C before using.
7. Before filling the samples into the vials of the sample changer, swirl the beer
gently.
This is to bring back any condensations of alcohol into the solution.
1. Literature: Brautechnische Analysenmethoden, Bd. 2. Methodensammlung der
Mitteleuropischen Brautechnischen Analysenkommission (MEBAK). 2. Auflage, 1987.
Selbstverlag der MEBAK, D-8050 Freising-Weihenstephan. p 75.
Information:
Do not use any anti-foaming agent!
Appendix B: Available Parameters
C27IB02 99
B.1 Method Parameters
When you select output parameters for display, printer and data memory, you get
a list of the available parameters.
The table shows which parameters can be used for the 5 predefined methods
("X"... the parameter is available for this method).
Table B.1: List of available parameters
Parameter Method
BEER CIDER SOFT DRINK WASH MOLASSES
no X X X X X
empty row X X X X X
line X X X X X
alcohol X X X X
alcohol cond X X X X
density X X X X X
density degassed (only for PBA-B) X X X X X
density cond X X X X X
alcohol /DMA X X X X
pH X X X X X
pH degassed (only for PBA-B) X X X X X
pH cond X X X X X
color X X X X X
color cond X X X X X
alcohol [%m/m] X X X X
SG 20/04 (spec. gravity) X X X X X
SG 20/20 (spec. gravity) X X X X X
Apparent SG 20/20 X X X X X
Apparent Density X X X X X
SG alcohol (spec. gravity) X X X X
SG extract (spec. gravity) X X X X
Er (real extract) [%m/m] X X X X
Er (real extract) [g/100mL] X X X X
Ea (apparent extract) [%m/m] X X X X
Ea (apparent extract) [g/100mL] X X X X
p (original extract) [%Plato] X X X
p (original extract) [g/100mL] X X X
RDF (real deg. of ferm.) [%] X X X
RDF-St (real deg. of ferm.) [%] X X X
100 C27IB02
RDF-US (real deg. of ferm.) [%] X X X
ADF (m/m) (app. deg. of ferm.) [%] X X X
ADF (g/100mL) (app. deg. of ferm.)
[%]
X X X
Calories (Steiner) [kcal/kg] X
Calories [kcal/kg] X
Calories [kcal/100mL] X
Calories [kJ/100mL] X
Calories [kcal/12oz] X
PG (present gravity) X X X
OG BMP (original gravity) X X X
OG (original gravity) X X X
SI (spirit indication) X X X
EG (extract gravity) X X X
DL (degrees lost) X X X
Ratio E/A (US) X X X
alcohol ASBC [%m/m] X X X
alcohol IUPAC [%m/m] X X X
Brix [Brix] X X
DMA xxxx#1 X X X X X
DMA xxxx#2 X X X X X
CQC CO2 (only for PBA-B) X X X X X
CQC air (only for PBA-B) X X X X X
CQC cond (only for PBA-B) X X X X X
CQC method (only for PBA-B) X X X X X
OQC O2 (only for PBA-B) X X X X X
OQC temp (only for PBA-B) X X X X X
Table B.1: List of available parameters
Parameter Method
BEER CIDER SOFT DRINK WASH MOLASSES
C27IB02 101
B.2 Printer Protocol Parameters
Table B.2: List of preset parameters of the printer protocols no. 6 to 9
Preset parameters Protocol no. 6
BEER
Protocol no. 7
CIDER
Protocol no. 8
WASH,
MOLASSES
Protocol no. 9
SOFT DRINK
date X X X X
time X X X X
sample no. X X X X
method X X X X
alcohol X X X
pH X X X X
color X X X X
alcohol [%m/m] X X X
SG 20/20 (spec. gravity) X X
Er (real extract) [%m/m] X X
Ea (apparent extract)
[%m/m]
X X
p (original extract) [%Plato] X X
RDF (real degree of
fermentation) [%]
X X
ADF (m/m) (apparent
degree of fermentation) [%]
X X
Calories [kJ/100ml] X X
Brix [Brix] X
pH degassed (only for
PBA-B)
X X X X
CQC CO2 (only for PBA-B) X X X X
OQC O2 (only for PBA-B) X X X X
Appendix C: Status and Error Messages
102 C27IB02
C.1 Status/Error Messages for the Alcohol
Measurement
Status message Meaning
stopped No measurement is carried out at the moment.
attemperating The measuring temperature is not yet stable (|t
actual

t
set
| > 0.02C).
measuring A measurement is performed.
predetermined The displayed value is 99 % equivalent to the final
measuring result.
valid The measuring result is valid.
invalid Invalid measuring result. An error message is
displayed.
Error message Meaning
no sample There is no sample in the measuring cell.
no adjustment No adjustment has been saved.
low value The measuring result is < -0.5%vol.
high value The measuring result is > 30%vol.
ADC out of range The input voltage of the AD converter is too high
(maybe there is no communication with the signal
processor DSP).
temp. error Error in the temperature sensor.
unknown Unknown condition.
time out The measurement has not been finished within 6
minutes (default).
ERROR:
WRONG SAMPLE
Error message for the adjustment:
The alcohol concentration of the sample is outside the
permissible range.
C27IB02 103
C.2 Status/Error Messages for the Color
Measurement
C.3 Status/Error Messages for the pH Measurement
measuring result.
displayed.
low value The measuring result is < -0.5 EBC (-0.25 ASBC).
high value The measuring result is > 130 EBC (66 ASBC).
minutes (default).
sample turbid Turbid sample.
ERROR:
WRONG SAMPLE
Error message for the adjustment:
The color concentration of the sample is outside the
permissible range.
measuring result.
displayed.
low value The voltage of the pH electrode is > 0.386V.
high value The voltage of the pH electrode is < -0.278V.
temp. error Error in the temperature sensor.
sensor error The pH electrode is defective or not connected.
minutes (default).
104 C27IB02
C.4 System Error Messages
C.5 Other Messages
Error messages for the adjustment
no buffer saved No buffer was found during the automatic adjustment.
slope out of range The slope is outside the permissible range
(-56.2 to -62.1mV).
offset out of range The zero point is outside the permissible range
(30mV).
buffer distance The distance between the buffers is < 1.5pH.
*** no factory adjustment *** The factory adjustment is missing.
no answer There was no answer during the automatic
identification of the DMA or sample changer.
error The RAM test failed.
set to default The configuration was reset during the start-
up procedure.
critical system ERROR The DSP could not be initialized.
incorrect firmware type Incorrect DIP switch configuration.
not processed The DMA is off line, the measurement could
not be carried out.
Appendix D: Technical Data
C27IB02 105
Appendix D: Technical Data
Measuring range:
Alcohol:
pH:
Color:
0 to 12 %V/V
0 to 14
0 to 120 EBC (0 to 60.96 ASBC)
Repeatability, s.d.:
Alcohol:
pH:
Color:
0.01 %V/V
0.02 (in a pH range from 3 to 7)
0.1 EBC (0.05 ASBC)
Temperature control: Built-in solid state thermostat (Peltier)
Repeatability, s.d.: 0.01C
Environmental conditions: For indoor use only
Ambient temperature: +15 to 32C (59 to 89.6F)
Air humidity: non-condensing,
20C < 90% relative humidity
Pollution degree: 2
Overvoltage category: II
Minimum sample volume: 30 mL
Typical measuring time per
sample: 4 minutes (incl. filling)
Dimensions (L x W x H): 420 x 280 x 210 mm
(16.5 x 11.8 x 8.3 inches)
Weight: 12.4 kg (26 lbs)
Power supply: AC 100 to 240 V, 50 to 60 Hz
Power consumption: 50VA
Serial interface (COM1): RS 232 C;
300 to 19200 Baud;
7 Bit Even Parity;
8 Bit No Parity and
8 Bit Even Parity
Serial interface (COM2): RS 232 C;
300 to 19200 Baud;
7 Bit Even Parity;
8 Bit No Parity and
8 Bit Even Parity
Appendix E: Interface Commands for Communication PC and Alcolyzer Plus Beer
106 C27IB02
Appendix E: Interface Commands for
Communication PC and
Alcolyzer Plus Beer
Measurement data stored in the memory can be transferred to a PC via the
serial interface COM1. In addition, a limited remote control of the Alcolyzer
Plus is possible.
Connect the Alcolyzer Plus interface COM1 to the PC interface RS 232 C
using an appropriate interface cable.
Synchronize the interface settings of the Alcolyzer Plus and the PC (see
Chapter 7.3).
The communication can be tested using a simple interface program, e.g.
Windows Terminal, Procomm or Hyper Terminal.
Lower and upper case letters are permitted.
If an unknown command is sent from the PC, the Alcolyzer Plus answers
with "?".
PC Alcolyzer Plus Meaning
get config serial no. : 00827195
firmware version : 5.02.09
firmware date : Mar 06 2009
firmware type : beer
boot version : 4.01
temperature : 20 C
density meter : DMA4500 v5.017.a
filling device : no
calc. parameter : OIML V/V
language : English
print language : English
country : other
color unit : EBC
keyboard : US
Com1 type : PC
Com1 baud rate : 9600
Com1 format : 8bit No
Com2 type : PIB
Com2 baud rate : 9600
Com2 format : 8bit No
Alcolyzer Plus Beer configuration.
get data head head;YYYY-MM-DD;hh:mm:ss;sample
number;method;offset;ready;alcohol;
density;pH;Er;Ea;p;RDF
Response, if items are selected, e.g.
factory default method BEER.
get data unit unit;;;;;%V/V;g/cm3;;;;%m/m;%m/m;
%Plato ;%
The units of the selected items are
transferred.
Appendix E: Interface Commands for Communication PC and Alcolyzer Plus Beer
C27IB02 107
To make the connection to a LIMS system easier, a binary number is sent
from the Alcolyzer Plus together with the data. This number indicates the
validity or invalidity of the results of alcohol, density, pH and color.
The table below shows the binary numbers that can be sent by the Alcolyzer
Plus and the corresponding numbers in the PC data record at the "ready"
position.
Examples:
The binary number 0111 indicates: color value is not valid, alcohol, density
and pH are valid. The "ready" position in the PC data record shows the
number 7.
The binary number 1010 indicates: pH and alcohol are not valid, color and
density are valid. The "ready" position in the PC data record shows the
number 10.
get data data;2007-04-04;07:18:08;Beer;01-
BEER;0.00;7;4.49;1.00745;5.17;4.017;
2.377;10.882;64.42
or
Alcolyzer no new data
Transfer of any available data.
reset data OK Resets read data, e.g. for a second
data transfer.
PC Alcolyzer Plus Meaning
X
a
X X X
a. X = 1 .... valid
X = 0 .... not valid
Alcohol
Density (DMA)
pH
Color
Binary code Data record number Binary code Data record number
0000 0 1000 8
0001 1 1001 9
0010 2 1010 10
0011 3 1011 11
0100 4 1100 12
0101 5 1101 13
0110 6 1110 14
0111 7 1111 15
Appendix F: Configuration for Communication between DMA and Alcolyzer Plus Beer
108 C27IB02
Appendix F: Configuration for
Communication between
DMA and Alcolyzer Plus
Beer
1. Connect the Alcolyzer Plus Beer interface COM2 to the DMA 4500/5000
interface COM1 using the appropriate interface cable, Mat. No. 2359.
2. Configure the DMA 4500/5000 as follows:
a) Manual configuration:
Select the method "OIML v/v" using the <Method> soft key.
If the measuring system will be adjusted according to other alcohol tables
(see Chapter 7.4.1), the DMA 4500/5000 has to be configured accordingly.
Select the menu instrument settings > computer interface configuration
and set as follows:
Select the menu method settings > memory configuration > edit
configuration and set as follows:
Select the menu method settings > memory configuration > memory
mode and set as follows:
Select the menu measurement settings and set as follows:
line delimiter: <CR>
data delimiter: , (comma)
handshake: none
data bits: 8
stop bits: 1
parity: No
baud rate: 9600
Y actual cell temperature (C)
Y density
Y OIML (%vol)
a
a. If the measuring system will be adjusted according to other alcohol tables (see
Chapter 7.4.1), the corresponding table has to be activated.
N condition
mode: measurement valid (after start)
Appendix F: Configuration for Communication between DMA and Alcolyzer Plus Beer
C27IB02 109
b) Configuration of the DMA 4500/5000 using the backup card
DMA 4500/5000 can be set up for communication with Alcolyzer Plus Beer
using the backup card Mat. No. 23913 for DMA 4500/5000 V4.xxx and
higher.
Switch off DMA 4500/5000.
Slot the backup card into the memory card drive at the back of the
instrument.
Switch on DMA 4500/5000.
Pressing the key <Restore all> automatically loads all the required
presettings into the DMA. The preconfigured method is called "Alcolyzer
Plus".
Detailed instructions on using the backup card are included with the card
itself.
pump switch off mode: time
pump switch off time: 900 seconds
Appendix G: Firmware Versions
110 C27IB02
Appendix G:Firmware Versions
Firmware
version
Date of
release
Document
number
Comments
V4.00 25.03.2003 C27IB02A First released firmware.
V4.01 26.08.2003 C27IB02B The adjustments for color and alcohol can be reset to
the factory adjustment in the menu adjustment.
The concentration of the color standard for the
adjustment can be between 1.00 and 60.00 EBC (0.50
to 30.48 ASBC).
Color values can be reported in case of turbid samples.
V4.01.01 16.09.2003 C27IB02C SOP Error (color (ASBC): known concentration)
corrected.
Color measurement is possible up to 130 EBC (66
ASBC).
V4.01.02 01.12.2003 C27IB02D Setting up a new method: Error after entering an offset
corrected.
For the color measurement, only a zero point
adjustment is necessary.
"No factory adjustment" is not shown anymore if no
color board is built in.
V4.01.03 20.07.2004 C27IB02E The selected table for parameter calculation is not set to
the default table "OIML vol" after switching off and on.
The selected sample identification is not set to default
after switching off and on.
The air pump is switched off automatically when an SF-
1 is used.
V4.01.04 02.03.2005 C27IB02F Recognition of stored buffer table during the pH
adjustment with SOP and automatic pH adjustment
improved.
V4.01.05 02.08.2005 C27IB02G Allows 8-digit serial number to be keyed in.
V5.00 14.12.2005 C27IB02H First released firmware for PBA-B
Anton Paar interface bus (PIB) for PBA-B realized with
the menu device list
Improved pH adjustment and measurement
Automatic deleting of the sample list at the end of a
measuring cycle possible
Compatible to "VisioLab for Alcolyzer"
Appendix G: Firmware Versions
C27IB02 111
V5.01 11.04.2007 C27IB02I
C27IB02J
C27IB02K
New method "WASH"
Slightly modified menu structure
New menu user functions
A user defined ethanol table can be entered to be
used for the parameter calculation
Parameter calculation based on OIML m/m or Kaempf is
no longer available
Only the method-relevant parameters for the currently
used method are printed
After conclusion of the zero point adjustment for alcohol,
the deviation of the signal (compared to the factory
adjustment) is displayed: information about the
condition of the cell or LED
An empty sample list automatically uses the currently
activated method as default method
Measuring data from OxyQC can be received,
displayed, printed and stored (only PBA-B)
Not compatible with VisioLab for Alcolyzer, version 1.10
V5.02.05 14.03.2008 C27IB02L COM settings: additional printer type selectable
(printer_4)
Pre-configured printer protocols for the methods BEER,
CIDER, SOFT DRINK and WASH
After conclusion of the zero point adjustment for color,
the deviation of the signal (compared to the factory
adjustment) is displayed: information about the
condition of the cell or LED
Compatible with VisioLab for Alcolyzer, version 1.20
V5.02.09 06.03.2009 C27IB02M For all measuring methods, you can enter a pH-offset
between -0.99 and +0.99.
Measuring method CIDER: You can enter the "residual
CO2" content.
SF-1 filling unit: a "turn on delay" can be entered.
New method MOLASSES is available.
Firmware
version
Date of
release
Document
number
Comments
Appendix H: Wetted Parts
112 C27IB02
Appendix H: Wetted Parts
Material Part
Stainless Steel DIN 1.4571/SS 316Ti Measuring cell
PTFE Filling adapter
Glass B270 Measuring window
Silicone Hose
TYGON Hose
PSU (Polysulfone) pH measuring cell
EPDM (Ethylene/propylene diene
Terpolymer)
Sealing ring
Appendix I: Material Safety Data Sheet for Tartrazine
C27IB02 113
Appendix I: Material Safety Data Sheet
for Tartrazine
Appendix I: Material Safety Data Sheet for Tartrazine
114 C27IB02
Appendix J: Density/Concentration Table for Binary Aqueous Ethanol Solutions
C27IB02 115
Appendix J: Density/Concentration Table
for Binary Aqueous Ethanol
Solutions
The following density/concentration table shows the density values for alcohol
concentrations of binary aqueous solutions (in %m/m and %V/V). The alcohol
concentrations are valid for 20C.
The table was calculated based on:
I. Rosendal & F. Schmidt. The Alcohol Table for Beer Analysis and
Polynomials for Alcohol and Extract. Monatsschrift fr Brauwissenschaft.
Heft 8/1987. pp. 334-338.
Organisation Internationale De Mtrologie Lgale. Recommandation
Internationale No. 22. Alcoomtrie. Tables Alcoomtriques Internationales.
1975.
Alcohol [%m/m] = alcohol content in percent by weight
Alcohol [%V/V] = alcohol content in percent by volume
Density [g/cm
3
] = true density at 20C
SG 20/04 = specific gravity 20/04
SG 20/20 = specific gravity 20/20
ASG = apparent specific gravity 20/20
Table J.1: Density and Concentration of Water/Ethanol Solutions
Alcohol Density SG20/04 SG20/20 ASG Alcohol Density SG20/04 SG20/20 ASG
%m/m %V/V
g/cm
3
- - - %m/m %V/V
g/cm
3
- - -
0.00 0.00 0.99820 0.99823 1.00000 1.00000 4.83 6.06 0.98965 0.98968 0.99144 0.99143
0.01 0.01 0.99818 0.99821 0.99998 0.99998 4.84 6.07 0.98964 0.98967 0.99142 0.99141
0.02 0.03 0.99816 0.99819 0.99996 0.99996 4.85 6.08 0.98962 0.98965 0.99140 0.99139
0.03 0.04 0.99814 0.99817 0.99994 0.99994 4.86 6.09 0.98961 0.98963 0.99139 0.99138
0.04 0.05 0.99812 0.99815 0.99992 0.99992 4.87 6.11 0.98959 0.98962 0.99137 0.99136
0.05 0.06 0.99810 0.99813 0.99990 0.99990 4.88 6.12 0.98957 0.98960 0.99135 0.99135
0.06 0.08 0.99809 0.99811 0.99988 0.99988 4.89 6.13 0.98956 0.98958 0.99134 0.99133
0.07 0.09 0.99807 0.99809 0.99986 0.99986 4.90 6.14 0.98954 0.98957 0.99132 0.99131
0.08 0.10 0.99805 0.99808 0.99984 0.99985 4.91 6.16 0.98952 0.98955 0.99131 0.99130
0.09 0.11 0.99803 0.99806 0.99982 0.99983 4.92 6.17 0.98951 0.98954 0.99129 0.99128
0.10 0.13 0.99801 0.99804 0.99981 0.99981 4.93 6.18 0.98949 0.98952 0.99127 0.99126
0.11 0.14 0.99799 0.99802 0.99979 0.99979 4.94 6.19 0.98948 0.98950 0.99126 0.99125
0.12 0.15 0.99797 0.99800 0.99977 0.99977 4.95 6.21 0.98946 0.98949 0.99124 0.99123
0.13 0.16 0.99795 0.99798 0.99975 0.99975 4.96 6.22 0.98944 0.98947 0.99122 0.99122
0.14 0.18 0.99793 0.99796 0.99973 0.99973 4.97 6.23 0.98943 0.98945 0.99121 0.99120
0.15 0.19 0.99791 0.99794 0.99971 0.99971 4.98 6.24 0.98941 0.98944 0.99119 0.99118
0.16 0.20 0.99789 0.99792 0.99969 0.99969 4.99 6.26 0.98939 0.98942 0.99118 0.99117
0.17 0.21 0.99787 0.99790 0.99967 0.99967 5.00 6.27 0.98938 0.98941 0.99116 0.99115
0.18 0.23 0.99786 0.99788 0.99965 0.99965 5.01 6.28 0.98936 0.98939 0.99114 0.99113
0.19 0.24 0.99784 0.99786 0.99963 0.99963 5.02 6.29 0.98935 0.98937 0.99113 0.99112
0.20 0.25 0.99782 0.99784 0.99961 0.99961 5.03 6.31 0.98933 0.98936 0.99111 0.99110
0.21 0.27 0.99780 0.99783 0.99959 0.99960 5.04 6.32 0.98931 0.98934 0.99109 0.99109
0.22 0.28 0.99778 0.99781 0.99957 0.99958 5.05 6.33 0.98930 0.98932 0.99108 0.99107
0.23 0.29 0.99776 0.99779 0.99956 0.99956 5.06 6.34 0.98928 0.98931 0.99106 0.99105
116 C27IB02
0.24 0.30 0.99774 0.99777 0.99954 0.99954 5.07 6.35 0.98926 0.98929 0.99105 0.99104
0.25 0.32 0.99772 0.99775 0.99952 0.99952 5.08 6.37 0.98925 0.98928 0.99103 0.99102
0.26 0.33 0.99770 0.99773 0.99950 0.99950 5.09 6.38 0.98923 0.98926 0.99101 0.99100
0.27 0.34 0.99768 0.99771 0.99948 0.99948 5.10 6.39 0.98922 0.98924 0.99100 0.99099
0.28 0.35 0.99766 0.99769 0.99946 0.99946 5.11 6.40 0.98920 0.98923 0.99098 0.99097
0.29 0.37 0.99764 0.99767 0.99944 0.99944 5.12 6.42 0.98918 0.98921 0.99096 0.99096
0.30 0.38 0.99763 0.99765 0.99942 0.99942 5.13 6.43 0.98917 0.98920 0.99095 0.99094
0.31 0.39 0.99761 0.99763 0.99940 0.99940 5.14 6.44 0.98915 0.98918 0.99093 0.99092
0.32 0.40 0.99759 0.99762 0.99938 0.99938 5.15 6.45 0.98914 0.98916 0.99092 0.99091
0.33 0.42 0.99757 0.99760 0.99936 0.99937 5.16 6.47 0.98912 0.98915 0.99090 0.99089
0.34 0.43 0.99755 0.99758 0.99935 0.99935 5.17 6.48 0.98910 0.98913 0.99088 0.99087
0.35 0.44 0.99753 0.99756 0.99933 0.99933 5.18 6.49 0.98909 0.98911 0.99087 0.99086
0.36 0.45 0.99751 0.99754 0.99931 0.99931 5.19 6.50 0.98907 0.98910 0.99085 0.99084
0.37 0.47 0.99749 0.99752 0.99929 0.99929 5.20 6.52 0.98905 0.98908 0.99084 0.99083
0.38 0.48 0.99747 0.99750 0.99927 0.99927 5.21 6.53 0.98904 0.98907 0.99082 0.99081
0.39 0.49 0.99745 0.99748 0.99925 0.99925 5.22 6.54 0.98902 0.98905 0.99080 0.99079
0.40 0.51 0.99744 0.99746 0.99923 0.99923 5.23 6.55 0.98901 0.98903 0.99079 0.99078
0.41 0.52 0.99742 0.99744 0.99921 0.99921 5.24 6.57 0.98899 0.98902 0.99077 0.99076
0.42 0.53 0.99740 0.99743 0.99919 0.99919 5.25 6.58 0.98897 0.98900 0.99075 0.99075
0.43 0.54 0.99738 0.99741 0.99917 0.99917 5.26 6.59 0.98896 0.98899 0.99074 0.99073
0.44 0.56 0.99736 0.99739 0.99916 0.99916 5.27 6.60 0.98894 0.98897 0.99072 0.99071
0.45 0.57 0.99734 0.99737 0.99914 0.99914 5.28 6.62 0.98893 0.98895 0.99071 0.99070
0.46 0.58 0.99732 0.99735 0.99912 0.99912 5.29 6.63 0.98891 0.98894 0.99069 0.99068
0.47 0.59 0.99730 0.99733 0.99910 0.99910 5.30 6.64 0.98889 0.98892 0.99067 0.99066
0.48 0.61 0.99728 0.99731 0.99908 0.99908 5.31 6.65 0.98888 0.98891 0.99066 0.99065
0.49 0.62 0.99726 0.99729 0.99906 0.99906 5.32 6.67 0.98886 0.98889 0.99064 0.99063
0.50 0.63 0.99725 0.99727 0.99904 0.99904 5.33 6.68 0.98885 0.98887 0.99063 0.99062
0.51 0.64 0.99723 0.99725 0.99902 0.99902 5.34 6.69 0.98883 0.98886 0.99061 0.99060
0.52 0.66 0.99721 0.99724 0.99900 0.99900 5.35 6.70 0.98881 0.98884 0.99059 0.99058
0.53 0.67 0.99719 0.99722 0.99898 0.99898 5.36 6.72 0.98880 0.98883 0.99058 0.99057
0.54 0.68 0.99717 0.99720 0.99897 0.99897 5.37 6.73 0.98878 0.98881 0.99056 0.99055
0.55 0.69 0.99715 0.99718 0.99895 0.99895 5.38 6.74 0.98877 0.98879 0.99055 0.99054
0.56 0.71 0.99713 0.99716 0.99893 0.99893 5.39 6.75 0.98875 0.98878 0.99053 0.99052
0.57 0.72 0.99711 0.99714 0.99891 0.99891 5.40 6.76 0.98873 0.98876 0.99051 0.99050
0.58 0.73 0.99709 0.99712 0.99889 0.99889 5.41 6.78 0.98872 0.98875 0.99050 0.99049
0.59 0.75 0.99708 0.99710 0.99887 0.99887 5.42 6.79 0.98870 0.98873 0.99048 0.99047
0.60 0.76 0.99706 0.99708 0.99885 0.99885 5.43 6.80 0.98869 0.98871 0.99047 0.99046
0.61 0.77 0.99704 0.99707 0.99883 0.99883 5.44 6.81 0.98867 0.98870 0.99045 0.99044
0.62 0.78 0.99702 0.99705 0.99881 0.99881 5.45 6.83 0.98865 0.98868 0.99043 0.99042
0.63 0.80 0.99700 0.99703 0.99880 0.99880 5.46 6.84 0.98864 0.98867 0.99042 0.99041
0.64 0.81 0.99698 0.99701 0.99878 0.99878 5.47 6.85 0.98862 0.98865 0.99040 0.99039
0.65 0.82 0.99696 0.99699 0.99876 0.99876 5.48 6.86 0.98861 0.98863 0.99039 0.99038
0.66 0.83 0.99694 0.99697 0.99874 0.99874 5.49 6.88 0.98859 0.98862 0.99037 0.99036
0.67 0.85 0.99693 0.99695 0.99872 0.99872 5.50 6.89 0.98857 0.98860 0.99035 0.99034
0.68 0.86 0.99691 0.99693 0.99870 0.99870 5.51 6.90 0.98856 0.98859 0.99034 0.99033
0.69 0.87 0.99689 0.99692 0.99868 0.99868 5.52 6.91 0.98854 0.98857 0.99032 0.99031
0.70 0.88 0.99687 0.99690 0.99866 0.99866 5.53 6.93 0.98853 0.98855 0.99031 0.99030
0.71 0.90 0.99685 0.99688 0.99864 0.99864 5.54 6.94 0.98851 0.98854 0.99029 0.99028
%m/m %V/V
g/cm
3
- - - %m/m %V/V
g/cm
3
- - -
C27IB02 117
0.72 0.91 0.99683 0.99686 0.99863 0.99863 5.55 6.95 0.98849 0.98852 0.99027 0.99026
0.73 0.92 0.99681 0.99684 0.99861 0.99861 5.56 6.96 0.98848 0.98851 0.99026 0.99025
0.74 0.93 0.99679 0.99682 0.99859 0.99859 5.57 6.98 0.98846 0.98849 0.99024 0.99023
0.75 0.95 0.99678 0.99680 0.99857 0.99857 5.58 6.99 0.98845 0.98847 0.99023 0.99022
0.76 0.96 0.99676 0.99678 0.99855 0.99855 5.59 7.00 0.98843 0.98846 0.99021 0.99020
0.77 0.97 0.99674 0.99677 0.99853 0.99853 5.60 7.01 0.98841 0.98844 0.99019 0.99018
0.78 0.99 0.99672 0.99675 0.99851 0.99851 5.61 7.03 0.98840 0.98843 0.99018 0.99017
0.79 1.00 0.99670 0.99673 0.99849 0.99849 5.62 7.04 0.98838 0.98841 0.99016 0.99015
0.80 1.01 0.99668 0.99671 0.99848 0.99848 5.63 7.05 0.98837 0.98839 0.99015 0.99014
0.81 1.02 0.99666 0.99669 0.99846 0.99846 5.64 7.06 0.98835 0.98838 0.99013 0.99012
0.82 1.04 0.99664 0.99667 0.99844 0.99844 5.65 7.08 0.98834 0.98836 0.99011 0.99010
0.83 1.05 0.99663 0.99665 0.99842 0.99842 5.66 7.09 0.98832 0.98835 0.99010 0.99009
0.84 1.06 0.99661 0.99663 0.99840 0.99840 5.67 7.10 0.98830 0.98833 0.99008 0.99007
0.85 1.07 0.99659 0.99662 0.99838 0.99838 5.68 7.11 0.98829 0.98832 0.99007 0.99006
0.86 1.09 0.99657 0.99660 0.99836 0.99836 5.69 7.12 0.98827 0.98830 0.99005 0.99004
0.87 1.10 0.99655 0.99658 0.99834 0.99834 5.70 7.14 0.98826 0.98828 0.99003 0.99002
0.88 1.11 0.99653 0.99656 0.99833 0.99833 5.71 7.15 0.98824 0.98827 0.99002 0.99001
0.89 1.12 0.99651 0.99654 0.99831 0.99831 5.72 7.16 0.98822 0.98825 0.99000 0.98999
0.90 1.14 0.99649 0.99652 0.99829 0.99829 5.73 7.17 0.98821 0.98824 0.98999 0.98998
0.91 1.15 0.99648 0.99650 0.99827 0.99827 5.74 7.19 0.98819 0.98822 0.98997 0.98996
0.92 1.16 0.99646 0.99649 0.99825 0.99825 5.75 7.20 0.98818 0.98820 0.98996 0.98995
0.93 1.17 0.99644 0.99647 0.99823 0.99823 5.76 7.21 0.98816 0.98819 0.98994 0.98993
0.94 1.19 0.99642 0.99645 0.99821 0.99821 5.77 7.22 0.98815 0.98817 0.98992 0.98991
0.95 1.20 0.99640 0.99643 0.99820 0.99820 5.78 7.24 0.98813 0.98816 0.98991 0.98990
0.96 1.21 0.99638 0.99641 0.99818 0.99818 5.79 7.25 0.98811 0.98814 0.98989 0.98988
0.97 1.22 0.99636 0.99639 0.99816 0.99816 5.80 7.26 0.98810 0.98813 0.98988 0.98987
0.98 1.24 0.99635 0.99637 0.99814 0.99814 5.81 7.27 0.98808 0.98811 0.98986 0.98985
0.99 1.25 0.99633 0.99636 0.99812 0.99812 5.82 7.29 0.98807 0.98809 0.98984 0.98983
1.00 1.26 0.99631 0.99634 0.99810 0.99810 5.83 7.30 0.98805 0.98808 0.98983 0.98982
1.01 1.27 0.99629 0.99632 0.99808 0.99808 5.84 7.31 0.98803 0.98806 0.98981 0.98980
1.02 1.29 0.99627 0.99630 0.99807 0.99806 5.85 7.32 0.98802 0.98805 0.98980 0.98979
1.03 1.30 0.99625 0.99628 0.99805 0.99805 5.86 7.34 0.98800 0.98803 0.98978 0.98977
1.04 1.31 0.99623 0.99626 0.99803 0.99803 5.87 7.35 0.98799 0.98801 0.98977 0.98976
1.05 1.33 0.99622 0.99624 0.99801 0.99801 5.88 7.36 0.98797 0.98800 0.98975 0.98974
1.06 1.34 0.99620 0.99623 0.99799 0.99799 5.89 7.37 0.98796 0.98798 0.98973 0.98972
1.07 1.35 0.99618 0.99621 0.99797 0.99797 5.90 7.39 0.98794 0.98797 0.98972 0.98971
1.08 1.36 0.99616 0.99619 0.99795 0.99795 5.91 7.40 0.98792 0.98795 0.98970 0.98969
1.09 1.38 0.99614 0.99617 0.99794 0.99793 5.92 7.41 0.98791 0.98794 0.98969 0.98968
1.10 1.39 0.99612 0.99615 0.99792 0.99792 5.93 7.42 0.98789 0.98792 0.98967 0.98966
1.11 1.40 0.99611 0.99613 0.99790 0.99790 5.94 7.43 0.98788 0.98790 0.98966 0.98964
1.12 1.41 0.99609 0.99611 0.99788 0.99788 5.95 7.45 0.98786 0.98789 0.98964 0.98963
1.13 1.43 0.99607 0.99610 0.99786 0.99786 5.96 7.46 0.98785 0.98787 0.98962 0.98961
1.14 1.44 0.99605 0.99608 0.99784 0.99784 5.97 7.47 0.98783 0.98786 0.98961 0.98960
1.15 1.45 0.99603 0.99606 0.99782 0.99782 5.98 7.48 0.98781 0.98784 0.98959 0.98958
1.16 1.46 0.99601 0.99604 0.99781 0.99780 5.99 7.50 0.98780 0.98783 0.98958 0.98957
1.17 1.48 0.99599 0.99602 0.99779 0.99779 6.00 7.51 0.98778 0.98781 0.98956 0.98955
1.18 1.49 0.99598 0.99600 0.99777 0.99777 6.01 7.52 0.98777 0.98779 0.98954 0.98953
1.19 1.50 0.99596 0.99599 0.99775 0.99775 6.02 7.53 0.98775 0.98778 0.98953 0.98952
%m/m %V/V
g/cm
3
- - - %m/m %V/V
g/cm
3
- - -
118 C27IB02
1.20 1.51 0.99594 0.99597 0.99773 0.99773 6.03 7.55 0.98774 0.98776 0.98951 0.98950
1.21 1.53 0.99592 0.99595 0.99771 0.99771 6.04 7.56 0.98772 0.98775 0.98950 0.98949
1.22 1.54 0.99590 0.99593 0.99769 0.99769 6.05 7.57 0.98770 0.98773 0.98948 0.98947
1.23 1.55 0.99588 0.99591 0.99768 0.99768 6.06 7.58 0.98769 0.98772 0.98947 0.98946
1.24 1.56 0.99587 0.99589 0.99766 0.99766 6.07 7.60 0.98767 0.98770 0.98945 0.98944
1.25 1.58 0.99585 0.99587 0.99764 0.99764 6.08 7.61 0.98766 0.98768 0.98943 0.98942
1.26 1.59 0.99583 0.99586 0.99762 0.99762 6.09 7.62 0.98764 0.98767 0.98942 0.98941
1.27 1.60 0.99581 0.99584 0.99760 0.99760 6.10 7.63 0.98763 0.98765 0.98940 0.98939
1.28 1.61 0.99579 0.99582 0.99758 0.99758 6.11 7.65 0.98761 0.98764 0.98939 0.98938
1.29 1.63 0.99577 0.99580 0.99757 0.99756 6.12 7.66 0.98759 0.98762 0.98937 0.98936
1.30 1.64 0.99575 0.99578 0.99755 0.99755 6.13 7.67 0.98758 0.98761 0.98936 0.98935
1.31 1.65 0.99574 0.99576 0.99753 0.99753 6.14 7.68 0.98756 0.98759 0.98934 0.98933
1.32 1.67 0.99572 0.99575 0.99751 0.99751 6.15 7.70 0.98755 0.98757 0.98933 0.98931
1.33 1.68 0.99570 0.99573 0.99749 0.99749 6.16 7.71 0.98753 0.98756 0.98931 0.98930
1.34 1.69 0.99568 0.99571 0.99747 0.99747 6.17 7.72 0.98752 0.98754 0.98929 0.98928
1.35 1.70 0.99566 0.99569 0.99746 0.99745 6.18 7.73 0.98750 0.98753 0.98928 0.98927
1.36 1.72 0.99564 0.99567 0.99744 0.99744 6.19 7.74 0.98748 0.98751 0.98926 0.98925
1.37 1.73 0.99563 0.99565 0.99742 0.99742 6.20 7.76 0.98747 0.98750 0.98925 0.98924
1.38 1.74 0.99561 0.99564 0.99740 0.99740 6.21 7.77 0.98745 0.98748 0.98923 0.98922
1.39 1.75 0.99559 0.99562 0.99738 0.99738 6.22 7.78 0.98744 0.98747 0.98922 0.98920
1.40 1.77 0.99557 0.99560 0.99736 0.99736 6.23 7.79 0.98742 0.98745 0.98920 0.98919
1.41 1.78 0.99555 0.99558 0.99735 0.99734 6.24 7.81 0.98741 0.98743 0.98918 0.98917
1.42 1.79 0.99554 0.99556 0.99733 0.99733 6.25 7.82 0.98739 0.98742 0.98917 0.98916
1.43 1.80 0.99552 0.99554 0.99731 0.99731 6.26 7.83 0.98738 0.98740 0.98915 0.98914
1.44 1.82 0.99550 0.99553 0.99729 0.99729 6.27 7.84 0.98736 0.98739 0.98914 0.98913
1.45 1.83 0.99548 0.99551 0.99727 0.99727 6.28 7.86 0.98734 0.98737 0.98912 0.98911
1.46 1.84 0.99546 0.99549 0.99725 0.99725 6.29 7.87 0.98733 0.98736 0.98911 0.98909
1.47 1.85 0.99544 0.99547 0.99724 0.99723 6.30 7.88 0.98731 0.98734 0.98909 0.98908
1.48 1.87 0.99543 0.99545 0.99722 0.99722 6.31 7.89 0.98730 0.98733 0.98908 0.98906
1.49 1.88 0.99541 0.99544 0.99720 0.99720 6.32 7.91 0.98728 0.98731 0.98906 0.98905
1.50 1.89 0.99539 0.99542 0.99718 0.99718 6.33 7.92 0.98727 0.98729 0.98904 0.98903
1.51 1.90 0.99537 0.99540 0.99716 0.99716 6.34 7.93 0.98725 0.98728 0.98903 0.98902
1.52 1.92 0.99535 0.99538 0.99714 0.99714 6.35 7.94 0.98724 0.98726 0.98901 0.98900
1.53 1.93 0.99533 0.99536 0.99713 0.99712 6.36 7.96 0.98722 0.98725 0.98900 0.98899
1.54 1.94 0.99532 0.99534 0.99711 0.99711 6.37 7.97 0.98720 0.98723 0.98898 0.98897
1.55 1.95 0.99530 0.99533 0.99709 0.99709 6.38 7.98 0.98719 0.98722 0.98897 0.98895
1.56 1.97 0.99528 0.99531 0.99707 0.99707 6.39 7.99 0.98717 0.98720 0.98895 0.98894
1.57 1.98 0.99526 0.99529 0.99705 0.99705 6.40 8.00 0.98716 0.98719 0.98893 0.98892
1.58 1.99 0.99524 0.99527 0.99704 0.99703 6.41 8.02 0.98714 0.98717 0.98892 0.98891
1.59 2.00 0.99523 0.99525 0.99702 0.99702 6.42 8.03 0.98713 0.98715 0.98890 0.98889
1.60 2.02 0.99521 0.99524 0.99700 0.99700 6.43 8.04 0.98711 0.98714 0.98889 0.98888
1.61 2.03 0.99519 0.99522 0.99698 0.99698 6.44 8.05 0.98710 0.98712 0.98887 0.98886
1.62 2.04 0.99517 0.99520 0.99696 0.99696 6.45 8.07 0.98708 0.98711 0.98886 0.98885
1.63 2.06 0.99515 0.99518 0.99694 0.99694 6.46 8.08 0.98706 0.98709 0.98884 0.98883
1.64 2.07 0.99513 0.99516 0.99693 0.99692 6.47 8.09 0.98705 0.98708 0.98883 0.98881
1.65 2.08 0.99512 0.99514 0.99691 0.99691 6.48 8.10 0.98703 0.98706 0.98881 0.98880
1.66 2.09 0.99510 0.99513 0.99689 0.99689 6.49 8.12 0.98702 0.98705 0.98880 0.98878
1.67 2.11 0.99508 0.99511 0.99687 0.99687 6.50 8.13 0.98700 0.98703 0.98878 0.98877
%m/m %V/V
g/cm
3
- - - %m/m %V/V
g/cm
3
- - -
C27IB02 119
1.68 2.12 0.99506 0.99509 0.99685 0.99685 6.51 8.14 0.98699 0.98702 0.98876 0.98875
1.69 2.13 0.99504 0.99507 0.99684 0.99683 6.52 8.15 0.98697 0.98700 0.98875 0.98874
1.70 2.14 0.99503 0.99505 0.99682 0.99682 6.53 8.17 0.98696 0.98698 0.98873 0.98872
1.71 2.16 0.99501 0.99504 0.99680 0.99680 6.54 8.18 0.98694 0.98697 0.98872 0.98871
1.72 2.17 0.99499 0.99502 0.99678 0.99678 6.55 8.19 0.98693 0.98695 0.98870 0.98869
1.73 2.18 0.99497 0.99500 0.99676 0.99676 6.56 8.20 0.98691 0.98694 0.98869 0.98867
1.74 2.19 0.99495 0.99498 0.99674 0.99674 6.57 8.22 0.98689 0.98692 0.98867 0.98866
1.75 2.21 0.99494 0.99496 0.99673 0.99672 6.58 8.23 0.98688 0.98691 0.98866 0.98864
1.76 2.22 0.99492 0.99495 0.99671 0.99671 6.59 8.24 0.98686 0.98689 0.98864 0.98863
1.77 2.23 0.99490 0.99493 0.99669 0.99669 6.60 8.25 0.98685 0.98688 0.98862 0.98861
1.78 2.24 0.99488 0.99491 0.99667 0.99667 6.61 8.26 0.98683 0.98686 0.98861 0.98860
1.79 2.26 0.99486 0.99489 0.99665 0.99665 6.62 8.28 0.98682 0.98685 0.98859 0.98858
1.80 2.27 0.99485 0.99487 0.99664 0.99663 6.63 8.29 0.98680 0.98683 0.98858 0.98857
1.81 2.28 0.99483 0.99486 0.99662 0.99662 6.64 8.30 0.98679 0.98681 0.98856 0.98855
1.82 2.29 0.99481 0.99484 0.99660 0.99660 6.65 8.31 0.98677 0.98680 0.98855 0.98854
1.83 2.31 0.99479 0.99482 0.99658 0.99658 6.66 8.33 0.98676 0.98678 0.98853 0.98852
1.84 2.32 0.99477 0.99480 0.99656 0.99656 6.67 8.34 0.98674 0.98677 0.98852 0.98850
1.85 2.33 0.99476 0.99478 0.99655 0.99654 6.68 8.35 0.98673 0.98675 0.98850 0.98849
1.86 2.34 0.99474 0.99477 0.99653 0.99653 6.69 8.36 0.98671 0.98674 0.98849 0.98847
1.87 2.36 0.99472 0.99475 0.99651 0.99651 6.70 8.38 0.98669 0.98672 0.98847 0.98846
1.88 2.37 0.99470 0.99473 0.99649 0.99649 6.71 8.39 0.98668 0.98671 0.98846 0.98844
1.89 2.38 0.99468 0.99471 0.99647 0.99647 6.72 8.40 0.98666 0.98669 0.98844 0.98843
1.90 2.39 0.99467 0.99469 0.99646 0.99645 6.73 8.41 0.98665 0.98668 0.98842 0.98841
1.91 2.41 0.99465 0.99468 0.99644 0.99644 6.74 8.43 0.98663 0.98666 0.98841 0.98840
1.92 2.42 0.99463 0.99466 0.99642 0.99642 6.75 8.44 0.98662 0.98665 0.98839 0.98838
1.93 2.43 0.99461 0.99464 0.99640 0.99640 6.76 8.45 0.98660 0.98663 0.98838 0.98837
1.94 2.44 0.99459 0.99462 0.99638 0.99638 6.77 8.46 0.98659 0.98661 0.98836 0.98835
1.95 2.46 0.99458 0.99460 0.99637 0.99636 6.78 8.48 0.98657 0.98660 0.98835 0.98834
1.96 2.47 0.99456 0.99459 0.99635 0.99635 6.79 8.49 0.98656 0.98658 0.98833 0.98832
1.97 2.48 0.99454 0.99457 0.99633 0.99633 6.80 8.50 0.98654 0.98657 0.98832 0.98830
1.98 2.49 0.99452 0.99455 0.99631 0.99631 6.81 8.51 0.98653 0.98655 0.98830 0.98829
1.99 2.51 0.99450 0.99453 0.99629 0.99629 6.82 8.52 0.98651 0.98654 0.98829 0.98827
2.00 2.52 0.99449 0.99451 0.99628 0.99627 6.83 8.54 0.98649 0.98652 0.98827 0.98826
2.01 2.53 0.99447 0.99450 0.99626 0.99626 6.84 8.55 0.98648 0.98651 0.98826 0.98824
2.02 2.55 0.99445 0.99448 0.99624 0.99624 6.85 8.56 0.98646 0.98649 0.98824 0.98823
2.03 2.56 0.99443 0.99446 0.99622 0.99622 6.86 8.57 0.98645 0.98648 0.98822 0.98821
2.04 2.57 0.99441 0.99444 0.99620 0.99620 6.87 8.59 0.98643 0.98646 0.98821 0.98820
2.05 2.58 0.99440 0.99442 0.99619 0.99618 6.88 8.60 0.98642 0.98645 0.98819 0.98818
2.06 2.60 0.99438 0.99441 0.99617 0.99617 6.89 8.61 0.98640 0.98643 0.98818 0.98817
2.07 2.61 0.99436 0.99439 0.99615 0.99615 6.90 8.62 0.98639 0.98642 0.98816 0.98815
2.08 2.62 0.99434 0.99437 0.99613 0.99613 6.91 8.64 0.98637 0.98640 0.98815 0.98814
2.09 2.63 0.99433 0.99435 0.99612 0.99611 6.92 8.65 0.98636 0.98638 0.98813 0.98812
2.10 2.65 0.99431 0.99434 0.99610 0.99609 6.93 8.66 0.98634 0.98637 0.98812 0.98810
2.11 2.66 0.99429 0.99432 0.99608 0.99608 6.94 8.67 0.98633 0.98635 0.98810 0.98809
2.12 2.67 0.99427 0.99430 0.99606 0.99606 6.95 8.69 0.98631 0.98634 0.98809 0.98807
2.13 2.68 0.99425 0.99428 0.99604 0.99604 6.96 8.70 0.98630 0.98632 0.98807 0.98806
2.14 2.70 0.99424 0.99426 0.99603 0.99602 6.97 8.71 0.98628 0.98631 0.98806 0.98804
2.15 2.71 0.99422 0.99425 0.99601 0.99600 6.98 8.72 0.98627 0.98629 0.98804 0.98803
%m/m %V/V
g/cm
3
- - - %m/m %V/V
g/cm
3
- - -
120 C27IB02
2.16 2.72 0.99420 0.99423 0.99599 0.99599 6.99 8.73 0.98625 0.98628 0.98803 0.98801
2.17 2.73 0.99418 0.99421 0.99597 0.99597 7.00 8.75 0.98624 0.98626 0.98801 0.98800
2.18 2.75 0.99416 0.99419 0.99595 0.99595 7.01 8.76 0.98622 0.98625 0.98800 0.98798
2.19 2.76 0.99415 0.99417 0.99594 0.99593 7.02 8.77 0.98620 0.98623 0.98798 0.98797
2.20 2.77 0.99413 0.99416 0.99592 0.99592 7.03 8.78 0.98619 0.98622 0.98796 0.98795
2.21 2.78 0.99411 0.99414 0.99590 0.99590 7.04 8.80 0.98617 0.98620 0.98795 0.98794
2.22 2.80 0.99409 0.99412 0.99588 0.99588 7.05 8.81 0.98616 0.98619 0.98793 0.98792
2.23 2.81 0.99408 0.99410 0.99587 0.99586 7.06 8.82 0.98614 0.98617 0.98792 0.98791
2.24 2.82 0.99406 0.99409 0.99585 0.99584 7.07 8.83 0.98613 0.98616 0.98790 0.98789
2.25 2.83 0.99404 0.99407 0.99583 0.99583 7.08 8.85 0.98611 0.98614 0.98789 0.98788
2.26 2.85 0.99402 0.99405 0.99581 0.99581 7.09 8.86 0.98610 0.98613 0.98787 0.98786
2.27 2.86 0.99400 0.99403 0.99579 0.99579 7.10 8.87 0.98608 0.98611 0.98786 0.98785
2.28 2.87 0.99399 0.99401 0.99578 0.99577 7.11 8.88 0.98607 0.98610 0.98784 0.98783
2.29 2.88 0.99397 0.99400 0.99576 0.99576 7.12 8.90 0.98605 0.98608 0.98783 0.98781
2.30 2.90 0.99395 0.99398 0.99574 0.99574 7.13 8.91 0.98604 0.98606 0.98781 0.98780
2.31 2.91 0.99393 0.99396 0.99572 0.99572 7.14 8.92 0.98602 0.98605 0.98780 0.98778
2.32 2.92 0.99392 0.99394 0.99571 0.99570 7.15 8.93 0.98601 0.98603 0.98778 0.98777
2.33 2.93 0.99390 0.99393 0.99569 0.99568 7.16 8.94 0.98599 0.98602 0.98777 0.98775
2.34 2.95 0.99388 0.99391 0.99567 0.99567 7.17 8.96 0.98598 0.98600 0.98775 0.98774
2.35 2.96 0.99386 0.99389 0.99565 0.99565 7.18 8.97 0.98596 0.98599 0.98774 0.98772
2.36 2.97 0.99385 0.99387 0.99563 0.99563 7.19 8.98 0.98595 0.98597 0.98772 0.98771
2.37 2.98 0.99383 0.99386 0.99562 0.99561 7.20 8.99 0.98593 0.98596 0.98771 0.98769
2.38 3.00 0.99381 0.99384 0.99560 0.99560 7.21 9.01 0.98592 0.98594 0.98769 0.98768
2.39 3.01 0.99379 0.99382 0.99558 0.99558 7.22 9.02 0.98590 0.98593 0.98768 0.98766
2.40 3.02 0.99377 0.99380 0.99556 0.99556 7.23 9.03 0.98589 0.98591 0.98766 0.98765
2.41 3.03 0.99376 0.99378 0.99555 0.99554 7.24 9.04 0.98587 0.98590 0.98765 0.98763
2.42 3.05 0.99374 0.99377 0.99553 0.99552 7.25 9.06 0.98586 0.98588 0.98763 0.98762
2.43 3.06 0.99372 0.99375 0.99551 0.99551 7.26 9.07 0.98584 0.98587 0.98761 0.98760
2.44 3.07 0.99370 0.99373 0.99549 0.99549 7.27 9.08 0.98583 0.98585 0.98760 0.98759
2.45 3.08 0.99369 0.99371 0.99548 0.99547 7.28 9.09 0.98581 0.98584 0.98758 0.98757
2.46 3.10 0.99367 0.99370 0.99546 0.99545 7.29 9.11 0.98579 0.98582 0.98757 0.98756
2.47 3.11 0.99365 0.99368 0.99544 0.99544 7.30 9.12 0.98578 0.98581 0.98755 0.98754
2.48 3.12 0.99363 0.99366 0.99542 0.99542 7.31 9.13 0.98576 0.98579 0.98754 0.98753
2.49 3.13 0.99362 0.99364 0.99540 0.99540 7.32 9.14 0.98575 0.98578 0.98752 0.98751
2.50 3.15 0.99360 0.99363 0.99539 0.99538 7.33 9.15 0.98573 0.98576 0.98751 0.98750
2.51 3.16 0.99358 0.99361 0.99537 0.99537 7.34 9.17 0.98572 0.98575 0.98749 0.98748
2.52 3.17 0.99356 0.99359 0.99535 0.99535 7.35 9.18 0.98570 0.98573 0.98748 0.98747
2.53 3.18 0.99355 0.99357 0.99533 0.99533 7.36 9.19 0.98569 0.98572 0.98746 0.98745
2.54 3.20 0.99353 0.99356 0.99532 0.99531 7.37 9.20 0.98567 0.98570 0.98745 0.98744
2.55 3.21 0.99351 0.99354 0.99530 0.99530 7.38 9.22 0.98566 0.98569 0.98743 0.98742
2.56 3.22 0.99349 0.99352 0.99528 0.99528 7.39 9.23 0.98564 0.98567 0.98742 0.98740
2.57 3.24 0.99348 0.99350 0.99526 0.99526 7.40 9.24 0.98563 0.98566 0.98740 0.98739
2.58 3.25 0.99346 0.99349 0.99525 0.99524 7.41 9.25 0.98561 0.98564 0.98739 0.98737
2.59 3.26 0.99344 0.99347 0.99523 0.99522 7.42 9.27 0.98560 0.98563 0.98737 0.98736
2.60 3.27 0.99342 0.99345 0.99521 0.99521 7.43 9.28 0.98558 0.98561 0.98736 0.98734
2.61 3.29 0.99341 0.99343 0.99519 0.99519 7.44 9.29 0.98557 0.98560 0.98734 0.98733
2.62 3.30 0.99339 0.99342 0.99518 0.99517 7.45 9.30 0.98555 0.98558 0.98733 0.98731
2.63 3.31 0.99337 0.99340 0.99516 0.99515 7.46 9.32 0.98554 0.98557 0.98731 0.98730
%m/m %V/V
g/cm
3
- - - %m/m %V/V
g/cm
3
- - -
C27IB02 121
2.64 3.32 0.99335 0.99338 0.99514 0.99514 7.47 9.33 0.98552 0.98555 0.98730 0.98728
2.65 3.34 0.99334 0.99336 0.99512 0.99512 7.48 9.34 0.98551 0.98554 0.98728 0.98727
2.66 3.35 0.99332 0.99335 0.99511 0.99510 7.49 9.35 0.98549 0.98552 0.98727 0.98725
2.67 3.36 0.99330 0.99333 0.99509 0.99508 7.50 9.36 0.98548 0.98551 0.98725 0.98724
2.68 3.37 0.99328 0.99331 0.99507 0.99507 7.51 9.38 0.98546 0.98549 0.98724 0.98722
2.69 3.39 0.99327 0.99329 0.99505 0.99505 7.52 9.39 0.98545 0.98548 0.98722 0.98721
2.70 3.40 0.99325 0.99328 0.99504 0.99503 7.53 9.40 0.98543 0.98546 0.98721 0.98719
2.71 3.41 0.99323 0.99326 0.99502 0.99501 7.54 9.41 0.98542 0.98545 0.98719 0.98718
2.72 3.42 0.99321 0.99324 0.99500 0.99500 7.55 9.43 0.98540 0.98543 0.98718 0.98716
2.73 3.44 0.99320 0.99322 0.99498 0.99498 7.56 9.44 0.98539 0.98542 0.98716 0.98715
2.74 3.45 0.99318 0.99321 0.99497 0.99496 7.57 9.45 0.98537 0.98540 0.98715 0.98713
2.75 3.46 0.99316 0.99319 0.99495 0.99494 7.58 9.46 0.98536 0.98539 0.98713 0.98712
2.76 3.47 0.99314 0.99317 0.99493 0.99493 7.59 9.48 0.98534 0.98537 0.98712 0.98710
2.77 3.49 0.99313 0.99315 0.99491 0.99491 7.60 9.49 0.98533 0.98536 0.98710 0.98709
2.78 3.50 0.99311 0.99314 0.99490 0.99489 7.61 9.50 0.98531 0.98534 0.98709 0.98707
2.79 3.51 0.99309 0.99312 0.99488 0.99487 7.62 9.51 0.98530 0.98533 0.98707 0.98706
2.80 3.52 0.99307 0.99310 0.99486 0.99486 7.63 9.53 0.98528 0.98531 0.98706 0.98704
2.81 3.54 0.99306 0.99308 0.99484 0.99484 7.64 9.54 0.98527 0.98530 0.98704 0.98703
2.82 3.55 0.99304 0.99307 0.99483 0.99482 7.65 9.55 0.98525 0.98528 0.98703 0.98701
2.83 3.56 0.99302 0.99305 0.99481 0.99480 7.66 9.56 0.98524 0.98527 0.98701 0.98700
2.84 3.57 0.99300 0.99303 0.99479 0.99479 7.67 9.57 0.98522 0.98525 0.98700 0.98698
2.85 3.59 0.99299 0.99301 0.99477 0.99477 7.68 9.59 0.98521 0.98524 0.98698 0.98697
2.86 3.60 0.99297 0.99300 0.99476 0.99475 7.69 9.60 0.98519 0.98522 0.98697 0.98695
2.87 3.61 0.99295 0.99298 0.99474 0.99473 7.70 9.61 0.98518 0.98521 0.98695 0.98694
2.88 3.62 0.99293 0.99296 0.99472 0.99472 7.71 9.62 0.98516 0.98519 0.98694 0.98692
2.89 3.64 0.99292 0.99294 0.99470 0.99470 7.72 9.64 0.98515 0.98518 0.98692 0.98691
2.90 3.65 0.99290 0.99293 0.99469 0.99468 7.73 9.65 0.98513 0.98516 0.98691 0.98689
2.91 3.66 0.99288 0.99291 0.99467 0.99466 7.74 9.66 0.98512 0.98515 0.98689 0.98688
2.92 3.67 0.99286 0.99289 0.99465 0.99465 7.75 9.67 0.98510 0.98513 0.98688 0.98686
2.93 3.69 0.99285 0.99288 0.99463 0.99463 7.76 9.69 0.98509 0.98512 0.98686 0.98685
2.94 3.70 0.99283 0.99286 0.99462 0.99461 7.77 9.70 0.98507 0.98510 0.98685 0.98683
2.95 3.71 0.99281 0.99284 0.99460 0.99460 7.78 9.71 0.98506 0.98509 0.98683 0.98682
2.96 3.72 0.99280 0.99282 0.99458 0.99458 7.79 9.72 0.98504 0.98507 0.98682 0.98680
2.97 3.74 0.99278 0.99281 0.99457 0.99456 7.80 9.73 0.98503 0.98506 0.98680 0.98679
2.98 3.75 0.99276 0.99279 0.99455 0.99454 7.81 9.75 0.98501 0.98504 0.98679 0.98677
2.99 3.76 0.99274 0.99277 0.99453 0.99453 7.82 9.76 0.98500 0.98503 0.98677 0.98676
3.00 3.77 0.99273 0.99275 0.99451 0.99451 7.83 9.77 0.98498 0.98501 0.98676 0.98674
3.01 3.79 0.99271 0.99274 0.99450 0.99449 7.84 9.78 0.98497 0.98500 0.98674 0.98673
3.02 3.80 0.99269 0.99272 0.99448 0.99447 7.85 9.80 0.98496 0.98498 0.98673 0.98671
3.03 3.81 0.99267 0.99270 0.99446 0.99446 7.86 9.81 0.98494 0.98497 0.98671 0.98670
3.04 3.82 0.99266 0.99268 0.99444 0.99444 7.87 9.82 0.98493 0.98495 0.98670 0.98668
3.05 3.84 0.99264 0.99267 0.99443 0.99442 7.88 9.83 0.98491 0.98494 0.98668 0.98667
3.06 3.85 0.99262 0.99265 0.99441 0.99440 7.89 9.85 0.98490 0.98492 0.98667 0.98665
3.07 3.86 0.99261 0.99263 0.99439 0.99439 7.90 9.86 0.98488 0.98491 0.98665 0.98664
3.08 3.87 0.99259 0.99262 0.99437 0.99437 7.91 9.87 0.98487 0.98489 0.98664 0.98662
3.09 3.89 0.99257 0.99260 0.99436 0.99435 7.92 9.88 0.98485 0.98488 0.98662 0.98661
3.10 3.90 0.99255 0.99258 0.99434 0.99434 7.93 9.90 0.98484 0.98486 0.98661 0.98659
3.11 3.91 0.99254 0.99256 0.99432 0.99432 7.94 9.91 0.98482 0.98485 0.98659 0.98658
%m/m %V/V
g/cm
3
- - - %m/m %V/V
g/cm
3
- - -
122 C27IB02
3.12 3.92 0.99252 0.99255 0.99431 0.99430 7.95 9.92 0.98481 0.98483 0.98658 0.98657
3.13 3.94 0.99250 0.99253 0.99429 0.99428 7.96 9.93 0.98479 0.98482 0.98656 0.98655
3.14 3.95 0.99248 0.99251 0.99427 0.99427 7.97 9.94 0.98478 0.98480 0.98655 0.98654
3.15 3.96 0.99247 0.99250 0.99425 0.99425 7.98 9.96 0.98476 0.98479 0.98653 0.98652
3.16 3.97 0.99245 0.99248 0.99424 0.99423 7.99 9.97 0.98475 0.98477 0.98652 0.98651
3.17 3.99 0.99243 0.99246 0.99422 0.99421 8.00 9.98 0.98473 0.98476 0.98651 0.98649
3.18 4.00 0.99242 0.99244 0.99420 0.99420 8.01 9.99 0.98472 0.98475 0.98649 0.98648
3.19 4.01 0.99240 0.99243 0.99419 0.99418 8.02 10.01 0.98470 0.98473 0.98648 0.98646
3.20 4.02 0.99238 0.99241 0.99417 0.99416 8.03 10.02 0.98469 0.98472 0.98646 0.98645
3.21 4.04 0.99236 0.99239 0.99415 0.99415 8.04 10.03 0.98467 0.98470 0.98645 0.98643
3.22 4.05 0.99235 0.99237 0.99413 0.99413 8.05 10.04 0.98466 0.98469 0.98643 0.98642
3.23 4.06 0.99233 0.99236 0.99412 0.99411 8.06 10.06 0.98464 0.98467 0.98642 0.98640
3.24 4.07 0.99231 0.99234 0.99410 0.99409 8.07 10.07 0.98463 0.98466 0.98640 0.98639
3.25 4.09 0.99230 0.99232 0.99408 0.99408 8.08 10.08 0.98461 0.98464 0.98639 0.98637
3.26 4.10 0.99228 0.99231 0.99406 0.99406 8.09 10.09 0.98460 0.98463 0.98637 0.98636
3.27 4.11 0.99226 0.99229 0.99405 0.99404 8.10 10.10 0.98458 0.98461 0.98636 0.98634
3.28 4.12 0.99224 0.99227 0.99403 0.99402 8.11 10.12 0.98457 0.98460 0.98634 0.98633
3.29 4.14 0.99223 0.99225 0.99401 0.99401 8.12 10.13 0.98456 0.98458 0.98633 0.98631
3.30 4.15 0.99221 0.99224 0.99400 0.99399 8.13 10.14 0.98454 0.98457 0.98631 0.98630
3.31 4.16 0.99219 0.99222 0.99398 0.99397 8.14 10.15 0.98453 0.98455 0.98630 0.98628
3.32 4.17 0.99218 0.99220 0.99396 0.99396 8.15 10.17 0.98451 0.98454 0.98628 0.98627
3.33 4.19 0.99216 0.99219 0.99394 0.99394 8.16 10.18 0.98450 0.98452 0.98627 0.98625
3.34 4.20 0.99214 0.99217 0.99393 0.99392 8.17 10.19 0.98448 0.98451 0.98625 0.98624
3.35 4.21 0.99212 0.99215 0.99391 0.99390 8.18 10.20 0.98447 0.98449 0.98624 0.98622
3.36 4.22 0.99211 0.99213 0.99389 0.99389 8.19 10.22 0.98445 0.98448 0.98622 0.98621
3.37 4.24 0.99209 0.99212 0.99388 0.99387 8.20 10.23 0.98444 0.98446 0.98621 0.98619
3.38 4.25 0.99207 0.99210 0.99386 0.99385 8.21 10.24 0.98442 0.98445 0.98619 0.98618
3.39 4.26 0.99206 0.99208 0.99384 0.99384 8.22 10.25 0.98441 0.98444 0.98618 0.98616
3.40 4.27 0.99204 0.99207 0.99382 0.99382 8.23 10.27 0.98439 0.98442 0.98617 0.98615
3.41 4.29 0.99202 0.99205 0.99381 0.99380 8.24 10.28 0.98438 0.98441 0.98615 0.98614
3.42 4.30 0.99200 0.99203 0.99379 0.99378 8.25 10.29 0.98436 0.98439 0.98614 0.98612
3.43 4.31 0.99199 0.99202 0.99377 0.99377 8.26 10.30 0.98435 0.98438 0.98612 0.98611
3.44 4.32 0.99197 0.99200 0.99376 0.99375 8.27 10.31 0.98433 0.98436 0.98611 0.98609
3.45 4.34 0.99195 0.99198 0.99374 0.99373 8.28 10.33 0.98432 0.98435 0.98609 0.98608
3.46 4.35 0.99194 0.99196 0.99372 0.99372 8.29 10.34 0.98430 0.98433 0.98608 0.98606
3.47 4.36 0.99192 0.99195 0.99371 0.99370 8.30 10.35 0.98429 0.98432 0.98606 0.98605
3.48 4.37 0.99190 0.99193 0.99369 0.99368 8.31 10.36 0.98428 0.98430 0.98605 0.98603
3.49 4.39 0.99189 0.99191 0.99367 0.99367 8.32 10.38 0.98426 0.98429 0.98603 0.98602
3.50 4.40 0.99187 0.99190 0.99365 0.99365 8.33 10.39 0.98425 0.98427 0.98602 0.98600
3.51 4.41 0.99185 0.99188 0.99364 0.99363 8.34 10.40 0.98423 0.98426 0.98600 0.98599
3.52 4.42 0.99183 0.99186 0.99362 0.99361 8.35 10.41 0.98422 0.98424 0.98599 0.98597
3.53 4.44 0.99182 0.99185 0.99360 0.99360 8.36 10.43 0.98420 0.98423 0.98597 0.98596
3.54 4.45 0.99180 0.99183 0.99359 0.99358 8.37 10.44 0.98419 0.98421 0.98596 0.98594
3.55 4.46 0.99178 0.99181 0.99357 0.99356 8.38 10.45 0.98417 0.98420 0.98594 0.98593
3.56 4.47 0.99177 0.99179 0.99355 0.99355 8.39 10.46 0.98416 0.98419 0.98593 0.98591
3.57 4.49 0.99175 0.99178 0.99353 0.99353 8.40 10.47 0.98414 0.98417 0.98592 0.98590
3.58 4.50 0.99173 0.99176 0.99352 0.99351 8.41 10.49 0.98413 0.98416 0.98590 0.98589
3.59 4.51 0.99172 0.99174 0.99350 0.99349 8.42 10.50 0.98411 0.98414 0.98589 0.98587
%m/m %V/V
g/cm
3
- - - %m/m %V/V
g/cm
3
- - -
C27IB02 123
3.60 4.52 0.99170 0.99173 0.99348 0.99348 8.43 10.51 0.98410 0.98413 0.98587 0.98586
3.61 4.54 0.99168 0.99171 0.99347 0.99346 8.44 10.52 0.98408 0.98411 0.98586 0.98584
3.62 4.55 0.99166 0.99169 0.99345 0.99344 8.45 10.54 0.98407 0.98410 0.98584 0.98583
3.63 4.56 0.99165 0.99168 0.99343 0.99343 8.46 10.55 0.98406 0.98408 0.98583 0.98581
3.64 4.57 0.99163 0.99166 0.99342 0.99341 8.47 10.56 0.98404 0.98407 0.98581 0.98580
3.65 4.59 0.99161 0.99164 0.99340 0.99339 8.48 10.57 0.98403 0.98405 0.98580 0.98578
3.66 4.60 0.99160 0.99162 0.99338 0.99338 8.49 10.59 0.98401 0.98404 0.98578 0.98577
3.67 4.61 0.99158 0.99161 0.99337 0.99336 8.50 10.60 0.98400 0.98402 0.98577 0.98575
3.68 4.62 0.99156 0.99159 0.99335 0.99334 8.51 10.61 0.98398 0.98401 0.98575 0.98574
3.69 4.64 0.99155 0.99157 0.99333 0.99332 8.52 10.62 0.98397 0.98400 0.98574 0.98572
3.70 4.65 0.99153 0.99156 0.99331 0.99331 8.53 10.63 0.98395 0.98398 0.98572 0.98571
3.71 4.66 0.99151 0.99154 0.99330 0.99329 8.54 10.65 0.98394 0.98397 0.98571 0.98569
3.72 4.67 0.99150 0.99152 0.99328 0.99327 8.55 10.66 0.98392 0.98395 0.98570 0.98568
3.73 4.69 0.99148 0.99151 0.99326 0.99326 8.56 10.67 0.98391 0.98394 0.98568 0.98567
3.74 4.70 0.99146 0.99149 0.99325 0.99324 8.57 10.68 0.98389 0.98392 0.98567 0.98565
3.75 4.71 0.99144 0.99147 0.99323 0.99322 8.58 10.70 0.98388 0.98391 0.98565 0.98564
3.76 4.72 0.99143 0.99146 0.99321 0.99321 8.59 10.71 0.98387 0.98389 0.98564 0.98562
3.77 4.74 0.99141 0.99144 0.99320 0.99319 8.60 10.72 0.98385 0.98388 0.98562 0.98561
3.78 4.75 0.99139 0.99142 0.99318 0.99317 8.61 10.73 0.98384 0.98386 0.98561 0.98559
3.79 4.76 0.99138 0.99141 0.99316 0.99316 8.62 10.75 0.98382 0.98385 0.98559 0.98558
3.80 4.77 0.99136 0.99139 0.99315 0.99314 8.63 10.76 0.98381 0.98383 0.98558 0.98556
3.81 4.79 0.99134 0.99137 0.99313 0.99312 8.64 10.77 0.98379 0.98382 0.98556 0.98555
3.82 4.80 0.99133 0.99135 0.99311 0.99310 8.65 10.78 0.98378 0.98381 0.98555 0.98553
3.83 4.81 0.99131 0.99134 0.99309 0.99309 8.66 10.79 0.98376 0.98379 0.98553 0.98552
3.84 4.82 0.99129 0.99132 0.99308 0.99307 8.67 10.81 0.98375 0.98378 0.98552 0.98550
3.85 4.84 0.99128 0.99130 0.99306 0.99305 8.68 10.82 0.98373 0.98376 0.98551 0.98549
3.86 4.85 0.99126 0.99129 0.99304 0.99304 8.69 10.83 0.98372 0.98375 0.98549 0.98548
3.87 4.86 0.99124 0.99127 0.99303 0.99302 8.70 10.84 0.98371 0.98373 0.98548 0.98546
3.88 4.87 0.99123 0.99125 0.99301 0.99300 8.71 10.86 0.98369 0.98372 0.98546 0.98545
3.89 4.89 0.99121 0.99124 0.99299 0.99299 8.72 10.87 0.98368 0.98370 0.98545 0.98543
3.90 4.90 0.99119 0.99122 0.99298 0.99297 8.73 10.88 0.98366 0.98369 0.98543 0.98542
3.91 4.91 0.99118 0.99120 0.99296 0.99295 8.74 10.89 0.98365 0.98368 0.98542 0.98540
3.92 4.92 0.99116 0.99119 0.99294 0.99294 8.75 10.91 0.98363 0.98366 0.98540 0.98539
3.93 4.94 0.99114 0.99117 0.99293 0.99292 8.76 10.92 0.98362 0.98365 0.98539 0.98537
3.94 4.95 0.99113 0.99115 0.99291 0.99290 8.77 10.93 0.98360 0.98363 0.98537 0.98536
3.95 4.96 0.99111 0.99114 0.99289 0.99289 8.78 10.94 0.98359 0.98362 0.98536 0.98534
3.96 4.97 0.99109 0.99112 0.99288 0.99287 8.79 10.95 0.98358 0.98360 0.98535 0.98533
3.97 4.99 0.99107 0.99110 0.99286 0.99285 8.80 10.97 0.98356 0.98359 0.98533 0.98532
3.98 5.00 0.99106 0.99109 0.99284 0.99284 8.81 10.98 0.98355 0.98357 0.98532 0.98530
3.99 5.01 0.99104 0.99107 0.99283 0.99282 8.82 10.99 0.98353 0.98356 0.98530 0.98529
4.00 5.02 0.99102 0.99105 0.99281 0.99280 8.83 11.00 0.98352 0.98354 0.98529 0.98527
4.01 5.04 0.99101 0.99104 0.99279 0.99279 8.84 11.02 0.98350 0.98353 0.98527 0.98526
4.02 5.05 0.99099 0.99102 0.99278 0.99277 8.85 11.03 0.98349 0.98352 0.98526 0.98524
4.03 5.06 0.99097 0.99100 0.99276 0.99275 8.86 11.04 0.98347 0.98350 0.98524 0.98523
4.04 5.07 0.99096 0.99099 0.99274 0.99273 8.87 11.05 0.98346 0.98349 0.98523 0.98521
4.05 5.09 0.99094 0.99097 0.99273 0.99272 8.88 11.07 0.98344 0.98347 0.98522 0.98520
4.06 5.10 0.99092 0.99095 0.99271 0.99270 8.89 11.08 0.98343 0.98346 0.98520 0.98518
4.07 5.11 0.99091 0.99094 0.99269 0.99268 8.90 11.09 0.98342 0.98344 0.98519 0.98517
%m/m %V/V
g/cm
3
- - - %m/m %V/V
g/cm
3
- - -
124 C27IB02
4.08 5.12 0.99089 0.99092 0.99267 0.99267 8.91 11.10 0.98340 0.98343 0.98517 0.98516
4.09 5.13 0.99087 0.99090 0.99266 0.99265 8.92 11.11 0.98339 0.98341 0.98516 0.98514
4.10 5.15 0.99086 0.99089 0.99264 0.99263 8.93 11.13 0.98337 0.98340 0.98514 0.98513
4.11 5.16 0.99084 0.99087 0.99262 0.99262 8.94 11.14 0.98336 0.98339 0.98513 0.98511
4.12 5.17 0.99082 0.99085 0.99261 0.99260 8.95 11.15 0.98334 0.98337 0.98511 0.98510
4.13 5.18 0.99081 0.99084 0.99259 0.99258 8.96 11.16 0.98333 0.98336 0.98510 0.98508
4.14 5.20 0.99079 0.99082 0.99257 0.99257 8.97 11.18 0.98331 0.98334 0.98508 0.98507
4.15 5.21 0.99077 0.99080 0.99256 0.99255 8.98 11.19 0.98330 0.98333 0.98507 0.98505
4.16 5.22 0.99076 0.99079 0.99254 0.99253 8.99 11.20 0.98329 0.98331 0.98506 0.98504
4.17 5.23 0.99074 0.99077 0.99252 0.99252 9.00 11.21 0.98327 0.98330 0.98504 0.98503
4.18 5.25 0.99072 0.99075 0.99251 0.99250 9.01 11.22 0.98326 0.98328 0.98503 0.98501
4.19 5.26 0.99071 0.99074 0.99249 0.99248 9.02 11.24 0.98324 0.98327 0.98501 0.98500
4.20 5.27 0.99069 0.99072 0.99247 0.99247 9.03 11.25 0.98323 0.98326 0.98500 0.98498
4.21 5.28 0.99067 0.99070 0.99246 0.99245 9.04 11.26 0.98321 0.98324 0.98498 0.98497
4.22 5.30 0.99066 0.99069 0.99244 0.99243 9.05 11.27 0.98320 0.98323 0.98497 0.98495
4.23 5.31 0.99064 0.99067 0.99242 0.99242 9.06 11.29 0.98318 0.98321 0.98495 0.98494
4.24 5.32 0.99062 0.99065 0.99241 0.99240 9.07 11.30 0.98317 0.98320 0.98494 0.98492
4.25 5.33 0.99061 0.99064 0.99239 0.99238 9.08 11.31 0.98316 0.98318 0.98493 0.98491
4.26 5.35 0.99059 0.99062 0.99237 0.99237 9.09 11.32 0.98314 0.98317 0.98491 0.98490
4.27 5.36 0.99057 0.99060 0.99236 0.99235 9.10 11.34 0.98313 0.98315 0.98490 0.98488
4.28 5.37 0.99056 0.99059 0.99234 0.99233 9.11 11.35 0.98311 0.98314 0.98488 0.98487
4.29 5.38 0.99054 0.99057 0.99232 0.99232 9.12 11.36 0.98310 0.98313 0.98487 0.98485
4.30 5.40 0.99053 0.99055 0.99231 0.99230 9.13 11.37 0.98308 0.98311 0.98485 0.98484
4.31 5.41 0.99051 0.99054 0.99229 0.99228 9.14 11.38 0.98307 0.98310 0.98484 0.98482
4.32 5.42 0.99049 0.99052 0.99228 0.99227 9.15 11.40 0.98306 0.98308 0.98483 0.98481
4.33 5.43 0.99048 0.99050 0.99226 0.99225 9.16 11.41 0.98304 0.98307 0.98481 0.98479
4.34 5.45 0.99046 0.99049 0.99224 0.99223 9.17 11.42 0.98303 0.98305 0.98480 0.98478
4.35 5.46 0.99044 0.99047 0.99223 0.99222 9.18 11.43 0.98301 0.98304 0.98478 0.98477
4.36 5.47 0.99043 0.99045 0.99221 0.99220 9.19 11.45 0.98300 0.98303 0.98477 0.98475
4.37 5.48 0.99041 0.99044 0.99219 0.99218 9.20 11.46 0.98298 0.98301 0.98475 0.98474
4.38 5.50 0.99039 0.99042 0.99218 0.99217 9.21 11.47 0.98297 0.98300 0.98474 0.98472
4.39 5.51 0.99038 0.99040 0.99216 0.99215 9.22 11.48 0.98296 0.98298 0.98472 0.98471
4.40 5.52 0.99036 0.99039 0.99214 0.99213 9.23 11.50 0.98294 0.98297 0.98471 0.98469
4.41 5.53 0.99034 0.99037 0.99213 0.99212 9.24 11.51 0.98293 0.98295 0.98470 0.98468
4.42 5.55 0.99033 0.99035 0.99211 0.99210 9.25 11.52 0.98291 0.98294 0.98468 0.98466
4.43 5.56 0.99031 0.99034 0.99209 0.99209 9.26 11.53 0.98290 0.98293 0.98467 0.98465
4.44 5.57 0.99029 0.99032 0.99208 0.99207 9.27 11.54 0.98288 0.98291 0.98465 0.98464
4.45 5.58 0.99028 0.99030 0.99206 0.99205 9.28 11.56 0.98287 0.98290 0.98464 0.98462
4.46 5.60 0.99026 0.99029 0.99204 0.99204 9.29 11.57 0.98285 0.98288 0.98462 0.98461
4.47 5.61 0.99024 0.99027 0.99203 0.99202 9.30 11.58 0.98284 0.98287 0.98461 0.98459
4.48 5.62 0.99023 0.99026 0.99201 0.99200 9.31 11.59 0.98283 0.98285 0.98460 0.98458
4.49 5.63 0.99021 0.99024 0.99199 0.99199 9.32 11.61 0.98281 0.98284 0.98458 0.98456
4.50 5.65 0.99019 0.99022 0.99198 0.99197 9.33 11.62 0.98280 0.98283 0.98457 0.98455
4.51 5.66 0.99018 0.99021 0.99196 0.99195 9.34 11.63 0.98278 0.98281 0.98455 0.98454
4.52 5.67 0.99016 0.99019 0.99194 0.99194 9.35 11.64 0.98277 0.98280 0.98454 0.98452
4.53 5.68 0.99015 0.99017 0.99193 0.99192 9.36 11.65 0.98275 0.98278 0.98452 0.98451
4.54 5.70 0.99013 0.99016 0.99191 0.99190 9.37 11.67 0.98274 0.98277 0.98451 0.98449
4.55 5.71 0.99011 0.99014 0.99189 0.99189 9.38 11.68 0.98273 0.98275 0.98450 0.98448
%m/m %V/V
g/cm
3
- - - %m/m %V/V
g/cm
3
- - -
C27IB02 125
4.56 5.72 0.99010 0.99012 0.99188 0.99187 9.39 11.69 0.98271 0.98274 0.98448 0.98446
4.57 5.73 0.99008 0.99011 0.99186 0.99185 9.40 11.70 0.98270 0.98273 0.98447 0.98445
4.58 5.75 0.99006 0.99009 0.99185 0.99184 9.41 11.72 0.98268 0.98271 0.98445 0.98444
4.59 5.76 0.99005 0.99007 0.99183 0.99182 9.42 11.73 0.98267 0.98270 0.98444 0.98442
4.60 5.77 0.99003 0.99006 0.99181 0.99180 9.43 11.74 0.98265 0.98268 0.98442 0.98441
4.61 5.78 0.99001 0.99004 0.99180 0.99179 9.44 11.75 0.98264 0.98267 0.98441 0.98439
4.62 5.80 0.99000 0.99003 0.99178 0.99177 9.45 11.77 0.98263 0.98265 0.98440 0.98438
4.63 5.81 0.98998 0.99001 0.99176 0.99176 9.46 11.78 0.98261 0.98264 0.98438 0.98436
4.64 5.82 0.98996 0.98999 0.99175 0.99174 9.47 11.79 0.98260 0.98263 0.98437 0.98435
4.65 5.83 0.98995 0.98998 0.99173 0.99172 9.48 11.80 0.98258 0.98261 0.98435 0.98434
4.66 5.84 0.98993 0.98996 0.99171 0.99171 9.49 11.81 0.98257 0.98260 0.98434 0.98432
4.67 5.86 0.98992 0.98994 0.99170 0.99169 9.50 11.83 0.98256 0.98258 0.98432 0.98431
4.68 5.87 0.98990 0.98993 0.99168 0.99167 9.51 11.84 0.98254 0.98257 0.98431 0.98429
4.69 5.88 0.98988 0.98991 0.99166 0.99166 9.52 11.85 0.98253 0.98255 0.98430 0.98428
4.70 5.89 0.98987 0.98989 0.99165 0.99164 9.53 11.86 0.98251 0.98254 0.98428 0.98426
4.71 5.91 0.98985 0.98988 0.99163 0.99162 9.54 11.88 0.98250 0.98253 0.98427 0.98425
4.72 5.92 0.98983 0.98986 0.99162 0.99161 9.55 11.89 0.98248 0.98251 0.98425 0.98424
4.73 5.93 0.98982 0.98985 0.99160 0.99159 9.56 11.90 0.98247 0.98250 0.98424 0.98422
4.74 5.94 0.98980 0.98983 0.99158 0.99157 9.57 11.91 0.98246 0.98248 0.98422 0.98421
4.75 5.96 0.98978 0.98981 0.99157 0.99156 9.58 11.93 0.98244 0.98247 0.98421 0.98419
4.76 5.97 0.98977 0.98980 0.99155 0.99154 9.59 11.94 0.98243 0.98245 0.98420 0.98418
4.77 5.98 0.98975 0.98978 0.99153 0.99153 9.60 11.95 0.98241 0.98244 0.98418 0.98416
4.78 5.99 0.98974 0.98976 0.99152 0.99151 9.61 11.96 0.98240 0.98243 0.98417 0.98415
4.79 6.01 0.98972 0.98975 0.99150 0.99149 9.62 11.97 0.98238 0.98241 0.98415 0.98414
4.80 6.02 0.98970 0.98973 0.99148 0.99148 9.63 11.99 0.98237 0.98240 0.98414 0.98412
4.81 6.03 0.98969 0.98971 0.99147 0.99146 9.64 12.00 0.98236 0.98238 0.98412 0.98411
4.82 6.04 0.98967 0.98970 0.99145 0.99144
%m/m %V/V
g/cm
3
- - - %m/m %V/V
g/cm
3
- - -
Appendix K: Menu Tree
126 C27IB02
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Index
128 C27IB02
Index
A
Adjustment 38, 41, 45, 48, 52, 76, 77, 102, 103,
104
Adjustment data 76, 77
Air bubbles 43
Air pump 27
Alcohol adjustment 38
Alcohol concentration 43, 76, 77, 90, 102, 115
Alcohol content 26, 38, 64, 86, 87, 88, 89, 90, 93,
96, 115
Alcohol correction factor 35, 64
Ambient temperature 46, 105
Apparent degree of fermentation 87, 88, 95
Apparent density 86, 88, 93
Apparent extract 86, 88, 94
ASBC 26, 51, 64, 79, 86, 87, 88, 89, 96
B
Bar code reader 28, 60, 61, 75
BEER 34, 60, 82
Beer parameter 91
Beer temperature 98
Beer types 64
Buffer 53, 54, 56, 104
Buffer data 52, 55, 77
C
Calculation 93
Calories 87, 88, 95
Checking procedure 43, 44, 45, 63
CIDER 34, 60, 82
Cleaning 72
Color concentration 103
Color measurement 26, 47, 79, 88, 96
Color standard 51
COM1 28, 30, 79, 92, 105, 106, 108
COM2 28, 30, 80, 105, 108
Concentration 38, 40, 41, 43, 48, 51
Control measurement 38, 45
Control parameter 23, 64
Control solution 38
D
Data memory 33, 66, 89
Data set 66, 83
Default settings 90
Degassing 98
Denaturant 43, 48
Density 59, 90, 93, 115
Density meter 43, 79
Desiccator 28
Device list 21, 23, 30, 34
Display 25, 33
Display configuration 33
Display contrast 25, 28, 29
DMA 87, 89, 108, 109
E
EBC 26, 51, 64, 79, 86, 88, 96
Error message 102, 103, 104
F
Factory adjustment 104
Filling time 34, 63
Firmware 90
G
Gas bubbles 48, 49, 63
I
Instrument settings 29, 78, 90
Interface cable 106, 108
Interface configuration 79
Interface settings 106
IUPAC 87, 89, 96
K
KCl solution 64
Keyboard 28, 60, 61, 75, 79
L
Language 78
M
Main menu 27, 29, 74
Measuring parameter 38, 44, 49, 91
Measuring range 105
Method 25, 34, 60, 63, 64, 82, 85
Method settings 82
MOLASSES 32, 33, 35, 99, 101
Index
C27IB02 129
O
Offset 82, 83, 85
Original extract 86, 88, 94
Output configuration 33, 85
P
Parameter 26, 33, 38, 59, 66, 78, 85, 91
Parameter calculator 90
Password 84, 91, 92
pH adjustment 38, 54
pH buffer 38, 52
pH electrode 17, 28, 52, 64, 69, 77
pH measuring cell 15, 16, 18, 44, 54, 112
pH value 26, 41, 44, 52, 64, 88
Printer 33, 78, 79, 80, 90
Printer protocol 35, 82, 85
Printout 59, 65
R
Real degree of fermentation 86, 88, 94, 95
Real extract 86, 88, 94
S
Sample changer 27, 34, 38, 59, 63, 64, 85, 91
Sample identification 27, 59, 63, 84
Sample list 62
SF-1 81, 97
SG 20/04 86, 88, 93, 115
SG 20/20 86, 88, 93, 115
SOFT 60
SOFT DRINK 34, 60
Soft keys 61
Software 92
SOP 27, 38, 40, 63, 89, 90
Specific gravity 86, 88, 93, 94, 115
Stabilization 21, 46
Status message 102, 103, 104
V
Voltage 15, 21, 53
W
WASH 32, 99
Z
Zero adjustment 47
Zero point adjustment 76, 77

Reference Manual: Alcolyzer Plus Beer

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Reference Manual: Alcolyzer Plus Beer

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M

Fill the sample vials 3 mm below the rim with sample

Put the sample vials into the sample changer

Press the <Start> key on the sample changer:

After the end of the measurement, the magazine

After the last measurement, clean the measuring

If a pH electrode is connected, store it in a 3 molar

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