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ENGINEERING MANAGEMENT SUPPORT, INC.

West Lake OU-1

STANDARD LEVEL IV

REPORT OF ANALYSIS

WORK ORDER #13-07154-0R

August 29, 2013

EBERLINE ANALYTICAL/OAK RIDGE LABORATORY

OAK RIDGE, TN

TABLE OF CONTENTS

DESCRIPTION

SECTION
I

Chain of Custody & pH Check Sheet

PAGE
0004
I

I .

II

Sample Acknowledgement

0011

III

Case Narrative

0014

IV

Analytical Results Summary

0018

Analytical Standards

0023

VI

Quality Control Sample Results Summary

0047

VII

Laboratory Technician's Notes

0056

VIII

Analytical Data (Isotopic Uranium)

0086

IX

Analytical Data (Isotopic Thorium)

0170

Analytical Data (Radium-226)

0254

XI

Analytical Data (Radium-228)

0333

XII

Barium-133 Analytical Tracer Data

0350

Last Page Number

0401

t:;:: I?. E;:. E!c. I,,... I N

STANDARD OPERATING PROCEDURE

MP-001, Rev. 12
Effective: 10131112
Page14of14

SERVICES

Sample Receiving

Eberline Services - Oak Ridge Laboratory

LABORATORY DATA SUPPORT CHECKLIST

MP-001-3

Eberline Services Work Order #_ _

~1~3~--0_7_1_5_4_ ____

The checklist items listed below are to be initialed by appropriate staff upon completion/verification.

Date for Partial

Initials

Date

Initials

Checklist Items
Sample Log-In

KC

t-JS: 13

Data Compilation
FirstTechnical Data Review
Second Technical Data Review
Data Entry/Electronic Deliverable
Case Narrative
Electronic Deliverable Proof
Samples A'IOOlyzed within Holding Time
v~ ...

A.

111.1,.? I

QA/QC/Review

'

Client 1n Possession of Data

ni-

l-l~::url

r':nn\I

Invoiced by Laboratory

Technical/Clerical Corrections,

Date package approved by:

Sign~tures

Date/Initials

Needed, Problems, Etc

~~ "\
I

Laboratory Manager

~r~1r tr<..._
'

Date

\._.,
Copy No.

Radiochemistry Services

SECTION I
CHAIN OF CUSTODY
&

pH CHECK SHEET

13-01154

Chain of Custody Record

N~

E1>ert1n1 Semen
601 Scalt>Olo Road

1604

Olk Ridgo, TN 37830


(865) 48Ml683 ~ (865) 483-4621 Fax

.
Project Name:fJh ""fl- f-.A~()Y/
)

Send Report To:~


Address:~C>

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Project Number:
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Sampler (Print Name):
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Laboratory Receiving:

Phone:

sample
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REC'D JUL 2 2 2013

Sample Receipt

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Level I

Level II
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Other

Cl

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Total # Containers Racelved?


COC Seals Present?
COC Seals Intact?
Received Containers Intact?
Temperature?

Internal
EBERLINE

Chain of
Custody

SERVICES

Oak Ridge Laboratory

Work Order#

Analysis
Sample Matrix

Sample
Fraction

Comments

UUISO - Level 4
Water

HP 210 I 270 i
Detector Activity I
I

Storage
Location

Wl.4

Fxns 04, 06, 08, 10 & 12 are TOTAL

Wl.4
Wl.4
Wl.4

Fxns 05, 07, 09, 11 & 13 are DISSOLVED

Wl.4
+

Wl.4
Wl.4
Wl.4

13

MUST USE FXN 08 FOR DUP

Location (circle one


Rough Prep

Received by

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Printed:

7/24/2013 1:41 PM

Sfilfilc

.
EBERLINE
SERVICES

Oak Ridge Laboratory

Internal

Work Order#

13-07154

Chain of
Custody

Lab Deadline

8/13/2013
ThlSO - Level 4

Analysis

Water

Sample Matrix

Sample
Fraction

Comments

04

HP 210 I 270

I Detector Activity

Storage
Location

42

Wl.4

42

Wl.4

38

Wl.4

Fxns 04, 06, 08, 10 & 12 are TOT AL

Wl.4
46

Wl.4

46

Wl.4

10

45

Wl.4

11

45

Wl.4

44

Wl.4

Fxns 05, 07, 09, 11 & 13 are DISSOLVED

MUST USE FXN 08 FOR DUP

Location circle one


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Printed: 712412013 1:41 PM

'fi:fi87

Internal
EBERLINE

Chain of
Custody

SERVICES

Oak Ridge Laboratory

Work Order#

13-07154

Lab Deadline

8/13/2013
Water

Sample Matrix

Sample
Fraction

Comments

Ra226 - Level 4

Analysis

Fxns 04, 06, 08, 10 & 12 are TOTAL


Fxns 05, 07, 09, 11 & 13 are DISSOLVED

HP 210 I 270
Detector Activity

Storage
Location

42

Wl.4

42

Wl.4

38

Wl.4

38

Wl.4

46

Wl.4

46

Wl.4

45

Wl.4

44

Wl.4

44

Wl.4

MUST USE FXN 08 FOR DUP

Location circle one


Received by

Prep

Separations

Count Room

Relinquished by

Sample Storage

Received by

Sample Storage

Relinquished by

Sample Storage

Rough Prep

Prep

Received by

Sample Storage

Rough Prep

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Sample Storage

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Rough Prep

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Received by

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Received by

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Prep

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Received by

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Rough Prep

Count Room

Count Room

Separations

Printed: 7/24/2013 1:41 PM

ilJi!JS

.
EBERLINE
SERVICES

Oak Ridge Laboratory

Internal

Work Order#

13-07154

Chain of
Custody

Lab Deadline

8/13/2013

Analysis

Ra228 - Level 4
Water

Sample Matrix

Comments

Sample
Fraction

HP 210 I 270
Detector Activity

Storage
Location

04
05
06

42

Wl.4

Fxns 04, 06, 08, 10 & 12 are TOTAL


Fxns 05, 07, 09, 11 & 13 are DISSOLVED

Wl.4
Wl.4

38

Wl.4

46

Wl.4

46

Wl.4

45

Wl.4

45

Wl.4

44

Wl.4

MUST USE FXN 08 FOR DUP

Date

Location circle one


Received by

Prep

Count Room

Separations

Relinquished by

Sample Storage

Count Room

Received by

Sample Storage

Count Room

Relinquished by

Sample Storage

Rough Prep

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Printed: 7/24/2013 1:41 PM

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Page 1of1

Printed: 7 /24/2013 11:14 AM

Internal Work Order

FR

KCOULSTON
ClientID

LCS

Comments

# Btls

BLANK
DUP

0
0
0

04

PZ-200-SS TOT,.

2
.....

....

Container Number
1
71

PZ-200-SS DIS"'

2
Container Number

PZ-102-SS TOT./

Wl.4
Wl.4
Wl.4

WA

Wl.4

.. Dl:!'Oria
<2
<:r

. DH Final
<2
<2

WA

Wl.4

oHOria

pHFinal

Rec Vol Ttl CPM Max

8.00

2
Container Number

PZ-107-SS TOT/

'.

4.

42

0.00

42

va1J1ine,1L1

oHOria
<.?...............

<2

42

<2
Wl.4

oH.Oria

l>HFinal

WA

Wl.4

38

CPM ....
oiumelLL .
4.0000 .
38
-~35-~
0000

PH Final.
<2

WA

09

PZ-107-SS DIS'

"

3
.

'

..

.,

...

0.00
Volume 1u.

DHFJnal
<2
<2
<2

4.0000
4.0000

..

~-:.roooo

PZ-106-KS TOT/

Container Number.
1

f.

11

PZ-106-KS DIS

,'

Container Number

12

DUP 08 TOT/

.. 43

I-

DUP 08 DIS /

..

by:~ Giiui:CM.,

Date:

1/24 /J..3

8.00

45

:volume Ill
4.0000

CPM..
45
45

Wl.4
pH Final
<2
<2

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WA

Wl.4

ioHOrla

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<2

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Wl.4
pH Final'
<2 ......

~-<2'

Wl.4
oHFinal

45

0.00

CPM' ,;;
45
45 ..........

Volum!fU.:l
I

WA
Container Number

Received

liHOria
<2
<2

WA
Container Number

13

'""'''~~

46

46
-~

,........

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.CPM'
39

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2
3

10

CPM'
39,
43

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38

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i

CPM
37 . ...

8.00

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<2
2
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3

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4~~-1.L~

08

42

....

Volunilf"' .

,..
WA

PZ-102-SS DIS/

Storaae

WA
WA
WA

2
Container Number

07

Matrix

,....

06

Received By

(Volumes, pH,&. CPM)

SERVICES

01
02
03

05

13-07154

Sample Receiving Report

E.a e:: R . L -1.N E:

44

8.00

:volume 1n> , ,
CPM
4.0000..
38
-44'""'
...
4.0000

~"~~,~-

44

0.00
vo111m:e-.1i::1.

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44

MP-001, Rev 5
Effective: 11/22/02

SECTION II

SAMPLE ACKNOWLEDGEMENT

Client Name

___

L__Contracti!'_Q _____j__l>r_oject_!e':' .

Engineering Management Support, Inc. I West Lake

ou-11
___l

Project Name

Client WO

West Lake OU-1

Westlake OU-1'

Internal ID

Client ID

Sample Date

Matrix

Environmental

07/22/2013

Sample D~f>

Lab Deadline

08/13/2013

Storage

01

LCS

07/24/13

WA

Wl.4

02

BLANK

07/24/13

WA

Wl.4

03

DUP

07/24/13

WA

Wl.4

04

PZ-200-SS TOT

07/19/13 10:19

WA

Wl.4

05

PZ-200-SS DIS

07/19/13 10:19

WA

Wl.4

06

PZ-102-SS TOT

07/19/13 10:30

WA

Wl.4

07

PZ-102-SS DIS

07/19/13 10:30

WA

Wl.4

08

PZ-107-SS TOT

07/19/13 12:10

WA

Wl.4

09

PZ-107-SS DIS

07/19/13 12: 10

WA

Wl.4

10

PZ-106-KS TOT

07/19/13 13:09

WA

Wl.4

11

PZ-106-KS DIS

07/19/13 13:09

WA

Wl.4

12

DUP 08 TOT

07/19/13 00:00

WA

Wl.4

13

DUP 08 DIS

07/19/13 00:00

WA

Wl.4

J
x
x
x
x
x
x
x
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. .....

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-----~e_'!"ired Tur_nar()_"_n_d D~ -

Date Received
-~--------

13-07154

28
Internal Deadline
-------------.. - - - - - -

I.'

08/19/2013

08/16/2013

I;::

XI

I 4

XI

I 4

XI

I 4

XI

I 4

x
x

4
4

XI

I 4

XI

I 4

x
x
x
x
x

4
4
4
4
4

I
Totals Per Analysis (non QA samples)

Invoice

~
...

EBERLINE
SERVICES

10 I 10

Oak Ridge Laboratory


601 Scarboro Rd.
Oak Ridge, TN 37830
Voice

Sample Log In Report

Voice: (865) 481-0683


Fax:
(865) 483-4621

10 I 10

0 i 0

i
I

Paul V. Rosasco, P .E.

o I o

i0

Report Data

0 ; 0

Engineering Management Support, Inc

7220 West Jefferson Avenue, Surte 406

7220 West Jefferson Ave, Suite 406

Lakewood, CO 80235

Lakewood, CO 80235

303-640-3426

I0

0 I 0

I I

Paul V. Rosasco, P.E.

Engineenng Management Support, Inc.

Fax

I0

Voia>

303-940-3426

Fax

Contact

Lyn Fitzgerald

Voice

1303-601-4255

Fax

~
J.il!ii

t..:V

Printed: 7/24/2013 1:41 PM

STANDARD OPERATING PROCEDURE

MP-001, Rev.12
Effective: 10131112
Page 13of14

Sample Receiving

Eberline Services - Oak Ridge Laboratory


SAMPLE RECEIPT CHECKLIST

MP-001-2

13-07154

WORK ORDER#_~~~---~~
SAMPLE MATRIX/MATRICES:

(CIRCLE ONE OR BOTH)

NON-AQUEOUS

(CIRCLE EITHER YES, NO, OR N/A)


WERE SAMPLES
Received in good condition?

If aqueous, properly preserved

Present on outside of package?

Unbroken on outside of package?

N/A

WERE CHAIN OF CUSTODY SEALS

Present on samples?
Unbroken on samples?
Was chain of custody present upon sample receipt?

(/)
(y)
~

N
N
N

IF THE RESPONSE TO ANY OF THE ABOVE IS NO, A DISCREPANT SAMPLE RECEIPT REPORT
(DSR) HAS BEEN ISSUED.
REMARKS:~~~~~~~~~~~~~~~~~~~~~~~~~~~~~

SIGNATURE:

Copy No. _ _ __

~~

DATE:

7/24 // 3

Radiochemistry Services

SECTION III

CASE NARRATIVE

EBERLINE ANALYTICAL CORPORATION


601 SCARBORO ROAD
OAK RIDGE, TENNESSEE 37830
PHONE (865) 481-0683
FAX (865) 483-4621

EBS-OR-36009
August 29, 2013
Paul V. Rosasco, P.E.
Engineering Management Support, Inc.
7220 West Jefferson Ave, Suite 406
Lakewood, CO 80235
CASE NARRATIVE
Work Order# 13-07154-0R
SAMPLE RECEIPT
This work order contains five water samples received 07/22/2013. All samples were analyzed as total and
dissolved for Isotopic Uranium, Isotopic Thorium and Radium-226/228.
CLIENT ID

LAB ID

CLIENT ID

LAB ID

PZ-200-SS TOT
PZ-200-SS DIS
PZ-102-SS TOT
PZ-102-SS DIS
PZ-107-SS TOT

13-07154-04
13-07154-05
13-07154-06
13-07154-07
13-07154-08

PZ-107-SS DIS
PZ-106-KS TOT
PZ-106-KS DIS
DUP08TOT
DUP08 DIS

13-07154-09
13-07I54-10
13-07154-11
13-07154-12

13-07154-13

ANALYTICAL METHODS

Isotopic Uranium and Isotopic Thorium were analyzed using Method HASL 300, 4.5.2. Radium-226 was

analyzed using Method EPA 903.0. Radium-228 was analyzed using Method EPA 904.0.

Laboratory qualifiers are as follows:

J-

Indicates a situation where the result minus the error is less than the detection limit but greater

than zero.

U-

Indicates a situation where the result minus the error is less than or equal to zero.

ANALYTICAL RESULTS
Combined Standard Uncertainty is reported at 2-sigma value.

Page I of3

ANALYTICAL RESULTS CONTINUED

ISOTOPIC URANIUM
Samples were prepared by removing representative aliquots followed by mixed acid digestions as
appropriate. Uranium was selectively extracted by ion exchange. Uranium was eluted, micro
precipitated and mounted on micro-porous filter media. Sample activities were then determined by alpha
spectroscopy using energy specific regions of interest for Uranium-234, Uranium-235 and Uranium-238.
Chemical recovery was determined by the use of a Uranium-232 tracer. Activity of the Uranium-232
tracer was determined by alpha spectroscopy using an energy specific region of interest.
Samples demonstrated acceptable results for all Uranium analyses. Chemical recovery was acceptable for
all samples. The Uranium-234 method blank demonstrated results slightly greater than the detection
limit. The Uranium-235 and Uranium-238 method blank demonstrated acceptable results. Results for the
Uranium-234 and Uranium-238 duplicate demonstrated an acceptable relative percent difference and
normalized difference. Results for the Uranium-235 duplicate demonstrated a high relative percent
difference; however, normalized difference is within acceptable limits for the analytical technique.
Results for the Uranium-234 and Uranium-238 laboratory control sample demonstrated an acceptable
percent recovery.
ISOTOPIC THORIUM
Samples were prepared by removing representative aliquots followed by mixed acid digestions as
appropriate. Thorium was selectively extracted by ion exchange. Thorium was eluted, micro-precipitated
and mounted on micro-porous filter media. Sample activities were then determined by alpha
spectroscopy using energy specific regions of interest for Thorium-228, Thorium-230 and Thorium-232.
Chemical recovery was determined by the use of a Thorium-229 tracer. Activity of the Thorium-229
tracer was determined by alpha spectroscopy using an energy specific region of interest.
Samples demonstrated acceptable results for all Thorium analyses. Chemical recovery was acceptable for
all samples. The Thorium-228, Thorium-230 and Thorium-232 method blank demonstrated acceptable
results. Results for the Thorium-228 duplicate demonstrated a high relative percent difference; however,
normalized difference is within acceptable limits for the analytical technique. Results for the Thorium
230 and Thorium-232 duplicate demonstrated an acceptable relative percent difference and normalized
difference. Results for the Thorium-228, Thorium-230 and Thorium-232 laboratory control sample
demonstrated an acceptable percent recovery.
RADIUM-226
Samples were prepared by removing representative aliquots as appropriate. This was followed by
selective sulfate precipitations of the Radium. Samples were then mounted by semi-micro-precipitations
onto micro-porous filters. Samples were counted by alpha spectroscopy using an energy specific region
of interest for Radium-226. Chemical recovery was calculated by the use of a Barium-133 tracer, which
was determined by HPGe gamma spectroscopy.
Samples demonstrated acceptable results for all Radium-226 analyses. Chemical recovery was acceptable
for all samples. The Radium-226 method blank demonstrated acceptable results. Results for the Radium
226 duplicate demonstrated an acceptable relative percent difference and normalized difference. Results
for the Radium-226 laboratory control sample demonstrated an acceptable percent recovery.

Page 2 of3

ANALYTICAL RESULTS CONTINUED


RADIUM-228
Following alpha spectroscopy analysis of Radium-226, Barium/Radium Sulfate precipitates were
redissolved and allowed for sufficient ingrowth of the Actinium-228 daughter. After ingrowth, Actinium
228 was selectively precipitated. Precipitates were filtered and beta emissions for Actinium-228 were
then counted on a gas proportional counter. Chemical recovery was determined by the use of a Barium
133 tracer, the activity of which was determined by HPGe gamma spectroscopy and an elemental Yttrium
carrier by gravimetric measurements. The product of these two recoveries was used to calculate chemical
yield.
Samples demonstrated acceptable results for all Radium-228 analyses. Chemical recovery was acceptable
for all samples. The Radium-228 method blank demonstrated acceptable results. Results for the Radium
228 duplicate demonstrated an acceptable relative percent difference and normalized difference. Results
for the Radium-228 laboratory control sample demonstrated an acceptable percent recovery.
CERTIFICATION OF ACCURACY
I certify that this data report is in compliance with the terms and conditions of the Purchase Order, both
technically and for completeness, for other than the conditions detailed above. Release of the data
contained in this hard copy data package has been authorized by the cognizant project manager or his/her
designee to be accurate as verified by the following signature.

M.R. McDougall
Laboratory Manager
Date: 8/29/2013
Eberline Analytical wants and encourages your feedback regarding our performance providing radioanalytical services. Please
visit http://www.eberlineservices.com/client.htm to provide us with feedback on our services.

Page 3 of3

SECTION IV

ANALYTICAL RESULTS SUMMARY

Paul V. Rosasco, P.E.


Engineering Management Support, Inc.
7220 West Jefferson Ave, Suite 406
Lakewood, CO 80235

Client Samole ID

~ ..tr.

tit!

Analv!e

08/09/2013 09:04:56
08/15/2013 07:52:38
08/14/201312:46:13
08/14/201312:46:13
08/14/2013 12:46:13
08/14/2013 09:26:34
08/14/2013 09:26:34
08/1412013 09:26:34

Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238

E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,

BLANK13-07154-02
BLANK13-07154-02
BLANK13-07154-02
BLANK13-07154-02
BLANK13-07154-02
BLANK13-07154-02
BLANK13-07154-02
BLANK13-07154-02

13-07154-02
13-07154-02
13-07154-02
13-07154-02
13-07154-02
13-07154-02
13-07154-02
13-07154-02

08/09/2013 09:04:58
08/15/2013 07:50:55
08/14/2013 12:46:14
08/14/201312:46:14
08/14/201312:46:14
08/14/2013 09:26:35
08/14/2013 09:26:35
08/14/2013 09:26:35

Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238

E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,

13-07154-03
13-07154-03
13-07154-03
13-07154-03
13-07154-03
13-07154-03
13-07154-03
13-07154-03

08/09/2013 09:04:59
08/15/2013 07:50:56
08/14/201312:46:15
08/14/201312:46:15
08/14/201312:46:15
08/14/2013 09:26:36
08/14/2013 09:26:36
08/14/2013 09:26:36

Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238

E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,

13-07154-04
13-07154-04
13-07154-04
13-07154-04
13-07154-04
13-07154-04
13-07154-04
13-07154-04

08/09/2013 09:05:01
08/15/2013 07:50:56
08/14/2013 12:46:39
08/14/2013 12:46:39
08/14/201312:46:39
08/14/2013 09:27:34
08/14/2013 09:27:34
08/14/2013 09:27:34

Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238

E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,

EBERLINE
SERVICES

Result

Error

CSU

MDA

4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2

10.39
8.26
4.75
4.35
4.63
7.96
1.16
8.93

1.17
1.74
0.87
0.82
0.85
1.08
0.30
1.19

2.49
2.55
0.98
0.98
0.95
1.22
0.31
1.35

0.16
1.74
0.13
0.09
0.08
0.06
0.09
0.07

4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2

0.14
0.59
-0.02
0.08
0.04
0.31
0.06
0.06

0.15
0.50
0.07
0.08
0.07
0.13
0.06
0.06

0.15
0.51
0.07
0.09
0.07
0.13
0.06
0.06

0.19
0.99
0.19
0.11
0.11
0.07
0.07
O.Q7

4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2

5.07
2.54
0.87
1.32
1.28
1.31
0.26
1.44

0.94
0.82
0.31
0.41
0.40
0.35
0.16
0.37

1.42
1.00
0.32
0.44
0.42
0.36
0.16
0.39

0.18
1.45
0.12
0.12
0.09
0.11
0.14
0.08

4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2

0.97
1.95
0.17
0.46
0.24
0.96
0.17
0.80

0.39
0.72
0.10
0.18
0.12
0.26
0.12
0.24

-0.44
0.85
0.11
0.19
0.12
0.27
0.12
0.24

0.26
1.30
0.07
0.09
0.07
0.09
0.11
0.08

Method

13-07154-01
13-07154-01
13-07154-01
13-07154-01
13-07154-01
13-07154-01
13-07154-01
13-07154-01

PZ-200-SS TOT_07_19_2013
PZ-200-SS TOT_07_19_2013
PZ-200-SS TOT_07_19_2013
PZ-200-SS TOT_07_19_2013
PZ-200-SS TOT_07_19_2013
PZ-200-SS TOT_07_19_2013
PZ-200-SS TOT_07_19_2013
PZ-200-SS TOT_07_19_2013

~r~

Analysis Date/Time

LCS13-07154-01
LCS13-07154-01
LCS13-07154-01
LCS13-07154-01
LCS13-07154-01
LCS13-07154-01
LCS13-07154-01
LCS13-07154-01

DUP
DUP
DUP
DUP
DUP
DUP
DUP
DUP

Final Report of Analysis


Date: 8/29/2013
Page 1 of 4

Matrix: Water

Lab Sample ID

PZ-107-SS TOT_07_19_2013
PZ-107-SS TOT_07_19_2013
PZ-107-SS TOT_07_19_2013
PZ-107-SS TOT_07_19_2013
PZ-107-SS TOT_07_19_2013
PZ-107-SS TOT_07_19_2013
PZ-107-SS TOT_07_19_2013
PZ-107-SS TOT_07_19_2013

Project: West Lake OU-1


SDG: 1307154
Received: 07/22/2013

EBERLINE ANALYTICAL CORPORATION

601 SCARBORO ROAD OAK RIDGE, TN 37830

865/481-0683

FAX 865/483-4621

Qualifier

Units

pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I

u
J

u
u
u
u
u

J
J

pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I

Paul V. Rosasco, P.E.


Engineering Management Support, Inc.
7220 West Jefferson Ave, Suite 406
Lakewood, CO 80235

Client Samole ID
PZ-200-SS
PZ-200-SS
PZ-200-SS
PZ-200-SS
PZ-200-SS
PZ-200-SS
PZ-200-SS
PZ-200-SS

lli!i

m
fi''1':ll

l:i!~

Project: West Lake OU-1


SDG: 1307154
Received: 07/22/2013
Matrix: Water

Lab Sample ID

Analvsis Dateffime

Analvte

Method

DIS_07_19_2013
DIS_07_19_2013
DIS_07_19_2013
DIS_07_19_2013
DIS_07_19_2013
DIS_07_19_2013
DIS_07_19_2013
DIS_07_19_2013

13-07154-05
13-07154-05
13-07154-05
13-07154-05
13-07154-05
13-07154-05
13-07154-05
13-07154-05

08/09/2013 09:05:03
08/15/2013 07:50:57
08/14/2013 12:46:40
08/14/2013 12:46:40
08/14/2013 12:46:40
08/14/2013 09:27:34
08/14/2013 09:27:34
08/14/2013 09:27:34

Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238

E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,

PZ-102-SS TOT_07_19_2013
PZ-102-SS TOT_07_19_2013
PZ-102-SS TOT_07_19_2013
PZ-102-SS TOT_07_19_2013
PZ-102-SS TOT_07_19_2013
PZ-102-SS TOT_07_19_2013
PZ-102-SS TOT_07_19_2013
PZ-102-SS TOT_07_19_2013

13-07154-06
13-07154-06
13-07154-06
13-07154-06
13-07154-06
13-07154-06
13-07154-06
13-07154-06

08/09/2013 09:05:04
08/15/2013 07:51:00
08/14/2013 12:46:41
08/14/2013 12:46:41
08/14/2013 12:46:41
08/14/2013 09:27:35
08/14/2013 09:27:35
08/14/2013 09:27:35

Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238

E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,

PZ-102-SS
PZ-102-SS
PZ-102-SS
PZ-102-SS
PZ-102-SS
PZ-102-SS
PZ-102-SS
PZ-102-SS

DIS_07_19_2013
DIS_07_19_2013
DIS_07_19_2013
DIS_07_19_2013
DIS_07_19_2013
DIS_07_19_2013
DIS_07_19_2013
DIS_07_19_2013

13-07154-07
13-07154-07
13-07154-07
13-07154-07
13-07154-07
13-07154-07
13-07154-07
13-07154-07

08/09/2013 09:05:06
08/15/2013 07:51 :01
08/14/201312:46:42
08/14/2013 12:46:42
08/14/2013 12:46:42
08/14/2013 09:27:36
08/14/2013 09:27:36
08/14/2013 09:27:36

Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238

E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,

PZ-107-SS TOT_07_19_2013
PZ-107-SS TOT_07_19_2013
PZ-107-SS TOT_07_19_2013
PZ-107-SS TOT_07_19_2013
PZ-107-SS TOT_07_19_2013
PZ-107-SS TOT_07_19_2013
PZ-107-SS TOT_07_19_2013
PZ-107-SS TOT_07_19_2013

13-07154-08
13-07154-08
13-07154-08
13-07154-08
13-07154-08
13-07154-08
13-07154-08
13-07154-08

08/09/2013 09:05:07
08/15/2013 07:51 :01
08/14/201312:46:43
08/14/201312:46:43
08/14/201312:46:43
08/14/2013 09:27:37
08/14/2013 09:27:37
08/14/2013 09:27:37

Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238

E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,

EBERLINE
SERVICES

Final Report of Analysis


Date: 8/29/2013
Page 2 of4

Result

Error

CSU

MDA

4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2

1.80
1.77
0.07
0.14
0.02
0.49
0.06
0.41

0.55
0.60
0.09
0.11
0.05
0.18
0.08
0.16

0.67
0.72
0.09
0.11
0.05
0.18
0.08
0.16

0.29
1.08
0.14
0.12
0.08
0.09
0.13
0.06

4.5.2
4. 5. 2
4.5.2
4.5.2
4.5.2
4.5.2

7.69
5.39
2.99
2.88
2.71
4.67
0.64
4.43

1.16
1.88
0.65
0.63
0.60
0.75
0.23
0.72

2.00
2.24
0.71
0.72
0.65
0.82
0.23
0.79

0.31
3.39
0.07
0.09
0.08
0.08
0.11
0.09

pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I

4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2

3.12
1.88
-0.01
0.19
-0.02
5.84
0.98
3.85

0.65
0.64
0.06
0.13
0.04
0.89
0.29
0.65

0.93
0.76
0.06
0.13
0.04
0.98
0.30
0.70

0.18
1.15
0.16
0.13
0.11
0.08
0.12
0.08

pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I

4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2

6.39
3.03
1.13
1.66
1.38
1.65
0.18
1.42

1.22
0.84
0.35
0.45
0.39
0.36
0.12
0.32

1.82
1.08
0.36
0.49
0.41
0.38
0.12
0.34

0.35
1.44
0.14
0.10
0.10
0.09
0.11
0.06

EBERLINE ANALYTICAL CORPORATION


601 SCARBORO ROAD OAK RIDGE, TN 37830
865/481-0683

FAX 865/483-4621

Qualifier

u
J

u
u

u
J

Units
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I

pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I

Paul V. Rosasco, P.E.


Engineering Management Support, Inc.
7220 West Jefferson Ave, Suite 406
Lakewood, CO 80235

Client Samole ID
PZ-107-SS
PZ-107-SS
PZ-107-SS
PZ-107-SS
PZ-107-SS
PZ-107-SS
PZ-107-SS
PZ-107-SS

~~

f1~)

l"'..!I.

Lab SamPle_IO

Analysis Date/Time

Analvte

13-07154-09
13-07154-09
13-07154-09
13-07154-09
13-07154-09
13-07154-09
13-07154-09
13-07154-09

08/09/2013 09:05:09
08/15/2013 07:51:02
08/14/201312:46:44
08/14/2013 12:46:44
08/14/2013 12:46:44
08/14/2013 09:27:38
08/14/2013 09:27:38
08/14/2013 09:27:38

Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238

E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,

PZ-106-KS TOT_07_19_2013
PZ-106-KS TOT_07_19_2013
PZ-106-KS TOT_07_19_2013
PZ-106-KS TOT_07_19_2013
PZ-106-KS TOT_07_19_2013
PZ-106-KS TOT_07_19_2013
PZ-106-KS TOT_07_19_2013
PZ-106-KS TOT_07_19_2013

13-07154-10
13-07154-10
13-07154-10
13-07154-10
13-07154-10
13-07154-10
13-07154-10
13-07154-10

08/09/2013
08/15/2013
08/1412013
08/14/2013
08/14/2013
08/14/2013
08/14/2013
08/14/2013

09:05: 10
07:50:54
12:46:45
12:46:45
12:46:45
09:27:39
09:27:39
09:27:39

Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238

E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,

PZ-106-KS
PZ-106-KS
PZ-106-KS
PZ-106-KS
PZ-106-KS
PZ-106-KS
PZ-106-KS
PZ-106-KS

13-07154-11
13-07154-11
13-07154-11
13-07154-11
13-07154-11
13-07154-11
13-07154-11
13-07154-11

08/09/2013 09:05:12
08/15/2013 07:50:54
08/14/201312:46:46
08/14/2013 12:46:46
08/14/2013 12:46:46
08/14/2013 09:27:40
08/14/2013 09:27:40
08/14/2013 09:27:40

Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238

E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,

13-07154-12
13-07154-12
13-07154-12
13-07154-12
13-07154-12
13-07154-12
13-07154-12
13-07154-12

08/09/2013
08/15/2013
08/1412013
08/14/2013
08/14/2013
08/14/2013
08/14/2013
08/14/2013

Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238

E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,

DIS_07_19_2013
DIS_07_19_2013
DIS_07_19_2013
DIS_07_19_2013
DIS_07_19_2013
DIS_07_19_2013
DIS_07_19_2013
DIS_07_19_2013

EBERLINE
SERVICES

09:05: 14
07:50:54
12:46:58
12:46:58
12:46:58
09:28:09
09:28:09
09:28:09

Final Report of Analysis


Date: 8/29/2013
Page 3 of4

Method

DIS_07_19_2013
DIS_07_19_2013
DIS_07_19_2013
DIS_07_19_2013
DIS_07_19_2013
DIS_07_19_2013
DIS_07_19_2013
DIS_07_19_2013

DUP 08 TOT_07_19_2013
DUP 08 TOT_07 _19_2013
DUP 08TOT_07_19_2013
DUP 08 TOT_07_19_2013
DUP 08 TOT_07_19_2013
DUP 08 TOT_07_19_2013
DUP 08 TOT_07_19_2013
DUP 08 TOT_07_19_2013

Project: West Lake OU-1


SDG: 1307154
Received: 07/22/2013
Matrix: Water

Result

Error

CSU

MDA

4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2

5.33
2.38
-0.04
0.32
0.04
1.85
0.16
0.83

0.89
0.63
0.14
0.27
0.13
0.55
0.17
0.34

1.43
0.83
0.14
0.28
0.13
0.57
0.17
0.35

0.19
1.08
0.39
0.32
0.29
0.19
0.21
0.18

4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2

0.33
0.22
-0.01
0.14
0.03
2.04
0.31
0.93

0.23
0.60
0.06
0.10
0.06
0.43
0.16
0.26

0.24
0.61
0.06
0.10
0.06
0.45
0.16
0.27

0.18
1.27
0.16
0.09
0.12
0.09
0.10
0.08

4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2

0.35
2.73
0.04
0.06
0.05
2.02
0.22
0.78

0.24
0.71
0.13
0.12
0.12
0.51
0.16
0.30

0.25
0.94
0.13
0.12
0.12
0.53
0.16
0.30

0.21
1.23
0.28
0.23
0.26
0.14
0.14
0.21

4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2

5.32
3.84
1.15
1.33
1.57
1.74
0.31
1.51

0.97
0.87
0.37
0.40
0.45
0.58
0.24
0.53

1.48
1.23
0.38
0.43
0.47
0.60
0.25
0.54

0.18
1.47
0.10
0.12
0.08
0.16
0.22
0.18

EBERLINE ANALYTICAL CORPORATION


601 SCARBORO ROAD OAK RIDGE, TN 37830

8651481-0683

FAX 865/483-4621

Qualifier

u
J

u
u
J

u
u
J

u
u
u
J

Units
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I

Project: West Lake OU-1


SDG: 1307154
Received: 07/22/2013
Matrix: Water

Paul V. Rosasco, P.E.


Engineering Management Support, Inc.
7220 West Jefferson Ave, Suite 406
Lakewood, CO 80235

Client Sample ID
DUP 08 DIS_07_19_2013
DUP 08 DIS_07_19_2013
DUP 08 DIS_07_19_2013
DUP 08 DIS_07_19_2013
DUP 08 DIS_07_19_2013
DUP 08 DIS_07_19_2013
DUP 08DIS_07_19_2013
DUP 08 DIS_07_19_2013

t:i!
~I!

1"1J
"\\~

Lab Sample ID

Analvsis Date/Time

13-07154-13
13-07154-13
13-07154-13
13-07154-13
13-07154-13
13-07154-13
13-07154-13
13-07154-13

08/09/2013 09:26:50
08/15/2013 07:50:55
08/14/2013 12:47:00
08/14/2013 12:47:00
08/14/2013 12:47:00
08/14/2013 09:28:10
08/14/2013 09:28:10
08/14/2013 09:28:10

~EBERLINE
~

SERVICES

Analvte
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238

Final Report of Analysis


Date: 8/29/2013
Page 4 of4

Method
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,

4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2

Result

Error

CSU

MDA

5.09
2.68
0.16
0.25
0.04
1.57
0.24
0.93

0.96
0.73
0.12
0.16
0.06
0.45
0.18
0.32

1.44
0.95
0.13
0.16
0.06
0.46
0.18
0.33

0.32
1.26
0.10
0.14
0.09
0.15
0.18
0.12

EBERLINE ANALYTICAL CORPORATION


601 SCARBORO ROAD OAK RIDGE, TN 37830

865/481-0683

FAX 865/483-4621

Qualifier

J
J

u
J

Units
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I

SECTIONV

ANALYTICAL STANDARDS

LL-8

QA/QC REVIEWED CERTIFICATE OF CALIBRATION


(?q(lllitials_k( ALPHA STANDARD SOLUTION
Date
Radionuclide:
Half Life:
Catalog No.:

7338

Source No.:

479-50

TMAEBERLINE

Customer:

U-238NAT
(4.468 0.005) x IOA9 years

OR2778

P.O.No.:
Reference Date:
January 11995
12:00 PST.
Contained Radioactivity: (Total U) 8.016 .Ci
Contained Radioactivity:

Description of Solution
a. Mass of solution:
b. Chemical form:
c. Carrier content:

(Total U) 297 kBq


.. :;'.

65. 2896 g in a 50 ml flame sealed ampoule


Uranyl Nitrate in H20
None
Approximately 1.3202

d. Density:

.-,.

~.

g/ml @20C.
,,.

Refer to attached technical data sheet

Radioimpurities
Radioactive Daughters

Refer to attached technical data sheet


Radionuclide Concentration

"./."

(fotal U) 0.1228

Method of Calibration

Ci/g.

..

Activity calculations are based upon known specific activity and mass.

...- ...

:.7....... . . .;

......
, ...

i" ~-

;.

Uncertainty of Measurement
a. Systematic uncertainty in instrument calibration:
b. Random uncertainty in assay:

3.0%
0.0%

c. Random uncertainty in weighing(s):


d. Total uncertainty at the 99 % confidence level:

2.0%
3.6%

.....

~. !

.. -.

NIST Traceability
This calibration is implicitly traceable to the National Institute of Standards and Technology.

....

::

'
-,._

...

....

.:.;.'.

Leak Test(s)
See reverse side for Leak Test(s) applied to this source.
Notes
1. Nuclear data were taken from "Table of Radioactive Isotopes", edited by Virginia S. Shirley, 1986 .
2. IPL participates in an NIST measurement assurance program to .:~tablish and maintain implicit traceability for a number of nuclides,
based on the blind assay (and later NIST ~ertitication) of Standard Reference Materials (As in NRC Regulatory Guide 4.15).

,... .

..'

.. ~. :

:.. -.

YCONTROL

! : ~

Date Signed
ISOTOPE PRODUCTS LA BORATORIES

:.''

......... ,

3017 N. SAN FERNANDO BLVD.


BURBANK, CALIFORNIA

91504

8188437000

8188436168

FAX

.. '

:..

,., ......

..
:;:

:-:-

:.

.,

QUALITY CONTROL PROGRAM


MP-009

Rev.a: 11/01/03
Title: Radioactive Reference Standards Solutions & Records

EBERLINE SERVICES - OAK RIDGE LABORATORY

RADIOACTIVE REFERENCE SOLUTIONS

PRIMARY DILUTION RECERTIFICATION


MP009

Half Life, Years

I: :4.4sse+osl
2

Radionuclide ::2~~' 35; '.U


Certified Activity :::a~016E+OO Ci
Certified Concentration
Ci per gram
Ampoule /Solution Gross '
Empty Ampoule 1 .
Solution Net
Total Activity In Ampoule

<

97;6400 Weight, Grams


>' 32.5020 Weight, Grams
65.1380 Weight, Grams
8.0160 Cl

Chemical Com osition of Standard Solution

Dilution Instructions:

l1M.HN93}.

Dilution Solvent Used

.....:..':<... .. :.. \ .. ;

Dilute to a volume ofl ; .1000:00 : !milliliters

Certified Total Activity ofl

. . 8;0160lCI

Which Eauals

1.780E+07ldpm at the date listed above

This activity concentration Is based on the original


And after dilution the activity of this solution is 1. 77955E+041 dpm/ml-eterence date listed above. All activities are corrected
to the date and time of analysis by the laboratory data
processing software,

Expiration Date: September 61 2013

9/26/2012 O:OO
------Date: ___,,,__/u-of-ftL__
Date:

Rev.8; 11/01/03
Title: Radioactive Reference Standards Solutions & Records

EBERLINE SERVICES - OAK RIDGE LABORATORY

RADIOACTIVE REFERENCE STANDARD SOLUTIONS

SECONDARY DILUTION RECERTIFICATION

Date
9/6/2012 0:00
Solution# . < U~a> '.
Half Life, Days
1.632E+12

MP-009
Solution Reference# IPL479-50
Princi al Radionuclide
Half Life, Years
~; 2~5.

238(J

I. 4.46aE+o9 I

Reference Date

l '

''-111i1995

o:oo I

Chemical Composition of Standard Solution

Dilution Instructions:

. I

.......
.....

Dilution Solvent Used


SECONDARY VOLUMETRIC DILUTION

Vol. Parent Solution: .:.. \;:.,_ ::::4~0000 ml


Total Activity: 7 .1182E+04 dpm
Final Volume:
. 1OOO;OO ml

Final Activity Concentration:!

7.1182E+01 ldpmlml

This activity concentration is based on the original


reference date listed above. All activities are
NOTES:
corrected to the date and time of analysis by the
..,_.,.......,-:::':'..,..,,.....,,...---------------11:1UJ.llLqtory data processing software.

Isotopic Distribution as:

U-238 Atom % 48.239 U-238 71.182 dpmiml X 0.48249 " 34.345 dpm/ml

U-235 Atom o/o = 2.25


U-235 = 71.182 dpm/ml X 0.0225 1.602 dpm/ml

U-234 Atom o/o = 49.501 U-238 =71.182 dpm/ml X 0.49501 =35.236 dpm/ml

All values +/. 3.6%

Expiration Date: September 6, 2013

Isotopic ratios from manufacturer's data sheet

Date:

9/26/2012 0:00
-------

Date: _ _
tt....{UP........,./t.....'Z-..___

RECORD COPY

Tracer Solution for Environmental Analysis & Disequilibrium Studies

Product Description & Measurement Certificate


uranium 232 (U-232)
Th-228

Product code: UDP10050


Batch Number: 911232/67

Description

Principal radionuclide:
Daughter Nuclide:

Measurement

Reference date:
Radioactive concentration U-232
which is equivalent to

01 March 2000
6.739E+03 becquerels per gram ofsolution
1.821E-01 microcuries per gram of solution

Volume of solution
Total activity ofU-232
which is equivalent to

5.035 millilitres
3.6IE+o4 becquerels
9.76E-Ol microcuries

Accuracy

Radionuc/idic
Purity

Method ofmeasurement (see reverse of this certificate)


Random uncertainty is: 0.7%
Systematic uncertainty: 0.5%
Overall uncertainty in the radioactive concentration quoted above: 1.7%
Overall uncertainty is defined on the reverse of this certificate.
Any radioactive impurities measured are listed below, expressed as percentages
of the activity ofthe principle radionuclide at the reference date.
Th-228 and daughter activity removed 2 Feb 2000
U-232 daughters activity will increase with time. By alpha 88% U-232, 12% daughters on 1/3/00

Isotopic
Purity

.....ne isotopic composition, exprP.ssed as atom per cent at the reference date .
i~ot

measured

Chemical
Composition

Calculated weight ofU-232, 4.42E-08 grams, as 2M HN03 solution in a flame sealed glass vial.
This Tracer solution has been produced 'carrier free'.

Physical
Data

Recommended halflifo of uranium 232: 6.980E+ol ye!U'S


Principle energies of alpha emissions (MeV): 5.263 31.7%, 5.320 68.00/o
Branching ratio for alpha emission: 100%
Calculated specific activity ofuranium 232: 8.167E+05 Bq per micro~ U-232.

Remarks

For safety information and notes to ensure correct usage by all persons handling this radio<!Ctive Tracer
solution please read the instructions accompanying the package.
AEA Technology operates a quality management system which has been independently audited and
approved to ISO 900 I.

Approved
Signatory

Project Ref. AE23 l S

Roger Wiltshire
Prepared and characterised in the UK, for world wide distn"bution by lsotrak, AEA Technology, QSA.

Trkcert.wps l0103/00

AEA Tecbn'llogy is the trading name ofAEA Technology pie

I
I
i

QUALITY CONTROL PROGRAM


MP-009

Rev.8; 11/01/03
Title: Radioactive Reference Standards Solutions & Records

EBERLINE SERVICES OAK RIDGE LABORATORY


RADIOACTIVE REFERENCE SOLUTIONS
PRIMARY DILUTION RECERT/FICATION
MP009

Half Life, Years

I. .

I . 1:200E:+o1I

RadionHr :'Pu < I

Reference Date!' ,

2.630E+04I
3/11200.0 O:OOl

Certified Activity < 9.760E~1 Ci


Certified Concentration . . ... ... . . . ........ Ci per gram
. . .. Weight, Grams
Ampoule /Solution Gross~...
Empty Ampoule .. ... ... Weight, Grams
Solution Net . . . Weight, Grams
Total Activity in Ampoule
0.9760 Cl

Dilution Instructions:

'.:.::.:

Diiution Solvent Used

. :.. 1

Dilute to a volume ofl 1000.00 '!milliliters

Certified Total Activity of

I .. 0.9760jCI

Which Eauals

1 . 2.1E37E+06jdpm at the date listed above


This activity concentration is based on the original

And after dilution the activity of this solution Is 12.167E+03jdpm/ml reference date listed above. All activities are corrected
to the date and time of analysis by the laboratory data
processing software.

Expiration Date:

Date:
Date:

I December 7, 2013 I

12113/2012 0:00

13fa

Rev.a: 11/01/03

Title: Radioactive Reference Standards Solutions & Records

EBERLINE SERVICES OAK RIDGE LABORATORY

RADIOACTIVE REFERENCE STANDARD SOLUTIONS

SECONDARY DILUTION RECERTIFICATION

MP009

Solution Reference # AEA/Amersham 92/232/67

Half Life, Years

j.. . 7 .200E+o1 l

Radionuclide of lnteres
Parent Solution Cone.

;:23 (J < >


2.167E+03 dpm/ml

I
Reference Datel

.
<

2.630E+04l

< 3/1 /2000 :o:ob

Chemical Composition of Standard Solution

Dilution Instructions:

Dilution Solvent Used

SECONDARY VOLUMETRIC DILUTION


Vol. Parent Solution: ' 10.0000 ml
Total Activity: . 2.1670E+04 dpm
Final Volume:. < 1000:00 ml

NOTES:

Final Activity Concentration:!

2.1670E+01 ldpm/ml

This activity concentration is based on the original


reference date listed above. All activities are
corrected to the date and time of analysis by the
laboratory data processing software.

Expiration Date:I December 7, 2013

Date:

1211312012 0:00
-------

Date: ___
1~...,._~..,.f....

+----

R11FICATE OF CALIBRATl<>til~
q\
PHA STANDARD SOLUTION'' l'lc' \~~~\\(\e
Radionuclide
Half Life:

Th-230
(7 .54

0.03) x 104 years

Catalog No.:

7230

Source No.:

388-116

Description of Solution
a. Mass of solution:
b. Chemical form:
c. Carrier content:
d. Density:

EB~ ~\~\)t \,i

Customer:

TMA

P.O.No.:

TI4944

..

\\\\l

Reference Date:
November 1 1991
Contained Radioactivity:
1.036

5.0042

12:00 PST.

"Ci.
gJ'llDIB.

Th(N03)4 in O.lN HN03


None added
1.0016

gram/ml @ 20C.

Radioimpurities

See attached technical data sheet


Radioactive Daughters

See attached technical data sheet


Radionuclide Concentration
0.207

Method of Calibration
Weighed aliquots of the solution were assayed using a liquid scintillation counter.

Uncertainty of Measurement
a. Systematic uncertainty in instrument calibration:
b. Random uncertainty in assay:
c. Random uncertainty in weighing(s):
d. Total uncertainty at the 99% confidence level:

2.0%
0.5%
0.2%
2.7%

NIST Traceability
This calibration is implicitly traceable to the National Institute of Standards and Technology.

Notes
1. Nuclear data were taken from Table of Isotopes", Seventh Edition, edited by Virginia S. Shi.dey.
2. IPL participates in an NIST measurement assurance prog11UD to establish and maintain implicit
traceability for a number of ouclides, based on the blind assay(and later NIST certification) of
Standard Reference Materials. (As in NRC Regulatory Guide 4.15)

ISOTOPE PRODUCTS LABORATORIES


1800 No. Keystone Street.,
Burbank, California 91504
818 843 7000

Rev.8; 11/01103
Trtle: Radioactive Reference Standards Solutions & Records

EBERLINE SERVICES - OAK RIDGE LABORATORY


RADIOACTIVE REFERENCE STANDARD SOLUTIONS
SECONDARY DILUTION RECERTIFICATION
MP-009
Solution Reference# IPL 3a~116 :: >
Princi al Radionuclide
Half Life, Years

Date
3/4/2013 0:00
Solution# .. ,
>Th~1b/:
. ...
Half Life, Days

I >

I:: 1.54oi=+@I

. 230tff<>

Radionuclide of lnteres ': ~ilHT:hBriJm'.J


Parent Solution Cone. > 2':30E+o3:> dpm/ml

Dilution Instructions:

Reference Date

P\

<2.754E+o1

C'11l111991'bY(lo

Dilution Solvent Used


SECONDARY VOLUMETRIC DILUTION

Vol. Parent Solution: \<:X::~:to;oooo ml


Total Activity: 2.2999E+04 dpm
Final Volume: , .. :.:taoctoo ml

Final Activity Concentration:! .

2.2999E+01 ldpm/ml

This activity concentration Is based on the orlglnal


reference date listed above. All activities are
corrected to the date and time of analysis by the
laboratory data processing software.

NOTES:

Expiration Date:

Recertified

Date:

Verified & Approved By

Date:

QC Approval

Date:

March 4, 2014

3/2112013 0:00

j~ll~

~t\("

QUALITY CONTROL PROGRAM


MP--009

Rev.8; 11/01/03
Title: Radioactive Reference Standards Solutions &Records

EBERLINE SERVICES - OAK RIDGE LABORATORY


RADIOACTIVE REFERENCE SOLUTIONS
PRIMARY DILUTION RECERTIFICATION

MP009

Principal Radionuclide

Half Life, Years

h<i;

>1;54C>e+o41

Radionuclide horiurrf
Certified Activity i 'f:1>36Ef(}O Ci
Certified Concentration
Ci per gram

Reference

Date!; '.'1111)1991'0:001

Ampoule /Solution Gross '<9;2660 Weight, Grams


Empty Ampoule - 0:4'.~2t8 Weight, Grams
Solution Net . 4~6442 Weight, Grams
Total Activity in Ampoule
1.0360 Ci
Chemical Composition of Standard Solution

Dilution Instructions:

Dilution Solvent Used

Dilute to a volume

Certified Total Activity ofl .

otl< tooo:oo> >!milliliters

l.0360lCi

Which Eauals

2:3QOE+06ldpm at the date listed above

And after dilution the activity of this solution Is I 2~300E+03ldpm/ml

This activity concentration Is based on the original


reference date listed above. All activities are corrected
to the date and time of analysis by the laboratory data
processing software.

Expiration Date:!

Date:
Date:

'March 4, 2014 .

3/21/2013 0:00

r'J.li I/, 3

14-8

CERTIFICATE OF CALIBRATION

ALPHA STANDARD SOLUTION

Radionuclide:
Th-232
Half Life: .. (l.405 0.006) x 10~ 10 years
Catalog No.:

7232

Source No.:

435-104-2

TMAEBERLINE

Customer:
P.O.No.:
Reference Date:

VH1632

November 1 1993

(fh-232) 0.0933
(Th-232)
3.45

Contained Radioactivity:
Contained Radioactivity:

Description of Solution
a. Mass of solution:

12:00 PST.

Ci.

kBq.

11.9712 g (iri: a 10 ml flame sealed ampoule)

b. Chemical form:

Th(N03)4 in water
None added
.Approx. 1.21

c. Carrier content:
d. Density:
Radioimpurities

g/ml@20~C .

None detected (other than daughters).

Radioactive Daughters
Ra-228, Ac-228. Th-228, Ra-224, Rn-220, Po-216, Pb-212, Bi-2!4,.Po-212, 11-208
Radionuclide Concentration
(Th-232) 0.00779

Ci/g.

Method of Calibration
Activity calculations are based upon known specific activity and mass.

Uncertainty of Measurement
a. Systematic uncertainty in instrument calibration:

b.. Random uncertainty in as$ay:


c. Random uncertainty in weighlng(s):.
d. Total uncertainty at the 99% confidence level:

3.0%

0.0%

2.0%
3.6%

NIST Traceability

This calibration is implicitly traceable to the National Institute of Standards and Technology.
Leak Test(s)
See reverse side for Leak Test(s) applied to this source.
Notes
..
1. Nuclear data '\Vere ~ken from "'ra~le Radioactive Isotopes", edited by Virgiitia S. Shirley, 986.
.
2. IPL particip~tes in an NIST measurement assurance program to establish and maintain implicit traceability for a number of nucli~,
balied on the blind assay (and later NIST certification) of Standard Reference Materials (As in NRC Regulatory Guide 4.15).

of

't

QUALITY CONTROL

Date Signed
ISOTOPE PRODUCTS LABORATORIES
1800 North Keystone Street
Burbank, California 91504

818 843 - 7000

~EBERLINE
I
~

QUALITY CONTROL PROGRAM


MP.009

SEAVICl!.S

R.ev.B; 1/10f03
Tdle: Radioactive Reference Standards Solutions & Records

EBERLINE SERVICES - OAK RIDGE LABORATORY

RADIOACTIVE REFERENCE SOLUTIONS


PRIMARY DILUTION RECERTIFICATION
MP009

Half Life, Years

IMt/'.jS4o5e1Jo.I

Ampoule /Solution Gross \:>:1'8.f@t5


Empty Ampoule }iy;~:e~.92$6
Solution Net 41~9119
Total Activity in Ampoule <oi0:0933

Weight, Grams
Weight, Grams
Weight, Grams

Cl

Chemical Composition of Standard Solution

Dilution Instructions:

Diiution Solvent Used

Diiute to a volume ofh\i"!lOO:O:oo::r :lmllllllters

Certified Total Activity

otl. > / 0.093.3lCi

Which Eauals

I .:.,::2.071E+o5ldpm at the date listed above

And after dilution the activity of thi!~ $olution isl 2;07-1E+:o2ldpm/ml

::r::~a:~:iU:,:e~s~~':iv':!::i~
to the date and time of analysis by the laboratory data
processing software.

Expiration Date:

Date:

I .. otooer9,201a..

10/9/2012 0:00

Rev.8; 1/10/03
TIUe: Radioactive Reference Standards Solutions & Records

EBERLINE SERVICES - OAK RIDGE LABORATORY

RADIOACTIVE REFERENCE STANDARD SOLUTIONS

SECONDARY DILUTION RECERTIFICATION


Date

MP-009

Solution Reference # IPL43s.;;104-2

11 /9/2012 0:00

Solution #

Th:,Sb .

Half Life, Days

Half Life, Years

I +.4ose;.;.1ol

Radionuclide of lnteres
Parent Solution Cone.

Reference Date I~

::228 ll 232Th '


2:07E+02

1111 /1993 Cl:OO l

dpm/ml

Chemical Composition of Standard Solution

Dilution Instructions:

Diiution Solvent Used

SECONDARY VOLUMETRIC DILUTION


Vol. Parent Solution: . '.soo;oooo. ml
Total Activity: 1.0365E.+05 dpm
Final Volume:
. 1000;00. ml

NOTES:

Final Activity Concentration:!

1.0355E+02 fdpm/ml

This activity concentration is based on the original


reference date llsted above. All activities are
corrected to the date and time of analysis by the
laboratory data processing software.

Expiration Date:f . October 9, 2013

Date:

1119/2012 0:00
--...----

Isotope Products

-U.-18

24937 Avenue Tibbitts


Valencia, California 91355

Laboratories

An Eckert & Ziegler Company

Tel 6613091010
Fax 6612578303

CERTIFICATE OF CALIBRATION

ALPHA STANDARD SOLUTION

Th-229
7340 160 years
7229
867-54

Radionuclide:
Half-life:
Catalog No.:
Source No.:

Physical
A.
B.
C.
D.

Description:
Mass of solution:
Chemical form:
Carrier content:
Density:

EBERLINE SERVICES
00009633
15-Jan-02 12:00 PST
1.013
Ci
37.48

Customer:
P.O. No.:
Reference Date:
Contained Radioactivity:
(Th-229 only)

kBq

5.0147 gin 5 ml flame-sealed ampoule


Th(N0 3) 4 in 0.1 M HN0 3
10g Th/ml
1.0016 g/mL @ 20c.

Radioimpurities:
None detected (daughters in equilibrium)

Radionuclide Concentration:

0.2020 CVg,

kBq/g

7.474

Method of Calibration:
This source was prepared from a weighed aliquot of solution whose activity in Ci/g was determined
using gamma ray spectrometry.

Peak energy used for integration:


193.5 keV
0.0441 gammas per decay
Branching ratio used:

Uncertainty of Measurement:
A. Type A (random) uncertainty:
8. Type B (systematic} uncertainty:
. C. Uncertainty in aliquot weighing:
D. Total uncertainty at the 99% confidence level:

0.7
3.0
0.0
3.1

%
%

Notes:
- See reverse side for leak test(s) performed on this source.
- IPL participates in a NIST measurement assurance program to establish and maintain implicit traceability
for a number of nuclides, based on the blind assay (and later NIST certification) of Standard Reference
Materials (As in NRC Regulatory Guide 4.15}.
- Nuclear data was taken from IAEA Technical Report Series No. 261.
- This solution has a working life of 5 years.

CJ- ftA/n-02...
Quality-Control

Date Signed

IPL Ref. No.:

867-54

- - - - - - - - - - - - - - - - - 1509001 CERTIFIED - - - - - - - - - - - - - - - -

Medical Imaging Laboratory


24937 Avenue Tibbitts

Valencia, California 91355

Industrial Gauging Laboratory

1800 North Keystone Street

Burbank, California 91504

QUALITY CONTROL PROGRAM


MP-009
Rev.8; 1/10/03
Title: Radioactive Reference Standards Solutions &Records

EBERLINE SERVICES - OAK RIDGE LABORATORY

RADIOACTIVE REFERENCE SOLUTIONS

PRIMARY DILUTION RECERTIFICATION


MP009

Half Lii.e, Days

Half Life, Years

r..

I> 7.34oe+osl

I 2.e~1 E+oel
Reference Date I < . 1h5/20oio:ool

Radionuclide
!l!9i'11; .
Certified Activity J.013E+o0 Ci
Certified Concentration > > ' ' Ci per gram
Ampoule /Solution Gross
Empty Ampoule
Solution Net
Total Activity in Ampoule

.. ,

a.ns2 Weight, Grams


3.7591 Weight, Grams
5.0161 Weight, Grams
1.0130 Ci

Chemical Composition of Standard Solution

Dilution Instructions:

lo;1iM HNQ3..

Dilution Solvent Used

:... :: ..': ..

".

Dilute to a volume ofl . 1000.00 < milliliters

Certified Total Activity of

I 1.0130jCi

Which Eauals 1

2.249E+06jdpm at the date listed above

And after dilution the activity of this solution Is 12.249E+03jdpm/ml

This activity concentration Is based on the original


reference date listed above. All activities are corrected
to the date and time of analysis by the laboratory data
processing software.

Expiration Date:

Date:
Date:

October 9, 2013 ]

11/9/2012 0:00
-------

____

ri/rz/,~

-~,.........,,,_

flti37 :

~E"'E"'h~1.t:!o!'i I QUALITY c:;i.~ROL PROGRAM


Rev.7; 0129/99

Tiiie: Radioactive Reference Stan<lards SOluUons & RecordS

EBERLINE SERVICES OAK RIDGE LABORATORY


RADIOACTIVE REFERENCE STANDARD SOLUTIONS
SECONDARY DILUTION RECERTIFICATION

Date
Solution'# >

MP-009

Solution Reference # IPL 867~54


Princi al Radionuclide
Half Life, Years

Half Life, Days

I . 1;34oE+o3 I

.\ 229Th .

1119/2012 0:00
... Th~18a\

Radionuclide of lnteresd . 2~ .. .,
Parent Solution Cone. 2,25E+03 .. dpm/ml

Reference Date

2~681E+06I

< 1lf5/20020:obl

Chemical Composition of Standard Solution


'.
> .. ...... .... . .I

jTH{N0s)41ri0.1MHNO:f

Dilution Instructions:

j0.1M HN03

Dilution Solvent Used

.. ... ............. .. 1

SECONDARY VOLUMETRIC DILUTION

Vol. Parent Solution:


Total ActlVlty.'
Final Volume :

NOTES:

. 10.0000 ml
2.2490E+04
dpm
..
1000.00 ml

Final Activity Concentration:!

2.2490E+01 ldpm/ml

This activity concentration Is based on the original


reference date listed above. All activities are
corrected to the date and time of analysis by the
laboratory data processing software.

Expiration

Date:I October 9, 2013

Date:

------
11/9/2012 0:00

Date: _ __.1.l.f1/JJ1zie.oj/'"'"1...,'Z--=-

J!attonal 3fn~tttute of

0/(/~.,'

i>tanbatb~

& ~ttbnologp

ctertificate'''
.

'i>

;./

..

..

.:

....

'

i 1;_;

'

Standard Reference Material 4251C


l3arium-133 Radioactivity<Standard

This Standard Reference Material (SRM) copsists o~ radioactive barium-133 cJ;tloride,_ non-radioactive barium

chloride, and hydrochloric acid diSsolved in 5 mL of distilled water. The solution is contain~d in a flame

sealed NIST borosilicate-glass ampoule. The SRM is intended for the calibration of ionization' chambers and

solid-state gamma-ray, spectrometry .sy~tems.


Radiological Hazard

'a

The SRM ampoule contains barium-133 with total activity of approximately 2.5 MBq. Barium-133 decays

by electron capture and during the decay process X-rays, and gam,ma,rays with energies from 4 to 400 keV are
emitted. Most of these photons escape from the SRM ampo~l~ and can represent a radlati()n hazard.

Approximate unshielded dose rates at several distances (as of the reference time) are given in note [a]*.
Appropriate shielding and/or distance should be used to minimize, personnel exposure~ .-.The ,SRM ~hould be
:used only by persons qualified to han?Je radioactiv~ material. '
, ,
,
Chemical

I
I

I
I

I
!

~rd

The SRM ampoule ~nta~ hydr~ch!.oric acid (HCl) with ~ concentration pf l mole per liter ,of.water. The

solution is corrosive and represents a health hazard if it comes in contact with.eyes or skin~. lf the ampoule

is to be opened to transfer the solution, the recommended procedure 'is given on page 2. The ampoule should

be opened only by perso~ qualified to handle both radioactive material and strong acid solution.

Storage and Handling


The SRM should be stored and used at a temperature between 5 and 65 C. The solution in an ~nopened

ampoule should remain stable and homogeneous until at least June 2004.

The ampoule (or any subsequent container) should always be clearly marked as containing radioactive
material. If the ampoule is transported it should be packed, marked, labeled, and shipped in accordance with
the applicable national, international, and carrier regulations. The solution in the ampoule is a dangerous
good (hazardous material) both because of the radioactivity and because of the strong acid.

Preparation

Ii

This Standard Reference Material was prepared in the Physics Laboratory, Ionizing Radiation Division,

Radioactivity Group, J.M.R. Hutchinson, Group Leader. The overall technical direction and physical

measurements leading to certification were provided by L.L. Lucas of the Radioactivity Group and D.B. Golas,
Nuclear Energy Institute Research Associate.

1>
i .,

j.
1

The support aspects involved in the preparation, certification, and issuance of this SRM were coordinated
through the Standar~ Reference Materials Program by N.M. Trahey.
Gaithersburg, Maryland 20899
October 1994

Thomas E. Gills, Chief


Standard Reference Materials Program

I'

I
I
1

SRf-14251C, p~ge.l of 6

*Notes and references. are. pn pages ~ and 6.

t
I

QUALITY CONTROL PROGRAM


QCP-009

Rev.a; 11110/03
Title: Radioactive Reference Standards Solulions & Records

EBERLINE SERVICES - OAK RIDGE LABORATORY


RADIOACTIVE REFERENCE SOLUTIONS
PRIMARY DILUTION RECERTIFICATION
QCP 009-1
CURRENT DATE
SOLUTION REFERENCE #rrN;;;IS~T~;S-.=R~Mi742Aj5:";.1:;;'C~:.~~~
SOLUTION # \'.
Princi al Radionuclide
,.i.~eaf:iurn\;

'6/16/20130:00
;\<';'~Ba$i'/:''\>'>)

Half Life, Days

Half Life, Years

I . . .

1~J:1:.048E:fb11

.H

:3.82SE:i-031

Reference DatePi'.;::<';/-9111d$$:3'(Qidd]

Radionuclide
Certified Activityt7'7~~ttrlCi
Certified Concentration }j)$t6E'tot Ci per gram

Ampoule /Solution Gross \\:.):;$;3P$1 Weight, Grams


Empty Ampoule :;}';\\'4}2~ Weight, Grams
Solution Net <5:04Q9 Weight, Grams
Total Activity in Ampoule > 66:5577 Ci
Chemical Composition of Standard Solution

Dilution Instructions:

Dilution Solvent Used


i
1

Dilute to a volume ofb;:.;'.:;tQOO;QO\;;;;:lmilliliters

I
Certified Total Activity ofl ;> 66:5577lCi

Which Eauals

k->

<'i1A78E+08ldpm at the date listed above

I
!

! -.

And after dilution the activity of this solution is I.1 ~4.78.E+.05 Idpm/ml This activity concentration is based on the original
.

reference date listed above. All activities are corrected


date and time of analysis by the laboratory data
to

the

processing software.

Expiration Date:!

June16;2014 --I

II:::

I .

Date:

__

711113

_..;..;~..;;....

__

Oata: _ _1..1.j/~~+:.r...::::d~-

I.

I'
l

!.
ii

Rev.8; 11/10/03
Tiiie: Radioactive Reference Standards Solutions & Records

EBERLINE SERVICES - OAK RIDGE LABORATORY


RADIOACTIVE REFERENCE STANDARD SOLUTIONS
SECONDARY DILUTION RECERTIFICATION
QCP-009-1~A

Princi

Solution Reference # NIS'E'$RM4251C'!c '/'


I Radionuclide
Half Life, Years

:;1f1sa;r:

Half Life, Days

l'hi1:04'8Ei-0'1'l

Radionuclide of Interest '\\(;Q~~Ji:!i;'fi


Parent Solution Cone. (:)1:"4ae+..o5!/!I, dpm/ml

Chemical Composition of Standard Solution

Dilution Instructions:

Dilution Solvent Used

SECONDARY VOLUMETRIC DILUTION


;;~:\{~~\:iZ5}000P ml
Total Activity: '3;695QE+Q6 dpm
Final Volume: /;.;:'.\\':4000iOO ml

Vol. Parent Solution:

NOTES:

Final Activity Concentration: I. ''\'3J3950E+03ldpm/ml

This activity concentration is based on the original


reference date listed above. All activities are
corrected to the date and time of analysis by the
laboratory data processing software.

Expiration Date:I

June 16, 2014

Date:

7/1/13

Date: _ _
'7,,_/:z--..i/._1:;.j_ _

CERTIFICATE OF CALIBRATI rsAtOC REVIEWED

ALPHA STANDARD SOLUTIO ote ef- g Initials_

Radionuclide:
Half Life:
Catalog No.:

1600

Source No.:

7 years

P~O.No.:

Reference Date:.
February 11994
12:00 PST.
Contained Radioactivity: (Ra-226) 1.001 14Ci.
Contained Radioactivity: (Ra-226)
37.0 kBq.

1m
453-26

Description of Solution
a. Mass of solution:

TMA EBERLINE
VH1888

Customer:

Ra-226

5.1864 g (in a 5 ml Flame Sealed Ampoule).

b. Chemical form:

Ra(N03)2 in 1 N HN03

c. Carrier content:

None added

d. Density:

l..0318

g/ml@20C.

None detected(other thai:l daughters)

Radioimpurities

Radioactive Daughters
Rn-222, Po-218, At-218, Pb-214, Bi-214, Po-214, Tl-210, Pb-210, Bi-210, Po-210 and Tl-206.
Radionuclide Concentration
(Ra-226)

0.1929

. ::.. Ci/g.

Method of Calibration
Weighed aljquots of the solution were assayed using gamma spectrometry:

Energy peak(s) integrated under: 186 keV.

Brancbillg ratio(s) used:


0.0351
gamma rays per decay.

Uncertainty of Measurement
a. Systematic uncertainty in instrument calibration:
b. Random uncertainty in assay:
c. Random uncertainty in weighing(s):

3.4%
3.1%
0.2%

d. Total uncertainty at the 99 % confidence level:

.4.6%

NIST Traceability
This calibration is implicitly traceable to the National Institute of Standards and Technology.
Leak Test(s)
See reverse side for Leak Test(s) applied to this source.
Notes

1. Nuclear data were taken from "Table ofRadioact~e Isotopes", edited by Virginia S. Shirley, 1986.
2. IPL participates in an NIST measurement assurance program to establish and maintain implicit traceability for a num~r of auclides,
----based oinhetiliiiii--ass:ay{rin<!-iater NIS'NerlifiCationrorsiiiildiiro RcferenceMateriillS\Aii"iii NRC~egu1at0rrGuidif4; rs): --

QUALITY CONTROL

/iA,. ; , 199/f
Date Signed
ISOTOPE PRODUCTS LABORATORIES
1800 North Keystone Street
Burbank, California 91504
818 843 - 7000

QUALITY CONTROL PROGRAM


MP009

Rev.8; 11/01/03
Title: Radioactive Reference Standards Solutions & Records

EBERLINE SERVICES - OAK RIDGE LABORATORY


RADIOACTIVE REFERENCE SOLUTIONS
PRIMARY DILUTION RECERTIFICATION
MP009
CURRENT DATE!
11/9/2012 0:001
SOLUTION REFERENCE #l"!'=IP~L-4"""5"""3-=2~6-.~---,.,..-..,,,
SOLUTION #i-l-...-.-R-a:--5... ---.-t.I
Princioal Radionuclide
~26 Radium I

Half Life, Days

Half Life, Years

1
. 22ti,. . .

(60()E+o31

. ..

Radionuclide .... Radium


Certified Activity t.00.1 E-tOO Ci
Certified Concentration . .
.. Ci per gram

Reference Date

5.844E+osl

I.

2/1]1994 O:ool

: ........ We~ght, Grams


Ampoule /Solution Gross~
Empty Ampoule . . : . Weight, Grams
Weight, Grams
Solution Net . .
Total Activity in Ampoule
1.0010 Cl
Chemical Composition of Standard Solution

2.26Ra(No).n .1M. H..No . '.'. ......... : ,': . :: '>.:::'." .. :.. '..:... ,

1. .

' . 3 2 . ..

: . .

. .

Dilution Instructions:

11MHN03< ..

Dilution Solvent Used

Dilute to a volume ofl . 1000~00

Certified Total Activity ofl ..... 1;0010htCi

jmflliliters

Which Eauals

. 2.222E+06ldpm at the date listed above


This activity concentration is based on the original

And after dilution the activity of this solution isl 2.222E+03jdprn/ml reference date listed above. All activities are corrected
to the date and time of analysis by the laboratory data
processing software.

Expiration Date:

Verified &Approved

By_~--~----+-~......,....-~_,,~-L~

QC Approval -~.,,..o........,.._..'-\\~~~~~---

Date:
Date:

November 9, 2013

11/912012
-------

11/1i/r1
/

---~----(

Rev.6; 11/01/03
Trtle: Radioactive Reference Standards Solutions & Records

EBERLINE SERVICES - OAK RIDGE LABORATORY


RADIOACTIVE REFERENCE STANDARD SOLUTIONS
SECONDARY DILUTION RECERTIFICATION
Date
11/9/2012 0:00
Solution # \/{>:~'R.a~5b):~: ;>l>:
Half Life, Days

MP009
Solution Reference# IPL-453"26/ .>\;/>
Princl al Radionuclide
Half Life, Years
<~~Raalumf
l.\.';,-.;:1'26ob6to31

I<' : 5:a44E+osl

Radionuclide of Interest S.~Radium:>;


Parent Solution Cone. ~Y2(22Et03fD dpm/ml

Chemical Com osition of Standard Solution

Dilution Instructions:

Dilution Solve!rt Used

SECONDARY VOLUMETRIC DILUTION


Vol. Parent Solution: ;7;'}i;:,u;:20:0000 ml
Total Activity: ;._4A440E+.04 dpm
Final Volume: ..: -.~ .}~OO(tOO ml

NOTES:

Final Activity Concentration: I''.: ' 4A440E+o1 jdpm/ml


This activity concentration Is based on the original
reference date listed above. All activities are
corrected to the date and time of analysis by the
laboratory data processing software.

Expiration Date: November 9, 2013

Date:

1119/2012 0:00

Date:

'' / rz. 1z...


I I

RA-\\
1380 Seaboard Industrial Blvd.
Atlanta, Georgia 30318 U.S.A.

ANALYTICS

Phone (404) 352-8677


Fax (404) 352-2837

CERTIFICATE OF CALIBRATION
Standard Radionuclide Source
62680-416

Ra-228 5 mL Liquid in Flame Sealed Vial

was
prepared
This
standard
radionuclide
source
The
gravimetrically from a calibrated master solution.
germanium
gamma
master solution was calibrated using a
spectrometer system.
Radionuclide purity and calibration were checked using a
germanium gamma spectrometer system. The nuclear decay rate
and assay date for this source are given below.
ANALYTICS maintains traceability to the National Institute
of Standards and Technology through Measurements Assurance
Programs as described in USNRC Reg. Guide 4.15, Revision 1.
ISOTOPE:

Ra-228

ACTIVITY (dps) :

2.585 E3

HALF-LIFE:

5.75 years

CALIBRATION DATE:

November 7, 2001 12:00 EST

TOTAL UNCERTAINTY*:

4.0%

SYSTEMATIC:

3.0%

RANDOM:

1. 0%

*99% Confidence Level

Impurities: y-impurities (other than decay products) <0.1%

5.07198 grams O.lM HCl solution with 50 g/g Ba carrier.

P 0 NUMBER

9508, Item 1 (Part #4339A)

SOURCE PREPARED BY:

Q A APPROVED:

M:di~mist
I

/ c tl{ u./

11

I )fr!

2J
EBERLl~_I;; l
~

QUALITY CONTROL PROGRAM


MP-009

SERVICl<I>

Rev.8; 1110/03
TlUe: Radioactive Reference Standards Solutions & Records

EBERLINE SERVICES - OAK RIDGE LABORATORY


RADIOACTIVE REFERENCE SOLUTIONS
RECERTIFICATION
MP009

.......---.CURRENT DATE ..

,,.............,.._,...,......,..~~,.......,

SOLUTION REFERENCE# Ai::\alytiSS2.saob1Je:\\? /),


Princi al Radionuclide
Half Life, Years

SOLUTION #

li:::'.U~'.s17soe:+oaI

Radionuclide l?)?;.~~8itt~'I;f!
Certified Activity ';'i},}~t9.8$E;o2: Ci
Certified Concentration
Ci per gram
Ampoule /Solution Gross H:\<>''9}49~2 Weight, Grams
Empty Ampoule ;f.~>#!4~~9$. Weight, Grams
Solution Net.~ >5~0087 Welght1 Grams
Total Activity in Ampoule > /o:os99 Ci
Chemical Com osition of Standard Solution

Dilution Instructions:

Dilution Solvent Used

Dilute to a volume ofj//J,.1:otJo:oo::;v;[(.jmmmters

Certified Total Activity offi :.:0:00.99jCi

Which Equals

.. ;:.:t~55fEt05ldpm at the date listed above

And after dilution the activity of this solution islMi51E+02ldpm/ml

::r:.iC:,,a:'~:::':::e~s~~~:i~~!::!ctoo
to the date and time of analysis by the laboratory data
processing software.

Expiration Date: <: March 26; 2014

Date:

5130/13

SECTION VI

QUALITY CONTROL SAMPLE RESULTS SUMMARY

Eberline Services
Analysis Control Chart

Printed: 811412013 2:45 PM

Page 1of2

WO

Analysis

13-07154

UUISO

Activity Units

Aliquot Units

pCi

Client Name

Engineering Management Support, Inc.

Laboratory Control Sample


Analyte

U-234

Normalized
Difference

LCS
Measured

CSU
Measured

LCS
Expected

Uncert.
Expected

Known

Known
Error

Result

CSU

Standard
ID

o.34

97.39%

15.38%

100.00%

3.60%

8.17E+OO

2.94E-01

7.96E+OO

1.22E+OO

U-8a

112.17%

15.14%

100.00%

,_....

'"....

1.35

u-

~;~-

U-238
,___ _ _ _ _

--------~---

J~:oo-

,_.,.-01

Standard
ACT(dpm)

Standard
Error

3.52E+01

, ......
1

Standard
Added (g)

3.60E+OO

5.15E-01

,.......

..,.E-01

Matrix Spike
Analyte

Nonnalized
Difference

MS Actual
%Rec

Expected
MS Result

Expected
MS Uncert

Actual
MS Result

Actual
MS CSU

Sample
Result

Sample
CSU

Replicate Sample
Analyte

Nonnalizec/
Difference

Sample
Aliquot

Standard
ID

Standard
ACT(dpm)

Standard
EtTOr %

Standard
Added(g)

RepRPD

Rep ND

OK

OK

OK

OK

NA

OK

QC Summary

RPO

Original
Result

Original
CSU

Replicate
Result

Replicate
CSU

LCS Relative
Bias

LCS%R

LCSND

MS%R

MSND

I
U-234

1.27

22.92

1.65E+OO

3.77E-01

1.31E+OO

3.63E-01

0.97

OK

OK

U-238

0.09

1.67

1.42E+OO

3.40E-01

1.44E+OO

3.85E-01

1.12

OK

OK

U-235

0.74

35.00

1.80E-01

1.19E-01

2.56E-01

1.62E-01

i;l~I

~~
Jf;n.,

OJI

Version

OK

i'

t-----t
i

~-----t

Printed: 8/14/2013 2:45 PM

Page 2 of 2

Eberline Services
Analysis Control Chart
_ _ _ _A_n<1!s~------

WO

Run

Activity Units

pCi

UUISO

13-07154

__(_

Aliquot Units

Client Name - - - - - - - - - - - - -

Engineering Management Support, Inc.

Replicate Sample RPO

LCS % Recovery
130.00

40.00
120.00

35.00
110.00

30.00
100 00

25.00
20.00

90.00

-------------i
I

15.00
80.00
10.00

10.oa

L--------~~--------,--------,;:;:'8-------1
U-234
U-238

78.40
116.37

%R
97.39
80
:::._ --=.L_LCgLL___--J-1------11100

93.43
130.91
112.17
80

Lower Error I
Uooer Error I

- Mean

""

-----+--- -----160

5.00

U-234
25.79
20.05
22.92
--------

120

-UCL

U-238
1.88
1.45
1.67
35

Normalized Difference
No Matrix Spike

3.50
3.00
2.50
2.00
1.50
1.00
0.50
0.00
-U-2341
=u-23a
UCL

ti!~

ta
,~,

..

(.i!:li

Version

LCS ND

REP ND

0.34
1.39
000
3

1.27
0.09

MSND
0.00

0.00:::__ _ _ _ _t

0.00

0.00
3

U-235
46.31
23.69
35.00
35

Eberline Services
Analysis Control Chart

Printed: S/14/2013 4:27 PM

Page 1of2

WO

Analysis

Run

Activity Units

13-07154

Th ISO

pCi

Aliquot_U~n~i~ts~---+-------

Client Name

Engineering Management Support, Inc.

Laboratory Control Sample


Analyte

II

Nonnalized
Difference

---~

TH-22S
-------

TH-230
TH-232

2.32

LCS
Measured

CSU
Measured

95.S9%

I ~~~~~% I

100.~0~-

7S.91%

I 22.47%

100.00%

93.30%

0.6S

20.47%

r
I

LCS
Expected

Uncert.
Expected

Known

Known
Error

3.60%

4.96E+OO

1.79E-01

4.75E+OO I 9.S3E-01

2.70%

5.51E+OO

1.49E-01

4.35E+OO

Result

9.77E-01

, -- -- -
100.00%

3.60%

4.96E+OO

1.79E-01

Standard

CSU

Standard
ACT(dpm)

ID

Standard
Error

Standard
Added (g)

I 1.04E+02

i Th-;~ --r

3.60E+OO

1.06E-01

2.35E.01

2.70E+OO

5.20E-01

Th-Sb

1.04E+02

3.60E+OO

1.06E-01

Th-Sb

4.63E+OO I 9.47E-01

t
I

Matrix Spike
Analyte

MS Actual
%Rec

Normalized
Difference

Expected
MS Result

Expected
MS Uncert

Actual
MS Result

Actual
MS CSU

Normalized
Difference

RPD

TH-22S

1.05

26.21

1.13E+OO

TH-230

1.02

23.21

I 1.66E+OO

TH-232

0.31

Original

Result

Sample
CSU

Replicate Sample
Analyte

Sample
Result

Original
CSU

Replicate
Result

Replicate
CSU

Sample
Aliquot

Standard
ID

Standard
ACT(dpm)

Standard
Error%

Standard
Added(g)

RepRPD

Rep ND

QC Summary

LCS Relative
Bias

LCS%R

LCSND

0.96

OK

OK

NA

OK

4.94E-01 t,.32E+OO , 4.41E-:~ 0.79

OK

OK

NA

OK

OK

OK

NA

OK

I 3.25E-01

MS%R

MSND

'

(il~

it:it~

l.11
t:lrlli

Version

----~.;-t~3SE+OO

3.64E-01 I 8.67E-01

4.11E-01

1.2SE+OO I 4.1SE-01

0.93

Eberline Services
Analysis Control Chart

Printed: 8/14/2013 4:27 PM

Page 2 of 2

Analysis

Run

Acti_vit}'~nits

ThISO

pCi

__ Aliquot Units

Client Name
-----------------
--------

Engineering Management Support, Inc.

Replicate Sample RPO

LCS % Recovery
130.00

40.00

---------------~

- - - - - - - - - - - - - - -

I
~------~

TH-228
71.62
120.15
95.89
80
100
120

Lower Error
Uooer Error

%R
-LCL

---Mean
-

-UCL

------

TH-230
53.74
104.08
78.91
80
100
120

----

LCL

TH-232
69.23
117.37
93.30
80
100
120

-~

----~--

Lower Error
Uooer Error

~- RPD

-CL

TH-228
30.74
21.69
26.21
35

TH-230
26.86
19.57

-23:21
35

Normalized Difference
No Matrix Spike

3.50,------
3_00 1-----~~2.50

+--

------

2_00
1.50

-j------_j

1_00 +-----__J
0_50 - ; - - - - - _ _ j
0_00

TH-228
=TH-230
UCL

~~
110."!(l1

U'll
i-'""

Version

LCS ND

040
2.32

-----r--

--3---

REP ND

1__05
1.02
3

MS ND

0 00
000

TH-232
7.95
5.81
6.88
35

Printed: 8/9/2013 1:20 PM

Page 1of2

Eberline Services
Analysis Control Chart
WO

________ Anal}'s~i;

Ra226

13-07154

Run

Activity Units

pCi

Client Name

------~lig_ll<:>t!Jriits _ _ _- + - - - -

Engineering Management Support, Inc.

Laboratory Control Sample


Analyte

RA-226

Normalized
Difference

LCS
Measured

CSU
Measured

LCS
Expected

Uncert.
Expected

0.03

100.32%

23.94%

100.00%

4.60%

Known

Known
Error

Result

1.04E+01

4.76E-01

1.04E+01

CSU

Standard
ID

2.49E+OO

Ra-Sb

Standard
Error

Standard
ACT(dpm)

4.41E+01

Standard
Added (g)

4.60E+OO

5.22E-01

Standard
Error%

Standard
Added(g)

RepRPD

Rep ND

OK

OK

--+-

-----+-----~-~-------- _.j_____ _ __ _ ,_ _ _ _ _

~--------------------

-+-------+

-----------------+------!-

l------

---

Matrix Spike
Analyte

Normalized

MS Actual

Expected

Difference

% Rec

MS Result

_____

Actual
MS Result

~--

Expected
MS Uncert

--.

Actual
MS CSU

Sample
Result

Sample
CSU

Sample
Aliquot

~-------+--

-+----------+-

'

QC Summary

Replicate Sample

RA-226

Gi'~
(~~

U1
r~,~

Version

Standard
ACT(dpm)

-1

Analyte

Standard
ID

Normalized
Difference

RPD

Original
Result

1.12

23.12

6.39E+OO

Replicate
Result

Original
CSU

1.82E+OO

5.07E+OO

Replicate
CSU

LCS Relative
Bias

LCS%R

1.42E+OO

1.00

OK

LCSND

OK

MS%R

MSND

Printed: 8/9/2013 1 :20 PM

Page 2 of 2

Eberline Services
Analysis Control Chart
Analysi~

__B_u_n_ _,

Ra226

__ Activity_'=!__~+

pCi

Client Name

Aliguot Units

Engineering Management Support, Inc.

Replicate Sample RPO

LCS % Recovery
130.00
"4U.UU

120.00

35.00
110.00

30.00

100.00

25.00
20.00

90.00

15.00
80.00
10.00

70.00

+-------------------------------------~

5.00

RA-226
1---

Lower Error I

71. 78

128.87

Upper Error
~

100~

r:::'--~

80
100
120

--Mean
-

---

0.00

-UCL

Lower Error
Unner Error

RPO

-CL

----~---

-------

RA-226
26.39
19.85
23.12
35

Normalized Difference
3.50,---
3.00

~-----

----

- - - -

2.50 + - - - - - - - - - - - - - - - -
2.00 1 - - - - - - - - -
1.50 + - - - - - - - - - - - - - - - - -
1.00+
0.50

--

+-----------

0.001---:-::::-:-::~--~---

-RA-226
UCL

11:.!l:ii
W~'ll

t..rn

(,,JI

Version

LCS ND

REP ND

0.03

1.12

MSND
0.00

No Matrix Spike

Eberline Services
Analysis Control Chart

Printed: 8/15/2013 10:33 AM

Page 1of2

. _. !--'1':'i)i~is

WO

Ra228

13-07154

Run

Activity Units

pCi

--+----'-'Aliquot Un~----+------------ _C~ent Name_ _ _ _ _ _ _---------


i
!

Engineering Management Support, Inc.

Laboratory Control Sample


Analyte

Normalized
Difference

LCS
Measured

+.. ,.

RA-228

, , _ , .

--[

CSU
Measured

LCS
Expected

Uncert.
Expected

Known

30.91%

100.00%

5.10%

8.80E+OO

Known
Error

4.49E-01

Result

8.26E+OO

CSU

2.55E+OO I

Standard
ID

Ra-11

Standard
ACT(dpm)

I 3.76E+01

Standard
Error

Standard
Added (g)

I 5.10E+OO I 5.19E-01

'

Matrix Spike
Analyte

Normalized
Difference

MS Actual
%Rec

Expected
MS Result

Expected
MS Uncert

Actual
MS Result

Actual
MS CSU

Sample
Result

Sample
CSU

RA-228

~ll11i

t:t'll
U"ll
.i:.~..

Version

Normalized
Difference

RPD

0.65

17.54

Original
Result

Standard
ID

Standard
ACT(dpm)

Standard
Error%

Standard
Added(g)

RepRPD

Rep ND

NA

OK

QC Summary

Replicate Sample
Analyte

Sample
Aliquot

Original
CSU

3.03E+OO I 1.08E+OO

Replicate
Result

2.54E+OO

Replicate
CSU

I 9=~E-01

LCS Relative
Bias

0.94

LCS%R

LCSND

OK

OK

MS%R

MSND

Printed: 8/15/2013 10:33 AM

Page 2 of 2

Eberline Services
Analysis Control Chart
WO

Analysis

13-07154

Ra228

Run
------!-----------

Activity Units

pCi

Aliquot Units

Client Name _ _ _ ____.


- -----

Engineering Management Support, Inc.

Replicate Sample RPO

LCS % Recovery
130.00

.
IU.UU

RA-228
57.85
129.87
93.86
80
100
120

Lower E~or I
--~~Upper Error - - - - -

%R

~--

-LCL

- - Me~..!!___._ __
-UCL

--

---

-------~---

Normalized Difference
No Matrix Spike

3.50
3.00
2.50
2.00
1.50
1.00
0.50
0.00
-RA-2281
UCL

il:i!'i~

G'll
U1I

Version

LCS NO

REP NO

0.41
3

0.65
3

MSNO

0.00

SECTION VII

LABO RA TORY TECHNICIAN'S NOTES

ISOUNOTES

Printed: 8/8/2013 7:51 AM

)!> E:: B
~

Page 1of1

Oak Ridge Laboratory

I;; R .I,,,,. I ........ I;;


SERVICES

Work Order Analysis Notes

Date

Dept

08/08/13 07:51

PREP

User
JWOLFE

601 Scarboro Rd.


Oak Ridge, TN 37830
Voice: 865.481.0683
www.eberlineservices.com

Internal Work Order

Analysis Code
Run Number

13-07154
UUISO
1

Notes
ALIQUOTED AND ADDED SPIKES AND TRACERS- PRESERVED FRACTIONS 4-6, 8 AND 9, 12 AND 13
WITH HN03- DRIED SAMPLES DOWN

Printed: 8/13/2013 3:46 PM

Page 1of1

~
E.e E R.~1 N
~

Oak Ridge Laboratory


I;::

SERVICES

Work Order Analysis Notes

Date

08/08/13 07:51

08/13/13 15:45

Dept

User

601 Scarboro Rd.


Oak Ridge, TN 37830
Voice: 865.481.0683
www.eberlineservices.com

Internal Wor1< Order

Analysis Code
Run Number

13-07154
UUISO
1

Notes

PREP

JWOLFE

ALIQUOTED AND ADDED SPIKES AND TRACERS- PRESERVED FRACTIONS 4-6, 8 AND 9, 12 AND 13
WITH HN03- DRIED SAMPLES DOWN

CHEM

JDEMELAS

Added concentrated HCI to sample beakers and heated to dryness; Added 20 ml 8N HCL to samples and
transferred to new, labeled C-Tubes, rinsing with 8N HCI to bring volume to -35 ml; Preconditioned resin
columns with 35 ml 8N HCI; Centrifuged samples and loaded onto columns; Rinsed C-Tubes with 20 ml 8N
HCI, centrifuged as needed and loaded onto columns; Rinsed columns with 35 ml 8N HCI 0.1 N NH41, 35 ml
of 6.5N HCI- 0.04N HF, and 10 ml of 6.5N HCI; Eluted Uranium with 50 ml of 0.5N HCI into clean, labeled 100
ml beakers; Dried-down samples on hotplate; Dissolved samples in -1 Oml of concentrated HCI; Transferred to
new, labeled C-Tubes with DI H20. Set samples aside for later precipitation and filtering.

-e-

-i659

Printed: S/14/2013 5:55 AM

<(

B i;;:;

Page 1 of 1

R~~~c!"i

Work Order Analysis Notes

Oak Ridge Laboratory

601 Scarboro Rd.


Oak Ridge, TN 37830
Voice: 865.481.0683
www.eberlineservices.com

Internal Work Order

Analysis Code
I

o-1un

l~umber

13-07154
UUISO
1

Notes
ALIQUOTED AND ADDED SPIKES AND TRACERS- PRESERVED FRACTIONS 4-6, 8 AND 9, 12 AND 13
WITH HN03- DRIED SAMPLES DOWN

Added concentrated HCI to sample beakers and heated to dryness; Added 20 ml BN HCC-tO..S8rTI'Pi9"i~"anc:r_,~,.,.,.....
transferred to new, labeled C-Tubes, rinsing with SN HCI to bring volume to -35 ml; Preconditioned resin
columns with 35 ml SN HCI; Centrifuged samples and loaded onto columns; Rinsed C-Tubes with 20 ml SN
HCI, centrifuged as needed and loaded onto columns; Rinsed columns with 35 ml SN HCI - 0.1 N NH41, 35 ml
of 6.5N HCI - 0.04N HF, and 10 ml of 6.5N HCI; Eluted Uranium with 50 ml of 0.5N HCI into clean, labeled 100
ml beakers; Dried-down samples on hotplate; Dissolved samples in -1 Oml of concentrated HCI; Transferred to
new, labeled C-Tubes with DI H20. Set samples aside for later precipitation and filtering.
3

08/14/13 05:55

CHEM

RMARTZ~~

ADDED 0.1 ML NEODYMIUM CARRIER, 0.3 ML TITANOUS CHLORIDE, & 1 ML HF TO C-TUBES; LET SET
SIT IN ICE BATH FOR ONE HOUR. SET UP FILTERS BY ADDING ALCOHOL & CARBON SUBSTRATE
THEN ADDED SAMPLES; WHEN SAMPLES WERE THROUGH FILTERS, ADDED 10 ML DI H20 RINSES
FROM C-TUBES, REMOVED FILTERS, LET DRY IN DESSICATOR, THEN SENT SET TO COUNT ROOM.

Eberline Analytical
Oak Ridge Laboratory

Printed: 8/14/2013 5:58 AM

Page 1 of 1

Internal Work Order

13-07154
Analysis Code

UUISO

Reagents Used in an Analysis


Reagent
ID

Reagent
Name

014109P

Run

Reagent
Concentration

Nitric Acid

1
Date
Recorded

Analyst
ID

Reagent Grade

S/S/2013

,,,,,,,,,,,,,,,+,,,,,,,,,,,,,,.,,,,,

014164P

Reagent Grade

S/13/2013

0142305

HCI - HF

014143001

Hydrochloric Acid

JDEMELAS

S/13/2013

Hydrochloric Acid

JDEMELAS

S/13/2013

S/13/2013

-----~-,--,,,~,--,

0140425
,,,,_.,_,,,,,,

013221P

""~'

Hydrochloric Acid

Reagent Grade

JDEMELAS

S/13/2013

HCI - NH41

SN - O.lM

JDEMELAS

S/13/2013

Hydrochloric Acid

SN

JDEMELAS

S/13/2013

Carbon substrate

Solution

RMARTZ

S/14/2013

Reagent Grade

RMARTZ

S/14/2013

RMARTZ

S/14/2013

,,,,_M~wwwww

Hydrofluoric Acid
.,,,.~,,,,,,,,,,,,,,,,,,,,,,,,,,,.

0131915
013574P

Neodymium Carrier

,,,_,,~,,.,_,,,,,,,,_,,,,,,,~,~.,,,+,,,

1 mg/ml

Reagent Alcohol

Reagent Grade

Titanous Chloride

Reagent Grade

" ' ' ' " ' ,,,,,,,b,,_,,,,

,,,,,<w_~,~-www,,wwww'---''I"'
,.,.~_,,,,,,'t _

--~

RMARTZ

I
,,,iI S/14/2013
,,,

RMARTZ

I S/14/2013 I

_ _ _ _,,_ _

NN;;ONNN~'""~~~-'"'""'"""''"

_,'

""~

-~~

,,,.;."

'''~-"~~""' ............

--

J--.

"/?,;#"

!P,JJ,,,~

~-JI~
_./

5]

J..~m t~lrt;:.....;.

t1V ~oo'IA{l-:MJ
Lr lf)t-05l. .,,...
t '1 CS( ~_'1_.__..f--'"I
,... f)~
_____....L~/~
@5
I ?01/.i"'"'IA U< \
~/h~~~-1--~
f)~_c..__k

it-

~-. ___,~

_.L

--u.r--- -1dk~=l,bfl.

c_..._

1-~-'t-- __0

"? l- f"'- UJ... ~~-~

L-

i.

~----c-----..1..,--~---t----------~------------1-------1--------

------._...---------+---------1-------1------~1-------1-------
~

-----___.v------1--~------~-----~--------1----r-----

-----------.i.-------1--------1------+--'-------t------r----------- --
-----'--------..L-----1~--------+------i------t------

ro

----------- -

- - - - - - - L - - - - - t - - - - - - - - - - 1 - - - - - - - - - . - - - - - 1 - - - - - - - - - - - - ----- ------- ----- - - ' - - - - - - - - ' - - - . - L - - - - - 1 - - - - - - - - 1 - - - - - - - - - - - - t - - - - - - - 1 - - - - - - - - - - - - - - - ------------- ------

_:________:___ _ _ _. L - - - - 1 1 - - - - - - - - - - + - - - - - - t - - - - - - - - - - - - - - - - - - - - - _

____:_~~-'------L-------11------------r--------+------t-------

---------- -

~~----L------ll-----------f------t----11--------------

-------t:-----1---------+------.---~-------------i-

- - - - - - - - - - - - l , - ' - - - - - - 1 - - - - - - - - - - - + - - - - - - t - - - - - r - - - - - - - - - 1 - - - - - - - - - -------------t-'-----1~-----------+--------+------1------1----------

--

- - ' - - - - - - - - + - - - - - t - - - - - - - - - - - - - l - - - - - - - - 1 - - - - - 1 - - - - - - - ----------r-
--------t---------1-------"--------1------------ -------------11---------t-------------1------- - - - -------1-------t----------.--------1-------------~-------l------1------

--~r-----------

-------------- -----

- - - - - - - t - - - - - - - t - - - - - - - - - - + - - - - - - - - 1 - - - - - - - - - - - - - _ _ _ _ _ ,_ _ _ _,_ __

---~----t--------1------------1-------------+----l------i-------

-----

~-:___~----t-------1---------t------t--------t--------- ~-~-
--------------~--------t-------11-------1--------------c--------

-------+-------1----------+------i----------t------~------r-----
---~---t---------1-----------+------r------l-------i----------

---------r------1----------------.--------t------------------"'---------~--

--------r------1----------------1---------1-----1-----~-------i---

------'-------t-----l----'---------1-----------1--------

--------1--------------

-'------------r------1-------------~--------+------I-----

---------

--~

27

-~~=-'.'J _ __IZZ!z_Jr-

L-(]._ _____u_~~0-

-i <-,,,.-.

wt.,.

<
c..._..

----1----"----~-I---~-- ~
/""- -

<

--""'---'------l------V--'---r._1--_1---fdu:t:}rf!___ __c::::_

1--------

-------1-----.--------------------------------I-------------+

------------- -- - - - - -

- - - - - l - - - - 1 - - - - - - - - - - - - - - - - - --------

-------------4----1---------

----------r----
-----------{------

_ _ _,.___

---1---------- -

------------ - - - -

--~-----------.--------

------~----0---------------------

---+

- - - - - - - - - ------~------------------------------

------ - - - - - - -

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- - - - - - - - - - - r - - - - t - - - - - - - - - - - - - --- - - - -

---~------,

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--

-------I-----

----------

----1-------------

- - - - - - - - - - - - - - - ! - - - - - - - - - - - - - - - - - 1 - - 1----------------------

----------r---r------
_ __.___________

---1------1-----1-------- --

--~~,

- - -

_ _ _,____________

- - - - - - - - - - - - ---

1 -----
_________________,-,
- - - - - - - - - - r -1
-------t-
~

_ _ _.__ _ _ _ _ - - - -

~----+---------------------- -------~-

-----------1-------,-----1---------

------------'---------r-------t------------ ___________,_ _ _ _,_______

--------------1----

----------------'---r----------t-------------------- - - - - - - - - - - - - - - - - - - - - --------------- -----------

---------1~'-------------~~--------~-- --------~- - - - - - - - 1 - - - - - - - - 1 - - - - - - - - - - - ----

______,____________

~-~--------

_ _ _J_----~--~-------

_______________, ____

-----------1------------------- -----1---------------- ---

_ ___________,:---------------------------------+- - - -
- - - - , - - - - - - - - - - - - - - - - _____,,~- - 1 - - - - - - - - - - - - - - - - - - -

-------------!--

+------------------

-----

- - - + - - - - - - - - - - - ------------- --------

10:

-:_-

---

-~-"

ISO TH NOTES

Printed: 8/8/2013 7:51 AM

~
E
~

Page 1of1

Oak Ridge Laboratory

BER L,.1 N . . .:::


SERVICES

Work Order Analysis Notes

Date

Dept

08/08/13 07:51

PREP

User
JWOLFE

601 Scarboro Rd.


Oak Ridge, TN 37830
Voice: 865.481.0683
www.eberlineservices.com

Internal Work Order

Analysis Code
Run Number

13-07154

Thi SO
1

Notes

ALIQUOTED AND ADDED SPIKES AND TRACERS- PRESERVED FRACTIONS 4-6, 8 AND 9, 12 AND 13
WITH HN03- DRIED SAMPLES DOWN

Printed: 8/13/2013 3:47 PM

Page 1of1

~EBER~~~c~
Work Order Analysis Notes

Date

08/08/13 07:51

08/13/13 15:47

Dept

User

Oak Ridge Laboratory


601 Scarboro Rd.
Oak Ridge, TN 37830
Voice: 865.481.0683
www.eberlineservices.com

Internal Work Order

Analysis Code
Run Number

13-07154

ThiSO
1

Notes

PREP

JWOLFE

ALIQUOTED AND ADDED SPIKES AND TRACERS- PRESERVED FRACTIONS 4-6, 8 AND 9, 12 AND 13
WITH HN03- DRIED SAMPLES DOWN

CHEM

JDEMELAS

Added concentrated HN03 to sample beakers and heated to dryness; Added 20 ml 8N HN03 to samples and
transferred to new, labeled C-Tubes, adding 8N HN03 to bring volume to -35 ml; Preconditioned resin
columns with 50 ml 8N HN03; Centrifuged samples as needed, and passed through columns; Rinsed C-Tubes
with 20 ml 8N HN03; Centrifuged rinsates and loaded onto columns; Rinsed columns with 40 ml 8N HN03;
Eluted Thorium with 50 ml of 8N HCI into clean, labeled 100-ml beakers; Dried-down samples on hotplate;
Dissolved samples in -10 ml of concentrated HCI; Transferred to new, labeled C-Tubes with deiononized
water brinoino volume to -15ml. Set samoles aside for later orecioitation and filterina.

Printed: 8/14/2013 5:57 AM

Page 1of1

Oak Ridge Laboratory

,E:aE:R......lN E:

SERVICES

Work Order Analysis Notes

# I

Date
08/08/13 07:51

Dept

PREP

User
JWOLFE

08/13/13

i5:47+

08/14/13 05:57

I
I
I

CHEM... +JDE--MELAsI

CHEM

RM ARTZ

601 Scarboro Rd.


Oak Ridge, TN 37830
Voice: 865.481.0683
www.eberlineservices.com

Internal Work Order

Analysis Code

13-07154

Thi SO
1

Notes
ALIQUOTED AND ADDED SPIKES AND TRACERS- PRESERVED FRACTIONS 4-6, 8 AND 9, 12 AND 13
WITH HN03- DRIED SAMPLES DOWN
Added concentrated HN63 to sample beakers and heated to dryne55;'A:cicieci2omiat::THN03fo sampies and
transferred to new, labeled C-Tubes, adding 8N HN03 to bring volume to -35 ml; Preconditioned resin
columns with 50 ml 8N HN03; Centrifuged samples as needed, and passed through columns; Rinsed C-Tubes
with 20 ml 8N HN03; Centrifuged rinsates and loaded onto columns; Rinsed columns with 40 ml 8N HN03;
Eluted Thorium with 50 ml of 8N HCI into clean, labeled 100-ml beakers; Dried-down samples on hotplate;
Dissolved samples in -10 ml of concentrated HCI; Transferred to new, labeled C-Tubes with deiononized
water brinaing volume to -15ml. Set samples aside for later precipitation and filterina.
ADDED 0.75 ML 0.1MG/ML CERIUM CARRIER & 1 ML HF TO C-TUBES & LET SET SIT IN ICE BATH FOR
ONE HOUR; SET UP FILTERS BY ADDING ALCOHOL & CARBON SUBSTRATE THEN ADDED SAMPLES;
WHEN SAMPLES WERE THROUGH FILTERS, ADDED 10 ML DI H20 RINSES FROM C-TUBES,
REMOVED FILTERS LET DRY IN DESSICATOR THEN SENT SET TO COUNT ROOM.

Eberline Analytical
Oak Ridge Laboratory

Printed: 8/14/2013 5:58 AM

Page 1 of 1

Internal Work Order

13-07154
Reagents Used in an Analysis
Reagent
ID

014109P

Reagent
Name

Analysis Code

Run

Th ISO

Reagent
Concentration

Nitric Acid

Analyst
ID

JWOLFE

"''"''''"'~'''''''"'.

Anion Exchange Resin

JDEMELA5

Hydrochloric Acid

JDEMELA5

,,,,y,,,,,,,,,,

Hydrochloric Acid
' ' ' ' ' ' ' ' ' " ' ' ' - ' ,,,,,

__

Reagent Grade

JDEMELA5

S/13/2013

SN
SN

JDEMELA5

S/13/2013

JDEMELA5

S/13/2013

, , , , , , , , , , ,,,,,

0142495

Nitric Acid

0142365

Nitric Acid

014109P

Nitric Acid

JDEMELA5

8113;20'13'1

0140425

Carbon substrate

RM ARTZ

S/14/2013

----

~-~~~,~

0140405

Cerrium Carrier

RM ARTZ

013221P

Hydrofluoric Acid

RM ARTZ

,_ _ _ _ ,,_,~-www+---~~---'''''-0---~--~~-~

,~~---,--~-~----A--~-~-----~-,,,,_,+---~~,---~--~-

013574P

Reagent Alcohol

RM ARTZ

,I

-~-,--1

14/2013 II
''l
12013 I
'""-.~"~""i

14;2013

"""""''''.,,,,"'~"'''J

- - - - 4 . . - - - - - + - - - - - - - - - - + - - - - - - - - 1 - - - - - - - - - - 1 - - - - - - - t r - - - - - - 1 - - - - - - - - - , _,_I'

..

.-.:

--~-----1---------------1-----------------1----------

- - - - - - - -------

-------';&...---~---------l--------+----T----------11-----------1--~~-

--~--~-------'-------1-------_.___--------------------1-------,

-------l-------------t-------i----------1--------1---

-----------------1-----------f-------f-----f------f-------I----.
------~ -~..........,..~

----------1-------------1------------+-------------
--~-------1-------------1--------

- - - - - - - - - . -~----~ - - - - -------------

-,,

----~---------11------------1--------f------- ---------1-------1----~'

- - - - ' 1 - - - - - - - J 1 - - - - - - - - - - - l - - - - - - - - - - - - 1 - - - - - - - - f - - - - - - - - - - - - - - ' - - - - - --.

--
-

-;._
- - - l " - - - - - - - J 1 - - - - - - - - - 1 - - - - - - - - - + - - - - - _ _ _ _ _ _ _ _,________.____ _r.,

.-,,_
_:

____________,__

~--'f'-----1--------------1----------<------------+-------

;:,. f

__,,_

'::
;

,_.;

-----<T------~---------'-----------1----------t------------+---------------~-Y

:_.:

'

.l

~--~---_J___----------1------------ - - - - - - - - - 1 - - - - - - - 1 - - - - - - - - l - - - - - - - - < v - .',_-_-,


:

i
,_ _ _ _ - - - ______________ ,______________._________,,
: .:

- - - - - - ' I -r - - - - - - - 1 - - - - - - - - - - -

,_
- - - ' - - ' - - - - - - - i - - - - - - - - 1 - - - - - - - - - - - - - - - - 1 - - - - - - - - ------ ---------1----------------1-----1----~--_ _ _ _______, _ _ _ _ _________. _ _ _ _ _ _ _ _ _------11------------~-----

:_

-----------I--------~---____.__--~-""

_ __..~---------t--------1--------1-- ------1-----~
I

a"s~
--------------------ff

I
r

__,~~---f__UO_

--~~~'-'--"-l~

--1r---~t-'-'-.- \ ,~Dl~-'flL'-4_-:JJ) ___6_tn_~,.____----1,--_,____--tc>L

_________._ _ ____.
-----ir------t----------------

-~-

--------11--------1-----1~---------

____;;------- - - - - - - - - - - - - - - - - - - - -

=1-

------1------- ----- - -

_..__ _______,,______ _ _,______

--------------------------'----------

--1--~i

-t- - .--------~-=--=~==~-=----=--- -~-===-===-- -


.. _ J - - - - - - - -- - - - ; - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - -

- - - - - - - - - - - - - - - ---------------------1------1------1---llilll
---1------ ------- ---

--------------'

- - - - - - - - - - - - - - - - - - - - - - - - - - --- - - - - - - - ----,.--~------------- ~------- ---------~~-

~~

----

--------------------------

-~-

------------- - -

103

72

RA-226 NOTES

riS73

Printed: 8/7/2013 10:35 AM

Page 1of1

~EBERLIN,!::

Oak Ridge Laboratory

SERVICES

Work Order Analysis Notes

#
1

Date

Dept

08/07/13 10:35

PREP

User
JWOLFE

601 Scarboro Rd.


Oak Ridge, TN 37830
Voice: 865.481.0683
www.eberlineservices.com

Internal Work Order

Analysis Code
Run Number

13-07154
Ra226
1

Notes
ALIQUOTED AND ADDED SPIKES AND TRACERS- PH'D SAMPLES- PRECIPITATED WITH BA AND PB
CARRIERS AND AMMONIUM SULFATE- DECANTED SAMPLES AND CENTRIFUGED- SUBMITTED
RADIUM PRECIP TO SEPARATIONS

Page 1of1

Printed: 8/8/2013 4:57 PM

j!J EB E;::R LI NE;;


~

SERVICES

Work Order Analysis Notes

Date

Dept

08/07 /13 10:35

PREP

JWOLFE

08/07 /13 19:42

PREP

LWALKER

08/08/13 16:57

PREP

User

LWALKER

Oak Ridge Laboratory


601 Scarboro Rd.
Oak Ridge, TN 37830
Voice: 865.481.0683
www.eberlineservices.com

Internal Work Order

Analysis Code
Run Number

13-07154
Ra226
1

Notes
ALIQUOTED AND ADDED SPIKES AND TRACERS- PH'D SAMPLES- PRECIPITATED WITH BA AND PB
CARRIERS AND AMMONIUM SULFATE- DECANTED SAMPLES AND CENTRIFUGED- SUBMITTED
RADIUM PRECIP TO SEPARATIONS
ADDED EDTA TO PRECIP-VORTEX-LET SIT OVERNIGHT TO DIGEST.
FOLLOWED STEPS 12.1 TO 12.8 IN AP-006 REV 12 FOR RA 226 ANAL YSIS-(SYRINGE FILTERED
PRECIP-FIL TERED-DRIED-OBTAIN FINAL WEIGHT)-SUBMIT TO COUNT ROOM.

875

Eberline Analytical
Oak Ridge Laboratory

Printed: 8/9/2013 8:45 AM

Page 1 of 1

Run

Ra226

Reagents Used in an Analysis

Reagent

lll"ame
013376P

Ammonium Hydroxide

JWOLFE

013930003

Ammonium Sulfate

JWOLFE

014007002

Barium Carrier

1 mg/ml

JWOLFE

014008002

Lead Carrier

166 mg/ml

JWOLFE

109P

Nitric Acid

JWOLFE

212S

EOTA

LWALKER

011383P

Acetic Acid

LWALKER

013575005

Ammonium Sulfate

200 mg/ml

LWALKER

fHJ76

10:

----1

-.-t-
.

---~

-----t--
----t
-----~--

---+-

,.

______;,___ - - - - - - - - - - - - - - - : - - - : - - - - - - - - -

---~-__...'...._.

______________ --

- ---- -----

--

------------

--~----------------

---

_:._.:.._~---~--------

----- ---

-- - -

---

--------- -

--

---

----- -

---

- - - - - - - - - ------~-

----- - - - - - - - - -

--- - - - - -

-- - -

--

----

--- - - - - - - - - - - - - - - -

- - -- - - - - - - - -

---- - - - - - - - - - -

-----

----------- - - - - - - i - - - - - - - -----I

fiiS78

RA-228 NOTES

Printed: 8/7/2013 10:35 AM

Page 1of1

3J
E: EIJ:: B. J-~ ~. J::
~

SERVICES

Work Order Analysis Notes

Date

Dept

08/07/13 10:35

PREP

User
JWOLFE

Oak Ridge Laboratory


601 Scarboro Rd.
Oak Ridge, TN 37830
Voice: 865.481.0683
www.eberlineservices.com

Internal Work Order

Analysis Code
Run Number

13-07154
Ra228
1

Notes
AUQUOTED AND ADDED SPIKES AND TRACERS- PH'D SAMPLES- PRECIPITATED WITH BA AND PB
CARRIERS AND AMMONIUM SULFATE- DECANTED SAMPLES AND CENTRIFUGED- SUBMITTED
RADI M PRECIP TO SEPARATI NS

Printed: 8/14/2013 5:12 PM

Page 1of1

;:EBER~~~~
Work Order Analysis Notes

Date
08/07/13 10:35

Oak Ridge Laboratory


601 Scarboro Rd.
Oak Ridge, TN 37830
Voice: 865.481.0683
www.eberlineservices.com

Internal Work Order

Analysis Code
Run Number

13-07154
Ra228
1

Dept
User
Notes
PREP ---;-J-W_O_L_F_E---+--A-Ll_Q_U_O_T_E_D_A_N_D_A_D_D_E_D_S_P_IK_E_S_A_N_D_T_RA_C-ER_S
___P_H-'D_S_A_M_P_L_E_S--P_R_EC-IP--l--TA_T
__
______
ED_W-..,,IT"""H"'""B_,,A-,A'"""N""D-:P:-:B:--t1

13 17:56

PREP

LWALKER

08/14/13 17:12

PREP

LWALKER

CARRIERS AND AMMONIUM SULFATE- DECANTED SAMPLES AND CENTRIFUGED- SUBMITTED


RADIUM PRECIP TO SEPARATIONS
RECEIVED FILTERS BACK FROM COUNT ROOM-PUT BACK INTO C-TUBES-ADDED EDTA AND
SWIRLED-LET SIT OVERNIGHT TO DIGEST.
FOLLOWED STEPS 12.1TO12.7 IN AP-007REV18 (CHEMICAL CLEANUP FOR RA 228)

Page 1of1

Printed: 8/15/2013 6: 11 AM

2J
E:.. e
~

Oak Ridge Laboratory

l;;.. .R LI

I;;

SERVICES

Work Order Analysis Notes

601 Scarboro Rd.


Oak Ridge, TN 37830
Voice: 865.481.0683
www.eberlineservices.com

Internal Wor1< Order

Analysis Code
Run Number

13-07154
Ra228
1

Date

Dept

08/07/13 10:35

PREP

JWOLFE

08/09/13 17:56

PREP

LWALKER

08/14/1317:12

PREP

LWALKER

FOLLOWED STEPS 12.1TO12.7 IN AP-007REV18 (CHEMICAL CLEANUP FOR RA 228)

08/15/13 06: 11

CHEM

TSMITH

Followed steps 12. 7 to 12.15 in AP-007 rev. 17 . ( Precipitated samples, hot bathed, centrifuged, and
discarded supernate. Dissolved precip, precipitated samples, hot bathed, centrifuged, and discarded
supernate. Dissolved precip, precipitated and filtered samples, obtained final weights, covered with aluminum
foil and took to count room \

----o

User

Notes
ALIQUOTED AND ADDED SPIKES AND TRACERS- PH'D SAMPLES- PRECIPITATED WITH BA AND PB
CARRIERS AND AMMONIUM SULFATE- DECANTED SAMPLES AND CENTRIFUGED- SUBMITTED
RADIUM PRECIP TO SEPARATIONS
RECEIVED FILTERS BACK FROM COUNT ROOM-PUT BACK INTO C-TUBES-ADDED EDTA AND
SWIRLED-LET SIT OVERNIGHT TO DIGEST.

Eberline Analytical
Oak Ridge Laboratory

Printed: 8/15/2013 7:20 AM

Page 1 of 1

Internal Work Order

13-07154
Ra228

Reagents Used in an Analysis


Reagent
ID

Reagent
Name

013376P

Reagent
Concentration

Ammonium Hydroxide

Grade

---t-----

013930003

Ammonium Sulfate

Analyst

ID

JWOLFE

8/7/2013

JWOLFE

8/7/2013

---+~--~------------------~~----+-~~~--~---~~........+--~~~~~-+~~~---1

014007002

Barium Carrier

1 mg/ml

JWOLFE

8/7/2013

014008002

Lead Carrier

166 mg/ml

JWOLFE

8/7/2013

014109P

Nitric Acid

Reagent Grade

JWOLFE

8/7/2013

011504033

Ammonium Sulfide

LWALKER

8/14/2013

014008003

Lead Carrier

1.5 mg/ml

LWALKER

8/14/2013

Reagent Grade

LWALKER

014109P

ic Acid

--~-~~~~~----~~~4-~

013065010
013955001

ium Hydroxide
Yttrium Carrier
Oxalate

lOM
9 mg/ml
5%

lN
Nitric Acid

6N

Sodium Hydroxide

lOM

8/15/2013

Sodium Hydroxide

18M

8/15/2013

LfJLfllD

1
.i.

1J

- - - - - - - ---------------- - - - - - - - - - - - - - - - - - - - - - - - - - 1 - - - - - - - - - - - 1 -

---~---

--" - - - - ------- -~---- - - ------------

-------1---------

--------------~-

--

---------lc---------1---

- - - - - - - ------ - - - - - - - - - - - - - - - - - 1 - - - - - - - - - -

--------- - - - - - - - - - - - - - - - - - - - - - - - - - - - - t - - - - - - - - - 1 - -

--------------------- - - - - - - - - - 1 - - - - - - - - - 1 - - - - -
------1-------1-----

-----------------
- ------------------ - - - - - - - - - - - 1 - - - - - - - - - 1

---- --------1--------
l

- - -------+-----
i

---r

---------------------~~------~-

------------ - - - -

-------------- - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - 1 - - - - - - - - - - - 1 - -

-. L- -.----------------------~=~~::==-=~----=-----~-~-----1----------t-~l--I

-----1--------------
I
'
----+---

_____,__________,___

-- --------------------- ------- -- ------------ ---- - - - - - - - - - - - - - - - - - - - + -


-------------- -----------1---------1

- - - ---------1-----------1-----
I

-~~--

--------- -----------1---------1

'------------
-------11----------

------- ------------- ---- - - - - - - - - J - - - - - - - - - - 1


-------------

- - - - - - 1 - - - - - - - - - - ----

-----:-----------------

L rJ"'t l lo /J't,k~
.

29

-:[ ifL~

"---"--'-----

____

,___

"

--

-------~----

_____ " - - -

,____

-"--------"-~~---+----"---------------

--

"--- --"

-----------------------~-----

_ _ _ ------

,____"

--+------!---------" - - - "

-----------'">

--

- - - - -------- -----1--

-------1----"----- - - - - -

----1-------------

--------

_ _ _ _____,
"

" - - - - --------

- " "

-------1-

- - - - - " - - - - - ---..---~-----

_ _ _ _,,__ _ _,_______,_

------

--------1-" - -

SECTION VIII

ANALYTICAL DAT A (ISOTOPIC URANIUM)

Eberline Services
Oak Ridge Laboratory
Analysis Sheet

Printed: 8/1412013 5:58 AM


Page 1of3

13-07154
UUISO
Run 1
I

Internal
Fraction

13-07154

Work Order

UUISO

Analysis Code

Run
Date Received I

I Sample
Desc
!

Client
ID

01

LCS

LCS

02

MBL

BLANK

DUP

03

8/13/2013

Client I Engineering Management Support, Inc.

01119113 12:10 I

TRG

PZ-200-SS TOT

42

07/19/13 10:1gr- 1.0000E+OO

TRG

PZ-200-SS DIS

42

07/19/13 10:19

1.0000E+OO

38

07/19/13 10:30

1.0000E+OO

38

07/19/13 10:30

-~

-1-

06

TRG

PZ-102-SS TOT

TRG

PZ-102-SS DIS

!--------~

Report Level

07

i
I

07/19/13 12:10

1.0000E+OO

07/19/13 12:10

1.0000E+OO

45

07/19/13 13:09

1.0000E+OO

PZ-106-KS DIS

45

07/19/13 13:09

1.0000E+OO

TRG

DUP 08 TOT

44

07 /19/13 00:00

1.0000E+OO

TRG

DUP 08 DIS

44

07/19/13 00:00

1.0000E+OO

DO

PZ-107-SS TOT

46

09

II TRG

PZ-107-SS DIS

46

WA

10

I TRG

PZ-106-KS TOT

HASL 300, 4.5.2

11

TRG

Alpha Spectroscopy

12

pCi

08

1.0000E+OO
...

-----

L__.._________.~~--

Activity Units

1.0000E+OO

46

--~~-

05

West Lake OU-1

1.0000E+OO
I

PZ-107-SS TOT

1----

Project I

1.0000E+OO

..

04
1---------------~-----

07 /24/13 00:00
--

7/22/2013

Sample
Aliquot

07/24/13 00:00

--

Lab Deadline I

Sample
Date

Login
CPM

C-----~

Aliquot Units
Matrix
Method
Instrument Type

Radiometric Tracer

U-232

13

Radiometric Sol#

U-10a

Tracer Act (dpm/g)

19.04

I
I

,
--

Carrier
II

Carrier Cone (mg/ml)

~.

----

11'.1,
~~

1"))

.....~

SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only.

Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.

Eberline Services
Oak Ridge Laboratory
Analysis Sheet

Printed: 8114/2013 5:58 AM


Page 2 of 3

13-07154
UUISO
Run 1

Internal
Fraction

I
I

Sample
Desc

Tracer
A/iquot(g)

Tracer Total
ACT(dpm)

01

LCS

0.6129

11.7

02

MBL

0.6069

11.6

03

DUP

0.6064

11.5

TRG

0.6051

11.5

Radiometric
Tracer (pCi)

I Radiometric
I %Rec
!

Grav Carrier
Added(ml)

Grav Filter
Final (g)

Grav Filter
Net(g)

Grav
%Rec

Mean
%Rec

!
I
!

SAF
1*

0.00
0.00

Grav Filter
Tare (g)

0.00

04

0.00

05

TRG

0.6041

11.5

0.00

06

TRG I

0.6021

11.5

0.00

07

TRG

0.6025

11.5

0.00

08

DO

0.6025

11.5

0.00

09

TRG

0.6058

11.5

0.00

10

TRG

0.6002

11.4

0.00

11

TRG

0.6056

11.5

0.00

12

TRG

0.6049

11.5

0.00

13

TRG

0.6040

11.5

0.00

'

I
~

112ii
t.t~

(.)i;)

0:)

* SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only.

Actual mass exceeded the calibration curve range_ Results should be qualified as appropriate.

SAF
2*

Eberline Services
Oak Ridge Laboratory
Analysis Sheet

Printed: 8/14/2013 5:58 AM


Page 3 of 3

13-07154
UUISO
Run 1

Internal
Fraction

Sample
Desc

01

Rough Prep
Date

Rough Prep

Prep
Date

Prep

LCS

08/08/13 07:47

JWOLFE

02

MBL

08/08/13 07:47

JWOLFE

03

DUP

08/08/13 07:47

JWOLFE

By

Sep to
Date/Time

By

Sep t1
Date/Time

Sep to

By

Sep t1

By

----

------

--

---

04

TRG

08/08/13 07:47

JWOLFE

05

TRG

08/08/13 07:47

JWOLFE

06

TRG

08/08/13 07:47

JWOLFE

07

TRG

08/08/13 07:4 7

JWOLFE

08

DO

08/08/13 07:47

JWOLFE

09

TRG

08/08/13 07:47

JWOLFE

10

TRG

08/08/13 07:4 7

JWOLFE

11

TRG

08/08/13 07:47

JWOLFE

12

TRG

08/08/13 07:47

JWOLFE

1-----------------

13

TRG

08/08/13 07:4 7

JWOLFE
I

I
I

m
~~~

()()

till

SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only.

Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.

Eberline Services
Oak Ridge Laboratory

Work Order: 13-07154-UUIS0-1

::i

Nuclide

Sample
Desc

Client
Identification

Activity
Units

01

U-234

LCS

LCS

pCi/I

7.96E+OO

1.08E+OO

6.48E-02

It

(.)

.,

.~

.,,

c:

C(

04

::>
::>

LCS
Known

8.17E+OO

LCS
%R

LCS
Flag

97.39

OK

RPO
Flag

MDA
Flag

Blank
Flag

OK

MBL

BLANK

pCUI

3.12E-01

1.29E-01

7.42E-02

U-234

DUP

PZ-107-SS TOT

pCUI

1.31E+OO

3.51E-01

1.06E-01

U-234

TRG

PZ-200-SS TOT

pCi/I

9.65E-01

2.65E-01

9.18E-02

OK

OK

OK

OK

---

OK
'

-----

f---------

en

MDA

U-234

03

Error Estimate

~---------

!--------

Results

02
~

Lab
Fraction

- - - - - -----

c:

Printed: 8/14/2013 2:45 PM

Page 1 of 3

Preliminary Data Report & Analytical Calculations

U-234

TRG

PZ-200-SS DIS

pCi/I

4.86E-01

1.76E-01

9.47E-02

OK

U-234

TRG

PZ-102-SS TOT

pCi/I

4.67E+OO

7.SOE-01

7.92E-02

OK

U-234

TRG

PZ-102-SS DIS

pCi/I

5.84E+OO

8.87E-01

8.42E-02

OK

U-234

DO

PZ-107-SS TOT

pCi/I

1.65E+OO

3.58E-01

9.18E-02

OK

09

U-234

TRG

PZ-107-SS DIS

pCi/I

1.85E+OO

5.SSE-01

1.94E-01

OK

10

U-234

TRG

PZ-106-KS TOT

pCi/I

2.04E+OO

4.29E-01

9.02E-02

OK

11

U-234

TRG

PZ-106-KS DIS

pCi/I

2.02E+OO

5.10E-01

1.39E-01

OK

U-234

TRG

DUP 08 TOT

pCi/I

1.74E+OO

5.84E-01

1.SSE-01

OK

U-234

TRG

DUP 08 DIS

pCi/I

1.57E+OO

4.46E-01

1.45E-01

OK

05
:----~-- ~

06

----------- 1------

07
------- --

08
-

- - - - ---

12
~

c.i

..5
~

13

--- -r----

Q.
Q.
::I
(/)

c:

------- ---- -

---------

--------------- -

-------~-------

Ql

~I

Ql

en
C'CI
c:
C'CI

::ii:
en
c:
;:
Ql
Ql

.::en
c:

w
~
ii:~

llll:li
(:It!!

---------l--------

--=-t~-----------r-----------1
I

c::

""""

.g

8
~

~
~

Printed: 8/14/2013 2:45 PM

Page 2 of 3

Preliminary Data Report & Analytical Calculations

Eberline Services
Oak Ridge Laboratory

Work Order: 13-07154-UUIS0-1

Sample
Desc

Sample
Date

01

U-234

LCS

07/24/13 00:00

1.00E+OO

104.75

0.00

0.00

02

U-234

1.00E+OO

116.05

0.00

0.00

1.00E+OO

95.27

0.00

0.00

07/19/13 10:19

1.00E+OO

104.50

0.00

0.00

07/19/13 10:19

1.00E+OO

120.62

0.00

0.00

07/19/13 10:30

1.00E+OO

102.86

0.00

0.00

07/19/13 10:30

1.00E+OO

103.98

0.00

0.00

07/19/13 12:10

1.00E+OO

104.99

0.00

0.00

07/19/13 12:10

1.00E+OO

49.93

0.00

0.00

07/19/13 13:09

1.00E+OO

85.34

0.00

0.00

07/19/13 13:09

1.00E+OO

80.80

0.00

0.00

03

U-234

04

U-234

TRG

MBL
-

Radiometric
%Rec

Mean
%Rec

Nuclide

07/24/13 00:00
-
DUP
07/19/13 12:10

Sample
Aliquot

Grav
%Rec

Lab
Fraction

SeptO
Date/Time

SAF

~-----

en

:::>

:::>

05

U-234

06

U-234

07

U-234

TRG

1.;~-~
TRG

------

------'--
I

08

U-234

09

U-234

DO

TRG

----

10

U-234

TRG

11

U-234

TRG

----

-----

..;
..E

12

U-234

TRG

07/19/13 00:00

1.00E+OO

38.59

0.00

0.00

13

U-234

TRG

07/19/13 00:00

1.00E+OO

59.06

0.00

0.00

- ------

~
0

c.
c.

:l

(/)

--

c:

c: I
~I

t----~----

QI

QI

--

Cl
tll

c:

tll

==Cl
c:

;:

QI
QI

.!:

Cl

c:

w
ti~

t:tar
(,jl

I~""

-----

Sep t1
DatefTime

,:

Sample
Desc

Counting
Date/Time

01

U-234

LCS

02

U-234

------ - - - - - - - - - - -

03
Gl

"O
0

(J

.!!!
II)

oq

l!

t:

(,/)

::>
::>

Cit

"'
"'
"'

(I)

Counts

Bkg
CPM

Eff

Carrier

08/14/13 09:26

A_Spec

Alpha_013

170.02 5.87 E+o2

2.00 E-03

18.7

MBL

08/14/13 09:26

A_Spec

Alpha_014

170 2.52 E+01

5.00 E-03

18.5

DUP

08/14/13 09:26

A_Spec

Alpha_015

170.02 6.93 E+01

4.00 E-03

14.8

04

U-234

TRG

08/14/13 09:27

A_Spec

Alpha_019

170.02 6.30 E+01

0.00 E+OO

16.6

05

U-234

TRG

08/14/13 09:27

A_Spec

Alpha_022

170.02 3.38 E+01

7.00 E-03

15.3

06

U-234

TRG

08/14/13 09:27

A_Spec

Alpha_023

170.02 3.09 E+02

3.00 E-03

17.1

07

U-234

TRG

08/14/13 09:27

A_Spec

Alpha_024

170.02 3.91 E+02

4.00 E-03

17.1

08

U-234

DO

08/14/13 09:27

A_Spec

Alpha_025

170.02 1.13 E+02

6.00 E-03

17.4

09

U-234

TRG

08/14/13 09:27

A_Spec

Alpha_027

170.02 6.00 E+01

6.00 E-03

17.3

10

U-234

TRG

08/14/13 09:27

A_Spec

Alpha_029

170 1.27 E+02

4.00 E-03

19.5

U-234

TRG

08/14/13 09:27

A_Spec

Alpha_031

170 8.72 E+01

5.00 E-03

14.2

U-234

TRG

08/14/13 09:28

A_Spec

Alpha_033

170 4.68 E+01

1.00 E-03

18.5

U-234

TRG

08/14/13 09:28

A_Spec

Alpha_034

170 6.50 E+01

0.00 E+OO

18.6

11

Count
Time

Detect

f-

U-234

----

--------

12

ifi

Halflife
(days)

---------

------

Work Order: 13-07154-UUIS0-1

Nuclide

Lab

Fraction

Printed: 8/14/2013 2:45 PM


Page 3 of 3

Preliminary Data Report & Analytical Calculations

Eberline Services
Oak Ridge Laboratory

.E

13

-----

------~

~
0

a.
a.

~-----i

::I

Cl)

....c

(J

-------------

QI

QI

-------

~-~-~~-~-=~t=
I!

----------

~~--~-~~-~-- -~-~~~r----

---------

---------------+---

.5

~- . --- ------- ------------!---

C'I
Cll

Cll

::E

C'I
QI
QI

C'I

w
a~

idirl
(,ll)

---

---

~-

a::

"""""

Printed: 8/14/2013 2:45 PM

Page 1 of 3

Preliminary Data Report & Analytical Calculations

Eberline Services
Oak Ridge Laboratory

Work Order: 13-07154-UUIS0-1

LCS
%R

LCS
Flag

112.17

OK

LCS
Known

RPO
Flag

MDA
Flag

Lab
Fraction

Nuclide

Sample
Desc

Client
Identification

Activity
Units

01

U-238

LCS

LCS

pCi/I

8.93E+OO

1.19E+OO

7.09E-02

02

U-238

MBL

BLANK

pCi/I

6.36E-02

6.03E-02

7.39E-02

U-238

DUP

PZ-107-SS TOT

pCi/I

1.44E+OO

3.71E-01

7.84E-02

U-238

TRG

PZ-200-SS TOT

pCi/I

8.00E-01

2.37E-01

8.00E-02

OK

U-238

TRG

PZ-200-SS DIS

pCi/I

4.13E-01

1.58E-01

5.97E-02

OK

U-238

TRG

PZ-102-SS TOT

pCi/I

4.43E+OO

7.20E-01

9.47E-02

OK

U-238

TRG

PZ-102-SS DIS

pCi/I

3.85E+OO

6.46E-01

8.38E-02

OK

08

U-238

DO

PZ-107-SS TOT

pCi/I

1.42E+OO

3.24E-01

6.0SE-02

OK

09

U-238

TRG

PZ-107-SS DIS

pCi/1

8.32E-01

3.45E-01

1.83E-01

OK

Results

Error Estimate

MDA

7.96E+OO

OK

- - - -r - -

03

OK
OK

OK

---------

.!!!
~
Cii
c:
<:(

0
en

::>
::>

04
---

----

05
--

06
---

~---

07
~--

----- !-------------
- - - ------------

10

~-- ~-

OK

U-238

TRG

PZ-106-KS TOT

pCi/I

9.31E-01

2.64E-01

8.36E-02

U-238

TRG

PZ-106-KS DIS

pCi/I

7.79E-01

2.97E-01

2.10E-01

OK

U-238

TRG

DUP 08 TOT

pCi/I

1.51E+OO

5.33E-01

1.77E-01

OK

TRG

DUP 08 DIS

pCi/I

9.33E-01

3.24E-01

1.15E-01

OK

----- --

11

--

r------------

12
~--

.5

---

13

U-238

-----

a.
a.

- - - ---

----

QI

- - - - - --------

:s

U)

c:

QI

u~1

Cl

ca
ca

Cl

c:

;:
QI
QI

.:

-=t--+--------

~-----

I
I

~~

tl!'l!I
1.:r~11
~-ll

c:

::il:

Blank
Flag

- >--------

OK

"""""

----

LCS

07/24/13 00:00

1.00E+OO

104.75

0.00

0.00

U-238

MBL

07/24/13 00:00

1.00E+OO

116.05

0.00

0.00

07/19/13 12:10

1.00E+OO

95.27

0.00

0.00

U-238

DUP

(J

.!!!
~

;;;
c:

c:(

04

Sep to
Date/Time

SAF

----

!------------

I
I

-------

~-

03

Mean
%Rec

Grav
%Rec

U-238

01

Sample

Sample
Aliquot

Radiometric
%Rec

Sample
Date

Nuclide

02

c:

Work Order: 13-07154-UUIS0-1

Desc

Lab
Fraction

Printed: 8/14/2013 2:45 PM

Page 2 of 3

Preliminary Data Report & Analytical Calculations

Eberline Services
Oak Ridge Laboratory

U-238

TRG

07/19/13 10:19

1.00E+OO

104.50

0.00

0.00

U-238

TRG

07/19/13 10:19

1.00E+OO

120.62

0.00

0.00

06

U-238

TRG

07/19/13 10:30

1.00E+OO

102.86

0.00

0.00

07

U-238

TRG

07/19/13 10:30

1.00E+OO

103.98

0.00

0.00

1------------ ---

en

::::>

05
>----

::::>

~t:

08

U-238

DO

07/19/13 12:10

1.00E+OO

104.99

0.00

0.00

09

U-238

TRG

07/19/13 12:10

1.00E+OO

49.93

0.00

0.00

U-238

TRG

07/19/13 13:09

1.00E+OO

85.34

0.00

0.00

U-238

TRG

07/19/13 13:09

1.00E+OO

80.80

0.00

0.00

1.00E+OO

38.59

0.00

0.00

1.00E+OO

59.06

0.00

0.00

----

:!

10

---

"'

Cl)

~-

11

"'
.!:

------.

't:
Cl>

12

[I

U-238

TRG

-----

13

c.i

.E

07/19/13 00:00
--- ---

U-238

TRG

07/19/13 00:00
------

----------~-

-i'
0

a.
a.
:s

------- - - - - - - - - - - - f------------ --

c:

------

(/)

---""

----

QI

i:

(J

QI

Cl

cu
cu
:ii:

-----

-- - - - - - - - - -

~~--

-------------

c:

~--------

Cl

c:
;:

----

~-

QI

QI

.5

Cl

c:

~~
e1
(.~Ji
.~iii

------------

Sep 11
Date/Time

Eberline Services
Oak Ridge Laboratory

~
I:
::i

a:

8
.~

~
iii
I:

<(

Lab

Work Order: 13-07154-UUIS0-1

I Sample

Nuclide

Fraction

01

Printed: 8/14/2013 2:45 PM

Page 3 of 3

Preliminary Data Report & Analytical Calculations

Desc

Counting
DatefTime

LCS

Halflife
(days)

Count
Time

Bkg
CPM

Carrier

08/14/13 09:26

A_Spec

Alpha_013

170.02 6.61 E+02

3.00 E-03

18.7

MBL

08/14/13 09:26

A_Spec

Alpha_014

170 5.15 E+OO

5.00 E-03

18.5

DUP

08/14/13 09:26

A_Spec

Alpha_015

170.02 7.68 E+01

1.00 E-03

14.8

08/14/13 09:27

A_Spec

Alpha_019

170.02 5.25 E+01

3.00 E-03

16.6

08/14/13 09:27

A_Spec

Alpha_022

170.02 2.88 E+01

1.00 E-03

15.3

08/14/13 09:27

A_Spec

Alpha_023

170.02 2.95 E+02

6.00 E-03

17.1

08/14/13 09:27

A_Spec

Alpha_024

170.02 2.59 E+02

4.00 E-03

17.1

08/14/13 09:27

A_Spec

Alpha_025

170.02 9.78 E+01

1.00 E-03

17.4

08/14/13 09:27

A_Spec

Alpha_027

170.02 2.71 E+01

5.00 E-03

17.3

08/14/13 09:27

A_Spec

Alpha_029

170 5.85 E+01

3.00 E-03

19.5

TRG

08/14/13 09:27

A_Spec

Alpha_031

170 3.38 E+01

1.90 E-02

14.2

TRG

08/14/13 09:28

A_Spec

Alpha_033

170 4.07 E+01

2.00 E-03

18.5

TRG

08/14/13 09:28

A_Spec

Alpha_034

170 3.87 E+01

2.00 E-03

18.6

U-238

Counts

-------~--~

02

U-238
-------

03

U-238

o4_[_

-:::> ~:
:::>

U)

07

--

~---

TRG

-r 2:

-- --- --

I TRG

U-238

08

~,;_

t-;:;;

----

I----'---

---- ------

-----t-~

09

U-238

----

~-

____j

----~--------

10

TRG
~-

~G

U-238

I
- =t~]=~
-~-238-- I

11

____j_

12

U-238

13

U-238

- - - - - ---------------

d
.5

--

U-238-+ DO
--------------

----

~
0

Q.
Q.

:I

(/)

1:
~

(.)

Ill
Cl
nl

c
nl
:!!!:
Cl
c
;:

.5

Cl

U:!i

U'll

c
Ill
E

Ill
Ill

~~
l:.'l1!/I

Eff

Detect

~+---~---

----------

1--

---

-------------- 1---------------------t----
I

c::

Lab

01

.!!!
~
ii
c::
q;

::>

::>

RPO
Flag

LCS
Flag

MDA
Flag

U-235

LCS

LCS

pCi/I

1.16E+OO

3.03E-01

8.78E-02

OK

U-235

MBL

BLANK

pCi/I

5.60E-02

6.07E-02

7.31E-02

OK

PZ-107-SS TOT

pCi/I

2.56E-01

1.61 E-01

1.40E-01

PZ-200-SS TOT

pCi/I

1.70E-01

1.19E-01

1.13E-01

OK

PZ-200-SS DIS

pCi/I

6.15E-02

8.00E-02

1.26E-01

OK

PZ-102-SS TOT

pCi/I

6.39E-01

2.28E-01

1.05E-01

OK

PZ-102-SS DIS

pCi/I

9.76E-01

2.88E-01

1.16E-01

OK

Results

Error Estimate

MDA

----

03

U-235

04

U-235

05

U-235

TRG

U-235

TRG

DUP

NA

OK

TRG
-

en

LCS
%R

Activity
Units

---

--

~
0
u

LCS
Known

Client
Identification

Sample

--------

06
- ------

--~------

07

U-235

TRG
-

-----~--

08

U-235

DO

PZ-107-SS TOT

pCi/I

1.80E-01

1.19E-01

1.08E-01

OK

09

U-235

TRG

PZ-107-SS DIS

pCi/I

1.64E-01

1.70E-01

2.14E-01

OK

10

U-235

TRG

PZ-106-KS TOT

pCi/I

3.06E-01

1.59E-01

1.04E-01

OK

11

U-235

TRG

PZ-106-KS DIS

pCi/I

2.19E-01

1.62E-01

1.37E-01

OK

DUP 08 TOT

pCi/I

3.06E-01

2.45E-01

2.20E-01

OK

DUP 08 DIS

pCi/I

2.39E-01

1.79E-01

1.79E-01

OK

----

-~-

12

U-235

TRG

U-235

TRG

-----~-

13
~

----------

--

------------

Q.
Q.

---------

::I

en

- ---

c:

------------------~~-

QI

t:G>

:::::
u

QI

Cl

n:s
n:s

-----------

-~

----

--- - - - - -

c:

:!:

- - - --

Cl

c:
;::

-----

QI

QI

.:Cl

---

-------

-----------

,_____ - - - - - - - - - - - - -

c:

w
il:t-!11
~J

en

Blank
Flag

-- -------

02
~

Work Order: 13-07154-UUIS0-1

Desc

Nuclide

Fraction

Printed: 8/14/2013 2:45 PM

Page 1 of 3

Preliminary Data Report & Analytical Calculations

Eberline Services
Oak Ridge Laboratory

OK

a:

Lab
Fraction

C(

Sample
Date

Sample
Aliquot

Grav
%Rec

Radiometric
% Rec

Mean
%Rec

SAF

Sep to
Date!Tlme

Sep t1
DatefTime

01

02

04

05

MBL

0.00

U-235

ji DUP
-----------1

0.00

0.00

i TRG

0.00

0.00

U-235

-----------+-

0.00

I--

0.00
0.00
TRG
--------------+-------l-- - - - - - - - - - + - - - - + - - - - - - l - - - - - - 1 - - - - - - - 1 - - - - 1 - - - - - - - - - + - - - - - - - - - I
U-235

1--------- -

07

----------------------

-
06

U-235

--------------+------+--------1----+------1--------j~-----+-----+---------+----------.

03

en
!I ::>::>
0

l.> .

Sample
Desc

0.00
1.00E+OOI
104.75
0.00
07/24/13 00:00
U-235
LCS
!------+-------------"----+-- - - - - - - - - - - + - - - - - - 1 - - - - - - - - 1 - - - - - - - - - + - - - - - -

Work Order: 13-07154-UUIS0-1

Nuclide

1-----

Printed: 8/14/2013 2:45 PM

Page 2 of 3

Preliminary Data Report & Analytical Calculations

Eberline Services
Oak Ridge Laboratory

U-235
-------------------

U-235

08

U-235

09

U-235

----1-~35

0.00

TRG

I
-t--. . ---

! TRG

0.00

0.00

0.00

0.00

0.00

0.00

-+------+
DO

-t TR~+-

l_~~~-+---------1-----1------1-------l-------+-----+----------+-----------t

U-2~ TRG

_u-_2_35_
U-235

0.001

0.00

0.00

0.00

0.00

0.00

0.00

0.00

0.00

~~l-------+----+-----+-----+------+-----+---------+--------1
TRG

-~----~----!

--- ----

[- -==-----=--

---- - + - - - - - - - - - - - - - _ _ _ , - - - - - + - - - - - - - + - - - - - - - t - - - - - - f - - - - - t - - - - - - - - - - - t - - - - - - - - - - - 1

--+

+~=-~---+--~I--

J_--------1----+-----+-------+--------1

Lab
Fraction

Nuclide

01

a::

Work Order: 13-07154-UUIS0-1

Counting
Date/Time

Sample
Desc

U-235

~---

LCS
--

---

.!!,!

;a~
c:

q:

Halflife
(days)

en

:::>

:::>

A_Spec

Alpha_013

170.02 6.95 E+01

3.00 E-03

18.7

A_Spec

Alpha_014

170 3.66 E+OO

2.00 E-03

18.5

A_Spec

Alpha_015

170.02 1.10 E+01

0.00 E+OO

14.8

'-----

U-235

MBL

08/14/13 09:26

03

U-235

DUP

08/14/13 09:26

04

U-235

TRG

08/14/13 09:27

A_Spec

Alpha_019

170.02 9.00 E+OO

0.00 E+OO

16.6

05

U-235

TRG

08/14/13 09:27

A_Spec

Alpha_022

170.02 3.47 E+OO

9.00 E-03

15.3

06

U-235

TRG

08/14/13 09:27

A_Spec

Alpha_023

170.02 3.43 E+01

4.00 E-03

17.1

07

U-235

TRG

08/14/13 09:27

A_Spec

Alpha_024

170.02 5.30 E+01

6.00 E-03

17.1

08

U-235

DO

08/14/13 09:27

A_Spec

Alpha_025

170.02 1.00 E+01

0.00 E+OO

17.4

09

U-235

TRG

08/14/13 09:27

A_Spec

Alpha_027

170.02 4.32 E+OO

4.00 E-03

17.3

10

U-235

TRG

08/14/13 09:27

A_Spec

Alpha_029

170 1.55 E+01

3.00 E-03

19.5

11

U-235

TRG

08/14/13 09:27

A_Spec

Alpha_031

170 7.66 E+OO

2.00 E-03

14.2

12

U-235

TRG

08/14/13 09:28

A_Spec

Alpha_033

170 6.66 E+OO

2.00 E-03

18.5

U-235

TRG

08/14/13 09:28

A_Spec

Alpha_034

170 8.00 E+OO

0.00 E+OO

18.6

13

------------t

"'...

c:

----

--

Q.
Q.
:I

----------------~-------

----

GI

I
-+

- - -------

GI
Cl

ca
c:
ca

___==

--

--

:E
en
c:

;:

--

GI
GI

.5

Cl

c:

i----------

--

~--------t--

. 1-------
I
I

Ci~

(}QI

Eff

02

U)

Bkg
CPM

Counts

08/14/13 09:26

Time

.E

c;;a~

Count

Carrier

~I

Detect

-----

{:
0
u

Printed: 8/14/2013 2:45 PM

Page 3 of 3

Preliminary Data Report & Analytical Calculations

Eberline Services
Oak Ridge Laboratory

--

Count Room Report


Client: Engineering Management Su

13-07154-UUIS0-1 (pCi/I) in WA
Tracer ID: U-10a

Printed: 8/1412013 5:58 AM


Page 1of1

<
/l \

Internal
Fraction

Sample
Desc

01

LCS

"'"

02

MBL

BLANK

\(

03

DUP

PZ-107-SS TOT

~
\)

I
!

Client
ID

Sample
Date

LCS

07/24/13 00:00

Tracer
Aliquot (g)

Sample
Aliquot

Tracer
ACT(dpm)

Radiometric
Tracer (pCi)

TRG

04

PZ-200-SS TOT

0.6129

11.6696

0.00

07/24/13OO:Orr1.0000

0.6069

11.5554 I

0.00 i

07/19/1312:10

0.6064

11.5459

o.oo
o.oo
o.oo

1.0000

07/19/13 10:19

0.6051

1.0000

11.5211

- --

05

TRG

PZ-200-SS DIS

07/19/13 10:19

06

TRG

PZ-102-SS TOT

07/19/1310:30

--iI

0.6041

11.5021

1.0000

0.6021

11.4640

0.00

TRG

PZ-102-SS DIS

07/19/1310:30

1.0000

0.6025

11.4716

0.00

08

DO

PZ-107-SS TOT

07/19/13 12:10

1.0000

0.6025

11.4716

0.00

09

TRG

PZ-107-SS DIS

07/19/13 12:10

1.0000

0.6058

11.5344

0.00

TRG II
--

PZ-106-KS TOT

07/19/1313:09

1.0000

0.6002

11.4278

0.00

11

TRG

PZ-106-KS DIS

07/19/1313:09

1.0000

0.6056

11.5306

0.00

12

TRG

DUP 08 TOT

07/19/13 00:00

1.0000

0.6049

11.5173

0.00

TRG

DUP 08 DIS

07/19/13 00:00

1.0000

0.6040

11.5002

0.00

1--

-'
")

L "'

"'

13

I
I

10
'?J

I
I

I
-

~~
G.,
(,i(;JI
~~lt:lt

SAF
2*

1.0000

SAF
1*

07

1.0000

----

1'\

Radiometric
%Rec

Eberline Services
Oak Ridge Laboratory

LCS & Matrix Spikes

.
Isotope

Sol#

U-234

U-8a

U-238

Activity
dpmlg

35.240

U-8a

Page 1of1
Printed: 8/8/2013 7:47 AM

Spike and Tracer Worksheet

'
Solution
Date

Date

Technician

UUISO

8/8/2013 7:46

JWOLFE

';; :.< .. ,

LCS

MS

LCSD.

NISO

Approx
Addition

Volume
Used(g)

Volume
Used(g)

Volume
Used(g)

Volume
Used(g)

8/8/2013

"

0.5146

0.500'

8/8/2013

34.350

Analysis Code

0.500

LCS
Known
pCi

' :.u.

0.5146
,,,

'

Witness Initials

MS

Error
Estimate

8.17

0.294

Added
pCi

0.00

LCSD

Error
Estimate

0.000

Known
pCi

MSD

0.00

0000
---- -

7.96

'

0.287

0.00

0.000

Added
pCi

Error
Estimate

0.00

0.000

Error
Estimate

0.00

0.000

0.00

0.000

',.

::,,
'

'

fraction

Trac,rs . i:,:\;i

:.:::

Isotope

Activity
dpmlg

Sol#

01

U-232

U-10a

19.040

8/8/2013

02

U-232

U-10a

19.040

8/8/2013

03

U-232

U-10a

19.040

8/8/2013

04

U-232

05
06

1---

'

;:

Solution
Date

Volume
Used(g)
1

.,,

I
i

Approx
Addition

0.6129

0.6300

0.6069

0.6300

0.6064

0.6300

',

Balance Printer Tap~s:

,.

Tracer

LCS

::1 ''"
<,. :'-,\,

------

U-10a

19.040

8/8/2013

0.6051

0.6300

U-232

U-10a

19.040

8/8/2013

0.6041

0.6300

U-232

U-10a

19.040

8/8/2013'

0-6021

0.6300
-----~

07

U-232

U-10a

19.040

8/8/2013 ' '

0.6025

0.6300

08

U-232

U-10a

19.040

8/8/2013

0.6025

0.6300

09

U-232

U-10a

19.040

8/8/2013

0:6058 '

0.6300

10

U-232

U-10a

19.040

8/8/2013

0-6002

0.6300

11

U-232

U-10a

19.040

8/8/2013 '

0.6056

0.6300

12

U-232

U-10a

19.040

8/8/2013

0,6049

0.6300

13

U-232

U-10a

19.040

8/8/2013

0.6040

0.6300

---

-
,.

~,!.(~
~.~.

t!~
~

Version 2.0 08/99

,-1, . '

Matrix Spike

Eberline Analytical
Oak Ridge Laboratory

Lab
Fraction

Engineering Management Support, Inc.

Type
LCS
MBL
DUP
TRG
TRG
TRG
TRG
DO
TRG
TRG
TRG
TRG
TRG

Anaiysis Code

Rpt Units

Lab Deadline

Technician

UUISO

liters

8/13/2013

JWOLFE

Dilution Data

Muffle Data

Sample

Client ID
LCS
BLANK
PZ-107-SS TOT
PZ-200-SS TOT
PZ-200-SS DIS
PZ-102-SS TOT
PZ-102-SS DIS
PZ-107-SS TOT
PZ-107-SS DIS
PZ-106-KS TOT
PZ-106-KS DIS
DUP 08 TOT
DUP 08 DIS

01
02
03
04
05
06
07
08
09
10
11
12
13

Ratio
Post/Pre

..
NoofQils

."

"

Pi!)"a!:tor
.;,;', ,/'

.. ,: ::I:+,

'

I: ;:;

~;

1;

..

...

..

J~

:"

.
I

;. '
.

::

'"

.,

... . .
"

'"' ..:

;.: ....
I

..

""'ltoii!ll

'"'"

Comments

Technician:

Aliquot

NetEqqiv

Net Equiv.

H-3 Solids Only


Water Added
(ml)

H3 Dist
Aliq

::
:.

.:; ...

./

::,::

Aliquot

'

Ratio

: ioooo:e+oo

:.

MS Aliquot Data

1.0000E+OO
t.ooooe+oo
1.0000E+OO . 1 :~OOE+OO
1.0000E+OO I 1,oooqezoo
1.0000E+OO 1 1.~00EtOO
1.0000E+OO I t(JOOOE+oo
1.0000E+OO
.1.00QOE+OO
1.0000E+OO . 1.000QE+OO
1.0000E+OO
1,0QOOE+OO
1.0000E+OO
1:J;i009e+oo
1.0000E+OO
1'.{jOOClE+oo
1.0000E+OO
1:1ClOOOJ::+OCl
1.0000E+OO
1.0000E+OO
1.0000E+OO

' ' r-.:;;


.
:
.
. ,:. .

Aliquot Data

<:

... [.' ~"

--

Printed: 8/8/2013 7:47 AM


Page 1 of 1

Aliquot Worksheet

1:: .:. "

..

;;.

:
/

' '

'

JL

Date

Su~!~

.A

--=Mpex- Al pha

TM

Sample Description:

Spectrum File:

Batch Identification:

Sample Identification:

Sample Geometry:

Procedure Description:

SPIKE
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000661
1307154A-UU
01
Shelf 2
U iso

Detector Name:

Alpha_013
Chamber Serial Number:

Detector Serial Number:


13
Env. Background:

System Bkgd 64769


Reagent Blank:

<not performed>
Sample Size:

Sample Date/Time:

Acquisition Date/Time:

Acquisition Live Time:

Acquisition Real Time:

1.000E+OOO +/- O.OOOE+OOO liter


8/14/2013
7:26:18 AM
9:26:34 AM
8/14/2013
170.0 minutes
170.0 minutes

Tracer Certificate:

Tracer Quantity:

Effective Efficiency:

Counting Efficiency:

Chem. Recovery Factor:

U232 UU-lOA
0.613 mL

0.1958 +/- 0.0109

0.1869 +/- 0.0035 on 12/15/2012 11:26:45 AM


1.0475 +/- 0.0617

Control Certificate Name:


NatU U-8A
Chem. Recov. of Control:
U-238
Peak Match Tolerance:

0.150 MeV

PEAK
Energy
(MeV)

Nuclide
U-232
U-234
U-235
U-238

5.273
4.725
4.406
4.145
T

Net
Pk Area
386.15
586.66
69.49
661.49

1.093428 +/-

AREA

0.081378

REPORT

Pk Area
Error %

Ambient
Backgnd

Reagent
Backgnd

FWHM
(keV)

9.99
8.09
23.61
7.62

0.85
0.34
0.51
0.51

O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

27.9
31. 9
3.3
25.4

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS


Nuclide

Id
Conf.

Energy
(keV)

U-232
U-234
U-235
U-238

0.994
0.991
0.997
0.989

5302.50*
4761.50*
4385.50*
4184.40*

Activity
(pCi/liter )
5.24E+OOO
7.96E+OOO
l.16E+OOO
8.93E+OOO

+/+/+/+/-

5.74E-001
1.08E+OOO
3.03E-001
1.19E+OOO

-PG

g/r4-/f3

MDA
(pCi/liter
8.12E-002
6.48E-002
8.78E-002
7.09E-002

+/+/+/+/-

8.90E-003
7.lOE-003
9.62E-003
7.76E-003

0000066136.CNF

Live Time :10201.000 sec


Real Time :10201.000 sec
start:
1:3547.S(kev)

Stop : 1024:6438.l(kev)

Acq. Start :wed Aug 14 09:26:34 2013

60
55

50

45

40

35

VI

c:
=s

8 30

25

,I

ii

20

""
,..... I :~

,-~

~;i!:!

liy.1
''I
I

15
10

4000

4500

mi
i-'""
\';?.~

t..'11

ROI Type: 1

5000

Energy(kev)

5500

6000
ROI Type: 3

Channel Data Report

8/14/2013

Page

12:34:35 PM

*******************************************************
s p E C T R A L DAT A R E P 0 R T *****
*****
*******************************************************
Sample Title:

01

Elapsed Live time:


Elapsed Real Time:

10201
10201

Channell------l-------1-------1-------1-------l-------l-------l-------I
1:
9:
17:
25:
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10201
0
1
0
0
1
0
0
1
0
1
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2
3
0
4
1
1
2
0
3
2
7
6
11
9
11
17
1
1
0
0
0
1
1
1
1
0
1
1
0
0
0
2

10201
0
1
0
0
0
1
1
0
0
0
2
2
1
2
2
0
1
0
1
5
4
5
3
7
8
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19
11
0
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0
0
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3
0
0
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3
2
2
1
1
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7
4
8
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19
6
1
1
0
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1
3
1
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0
1
1
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0
3

0
0
0
0
1
1
1
1
1
1
2
4
0
0
1
1
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2
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1
7
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5
15
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20
19
5
1
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3
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0
2
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1
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2
1
2
2

0
0
0
2
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1
0
1
3
0
0
1
3
0
1
1
2
3
1
0
2
7
3
5
9
8
12
17
21
3
1
0
1
0
0
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0
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1
2
2
2
2
2

0
0
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1
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1
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2
5
1
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2
1
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2
4
9
17
15
22
4
2
0
2
1
0
4
2
4
1
3
1
3
2
2
1
1

0
0
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1
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1
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12
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18
1
1
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0
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1
0
2
2

0
0
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0
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2
3
1
5
2
4
2
1
5
5
5
10
14
20
2
0
0
0
1
1
0
1
1
2
1
1
0
0
2
3
1
~18.l

Channel Data Report


369:

8/14/2013
4

Sample Title:

12:34:35
3

Page

PM
2

01

Channell------l-------l-------1-------1-------1-------l-------l-------I
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1
6
4
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7
13
19
18
3
1
0
0
0
1
1
1
0
0
0
1
1
0
2
0
1
1
1
4
3
12
9
12
7
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

1
2
4
8
7
7
12
19
1
1
0
0
0
1
0
0
1
1
1
0
1
0
1
1
1
1
4
6
6
9
7
10
1
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

5
1
5
4
10
11
11
18
0
0
1
0
1
1
1
0
2
1
0
0
3
1
2
0
3
2
0
5
6
9
11
12
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
4
1
7
12
13
16
16
0
0
2
0
0
2
0
0
0
0
1
1
1
1
5
2
0
2
1
4
10
4
9
14
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

2
3
4
7
13
13
17
15
0
1
0
0
2
1
0
0
0
0
2
1
1
2
0
2
4
4
2
1
7
7
7
13
2
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
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0
0

4
3
3
5
10
6
24
19
0
0
2
3
0
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3
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2
2
3
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0
3
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3
6
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11
0
0
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0
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0
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0

2
5
7
8
9
14
18
5
0
0
1
0
0
0
0
0
0
0
1
1
1
0
2
1
3
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4
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4
7
13
10
0
0
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1
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3
8
6
12
10
16
18
7
1
0
1
1
0
1
0
0
1
0
2
0
0
1
2
2
3
0
4
1
6
13
17
6
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

e18s

Channel Data Report


801:

8/14/2013
0

Sample Title:

Page

12:34:35 PM
0

01

Channell------l-------1-------1-------1-------l-------l-------l-------I
809:
817:
825:
833:
841:
849:
857:
865:
873:
881:
889:
897:
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913:
921:
929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:

0
0
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0

0
0
0
0
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0
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0
0
0
0
0
0
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0
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0
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0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
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0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

~~Apex-Alpha'"

Sample Description:

Spectrum File:

Batch Identification:

Sample Identification:

Sample Geometry:

Procedure Description:

BLANK
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000661
1307154A-UU
02
Shelf 2
U iso

Detector Name:

Alpha_014
Chamber Serial Number:

Detector Serial Number:


14
Env. Background:

System Bkgd 64770


Reagent Blank:

<not performed>
Sample Size:

Sample Date/Time:

Acquisition Date/Time:

Acquisition Live Time:

Acquisition Real Time:

1.000E+OOO +/- O.OOOE+OOO liter

8/14/2013
7:26:18 AM

8/14/2013
9:26:35 AM

170.0 minutes
170.0 minutes

Tracer Certificate:

Tracer Quantity:

Effective Efficiency:

Counting Efficiency:

Chem. Recovery Factor:

U232 UU-lOA
0.607 mL
0.2142 +/- 0.0116
0.1846 +/- 0.0034 on 12/15/2012 11:26:44 AM
1.1605 +/- 0.0665

Peak Match Tolerance:

0.150 MeV

PEAK
Energy
(MeV)

Nuclide

Net
Pk Area

AREA

REPORT

Pk Area
Error %

Ambient
Backgnd

Reagent
Backgnd

FWHM
(keV)

-------------------------------------------------------------------------------U-232
U-234
U-235
U-238

5.279
4.735
4.348
4.124

418.28
25.15
3.66
5.15

9.62
39.85
107.87
94.34

2.72
0.85
0.34
0.85

O.OOE+OOO
0.00E+OOO
O.OOE+OOO
O.OOE+OOO

11.6
2.9
2.9
2.9

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS


Nuclide

Id
Conf.

Energy
(keV)

Activity
(pCi/liter )

MDA

(pCi/liter

-------------------------------------------------------------------------------U-232
U-234
U-235
U-238

0.996
0.995
0.990
0.974

5302.50*
4761.50*
4385.50*
4184.40*

5.18E+OOO
3.12E-001
5.60E-002
6.36E-002

+/+/+/+/-

5.51E-001
1.29E-001
6.07E-002
6.03E-002

A-G
g-\14-/13

1. 06E- 001
7.42E-002
7.31E-002
7.39E-002

+/+/+/+/-

1.13E- 002
7.89E-003
7.77E-003
7.85E-003

0000066137.CNF

Live Time :10200.000 sec

Real Time :10200.000 sec

Start:
1: 3507. 9(kev)

Stop : 1024: 6512. 2(kev)

Acq. Start :wed Aug 14 09:26:35 2013

60
55

50

45

40

35

V'l
......
c:

::J

B 30

25

20

15

10

Ml\ I

1!,

4000

4500

~~

......
~it'
(Ir,)

ROI Type: 1

5000

Energy (kev)

5500

6000
ROI Type: 3

6500

Channel Data Report

8/14/2013

Page

12:34:4! l9M

*******************************************************
R E P 0 R T
S P E C T R A L
DAT A
*****
*****
*******************************************************
Sample Title:

02

Elapsed Live time:


Elapsed Real Time:

10200
10200

Channell------l-------l-------1-------1-------1-------l-------l-------I
1:
9:
17:
25:
33:
41:
49:
57:
65:
73:
81:
89:
97:
105:
113:
121:
129:
137:
145:
153:
161:
169:
177:
185:
193:
201:
209:
217:
225:
233:
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257:
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289:
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305:
313:
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1!11l5!9

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1
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1
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0
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489:
1
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1
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0
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0
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4
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3
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'&11ti

Channel Data Report


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1
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!!1111

~.JtApex-Alpha

Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:

PZ-107-SS TOT-DUP
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000661
1307154A-UU
03
Shelf 2
u iso

Detector Name:
Chamber Serial Number:
Detector Serial Number:
Env. Background:
Reagent Blank:

Alpha_015
15
System Bkgd 64771
<not performed>

Sample Size:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:

1.000E+OOO +/
O.OOOE+OOO liter
7/19/2013
7:26:18 AM
8/14/2013
9:26:36 AM
170.0 minutes
170.0 minutes

Tracer Certificate:
Tracer Quantity:
Effective Efficiency:
Counting Efficiency:
Chem. Recovery Factor:

U232 UU-lOA
0.606 mL
0.1407 +/
0.0091
0.1477 +/
0.0027 on 7/20/2013
0.9527 +/
0.0639

Peak Match Tolerance:

0.150 MeV

PEAK
Energy
(MeV)

Nuclide
U-232
U-234
U-235
U-238

5.283
4.739
4.396
4.152
T

Net
Pk Area

AREA

REPORT

Pk Area
Error %

274.66
69.32
11. 00
76.83

6:27:27 PM

Ambient
Backgnd

11.84
23.68
61. 72
22.39

0.34
0.68
0.00
0.17

Reagent
Backgnd

FWHM
(keV)

O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

11.1
4.0
3.0
8.2

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS


Nuclide

Id
Conf.

Energy
(keV)

U-232
U-234
U-235
U-238

0.997
0.996
0.999
0.993

5302.50*
4761.50*
4385.50*
4184.40*

Activity
(pCi/liter )
5.18E+OOO
l.31E+OOO
2.56E-001
1. 44E+OOO

+/
+/
+/
+/

6.57E-001
3.51E-001
1. 61E-001
3.71E-001

MDA
(pCi/liter
9.02E-002
1.06E-001
1. 40E-001
7.84E-002

+/
+/
+/
+/

1.14E-002
1.35E-002
1. 77E-002
9.93E-003

A4

'i Irt.Pl' 3

m112

0000066138.CNF

Live Time 10201.000 sec


Real Time 10201.000 sec
Start:
1 3490.S(kev)
Stop : 1024 6558.S(kev)
Acq. Start wed Aug 14 09: 26: 36 2013

60
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50

45

40

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I
6500

Channel Data Report

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Page

12:34:48 I'M

*******************************************************
s p E CTR AL DAT A R E P 0 R T *****
*****
*******************************************************
Sample Title:

03

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Elapsed Real Time:

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mi is

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Sample Title:

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12:34:48 'PM
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03

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0
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0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

.A

--===~=MP8X-

Al pha

TM

Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:

PZ-200-SS TOT
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000661
1307154A-UU
04
Shelf 2
U iso

Detector Name:
Chamber Serial Number:
Detector Serial Number:
Env. Background:
Reagent Blank:

Alpha_Ol9
19
System Bkgd 64773
<not performed>

Sample Size:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:

l.OOOE+OOO +/ O.OOOE+OOO liter


7/19/2013
7:26:18 AM
8/14/2013
9:27:34 AM
170.0 minutes
170.0 minutes

Tracer Certificate:
Tracer Quantity:
Effective Efficiency:
Counting Efficiency:
Chem. Recovery Factor:

U232 UU-lOA
0.605 mL
0.1734 +/ 0.0103
0.1659 +/ 0.0029 on 2/17/2013
1.0450 +/ 0.0645

Peak Match Tolerance:

0.150 MeV

PEAK
Energy
{MeV)

Nuclide
U-232
U-234
U-235
U-238

5.248
4.723
4.415
4 .143
T

Net
Pk Area
337.66
63.00
9.00
52.49

AREA

10:45:23 AM

REPORT

Pk Area
Error %

Ambient
Backgnd

Reagent
Backgnd

FWHM
{keV)

10.67
24.89
68.87
27.21

0.34
0.00
0.00
0.51

O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

37.7
7.1
3.3
4.9

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS


Nuclide

Id
Conf.

Energy
{keV)

U-232
U-234
U-235
U-238

0.979
0.990
0.994
0.988

5302.50*
4761.50*
4385.50*
4184.40*

Activity
{pCi/liter )
5.17E+OOO
9.65E-001
l.70E-001
8.00E-001

+/
+/
+/
+/

5.99E-001
2.65E-001
l.19E-001
2.37E-001

MDA
{pCi/liter
7.33E-002
9.18E-002
l.13E-001
8.00E-002

+/
+/
+/
+/

8.49E-003
1. 06E-002
1.31E-002
9.27E-003

A<1

g-(14-{ 13

ti117

0000066139.CNF

Live Time :10201.000 sec


Rea1 Ti me :10201. 000 sec
Start:
1:3279.3(kev)
Stop : 1024:6687 .O(keV)
Acq. Start :wed Aug 14 09:27:34 2013

60
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Vl

......
s::::
::J

8 30

25

20

15

10

3500

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....
......
00
~

ROI Type: 1

4500

5000
Energy(kev)

5500

6000
ROI Type: 3

6500

Channel Data Report

8/14/2013

Page

12:34:55 PM

*******************************************************
s p E C T R A L DAT A R E P 0 R T *****
*****
*******************************************************
Sample Title:

04

Elapsed Live time:


Elapsed Real Time:

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1119

Channel Data Report


369:

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2

Sample Title:

Page

12:34:55 PM
0

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0
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4
1
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1
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6
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0
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0
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0
0
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1
1
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1
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1
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1
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0
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4
1
3
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13
3
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0
1
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1
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1
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0
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0
0
1
1
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1
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7
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0

0
0
0
0
1
1
0
1
2
1
0
0
0
1
1
0
0
0
1
1
1
2
1
4
5
2
8
11
16
0
0
0
0
0
0
0
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0
0
0
0
0
0
0
0
0
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0
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0
0

1
0
0
2
0
1
1
2
1
0
0
0
0
0
0
0
1
1
0
0
1
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4
5
4
3
10
10
11
0
0
0
0
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0
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1
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4
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12
0
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0
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'.m12m

Channel Data Report


801:

8/14/2013
0

Sample Title:

Page

12:34:55 PM
0

04

Channell------l-------l-------l-------l-------1-------1-------1-------I
809:
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897:
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913:
921:
929:
937:
94 5:
953:
961:
969:
977:
985:
993:
1001:
1009:
101 7:

0
0
0
0
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0
0
0
0
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0
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0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
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0
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0

0
0
0
0
0
0
0
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0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
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0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

1121

~~Apex-Alpha'"

Sample Description:
Spectrum File:
Batch Identification:

Sample Identification:

Sample Geometry:

Procedure Description:

PZ-200-SS DIS
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000661
1307154A-UU
05
Shelf 2
U iso

Detector Name:

Alpha_022
Chamber Serial Number:

Detector Serial Number:


22
Env. Background:

System Bkgd 64774


Reagent Blank:

<not performed>
Sample Size:

Sample Date/Time:

Acquisition Date/Time:

Acquisition Live Time:

Acquisition Real Time:

l.OOOE+OOO +/- O.OOOE+OOO liter


7/19/2013
7:26:18 AM
8/14/2013
9:27:34 AM
170.0 minutes
170.0 minutes

Tracer Certificate:

Tracer Quantity:

Effective Efficiency:

Counting Efficiency:

Chem. Recovery Factor:

U232 UU-lOA
0.604 mL

0.1847 +/0.0107

0.1531 +/0.0029 on 12/15/2012


1.2062 +/0.0733

Peak Match Tolerance:

0.150 MeV

PEAK
Energy
(MeV)

Nuclide
U-232
U-234
U-235
U-238

5.290
4. 716
4.382
4.154
T

Net
Pk Area

AREA

REPORT

Pk Area
Error %

359.13
33.81
3.47
28.83

1:57:26 PM

10.37
34.40
129.55
36.63

Ambient
Backgnd
1. 87
1.19
1. 53
0.17

Reagent
Backgnd

FWHM
(keV)

O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

31. 2
4.7
3.1
3.1

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS

Nuclide

Id
Conf.

Energy
(keV)

U-232
U-234
U-235
U-238

0.999
0.985
1. 000
0.994

5302.50*
4761. 50*
4385.50*
4184.40*

Activity
(pCi/liter )
5.16E+OOO
4.86E-001
6.15E-002
4.13E-001

+/
+/
+/
+/

5.84E-001
1. 76E-001
8.00E-002
l.58E-001

P6.

&llff 13

MDA
(pCi/liter
l.09E-001
9.47E-002
1. 26E-001
5.97E-002

+/+/+/+/-

1.23E-002
l.07E-002
1.43E-002
6.76E-003

0000066140.CNF

Live Time :10201.000 sec


Rea1 Ti me :10201. 000 sec
start:
1: 3421.S (kev)

stop : 1024:6608.S(kev)

Acq. start :wed Aug 14 09: 27: 34 2013

60

55

50

45

40

35

V)

......
c:
::::s

8 30

25

20

~
~
~

15

'

=>

10

/;1 ~-

0
3500

4000

4500

~I

n.-"

W'J
(,<,Ji

ROI Type: 1

5000

Energy(kev)

5500

6000
ROI Type: 3

6500

Channel Data Report

8/14/2013

Page

12: 35: 14 PM

*******************************************************
s p E C T R A L DAT A R E P 0 R T *****
*****
*******************************************************
Sample Title:

05

Elapsed Live time:


Elapsed Real Time:

10201
10201

Channell------l-------1-------1-------1-------l-------l-------l-------I
1:
9:
17:
25:
33:
41:
49:
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145:
153:
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169:
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249:
257:
265:
273:
281:
289:
297:
305:
313:
321:
329:
337:
345:
353:
361:

10201
0
0
0
0
0
0
0
0
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0
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0
0
0
0
0
0
0
0
0
0
1
0
1
0
0
0
3
1
2
0
1
0
0
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0
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10201
0
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1
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1
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1
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0
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0
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1
0
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0
1
0
0
0
0
0

0
0
0
0
0
0
0
0
0
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0
1
0
0
1
0
0
0
0
0
0
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0
0
0
1
0
0
1
1
1
0
0
0
0
0
0
0
0
0
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0

0
0
0
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0
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1
0
0
0
0
0
0
1
0
0
0
1
0
0
0
0
0
0
0
0
1
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0

0
0
0
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1
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0
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1

B124

Channel Data Report


369:

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0

Sample Title:

Page

12:35:14 PM
0

05

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793:

0
0
2
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1
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1
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1
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1
4
14
12
14
1
0
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0
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0
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0
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0
0
0
0
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0
0
1
0
0
0
0

0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
1
3
0
3
3
0
2
3
1
4
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9
0
0
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0
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0
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1
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0

8125

Channel Data Report


801:

8/14/2013
0

Sample Title:

12:35:14
0

,..
0

Page
0

05

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0
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0
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0
0
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0
0
0

ffl126

~~Apex-Alpha'"

Sample Description:
Spectrum File:
Batch Identification:

Sample Identification:

Sample Geometry:

Procedure Description:

PZ-102-SS TOT
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000661
13 07154A-UU
06
Shelf 2
u iso

Detector Name:

Alpha_023
Chamber Serial Number:

Detector Serial Number:


23
Env. Background:

System Bkgd 64775


Reagent Blank:

<not performed>
Sample Size:

Sample Date/Time:

Acquisition Date/Time:

Acquisition Live Time:

Acquisition Real Time:

l.OOOE+OOO +/- O.OOOE+OOO liter


7/19/2013
7:26:18 AM
8/14/2013
9:27:35 AM
170.0 minutes
170.0 minutes

Tracer Certificate:

Tracer Quantity:

Effective Efficiency:

Counting Efficiency:

Chem. Recovery Factor:

U232 UU-lOA
0.602 mL

0.1759 +/- 0.0104

0.1710 +/- 0.0030 on 7/20/2013


1. 0286 +/- 0.0632

Peak Match Tolerance:

0.150 MeV

PEAK
Energy
(MeV)

Nuclide
U-232
U-234
U-235
U-238

5.283
4.736
4.393
4.162
T

Net
Pk Area
340.83
309.49
34.32
294. 98

AREA

6:18:25 PM

REPORT
FWHM
(keV)

Pk Area
Error %

Ambient
Backgnd

Reagent
Backgnd

10.62
11.15
33.84
11.44

0.17
0.51
0.68
1. 02

O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

10.8
4.5
4.7
20.9

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS

Nuclide

Id
Conf.

Energy
(keV)

U-232
U-234
U-235
U-238

0.997
0.995
1. 000
0.996

5302.50*
4761.50*
4385.50*
4184.40*

Activity
(pCi/liter )
5.15E+OOO
4.67E+OOO
6.39E-001
4.43E+OOO

+/+/+/+/-

5.94E-001
7.50E-001
2.28E-001
7.20E-001

z; I1'-Pf 13

MDA
(pCi/liter
6.30E-002
7.92E-002
l.05E-001
9.47E-002

+/+/+/+/-

7.27E-003
9.14E-003
1.21E-002
1. 09E-002

0000066141.CNF

Live Time :10201.000 sec


Real Time :10201.000 sec
start:
1:3403 .O(kev)
stop : 1024: 6588 .3 (kev)
Acq. Start :wed Aug 14 09: 27: 35 2013

60
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Vl
.j..J

s:::
:::s

8 30

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5
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4500

4000

t~

5000
Energy(kev)

5500

6000

noo..J111

!".)
o:~

ROI Type: 1

ROI Type: 3

6500

Channel Data Report

8/14/2013

Page

12:35:33 PM

*******************************************************
S P E C T R A L
R E P 0 R T
DAT A
*****
*****
*******************************************************
Sample Title:

06

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Elapsed Real Time:

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N129

Channel Data Report


369:

8/14/2013
0

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12:35:33
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Page

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2
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10
8
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0
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13
3
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0
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0
2
1
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2
5
6
8
10
1
0
0
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1
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0
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6
7
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11
6
1
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0
2
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7
10
3
0
1
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2
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0
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7
11
14
1
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1
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0
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11
9
13
14
2
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0
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1
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2
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9
5
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0
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1
1
3
1
1
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4
14
5
0
0
0
0
0
0
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2
1
1
2
1
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4
10
9
16
2
0
0
1
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1
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4
2
3
6
8
6
7
0
1
1
0
0
0
1
1
0
1
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0
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2
1
5
4
4
3
6
5
0
0
0
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0
0
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0
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0

2
2
2
2
1
4
7
7
3
0
0
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1
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7
10
4
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813S

Channel Data Report


801:

8/14/2013
0

Sample Title:

Page

12:35:33 ttM
0

06

Channell------l-------l-------l-------1-------1-------1-------l-------I
809:
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913:
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929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:

0
0
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0
0
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0
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0
0
0
2
0
0
0
0
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0
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0
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0

0
0
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0
0
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0
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0
0
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0
0
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0
0
0
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0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0

fi:131

~Apex-Alpha'"

Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:

PZ-102-SS DIS
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000661
1307154A-UU
07
Shelf 2
U iso

Detector Name:
Chamber Serial Number:
Detector Serial Number:
Env. Background:
Reagent Blank:

Alpha_024
24
System Bkgd 64776
<not performed>

Sample Size:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:

1.000E+OOO +/ O.OOOE+OOO liter


7/19/2013
7:26:18 AM
8/14/2013
9:27:36 AM
170.0 minutes
170.0 minutes

Tracer Certificate:
Tracer Quantity:
Effective Efficiency:
Counting Efficiency:
Chem. Recovery Factor:

U232 UU-lOA
0.603 mL
0.1778 +/ 0.0104
0.1710 +/ 0.0032 on 12/15/2012
1.0398 +/ 0.0640

Peak Match Tolerance:

0.150 MeV

PEAK
Energy
(MeV)

Nuclide
U-232
U-234
U-235
U-238

5.269
4. 719
4.408
4.136
T

Net
Pk Area

AREA

REPORT

Pk Area
Error %

344.81
391.32
52.98
259.32

2:02:15 PM

10.58
9.92
27.23
12.19

Ambient
Backgnd
1.19
0.68
1. 02
0.68

Reagent
Backgnd

FWHM
(keV)

O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

31. 9
6.9
3.1
5.1

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS

Nuclide

Id
Conf.

Energy
(keV)

U-232
U-234
U-235
U-238

0.992
0.987
0.996
0.983

5302.50*
4761.50*
4385.50*
4184.40*

Activity
(pCi/liter )
5.15E+OOO
5.84E+OOO
9.76E-001
3.85E+OOO

+/
+/
+/
+/

5.92E-001
8.87E-001
2.88E-001
6.46E-001

MDA
(pCi/liter
9.84E-002
8.42E-002
1.16E- 001
8.38E-002

+/
+/
+/
+/

1.13E-002
9.68E-003
1.33E-002
9.64E-003

I\~

g/1'-fft)

nl132

0000066142.CNF

Live Time :10201.000 sec


Real Time :10201.000 sec
start:
1:3411.6(kev)

stop : 1024: 6597. O(kev)

Acq. start :wed Aug 14 09:27:36 2013

60

55

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35

VI

.f-J

c:

:::s

8 30

25

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10

3500

4000

4500

m
f.;A.1
t.,,~

(,oJ!

ROI Type: 1

5000
Energy(kev)

5500

6000
ROI Type: 3

6500

Channel Data Report

8/14/2013

Page

12:35:4:! Mt

*******************************************************
s p E C T R A L DAT A R E P 0 R T *****
*****
*******************************************************
Sample Title:

07

Elapsed Live time:


Elapsed Real Time:

10201
10201

Channell------l-------l-------l-------1-------1-------1-------l-------I
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0
1
1
0
1
0
0
1
0
1
5
10
5
10
3
0
1
1
2
0
1
0
3
0
2
1
2
0

10201
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
1
0
0
1
1
0
2
0
2
2
0
5
6
5
5
0
0
0
0
0
1
0
0
2
1
1
1
1

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
2
0
1
0
1
2
2
0
3
5
0
5
2
8
7
2
0
1
0
2
1
0
1
1
1
1
1
2

0
0
0
0
1
1
0
0
0
0
0
0
0
1
0
0
0
0
0
0
2
0
0
1
2
2
3
3
5
9
5
4
2
0
1
0
0
1
1
0
1
2
0
1
2
2

0
0
0
1
0
0
0
0
0
1
0
0
1
0
0
0
2
0
1
2
0
2
1
4
2
3
1
6
5
4
7
2
3
0
0
1
2
2
2
2
2
0
0
2
1
1

0
2
0
0
0
0
0
0
0
0
0
1
1
0
0
0
0
1
0
0
0
0
1
2
1
1
3
3
4
6
3
4
0
0
0
0
0
0
3
2
1
1
0
4
2
2

0
0
1
0
0
1
0
0
1
0
1
0
1
1
0
0
0
0
1
1
0
3
0
1
3
0
2
2
3
8
3
4
0
0
1
0
1
0
0
1
0
0
0
1
0
0

0
0
1
0
0
0
0
0
1
0
0
2
0
0
2
0
1
1
0
0
0
0
0
4
0
5
3
5
2
6
4
5
2
1
0
0
1
1
0
0
0
0
0
0
1
1
913~

Channel Data Report


369:

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3

Sample Title:

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12:35:42 l?M
1

07

Channell------l-------l-------1-------1-------1-------l-------l-------I
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721:
729:
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769:
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0
2
2
5
3
8
10
9
3
0
2
0
0
0
0
0
0
1
1
0
1
1
0
0
0
3
3
7
8
13
2
0
0
0
0
1
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0

2
4
5
3
8
7
19
10
2
0
1
0
1
0
0
0
1
0
1
0
3
0
4
0
3
0
7
9
14
5
4
1
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0

1
5
2
3
7
6
9
6
5
0
0
1
0
0
0
0
1
0
1
0
1
2
0
1
4
3
6
6
9
9
6
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

2
1
5
3
6
6
11
11
3
0
0
0
0
0
0
0
1
1
2
0
2
0
2
2
3
2
4
6
8
9
2
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
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2
0
4
2
9
2
14
7
3
0
0
0
0
0
1
1
0
0
2
1
1
1
2
2
4
4
6
11
14
8
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

4
2
5
4
10
11
9
10
3
0
1
2
0
0
2
0
0
0
1
0
1
1
1
1
3
10
5
11
10
10
3
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

1
1
3
3
10
13
13
9
2
0
0
1
1
0
0
2
1
1
0
2
1
1
2
3
4
3
2
5
13
5
3
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0

1
3
3
5
6
8
9
6
5
0
0
1
1
1
0
1
0
0
1
0
1
3
3
2
4
5
7
9
11
3
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

61135

Channel Data Report


801:

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0

Sample Title:

Page

12:35:42 PM
0

07

Channell------l-------l-------l-------1-------1-------1-------l-------I
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913:
921:
929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
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0
0
0

0
0
0
0
0
0
0
0
0
0
0
1
0
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0
0
0
0
0
0
0
0
0
0
0
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0
0
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0
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1
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1
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0
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0
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1
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0
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0
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0
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0

0
0
0
0
0
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0
0
0
0
0
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0
0
1
0
0
0
0
0
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0
0
0
0

fiJ 136

Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:

PZ-107-SS TOT
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000661
1307154A-UU
08
Shelf 2
U iso

Detector Name:
Chamber Serial Number:
Detector Serial Number:
Env. Background:
Reagent Blank:

Alpha_025
25
System Bkgd 64777
<not performed>

Sample Size:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:

l.OOOE+OOO +/ O.OOOE+OOO liter


7 /19/2013
7:26:18 AM
8/14/2013
9:27:37 AM
170.0 minutes
170.0 minutes

Tracer Certificate:
Tracer Quantity:
Effective Efficiency:
Counting Efficiency:
Chem. Recovery Factor:

U232 UU-lOA
0.603 mL
0.1822 +/ 0.0106
0.1736 +/ 0.0032 on 12/15/2012
1.0499 +/ 0.0640

Peak Match Tolerance:

0.150 MeV

PEAK
Energy
(MeV)

Nuclide
U-232
U-234
U-235
U-238

5.260
4.708
4.397
4.140
T

Net
Pk Area

AREA

REPORT

Pk Area
Error %

353.32
112. 98
10.00
97.83

1:57:27 PM

10.44
18.54
65.01
19.84

Ambient
Backgnd

Reagent
Backgnd

0.68

O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

1. 02

0.00
0.17

FWHM
(keV)
4.4
8.2
3.1
4.4

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS


Nuclide

Id
Conf.

Energy
(keV)

U-232
U-234
U-235
U-238

0.987
0.980
0.999
0.986

5302.50*
4761.50*
4385.50*
4184.40*

Activity
(pCi/liter )
5.15E+OOO
l.65E+OOO
l.80E-001
l.42E+OOO

+/
+/
+/
+/

5.86E-001
3.58E-001
l.19E-001
3.24E-001

MDA
(pCi/liter
8.22E-002
9.18E-002
1. 08E-001
6.05E-002

+/
+/
+/
+/

9.35E-003
1. 04E-002

l.23E-002
6.88E-003

Ac,
gl1Lf11J

:!} 137

0000066144.CNF

Live Time :10201.000 sec


Real Time :10201.000 sec
start:
1: 3405. 9(kev)
stop : 1024: 6615. S(kev)
Acq. Start :wed Aug 14 09:27:37 2013

60
55

50

45

40

35

VI

+-'

s:::
::s

8 30

25

20

15

10

5
0

3500

4500

4000

5000

Energy(kev)

5500

6000

Q;1I
!I-"

t.iJI
()I)

ROI Type: 1

ROI Type: 3

6500

Channel Data Report

8/14/2013

Page

12:35:49 PM

*******************************************************
s p E c T R A L DAT A R E p 0 R T *****
*****
*******************************************************
Sample Title:

08

Elapsed Live time:


Elapsed Real Time:

10201
10201

Channell------l-------l-------l-------1-------1-------1-------l-------I
1:
9:
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10201
0
1
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1
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1
3
2
4
3
0
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0
0
0
1
1
0
0
0
0
0

10201
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1
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0
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0
0
1
0
1
1
0
0
0
0
0
0
0
0
0
0
0
0
1
2
0
2
0
1
2
4
0
0
0
1
0
0
0
1
1
0
0
0
0
1

1
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
1
0
2
1
1
4
0
2
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
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1
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0
2
0
0
0
0
0
0
0
0
0
0
0
0
1
0
1
1
2
1
4
1
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
1
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0
0
0
0
0
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0
1
2
0
0
0
0
1
0
0
1
0
1
0
2
2
2
3
0
0
0
1
0
0
0
1
1
0
1
0
1
0

0
0
0
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1
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0
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1
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0
7
0
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3
0
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3
2
1

0
0
0
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2
0
0
1
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0
1
0
0
0
1
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0
2
3
2
5
3
1
1
0
2
0
1
0
0
0
0
0
0
0
0
0

0
2
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1
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1
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1
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1
2
4
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1
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1
0
0
0
0
.~,.;

.;::t;a.fi

~iJ!j

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4S7:
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497:
SOS:
S13:
S21:
S29:
S37:
S4S:
SS3:
S61:
S69:
S77:
S8S:
S93:
601:
609:
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62S:
633:
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6S7:
66S:
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681:
689:
697:
70S:
713:
721:
729:
737:
74S:
7S3:
761:
769:
777:
78S:
793:

1
0
1
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2
1
3
2
1
0
0
0
0
1
1
0
0
0
0
1
1
0
0
2
2
7

lS
17
6
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
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0
0
0

1
3
4
2
4
2
2
1
0
1
0
0
0
0
0
0
1
0
1
1
0
2
3
3
2
1
12
7
8
6
0
0
0
0
0
0
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0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0

2
1
0
3
2
0
2
2
1
0
0
0
0
0
0
2
0
0
1
1
1
1
1
0

3
9
12
11

0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

1
0
3
3
1
1
4
2
0
0
0
1
1
0
1
0
0
2
0
1
0
1
2

s
6
3
9
8
6
2
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
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0
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0
2
1
2

s
4
4
0
0
0
0
0
1
0
0
1
0
0
0
1
2
2
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2
3

13
7
21
2
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0
1
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1
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0
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0
0
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0
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2
1
0
1
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3
4
1
0
0
1
1
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0
1
0
0
0
1
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1
0
2
1
3
6
7
7
6
1
0
0
0
0
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0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
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1
0
0
1
1

s
2
2
0
0
0
1
0
1
1
0
0
2
4
0
1
2
2
0
7
6
7
8
8
1
0
0
0
0
0
0
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0
0
0
0
0
0
0
0
0
0
0
0
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1
2
0
0
2
7
4
0
1
0
0
0
1
1
0
0
1
0
0
0
0
0
1
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6
7
12
13
10
1
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0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

E146?

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Page

12:35:49 PM
0

08

Channell------l-------1-------1-------1-------l-------l-------l-------I
809:
817:
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833:
841:
849:
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865:
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889:
897:
905:
913:
921:
929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
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0
0
0
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0
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0
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0
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0
0
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0
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0
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0
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0
0
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0
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0
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0
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0
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0
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0
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0
0
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0
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1
0
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0
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0
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0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0

.~~Apex-Alpha

Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:

PZ-107-SS DIS
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000661
1307154A-UU
09
Shelf 2
u iso

Detector Name:
Chamber Serial Number:
Detector Serial Number:
Env. Background:
Reagent Blank:

Alpha_027
27
System Bkgd 64778
<not performed>

Sample Size:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:

1.000E+OOO +/ O.OOOE+OOO liter


7/19/2013
7:26:18 AM
8/14/2013
9:27:38 AM
170.0 minutes
170.0 minutes

Tracer Certificate:
Tracer Quantity:
Effective Efficiency:
Counting Efficiency:
Chem. Recovery Factor:

U232 UU-lOA
0.606 mL
0.0863 +/ 0.0070
0.1728 +/ 0.0032 on 12/15/2012
0.4993 +/ 0.0414

Peak Match Tolerance:

0.150 MeV

PEAK
Energy
(MeV)

Nuclide
U-232
U-234
U-235
U-238

5.270
4. 710
4 .413
4.147
T

Net
Pk Area

AREA

REPORT

Pk Area
Error %

168.15
59.98
4.32
27.15

2:27:41 PM

15.16
25.56
102.62
38.30

Ambient
Backgnd

Reagent
Backgnd

FWHM
(keV)

0.85
1. 02
0.68
0.85

O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

4.9
11.1
3.2
4.0

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS


Nuclide

Id
Conf.

Energy
(keV)

U-232
U-234
U-235
U-238

0.993
0.982
0.995
0.990

5302.50*
4761.50*
4385.50*
4184.40*

Activity
(pCi/liter )
5.18E+OOO
1.85E+OOO
1.64E-001
8.32E-001

+/+/+/+/-

8.19E-001
5.55E-001
1. 70E-001
3.45E-001

./t4
cg1 14-/ '3

MDA
(pCi/liter
1.84E-001
1.94E-001
2.14E-001
l.83E-001

+/+/+/+/-

2.92E-002
3.07E-002
3.39E-002
2.90E-002

0000066143.CNF

Live Time :10201.000 sec


Real Time :10201.000 sec
start:
1: 3402. 4(kev)
stop : 1024: 6658. l(kev)
Acq. Start :wed Aug 14 09:27:38 2013

60
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50

45

40

35

VI

.f-J

c:

:::J

8 30

25

20

15

......
m
......
'
=>

10

3500

4000

t..)

4500

"'r.i..""

1,n

ROI Type: 1

5000

Energy(kev)

5500

6000
ROI Type: 3

6500

Channel Data Report

8/14/2013

Page

12:35:56 PM

*******************************************************
s p E C T R A L DAT A R E P 0 R T *****
*****
*******************************************************
Sample Title:

09

Elapsed Live time:


Elapsed Real Time:

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'!144

Channel Data Report


369:

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0

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0
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1
0
0
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1
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0
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6
6
3
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0
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1
1
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0
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2
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m145

Channel Data Report


801:

8/14/2013
0

Sample Title:

Page

12:35:56 PM
0

09

Channell------l-------l-------1-------1-------1-------l-------l-------I
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0
0
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0
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0
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0
1
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1
0
0
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0
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1
0
0
0
0
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1
0
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0
0
1
0
1
0
0
0
0
0
0
0
0
0
0
0

Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:

PZ-106-KS TOT
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000661
1307154A-UU
10
Shelf 2
u iso

Detector Name:
Chamber Serial Number:
Detector Serial Number:
Env. Background:
Reagent Blank:

Alpha_029
29
System Bkgd 64779
<not performed>

Sample Size:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:

1.000E+OOO +/ O.OOOE+OOO liter


7/19/2013
7:26:18 AM
8/14/2013
9:27:39 AM
170.0 minutes
170.0 minutes

Tracer Certificate:
Tracer Quantity:
Effective Efficiency:
Counting Efficiency:
Chem. Recovery Factor:

U232 UU-lOA
0.600 mL
0.1660 +/ 0.0100
0.1945 +/ 0.0036 on 12/15/2012
0.8534 +/ 0.0540

Peak Match Tolerance:

0.150 MeV

PEAK
Energy
(MeV)

Nuclide
U-232
U-234
U-235
U-238

5.274
4.724
4.409
4.147

Net
Pk Area

AREA

REPORT

Pk Area
Error %

320.64
127.32
15.49
58.49

2:30:02 PM

Ambient
Backgnd

10.97
17.42
50.75
25.76

1. 36
0.68
0.51
0.51

Reagent
Backgnd

FWHM
(keV)

O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
0.00E+OOO

11. 8

4.0
3.1
4.1

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS


Nuclide

Id
Conf.

Energy
(keV)

U-232
U-234
U-235
U-238

0.994
0.990
0.996
0.990

5302.50*
4761.50*
4385.50*
4184.40*

Activity
(pCi/liter )
5. 13E+OOO
2.04E+OOO
3.06E-001
9.31E-001

+/
+/
+/
+/

6.09E-001
4.29E-001
1.59E-001
2.64E-001

MDA
(pCi/liter
l.lOE-001
9.02E-002
1.04E-001
8.36E-002

+/
+/
+/
+/

1. 30E-002
1.07E-002
1.23E-002
9.91E-003

AG

&"l1+f1~

6147

0000066145.CNF

Live Time :10200.000 sec


Real Time :10200.000 sec
start:
1: 3413. S(kev)

stop : 1024: 6597. S(kev)

Acq. start :wed Aug 14 09:27:39 2013

60

55

50

45

40

35

VI

......
r::::
::::s

8 30

25

20

15

10

3500

4000

4500

II"~

5000
Energy(kev)

5500

6000

Mi.....&.

,Jt:i1,

00

ROI Type: 1

ROI Type: 3

6500

Channel Data Report

8/14/2013

Page

12:36:03 PM

*******************************************************
s p E C T R A L DAT A R E P 0 R T *****
*****
*******************************************************
Sample Title:

10

Elapsed Live time:


Elapsed Real Time:

10200
10200

Channell------l-------l-------l-------l-------1-------1-------1-------I
1:
9:
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305:
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345:
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10200
0
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10200
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0
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1
0
0
1
0
0
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0
0
1
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0
2
3
0
0
2
0
0
0
0
0
1
1
1
0
1
2

0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
1
1
0
0
1
0
0
1
1
1
2
1
1
0
1
0
0
0
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1
0
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0
0
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1
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0
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0
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!!i149

Channel Data Report


369:

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1

Sample Title:

Page

12:36:0J PM
0

10

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0
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3
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0

0
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4
2
7
1

0
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0
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1
1

1
1

1
1
1

2
3
3

0
0
0

0
0
2
5
2
0
0

0
0
0
4
5
3

1
1

0
7
6
7
0
0
0
0
0
0
0
0
0
0
0
5

1
1
1

0
0
0
0

2
3
0

0
0
0

0
0

0
0
0

0
0

5
4

0
0

0
0
0
0

2
2

1
1

2
0

1
1
1

2
2
4
5
6
6
10
8
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
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0
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0
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0
0
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0
0

2
0
4
7
9
11

4
0
0
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0
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0
0
0
1

0
0
0
0
0
0
0
0
0
0

0
3

1
1
1

1
1
1

2
0

0
2

0
0
0
0
0
0
0
0
0
0
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3
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0

0
1

2
0
2
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4
14
8
10
6
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

B15fil

Channel Data Report


801:

8/14/2013
0

Sample Title:

Page

12:36:03 PM
0

10

Channell------l-------l-------l-------l-------1-------1-------1-------I
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0
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0
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0
0
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1
0
0
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0
0
0
0
0
0
0
0
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0
0
0
0
0
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0
0
0
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0
0
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0
0
0
0
0
0
1
0
0
0
0
0
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0
0
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0
0
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0
0
0
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0
0
0
0
0
0
0
0
0
0
0
0

ti151

~~~'ifrApex-Alpha,.

Sample Description:
Spectrum File:
Batch Identification:

Sample Identification:

Sample Geometry:

Procedure Description:

PZ-106-KS DIS
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000661
1307154A-UU
11
Shelf 2
u iso

Detector Name:

Alpha_031
Chamber Serial Number:

Detector Serial Number:


31
Env. Background:

System Bkgd 64780


Reagent Blank:

<not performed>
Sample Size:

Sample Date/Time:

Acquisition Date/Time:

Acquisition Live Time:

Acquisition Real Time:

l.OOOE+OOO +/- O.OOOE+OOO liter


7/19/2013
7:26:18 AM
8/14/2013
9:27:40 AM
170.0 minutes
170.0 minutes

Tracer Certificate:

Tracer Quantity:

Effective Efficiency:

Counting Efficiency:

Chem. Recovery Factor:

U232 UU-lOA
0.606 mL

0.1146 +/- 0.0081

0.1418 +/- 0.0034 on 6/13/2013


0.8080 +/- 0.0605

Peak Match Tolerance:

0.150 MeV

PEAK
Energy
(MeV)

Nuclide
U-232
U-234
U-235
U-238

5.265
4. 715
4.414
4.153
T

Net
Pk Area
223.32
87.15
7.66
33.77

AREA

3:23:29 PM

REPORT
FWHM
(keV)

Pk Area
Error %

Ambient
Backgnd

Reagent
Backgnd

13.14
21.11
72.63
35.57

0.68
0.85
0.34
3.23

O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
0.00E+OOO

13 .3

4.2
3.1
7.1

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS

Nuclide

Id
Conf.

Energy
(keV)

U-232
U-234
U-235
U-238

0.990
0.985
0.994
0.993

5302.50*
4761.50*
4385.50*
4184.40*

Activity
(pCi/liter )
5.18E+OOO
2.02E+OOO
2.19E-001
7.79E-001

+/+/+/+/-

7.19E-001
5.lOE-001
l.62E-001
2.97E-001

1\4
8ff4/IJ

MDA
(pCi/liter
l.31E-001
1. 39E-001
1. 37E-001
2.lOE-001

+/+/+/+/-

l.82E-002
l.93E-002
l.90E-002
2.92E-002

0000066146.CNF

Live Time :10200.000 sec


Real Time :10200.000 sec
start:
1: 3388. 9(kev)
stop : 1024:6594.6(kev)
Acq. Start :wed Aug 14 09:27:40 2013

60

55

50

45

40

35

V'I

.f--1

c:

::::s

8 30

25
20
15
10

5
0

3500
'~

~~
U11
l~~11

4000

4500
ROI Type: 1

5000

Energy(kev)

5500

6000

ROI Type: 3

6500

Channel Data Report

8/14/2013

12: 36 :i.t

Page

*******************************************************
s p E C T R A L DAT A R E P 0 R T *****
*****
*******************************************************
Sample Title:

11

Elapsed Live time:


Elapsed Real Time:

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m1sa

Channel Data Report


369:

8/14/2013
1

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0
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3
3
1
0
0
0
1
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0
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1
1
1
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3
1
3
1
1
8
3
8
5
0
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0
1
1
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1
3
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2
0
0
0
0
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1
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0
1
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0
1
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0
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1
1
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2
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5
8
1
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0
0
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2
3
0
0
0
0
0
0
0
0
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2
0
0
0
0
0
2
2
4
3
1
5
7
3
0
0
0
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0
0
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0
0
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0
0
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0

0
1
0
1
5
2
2
2
0
1
0
0
0
1
0
0
0
0
1
1
0
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0
1
2
4
4
4
4
7
1
0
0
0
0
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0
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1
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0
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0
3
6
5
4
3
3
0
0
0
0
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0
0
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1
0
0
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0
0
0
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0
0
0
~155

Channel Data Report


801:

8/14/2013
0

Sample Title:

12:36:11
0

Page

PM
0

11

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953:
961:
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1001:
1009:
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0
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0
0
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0
0
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0
0
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0
0
0
0
0
0
0
0
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0
0

0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
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0
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0
0
0
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0
0
0
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0
0
0
0
0
0
0
0
0
0
0
0
0
0

fl15E

Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:

DUP 08 TOT

\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000661

1307154A-UU

12

Shelf 2

U iso

Detector Name:
Chamber Serial Number:
Detector Serial Number:
Env. Background:
Reagent Blank:

Alpha_033

04026479A

91132

System Bkgd 64781

<not performed>

Sample Size:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:

l.OOOE+OOO +/- O.OOOE+OOO liter

7/19/2013
7:26:18 AM

8/14/2013
9:28:09 AM

170.0 minutes

170.1 minutes

Tracer Certificate:
Tracer Quantity:
Effective Efficiency:
Counting Efficiency:
Chem. Recovery Factor:

U232 UU-lOA
0.605 mL

0.0713 +/0.1848 +/0.3859 +/-

Peak Match Tolerance:

0.150 MeV

PEAK
Energy
(MeV)

Nuclide

Net
Pk Area

0.0063

0.0032 on 7/20/2013
0.0346

AREA

2: 31: 30 PM

REPORT

Pk Area
Error %

Ambient
Backgnd

Reagent
Backgnd

0.17
0.17
0.34
0.34

O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

FWHM

(keV)

-------------------------------------------------------------------------------U-232
U-234
U-235
U-238

5.275
4.738
4.433
4.158

138.83
46.83

6.66
40.66

16.65
28.70
78.18
30.89

10.1

5.0
3.0

7.5

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS


Nuclide

Id
Conf.

Energy
(keV)

Activity
(pCi/liter )

MDA

(pCi/liter

-------------------------------------------------------------------------------U-232
U-234
U-235
U-238

0.995
0.996
0.984
0.995

5302.50*
4761.50*
4385.50*
4184.40*

5.17E+OOO
l.74E+OOO
3.06E-001
l.51E+OOO

+/+/+/+/-

8.92E-001
5.84E-001
2.45E-001
5.33E-001

l.55E-001
l.55E-001
2.20E-001
l.77E-001

+/+/+/+/-

2.68E-002
2.68E-002
3.79E-002
3.06E-002

g(1tH~

ill 157

0000066148.CNF

Live Ti me :10200. 000 sec


Rea1 Ti me :10208. 400 sec
start:
1: 3447. 3(kev)
Stop : 1024: 6496. 6(kev)
Acq. start :wed Aug 14 09: 28: 09 2013

60
55
50
45
40
35
V)

......
c:
:::s

8 30

25
20
15
10

5
0

!.

w.

u:

3500

4000

4500

llt~

5000

Energy(kev)

6000

5500

~~~

U1l

(10

ROI Type: 1

ROI Type: 3

6500

Channel Data Report

8/14/2013

Page

12:36:18 PM

*******************************************************
s p E C T R A L DAT A R E P 0 R T *****
*****
*******************************************************
Sample Title:

12

Elapsed Live time:


Elapsed Real Time:

10200
10208

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N159

Channel Data Report


369:

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0

Sample Title:

Page

12:36:18 PM
0

12

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1
1
1
0
0
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1
3
7
0
0
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0
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0
~16m

Channel Data Report


801:

8/14/2013
0

Sample Title:

Page

12:36:11 ~
0

12

Channell------l-------1-------1-------1-------l-------l-------l-------I
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ti161

~Apex-Alpha

Sample Description:

Spectrum File:

Batch Identification:

Sample Identification:

Sample Geometry:

Procedure Description:

DUP 08 DIS
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000661
1307154A-UU
13
Shelf 2
U iso

Detector Name:

Alpha_034
Chamber Serial Number:

04026479B
Detector Serial Number:
91136
Env. Background:

System Bkgd 64782


Reagent Blank:

<not performed>
Sample Size:

Sample Date/Time:

Acquisition Date/Time:

Acquisition Live Time:

Acquisition Real Time:

l.OOOE+OOO +/- O.OOOE+OOO liter


7/19/2013
7:26:18 AM
8/14/2013
9:28:10 AM
170.0 minutes
170.1 minutes

Tracer Certificate:

Tracer Quantity:

Effective Efficiency:

Counting Efficiency:

Chem. Recovery Factor:

U232 UU-lOA
0.604 mL

0.1096 +/- 0.0079

0.1856 +/- 0.0032 on 12/16/2012


0.5906 +/- 0.0440

Peak Match Tolerance:

0.150 MeV

PEAK
Energy
(MeV)

Nuclide
U-232
U-234
U-235
U-238

5.279
4.725
4.448
4.135
T

Net
Pk Area

AREA

REPORT

Pk Area
Error %

213.00
65.00
8.00
38.66

5:49:43 PM

13.46
24.50
73.50
31.68

Ambient
Backgnd
0.00
0.00
0.00
0.34

FWHM
(keV)

Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

5.4
4.8
3.0
3.7

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS

Nuclide

Id
Conf.

Energy
(keV)

U-232
U-234
U-235
U-238

0. 996
0.990
0.973
0.983

5302.50*
4761.50*
4385.50*
4184.40*

Activity
(pCi/liter )
5.16E+OOO
l.57E+OOO
2.39E-001
9.33E-001

+/
+/
+/
+/

7.33E-001
4.46E-001
1. 79E-001
3.24E-001

MDA
(pCi/liter
l.45E-001
l.45E-001
1. 79E-001
l.15E-001

+/
+/
+/
+/

2.06E-002
2.06E-002
2.54E-002
1. 64E-002

<i( ('tf')

11!162

0000066147.CNF

Live Time 10200.000 sec


Real Time 10208.400 sec
start:
1 3439.l(kev)
stop : 1024 6479.9(kev)
Acq. Start wed Aug 14 09:28:10 2013

60
55
50
45
40
35
V>

+-'
s::::
=3

8 30

25
20
15
10
5
0

3500

4000

4500

(ii"
~"'"Iii

m
~;..JI

ROI Type: 1

5000

Energy(kev)

6000

5500
ROI Type: 3

Channel Data Report

8/14/2013

Page

12:36:25 PM

*******************************************************
s p E C T R A L DAT A R E P 0 R T *****
*****
*******************************************************
Sample Title:

13

Elapsed Live time:


Elapsed Real Time:

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~164.

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s-1ss

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801:

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Sample Title:

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12:36:25 ?M
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13

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il! 166

Page 1 of 2
8/14/2013 5:45:39 AM

QA SUMMARY REPORT

Review Of QA Results - Pulser Check


Date
Time

: 8/14/2013
: 5:45:39 AM

CHAMBER
Alpha 001
Alpha 002
Alpha 003
Alpha 004
Alpha 005
Alpha 006
Alpha 007
Alpha 008
Alpha 009
Alpha 010
Alpha 011
Alpha 012
Alpha 013
Alpha 014
Alpha 015
Alpha 016
Alpha 017
Alpha 018
Alpha 019
Alpha 020
Alpha 021
Alpha 022
Alpha 023
Alpha 024
Alpha 025
Alpha 026
Alpha 027
Alpha 028
Alpha 029
Alpha 030
Alpha 031
Alpha 032
Alpha 033
Alpha 034
Alpha 035
Alpha 036
Alpha 037
Alpha 038
Alpha 039
Alpha 040
Alpha 041
Alpha 042

DEVICE
2lf
2lf
2lf
2lf
2lf
2lf
2lf
2lf
2lf
2lf
21f
21f
21f
21f
21f
21f
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
Alpha AnalystlOODC
Alpha Analvstl OODC
Alpha Analyst! OODC
Alpha Analystl OODC
Alpha Analyst! OODC
Alpha AnalystlOODC
Alpha Analyst! OODC
Alpha Analyst! OODC
Alpha Analvstl OODC
Alpha Analystl OODC

PARAMETER
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
Peak Energy
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL

FLAG
Not Done
Not Done
Passed
Passed
Not Done
Not Done
Not Done
Not Done
Not Done
Passed
Passed
Passed
Passed
Passed
Action
Not Done
Not Done
Passed
Passed
Not Done
Not Done
Passed
Passed
Passed
Passed
Not Done
Passed
Not Done
Passed
Not Done
Passed
Not Done
Passed
Passed
Passed
Passed
Passed
Passed
Passed
Passed
Passed
Passed

DATE

8/14/2013 5:27:31 AM
8/14/2013 5:27:32 AM

8/14/2013
8/14/2013
8/14/2013
8/14/2013
8/14/2013
8/14/2013

5:27:33 AM
5:27:34 AM
5:27:34 AM
5:27:35 AM
5:27:36 AM
5:27:37 AM

8/10/2013 11:23:01 AM
8/14/2013 5:27:38 AM

8/14/2013
8/14/2013
8/14/2013
8/14/2013

5:27:38 AM
5:27:39 AM
5:27:40 AM
5:27:41 AM

8/14/2013 5:27:42 AM
8/14/2013 5:27:42 AM
8/14/2013 5:27:43 AM
8/14/2013 5:27:44 AM
8/14/2013 5:27:46 AM
8/13/2013 5:25:31 AM
8/14/2013 5:27:49 AM
8/14/2013 5:27:50 AM
8/14/2013 5:27:52 AM
8/14/2013 5:27:54 AM
8/14/2013 5:27:56 AM
8/14/2013 5:27:58 AM
8/14/2013 5:28:00 AM

6167

Page 2 of 2

Review of QA Results - Pulser

Ch~k

8/14/2013 5:45:39 AM

CHAMBER
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha

043
044
045
046
047
048

DEVICE

PARAMETER

Alpha Analystl OODC


Alpha Analyst 1OODC
Alpha Analystl OODC
Alpha Analystl OODC
Alpha Analyst 1OODC
Alpha Analystl OODC

ALL
ALL
ALL
ALL
ALL
ALL

APPROVED BY:

APPROVAL DATE:

FLAG
Passed
Passed
Passed
Passed
Passed
Passed

DATE
8/14/2013
8/14/2013
8/14/2013
8/14/2013
8/14/2013
8/14/2013

5:28:02 AM
5:28:04 AM
5:28:07 AM
5:28:10 AM
5:28:13 AM
5:28:15 AM

6/12/12

Library Listing Report

Page

12:17:04 PM

*************************************************************************
*****
L I B R A R Y L I S T I N G R E P 0 R T
*****
*************************************************************************
Nuclide Library Title:

Uranium

Nuclide Library Description:


Nuclide
Name

Half-Life
(Seconds)

U-232
U-234
U-235
U-238

2.174E+009
7.731E+012
2.221E+016
1.410E+017

Energy
(keV )

U-232,-234,-235,-238
Energy
uncert. (keV
0.000
0.000
0.000
0.000

5302.500*
4761.500*
4385.500*
4184 .400*

Yield
(%)
99.8000
99.8000
80.9000
100.2300

Yield
Uncert. (Abs.+-)
0.0000
0.0000
0. 0000
0.0000

key line

TOTALS:

Nuclides

Energy Lines

6J169

SECTION IX

ANALYTICAL DATA (ISOTOPIC THORIUM)

617&1

Eberline Services
Oak Ridge Laboratory
Analysis Sheet

Printed: 811412013 5:58 AM


Page 1of3

13-07154
Th ISO
Run 1
Internal I Sample
I
Fraction ; Desc

13-07154

Work Order

Client
ID

Login
CPM

Sample
Date

07/24/13 00:00

Sample
Aliquot

Analysis Code

ThlSO

Run

01

LCS

LCS

1.0000E+OO

r--~--

02

I MBL

BLANK

07 /24/13 00:00

1.0000E+OO

~--

7/22/2013

Date Received

DUP

PZ-107-SS TOT

46

07/19/13 12:10

1.0000E+OO

04

I TRG

PZ-200-SS TOT

42

07/19/13 10:19

1.0000E+OO

05

TRG

PZ-200-SS DIS

42

07/19/13 10:19 I

1.0000E+OO

TRG

PZ-102-SS TOT

38

07 /19/13 10:30

1.0000E+OO

TRG

PZ-102-SS DIS

38

07/19/13 10:30

1.0000E+OO

03
f---

8/13/2013

Lab Deadline

Client I Engineering Management Support, Inc.

Project I
Report Level

West Lake OU-1

06

07

I
I

-----

pCi

DO

PZ-107-SS TOT

46

07/19/1312:10

1.0000E+OO

09

TRG

PZ-107-SS DIS

46

07/19/13 12:10

1.0000E+OO

WA

10

TRG

PZ-106-KS TOT

45

07/19/13 13:09

1.0000E+OO

HASL 300, 4.5.2

11

TRG

PZ-106-KS DIS

45

07/19/13 13:09

1.0000E+OO

Alpha Spectroscopy

12

TRG

DUP 08 TOT

44

07/19/13 00:00

1.0000E+OO

Radiometric Tracer

Th-229

13

TRG

DUP 08 DIS

44

07/19/13 00:00

1.0000E+OO

Radiometric Sol#

Th-18a

Tracer Act (dpm/g)

22.466

Activity Units

08
-

Aliquot Units
Matrix
Method
Instrument Type

-~

Carrier
Carrier Cone (mg/ml)

I
~~
y.....im.

"'~
!lirllu~

SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only.

Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.

----

Eberline Services
Oak Ridge Laboratory
Analysis Sheet

Printed: 8114/2013 5:58 AM


Page 2 of 3

13-07154
Th ISO
Run 1

Internal
Fraction

Sample
Desc

01

LCS

Tracer
Aliquot (g)

0.4800

02

MBL

0.2373

03

DUP

04

I
I
I

Tracer Total
ACT(dpm)

Radiometric
Tracer (pCi)

10.8+

Radiometric Grav Carrier


%Rec
Added(ml)

Grav Filter
Tare (g)

Grav Filter
Final(g)

I
I

Grav Filter
Net(g)

Grav
%Rec

Mean
%Rec

SAF
1

O.OOi

----

5.3

0.00

0.2369

5.3

0.00

TRG

0.2345

5.3

0.00

05

TRG

0.2339

5.3

0.00

06

TRG

0.2354

5.3 '

0.00

07

TRG

0.2320

5.2

0.00
-

08

DO

0.2328

5.2

0.00

09

TRG

0.2361

5.3

0.00

10

TRG

0.2338

5.3

0.00

11

TRG

0.2346

5.3

0.00

12

TRG

0.2345

5.3

0.00

_____ ___
,

TRG

13

0.2350

5.3

0.00
I

I
I

Ii

I
I
I

'~
ll'ttlilf
"~.~
~Ji

* SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only.

**Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.

SAF
2

Eberline Services
Oak Ridge Laboratory
Analysis Sheet

Printed: 811412013 5:58 AM


Page 3 ofJ

13-07154
Thi SO
Run 1

Internal j Sample
Fraction ! Desc

01

Rough Prep
Date

Rough Prep

LCS

02

I 08/08/13 07:46

Prep

By

JWOLFE

08/08/13 07:46

JWOLFE

I 08/08113 07:46

JWOLFE

I MBL

Prep
Date

By

I DUP

03

04

TRG

08/08/13 07:46

JWOLFE

=05

I TRG

08/08/13 07:46

JWOLFE

TRG

08/08/13 07:46

JWOLFE

TRG

08/08/13 07:46

JWOLFE

08/08/13 07:46

JWOLFE

06

07
!

DO

By

Sep t1
Date/Time

Sep t1

By

-~

..

---

08

Sep tO

..

~-

Sep tO
Date/Time

l
I
I
I

09

TRG

08/08/13 07:46

JWOLFE

10

TRG

08/08/13 07:46

JWOLFE

TRG

08/08/13 07:46

JWOLFE

12

TRG

08/08/13 07:46

JWOLFE

13

TRG

08/08/13 07:46

. JWOLFE

11
--

I
I
I
I

r
I
I

II

I
I

II
~---

II

f,.~
.....
,

....Ji

t.,Ji

SAF1

is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only.

Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.

~-

Work Order: 13-07154-ThlS0-1

LCS
Known

LCS
%R

LCS
Flag

95.89

OK

RPO
Flag

MDA
Flag

Nuclide

Sample
Desc

Client
Identification

Activity
Units

01

TH-228

LCS

LCS

pCl/I

4.75E+OO

8.75E-01

1.33E-01

02

TH-228

MBL

BLANK

pCi/I

-2.03E-02

7.09E-02

1.86E-01

03

TH-228

DUP

PZ-107-SS TOT

pCi/I

8.67E-01

3.14E-01

1.18E-01

04

TH-228

TRG

PZ-200-SS TOT

pCi/I

1.72E-01

1.04E-01

7.06E-02

OK'

05

TH-228

TRG

PZ-200-SS DIS

pCi/I

7.25E-02

8.80E-02

1.37E-01

OK

06

TH-228

TRG

PZ-102-SS TOT

pCi/I

2.99E+OO

6.53E-01

7.37E-02

OK

07

TH-228

TRG

PZ-102-SS DIS

pCi/I

-7.39E-03

5.91E-02

1.59E-01

OK

TH-228

DO

PZ-107-SS TOT

pCi/I

1.13E+OO

3.48E-01

1.35E-01

OK

09

TH-228

TRG

PZ-107-SS DIS

pCi/I

-3.96E-02

1.38E-01

3.90E-01

OK

10

TH-228

TRG

PZ-106-KS TOT

pCi/I

-1.31 E-02

5.62E-02

1.56E-01

OK

11

TH-228

TRG

PZ-106-KS DIS

pCi/I

4.33E-02

1.28E-01

2.79E-01

OK

12

TH-228

TRG

DUP 08 TOT

pCi/I

1.15E+OO

3.67E-01

1.04E-01

OK

13

TH-228

TRG

DUP 08 DIS

pCl/I

1.58E-01

1.24E-01

9.65E-02

OK

Lab

Fraction

Printed: 8/14/2013 4:27 PM

Page 1 of 3

Preliminary Data Report & Analytical Calculations

Eberline Services
Oak Ridge Laboratory

Results

Error Estimate

MDA

4.96E+OO

OK
OK

------

NA

OK

----'-

QI

0
(.J
.~

~
.,,
i::

"(

en

.c

I-

08
-

..5

t!
0

a.
a.

---

::I

"'-c

QI

i:

E
QI

.,,Cl
.,,c

::!:

---------

--------- -

1-----

;;~

i-1'

"'.J

l:l:~.

Blank
Flag

OK

Eberline Services
Oak Ridge Laboratory

c::;,
a::

.g
0

u
.!!!

~
Ill
c:
c:c

""""-

Grav
%Rec

Mean
%Rec

Sample
Desc

Sample
Date

01

TH-228

LCS

07/24/13 00:00

1.00E+OO

75.64

o.oo

0.00

02

TH-228

MBL

07/24/13 00:00

1.00E+OO

76.40

0.00

0.00

TH-228

DUP

07/19/13 12:10

1.00E+OO

87.77

0.00

0.00

TH-228

TRG

07/19/13 10:19

1.00E+OO

111.03

0.00

0.00

TH-228

TRG

07/19/13 10:19

1.00E+OO

109.00

0.00

0.00

TRG

07/19/13 10:30

1.00E+OO

103.20

0.00

0.00

TRG

07/19/13 10:30

1.00E+OO

81.80

0.00

0.00

03

Sample
Aliquot

Radiometric
%Rec

Nuclide

SAF

SeptO
Date/Time

Sep t1
DalerTime

04

Work Order: 13-07154-ThlS0-1

Lab
Fraction

---~--

Printed: 8/14/2013 4:27 PM

Page 2 of 3

Preliminary Data Report & Analytical Calculations

~-

en

05

!--------

I-

-----

.c

~--

06

TH-228
~-~----

07

TH-228

---- ---------r--

08

TH-228

I DO

07/19/13 12:10

1.00E+OO

87.69

0.00

0.00

09

TH-228

TRG

07/19/13 12:10

1.00E+OO

35.40

0.00

o.oo

10

TH-228

TRG

07/19/13 13:09

1.00E+OO

76.65

0.00

0.00

11

TH-228

TRG

07/19/13 13:09

1.00E+OO

43.40

0.00

0.00

12

TH-228

TRG

07/19/13 00:00

1.00E+OO

74.61

0.00

0.00

07/19/13 00:00

1.00E+OO

63.44

0.00

0.00

---

.5

13

TH-228

TRG
--~--

t:
0

c..
c..
::s

--

f--

(/)

c:

--~--

1---

Cl)

~I

E
Cl)

Cl

111

c:

111

:E
Cl

c:
;:
Cl)
Cl)

.5

Cl

c:

w
~
~

hllt,h~

Uil

---------~-

r------------------- ------ -----


I

Eberline Services
Oak Ridge Laboratory

Printed: 8/14/2013 4:27 PM

Page 3 of 3

Preliminary Data Report & Analytical Calculations

Work Order: 13-07154-ThlS0-1

Lab
Fraction

Nuclide

Sample
Desc

Counting
Date/Time

01

TH-228

LCS

08/14/13 12:46

Halflife
(days)

ii

Detect

Carrier

A_Spec

Alpha_013

Count
Time

Counts

170 2.53 E+02

Bkg
CPM

Eff

9.00 E-03

18.7

c:
:::.

a::

Q)

""

02

""""
0

en

"'

I-

c:
c:t

-..c:

.E
t::
0
c..
c..

08/14/13 12:46

A_Spec

Alpha_014

170.02 -1.08 E+OO

2.40 E-02

18.5

DUP

08/14/13 12:46

A_Spec

Alpha_015

170.02 4.13 E+01

4.00 E-03

14.8

TH-228

TRG

08/14/13 12:46

A_Spec

Alpha_019

170.02 1.17 E+01

2.00 E-03

16.6

TH-228

TRG

08/14/13 12:46

A_Spec

Alpha_022

170.02 4.45 E+OO

1.50 E-02

15.3

TRG

08/14/13 12:46

A_Spec

Alpha_023

170.02 1.94 E+02

2.00 E-03

17.1

---

03

TH-228
--

04

.!!!

0
(.)

MBL

TH-228

05

06

TH-228

07

TH-228

TRG

08/14/13 12:46

A_Spec

Alpha_024

170.02 -3.80 E-01

1.40 E-02

17.1

08

TH-228

DO

08/14/13 12:46

A_Spec

Alpha_025

170.02 6.31 E+01

1.10 E-02

17.4

09

TH-228

TRG

08/14/13 12:46

A_Spec

Alpha_027

170.02 -8.90 E-01

1.70 E-02

17.3

10

TH-228

TRG

08/14/13 12:46

A_Spec

Alpha_029

170.02 -7.20 E-01

1.60 E-02

19.5

11

TH-228

TRG

08/14/13 12:46

A_Spec

Alpha_031

170 9.80 E-01

6.00 E-03

14.2

12

TH-228

TRG

08/14/13 12:46

A_Spec

Alpha_033

170 5.85 E+01

3.00 E-03

18.5

13

TH-228

TRG

08/14/13 12:47

A_Spec

Alpha_034

170 6.83 E+OO

1.00 E-03

18.6

- - - - -------------

::I

(/)

c:

- - - !-------

Cll

t:

Q)

Cll

(.)

111

::::

en

c:

111

:ii:
en
c:
;;:
Cll
Cll

.5

en

c:

w
C!l~
Wiii<

..J

en

----~-

+~

1-----

t=
!

I
- - - - - - ~-----------T

Alo B, Cor

,:

a::

"C""'"

Printed: 8/14/2013 4:27 PM

Page 1 of 3

Preliminary Data Report & Analytical Calculations

Eberline Services
Oak Ridge Laboratory

Work Order: 13-07154-ThlS0-1

LCS
Known

LCS
%R

LCS
Flag

78.91

OK

RPO
Flag

MDA
Flag

Lab
Fraction

Nuclide

Sample
Desc

Client
Identification

Activity
Units

01

TH-230

LCS

LCS

pCi/I

4.35E+OO

8.16E-01

8.98E-02

02

TH-230

MBL

BLANK

pCi/I

8.13E-02

8.48E-02

1.06E-01

03

TH-230

DUP

PZ-107-SS TOT

pCi/I

1.32E+OO

4.10E-01

1.15E-01

04

TH-230

TRG

PZ-200-SS TOT

pCi/I

4.61E-01 I

1.79E-01

8.64E-02

OK

05

TH-230

TRG

PZ-200-SS DIS

pCl/I

1.42E-01 I

1.08E-01

1.24E-01

OK

TH-230

TRG

PZ-102-SS TOT

pCi/I

2.88E+OO

6.31E-01

9.01E-02

OK

TH-230

TRG

PZ-102-SS DIS

pCUI

1.86E-01

1.29E-01

1.25E-01

OK

TH-230

DO

PZ-107-SS TOT

pCi/I

1.66E+OO

4.49E-01

9.84E-02

OK

TH-230

TRG

PZ-107-SS DIS

pCi/I

3.17E-01

2.73E-01

3.19E-01

OK

TH-230

TRG

PZ-106-KS TOT

pCi/I

1.36E-01

1.02E-01

8.51E-02

OK

TH-230

TRG

PZ-106-KS DIS

pCi/I

6.43E-02

1.23E-01

2.26E-01

OK

TH-230

TRG

DUP 08 TOT

pCi/I

1.33E+OO

4.02E-01

1.15E-01

OK

TH-230

TRG

DUP 08 DIS

pCi/I

2.48E-01

1.61E-01

1.35E-01

OK

Results

Error Estimate

MDA

5.51E+OO

OK
OK

>-----

NA

OK

-------- -

.!!!
~

cuc::

ct

-----

en

.c

--------- - -

06

~------L--

07
-------~---

08
~----

-----

-----

09
~

10
----~

~-

11
------

.,

____

12
- - - - ----

c..i

.E

13
-- -----

i'
0

a.
a.

------~

--

--------

Cll

----- --- --

::J

I/)

c:

c:
Cll
E

Cl

Ill

c:

Ill

::!!

--

Cl

c:

;:

-----

Cll
Cll

c:

c,
c:
w
Q~I

......

JI
"'.Ji

'--

Blank
Flag

OK

Eberline Services
Oak Ridge Laboratory

~~
~1

~I
II)

Work Order: 13-07154-ThlS0-1

Lab
Fraction

Nuclide

01

TH-230

02

TH-230

en
-

..c:

03

TH-230

04

TH-230

05

TH-230

06

TH-230

Mean
%Rec

Grav
%Rec

Radiometric
%Rec

Sample
Date

LCS

07/24/13 00:00

1.00E+OO

75.64

0.00

0.00

07/24/13 00:00

1.00E+OO

76.40

0.00

0.00

07/19/13 12:10

1.00E+OO

87.77

0.00

0.00

07/19/13 10:19

1.00E+OO

111.03

0.00

0.00

07/19/13 10:19

1.00E+OO

109.00

0.00

0.00

07/19/13 10:30

1.00E+OO

103.20

0.00

0.00

07/19/13 10:30

1.00E+OO

81.80

0.00

0.00

MBL
-~--

SAF

f--

DUP

t----
1

TRG

+----
1

T~-~-

~-----

TH-230

--r
I

I
I

TRG
'

---

TRG

----

07

Sample
Aliquot

Sample
Desc

-- ----- --------
-

Printed: 8/14/2013 4:27 PM

Page 2 of 3

Preliminary Data Report & Analytical Calculations

-------~

08

TH-230

DO

07/19/13 12:10

1.00E+OO

87.69

0.00

0.00

09

TH-230

TRG

07/19/13 12:10

1.00E+OO

35.40

0.00

0.00

10

TH-230

TRG

07/19/13 13:09

1.00E+OO

76.65

0.00

0.00

11

TH-230

TRG

07/19/13 13:09

1.00E+OO

43.40

0.00

0.00

TRG

07/19/13 00:00

1.00E+OO

74.61

0.00

0.00

07/19/13 00:00

1.00E+OO

63.44

0.00

0.00

12

TH-230

- -t--

=
~

13

Ill

QI

E
QI

01

"'c:
"'
::!!!:

01

c:
;:
QI
QI

c:

c;,

--t--

t_

I
I

'~

1
~~J

!))

--

I
I

- - - - - -----------

~------
________ _)_ _______ -

c:

----1----
I

::I

.....c:

TRG
I

c.
c.

_,
~I

TH-230

- - - - - - - - - - - - r----------- -

-~----

SeptO
Date/Time

Sep t1
Date/Time

Eberline Services
Oak Ridge Laboratory

Lab

Fraction

01

Printed: 8/14/2013 4:27 PM

Page 3 of 3

Preliminary Data Report & Analytical Calculations

Work Order: 13-07154-ThlS0-1

Nuclide

Sample
Desc

Counting
Date/Time

TH-230

LCS

08/14/13 12:46

TH-230

MBL

08/14/13 12:46

Halflife
(days)

Count
Time

Bkg
CPM

Counts

Eff

Detect

Carrier

A_Spec

Alpha_013

170 2.32 E+02

2.00 E-03

18.7

A_Spec

Alpha_014

170.02 4.32 E+OO

4.00 E-03

18.5

A_Spec

Alpha_015

170.02 6.43 E+01

4.00 E-03

14.8

A to B, Cor

- - !------

02

a::

"""""

f-----l-------
03

TH-230

DUP

08/14/13 12:46

!-------------- ------------

.!!/

~
iU
c:
ct

UJ

..c

I-

j__

----

04

TH-230

TRG

08/14/13 12:46

A_Spec

Alpha_019

170.02 3.20 E+01

0.00 E+OO

16.6

TH-230

TRG

08/14/13 12:46

A_Spec

Alpha_022

170.02 8.96 E+OO

1.20 E-02

15.3

TH-230

TRG

08/14/13 12:46

A_Spec

Alpha_023

170.02 1.91 E+02

5.00 E-03

17.1

TRG

08/14/13 12:46

A_Spec

Alpha_024

170.02 9.81 E+OO

7.00

E~03

17.1

TH-230

DO

08/14/13 12:46

A_Spec

Alpha_025

170.02 9.53 E+01

4.00 E-03

17.4

TH-230

TRG

08/14/13 12:46

A_Spec

Alpha_027

170.02 7.30 E+OO

1.00 E-02

17.3

TH-230

TRG

08/14/13 12:46

A_Spec

Alpha_029

170.02 7.66 E+OO

2.00 E-03

19.5

11

TH-230

TRG

08/14/13 12:46

A_Spec

Alpha_031

170 1.49 E+OO

3.00 E-03

14.2

12

TH-230

TRG

08/14/13 12:46

A_Spec

Alpha_033

170 6.90 E+01

0.00 E+OO

18.5

TH-230

TRG

08/14/13 12:47

A_Spec

Alpha_034

170 1.10 E+01

0.00 E+OO

18.6

~<>s--r

os-r -
I

----07_j_____
------

08
---

---------

II------

09
--~-~---

10

TH-230

-------r
I

1-----------

-- r----

------1---

.5

t:

13

----------- -----------

Q.
Q.

-------

----

:s

-
-------+ ---- -

(/)

Cll

E
Cll

Cl

ca
c
ca

:ii:
Cl
c

~--+---------

c:
Cll
Cll

c
c

'Ci

w
~~:~1

n--

...,JI
U)

--------- ---

a::

Lab
Fraction

Nuclide

01

TH-232

02

"""'"

Work Order: 13-07154-ThlS0-1


I Sample
,

LCS
Known

LCS
%R

LCS
Flag

93.30

OK

RPO
Flag

MDA
Flag

Client
Identification

Activity
Units

LCS

pCi/I

4.63E+OO

8.SSE-01

7.82E-02

BLANK

pCi/I

4.36E-02

6.SSE-02

1.06E-01

DUP

PZ-107-SS TOT

pCi/I

1.28E+OO

4.02E-01

8.53E-02

PZ-200-SS TOT

pCi/I

2.40E-01

1.23E-01

6.88E-02

OK

PZ-200-SS DIS

pCl/I

2.36E-02

4.51E-02

8.33E-02

OK

TRG

PZ-102-SS TOT

pCi/I

2.71E+OO

6.02E-01

7.88E-02

OK

PZ-102-SS DIS

pCi/I

-1.61E-02

3.98E-02

1.13E-01

OK

PZ-107-SS TOT

pCi/I

1.38E+OO

3.93E-01

1.04E-01

OK

PZ-107-SS DIS

pCl/I

3.51E-02

1.26E-01

2.85E-01

OK

Desc

LCS

TH-232=

t---

Printed: 8/14/2013 4:27 PM

Page 1 of 3

Preliminary Data Report & Analytical Calculations

Eberline Services
Oak Ridge Laboratory

03

TH-232

04

TH-232

en

05

TH-232

.c

06

TH-232

r=~

TH-232

TRG

Results

Error Estimate

MDA

4.96E+OO

Blank
Flag

OK

--------~--

OK

NA

OK

OK

r-

{l
0
u
.!!!

;;;~
c:
ct

I-

07

- - - - - - - - -----

08

TH-232

DO

09

TH-232

TRG

~-

--

c.i
.E

~I

u,

E
QI

Cl

"'c:
:a:"'

PZ-106-KS TOT

pCi/I

3.22E-02

6.26E-02

1.17E-01

OK

11

TH-232

TRG

PZ-106-KS DIS

pCi/I

4.95E-02

1.24E-01

2.58E-01

OK

12

TH-232

TRG

DUP 08 TOT

pCi/I

1.57E+OO

4.SOE-01

8.02E-02

OK

TH-232

-+-TRG

DUP 08 DIS

pCi/I

4.12E-02

6.34E-02

9.39E-02

OK

--

QI

TRG

13

Q.
Q.
:I
U)

c:

TH-232

-----~

10

----

-------~---

~----

~- =i~

----- -------

----

----- --1- ------r---

---1-----+
------

~------

~----

----------~+--

I
~~
.....

(~Ji
~!!!ll

Work Order: 13-07154-ThlS0-1

Mean
%Rec

Grav
%Rec

Nuclide

Sample
Desc

Sample
Date

01

TH-232

LCS

07/24/13 00:00

1.00E+OO

75.64

0.00

0.00

02

TH-232

MBL

07/24/13 00:00

1.00E+OO

76.40

0.00

0.00

TH-232

DUP

07/19/13 12:10

1.00E+OO

87.77

0.00

0.00

04

TH-232

TRG

07/19/13 10:19

1.00E+OO

111.03

0.00

0.00

en

05

TH-232

TRG

07/19/13 10:19

1.00E+OO

109.00

0.00

0.00

.c

06

TH-232

TRG

07/19/1310:30

1.00E+OO

103.20

0.00

0.00

07

TH-232

TRG

07/19/13 10:30

1.00E+OO

81.80

0.00

0.00

08

TH-232

DO

07/19/13 12:10

1.00E+OO

87.69

0.00

0.00

t:

09

TH-232

TRG

07/19/13 12:10

1.00E+OO

35.40

0.00

0.00

10

TH-232

TRG

07/19/13 13:09

1.00E+OO

76.65

0.00

0.00

11

TH-232

TRG

07/19113 13:09

1.00E+OO

43.40

0.00

0.00

&

""""

Sample
Aliquot

Radiometric
%Rec

Lab
Fraction

s:::

SAF

--

03
----

"'0

"tl
(.)

.!!!

..."'

s:::

q;

I-

...

-e
0

<%

.Q

IU

.5

12

TH-232

TRG

07/19/13 00:00

1.00E+OO

74.61

0.00

0.00

13

TH-232

TRG

07/19/13 00:00

1.00E+OO

63.44

0.00

0.00

~
0

Q.
Q.

:I

"'....c:

Q)

i: I

~I

E
Q)

Cl

"'c:
:::!!
"'

Cl

c:

;::
Q)

Q)

c:

c,
c:

w
lf:i:!ll

.....

(')rJ1

...

----- -

Printed: 8/14/2013 4:27 PM

Page 2 of 3

Preliminary Data Report & Analytical Calculations

Eberline Services
Oak Ridge Laboratory

----

Sep to
Date/Time

Sep t1
DatefTime

Lab
Fraction

01

a:

02
"'l""9

....-------------

Work Order: 13-07154-ThlS0-1

Sample
Oesc

Counting
DatefTime

LCS

Count
Time

Counts

Bkg
CPM

Eff

Carrier

08/14/13 12:46

A_Spec

Alpha_013

170 2.47 E+02

1.00 E-03

18.7

08/14/13 12:46

A_Spec

Alpha_014

170.02 2.32 E+OO

4.00 E-03

18.5

DUP

08/14/13 12:46

A_Spec

Alpha_015

170.02 6.28 E+01

1.00 E-03

14.8

TRG

08/14/13 12:46

A_Spec

Alpha_019

170.02 1.67 E+01

2.00 E-03

16.6

TH-232

TRG

08/14/13 12:46

A_Spec

Alpha_022

170.02 1.49 E+OO

3.00 E-03

15.3

TH-232

TRG

08/14/13 12:46

A_Spec

Alpha_023

170.02 1.80 E+02

3.00 E-03

17.1

TRG

08/14/13 12:46

A_Spec

Alpha_024

170.02 -8.50 E-01

5.00 E-03

17.1

TH-232

-----------~

Halflife
(days)

Detect

Nuclide

~------

Printed: 8/14/2013 4:27 PM

Page 3 of 3

Preliminary Data Report & Analytical Calculations

Eberline Services
Oak Ridge Laboratory

~l-

TH-232
--- -----------

03

TH-232

Ato B, Cor

- - - -----------

~
0

.!!!

~
iii
i::

<:(

04

TH-232
-------

en

.c

I-

05
--

06
-----

07

TH-232

--

08

TH-232

DO

08/14/13 12:46

A_Spec

Alpha_025

170.02 7.90 E+01

0.00 E+OO

17.4

09

TH-232

TRG

08/14/13 12:46

A_Spec

Alpha_027

170.02 8.10 E-01

7.00 E-03

17.3

10

TH-232

TRG

08/14/13 12:46

A_Spec

Alpha_029

170.02 1.81 E+OO

7.00 E-03

19.5

11

TH-232

TRG

08/14/13 12:46

A_Spec

Alpha_031

170 1.15 E+OO

5.00 E-03

14.2

- -- - - - - -

- - f-

12

TH-232

------

.E

t:'
0

c..
c..

::I

(/)

c:

GI

~I

GI
Cl

.,,
.,,c:

:::.?:
Cl

c:

;:
GI
GI

c:

'Ci
c:

w
Ciii.!11
II-'~'

t,)r.)1
fl,~

TRG

08/14/13 12:46

A_Spec

Alpha_033

170 8.18 E+01

1.00 E-03

18.5

TRG

08/14/1312:47

A_Spec

Alpha_034

170 1.83 E+OO

1.00 E-03

18.6

- ----------

13

TH-232

-----1-- --

---+-
-3
~---=~-=-1

'

'

----------t-- -
I

Count Room Report


Client: Engineering Management Su

13-07154-ThlS0-1 (pCi/I} in WA

Printed: 811412013 5:58 AM


Page 1of1

TracerlD: Th-18a

../\ \,
/
,-,

")

Internal
Fraction

Sample
Desc

Client
ID

Sample
Date

.
~

'

01

LCS

02

MB~1

03

DUP

LCS

01124113

oo:oo

Tracer
Aliquot(g)

Tracer
ACT(dpm)

'
I

Sample
Aliquot

1.0000

0.4800

10.7837

0.00
0.00

1.0000

0.2373

5.3312

PZ-107-SS TOT

07/19/1312:10

1.0000

0.2369

5.3222

0.00

TRG

05

TRG

TRG

07

TRG
__ _______
DO

09

TRG

PZ-200-SS TOT

07/19/13 10:19

1.0000

0.2345

5.2683

0.00

PZ-200-SS DIS

07/19/13 10:19

1.0000

0.2339

5.2548

0.00

---

PZ-102-SS TOT

07/19/1310:30

1.0000

0.2354

5.2885

0.00

PZ-102-SS DIS

07/19/13 10:30

1.0000

0.2320

5.2121

0.00

PZ-107-SS TOT

07/19/1312:10

1.0000

0.2328

5.2301

0.00

PZ-107-SS DIS

07/19/1312:10

1.0000

0.2361

5.3042

0.00

,,

08

----

06

SAF
1*

07/24/13 00:00

04

Radiometric
%Rec

BLANK

!I

Radiometric
Tracer (pCi)

i
-

I')

iJ
I

10

TRG

PZ-106-KS TOT

07/19/13 13:09

1.0000

0.2338

5.2526

0.00

11

TRG

PZ-106-KS DIS

07/19/1313:09

1.0000

0.2346

5.2705

0.00

12

TRG

DUP 08 TOT

07/19/13 00:00

1.0000

0.2345

5.2683

0.00

DUP 08 DIS

07/19/13 00:00

1.0000

0.2350

5.2795

0.00

--

13

I
I

TRG

f'11;~

!>'""
(~)

(.,i,J\

SAF
2*

Eberline Services
Oak Ridge Laboratory

Isotope

Sol#

Th-228

Th-Sb

Th-230

Th-1b

Th-232

Th-Sb

..

___j_

Activity
dpmlg

103.560

Solution
Date

Approx
Addition

S/S/2013

0.100

Analysis Code

Date

Technician

Thi SO

8/8/2013 7:45

JWOLFE

LCS

MS

LCSD

- '41811. -

Volume
Used(g)

Volume
Used(g)

Volume
Used(g)

Volume
Used(g)

0.5202

103.560

S/S/2013

0.100

0.1-063

4.96r--0.179 ..

Tracf!"' .._.
Isotope

01

Th-229

02

Th-229

03

Th-229

!
i

Sol#

Solution
Date

Volume
Used(g}

Approx
Addition

Th-1Sa

22.466

S/S/2013

0.4800

0.2200

Th-1Sa

22.466

S/S/2013

0.2373

0.2200

Th-1Sa

22.466

S/S/2013

0.2369

0.2200

Th-1Sa

22.466

S/S/2013

0.2345

0.2200

Th-1Sa

22.466

S/S/2013

0.2339

0.2200

Th-18a

22.466

S/S/2013

Th-229

05

Th-229

06

Th-229

o.2354

0.2200

07

Th-229

Th-1Sa

22.466

S/S/2013

0.2320

0.2200

08

Th-229

Th-1Sa

22.466

S/S/2013

0.2328

0.2200

09

Th-229

Th-1Sa

22.466

S/S/2013

0.2361

0.2200

10

Th-229

Th-1Sa

22.466

S/S/2013

-0.2338

0.2200

11

Th-229

Th-1Sa

22.466

S/S/2013

0;234i>

0.2200

12

Th-229

Th-1Sa

22.466

S/S/2013

0.2345

0.2200

13

Th-229

Th-18a

22.466

S/S/2013

0.2350

0.2200

i
I

.....
()()
i~

-.

Tracer

Added
pCi

LCSO

Error
Estimate

Known
pCi

0.00

0.000

o.ooj
o.oor-

0.00

0.000

o.ool

0.00

0.000

MSO

Error
Estimate

Added
pCi

0.000

Version 2.0 OS/99

Error
Estimate

0.00

0.000

0 000

0.00

0.000

0.000

0.00

0.000

Balance Pripte~Tap~s
LCS

'''

04

11,il~

0.179

5.511--0-1~9

0.500

Activity
dpmlg

Error
Estimate

4.96.

S/S/2013

Witness Initials

~f4S.

(."CS
Known
pCi

0.1063

23.525

..

fraction

Page 1of1
Printed: 8/8/2013 7:46 AM

Spike and Tracer Worksheet

Matrix Spike

Eberline Analytical
Oak Ridge Laboratory

Lab
Fraction
01
02
03
04
05
06
07
08
09
10
11
12
13

Engineering Management Support, Inc.

Client ID
LCS
BLANK
PZ-107-SS TOT
PZ-200-SS TOT
PZ-200-SS DIS
PZ-102-SS TOT
PZ-102-SS DIS
PZ-107-SS TOT
PZ-107-SS DIS
PZ-106-KS TOT
PZ-106-KS DIS
DUP 08 TOT
DUP 08 DIS

Sample
Type
LCS
MBL
DUP
TRG
TRG
TRG
TRG
DO
TRG
TRG
TRG
TRG
TRG

Analysis Code

Rpt Units

Lab Deadline

Technician

Thi SO

liters

8/13/2013

JWOLFE

Dilution Data

Muffle Data

Aliquot Data

NoofD!ls

Oil F.actor

Ratio

./

...

.
.

.
<.

"

.
.

..

..

.
I

.
..

..

(ii!~!
~tt1.lt.

m
U11

Technician:

1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
-
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO

NCltEquiv

1.UOOOE+OO
1.0000E+oo
1.0f)Of)Ei:OO
1-0GOOE+OO
1.0000~+00

1:OOOOE"+OO
1.00QpE.f()fl
1.0000E+Qfl
1:000~+00
1.0000E+OO
1.0000E+QO
1.0oOQE+OO
1.ooooE+oo

Aliquot

Net Equiv

H3 Dist
Aliq
-

--

--

--

--

.:

I
, JL.Jd~

Aliquot

H-3 Solids Only


Water Added
(ml)

..

Comments

MS Aliquot Data

..

Ratio
Post/Pre

...

Printed: 8/8/2013 7:46 AM


Page 1of1

Aliquot Worksheet

Date

__'ir~_}b-

Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:

SPIKE
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000661
1307154A-TH
01
Shelf 2
Th iso

Detector Name:
Chamber Serial Number:
Detector Serial Number:
Env. Background:
Reagent Blank:

Alpha_013
13
System Bkgd 64769
<not performed>

Sample Size:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:

1.000E+OOO +/- O.OOOE+OOO liter


8/14/2013
7:22:05 AM
8/14/2013 12:46:13 PM
170.0 minutes
170.0 minutes

Tracer Certificate:
Tracer Quantity:
Effective Efficiency:
Counting Efficiency:
Chem. Recovery Factor:

Th229 TH-18A
0.480 mL
0.1414 +/0.0098
0.1869 +/0.0035 on 12/15/2012 11:26:45 AM
0.7564 +/0.0544

Control Certificate Name: NatTh Th-8


Chem. Recov. of Control:
TH-232
Peak Match Tolerance:
0.175 MeV

PEAK
Energy
(MeV)

Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232

5.827
5.376
4.894
4.634
3.966

Net
Pk Area
9.30
253.47
259.15
231.66
246.83

0.932977 +/-

AREA

0.092309

REPORT
FWHM
(keV)

Pk Area
Error %

Ambient
Backgnd

Reagent
Backgnd

70.81
12.35
12.20
12.89
12.48

1. 70
1. 53
0.85
0.34
0.17

O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

0.0
21. 5
4.8
25.3
4.6

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS


Nuclide

Id
Conf.

Energy
(keV)

TH-227
TH-228
TH-229
TH-230
TH-232

0.997
0.997
0.998
0.992
0.995

5850.00*
5400.00*
4872.00*
4672.00*
3997.00*

Activity
(pCi/liter )
1.79E-001
4.75E+OOO
4.88E+OOO
4.35E+OOO
4.63E+OOO

+/
+/
+/
+/
+/

l.29E-001
8.75E-001
6.65E-001
8.16E-001
8.55E-001

MDA
(pCi/liter
1.41E-001
1.33E-001
1.13E-001
8.98E-002
7.82E-002

+/
+/
+/
+/
+/

1. 92E-002
1. 82E-002
1. 54E-002
l.22E-002
1. 07E-002

-/'<j
~/14--/13
t'ii1S6

0000066194.CNF

Live Ti me :10200. 000 sec


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.A

~/""\pexSample Description:

Spectrum File:

Batch Identification:

Sample Identification:

Sample Geometry:

Procedure Description:

Al pha

TM

BLANK
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000661
1307154A-TH
02
Shelf 2
Th iso

Detector Name:

Alpha_Ol4
Chamber Serial Number:

Detector Serial Number:


14
Env. Background:

System Bkgd 64770


Reagent Blank:

<not performed>
Sample Size:

Sample Date/Time:

Acquisition Date/Time:

Acquisition Live Time:

Acquisition Real Time:

l.OOOE+OOO +/- O.OOOE+OOO liter


8/14/2013
7:22:05 AM
8/14/2013 12:46:14 PM
170.0 minutes
170.0 minutes

Tracer Certificate:

Tracer Quantity:

Effective Efficiency:

Counting Efficiency:

Chem. Recovery Factor:

Th229 TH-18A
0.237 mL

0.1410 +/0.0133

0.1846 +/0.0034 on 12/15/2012 11:26:44 AM


0.7640 +/0.0733

Peak Match Tolerance:

0.175 MeV

PEAK
Energy
(MeV)

Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232

5.873
5.362
4.883
4.684
3.960

Net
Pk Area
5.28
-1. 08
127.81
4.32
2.32

AREA

REPORT

Pk Area
Error %

Ambient
Backgnd

107.99
348.68
17.43
102.62
149.13

2.72
4.08
1.19
0.68
0.68

Reagent
Backgnd

FWHM
(keV)

O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

2.9
2.9
4.7
2.9
2.9

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS

Nuclide

Id
Conf.

Energy
(keV)

TH-227
TH-228
TH-229
TH-230
TH-232

0.997
0.992
0.999
0.999
0.993

5850.00*
5400.00*
4872.00*
4672.00*
3997.00*

Activity
(pCi/liter )
l.02E-001
-2.03E-002
2.41E+OOO
8.13E-002
4.36E-002

+/+/+/+/+/-

l. llE- 001
7.09E-002
4.45E-001
8.48E-002
6.55E-002

MDA
(pCi/liter
l.65E-001
l.86E-001
1. 24E- 001
1. 06E- 001
l.06E-001

+/+/+/+/+/-

3.05E-002
3.43E-002
2.30E-002
l.96E-002
l.96E-002

I'(;

'bf 1'4 13
ii191

0000066168.CNF

Live Time :10201.000 sec


Real Time :10201.000 sec
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stop : 1024:6512.2(kev)
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0

S19t1

Channel Data Report


801:

8/14/2013
0

Sample Title:

3:48:54
0

Page

PM
0

02

Channell------l-------l-------l-------1-------1-------1-------l-------I
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1
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0
0
0
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0
0
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0
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0
0
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0
0
0
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0
0
0
0
0
1
0
0
0
0
0
1
0
0
0
0
0
0
0

~195

Sample Description:

Spectrum File:

Batch Identification:

Sample Identification:

Sample Geometry:

Procedure Description:

PZ-107-SS TOT
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000661
1307154A-TH
03
Shelf 2
Th iso

Detector Name:

Alpha_015
Chamber Serial Number:

Detector Serial Number:


15
Env. Background:

System Bkgd 64771


Reagent Blank:

<not performed>
Sample Size:

Sample Date/Time:

Acquisition Date/Time:

Acquisition Live Time:

Acquisition Real Time:

1.000E+OOO +/- O.OOOE+OOO liter


7/19/2013
7:22:05 AM
8/14/2013 12:46:15 PM
170.0 minutes
170.0 minutes

Tracer Certificate:

Tracer Quantity:

Effective Efficiency:

Counting Efficiency:

Chem. Recovery Factor:

Th229 TH-18A
0.237 mL

0.1297 +/- 0.0127

0.1477 +/- 0.0027 on 7/20/2013


0.8777 +/- 0.0872

Peak Match Tolerance:

0.175 MeV

PEAK
Energy
(MeV)

Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232

5.763
5.391
4.878
4.648
3. 971

Net
Pk Area

AREA

REPORT

Pk Area
Error %

1.15
41.32
117.32
64.32
62.83

6:27:27 PM

Ambient
Backgnd

Reagent
Backgnd

0.85
0.68
0.68
0.68
0.17

O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

249.60
30.78
18.16
24.59
24.77

FWHM
(keV)
3.0
4.4
3.6
18.0
4.0

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS


Nuclide

Id
Conf.

Energy
(keV)

TH-227
TH-228
TH-229
TH-230
TH-232

0.961
1.000
1. 000
0.997
0.997

5850.00*
5400.00*
4872.00*
4672.00*
3997.00*

Activity
(pCi/liter )
2.42E-002
8.67E-001
2.41E+OOO
1.32E+OOO
1.28E+OOO

+/+/+/+/+/-

6.05E-002
3.14E-001
4.61E-001
4.lOE-001
4.02E-001

MDA
(pCi/liter
1.26E-001
1.18E-001
1.16E-001
1.15E-001
8.53E-002

+/+/+/+/+/-

2.41E-002
2.27E-002
2.22E-002
2.21E-002
1.63E-002

PrG

~It.Ff!J

_EJ 1 SS

0000066169.CNF

Live Time 10201.000 sec


Real Time 10201.000 sec
Start:
1 3490. B(kev)
Stop : 1024 6558. B(kev)
Acq. Start wed Aug 14 12:46:15 2013

60
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40

35

VI
.f-1

c:

:::::s

8 30

25
20
15
10
5
0
3500

1.

4000

4500

&;l~I
~-~
C,~)

.,,,,,M

ROI Type: 1

5000

Energy(kev)

5500

6000
ROI Type: 3

6500

Channel Data Report

8/14/2013

Page

3:49:01 PM

*******************************************************
s P E C T R A L DAT A R E P 0 R T *****
*****
*******************************************************
Sample Title:

03

Elapsed Live time:


Elapsed Real Time:

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1
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2
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5
2
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1
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0
3
3
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0
3
0
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1
3
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4
1
1
1
1
0
1
2
0
0
0
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1
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0
0
0
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0
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199

Channel Data Report


801:

8/14/2013
0

Sample Title:

3:49:01 PM
0

Page
0

03

Channell------l-------l-------l-------1-------1-------1-------l-------I
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913:
921:
929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:

0
0
0
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0
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0
0
0
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0

0
0
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0
0

0
0
0
0
0
0
0
0
0
0
0
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0
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0
0
0
0
0
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0
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0

0
0
0
0
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0
0
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0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
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0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
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0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
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0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

~~.Apex-Alpha'"

Sample Description:
Spectrum File:
Batch Identification:

Sample Identification:

Sample Geometry:

Procedure Description:

PZ-200-SS TOT
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000661
1307154A-TH

04

Shelf 2

Th iso

Detector Name:

Alpha_Ol9
Chamber Serial Number:

Detector Serial Number:


19

Env. Background:

System Bkgd 64773

Reagent Blank:

<not performed>

Sample Size:

Sample Date/Time:

Acquisition Date/Time:

Acquisition Live Time:

Acquisition Real Time:

l.OOOE+OOO +/- O.OOOE+OOO liter

7/19/2013
7:22:05 AM

8/14/2013 12:46:39 PM

170.0 minutes
170.0 minutes

Tracer Certificate:

Tracer Quantity:

Effective Efficiency:

Counting Efficiency:

Chem. Recovery Factor:

Th229 TH-18A
0.235 mL
0.1842 +/0.0155
0.1659 +/0.0029 on 2/17/2013
1.1103 +/0.0953

Peak Match Tolerance:

0.175 MeV

PEAK
Energy
(MeV)

Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232

5.914
5.358
4.877
4.636
3.973

Net
Pk Area

AREA

REPORT

Pk Area
Error %

1. 64
11. 66
165.00
32.00
16.66

10:45:23 AM

214.85
58.37
15.30
35.19
48.59

Ambient
Backgnd
1. 36
0.34
0.00
0.00
0.34

FWHM
(keV)

Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

3.3
3.3
7.9
5.6
5.0

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS

Nuclide

Id
Conf.

Energy
(keV)

TH-227
TH-228
TH-229
TH-230
TH-232

0.979
0.991
1. 000
0.993
0.997

5850.00*
5400.00*
4872.00*
4672.00*
3997.00*

Activity
(pCi/liter )
2.42E-002
l.72E-001
2.38E+OOO
4.61E-001
2.40E-001

+/
+/
+/
+/
+/

5.22E-002
l.04E-001
3.93E-001
1. 79E-001
1. 23E-001

A6

~/ti/f3

MDA
(pCi/liter
l.OlE-001
7.06E-002
8.67E-002
8.64E-002
6.88E-002

+/+/+/+/+/-

l.67E-002
l.16E-002
l.43E-002
l.42E-002
l.13E-002

0000066170.CNF
Live Time :10201.000 sec
Real Time :10201.000 sec
1:3279.3(kev)

Start:
stop : 1024:6687 .O(kev)

Acq. Start :wed Aug 14 12:46:39 2013

60+
55

50

45

40

35

V)

......
c:
::::s

8 30

25
20
15
10

3500
~lll
~~
~1'2ll
HI'~~)

.~ !,

4000

ROI Type: 1

4500

5000

Energy(kev)

5500

6000

6500

ROI Type: 3

Channel Data Report

8/14/2013

Page

3:49:08 PM

*******************************************************
s p E C T R A L DAT A R E P 0 R T *****
*****
*******************************************************
Sample Title:

04

Elapsed Live time:


Elapsed Real Time:

10201
10201

Channell------l-------l-------1-------1-------1-------l-------l-------I
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0
0
0
0
0
0
0
0
0
0
0
2
0
0
1
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
1
0
1
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
1

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0

B283

Channel Data Report


369:

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0

Sample Title:

3:49:08
1

Page

PM
0

04

Channell------l-------l-------l-------1-------1-------1-------l-------I
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681:
689:
697:
705:
713:
721:
729:
737:
745:
753:
761:
769:
777:
785:
793:

0
0
0
0
0
1
0
0
2
0
5
7
5
0
1
3
3
1
1
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0
0
0
0
0
1
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0
0
0
0
0
0
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0
0
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0
0
0
0
0
0
0
0
0
0

0
1
1
0
2
3
0
0
1
2
3
3
3
2
2
2
3
1
0
1
0
0
0
0
0
0
0
0
0
1
0
0
2
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
1
0
1
0
0
0
1
3
4
2
3
0
1
0
1
0
2
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
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0
0
0
0
0
0
0
0
0
1
0
0

0
0
0
0
1
2
0
0
2
1
4
2
2
1
2
4
1
1
1
1
0
0
0
0
0
0
0
0
0
0
0
0
2
0
0
1
0
0
0
0
1
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0
0
0
0
0
0
0
0
0
0
0

0
0
0
1
2
4
0
0
1
0
2
3
1
1
3
1
2
0
1
1
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0

0
1
1
1
0
1
1
1
2
1
1
5
2
0
1
3
2
0
2
2
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
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0
1
0
0
0
0
0
0
0
0
0
0

0
0
0
0
1
0
0
0
0
2
2
3
4
2
2
1
2
0
1
0
0
0
0
0
0
0
0
0
0
0
1
1
0
0
0
0
0
0
0
0
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0
0
0
0
0
0
0
0
0
0

0
1
0
0
2
0
0
0
2
3
5
2
1
2
1
1
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
1
0
0
0
0
0
0
0
1
0
1
0
0
0
0
0
1
0
0
0
0

_211

Channel Data Report


801:

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0

Sample Title:

3:49:08
0

Page

PM
0

04

Channell------l-------l-------l-------l-------1-------1-------1-------I
809:
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881:
889:
897:
905:
913:
921:
929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

.~!t'.Apex-Alpha'"

Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:

PZ-200-SS DIS
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000661
1307154A-TH
05
Shelf 2
Th iso

Detector Name:
Chamber Serial Number:
Detector Serial Number:
Env. Background:
Reagent Blank:

Alpha_022
22
System Bkgd 64774
<not performed>

Sample Size:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:

l.OOOE+OOO +/- O.OOOE+OOO liter


7/19/2013
7:22:05 AM
8/14/2013 12:46:40 PM
170.0 minutes
170.0 minutes

Tracer Certificate:
Tracer Quantity:
Effective Efficiency:
Counting Efficiency:
Chem. Recovery Factor:

Th229 TH-18A
0.234 mL
0.1669 +/- 0.0147
0.1531 +/- 0.0029 on 12/15/2012
1. 0900 +/0.0983

Peak Match Tolerance:

0.175 MeV

PEAK
Energy
(MeV)

Nuclide

Net
Pk Area

AREA

1:57:26 PM

REPORT

Pk Area
Error %

Ambient
Backgnd

Reagent
Backgnd

1. 36
2.55
1. 87
2.04
0.51

O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

FWHM
(keV)

-------------------------------------------------------------------------------TH-227
TH-228
TH-229
TH-230
TH-232

5.804
5.398
4.902
4.597
3.993

1. 64
4.45
149.13
8.96
1.49

214.85
120.09
16.17
73.69
190.03

3.1
3.1
12.5
3.1
6.2

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS


Nuclide

Id
Conf.

Energy
(keV)

Activity
(pCi/liter )

MDA

(pCi/liter

-------------------------------------------------------------------------------TH-227
TH-228
TH-229
TH-230
TH-232

0.989
1. 000
0.995
0. 971
1. 000

5850.00*
5400.00*
4872.00*
4672.00*
3997.00*

2.68E-002
7.25E-002
2.38E+OOO
l.42E-001
2.36E-002

+/+/+/+/+/-

5.77E-002
8.80E-002
4.llE-001
l.08E-001
4.51E-002

5/14-( f'J

l.12E-001
l.37E-001
1. 21E-001
l.24E-001
8.33E-002

+/+/+/+/+/-

l.93E-002
2.36E-002
2.09E-002
2.14E-002
1.44E-002

0000066171.CNF

Live Time :10201.000 sec


Real Time :10201.000 sec
start:
1: 3421.S(kev)

stop : 1024:6608.S(kev)

Acq. Start :wed Aug 14 12:46:40 2013

60

55

50

45

40

35

V)

.f-1

s:::

:::J

8 30

25

20

15

10

......
'
I

~
~

"'

I.
I

3500

4000

4500

tf1l!
r-.:i1

ltt1

..,,J

ROI Type: 1

5000
Energy(kev)

rL.

'""

5500

6000
ROI Type: 3

6500

Channel Data Report

8/14/2013

3:49:15

PM

Page

*******************************************************
s p E C T R A L DAT A R E P 0 R T *****
*****
*******************************************************
Sample Title:

05

Elapsed Live time:


Elapsed Real Time:

10201
10201

Channell------l-------l-------1-------1-------1-------l-------l-------I
1:
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10201
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10201
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1
0
0
0
0
1
0
~~fil~

~J!~Q

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681:
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721:
729:
737:
745:
753:
761:
769:
777:
785:
793:

0
0
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1
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0
1
0
0
0
0
0
1
1
1
3
3
2
2
2
2
1
0
1
1
1
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
1
0
1
1
5
5
2
1
1
1
1
1
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
1
0
1
1
1
0
6
5
1
2
2
1
2
0
1
2
0
0
0
0
0
0
0
0
0
0
0
0
0
0
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0
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0
0
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0
0
0
0
0
0

0
0
1
0
1
1
0
1
2
1
4
3
4
1
0
1
0
0
0
1
0
0
0
0
0
0
0
0
0
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1
0
2
0
1
0
0
0
0
0
0
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0
0
0
0
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1
0
1
0

0
0
0
0
0
0
0
0
1
1
3
2
4
0
2
1
0
1
3
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0
0
0
0
0
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1
1
0
4
1
2
2
1
1
0
0
1
0
0
0
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0
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0
0
0
0
0
1
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0
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0
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0
1
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0
0
0
0
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0

1
0
0
0
0
0
1
0
0
0
6
4
0
0
3
0
1
0
2
0
0
0
0
0
0
0
0
0
0
0
0
1
0
1
0
0
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0
0
0
0
0
0
0
0
0
0
0
0

s 2 s-9

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801:

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Sample Title:

3:49:15
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Page

PM
0

05

Channell------1-------1-------1-------l-------l-------l-------l-------I
809:
817:
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833:
841:
849:
857:
865:
873:
881:
889:
897:
905:
913:
921:
929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

~~Apex-Alpha'"

Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:

PZ-102-SS TOT
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000661
1307154A-TH
06
Shelf 2
Th iso

Detector Name:
Chamber Serial Number:
Detector Serial Number:
Env. Background:
Reagent Blank:

Alpha_023
23
System Bkgd 64775
<not performed>

Sample Size:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:

l.OOOE+OOO +/
O.OOOE+OOO liter
7/19/2013
7:22:05 AM
8/14/2013 12:46:41 PM
170.0 minutes
170.0 minutes

Tracer Certificate:
Tracer Quantity:
Effective Efficiency:
Counting Efficiency:
Chem. Recovery Factor:

Th229 TH-18A
0.235 mL
0.1765 +/
0.0151
0.1710 +/
0.0030 on 7/20/2013
1. 0320 +/
0.0899

Peak Match Tolerance:

0.175 MeV

PEAK
Energy
(MeV)

Nuclide

Net
Pk Area

AREA

6:18:25 PM

REPORT

Pk Area
Error %

Ambient
Backgnd

Reagent
Backgnd

FWHM
(keV)

-------------------------------------------------------------------------------TH-227
TH-228
TH-229
TH-230
TH-232

5.876
5. 393

4.909
4.650
3.979

12.15
193.66
158.66
191.15
180.49

58.49
14.10
15.58
14.21
14.61

0.85
0.34
0.34
0.85
0.51

O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

0.0
14.2
4.1
8.3
6.8

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS


Nuclide

Id
Conf.

Energy
(keV)

Activity
(pCi/liter )

MDA

(pCi/liter

-------------------------------------------------------------------------------TH-227
TH-228
TH-229
TH-230
TH-232

0.997
1. 000
0.993
0.997
0.998

5850.00*
5400.00*
4872.00*
4672.00*
3997.00*

l.88E-001
2.99E+OOO
2.39E+OOO
2.88E+OOO
2.71E+OOO

+/+/+/+/+/-

l.14E-001
6.53E-001
4.00E-001
6.31E-001
6.02E-001

9.24E-002
7.37E-002
7.21E-002
9.0lE-002
7.88E-002

+/+/+/+/+/-

l.55E-002
l.23E-002
1.21E-002
l.51E-002
l.32E-002

g/14'/ '3

ti211

0000066172.CNF

Live Time :10201.000 sec


Rea1 Ti me :10201. 000 sec
start:
1:3403.0(kev)
stop : 1024:6588.3(kev)
Acq. Start :wed Aug 14 12:46:41 2013

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~;!II
~JI

le"'"

!\.~

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6000

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s p E C T R A L DAT A R E P 0 R T *****
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ti.213

Channel Data Report


369:

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1
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1
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1
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2
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4
6
1
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1
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0
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0

3
3
2
6
15
1
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2
1
3
1
2
2
0
3
1
1
2
1
2
0
0
0
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3
4
0
3
8
8
1
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1
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2
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3
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6
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3
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1
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1
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1
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1
1
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0

ti214

Channel Data Report


801:

8/14/2013
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3:49:22
0

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0

06

Channell------l-------l-------l-------l-------l-------1-------1-------1
809:
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905:
913:
921:
929:
937:
945:
953:
961:
969:
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985:
993:
1001:
1009:
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0
0
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1
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0
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0
0
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1
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1
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1
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0

0
0
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1
0
0
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1
0
0
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0
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0
0
0
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1

0
0
0
0
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0
0
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0
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1
0
0
0
1
0
0
0
0
0
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0

0
0
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0
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0
0
0
0
0
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0
0
0
1
0
0
0
0
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0
0
0
1
1
0
0
0
0
0
1
0
0
0
0
1
0
0
0
0
0
0
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0

0
0
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0
0
0
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1
1
0
1
0
0
0
0
0
0
0
0

~~Apex-Alpha,.

Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:

PZ-102-SS DIS
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000661

1307154A-TH

07

Shelf 2

Th iso

Detector Name:
Chamber Serial Number:

Detector Serial Number:


Env. Background:
Reagent Blank:

Alpha_024

24

System Bkgd 64776

<not performed>

Sample Size:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:

l.OOOE+OOO +/- O.OOOE+OOO liter


7/19/2013
7:22:05 AM

8/14/2013 12:46:42 PM

170.0 minutes

170.0 minutes

Tracer Certificate:
Tracer Quantity:
Effective Efficiency:
Counting Efficiency:
Chem. Recovery Factor:

Th229 TH-18A

0.232 mL

0.1399 +/0.0134

0.1710 +/- 0.0032 on 12/15/2012


0.8180 +/- 0.0799

Peak Match Tolerance:

0.175 MeV

PEAK
Energy
(MeV)

Nuclide

Net
Pk Area

AREA

2:02:15 PM

REPORT

Pk Area
Error %

Ambient
Backgnd

Reagent
Backgnd

FWHM

(keV)

-------------------------------------------------------------------------------TH-227
TH-228
TH-229
TH-230
TH-232

5. 871
5.397
4.854
4.620
3.947

-2.72
-0.38
123.96
9.81
-0.85

87.14
799.43
17.77
66.87
246.67

2.72
2.38
2.04
1.19
0.85

O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

0.0
3.1
5.4
3.1
0.0

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS


Nuclide

Id
Conf.

Energy
(keV)

Activity
(pCi/liter )

MDA

(pCi/liter

-------------------------------------------------------------------------------TH-227
TH-228
TH-229
TH-230
TH-232

0.998
1. 000
0.998
0.986
0.987

5850.00*
5400.00*
4872.00*
4672.00*
3997.00*

-5.30E-002
-7.39E-003
2.36E+OOO
l.86E-001
-l.61E-002

+/+/+/+/+/-

4.72E-002
5.91E-002
4.43E-001
l.29E-001
3.98E-002

l.67E-001
l.59E-001
l.48E-001
l.25E-001
l.13E-001

+/+/+/+/+/-

3.14E-002
2.99E-002
2.78E-002
2.35E-002
2.13E-002

}6
<6f 14f r~

621-6

0000066173.CNF

Live Time :10201.000 sec


Real Time :10201.000 sec
start:
1:3411.6(kev)
stop : 1024:6597 .O(kev)
Acq. start :wed Aug 14 12:46:42 2013

60
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VI
.j...J

c=

::::I

8 30

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'~
t,)
~""
--~1tj~

1\

I l

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5500

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6500

Channel Data Report

8/14/2013

3:49:30

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*******************************************************
s p E CTR AL DAT A R E P 0 R T *****
*****
*******************************************************
Sample Title:

07

Elapsed Live time:


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0
0
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~218

Channel Data Report


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0
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7
0
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3
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0
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1
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,8219

Channel Data Report


801:

8/14/2013
0

Sample Title:

3:49:30
0

Page

PM
0

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Channell------l-------1-------1-------1-------l-------l-------l-------I
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0
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0
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0
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0
0
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0
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0
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1
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0
0
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0
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0
0
0
0
0
0
0
0

~~Apex-Alpha'"

Sample Description:
Spectrum File:
Batch Identification:

Sample Identification:

Sample Geometry:

Procedure Description:

PZ-107-SS TOT
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000661
1307154A-TH
08
Shelf 2
Th iso

Detector Name:

Alpha_025
Chamber Serial Number:

Detector Serial Number:


25
Env. Background:

System Bkgd 64777


Reagent Blank:

<not performed>
Sample Size:

Sample Date/Time:

Acquisition Date/Time:

Acquisition Live Time:

Acquisition Real Time:

l.OOOE+OOO +/- O.OOOE+OOO liter


7/19/2013
7:22:05 AM
8/14/2013 12:46:43 PM
170.0 minutes
170.0 minutes

Tracer Certificate:

Tracer Quantity:

Effective Efficiency:

Counting Efficiency:

Chem. Recovery Factor:

Th229 TH-18A
0.233 mL

0.1522 +/- 0.0139

0.1736 +/- 0.0032 on 12/15/2012


0.8769 +/- 0.0820

Peak Match Tolerance:

0.175 MeV

PEAK
Energy
(MeV)

Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232

5. 911
5.347
4.865
4.637
3.970

Net
Pk Area

AREA

REPORT

Pk Area
Error %

1. 81
63 .13
135.32
95.32
79.00

1:57:27 PM

Ambient
Backgnd

193.79
25.09
16.90
20.16
22.19

1.19
1. 87
0.68
0.68
0.00

FWHM
(keV)

Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

3.1
4.2
5.5
5.5
4.2

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS


Nuclide

Id
Conf.

Energy
(keV)

TH-227
TH-228
TH-229
TH-230
TH-232

0.981
0.986
1.000
0. 994
0.996

5850.00*
5400.00*
4872.00*
4672.00*
3997.00*

Activity
(pCi/liter )
3.24E-002
l.13E+OOO
2.37E+OOO
l.66E+OOO
l.38E+OOO

+/
+/
+/
+/
+/

6.30E-002
3.48E-001
4.25E-001
4.49E-001
3.93E-001

f'G

8/ tc/-f'3

MDA
(pCi/liter
l.18E-001
l.35E-001
9.87E-002
9.84E-002
l.04E-001

+/+/+/+/+/-

2.12E-002
2.43E-002
1. 77E-002
l.77E-002
l.87E-002

0000066174.CNF

Live Time :10201.000 sec


Real Time :10201.000 sec
start:
1:3405.9(kev)
stop : 1024: 6615. S(kev)
Acq. start :wed Aug 14 12:46:43 2013

60
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V)

.......
s::::

8 30
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Li
I

3500

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4500

a~

,,,,)
r1,)

r,)

ROI Type: 1

5000
Energy(kev)

5500

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ROI Type: 3

6500

Channel Data Report

8/14/2013

Page

3:49:37 PM

*******************************************************
s p E C T R A L DAT A R E P 0 R T *****
*****
*******************************************************
Sample Title:

08

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1
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1
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0
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3
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0
0
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1
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4
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1
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3
6
1
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1
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0
0
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0
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1
1
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224

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801:

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0

Sample Title:

3:49:37
0

Page

PM
0

08

Channell------l-------l-------1-------1-------1-------l-------l-------I
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953:
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969:
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993:
1001:
1009:
1017:

0
1
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0
0
0
0
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0
0
0

0
0
0
0
0
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0
0
0
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0
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0
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0
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0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
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0
0
0
0
0
0
0
0

0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
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0

0
0
0
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0
0
0
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0
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0
1
0
0
0
0
0
0
0
0
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0

0
0
0
0
0
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0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

~Jt'Apex-Alpha'"

Sample Description:

Spectrum File:

Batch Identification:

Sample Identification:

Sample Geometry:

Procedure Description:

PZ-107-SS DIS
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000661
1307154A-TH
09
Shelf 2
Th iso

Detector Name:

Alpha_027
Chamber Serial Number:

Detector Serial Number:


27
Env. Background:

System Bkgd 64778


Reagent Blank:

<not performed>
Sample Size:

Sample Date/Time:

Acquisition Date/Time:

Acquisition Live Time:

Acquisition Real Time:

l.OOOE+OOO +/- O.OOOE+OOO liter


7/19/2013
7:22:05 AM
8/14/2013 12:46:44 PM
170.0 minutes
170.0 minutes

Tracer Certificate:

Tracer Quantity:

Effective Efficiency:

Counting Efficiency:

Chem. Recovery Factor:

Th229 TH-18A
0.236 mL

0.0612 +/- 0.0085

0.1728 +/- 0.0032 on 12/15/2012


0.3540 +/- 0.0498

Peak Match Tolerance:

0.175 MeV

PEAK
Energy
(MeV)

Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232

Net
Pk Area

5.766
5.291
4.866
4.632
3.972

1. 30
-0.89
55.15
7.30
0.81

AREA

2:27:41 PM

REPORT

Pk Area
Error %
273.47
347.50
26.63
81. 83
359.15

Ambient
Backgnd
1. 70
2.89
0.85
1. 70
1.19

FWHM
(keV)

Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

3.2
3.2
10.6
3.2
3.2

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS


Nuclide

Id
Conf.

Energy
(keV)

TH-227
TH-228
TH-229
TH-230
TH-232

0.964
0.940
1. 000
0.992
0.997

5850.00*
5400.00*
4872.00*
4672.00*
3997.00*

Activity
(pCi/liter )
5.79E-002
-3.96E-002
2.40E+OOO
3.17E-001
3.51E-002

+/+/+/+/+/-

l.59E-001
l.38E-001
6.56E-001
2.73E-001
1.26E-001

MDA
(pCi/liter
3.27E-001
3.90E-001
2.61E-001
3.19E-001
2.85E-001

+/+/+/+/+/-

8.94E-002
l.06E-001
7.12E-002
8.71E-002
7.80E-002

~
gl 14f~

8226

0000066175.CNF

Live Ti me :10201. 000 sec


Real Time :10201.000 sec
start:
1: 3402 .4(kev)

stop : 1024: 6658. l(kev)

Acq. start :wed Aug 14 12:46:44 2013

60
55

50

45

40

35

VI

-I-'

c:
::::s

8 30

25

20

15

10

5
0

3500

~Ii:~

I\,~

W,,Jt

...J

...'.

A ~-

f,!\l,.i i,!I!

I~

l'i\

4000

4500
ROI Type: 1

5000

Energy(kev)

5500

6000
ROI Type: 3

6500

Channel Data Report

8/14/2013

Page

3:49:52 PM

*******************************************************
s p E C T R A L DAT A R E P 0 R T *****
*****
*******************************************************
Sample Title:

09

Elapsed Live time:


Elapsed Real Time:

10201
10201

Channell------l-------l-------l-------1-------1-------1-------l-------I
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801:

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3:49:52
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~Apex-Alpha

Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:

PZ-106-KS TOT
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000661

1307154A-TH

10

Shelf 2

Th iso

Detector Name:
Chamber Serial Number:

Detector Serial Number:


Env. Background:
Reagent Blank:

Alpha_029

29

System Bkgd 64779

<not performed>

Sample Size:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:

l.OOOE+OOO +/- O.OOOE+OOO liter

7/19/2013
7:22:05 AM

8/14/2013 12:46:45 PM

170.0 minutes

170.0 minutes

Tracer Certificate:
Tracer Quantity:
Effective Efficiency:
Counting Efficiency:
Chem. Recovery Factor:

Th229 TH-18A

0.234 mL

0.1491 +/- 0. 0138

0.1945 +/- 0.0036 on 12/15/2012


0. 7665 +/- 0.0722

Peak Match Tolerance:

0.175 MeV

PEAK
Energy
(MeV)

Nuclide

Net
Pk Area

AREA

2:30:02 PM

REPORT

Pk Area
Error %

Ambient
Backgnd

Reagent
Backgnd

0.68
2.72
0.85
0.34
1.19

O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

FWHM

(keV)

-------------------------------------------------------------------------------TH-227
TH-228
TH-229
TH-230
TH-232

5.757
5.272
4.880
4.621
3.950

4.32
-0.72
133.15
7.66
1. 81

102.62
427.02
17.05
72.63
193.79

3.1
3.1
5.7
3.1
3.1

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS


Nuclide

Id
Conf.

Energy
(keV)

Activity
(pCi/liter )

MDA

(pCi/liter

-------------------------------------------------------------------------------TH-227
TH-228
TH-229
TH-230
TH-232

0.956
0. 917
1.000
0.987
0.988

5850.00*
5400.00*
4872.00*
4672.00*
3997.00*

7.89E-002
-1. 31E-002
2.38E+OOO
1.36E-001
3.22E-002

+/+/+/+/+/-

8.22E-002
5.62E-002
4.30E-001
l.02E-001
6.26E-002

l.03E-001
1. 56E- 001
l.07E-001
8.51E-002
1.17E-001

+/+/+/+/+/-

1.86E-002
2.83E-002
1.93E-002
l.54E-002
2.12E-002

fG
'iS

1rctf13

8231

0000066176.CNF

Live Time :10201.000 sec


Real Time :10201.000 sec
start:
1:3413.5(kev)

Stop : 1024: 6597. 5(keV)

Acq. start :wed Aug 14 12:46:45 2013

60
55

50

45

40

35

Vl

........

r::::
::::s

8 30

25

20

15

10

l,1

'i\

.\

3500

4000

4500

~il!~

r~
(1.JI

ROI Type: 1

5000
Energy(kev)

5500

6000
ROI Type: 3

6500

Channel Data Report

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Page

3:50:01 PM

*******************************************************
s P E C T R A L DAT A R E P 0 R T *****
*****
*******************************************************
Sample Title:

10

Elapsed Live time:


Elapsed Real Time:

10201
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E234

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913:
921:
929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:

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1
0
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13235

~Jt.Apex-Alpha
Sample Description:

Spectrum File:

Batch Identification:

Sample Identification:

Sample Geometry:

Procedure Description:

PZ-106-KS DIS
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000661
1307154A-TH
11

Shelf 2
Th iso

Detector Name:

Alpha_031
Chamber Serial Number:

Detector Serial Number:


31
Env. Background:

System Bkgd 64780


Reagent Blank:

<not performed>
Sample Size:

Sample Date/Time:

Acquisition Date/Time:

Acquisition Live Time:

Acquisition Real Time:

l.OOOE+OOO +/- O.OOOE+OOO liter


7/19/2013
7:22:05 AM
8/14/2013 12:46:46 PM
170.0 minutes
170.0 minutes

Tracer Certificate:

Tracer Quantity:

Effective Efficiency:

Counting Efficiency:

Chem. Recovery Factor:

Th229 TH-18A
0.235 mL

0.0616 +/- 0.0086

0.1418 +/- 0.0034 on 6/13/2013


0.4340 +/- 0.0614

Peak Match Tolerance:

0.175 MeV

PEAK
Energy
(MeV)

Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232

Net
Pk Area

5.817
5.387
4.890
4.592
3.958

AREA

REPORT

Pk Area
Error %

1. 32
0.98
55.15
1.49
1.15

3:23:29 PM

FWHM
(keV)

Ambient
Backgnd

Reagent
Backgnd

0.68
1. 02
0.85
0.51
0.85

O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

215.97
294.85
26.63
190.02
249.59

3.1
3.1
3.1
3.1
3.1

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS


Nuclide

Id
Conf.

Energy
(keV)

TH-227
TH-228
TH-229
TH-230
TH-232

0.994
0.999
0.998
0.967
0.992

5850.00*
5400.00*
4872.00*
4672.00*
3997.00*

Activity
(pCi/liter )
5.84E-002
4.33E-002
2.39E+OOO
6.43E-002
4.95E-002

+/+/+/+/+/-

l.27E-001
1.28E-001
6.52E-001
l.23E-001
1. 24E- 001

MDA
(pCi/liter
2.50E-001
2.79E-001
2.59E-001
2.26E-001
2.58E-001

+/+/+/+/+/-

6.82E-002
7.61E-002
7.07E-002
6.18E-002
7.04E-002

AG,

s lrtfl ry_,
G.236

0000066177.CNF

Live Time :10200.000 sec


Real Time :10200.000 sec
start:
1:3388.9(kev)
stop : 1024:6594.6(kev)
Acq. start :wed Aug 14 12:46:46 2013

60
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VI
.f--1

c:

::::s

8 30

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h I

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Jtii.l~I
t.,~
i~JI

......~

'i

4000

4500
ROI Type: 1

5000
Energy(kev)

5500

6000
ROI Type: 3

6500

Channel Data Report

8/14/2013

Page

3:50:10 PM

*******************************************************
s p E C T R A L DAT A R E P 0 R T *****
*****
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1

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11

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0

.A

~~~/""\pexSample Description:

Spectrum File:

Batch Identification:

Sample Identification:

Sample Geometry:

Procedure Description:

Al pha

TM

DUP 08 TOT
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000661
1307154A-TH
12
Shelf 2
Th iso

Detector Name:

Alpha_033
Chamber Serial Number:

04026479A
Detector Serial Number:
91132
Env. Background:

System Bkgd 64781


Reagent Blank:

<not performed>
Sample Size:

Sample Date/Time:

Acquisition Date/Time:

Acquisition Live Time:

Acquisition Real Time:

l.OOOE+OOO +/- O.OOOE+OOO liter


7/19/2013
7:22:05 AM
8/14/2013 12:46:58 PM
170.0 minutes
170.1 minutes

Tracer Certificate:

Tracer Quantity:

Effective Efficiency:

Counting Efficiency:

Chem. Recovery Factor:

Th229 TH-18A
0.235 mL

0.1379 +/- 0.0132

0.1848 +/- 0.0032 on 7/20/2013


0.7461 +/- 0.0724

Peak Match Tolerance:

0.175 MeV

PEAK
Energy
(MeV)

Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232

5.836
5.386
4.894
4.648
3.979

Net
Pk Area

AREA

REPORT

Pk Area
Error %

3.15
58.49
123.49
69.00
81.83

2: 31: 30 PM

126.67
25.76
17.68
23.77
21. 69

Ambient
Backgnd
0.85
0.51
0.51
0.00
0.17

FWHM
(keV)

Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

3.0
8.9
3.3
12.9
4.0

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS


Nuclide

Id
Conf.

Energy
(keV)

TH-227
TH-228
TH-229
TH-230
TH-232

0.999
0.999
0.998
0.997
0.998

5850.00*
5400.00*
4872.00*
4672.00*
3997.00*

Activity
(pCi/liter )
6.22E-002
l.15E+OOO
2.38E+OOO
l.33E+OOO
l.57E+OOO

+/
+/
+/
+/
+/

7.97E-002
3.67E-001
4.46E-001
4.02E-001
4.50E-001

MDA
(pCi/liter
l.18E-001
1. 04E- 001
l.OlE-001
1.15E- 001
8.02E-002

+/+/+/+/+/-

2.21E-002
1. 94E-002
l.89E-002
2.16E-002
l.50E-002

N4
8l1lf-l 13
8241

0000066180.CNF

Live Time :10200.000 sec

Real Time :10204.100 sec

start:
1:3447.3(kev)

Stop : 1024: 6496. 6(kev)

Acq. start :wed Aug 14 12:46:58 2013

55

50

45

40

35

VI

-I-'

c:

:::J

8 30

25

20

15

10

5
0

!, \
I

3500

4000

4500

11'.ll?li

5000
Energy(kev)

5500

6000

....Ji
~i.,

f\:tl

ROI Type: 1

ROI Type: 3

6500

Channel Data Report

8/14/2013

Page

3:50:17 PM

*******************************************************
s p E CTR AL DAT A R E P 0 R T *****
*****
*******************************************************
Sample Title:

12

Elapsed Live time:


Elapsed Real Time:

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0
0
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1
2
1
2
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0
0
0
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0
0
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0
0

1
1
0
1
0
3
0
1
0
0
4
0
5
2
2
1
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
1
1
0
2
1
2
0
0
0
0
0
0
0
0
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1
0
0
0
0
0
0

0
2
1
2
1
2
0
1
1
0
3
1
2
1
0
0
2
1
0
1
0
0
0
0
0
0
0
0
0
0
0
1
2
0
0
0
4
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

1
0
1
1
4
2
0
0
0
0
3
4
1
1
2
1
3
1
0
0
2
0
0
0
0
0
0
0
0
0
0
0
1
2
0
2
4
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0

0
1
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1
3
1
1
1
1
0
1
1
4
6
2
2
0
1
0
1
1
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0
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1
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3
2
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0
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0
0

8244

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801:

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0

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3:50:17
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PM
0

12

Channell------l-------1-------1-------1-------l-------l-------l-------I
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0
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0
0
0
0
0
0
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0
0
0
0
0
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0

0
0
1
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
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0

0
0
0
0
0
0
0
0
0
0
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0
0
0
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0
0
0
0
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0

0
0
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0
0
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0
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0
0
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0
0
0
0
0
0
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0
0
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0
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0
0
0
0
0
0
0
0
0
0
0

1245

------

----

------------------------------------------------

Sample Description:

Spectrum File:

Batch Identification:

Sample Identification:

Sample Geometry:

Procedure Description:

DUP 08 DIS
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000661
1307154A-TH
13
Shelf 2
Th iso

Detector Name:

Alpha_034
Chamber Serial Number:

04026479B
Detector Serial Number:
91136
Env. Background:

System Bkgd 64782


Reagent Blank:

<not performed>
Sample Size:

Sample Date/Time:

Acquisition Date/Time:

Acquisition Live Time:

Acquisition Real Time:

1.000E+OOO +/- O.OOOE+OOO liter


7/19/2013
7:22:05 AM
8/14/2013 12:47:00 PM
170.0 minutes
170.1 minutes

Tracer Certificate:

Tracer Quantity:

Effective Efficiency:

Counting Efficiency:

Chem. Recovery Factor:

Th229 TH-18A
0.235 mL

0.1177 +/- 0.0120

0.1856 +/- 0.0032 on 12/16/2012


0.6344 +/- 0.0658

Peak Match Tolerance:

0.175 MeV

PEAK
Energy
(MeV)

Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232

5.874
5.391
4. 871
4.632
3.884

Net
Pk Area
-0.17
6.83
105.66
11. 00
1. 83

AREA

5:49:43 PM

REPORT

Pk Area
Error %

Ambient
Backgnd

1169.4
76.08
19.10
61.72
152.56

0.17
0.17
0.34
0.00
0.17

Reagent
Backgnd

FWHM
(keV)

O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

0.0
5.9
7.3
3.0
3.0

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS


Nuclide

Id
Conf.

Energy
(keV)

Activity
(pCi/liter )

MDA

(pCi/liter

-------------------------------------------------------------------------------TH-227
TH-228
TH-229
TH-230
TH-232

0.997
1. 000
1. 000
0.992
0.935

5850.00*
5400.00*
4872.00*
4672.00*
3997.00*

-3.93E-003
1.58E-001
2.39E+OOO
2.48E-001
4.12E-002

+/
+/
+/
+/
+/

4.60E-002
1. 24E- 001
4.79E-001
1. 61E- 001
6.34E-002

f\G

glt~fj

9.66E-002
9.65E-002
1.08E-001
1.35E-001
9.39E-002

+/
+/
+/
+/
+/

1.94E-002
1.93E-002
2.17E-002
2. 71E-002
1. 88E- 002

0000066181.CNF

Live Time :10200.000 sec


Real Time :10204.100 sec
start:
1:3439.l(kev)

stop : 1024:6479.9(kev)

Acq. Start :wed Aug 14 12:47:00 2013

60
55

50

45

40

35

Vl
.f-1

s::::

:::::s

8 30

25

20

15

10

I
,1

t lj
I

3500

4000

4500

II<~~

M
l.~llm,

"iii,h~

1\~,J

ROI Type: 1

5000
Energy(kev)

6000

5500
ROI Type: 3

Channel Data Report

8/14/2013

Page

3:50:24 PM

*******************************************************
R E P 0 R T
S P E C T R A L
DAT A
*****
*****
*******************************************************
Sample Title:

13

Elapsed Live time:


Elapsed Real Time:

10200
10204

Channell------l-------l-------1-------1-------1-------l-------l-------I
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1
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0
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0
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1
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0
0
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0

0
1
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2
2
1
1
1
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S249

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0

13

Channell------l-------l-------1-------1-------1-------l-------l-------I
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Page 1 of 2
8/14/2013 5:45:39 AM

~Jt'Apex-AlphaTJ
QA SUMMARY REPORT

Review Of QA Results - Pulser Check


Date
Time

: 8/14/2013
: 5:45:39 AM

CHAMBER
Alpha 001
Alpha 002
Alpha 003
Alpha 004
Alpha 005
Alpha 006
Alpha 007
Alpha 008
Alpha 009
Alpha 010
Alpha 011
Alpha 012
Alpha 013
Alpha 014
Alpha 015
Alpha 016
Alpha 017
Alpha 018
Alpha 019
Alpha 020
Alpha 021
Alpha 022
Alpha 023
Alpha 024
Alpha 025
Alpha 026
Alpha 027
Alpha 028
Alpha 029
Alpha 030
Alpha 031
Alpha 032
Alpha 033
Alpha 034
Alpha 035
Alpha 036
Alpha 037
Alpha 038
Alpha 039
Alpha 040
Alpha 041
Alpha 042

DEVICE
21f
21f
21f
21f
21f
21f
21f
21f
21f
21f
21f
21f
21f
21f
21f
21f
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
Alpha AnalystlOODC
Alpha Analyst I OODC
Alpha Analyst! OODC
Alpha Analyst I OODC
Alpha Analvstl OODC
Alpha AnalvstlOODC
Alpha AnalystlOODC
Alpha AnalystlOODC
Alpha Analystl OODC
Alpha Analyst 1OODC

PARAMETER
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
Peak Energy
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL

FLAG
Not Done
Not Done
Passed
Passed
Not Done
Not Done
Not Done
Not Done
Not Done
Passed
Passed
Passed
Passed
Passed
Action
Not Done
Not Done
Passed
Passed
Not Done
Not Done
Passed
Passed
Passed
Passed
Not Done
Passed
Not Done
Passed
Not Done
Passed
Not Done
Passed
Passed
Passed
Passed
Passed
Passed
Passed
Passed
Passed
Passed

DATE

8/14/2013 5:27:31 AM
8/14/2013 5:27:32 AM

8/14/2013
8/14/2013
8/14/2013
8114/2013
8/14/2013
8/14/2013

5:27:33 AM
5:27:34 AM
5:27:34 AM
5:27:35 AM
5:27:36 AM
5:27:37 AM

8/10/2013 11:23:01 AM
8/14/2013 5:27:38 AM

8/14/2013
8/14/2013
8114/2013
8/14/2013

5:27:38 AM
5:27:39 AM
5:27:40 AM
5:27:41 AM

8/14/2013 5:27:42 AM
8/14/2013 5:27:42 AM
8/14/2013 5:27:43 AM
8/14/2013 5:27:44 AM
8/14/2013 5:27:46 AM
8/13/2013 5:25:31 AM
8/14/2013 5:27:49 AM
8/14/2013 5:27:50 AM
8/14/2013 5:27:52 AM
8/14/2013 5:27:54 AM
8/14/2013 5:27:56 AM
8/14/2013 5:27:58 AM
8114/2013 5:28:00 AM

Page 2 of 2

Review of QA Results - Pulser Ch~k


8/14/2013 5:45:39 AM

CHAMBER
Alpha 043
Alpha 044
Alpha 045
Alpha 046
Alpha 047
Alpha 048

DEVICE
Alpha AnalystlOODC
Alpha Analyst! OODC
Alpha AnalystlOODC
Alpha AnalystlOODC
Alpha AnalystlOODC
Alpha Analyst 1OODC

PARAMETER
ALL
ALL
ALL
ALL
ALL
ALL

FLAG
Passed
Passed
Passed
Passed
Passed
Passed

DATE
8/14/2013 5:28:02 AM
8/14/2013 5:28:04 AM
8/14/2013 5:28:07 AM
8/14/2013 5:28:10 AM
8/14/2013 5:28:13 AM
8/14/2013 5:28:15 AM

APPROVED BY:

APPROVAL DATE:

N252

6/12/12

Library Listing Report

Page

12:16:29 PM

*************************************************************************
*****
L I B R A R Y L I S T I N G R E P 0 R T
*****
*************************************************************************
Nuclide Library Title:

Thorium

Nuclide Library Description:


Nuclide
Name

Half-Life
(Seconds)

TH-227
TH-228
TH-229
TH-230
TH-232

6.873E+008
6.034E+007
2.487E+Oll
2.379E+Ol2
4.434E+Ol7

Energy
(keV )

Th-227,-228,-229,-230,-232
Energy
Uncert. (keV
0.000
0.000
0.000
0.000
0.000

5850.000*
5400.000*
4872.000*
4672.000*
3997.000*

key line

TOTALS:

Nuclides

Energy Lines

Yield
( %)

97.5000
99.9400
99.5200
99.8200
100.0000

Yield
Uncert. (Abs.+-)
0.0000
0.0000
0.0000
0.0000
0.0000

SECTIONX

ANALYTICAL DATA (RADIUM-226)

6254

Eberline Services
Oak Ridge Laboratory
Analysis Sheet

Printed: 81912013 8:45 AM


Page 1of3

13-07154
Ra226
Run 1

13-07154

Work Order

Ra226
1

Analysis Code
Run

Internal
Fraction

Sample
Desc

Client
ID

01

LCS

LCS

07/24/13 00:00

1.0000E+OO

02

MBL

BLANK

07 /24/13 00:00

1.0000E+OO

Login
CPM

Sample
Date

Sample
Aliquot

7/22/2013

03

DUP

PZ-107-SS TOT

46

07/19/13 12:10

1.0000E+OO

Lab Deadline I

8/13/2013

04

TRG

PZ-200-SS TOT

42

07/19/13 10:19

1.0000E+OO

05

TRG

PZ-200-SS DIS

42

07/19/13 10:19

1.0000E+OO

West Lake OU-1

06

TRG

PZ-102-SS TOT

38

07/19/13 10:30

1.0000E+OO

Date Received

Client I Engineering Management Support, Inc.


Project I
Report Level

07

TRG

PZ-102-SS DIS

38

07/19/13 10:30

1.0000E+OO

Activity Units

pCi

08

DO

PZ-107-SS TOT

46

07/19/13 12:10

1.0000E+OO

09

TRG

PZ-107-SS DIS

46

07/19/13 12:10

1.0000E+OO

WA

10

TRG

PZ-106-KS TOT

45

07/19/13 13:09

1.0000E+OO

E903.0

11

TRG

PZ-106-KS DIS

45

07/19/13 13:09

1.0000E+OO

12

TRG

DUP 08 TOT

44

07 /19/13 00:00

1.0000E+OO

13

TRG

DUP 08 DIS

44

07/19/13 00:00

Aliquot Units
Matrix
Method

Instrument Type
Radiometric Tracer

Alpha Spectroscopy

Ba-133

Radiometric Sol#

Ba-6a

Tracer Act (dpm/g)

990.223

1.0000E+OO

Carrier
Carrier Cone (mg/ml)

it:lr!I
i\JI
l[J1J

U'1I

* SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only.

** Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.

Eberline Services
Oak Ridge Laboratory
Analysis Sheet

Printed: 8/9/2013 8:45 AM


Page 2 of 3

13-07154
Ra226
Run 1

Internal
Fraction

Sample
Desc

01

LCS

0.9259

916.8

438.4

106.15

0.0231

0.0291

02

MBL

0.9151

906.2

393.9

96.50

0.0230

Tracer
Aliquot (g)

Tracer Total
ACT(dpm)

Radiometric
Tracer (pCi)

Radiometric Grav Carrier


%Rec
Added(ml)

Grav Filter
Tare (g)

Mean
%Rec

SAF
1*

SAF
2*

0.0060

106.15

2.16

1.00

0.0292

0.0062

96.50

2.23

1.00

Grav Filter
Final (g)

Grav Filter
Net(g)

Grav
%Rec

03

DUP

0.9164

907.4

310.4

75.94

0.0224

0.0287

0.0063

75.94

2.27

1.00

04

TRG

0.9147

905.8

316.8

77.65

0.0229

0.0288

0.0059

77.65

2.12

1.00

05

TRG

0.9134

904.5

392.2

96.26

0.0227

0.0302

0.0075

96.26

2.64

1.00

06

TRG

0.9122

903.3

128.6

31.61

0.0229

0.0260

0.0031

31.61

0.40

1.00

07

TRG

0.9120

903.1

413.2

101.57

0.0231

0.0300

0.0069

101.57

2.47

1.00

08

DO

0.9118

902.9

300.7

73.94

0.0233

0.0322

0.0089

73.94

2.99

1.00

09

TRG

0.9102

901.3

407.9

100.47

0.0230

0.0305

0.0075

100.47

2.64

1.00

10

TRG

0.9126

903.7

390.7

95.98

0.0227

0.0297

0.0070

95.98

2.50

1.00

11

TRG

0.9091

900.2 I

418.0

103.08

0.0228

0.0302

0.0074

103.08

2.61

1.00

12

TRG

0.9079

899.0

343.8

84.90

0.0227

0.0293

0.0066

84.90

2.37

1.00

13

TRG

0.9079

899.0

376.0

92.85

0.0226

0.0306

0.0080

92.85

2.77

1.00

t!E~

l'J

lf..W~

* SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only.

Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.

Eberline Services
Oak Ridge Laboratory
Analysis Sheet

Printed: 81912013 8:45 AM


Page 3 of 3

13-07154

Ra226

Run 1

Internal
Fraction

Sample
Desc

01

Rough Prep
Date

Rough Prep
By

Prep
Date

Prep
By

Sep tO
Date/Time

Sep tO
By

LCS

08/07/13 10:33

JWOLFE

08/08/13 14:54

LWALKER

02

MBL

08/07/13 10:33

JWOLFE

08/08/13 14:54

LWALKER

03

DUP

08/07/13 10:33

JWOLFE

08/08/13 14:54

LWALKER

04

TRG

08/07/13 10:33

JWOLFE

08/08/13 14:54

LWALKER

05

TRG

08/07/13 10:33

JWOLFE

08/08/13 14:54

LWALKER

06

TRG

08/07/13 10:33

JWOLFE

08/08/13 14:54

LWALKER

07

TRG

08/07/13 10:33

JWOLFE

08/08/13 14:54

LWALKER

08

DO

08/07/13 10:33

JWOLFE

08/08/13 14:54

LWALKER

09

TRG

08/07/13 10:33

JWOLFE

08/08/13 14:54

LWALKER

10

TRG

08/07/13 10:33

JWOLFE

08/08/13 14:54

LWALKER

11

TRG

08/07/13 10:33

JWOLFE

08/08/13 14:54

LWALKER

12

TRG

08/07/13 10:33

JWOLFE

08/08/13 14:54

LWALKER

13

TRG

08/07/13 10:33

JWOLFE

08/08/13 14:54

LWALKER

Sep t1
Date/Time

Sep t1
By

Glli

~
"....JI

* SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only.

**Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.

Client

Desc

Identification

Activity
Units

RA-226

LCS

LCS

pCill

1.04E+01

1.17E+OO

1.62E-01

RA-226

MBL

BLANK

pCi/I

1.43E-01

1.46E-01

1.86E-01

RA-226

DUP

PZ-107-SS TOT

pCi/I

5.07E+OO

9.36E-01

1.81E-01

Nuclide

01

~
0

.!I!

~
.,,
i::

q;

02
~

N
N

ns

0::

Error Estimate

MDA

LCS
Known

LCS
%R

1.04E+01 - 100.32

LCS
Flag

RPO
Flag

MDA
Flag

___ -

---- ,

04
---~-

OK

05

OK

TRG

PZ-200-SS TOT

pCi/I

9.71E-01

3.89E-01

2.60E-01

OK

TRG

PZ-200-SS DIS

pCi/I

1.80E+OO

5.54E-01

2.89E-01

OK

RA-226

TRG

PZ-102-SS TOT

pCi/I

7.69E+OO

1.16E+OO

3.13E-01

OK

RA-226

TRG

PZ-102-SS DIS

pCill

3.12E+OO

6.53E-01

1.81E-01

OK

DO

PZ-107-SS TOT

pCi/I

6.39E+OO

1.22E+OO

3.47E-01

OK

TRG

PZ-107-SS DIS

pCi/I

5.33E+OO

8.87E-01

1.92E-01

OK

RA-226

TRG

PZ-106-KS TOT

pCi/I

3.34E-01

2.28E-01

1.84E-01

OK

RA-226

TRG

PZ-106-KS DIS

pCi/I

3.54E-01

2.37E-01

2.14E-01

OK

RA-226

TRG

DUP 08 TOT

pCill

5.32E+OO

9.67E-01

1.84E-01

OK

RA-226

TRG

DUP 08 DIS

pCi/I

5.09E+OO

9.59E-01

3.16E-01

OK

RA-226
---

OK

------

------

----

RA-226

- - - - ---------

06
f.-----------

----

07

~:t==~~
>---~ 0-~ 11

----+

12
f - - - - - '---

-=~

13
- - - - - f----

c..
c..

-------- f - -

----------r

:i

CJ)

c:

c:

QI

E
QI

Cl

----

~-

Ill

c:

Ill

:E

----------

Cl

c:
;:

QI
QI

c:

c,
c:
w
t!i!ll
r~,)

U'~

(~')

-----

Blank
Flag

OK

OK

--

03
>

Results

--

~------

a::

Work Order: 13-07154-Ra226-1

Sample

Lab
Fraction

Printed: 8/9/2013 1:20 PM

Page 1of3

Preliminary Data Report & Analytical Calculations

Eberline Services
Oak Ridge Laboratory

t----

- --- --1 -------


I

OK

Lab
Fraction

Nuclide

01

RA-226

Work Order: 13-07154-Ra226-1

:::s

Q;:

Ill

"O
0

.!!!

"'c::

c:(

02

Desc

03
04

CD
N
N

ns

a::

DUP

RA-226

RA-226

~f~G-

05

RA-226

06

RA-226

07

RA-226

-+-

08

RA-226

--t-T R:
0

09

RA-226

TRG

12
u

13

.5

_t~~-

RA-226

ti)

----

Cll

Cl

ns
c
ns
::i

Cl

c
c

Cll
Cll

tll::!ll
U'i

~,~)

RA-226 _

__l

SAF

Sep to
Date/Time

100.00

0.00

106.15

8/8/2013 14:54

07/24/13 00:00

1.00E+OO

96.50

0.00

96.50

8/8/2013 14:54

07/19/13 12:10

1.00E+OO

75.94

0.00

75.94

07/19/13 10:19

1.00E+OO

77.65

0.00

77.65

8/8/2013 14:54

07/19/13 10:19

1.00E+OO

96.26

0.00

96.26

8/8/2013 14:54

07/19/13 10:30

1.00E+OO

31.60

0.00

31.61

8/8/2013 14:54

07/19/13 10:30

1.00E+OO

100.00

0.00

101.57

8/8/2013 14:54

07/19/13 12:10

1.00E+OO

73.94

0.00

73.94

8/8/2013 14:54

07/19/13 12:10

1.00E+OO

100.00

0.00

100.47

8/8/2013 14:54

07/19/13 13:09

1.00E+OO

95.98

0.00

95.98

8/8/2013 14:54

07/19/13 13:09

1.00E+OO

100.00

0.00

103.08

8/8/2013 14:54

07/19/13 00:00

1.00E+OO

84.90

0.00

84.90

8/8/2013 14:54

---+

07/19/13 00:00

1.00E+OO

92.85

0.00

92.85

8/8/2013 14:54

1------

-
-

TRG

TRG

--------- - - - - -

-~--------

-
--

=rr
I

_________T___
I

8/8/2013 14:54

--

+~~~- -

-- r

RA-226

----

a.
a.

:;,

r".:it

--------

TRG

t-;~-

11

c
c
w

Mean
%Rec

- - ----

RA-226
- - - - -- - - - - - - -

c,

Grav
%Rec

10

~I

Radiometric
%Rec

~---

MBL

RA-226

Sample
Aliquot

1.00E+OO

07/24/13 00:00

LCS

T"'9

c
Cll
E

Sample
Date

Sample

c::

Printed: 8/9/2013 1:20 PM

Page 2 of 3

Preliminary Data Report & Analytical Calculations

Eberline Services
Oak Ridge Laboratory

-
--------

I
~--

Sep t1
Date/Time

Eberline Services
Oak Ridge Laboratory

(
c:
~

T"9

Work Order: 13-07154-Ra226-1

Nuclide

Sample
Desc

Counting
Date/Time

I
I

01

RA-226

LCS

08/09/13 09:04

02

RA-226

MBL

08/09/13 09:04

RA-226

DUP

08/09/13 09:04

RA-226

TRG

08/09/13 09:05

RA-226

TRG

08/09/13 09:05

06

RA-226

TRG

08/09/13 09:05

07

RA-226

TRG

08/09/13 09:05

RA-226

DO

08/09/13 09:05

RA-226

TRG

08/09/13 09:05

RA-226

TRG

RA-226

Lab
Fraction

CD

N
N

a::

Count
Time

Counts

Bkg
CPM

Eff

Carrier

A_Spec

Alpha_033

170 3.35 E+02

3.00 E-03

18.5

A_Spec

Alpha_034

170 4.32 E+OO

4.00 E-03

18.6

A_Spec

Alpha_035

170 1.17 E+02

1.00 E-03

18.3

A_Spec

Alpha_036

170 2.56 E+01

8.00 E-03

19.1

A_Spec

Alpha_038

170 4.26 E+01

8.00 E-03

17.2

A_Spec

Alpha_039

170 1.80 E+02

1.00 E-02

19.7

A_Spec

Alpha_040

170 9.05 E+01

3.00 E-03

19

A_Spec

Alpha_042

170 1.10 E+02

5.00 E-03

18.5

A_Spec

Alpha_045

170 1.45 E+02

3.00 E-03

19.1

08/09/13 09:05

A_Spec

Alpha_046

170 8.66 E+OO

2.00 E-03

17.9

TRG

08/09/13 09:05

A_Spec

Alpha_047

170 9.32 E+OO

4.00 E-03

18.2

RA-226

TRG

08/09/13 09:05

A_Spec

Alpha_048

170 1.21 E+02

1.00 E-03

16.8

RA-226

TRG

08/09/13 09:26

A_Spec

Alpha_018

170.02 1.14 E+02

9.00 E-03

17.8

---

03
04
05

ca

Halflife
(days)

Detect

-------

.g

Printed: 8/9/2013 1:20 PM

Page 3 of 3

Preliminary Data Report & Analytical Calculations

--

f------------

08
---

~---------

09

------- - - -

10

i
I

II

-------

e--22J
u

.5

ji

c.
c.

:::s

Cl)

.~I
0

c
tll
E
tll
en
ns
c
ns
:i
en
c

c
tll
tll

.5

en
c

w
~

!';ll

fJill
~~:ll

~-------c-;------------

~----------1-----

f--------t------

i
I

~-----1

---------i--------

iI

Count Room Report


Client: Engineering Management Su

fl}'\-\
~

ho~

Printed: 81912013 8:45 AM


Page 1 of 1

13-07154-Ra226-1 (pCi/I) in WA
Tracer ID: Ba-Sa

Radiometric
%Rec

SAF
1

SAF

438.4000

106.15

2.16

1.00

906.1531

393.9000

96.50

2.23

1.00

0.9164

907.4404

310.4000

75.94

2.27

1.00

1.0000

0.9147

905.7570

316.8000

77.65

2.12

1.00

07/19/13 10:19

1.0000

0.9134

904.4697

392.2000

96.26

2.64

1.00

PZ-102-SS TOT

07/19/13 10:30

1.0000

0.9122

903.2814

128.6000

31.61

0.40

1.00

TRG

PZ-102-SS DIS

07/19/13 10:30

1.0000

0.9120

903.0834

413.2000

101.57

2.47

1.00

08

DO

PZ-107-SS TOT

07/19/13 12:10

1.0000

0.9118

902.8853

300.7000

73.94

2.99

1.00

09

TRG

PZ-107-SS DIS

07/19/13 12:10

1.0000

0.9102

901.3010

407.9000

100.47

2.64

1.00

10

TRG

PZ-106-KS TOT

07/19/13 13:09

1.0000

0.9126

903.6775

390.7000

95.98

2.50

1.00

11

TRG

PZ-106-KS DIS

07/19/13 13:09

1.0000

0.9091

900.2117

418.0000

103.08

2.61

1.00

12

TRG

DUP 08 TOT

07 /19/13 00:00

1.0000

0.9079

899.0235

343.8000

84.90

2.37 I 1.00

13

TRG

DUP 08 DIS

07/19/13 00:00

1.0000

0.9079

899.0235

376.0000

92.85

2.77

Tracer
Aliquot (g)

Tracer
ACT(dpm)

Internal
Fraction

Sample
Desc

Client
ID

Sample
Date

Sample
Aliquot

01

LCS

LCS

07/24/13 00:00

1.0000

0.9259

916.8475

02

MBL

BLANK

07/24/13 00:00

1.0000

0.9151

03

DUP

PZ-107-SS TOT

07/19/13 12:10

1.0000

04

TRG

PZ-200-SS TOT

07/19/13 10:19

05

TRG

PZ-200-SS DIS

06

TRG

07

Radiometric
Tracer (pCi)

~-

-~,

1.00

I
I

Gal
rlil

en

Il"'d!'

Eberline Services
Oak Ridge Laboratory

..

LCS & Matrix Spikes

Isotope

So/#

Ra-226

Ra-5b

Activity
dpm/g

44.066

Solution
Date

..

::.,;

Approx
Addition

81712013

0.500

Analysis Code

Date

Technician

Ra226

8/7/2013 10:32

JWOLFE

LCS

MS

LCSD

1!o'$D

Volume
Used(g)

Volume
Used(g)

Volume
Used(g)

Volume
Used(g)

0.5217

---

..
Isotope

So/#

01

Ba-133

Ba-6a

02

Ba-133

Ba-6a

03

Ba-133

Ba-6a

04

Ba-133

Ba.Sa

05

Ba-133

06

Ba-133

07

Activity
dpm/g

990.223

Solution
Date

I
i

Approx
Addition

81712013

o.9259

990.223

81712013

0.9151

1.0200

990.223

81712013

0.9164

1.0200

990.223

81712013

0.9147

1.0200

Ba-6a

990.223

8f7/2013

0.9134

1.0200

Ba-6a

990.223

81712013

0.9122

1.0200

Ba-133

Ba-6a

990.223

81712013

0.9120

1.0200

08

Ba-133

Ba.Sa

990.223

81712013

0.9118

1.0200

09

Ba-133

Ba-6a

990.223

8f7/2013

0.9102

1.0200

990.223

10

Ba-133

81712013

0.9126

1.0200

11

Ba-133

Ba.Sa

990.223

81712013

0.9091

1.0200

12

Ba-133

Ba-6a

990.223

81712013

0.9079

1.0200

13

Ba-133

Ba-6a

990.223

81712013

0.9079

1.0200

en
M

Version 2.0 08/99

0.000

Known
pCi

MSD

i
o.oo!

Added
pCi

Error
Estimate

0000

Error
Estimate

0.000

0.00
...

--- ---

Balance Pri.riter Tapes


Tracer

..

LCS

1.0200

Ba-6a

~~I

0.00

Error
Estimate

..

Volume
Used(g)

l"IJ

0476

Added
pCi

Witness Initials

LCSD

MS

Error
Estimate

----~--

Tracer.f.' .

fraction

Technician Initials

LCS
Known
pCi

10.36

:.:_:___+

Page 1of1
Printed: 817/2013 10:33 AM

Spike and Tracer Worksheet

Matrix Spike

Eberline Analytical
Oak Ridge Laboratory

Lab
Fraction
01
02
03
04
05
06
07
08
09
10
11
12
13

Engineering Management Support, Inc.

Printed: 8n/2013 10:34 AM

Page 1of1

Aliquot Worksheet

Rpt Units

Lab Deadline

Technician

Ra226

liters

8/13/2013

JWOLFE

Dilution Data

Muffle Data

Sample

Client ID
LCS
BLANK
PZ-107-SS TOT
PZ-200-SS TOT
PZ-200-SS DIS
PZ-102-SS TOT
PZ-102-SS DIS
PZ-107-SS TOT
PZ-107-SS DIS
PZ-106-KS TOT
PZ-106-KS DIS
DUP 08 TOT
DUP 08 DIS

Analysis Code

Ratio
Post/Pre

Type
LCS
MBL
DUP
TRG
TRG
TRG
TRG
DO
TRG
TRG
TRG
TRG
TRG

I
I

,i ,

,',

<
'~. '\
twtlo,

. .NO!of Dils

DU Factor

tin
,'
.\' 1",,,
'

''(

...

..

..

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..

....

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'

.1"..

r/ Ir
' '(<'.
> ...,

..

;~

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'1.''.

i'I

'I

,
I'

.,
-.I

Aliquot Data
Aliquot
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO

Net Equiv

1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO

MS Aliquot Data
Aliquot

,. NeH:quiv

... '
I

.
I

Cmn~nts

m
t.i,Ji

Techo;c;ao

I'

..'
"

<
IL

- 'i
-

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'

..

1.0000E+OQ
1.0000E+OQ

..

'

'
.

.,

'

"

'

'

=1

~.,,

l'\l

HJ Dist
Aliq

!,

"

..

H-3 Solids Only


Water Added
(ml)

',I
...

\l Jo~ate ~ :J-, f(:5'

Eberline Services - Oak Ridge


Version 1.0 9/1999

Printed: 8/8/2013 4:55 PM


Page 1 of 1

Gravimetric Worksheet

Gravimetric
Carrier

Analysis
Code

Work Order

Carrier Cone
(mgfm!)

Ra226
TRetec

Engineering Management Support, Inc.

Carrier Data
Carrier Added
(ml)

Client ID

Type

01
02
03
04
05
06
07
08
09
10
11
12
13

LCS.
BLANK
DUP
PZ-200-SS TOT
PZ-200-SS DIS
PZ-102-SS TOT
PZ-102-SS DIS
PZ-107-SS TOT
PZ-107-SS DIS
PZ-106-KS TOT
PZ-106-KS DIS
DUP 08 TOT
DUP 08 DIS

LCS
MBL
DUP
TRG
TRG
TRG
TRG
DO
TRG
TRG
TRG
TRG
TRG

LWALKER

Sample

Fraction

Technician

Filter Data
Filter Tare
(g)

0.0231
0.0230
0.0224
0.0229
0.0227
0.0229
0.0231
0.0233
0.0230
0.0227
0.0228
0.0227
0.0226

------

..

Filter Final
(g)

0.0291
0.0292
0.0287
0.0288
0.0302
0.0260
0.0300
0.0322
0.0305
0.0297
0.0302
0.0293
0.0306

Gravimetric
Filter Net
(gJ

%
RecoverJ

0.0060
0.0062
0.0063
0.1)059
0.0075
0;0031
0.0069
0.0089
0..0075

. ..

0,0010
0.0074
(l.0066
0;0080

..

:t<'.1~

!')

m
$~\la!!

Technician:

--....---------+-------

Date:

_B_, 8 /(3

~jApex-Alpha"'

Sample Description:
Spectrum File:
Batch Identification:

Sample Identification:

Sample Geometry:

Procedure Description:

SPIKE
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000656
1307154A-RA
01
Shelf 2
Ra

Detector Name:

Alpha_033
Chamber Serial Number:

04026479A
Detector Serial Number:
91132
Env. Background:

System Bkgd 64051


Reagent Blank:

<not performed>
Sample Size:

Generic Mult. Factor:

Sample Date/Time:

Acquisition Date/Time:

Acquisition Live Time:

Acquisition Real Time:

l.OOOE+OOO +/- O.OOOE+OOO liter


2.160E+OOO
Generic Div. Factor:
8/9/2013
8:51:08 AM
8/9/2013
9:04:56 AM
170.0 minutes
175.7 minutes

Chem. Recovery Factor:

Counting Efficiency:

Effective Efficiency:

1.0000 +/0.1848 +/0.1848 +/-

0.0000
0.0032 on 7/20/2013
0.0032

Control Certificate Name:


Ra226 Ra-Sb

Chem. Recov. of Control:


RA-226
0.464441 +/Peak Match Tolerance:

0.350 MeV

PEAK
Nuclide

Energy
(MeV)

Net
Pk Area

AREA

l.OOOE+OOO

2:31:30 PM

0.030076

REPORT

Pk Area
Error %

Ambient
Backgnd

Reagent
Backgnd

8.50
10. 71

0.85
0.51

O.OOE+OOO
O.OOE+OOO

FWHM
(keV)

-------------------------------------------------------------------------------RA-224
RA-226

5.538
4.546

532.15
335.49

8.1
4.0

-------------------------------------------------
NUCLIDE ANALYSIS RESULTS
-------------------------------------------------

Nuclide

Id
Conf.

Energy
(keV)

Activity
(pCi/liter )

MDA
(pCi/liter

-------------------------------------------------------------------------------RA-224
RA-226

0.972
0.928

5685.50*
4785.00*

l.73E+001 +/- l.59E+OOO


l.04E+001 +/- l.17E+OOO

l.95E-001 +/- 6.70E-003

l.62E-001 +/- 5.59E-003

G265

0000065676.CNF

Live Time :10200.000 sec


Real Time :10543.700 sec
start:
1: 3447. 3(kev)
stop : 1024: 6496. 6(kev)
Acq. Start :Fri Aug 09 09:04:56 2013

60

55

50

45

40

35

VI
.f.-1

c:

:::J

8 30

25

20

15

10

5
0

ll!ll!!j! !!l!f!!!!!

!f

V lll!ll!!!!!!

3500
~~
t'~)

fJrl
t"lr)

ROI Type: 1

1!

![II 11!1!

JI

U!J! I

4000

llJ!!

U!

1!

!}! !

11

4500

JI

II!!

5000
Energy(kev)

5500

JI I

!!

6000

!!

l!

IJ

J!'

6500

Channel Data Report

1/9/2e13

i,,.

,.,ge

*******************************************************
s p E C T R A L DAT A R E P 0 R T *****
*****
*******************************************************
Sample Title:

01

Elapsed Live time:


Elapsed Real Time:

10200
10544

Channell------l-------l-------l-------1-------1-------1-------l-------I
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0
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1
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1
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3
1
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1
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2
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1
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1
3
1
3
0
1
2
1
2
0
3
3
4
3
3
2
0
1
3
1
3
1

1
0
1
1
0
2
1
2
0
0
1
0
0
3
2
0
1
0
0
3
2
2
3
6
1
3
2
1
3
3
2
3
2
5
4
7
2
1
4
1
4
2
3
5
1
3

1267

Channel Data Report


369:

8/9/2613
4

Sample Title:

..

~.

12i'htf
2

01

Channell------l-------l-------1-------1-------1-------l-------l-------I
377:
385:
393:
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1

3
4
7
4
4
4
3
3
4
1

3
6
3
5
6
2
2
5
3
7
3
10
5
5
1

3
4
3

2
2
4
2
3
2
2
3

2
4
6
5
2
8
6
2

2
2
4
3
3
3
5
4
2
3
0
5
4
6
0
5
4
4
2

3
3
2

4
5
6
6
5
2
4
5
6
7
5
5
6
9
4
7
4
8
9
3
5
5
0
3

6
2

4
3
2
0
3
3

3
1

8
4
6
3
2
1

1
1

6
2
6

4
4

1
1

0
3
2
2

3
4
2
2
3

5
4
5
3
5
6
4
7
2
3

3
4
0
3
5
4
4
6
4
5
3
2

8
7
6
5
5
4
9

6
3
6
3
8
6
10
4
9
5
4
8
3
2

4
10
5
9
5
2
2
4
6
4
6

3
1

8
4

1
1
1

2
1
1
1

2
1

2
5
1

5
2
4
2
2
6
4
3
6
8
7
3
2
6
6
4
5
2
4
6
3
4
6
6
4
6
4
6
4
3
0
6
3

6
5
7
2
6
4
6
3
3
4
6
1
1

5
4
7
2
4
3
3
5
5
3
7
3
2
4
7
4
4
4
2
4
1

5
4
5
6
7
5
4
5
3
1

3
5
5
2
2
6
3
4
5

4
4
4
3
3
5
4
0
3
3
1
1
1
1

2
2
0
7
1

4
8
4
1

5
6
7
4
3
8
2
2
4
2
4
3
7
3
6
2
2
3
7
1
1

7
4
7
5
2
6

6
4
5
5
6
6
4
3
3
4
4
1
1

2
2
1

2
3
2
2
2
0
2
5
2
3
5
6
1

5
6
5
2
6
1

5
3
2
7
7
4
6
2
9
9
8
3
2
5
2

1
1

f:2E8

Channel Data Report


801:

8/9/2013
3

Sample Title:

Page

12:37:11 PM
3

01

Channell------l-------1-------1-------1-------l-------l-------l-------I
809:
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889:
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2
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4
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7
9
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4
1
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3
2
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0

3
2
1
2
6
8
3
1
6
5
3
4
6
1
0
6
7
3
6
3
3
4
5
1
4
2
6

0
4
7
9
3
6
1
3
9
2
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4
5
2
4
6
6
6
6
2
2
3
0
0
3
3
4

1
0
7
7
7
3
4
3
4
1
3
4
4
4
2
4
4
3
5
4
1
4
1
4
0
1
1

2
2
1
7
3
2
2
3
3
4
2
4
3
1
10
3
8
2
1
4
4
3
4
2
1
7
1

8
1
5
4
5
5
3
2
7
2
3
4
5
4
1
5
2
5
4
3
2
1
2
5
3
2
1

4
1
4
6
3
1
8
1
6
6
4
3
4
3
1
7
7
1
5
0
1
3
5
6
2
0
3

9
2
4
7
2
10
6
8
4
3
6
3
4
1
6
4
2
3
3
0
1
4
3
7

Sample Description:

Spectrum File:

Batch Identification:

Sample Identification:

Sample Geometry:

Procedure Description:

BLANK
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000656
1307154A-RA
02
Shelf 2
Ra

Detector Name:

Alpha_034
Chamber Serial Number:

04026479B
Detector Serial Number:
91136
Env. Background:

System Bkgd 64052


Reagent Blank:

<not performed>
Sample Size:

Generic Mult. Factor:

Sample Date/Time:

Acquisition Date/Time:

Acquisition Live Time:

Acquisition Real Time:

l.OOOE+OOO +/- O.OOOE+OOO liter


Generic Div. Factor:
2.230E+OOO
8/9/2013
8:51:08 AM
9:04:58 AM
8/9/2013
170.0 minutes
175.7 minutes

Chem. Recovery Factor:

Counting Efficiency:

Effective Efficiency:

0.9650 +/0.1856 +/0.1791 +/-

Peak Match Tolerance:

Energy
(MeV)

RA-224
RA-226

5:49:43 PM

0.350 MeV

PEAK
Nuclide

0.0000
0.0032 on 12/16/2012
0.0031

l.OOOE+OOO

Net
Pk Area

5.532
4.613

AREA

REPORT

Pk Area
Error %-

3.83
4.32

102.72
102.62

Ambient
Backgnd
0.17
0.68

FWHM
(keV)

Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO

3.0
3.0

NUCLIDE ANALYSIS RESULTS


Nuclide

Id
Conf.

Energy
(keV)

RA-224
RA-226

0.970
0.962

5685.50*
4785.00*

Activity
(pCi/liter )
l.33E-001 +/
l.43E-001 +/

l.37E-001
l.46E-001

MDA
(pCi/liter
l.45E-001 +/
l.86E-001 +/

4.94E-003
6.35E-003

0000065664.CNF

Live Time 10200.000 sec


Real Time 10543.700 sec
Start:
1 3439.l(kev)

Stop : 1024 6479. 9(kev)

Acq. Start Fri Aug 09 09:04:58 2013

60
55

50

45

40

35

V)

.......

c:

::I

8 30

25

20

15

10

3500
!IM~

r,:li

""Ji
i!u--~911

ROI Type: 1

4000

4500

5000
Energy(kev)

5500

6000

Channel Data Report

8/9/2013

Page

12: 37: ;J,.&..

*******************************************************
s p E C T R A L DAT A R E P 0 R T *****
*****
*******************************************************
Sample Title:

02

Elapsed Live time:


Elapsed Real Time:

10200
10544

Channell------l-------1-------1-------1-------l-------l-------l-------I
1:
9:
17:
25:
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41:
49:
57:
65:
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249:
257:
265:
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281:
289:
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305:
313:
321:
329:
337:
345:
353:
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0
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0
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1
0
0
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0
0
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0

0
0
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0
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0
0
0
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0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
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0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
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0

0
0
0
0
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fd272

Channel Data Report


369:

i/i/201:3
0

Sample Title:

...

la,,. tit ,,.. .


...

Page
0

02

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ii;! F;?"'
Y~-if~

Channel Data Report


801:

8/9/2013
0

Sample Title:

12:37:1f.
0

.
0

Page
0

02

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Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:

PZ-107-SS TOT-DUP
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000656

1307154A-RA

03

Shelf 2

Ra

Detector Name:
Chamber Serial Number:
Detector Serial Number:
Env. Background:
Reagent Blank:

Alpha_035

04026477A

58771

System Bkgd 64053

<not performed>

Sample Size:
Generic Mult. Factor:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:

l.OOOE+OOO +/- O.OOOE+OOO liter

2.270E+OOO
Generic Div. Factor:
l.OOOE+OOO

7/19/2013
8:51:08 AM

8/9/2013
9:04:59 AM

170.0 minutes

175.7 minutes

Chem. Recovery Factor:


Counting Efficiency:
Effective Efficiency:

0.7594 +/0.1826 +/0.1387 +/-

Peak Match Tolerance:

Energy
(MeV)

5:49:42 PM

0.350 MeV

PEAK
Nuclide

0.0000

0.0032 on 12/16/2012
0.0024

Net
Pk Area

AREA

REPORT

Pk Area
Error %

Ambient
Backgnd

Reagent
Backgnd

FWHM

(keV)

-------------------------------------------------------------------------------RA-224
RA-226

5.512
4.580

36.66

116. 83

32.55
18.15

0.34
0.17

O.OOE+OOO
O.OOE+OOO

4.4

3.4

NUCLIDE ANALYSIS RESULTS


Nuclide

Id
Conf.

Energy
(keV)

RA-224
RA-226

0.961
0.946

5685.50*
4785.00*

Activity
(pCi/liter )
l.68E+OOO +/- 5.51E-001
5.07E+OOO +/- 9.36E-001

MDA

(pCi/liter

2.20E-001 +/- 7.54E-003


l.81E-001 +/- 6.20E-003

il!275

0000065662.CNF

Live Time 10200.000 sec


Real Time 10543.800 sec
Start:
1 3463.4(kev)
Stop : 1024 6473. 5(kev)

Acq. Start Fri Aug 09 09:04:59 2013

60
55

50

45

40

35

Vl

.......

c:

8 30

25

20

15

10

3500
I

tr.~1

1-~~

....,J
c~~

ROI Type: 1

4000

4500

5000
Energy(kev)

5500

6000

Channel Data Report

8/9/2013

Page

12:37:2C wt

*******************************************************
s p E c TR AL DAT A R E P 0 R T *****
*****
*******************************************************
Sample Title:

03

Elapsed Live time:


Elapsed Real Time:

10200
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m2-77

Channel Data Report


369:

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2

Sample Title:

12:3'7tff
4

Page
2

03

Channe 1 I- - - - - - I - - - - - - - I - - - - - - - I - - - - - - - I - - - - - - - I - - - - - - - I - - - - - - - I - - - - - - - I
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3
1
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1
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1
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2
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1
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1
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1
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1
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1
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0
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1
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1
1
0
1
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1
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2
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1
0
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2
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1
2
1
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0
0
0
1
0
0
0
0
0

8278

Channel Data Report


801:

8/9/2611
0

Sample Title:

12:).IJiji
0

...,.
0

03

Channell------l-------1-------1-------1-------l-------l-------l-------I
809:
817:
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833:
841:
849:
857:
865:
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889:
897:
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913:
921:
929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:

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0
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0
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0
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fii 279

~Apex-Alpha"'

Sample Description:

Spectrum File:

Batch Identification:

Sample Identification:

Sample Geometry:

Procedure Description:

PZ-200-SS TOT
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000656
1307154A-RA
04
Shelf 2
Ra

Detector Name:

Alpha_036
Chamber Serial Number:

04026477B
Detector Serial Number:
84167
Env. Background:

System Bkgd 64054


Reagent Blank:

<not performed>
Sample Size:

Generic Mult. Factor:

Sample Date/Time:

Acquisition Date/Time:

Acquisition Live Time:

Acquisition Real Time:

l.OOOE+OOO +/- O.OOOE+OOO liter


2.120E+OOO
Generic Div. Factor:
7/19/2013
8:51:08 AM
8/9/2013
9:05:01 AM
170.0 minutes
175.7 minutes

Chem. Recovery Factor:

Counting Efficiency:

Effective Efficiency:

0.7765 +/0.1910 +/0.1483 +/-

Peak Match Tolerance:

Energy
(MeV)

2:31:37 PM

0.350 MeV

PEAK
Nuclide

0.0000

0.0033 on 7/20/2013
0.0026

l.OOOE+OOO

Net
Pk Area

AREA

REPORT

Pk Area
Error %

Ambient
Backgnd

FWHM
(keV)

Reagent
Backgnd

-------------------------------------------------------------------------------RA-224

RA-226

5.545
4.539

13.32
25.64

55.28
39.89

0.68
1. 36

O.OOE+OOO
O.OOE+OOO

3.0
3.0

NUCLIDE ANALYSIS RESULTS


Nuclide

Id
Conf.

Energy
(keV)

Activity
(pCi/liter )

MDA

(pCi/liter

-------------------------------------------------------------------------------RA-224
RA-226

0.975
0.924

5685.50*
4785.00*

5.34E-001 +/- 2.96E-001


9.71E-001 +/- 3.89E-001

2.26E-001 +/- 7.73E-003


2.60E-001 +/- 8.85E-003

0000065661.CNF

Live Time 10200.000 sec


Real Time 10543.800 sec
start:
1 3452. 9(kev)

stop : 1024 6474.2(kev)


Acq. start Fri Aug 09 09:05:01 2013

60
55

50

45

40

35

Vl

......
c:
:::3

8 30

25

20

15

10

' :i\

3500
~~~

f',)
()1:)1

.,...,,

11 .~

\I

41 ! 1

ROI Type: 1

4000

4500

5000
Energy(kev)

5500

6000

-----

Channel Data Report

8/9/2013

Page

12:37:1! JIM

*******************************************************
*****
s p E C T R A L DAT A R E P 0 R T *****
*******************************************************

Sample Title:

04

Elapsed Live time:


Elapsed Real Time:

10200
10544

Channell------l-------l-------1-------1-------1-------l-------l-------I
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ftJ282

Channel Data Report


369:

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0

Sample Title:

12:37:1.J
0

Page
0

04

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s2s3

Channel Data Report


801:

8/9/2013
0

Sample Title:

l~:

iii..,

:fl~~e

04

Channell------l-------l-------1-------1-------1-------l-------l-------I
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Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:

PZ-200-SS DIS
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000656

1307154A-RA

05

Shelf 2

Ra

Detector Name:
Chamber Serial Number:
Detector Serial Number:
Env. Background:
Reagent Blank:

Alpha_038

04026478B

91134

System Bkgd 64055

<not performed>

Sample Size:
Generic Mult. Factor:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:

l.OOOE+OOO +/- O.OOOE+OOO liter


2.640E+OOO
Generic Div. Factor:
7 /19/2013
8:51:08 AM

8/9/2013
9:05:03 AM

170.0 minutes

175.7 minutes

Chem. Recovery Factor:


Counting Efficiency:
Effective Efficiency:

0.9626 +/0.1722 +/0.1657 +/-

Peak Match Tolerance:

Energy
(MeV)

5:13:35 PM

0.350 MeV

PEAK
Nuclide

0.0000

0.0030 on 5/11/2013
0.0029

l.OOOE+OOO

Net
Pk Area

AREA

REPORT

Pk Area
Error %

Ambient
Backgnd

Reagent
Backgnd

61.26
30.57

0.85
1. 36

O.OOE+OOO
O.OOE+OOO

FWHM

(keV)

-------------------------------------------------------------------------------RA-224
RA-226

5.525
4.594

11.15
42.64

3.0

4.4

NUCLIDE ANALYSIS RESULTS


Nuclide

Id
Conf.

Energy
(keV)

Activity
(pCi/liter )

MDA

(pCi/liter

-------------------------------------------------------------------------------RA-224
RA-226

0. 967

0.954

5685.50*
4785.00*

4.98E-001 +/- 3.06E-001


l.80E+OOO +/- 5.54E-001

2.68E-001 +/- 9.23E-003


2.89E-001 +/- 9.96E-003

B28S

0000065658.CNF

Live Time :10200.000 sec


Real Time :10543. 700 sec
start:
1: 3482. 5(kev)

stop : 1024: 6501. 6(kev)

Acq. Start :Fri Aug 09 09:05:03 2013

60

55

50

45

40

35

V)

.j.....I

c:

:::::s

8 30

25

20

15

10

3500
t".li~I
~JI
(~)

ROI Type: 1

4000

4500

5000
Energy(kev)

r:

I~,

F1

M!1 !\~;

5500

6000

6500

Channel Data Report

8/9/2013

Page

12:37:39 PM

*******************************************************
s p E C T R A L DAT A R E P 0 R T *****
*****
*******************************************************

Sample Title:

05

Elapsed Live time:


Elapsed Real Time:

10200

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12:3"7:H
1

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8288

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0

Sample Title:

Page

12:i1.iii.
0

05

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0
0
0
0
0
0
0
0
1
0
0
1
0
1
1
0
1
0
0
0
0
0
0
0

3283

Sample Description:

Spectrum File:

Batch Identification:

Sample Identification:

Sample Geometry:

Procedure Description:

PZ-102-SS TOT
\\OR-ALPHAl\Canberra\Apex.Alpha\Root\Data\00000656
1307154A-RA
06
Shelf 2
Ra

Detector Name:

Alpha_039
Chamber Serial Number:

060273 96A
Detector Serial Number:
83109
Env. Background:

System Bkgd 64056


Reagent Blank:

<not performed>
Sample Size:

Sample Date/Time:

Acquisition Date/Time:

Acquisition Live Time:

Acquisition Real Time:

l.OOOE+OOO +/O.OOOE+OOO liter

7 /19/2013
8:51:08 AM

8/9/2013
9:05:04 AM

170.0 minutes
175.7 minutes

Chem. Recovery Factor:

Counting Efficiency:

Effective Efficiency:

0.3160 +/0.1965 +/0.0621 +/-

Peak Match Tolerance:

Energy
(MeV)

RA-224
RA-226

5.526
4.609

2:01:25 PM

0.350 MeV

PEAK

Nuclide

0.0000

0.0034 on 4/20/2013
0.0011

Net
Pk Area

AREA

REPORT

Pk Area
Error %

56.66
180.30

26 .13
14.68

Ambient
Backgnd
0.34
1. 70

Reagent
Backgnd

FWHM
(keV)

O.OOE+OOO
O.OOE+OOO

3.7
5.0

NUCLIDE ANALYSIS RESULTS

Nuclide

Id
Conf.

Energy
(keV)

RA-224
RA-226

0.967
0.960

5685.50*
4785.00*

Activity
(pCi/liter )
2.56E+OOO +/- 6.75E-001
7.69E+OOO +/- l.16E+OOO

MDA
(pCi/liter
2.16E-001 +/- 7.35E-003
3.13E-001 +/- l.06E-002

0000065677.CNF

Live Ti me 10200. 000 sec


Real Time 10543.800 sec
start:
1 3449. 7(kev)
stop : 1024 6497. l(kev)
Acq. Start Fri Aug 09 09:05:04 2013

60
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Vl
.j.-1

8 30
25
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15
10

5
0

3500
~m~

N
U:JI
i-'

ROI Type: 1

4000

4500

5000
Energy(kev)

5500

6000

6500

Channel Data Report

8/9/)0ll

l.i~,-~

~Me

*******************************************************
s p E C T R A L DAT A R E P 0 R T *****
*****
*******************************************************
Sample Title:

06

Elapsed Live time:


Elapsed Real Time:

10200
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__

....
fj?Q?

Channel Data Report


369:

8/9/2013
2

Sample Title:

12:37:
0

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!Q293

Channel Data Report


801:

8/9/2013
1

Sample Title:

12:37t .. ~
2

Page
1

06

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~~Apex-Alpha'"

Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:

PZ-102-SS DIS
\\OR-ALPHAl\Canberra\Apex.Alpha\Root\Data\00000656
1307154A-RA
07
Shelf 2
Ra

Detector Name:
Chamber Serial Number:
Detector Serial Number:
Env. Background:
Reagent Blank:

Alpha_040
06027396B
91135
System Bkgd 64057
<not performed>

Sample Size:
Generic Mult. Factor:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:

l.OOOE+OOO +/- O.OOOE+OOO liter


2.470E+OOO
Generic Div. Factor:
7/19/2013
8:51:08 AM
8/9/2013
9:05:06 AM
170.0 minutes
175.7 minutes

Chem. Recovery Factor:


Counting Efficiency:
Effective Efficiency:

1. 0000 +/-

0 .1900 +/0.1900 +/-

Peak Match Tolerance:

Energy
(MeV)

RA-224
RA-226

5: 49: 33 PM

0.350 MeV

PEAK

Nuclide

0.0000
0.0033 on 12/16/2012
0.0033

l.OOOE+OOO

Net
Pk Area

5.569
4.580

AREA

REPORT

Pk Area
Error %

17.15
90.49

48.68
20.67

Ambient
Backgnd
0.85
0.51

Reagent
Backgnd

FWHM
(keV)

O.OOE+OOO
O.OOE+OOO

3.0
3.7

NUCLIDE ANALYSIS RESULTS


Nuclide

Id
Conf.

Energy
(keV)

RA-224
RA-226

0.982
0.946

5685.50*
4785.00*

Activity
(pCi/liter )
6.25E-001 +/- 3.05E-001
3.12E+OOO +/- 6.53E-001

MDA
(pCi/liter
2.18E-001 +/- 7.44E-003
l.81E-001 +/- 6.15E-003

S295

0000065660.CNF

Live Time 10200.000 sec


Real Time 10543.800 sec
start:
1 3459.0(kev)

stop : 1024 6497. 3(kev)

Acq. Start Fri Aug 09 09:05:06 2013

60
55

50

45

40

35

.....
c:
V)

:::::s

8 30

25

20

15

10

5
0

3500

!\ !i~\!\ i'.,11i

J!\

la
1\11

UJI

ROI Type: 1

4000

4500

5000
Energy(kev)

5500

6000

6500

Channel Data Report

Page

8/9/2013

*******************************************************
S P E C T R A L
*****
DAT A
R E P 0 R T
*****
*******************************************************
Sample Title:

07

Elapsed Live time:


Elapsed Real Time:

10200
10544

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-~.M~l=iii

UL~!

Channel Data Report


369:

8/9/201)
0

Sample Title:

t~;lli.tt
2

w
0

Page
3

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1
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1
1
0
1
0
0
0
0
0
0
0
0
1
0
0
0
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1
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1
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0
0
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0
0
0
0
0
0
0
0
0

8298

Channel Data Report


801:

8/9/2013
0

Sample Title:

12:38:J,j
0

Page
0

07

Channell------l-------l-------l-------1-------1-------1-------l-------I
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0
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1
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1
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0
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0
0

8299

~~Apex-Alpha

Sample Description:

Spectrum File:

Batch Identification:

Sample Identification:

Sample Geometry:

Procedure Description:

PZ-107-SS TOT
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000656
1307154A-RA
08
Shelf 2
Ra

Detector Name:

Alpha_042
Chamber Serial Number:

05026930B
Detector Serial Number:
84185
Env. Background:

System Bkgd 64059


Reagent Blank:

<not performed>
Sample Size:

Generic Mult. Factor:

Sample Date/Time:

Acquisition Date/Time:

Acquisition Live Time:

Acquisition Real Time:

l.OOOE+OOO +/- O.OOOE+OOO liter


2.990E+OOO
Generic Div. Factor:
7/19/2013
8:51:08 AM
8/9/2013
9:05:07 AM
170.0 minutes
175.7 minutes

Chem. Recovery Factor:

Counting Efficiency:

Effective Efficiency:

0.7394 +/0.1846 +/0.1365 +/-

Peak Match Tolerance:

Energy
(MeV)

RA-224
RA-226

5.524
4.596

5:49:29 PM

0.350 MeV

PEAK
Nuclide

0.0000

0.0032 on 12/16/2012
0.0024

l.OOOE+OOO

Net
Pk Area

AREA

REPORT

Pk Area
Error %

33.81
110 .15

34.40
18.76

Ambient
Backgnd
1.19
0.85

Reagent
Backgnd

FWHM
(keV)

O.OOE+OOO
O.OOE+OOO

6.0
4.5

NUCLIDE ANALYSIS RESULTS


Nuclide

Id
Conf.

Energy
(keV) .

Activity
(pCi/liter )

MDA
(pCi/liter

-------------------------------------------------------------------------------RA-224
RA-226

0.967
0.955

5685.50*
4785.00*

2.08E+OOO +/- 7.18E-001


6.39E+OOO +/- l.22E+OOO

4.05E-001 +/- l.38E-002


3.47E-001 +/- l.18E-002

0000065659.CNF

Live Time 10200.000 sec


Real Time 10543.800 sec
1 3450.2(kev)
Start:
Stop : 1024 6505. 5(kev)
Acq. Start Fri Aug 09 09:05:07 2013

60+
55

50
45
40
35
Vl

......
c

:::3

8 30

25
20
15
10

5
0

3500
;~

t~
~'ll

I<""'

ROI Type: 1

4000

4500

5000
Energy(kev)

5500

6000

6500

Channel Data Report

8/9/2013

12:38:22

Page

!)llM

*******************************************************
s p E C T R A L DAT A R E P 0 R T *****
*****
*******************************************************
Sample Title:

08

Elapsed Live time:


Elapsed Real Time:

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10544

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1

fi3f:il2

Channel Data Report


369:

8/9/2013
2

Sample Title:

12:lN
0

.,
1

Page
0

08

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1
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0
1
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0
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0

1
1
3
0
1
0
1
1
1
0
0
0
0
0
0
1
1
0
0
0
0
0
1
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0
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0
0
2
0
0
0
1
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2
0
0
2
0
1
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0
0
0

1
0
0
1
1
1
0
1
1
0
0
0
0
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1
2
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1
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1
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1
0
1
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0

2
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0
2
1
0
1
2
0
0
0
0
1
1
0
0
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1
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1
1
2
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2
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0
2
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0
1
1
0
0
0
0
0
0
0
0
0
0

S3ri23

Channel Data Report


801:

8/9/2013
0

Sample Title:

Page

12:31.
0

08

Channell------l-------1-------1-------1-------l-------l-------l-------I
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969:
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985:
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1
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1
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0
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0
0
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1
0
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1
0
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0
0
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1
0
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1
2
0
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0
0
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0
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1
1
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1
0
0
2
1
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0
0
0
0
1
0
0
0
0
0
0
1
2
0
0
0

0
0
0
0
0
1
0
0
0
1
1
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0

0
0
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0
0
0
0
0
0
0
0
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0
0
1
0
0
0
0
0
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0

0
0
0
1
1
0
2
0
1
0
0
0
1
1
1
0
0
0
0
0
0
0
0
0

Sample Description:

Spectrum File:

Batch Identification:

Sample Identification:

Sample Geometry:

Procedure Description:

PZ-107-SS DIS
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000656
1307154A-RA
09
Shelf 2
Ra

Detector Name:

Alpha_045
Chamber Serial Number:

04026482A
Detector Serial Number:
91131
Env. Background:

System Bkgd 64060


Reagent Blank:

<not performed>
Sample Size:

Generic Mult. Factor:

Sample Date/Time:

Acquisition Date/Time:

Acquisition Live Time:

Acquisition Real Time:

l.OOOE+OOO +/- O.OOOE+OOO liter


2.640E+OOO
Generic Div. Factor:
7/19/2013
8:51:08 AM
8/9/2013
9:05:09 AM
170.0 minutes
170.0 minutes

Chem. Recovery Factor:

Counting Efficiency:

Effective Efficiency:

1.0000 +/0.1909 +/0.1909 +/-

Peak Match Tolerance:

Energy
(MeV)

2:31:26 PM

0.350 MeV

PEAK
Nuclide

0.0000
0.0033 on 7/20/2013
0.0033

l.OOOE+OOO

Net
Pk Area

AREA

REPORT

Pk Area
Error %

Ambient
Backgnd

Reagent
Backgnd

FWHM
(keV)

-------------------------------------------------------------------------------RA-224
RA-226

5.532
4.574

23.49
145.49

40.95
16.28

0.51
0.51

O.OOE+OOO
O.OOE+OOO

3.0

4.9

NUCLIDE ANALYSIS RESULTS


Nuclide

Id
Conf.

Energy
(keV)

Activity
(pCi/liter )

MDA

(pCi/liter

-------------------------------------------------------------------------------RA-224
RA-226

0.970
0.943

5685.50*
4785.00*

9.llE-001 +/- 3.74E-001


5.33E+OOO +/- 8.87E-001

2.04E-001 +/- 6.96E-003


l.92E-001 +/- 6.55E-003

0000065654.CNF

Live Time 10200.000 sec


Rea1 Ti me 10200 .100 sec
start:
1 3453.7(kev)
stop : 1024 6489.S(kev)
Acq. Start Fri Aug 09 09:05:09 2013

60
55

50

45

40

35

V)

.j....I

c:

:::J

8 30

25

20

15

10

3500
I

~!JI
~..Ji

ti-~

CU")!

ROI Type: 1

4000

4500

5000
Energy(kev)

5500

6000

Channel Data Report

8/9/2013

12~iiiii

Page

*******************************************************
s p E C T R A L DAT A R E P 0 R T *****
*****
*******************************************************
Sample Title:

09

Elapsed Live time:


Elapsed Real Time:

10200
10200

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3

s3m1

Channel Data Report


369:

8/9/2013
1

Sample Title:

l~;il~)i

Pa~

09

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2
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0

fj3fl8

Channel Data Report


801:

8/9/2013
0

Sample Title:

12:311j.f
0

Page
0

09

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Sample Description:

Spectrum File:

Batch Identification:

Sample Identification:

Sample Geometry:

Procedure Description:

PZ-106-KS TOT
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000656
1307154A-RA
10
Shelf 2
Ra

Detector Name:

Alpha_046
Chamber Serial Number:

04026482B
Detector Serial Number:
58762
Env. Background:

System Bkgd 64061


Reagent Blank:

<not performed>
Sample Size:

Generic Mult. Factor:

Sample Date/Time:

Acquisition Date/Time:

Acquisition Live Time:

Acquisition Real Time:

l.OOOE+OOO +/- O.OOOE+OOO liter


2.500E+OOO
Generic Div. Factor:
7/19/2013
8:51:08 AM
8/9/2013
9:05:10 AM
170.0 minutes
170.0 minutes

Chem. Recovery Factor:

Counting Efficiency:

Effective Efficiency:

0.9598 +/0.1789 +/0.1717 +/-

Peak Match Tolerance:

Energy
(MeV)

RA-224
RA-226

5:49:23 PM

0.350 MeV

PEAK
Nuclide

0.0000
0.0031 on 12/16/2012
0.0030

l.OOOE+OOO

Net
Pk Area

5.556
4.679

AREA

REPORT

Pk Area
Error %

2.83
8.66

120.53
68.12

FWHM
(keV)

Ambient
Backgnd

Reagent
Backgnd

0.17
0.34

O.OOE+OOO
O.OOE+OOO

3.0
3.0

NUCLIDE ANALYSIS RESULTS


Nuclide

Id
Conf.

Energy
(keV)

RA-224
RA-226

0.978
0.985

5685.50*
4785.00*

Activity
(pCi/liter )
l.16E-001 +/
3.34E-001 +/

l.39E-001
2.28E-001

MDA
(pCi/liter
l.70E-001 +/
l.84E-001 +/

5.88E-003
6.34E-003

0000065655.CNF

Live Time 10200 .000 sec


Rea1 Ti me 10200 .100 sec
start:
1 3453.7(kev)
stop : 1024 6515 .4(kev)
Acq. Start Fri Aug 09 09:05:10 2013

60
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Vl

......
s::::

8 30
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5
0

\I,

3500
~2~1
~~,JI
Uto0i.11t.
~ofto.11!

!_

i~

!J

I ll

,!.

ROI Type: 1

4000

4500

5000
Energy(kev)

5500

6000

6500

Channel Data Report

8/9/2013

12: 38 t)...

Page

*******************************************************
s p E C T R A L DAT A R E P 0 R T *****
*****
*******************************************************
Sample Title:

10

Elapsed Live time:


Elapsed Real Time:

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8312

Channel Data Report


369:

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~iiU~ ..
0

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Channel Data Report


801:

8/9/2013
0

Sample Title:

Page

12:31t'i.
0

10

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1314

~~Apex-Alpha'"

Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:

Shelf 2
Ra

Detector Name:
Chamber Serial Number:
Detector Serial Number:
Env. Background:
Reagent Blank:

Alpha_047
02030596A
91086
System Bkgd 64062
<not performed>

PZ-106-KS DIS
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000656
1307154A-RA
11

Sample Size:
Generic Mult. Factor:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:

l.OOOE+OOO +/- O.OOOE+OOO liter


2.610E+OOO
Generic Div. Factor:
7/19/2013
8:51:08 AM
8/9/2013
9:05:12 AM
170.0 minutes
170.0 minutes

Chem. Recovery Factor:


Counting Efficiency:
Effective Efficiency:

1.0000 +/0.1822 +/0.1822 +/-

Peak Match Tolerance:

Energy
(MeV)

RA-224
RA-226

5:49:21 PM

0.350 MeV

PEAK

Nuclide

0.0000
0.0032 on 12/16/2012
0.0032

l.OOOE+OOO

Net
Pk Area

5.479
4.639

AREA

REPORT

Pk Area
Error %

3.83
9.32

102.72
66.89

Ambient
Backgnd

Reagent
Backgnd

FWHM
(keV)

0.17
0.68

O.OOE+OOO
O.OOE+OOO

2.9
2.9

NUCLIDE ANALYSIS RESULTS


Nuclide

Id
Conf.

Energy
(keV)

RA-224
RA-226

0.946
0.972

5685.50*
4785.00*

Activity
(pCi/liter )
l.54E-001 +/- l.58E-001
3.54E-001 +/- 2.37E-001

MDA
(pCi/liter
l.68E-001 +/- 5.77E-003
2.14E-001 +/- 7.35E-003

ti315

0000065656.CNF

Live Time :10200.000 sec

Real Time :10200.000 sec

Start:
1:3457.9(kev)

Stop : 1024: 6467. 7(kev)

Acq. Start :Fri Aug 09 09:05:12 2013

60
55

50

45

40

35

VI

.f.-1

c:

:::::s

8 30

25

20

15

10

0
3500
I

(Ii~

~--~

Ji-""ib'

tn

ROI Type: 1

!. .~

IA

!,

4000

4500

5000
Energy(kev)

5500

6000

Channel Data Report

Jilage

8/9/2613

*******************************************************
R E P 0 R T
S P E C T R A L
DAT A
*****
*****
*******************************************************
Sample Title:

11

Elapsed Live time:


Elapsed Real Time:

10200
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fii318

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Sample Title:

12

38 ;.

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1319

Sample Description:

Spectrum File:

Batch Identification:

Sample Identification:

Sample Geometry:

Procedure Description:

DUP 08 TOT
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000656
1307154A-RA
12
Shelf 2
Ra

Detector Name:

Alpha_048
Chamber Serial Number:

02030596B
Detector Serial Number:
83111
Env. Background:

System Bkgd 64063


Reagent Blank:

<not performed>
Sample Size:

Generic Mult. Factor:

Sample Date/Time:

Acquisition Date/Time:

Acquisition Live Time:

Acquisition Real Time:

l.OOOE+OOO +/- O.OOOE+OOO liter


2.370E+OOO
Generic Div. Factor:
7/19/2013
8:51:08 AM
8/9/2013
9:05:14 AM
170.0 minutes
170.0 minutes

Chem. Recovery Factor:

Counting Efficiency:

Effective Efficiency:

0.8490 +/0.1680 +/0.1426 +/-

Peak Match Tolerance:

Energy
(MeV)

RA-224
RA-226

5.505
4.575

5:49:20 PM

0.350 MeV

PEAK
Nuclide

0.0000

0.0030 on 12/16/2012
0.0025

l.OOOE+OOO

Net
Pk Area
33.32
120.83

AREA

REPORT

Pk Area
Error %

Ambient
Backgnd

Reagent
Backgnd

FWHM
(keV)

34.36
17.85

0.68
0.17

O.OOE+OOO
O.OOE+OOO

3.0
4.9

NUCLIDE ANALYSIS RESULTS


Nuclide

Id
Conf.

Energy
(keV)

RA-224
RA-226

0.958
0.944

5685.50*
4785.00*

Activity
(pCi/liter )
l.55E+OOO +/
5.32E+OOO +/

5.36E-001
9.67E-001

MDA
(pCi/liter
2.63E-001 +/
l.84E-001 +/

9.13E-003
6.36E-003

---

0000065657.CNF

Live Time 10200.000 sec


Rea1 Ti me 10200. 000 sec
1 3453.0(kev)
Start:
stop : 1024 6472.l(kev)
Acq. Start Fri Aug 09 09:05:14 2013

60+
55

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V>
.j....I

s:::

:::I

8 30

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W!JI
t..l!
~Jt
~'"'I'

ROI Type: 1

4000

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5000
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5500

6000

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8/9/20'.tl

Page

12:)fJij

*******************************************************
s p E C T R A L DAT A R E P 0 R T *****
*****
*******************************************************
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i324

.A

-===/""\pex- Al pha

TM

Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:

Sample Geometry:

Procedure Description:

DUP 08 DIS
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000656
1307154A-RA
13
Shelf 2
Ra

Detector Name:

Alpha_Ol8
Chamber Serial Number:

Detector Serial Number:


18
Env. Background:

System Bkgd 64042


Reagent Blank:

<not performed>
Sample Size:

Generic Mult. Factor:

Sample Date/Time:

Acquisition Date/Time:

Acquisition Live Time:

Acquisition Real Time:

l.OOOE+OOO +/- O.OOOE+OOO liter


2. 770E+OOO
Generic Div. Factor:
7 /19/2013
8:51:08 AM
8/9/2013
9:26:50 AM
170.0 minutes
170.0 minutes

Chem. Recovery Factor:

Counting Efficiency:

Effective Efficiency:

0.9285 +/0.1776 +/0.1649 +/-

Peak Match Tolerance:

Energy
(MeV)

1:57:26 PM

0.350 MeV

PEAK
Nuclide

0.0000

0.0033 on 12/15/2012
0.0031

l.OOOE+OOO

Net
Pk Area

AREA

REPORT

Pk Area
Error %

Ambient
Backgnd

Reagent
Backgnd

3.74

O.OOE+OOO
O.OOE+OOO

FWHM
(keV)

-------------------------------------------------------------------------------RA-224

RA-226

5.512
4.575

13 .26
114. 47

62.08
18.46

1. 53

0.0

6.3

NUCLIDE ANALYSIS RESULTS


Nuclide

Id
Conf.

Energy
(keV)

Activity
(pCi/liter )

MDA

(pCi/liter

-------------------------------------------------------------------------------RA-224
RA-226

0.961
0.944

5685.50*
4785.00*

6.25E-001 +/- 3.88E-001


5.09E+OOO +/- 9.59E-001

4.52E-001 +/- l.65E-002


3.16E-001 +/- l.15E-002

0000065666.CNF
Live Ti me :10201. 000 sec
Real Ti me :10201. 000 sec
start:
1: 3404. l(kev)
stop : 1024:6604.2(kev)
Acq. Start :Fri Aug 09 09:26:50 2013

55
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45
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35
VI
.f-J

c:

:::J

8 30

25
20
15
10

5
0

3500

4000

Ii':~

C11'11

ROI Type: 1

4500

5000
Energy(kev)

5500

6000

6500

Channel Data Report

Page

8/9/2013

*******************************************************
*****
S P E C T R A L
DAT A
R E P 0 R T
*****
*******************************************************
Sample Title:

13

Elapsed Live time:


Elapsed Real Time:

10201
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1
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1
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0
0
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1
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1
0
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1
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0
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0
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4

1
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1
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1
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1
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1
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1
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2

1327

Channel Data Report


369:

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0

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Page

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13

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1
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0
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1
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0
0
0
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0
0
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0
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0
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0

0
1
1
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2
0
2
1
0
0
0
0
0
0
0
0
1
0
0
0
0
0
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0
1
0
0
0
0
0
2
0
0
0
0
0
1
0
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1
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0
0
0
0
0
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0
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0
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1

0
0
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1
0
2
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1
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0
0
0
0
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0
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1
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1
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0
0
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1
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1
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2
1
1
0
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1
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1
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0
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1
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0
1
1
4
0
0
3
0
0
0
0
0
1
0
0
0
0
0
0
0
0
1
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0
0
1
0
0
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0
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1
0
0
0
0
0
1
0
0
0
1
0
0
1
0
0
0
0
0
0
0
0

0
0
1
1
0
2
1
0
0
0
2
1
0
1
0
0
1
0
0
0
0
1
1
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1
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0
0
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1
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1
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0
0
1
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1
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0
0
0
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0
0
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2
2
1
1
1
1
0
1
0
0
0
1
0
1
1
0
0
0
0
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0
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1
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1
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0
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1
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0
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1
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0
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0
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1
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1
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0
1
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
1
1
0
0
0
0
0

E328

Channel Data Report


801:

8/9/2013
0

Sample Title:

12:39. . .
0

Page

Iii
0

13

Channell------l-------1-------1-------1-------l-------l-------l-------I
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0
1
0
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0
0
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0
0
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0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
1
0
0
0
0
0
0
0
1
0

1
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
1
0
0

0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
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0
0

0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0

8329

Page 1 of 2
8/9/2013

5:22:10 AM

QA SUMMARY REPORT
Review Of QA Results - Pulser Check
Date
Time

: 8/9/2013
: 5:22:10 AM

CHAMBER
Alpha 001
Alpha 002
Alpha 003
Alpha 004
Alpha 005
Alpha 006
Alpha 007
Alpha 008
Alpha 009
Alpha 010
Alpha 011
Alpha 012
Alpha 013
Alpha 014
Alpha 015
Alpha 016
Alpha 017
Alpha 018
Alpha 019
Alpha 020
Alpha 021
Alpha 022
Alpha 023
Alpha 024
Alpha 025
Alpha 026
Alpha 027
Alpha 028
Alpha 029
Alpha 030
Alpha 031
Alpha 032
Alpha 033
Alpha 034
Alpha 035
Alpha 036
Alpha 037
Alpha 038
Alpha 039
Alpha 040
Alpha 041
Alpha 042

DEVICE
21f
21f
21f
21f
21f
21f
21f
21f
21f
2lf
21f
21f
21f
21f
21f
21f
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
Alpha Analyst 1OODC
Alpha AnalystlOODC
Alpha AnalystlOODC
Alpha AnalystlOODC
Alpha AnalystlOODC
Alpha AnalystlOODC
Alpha AnalystlOODC
Alpha AnalystlOODC
Alpha AnalystlOODC
Alpha AnalystlOODC

PARAMETER
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
Peak Energy
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
Peak CPS
ALL
ALL
PeakFWHM
ALL
ALL
ALL
ALL

FLAG
Not Done
Not Done
Passed
Passed
Not Done
Not Done
Not Done
Not Done
Not Done
Passed
Passed
Passed
Passed
Passed
Action
Not Done
Not Done
Passed
Passed
Not Done
Not Done
Passed
Passed
Passed
Passed
Not Done
Passed
Not Done
Passed
Not Done
Passed
Not Done
Passed
Passed
Action
Passed
Not Done
Action
Passed
Passed
Passed
Passed

DATE

8/9/2013 5:06:27 AM
8/9/2013 5:06:28 AM

8/9/2013
8/9/2013
8/9/2013
8/9/2013
8/9/2013
8/9/2013

5:06:29 AM
5:06:30 AM
5:06:31 AM
5:06:31 AM
5:06:32 AM
5:06:33 AM

8/9/2013 5:06:34 AM
8/9/2013 5:06:35 AM

8/9/2013
8/9/2013
8/9/2013
8/9/2013

5:06:35 AM
5:06:36 AM
5:06:37 AM
5:06:38 AM

8/9/2013 5:06:39 AM
8/9/2013 5:06:39 AM
8/9/2013 5:06:40 AM
8/9/2013
8/9/2013
8/9/2013
8/9/2013

5:06:41
5:06:43
5:06:44
5:06:46

AM
AM
AM
AM

8/9/2013
8/9/2013
8/9/2013
8/8/2013
8/9/2013

5:06:48 AM
5:06:50 AM
5:06:53 AM
5:39:00 AM
5:06:55 AM

Page 2 of 2

CHAMBER
Alpha 043
Alpha 044
Alpha 045
Alpha 046
Alpha 047
Alpha 048

Review of QA ~It$ - ~ ~

DEVICE
Alpha AnalystlOODC
Alpha AnalystlOODC
Alpha AnalystlOODC
Alpha Analyst! OODC
Alpha AnalystlOODC
Alpha AnalystlOODC

FLAG

PARAMETER
ALL
ALL
ALL
ALL
ALL
ALL

Not Done
Not Done
Passed
Passed
Passed
Passed

8/9/2013 5:22:10 AM
DATE

8/9/2013
8/9/2013
8/9/2013
8/9/2013

5:06:58 AM
5:07:00 AM
5:07:03 AM
5:07:05 AM

APPROVED BY:

APPROVAL DATE:

/Cf(()

8331

6/12/12

Library Listing Report

Page

12:16:17 PM

*************************************************************************
*****
L I B R A R Y L I S T I N G R E P 0 R T
*****
*************************************************************************
Nuclide Library Title:

Radium

Nuclide Library Description:


Nuclide
Name

Half-Life
(Seconds)

P0-218
RN-222
RA-226

5.049E+Ol0
5.049E+010
5.049E+Ol0

Energy
(keV )

Ra-226, Po-218, Rn-222

Energy
Uncert. (keV

0.000
0.000
0.000

6003.000*
5490.000*
4785.000*

* =key line
TOTALS:

Nuclides

Energy Lines

Yield
( %)
99.9800
99.9200

100.0000

Yield
Uncert. (Abs . +-)
0.0000

0.0000
0.0000

SECTION XI

ANALYTICAL DATA (RADIUM-228)

Eberline Services
Oak Ridge Laboratory
Analysis Sheet

Printed: 811512013 7:20 AM


Page 1of3

13-07154
Ra228
Run 1

Sample
Desc

Client
ID

Login
CPM

Sample
Date

Sample
Aliquot

13-07154

Internal
Fraction

Ra228

01

LCS

LCS

07 /24/13 00:00

1.0000E+OO

02

MBL

BLANK

07/24/13 00:00

1.0000E+OO

7/22/2013

03

I DUP

07/19/13 12:10

1.0000E+OO

Lab Deadline I

8/13/2013

04

TRG

07/19/13 10:19

1.0000E+OO

05

: TRG-

07/19/13 10:19

1.0000E+OO

07/19/13 10:30

1.0000E+OO

07/19/13 10:30

1.0000E+OO

Work Order

I
I

Analysis Code

--"------~----~

Run
Date Received

Client I Engineering Management Support, Inc.

PZ-107-SS TOT
PZ-200-SS TOT

PZ-200-SS DIS

46
I
I

42

-1
I

42
-

Project I

West Lake OU-1

TRG

06

...

Report Level

07

Activity Units

pCi

08

PZ-102-SS TOT

38
I

TRG

PZ-102-SS DIS

DO

PZ-107-SS TOT

46

07/19/13 12:10

1.0000E+OO

38

..

Aliquot Units
Matrix

WA

09

TRG

PZ-107-SS DIS

46

07/19/13 12:10

1.0000E+OO

10

TRG ,

PZ-106-KS TOT

45

07/19/13 13:09

1.0000E+OO

PZ-106-KS DIS

45

07 /19/13 13:09

1.0000E+OO

Method

E904.0

11

I
I TRG
I

Alpha/Beta GPC

12

Radiometric Tracer

Ba-133

13

Radiometric Sol#

Ba-6a

Tracer Act (dpm/g)

990.223

Instrument Type

--

------~---

I TRG

DUP 08 TOT

44

07 /19/13 00:00

1.0000E+OO

DUP 08 DIS

44

07/19/13 00:00

1.0000E+OO

--

TRG

I
I

Carrier
Carrier Cone (mg/ml)

Yttirum

34

m
(,,JI

Jl'.,.J1
i~,

SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only.

Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.

Eberline Services
Oak Ridge Laboratory
Analysis Sheet

Printed: 8/15/2013 7:20 AM


Page 2 of 3

13-07154
Ra228
Run 1

Internal
Fraction

01

Sample
Desc

Tracer
Aliquot (g)

I
I

Tracer Total
ACT(dpm)

i Radiometric Grav Carrier

Radiometric
Tracer (pCi)

%Rec

Added(ml)

Grav Filter
Tare (g)

LCS

0.9259

Grav Filter
Net(g)

Grav Filter
Final (g)

Grav
%Rec

Mean
%Rec

I
I

916.8

438.4

106.15

2.000

0.09201

2.000

0.0917\

SAF
1*

SAF
2*

0.145~ 0.0539

79.26

84.14

1.00

1.00

0.1494

0.0577

84.85

81.88

1.00

1.00

0.1476

0.0560

82.351

62.541

1.00

1.00
1.00

--~~-

02

MBL

906.2

0.9151

96.50

393.9

---

03

DUP

~-----

907.4

0.9164

75.94

310.4

2.000

0.0916]
.

04

TRG

0.9147

905.8

316.8

77.65

2.000

0.09251

0.1481

0.0556

81.76

63.49

1.00

05

TRG

0.9134

904.5

392.2 I

96.26

2.000

0.092~

0.1489

0.0563

82.79

79.70

1.00 I 1.00

06

TRG

0.9122 '

903.3

128.6

31.61

2.000

0.0922

0.1493

0.0571

83.97

26.54

1.00

1.00
1.00

..

07

TRG

0.9120

903.1

08

DO

0.9118

902.9

09

TRG

0.9102

901.3

101.57

2.000

0.0922

300.7

73.94

2.000

407.9

100.47

2.000

413.2
I

0.1480

0.0558

82.06

83.35

1.00

0.09241

0.1495

0.0571

83.97

62.08

1.00 I 1.00

0.0919

0.1475

0.0556

81.76

82.15

1.00

1.00

..

10

TRG

0.9126

11

TRG

0.9091

903.7

390.7

95.98

2.000

0.0920

0.1474

0.0554

81.47

78.20

1.00

1.00

900.2

418.0

103.08

2.000

0.0924

0.1472

0.0548

80.59

83.07

1.00

1.00

899.0

343.8

84.90

2.000

0.0918

0.1475

0.0557

81.91

69.54

1.00

1.00

75.51

1.00

1.00

12

TRG

0.9079

. -+

13

TRG

0.9079

899.0

376.0

92.85

2.000

0.0920

0.1473

0.0553

81.32

I
I
I

--'~--

--

--~

I
I

~"
(,.,JI
t ..:i1
Mil

SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only.

**Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.

-~

Eberline Services
Oak Ridge Laboratory
Analysis Sheet

Printed: 811512013 7:20 AM


Page 3 of 3

13-07154

Ra228

Run 1

Internal
Fraction

Sample
Desc

01

LCS

02

MBL

Rough Prep
Date

Rough Prep
By

Prep
Date

Prep
By

Sep to
Date/Time

08/07/13 10:34

JWOLFE

08/08/13 14:54

08/07/13 10:34

JWOLFE

08/08/13 14:54

II

Sep to
By

Sep t1
Date/Time

Sep t1
By

LWALKER ; 08/15/13 04:18

TSMITH

LWALKER

08/15/13 04: 18

TSMITH

-----

03

DUP

08/07 /13 10:34

JWOLFE

08/08/13 14:54

LWALKER

08/15/13 04:18

TSMITH

04

TRG

08/07/13 10:34

JWOLFE

08/08/13 14:54

LWALKER

08/15/13 04:18

TSMITH

08/15/13 04: 18

TSMITH

08/15/13 04: 18

TSMITH

LWALKER I 08/15/13 04:18

TSMITH

---

--

05

TRG

08/07/13 10:34

JWOLFE

06

08/08/13 14:54

LWALKER
-

TRG

08/07 /13 10:34

JWOLFE

08/08/13 14:54 ' LWALKER

07

TRG

08/07/13 10:34

-----

JWOLFE

08/08/13 14:54

08

08/07/13 10:34

DO

JWOLFE

08/08/13 14:54

LWALKER

08/15/13 04: 18

TS MITH

09

TRG

08/07/13 10:34

JWOLFE

08/08/13 14:54

LWALKER

08/15/13 04:18

TSMITH

08/07 /13 10:34

JWOLFE

08/08/13 14:54

LWALKER

08/15/13 04:18

TSMITH

08/08/13 14:54

LWALKER

08/15/13 04:18

TSMITH

----

10

TRG

11

TRG

08/07/13 10:34

JWOLFE
.

12

TRG

08/07 /13 10:34

JWOLFE

08/08/13 14:54

LWALKER

08/15/13 04: 18

TSMITH

13

TRG

08/07/13 10:34

JWOLFE

08/08/13 14:54

LWALKER

08/15/13 04:18

TS MITH

I!

--
i

t!.1'~

(ol
~,.JI

C!l'll

SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only.

Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.

(
i::

Printed: 8/15/2013 10:33 AM

Page 1of3

Preliminary Data Report & Analytical Calculations

Eberline Services
Oak Ridge Laboratory

Work Order: 13-07154-Ra228-1

LCS
Known

LCS
%R

LCS
Flag

93.86

OK

RPO
Flag

MDA
Flag

Lab
Fraction

Nuclide

Sample
Oesc

Client
Identification

Activity
Units

01

RA-228

LCS

LCS

pCl/I

8.26E+OO

1.74E+OO

1.74E+OO

02

RA-228

MBL

BLANK

pCl/I

5.94E-01

4.97E-01

9.90E-01

03

RA-228

DUP

PZ-107-SS TOT

pCl/I

2.54E+OO

8.16E-01

1.45E+OO

TRG

PZ-200-SS TOT

pCl/I

1.95E+OO

7.20E-01

1.30E+OO

OK

PZ-200-SS DIS

pCl/I

1.77E+OO

6.04E-01

1.08E+OO

OK

~RG

PZ-102-SS TOT

pCl/I

5.39E+OO

1.88E+OO

3.39E+OO

INV

TRG

PZ-102-SS DIS

pCl/I

1.88E+OO

6.35E-01

1.15E+OO

OK

DO

PZ-107-SS TOT

pCl/I

3.03E+OO

8.36E-01

1.44E+OO

OK

PZ-107-SS DIS

pCi/I

2.38E+OO

6.32E-01

1.08E+OO

OK

PZ-106-KS TOT

pCi/I

2.22E-01

6.03E-01

1.27E+OO

OK

Results

Error Estimate

MDA

8.80E+OO

Blank
Flag

OK
OK

OK

0::

~
0
u

"""""

co

N
N

04
r-----

05
--~

ca

a::

RA-228

NA

OK

----

~-------

RA-228

TRG

~-----------i--- -

06

RA-228

07

RA-228

- - -r - - - - - - - - - - - -

--

- - - - - f-------------

08

RA-228

- -- - - - - -

09

RA-228

10

TRG

-~-2~

--

11

RA-228

TRG

PZ-106-KS DIS

pCl/I

2.73E+OO

7.07E-01

1.23E+OO

OK

RA-228

TRG

DUP 08 TOT

pCi/I

3.84E+OO

8.72E-01

1.47E+OO

OK

RA-228

TRG

DUP 08 DIS

pCl/I

2.68E+OO

7.26E-01

1.26E+OO

OK

12
d

.5

13
-

~
0

c.
c.

=+

::I

en

....c:

Cll

~I

U1

E
Cll

en

ca
c:
ca

:::!l
en
c:
;:
Cll
Cll

en

w
~~
t,.~

(,,.JI

"'..Ji

-----1---

.5
c:

--- - - - - - - -r
I

~----

(
t:

Work Order: 13-07154-Ra228-1

Radiometric
%Rec

Grav
%Rec

Mean
%Rec

Sep 10
DatefTime

Sep 11
DatefTime

Lab
Fraction

Nuclide

Sample
Oesc

Sample
Date

Sample
Aliquot

01

RA-228

LCS

07/24/13 00:00

I 1.00E+OO

106.15

79.26

84.14

1.00

8/8/2013 14:54

8/15/2013 4:18

RA-228

t-:BL

1.00E+OO

96.50

84.85

81.88

1.00

8/8/2013 14:54

8/15/2013 4:18

1.00E+OO

75.94

82.35

62.54

1.00

8/8/2013 14:54

8/15/2013 4:18

02
or

Printed: 8/15/2013 10:33 AM

Page 2 of 3

Preliminary Data Report & Analytical Calculations

Eberline Services
Oak Ridge Laboratory

--------- -

03

07/24/13 00:00
---

SAF

---

RA-228

DUP

07/19113 12:10

RA-228

TRG

07/19/13 10:19

1.00E+OO

77.65

81.76

63.49

1.00

8/8/2013 14:54

8/15/2013 4:18

- - - -----

{:

co

.!!!

N
N

ca

..5

04
--

05

RA-228

TRG

07/19/13 10:19

1.00E+OO

96.26

82.79

79.70

1.00

8/8/2013 14:54

8/15/2013 4:18

06

RA-228

TRG

07/19/13 10:30

1.00E+OO

31.61

83.97

26.54

1.00

8/8/201314:54

8/15/2013 4:18

07

RA-228

-+TRG

07/1911310:30

1.00E+OO

101.57

82.06

83.35

1.00

8/8/2013 14:54

8/15/2013 4: 18

08

RA-228

DO

07/19/13 12:10

1.00E+OO

73.94

83.97

62.08

1.00!

8/8/2013 14:54

8/15/2013 4:18

09

RA-228

TRG

07/19/13 12:10

1.00E+OO

100.47

81.76

82.15

1.00

8/8/201314:54

8/15/2013 4:18

10

RA-228

TRG

07/19/13 13:09

1.00E+OO

95.98

81.47

78.20

1.00

8/8/2013 14:54

8/15/2013 4:18

11

RA-228

TRG

07/19/13 13:09

1.00E+OO

103.08

80.59

83.07

1.00

8/8/2013 14:54

8/15/2013 4:18

12

RA-228

TRG

07/19/13 00:00

1.00E+OO

84.90

81.91

69.54

1.00

8/8/201314:54

8/15/2013 4:18

TRG

07/19/13 00:00

1.00E+OO

92.85

81.32

75.51

1.00

8/8/2013 14:54

8/15/2013 4: 18

1 _

c.
c.
:::s

en
c:

_!_3__ --~~228_ _

-t'

- -

-----------r=

~--

_j__

----~+-------------------

Q)

i:

(.)

E
Q)

Cl

ca
c:
ca

----~--------------i-------

Cl

---+------~---

Q)
Q)

.:Cl
c:

w
Cfl~~I
~..ii

o~

:ii:
c:
;:

t:.rJ

------~--------------1---

~---

----------+
I

~---~-,

Lab

Fraction

01
02

c:

Q:

--~--------

"""""
---

~
0

.!!!

~
<II
c:

ct

00
N
N

cu

Work Order: 13-07154-Ra228-1

Nuclide

Sample
Desc

Counting
DatefTlme

RA-228

LCS

RA-228

Halflife
(days)

Count
Time

Detect

Carrier

08/15/13 07:52

L64110A

02

30

M6L

08/15/13 07:50

L64110R

A1

RA-228

DUP

08/15/13 07:50

LB4110R

RA-228

TRG

08/15/13 07:50

RA-228

TRG

Counts

Bkg
CPM

Eff

1.45

0.4682

120

143 0.883333333

0.4776

A2

120

249 1.083333333

0.4699

L64110R

A3

120

207 0.933333333

0.4809

08/15/13 07:50

L64110R

A4

120

224 0.983333333

0.4732

08/15/13 07:51

L64110R

61

120

238 1.083333333

0.4754

L64110R

62

120

258 1.183333333

0.4658

184

----

~----~

::,

Printed: 8/15/2013 10:33 AM

Page 3 of 3

Preliminary Data Report & Analytical Calculations

Eberline Services
Oak Ridge Laboratory

03
~---- ~

04
----

05

---

f-----

06

a:::

RA-228

TRG

RA-228

TRG

--

07
----- ----- --

08

08/15/13 07:51

RA-228

DO

08/15/13 07:51

L64110R

63

120

267

1.05

0.4713

RA-228

TRG

08/15/13 07:51

L64110R

64

120

276 1.066666667

0.4773

RA-228

TRG

08/15/13 07:50

L64110R

C1

120

169

1.3

0.4705

11

RA-228

TRG

08/15/13 07:50

L64110R

C2

120

333 1.366666667

0.4676

12

RA-228

TRG

08/15/13 07:50

L64110R

C3

120

356 1.333333333

0.4614

RA-228

TRG

08/15/13 07:50

L64110R

C4

120

296

0.4714

------!--

09 .____
______
10
----~-!--

13

.E
~

-----r--

c..
c..

---.,~----

----

::s

(/)

c:

c
QI
E
QI

Ol

---

Ill

c
Ill
:!:

- - - - - - - -f - -

Ol

;:

>----- f-

QI
QI

o,
c
w
a~

tJI
f"~~

00!

-------TI ---------

1.2

Count Room Report


Client: Engineering Management Su

Internal
Fraction

Sample
Desc

01

LCS

Client
ID

'

02
03

. _i________

MBL I
i
i
DUP i

LCS

Sample
Date

05
06

TRG
TRG

Tracer
Aliquot (g)

0.9259

Tracer
ACT(dpm)

Radiometric
Tracer (pCi)

916.8475

BLANK

07/24/13 00:00 !

1.0000

0.9151

906.1531

PZ-107-SS TOT

07/19/13 12:10 I - 1.0000

PZ-200-SS TOT

l~--

;: I -

PZ-200-SS DIS
PZ-102-SS TOT

07/19/13 10:19

0.9164

907.4404

0.9147

PZ-107-SS TOT

TRG
.

393.9000

96.50 I 1.00

1.00

0.9134

07/19/13 10:30 !

0.9122

904.4697

310.4000

75.94 I 1.00 i 1.00

316.8000

77.65 I

~ .00

I 1.00

392.2000

96.26 I 1.00

1.00

128.6000

31.61

----

903.2814
____

----

07/19/1310:~000
1.0000

905.7570

SAF
2

1.00

--

1.0000

-1.00

'1

1.00

PZ-102-SS DIS
DO

'

SAF
1

106.15 Ii 1.00

-1

07/19/13 10:30
07/19/13 12:10

1.0000
I

0.9120

903.0834

413.2000

101.57 I 1.00
I

..

1.0000

0.9118

902.8853

09

Radiometric
%Rec

438.4000

07
08

Sample
Aliquot

07/24/13 00:0~:0000

04

Printed: 8/15/2013 7:20 AM


Page 1of1

13-07154-Ra228-1 (pCi/I) in WA
Tracer ID: Ba-Sa

300.7000

73.94

PZ-107-SS DIS

07/19/13 12:10

1.0000

0.9102

901.3010

407.9000

1.00

--

1.00

100.47 I 1.00

1.00
1.00

~-.

10

TRG

PZ-106-KS TOT

07/19/13 13:09

1.0000

0.9126

903.6775

390.7000

95.98

1.00

1.00

11

TRG

PZ-106-KS DIS

07/19/13 13:09

1.0000

0.9091

900.2117

418.0000

103.08

1.00

1.00

12

TRG

DUP 08 TOT

07/19/13 00:00

1.0000

0.9079

899.0235

343.8000

84.90

1.00

1.00

0.9079

899.0235

376.0000

92.85

1.00

1.00

13

TRG

DUP 08 DIS

07/19/13 00:00

1.0000

'

I
-1 I
I

I
!

I
I

~it'll

,.,.J
t:~~

Eberline Services
Oak Ridge Laboratory

LCS & Ma~rix $1Jil<:e'S:


Isotope

Sol#

Ra-228

Ra-11

Page 1of1
Printed: 817/2013 10:34 AM

Spike and Tracer Worksheet

Activity
dpmlg

Solution
Date

Approx
Addition

Analysis Code

Date

Technician

Ra228

8/7/2013 10:33

JWOLFE

LCS

Ms

l,,CSD

MSD

Volume
Used(g)

Volume
Used(g)

Volume
Used(g)

Volume
Used(g)

Witness Initials

LCS
Known
pCi

MS.

Error
Estimate

Added
pCi

Error
Estimate

LCSO
I Error

Known
pCi

MSO
Added
pCi

Estimate

Error
Estimate

37.628

817/2013

0.5194

0.530

....

...

0.449

8.80

'

0.00

0.000

. :

.111!~cers
Activity
dpmlg

:
Solution
Date

fraction

Isotope

Sol#

01

Ba-133

Ba-6a

990.223

817/2013

02

Ba-133

Ba-6a

990.223

817/2013

03

Ba-133

Ba-6a

990.223

04

Ba-133

Ba-6a

05

Ba-133

06

Volume
Used(g)

0.9259

1.0200

0.9151

1.0200

817/2013

0.9164

1.0200

990.223

817/2013

0.9147

1.0200

Ba-6a

990.223

817/20131

0.9134

1.0200

Ba-133

Ba-6a

990.223

817/2013

0.91'22

1.0200

07

Ba-133

Ba-6a

990.223

817/2013

0.9120

1.0200

08

Ba-133

Ba-6a

990.223

817/2013

o.9118
.

1.0200

09

Ba-133

Ba-6a

990.223

817/2013

0.9102

1.0200

10

Ba-133

Ba-6a

990.223

817/2013

0.9126

1.0200

11

Ba-133

Ba-6a

990.223

817/2013

0.9091

1.0200

12

Ba-133

Ba6a

990.223

817/2013'

0.9079

1.0200

13

Ba-133

Ba-6a

990.223

817/2013

0.9079 .

1.0200

'

..

. .

m
t....:11
&:lo.
~-JI~

Version 2.0 08/99

__

0.00

.
Tracer

0000

II

Approx
Addition

0.000

000

:.
..

:.

..

Baliince Printer Tapes

::

LCS

Matrix Spike

Eberline Analytical
Oak Ridge Laboratory

Printed: 817/2013 10:34 AM


Page 1 of 1

Aliquot Worksheet

Analysis Code

Lab Deadline

Technician

8/13/2013

JWOLFE

Rpt Units

1--~~~~~~--<~~~

Ra228
Engineering Management Support, Inc.

Lab
Fraction
01
02
03
04
05
06
07
08
09
10
11
12
13

Sample

Client ID
LCS
BLANK
PZ-107-SS TOT
PZ-200-SS TOT
PZ-200-SS DIS
PZ-102-SS TOT
PZ-102-SS DIS
PZ-107-SS TOT
PZ-107-SS DIS
PZ-106-KS TOT
PZ-106-KS DIS
DUP 08 TOT
DUP 08 DIS

~-

liters

Muffle Data

Dilution Data

Ratio
PostfPre

Type
LCS
MBL
DUP
TRG
TRG
TRG
TRG
DO
TRG
TRG
TRG
TRG
TRG

~F11ctor.

No.of Dils

... .:;.=:..
:

..

:..
:

.
..

..

":

:.:.

=:

:. ..

..

1.

I:

,;
-

f------~- ~-

..

t;"OQp{)E,:iiEJo
'1.QQOQEiOO

1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO

1.Gqpolt-'1;00
. 1.,~J;::iifJo
1.~0QQEE+oo
1.(i()Q!)e+oe

1.oOQoE+oo
1.0!)00~~0Q

1,,000QE'i:.OO
:.

;:;

::=

Com~nts

t!!!ll

.r.i..
~-~

Technician:

-:

..

::

HJ Dist
Aliq

. f:-O~~oe+o=o

..

:.

Net Equiv

1.~+00

...

Aliquot

H-3 Solids Only


Water Added
(ml)

f.~oooi:+oo
1.00Q~OQ

1.0000E+OO
1.0000E+OO

1.0000E+OO
1.0000E+OO

:.

NetE
. .....<I~
..

1.0000E+OO
1.0000E+OO

1.0000E+OO
1.0000E+OO

..

::

1.0000E+OO

:..

=,.
..

Aliquot

Ratio

MS Aliquot Data

....

r----

Aliquot Data

..

.,

..
:

: ...

~\~

Date

~-.+-,Q

Eberline Services - Oak Ridge


Version 1.0 9/1999

Work Order

Analysis

Code

Gravimetric

Carrier

Carrier Cone
(mg/ml)

Technician

Ra228

Yttirum

34.0000

TSMITH

TRetec Engineering Management Support, Inc. Sample

Carrier Data

Fraction

Client ID

Type

Carrier Added
(ml)

01
02
03
04
05
06
07
08
09
10
11
12
13

LCS
BLANK
DUP
PZ-200-SS TOT
PZ-200-SS DIS
PZ-102-SS TOT
PZ-102-SS DIS
PZ-107-SS TOT
PZ-107-SS DIS
PZ-106-KS TOT
PZ-106-KS DIS
DUP 08 TOT
DUP 08 DIS

LCS
MBL
DUP
TRG
TRG
TRG
TRG
DO
TRG
TRG
TRG
TRG
TRG

--

Printed: 8/15/2013 7:19 AM


Page 1 of 1

Gravimetric Worksheet

2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000

Filter Data

Gravimetric

Filter Final
(g)

Filter Tare
(g)

0.0920
0.0917
0.0916
0.0925
0.0926
0.0922
0.0922
0.0924
0.0919
0.0920
0.0924
0.0918
0.0920

0.1459
0.1494
0.1476
0.1481
0.1489
0.1493
0.1480
0.1495
0.1475
0.1474
0.1472
0.1475
0.1473

Filt"rNet

. mr .
0.0539

. d;o5-tt
.

0~0557

0~0553

..

Cif~I

t..Ji
~

t "11

Technician:

~~

~~~~~~~~~~~~~~~~-

Date:

~ l~ ,Jl._

. ~:0571
. ~~0558
. 0.05-71
0;0556
O;U554
.
0.0548

..

..

---

0.0560
IUJ556
0.0563

....

..

.....

%
Recovery

79.26
84.85
82.35
81.76
82.79
83.97
82.06
83.97
81.76
81.47
80.59
81.91
81.32

C-

Sheet1

f11rt-1

C!J

Detector ID Sample ID Alpha Beta Count Time Voltage


TOD
D2
1307154-01
8
184
30
1400 8/15/13 8:22

!l;lt~I

$:~

g:i,,,

Page 1

C-
Sheet1

fJfl(lt)

Detector ID Sample ID Alpha


Beta Count Time
Voltage
C1
1307154-10 15
169
120

1400
1307154-11
C2
38
333
120

1400
C3
1307154-12 17
356
120

1400
C4
1307154-13 16
296
120

1400
A1
1307154-02 17
143
120

1400
A2
1307154-03 11
249
120

1400
A3
1307154-04 16
207
120

1400
A4
1307154-05
5
224
120

1400
81
1307154-06
8
238
120

1400
82
1307154-07 21
258
120

1400
83
1307154-08 13
267
120

1400
84
1307154-09 15
276
120

1400

tit~
~~
~~.

U11

Page 1

TOD
8/15/13 9:50
8/15/13 9:50
8/15/13 9:50
8/15/13 9:50
8/15/13 9:50
8/15/13 9:50
8/15/13 9:50
8/15/13 9:50
8/15/13 9:51
8/15/13 9:51
8/15/13 9:51
8/15/13 9:51

Eberline Analytical
Oak Ridge Laboratory

Detector

Alpha/Beta

Calibration Date

Count Date

Bkg CPM

PFW

LB4110A - Al

Alpha

11/18/2007

8/15/2013

6.67E-02

~n

UCL

-2.13E+Ol

2.82E-Ol

2.19E+Ol

-1.81E+Ol

2.53E-01

1.86E+Ol

Alpha

11/18/2007

8/15/2013

1.67E-02

LB4110A - A3

'Alpha

11/18/2007

8/15/2013

5.00E-02

-1.76E+Ol

2.16E-01

l .80E+Ol

LB4110A - A4

Alpha

11/18/2007

8/15/2013

3.33E-02

-1.87E+Ol

2.36E-01

1.92E+Ol

LB4110A - Bl

Alpha

8/15/2013

O.OOE+OO

-9.69E-02

7.51E-02

2.47E-01
2.22E-01

11/18/2007

LB4110A - B2

Alpha

11/18/2007

8/15/2013

8.33E-02

-7.81E-02

7.22E-02

LB4110A - B3

Alpha

11/18/2007

8/15/2013

1.00E-01

-6.29E-02

5.35E-02

1.70E-01

LB4110A - B4

Alpha

11/18/2007

8/15/2013

5.00E-02

-1.40E-01

7.87E-02

2.98E-01

LB4110A - Cl

Alpha

11/18/2007

8/15/2013

6.67E-02

-1.49E-01

8.86E-02

3.26E-01

LB4110A - C2

Alpha

11/18/2007

8/15/2013

3.33E-02

-1.77E-01

8.66E-02

3.50E-01

LB4110A - C3

Alpha

11/18/2007

8/15/2013

8.33E-02

-1. 72E-Ol

1.00E-01

3.72E-Ol

1.67E-02

-6.27E-02

6.83E-02

1.99E-01

Alpha

11/18/2007

8/15/2013

LB4110A - Dl

Alpha

11/18/2007

8/15/2013

5.00E-02

-5.36E-02

8.32E-02

2.20E-01

LB4110A - D2

Alpha

11/18/2007

8/15/2013

1.67E-02

-6.99E-02

6.06E-02

1.91E-01

LB4110A - D3

Alpha

11/18/2007

8/15/2013

1.67E-02

-4.85E-02

7.06E-02

l.90E-01

LB4110A - D4

Alpha

11/18/2007

8/15/2013

1.67E-02

-5.72E-02

7.03E-02

1.98E-01

LB4110R - Al

Alpha

11/24/2006

8/15/2013

8.33E-02

-9.81E-02

1.0lE-01

3.00E-01

LB4110R - A2

Alpha

11/24/2006

8/15/2013

6.67E-02

-8.91E-02

7.63E-02

2.42E-01

1.33E-Ol

-7.31E-02

7.73E-02

2.28E-01

Alpha

11/24/2006

8/15/2013

LB4110R - A4

Alpha

11/24/2006

8/15/2013

1.00E-01

-5.26E-02

7.09E-02

1.94E-01

LB4110R - Bl

Alpha

11/24/2006

8/15/2013

O.OOE+OO

-9.42E-02

6.16E-02

2.17E-01

3.33E-02

-6.94E-02

6.33E-02

1.96E-01

LB4110R - B2

,i::eo,

Mean

LB4110A - A2

LB4110R - A3

illl!~

LCL

LB4110A - C4

tN.

Printed: 8/15/2013 6:46 AM

Page 1 of 1

GPC Detector Report


(ALL Backgrounds)

Alpha

11/24/2006

8/15/2013

LB4110R - B3

Alpha

11/24/2006

8/15/2013

6.67E-02

-6.48E-02

6.99E-02

2.05E-01

LB4110R - B4

Alpha

11/24/2006

8/15/2013

5.00E-02

-6.38E-02

7.02E-02

2.04E-01

LB4110R - Cl

Alpha

8/15/2013

6.67E-02

-7.67E-02

7.36E-02

2.24E-01

11/24/2006

LB4110R - C2

Alpha

11/24/2006

8/15/2013

1.67E-02

-7.55E-02

7.09E-02

2.17E-01

LB4110R - C3

Alpha

11/24/2006

8/15/2013

8.33E-02

-8. 78E-02

8.43E-02

2.56E-01

LB4110R - C4

Alpha

11/24/2006

8/15/2013

3.33E-02

-6.18E-02

8.12E-02

2.24E-01

LB4110R - Dl

Alpha

11/24/2006

8/15/2013

O.OOE+OO

-1.03E-01

7.0lE-02

2.43E-01

LB4110R - D2

'Alpha

11/24/2006

8/15/2013

0.00E+OO

-7.80E-02

6.95E-02

2.17E-Ol

LB4110R - D3

Alpha

11/24/2006

8/15/2013

O.OOE+OO

-8.30E-02

6.93E-02

2.22E-Ol

-7.54E-02

7.40E-02

2.23E-01

-1.56E-02

9.58E-02

2.07E-01

LB4110R - 04

Alpha

11/24/2006

8/15/2013

O.OOE+OO

LB5100 - 1

Alpha

7/10/2006

10/26/2007

5.00E-02

C-

fJ1111t7

Eberline Analytical
Oak Ridge Laboratory

GPC Detector Report


(ALL Backgrounds)

Detector

Alpha/Beta

Calibration Date

Count Date

Bkg CPM

PFW

LCL

Mean

UCL

LB4110A - Al

Beta

11/18/2007

8/15/2013

7.57E+OO

-2.89E+02

7.63E+OO

3.04E+02

3.50E+OO

-3.03E+Ol

2.59E+OO

3.55E+Ol

LB4110A - A2

Beta

LB4110A - A3
LB4110A - A4
LB4110A - Bl

ta

it,.,~

tr...
~~kl!~

Printed: 8/15/2013 6:46 AM

Page 1 of 1

11/18/2007

8/15/2013

.Beta

11/18/2007

8/15/2013

l.85E+OO

-5.0lE+Ol

2.63E+OO

5.54E+Ol

Beta

11/18/2007

8/15/2013

7.47E+OO

-3.24E+Ol

3.22E+OO

3.88E+Ol

8/15/2013

1.45E+OO

-1.04E+Ol

3.23E+OO

1.68E+Ol

Beta

11/18/2007

LB4110A - B2

Beta

11/18/2007

8/15/2013

1.27E+OO

-7.62E+OO

1.99E+OO

1.16E+Ol

LB4110A - B3

Beta

11/18/2007

8/15/2013

1.18E+OO

1.16E-01

1.36E+OO

2.60E+OO

LB4110A - B4

Beta

11/18/2007

8/15/2013

1.12E+OO

-7.61E+OO

1.97E+OO

1.16E+Ol
9.61E+OO

LB4110A - Cl

Beta

11/18/2007

8/15/2013

l.40E+OO

-5.38E+OO

2.12E+OO

LB4110A - C2

Beta

11/18/2007

8/15/2013

1.00E+OO

3.81E-01

1.27E+OO

2.15E+OO

LB4110A - C3

Beta

11/18/2007

8/15/2013

1.22E+OO

4.72E-01

1.46E+OO

2.45E+OO

LB4110A - C4

Beta

11/18/2007

8/15/2013

1.02E+OO

-1.75E+OO

2.lOE+OO

5.95E+OO

LB4110A - Dl

Beta

11/18/2007

8/15/2013

1.90E+OO

-2.31E+OO

2.56E+OO

7.43E+OO

LB4110A - D2

Beta

11/18/2007

8/15/2013

l.45E+OO

-6.39E-Ol

1.56E+OO

3.76E+OO

LB4110A - 03

Beta

11/18/2007

8/15/2013

3.97E+OO

1.29E+OO

4.47E+OO

7.66E+OO
3.16E+OO

LB4110A - 04

Beta

11/18/2007

8/15/2013

1.22E+OO

-4.23E-01

1.37E+OO

LB4110R - Al

Beta

11/24/2006

8/15/2013

8.83E-01

-6.08E+Ol

3.66E+OO

6.81E+Ol

LB4110R - A2

Beta

11/24/2006

8/15/2013

l.08E+OO.

-4.83E+Ol

2.0lE+OO

5.23E+Ol

LB4110R - A3

Beta

11/24/2006

8/15/2013

9.33E-01 .

-4.47E+Ol

2.73E+OO

5.0lE+Ol

LB4110R - A4

Beta

11/24/2006

8/15/2013

9.83E-01

-4.46E+Ol

1.99E+OO

4.85E+Ol

LB4110R - Bl

Beta

11/24/2006

8/15/2013

1.08E+OO

-4.69E+Ol

2.02E+OO

5.09E+Ol
5.lOE+Ol

LB4110R - B2

Beta

11/24/2006

8/15/2013

1.18E+OO

-4.69E+Ol

2.04E+OO

LB4110R - B3

Beta

11/24/2006

8/15/2013

1.05E+OO

-4.67E+Ol

2.65E+OO

5.20E+Ol

LB4110R - B4

Beta

11/24/2006

8/15/2013

1.07E+OO

-4.70E+Ol

1.92E+OO

5.08E+Ol

LB4110R - Cl

Beta

11/24/2006

8/15/2013

1.30E+OO ,

-4.68E+Ol

2.96E+OO

5.27E+Ol
5.22E+Ol

LB4110R - C2

Beta

11/24/2006

8/15/2013

1.37E+OO

-4.68E+Ol

2.71E+OO

LB4110R - C3

Beta

11/24/2006

8/15/2013

1.33E+OO'

-4.72E+Ol

2.51E+OO

5.23E+Ol

LB4110R - C4

Beta

11/24/2006

8/15/2013

1.20E+OG

-5.33E+Ol

2.95E+OO

5.92E+Ol

LB4110R - Dl

Beta

11/24/2006

8/15/2013

O.OOE+OO

-4.44E+Ol

5.55E+OO

5.55E+Ol

LB4110R - 02

Beta

11/24/2006

8/15/2013

O.OOE+OO

-4.77E+Ol

1.87E+OO

5.15E+Ol

LB4110R - D3

Beta

11/24/2006

8/15/2013

O.OOE+OO

-5.llE+Ol

5.52E+OO

6.21E+Ol

-4.74E+Ol

2.23E+OO

5.19E+Ol

-3.19E-01

1.58E+OO

3.48E+OO

LB4110R - 04

Beta

11/24/2006

8/15/2013

O.OOE+OO

LB5100 - 1

Beta

7/10/2006

10/26/2007

4.52E+00

c.-

er1r1(">

Eberline Analytical
Oak Ridge Laboratory
Detector

Count Date

Eff

PFW

LCL

Mean

UCL

-0.0127

0.2159

0.4446

Alpha

11/18/2007

8/15/2013

0.2503

LB4110A - A2

Alpha

11/18/2007

8/15/2013

0.2107

-0.0502

0.1742

0.3986

LB4110A - A3

Alpha

11/18/2007

8/15/2013

0.2046

-0.0735

0.1634

0.4003

0.2184

-0.0520

0.1821

0.4162

0.1943

0.2243

0.2543

LB4110A - A4

Alpha

LB4110A - Bl

Alpha

11/18/2007

8/15/2013

0.2045

LB4110A - B2

Alpha

11/18/2007

8/15/2013

0.2161

0.1924

0.2213

0.2502

0.2237

0.1279

0.2323

0.3366

0.2088

0.2364

0.2639

Alpha

11/18/2007

11/18/2007

8/15/2013

8/15/2013

LB4110A - B4

Alpha

11/18/2007

8/15/2013

0.2259

LB4110A - Cl

Alpha

11/18/2007

8/15/2013

0.2175

0.1976

0.2207

0.2438

0.2284

0.1971

0.2252

0.2532

Alpha

11/18/2007

8/15/2013

LB4110A - C3

Alpha

11/18/2007

8/15/2013

0.2575

0.2234

0.2494

0.2755

LB4110A - C4

Alpha

11/18/2007

8/15/2013

0.2236

0.1969

0.2256

0.2543

0.2173

0.2028

0.2328

0.2628

LB4110A - 01

Alpha

11/18/2007

8/15/2013

LB4110A - 02

Alpha

11/18/2007

8/15/2013

0.2485

0.2276

0.2580

0.2884

LB4110A - D3

Alpha

11/18/2007

8/15/2013

0.2535

0.2309

0.2634

0.2958

0.1880

0.1642

0.1992

0.2342

LB4110A - 04

i:i~

Calibration Date

LB4110A - Al

LB4110A - C2

Clil

Alpha/Beta

LB4110A - B3

tl!fJI
t...ii

Printed: 8/15/2013 6:47 AM

Page 1 of 1

GPC Detector Report


(ALL Efficiencies)

Alpha

11/18/2007

8/15/2013

LB4110R - Al

Alpha

11/24/2006

8/15/2013

0.2269

0.1983

0.2385

0.2786

LB4110R - A2

Alpha

11/24/2006

8/15/2013

0.2058

0.1851

0.2201

0.2551

LB4110R - A3

Alpha

11/24/2006

8/15/2013

0.2158

0.1924

0.2243

0.2563

LB4110R - A4

Alpha

11/24/2006

8/15/2013

0.2442

0.2118

0.2453

0.2789

LB4110R - Bl

Alpha

11/24/2006

8/15/2013

0.2197

0.1832

0.2257

0.2681

LB4110R - B2

Alpha

11/24/2006

8/15/2013

0.2072

0.1754

0.2169

0.2585

LB4110R - B3

Alpha

11/24/2006

8/15/2013

0.2481

0.2016

0.2438

0.2861

LB4110R - B4

Alpha

11/24/2006

8/15/2013

0.2171

0.1882

0.2312

0.2742

LB4110R - Cl

Alpha

8/15/2013
8/15/2013

0.2136

0.1833
0.1932

0.2150
0.2245

0.2466
0.2558

LB4110R - C2

Alpha

11/24/2006
11/24/2006

0.2152

LB4110R - C3

Alpha

11/24/2006

8/15/2013

0.2329

0.2034

0.2394

0.2754

LB4110R - C4

Alpha

11/24/2006

8/15/2013

0.2062

0.1826

0.2222

0.2618

LB4110R - Dl

Alpha

11/24/2006

8/15/2013

0.0000

0.0031

0.1991

0.3951

LB4110R - D2

Alpha

11/24/2006

8/15/2013

0.0000

0.0042

0.2264

0.4486

LB4110R - D3

Alpha

11/24/2006

8/15/2013

0.0000

0.0041

0.2224

0.4407

LB4110R - D4

Alpha

11/24/2006

8/15/2013

0.0000

0.0019

0.1792

0.3566

LB5100 - 1

Alpha

7/10/2006

10/26/2007

0.3368

F
p

0.3332

0.3455

0.3578

c..

~trrt)

Eberline Analytical
Oak Ridge Laboratory
Detector

Alpha/Beta

Calibration Date

LB4110A - Al

Beta

11/18/2007

LB4110A - A2

Beta

11/18/2007

~~

r.:,,,

U)

Eff

PFW

LCL

Mean

UCL

8/15/2013

0.5664

0.2113

0.5625

0.9137

8/15/2013

0.4909

0.1622

0.4649

0.7675

0.0902

0.4572

0.8242

Count Date

LB4110A - A3

Beta

11/18/2007

8/15/2013

0.4732

LB4110A - A4

Beta

11/18/2007

8/15/2013

0.5253

0.1430

0.4892

0.8355

LB4110A - Bl

Beta

11/18/2007

8/15/2013

0.4878

0.4633

0.5297

0.5961

LB4110A - B2

Beta

11/18/2007

8/15/2013

0.5066

0.4632

0.5268

0.5904

LB4110A - B3

Beta

11/18/2007

8/15/2013

0.5143

0.3169

0.5314

0.7458

LB4110A - B4

Beta

11/18/2007

8/15/2013

0.5187

0.4918

0.5538

0.6158

LB4110A - Cl

Beta

11/18/2007

8/15/2013

0.5027

0.4511

0.5026

0.5541

LB4110A - C2

Beta

11/18/2007

8/15/2013

0.4959

0.4293

0.5010

0.5727

LB4110A - C3

Beta

11/18/2007

8/15/2013

0.6057

0.5291

0.5907

0.6523

LB4110A - C4

Beta

11/18/2007

8/15/2013

0.5217

0.4578

0.5248

0.5918

0.5241

0.4784

0.5529

0.6275

LB4110A - Dl

Beta

LB4110A - D2

Beta

11/18/2007

8/15/2013

0.5458

0.4887

0.5871

0.6855

LB4110A - D3

Beta

11/18/2007

8/15/2013

0.5996

0.5374

0.6149

0.6924

11/18/2007

8/15/2013

LB4110A - 04

Beta

11/18/2007

8/15/2013

0.4392

0.3845

0.4718

0.5592

LB4110R - Al

Beta

11/24/2006

8/15/2013

0.5525

0.4744

0.5672

0.6601

LB4110R - A2

Beta

11/24/2006

8/15/2013

0.4942

0.4158

0.5085

0.6013

0.5065

0.4503

0.5384

0.6264

LB4110R - A3

t;JJ

Printed: 8/15/2013 6:47 AM

Page 1 of 1

GPC Detector Report


(ALL Efficiencies)

Beta

11/24/2006

8/15/2013

LB4110R - A4

Beta

11/24/2006

8/15/2013

0.5924

0.5032

0.5914

0.6796

LB4110R - Bl

Beta

11/24/2006

8/15/2013

0.5274

0.4463

0.5421

0.6380

LB4110R - B2

Beta

11/24/2006

8/15/2013

0.5029

0.4247

0.5195

0.6144

LB4110R - B3

Beta

11/24/2006

8/15/2013

0.6058

0.4939

0.5917

0.6895

LB4110R - B4

Beta

11/24/2006

8/15/2013

0.5251

0.4540

0.5489

0.6437

LB4110R - Cl

Beta

11/24/2006

8/15/2013

0.4689

0.4159

0.5015

0.5871

LB4110R - C2

Beta

11/24/2006

8/15/2013

0.5136

0.4440

0.5283

0.6126

LB4110R - C3

Beta

11/24/2006

8/15/2013

0.5626

0.4755

0.5705

0.6656

LB4110R - C4

Beta

11/24/2006

8/15/2013

0.5001

0.4258

0.5249

0.6240

LB4110R - Dl

Beta

11/24/2006

8/15/2013

0.0000

0.0066

0.4761

0.9455

LB4110R - 02

Beta

11/24/2006

8/15/2013

0.0000

0.0081

0.5349

1.0618

LB4110R - 03

Beta

11/24/2006

8/15/2013

0.0000

0.0077

0.5195

1.0314

LB4110R - D4

Beta

11/24/2006

8/15/2013

0.0000

0.0035

0.4277

0.8518

LB5100 - 1

Beta

7/10/2006

10/26/2007

0.4428

0.4555

0.4731

0.4906

c.,....

01 (flt;>

SECTION XII

BARIUM-133 ANALYTICAL TRACER DATA

VAX/VMS Peak Search Report Generated


Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level

8-AUG-2013 17:19:55.52

DKAlOO: [GAMMA.SCUSR.ARCHIVE]SMP_130715401 GE5 BAFIL 194500.CN


PEAK V16.9 PEAKEFF V2.2
SPIKE
8-AUG-2013 00:00:00.
1307154-01
FILTER
GE5
0 00:15:00.00
25
3.00000
No

Pk It

Energy

Area

Bkgnd

1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27

19.93
21.05
28.27
30.97
35.08
35.90
61.69
65.80
79.41
80.96
84.26
111.82
116.10
160.35
275.19
275.85
301.66
302.49
306.60
331.98
332.61
355.11
382.89
385.13
385.81
386.59
390.09

24
91
46
2066
322
59
256
108
34
868
14
156
50
21
18
38
91
91
28
11
73
431
57
40
64
27
28

13
36
9
38
84
64
22
37
11
10
16
71
25
17
2
2
0
0
6
6
13
3
29
19
16
7
12

3
3
3
3
2
2
0
0
2
2
0
0
0
0
4
4
1
1
0
1
1
0
0
7
7
7
0

W''?

Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian

FWHM Channel

Left

Pw

196.59
207.38
276.63
302.52
341.96
349.86
597.32
636.79
767.40
782.29
813.91
1078.38
1119.42
1544.08
2646.00
2652.34
2900.00
2908.00
2947.40
3191. 00
3197.00
3412.87
3679.49
3701.00
3707.47
3714.94
3748.56

191
191
268
268
332
332
586
627
759
759
804
1067
1106
1533
2636
2636
2888
2888
2935
3184
3184
3396
3663
3693
3693
3693
3732

27
27
52
52
24
24
22
22
34
34
14
23
21
19
24
24
28
28
22
26
26
31
25
27
27
27
26

0.66
0.67
0.71
0.73
0.62
0.62
0.86
0.73
0.84
0.69
0.58
0.72
0.35
0.48
1. 03
0.91
1. 06
1. 06
0.43
1.10
1.10
1. 04
1. 01
1.16
0.55
0.94
0.18

8-AUG-2013 17:04:36.
1.00000E+OO filter
0
BAFIL
0 00:15:01.22 0.1%
4096
10.00000
Cts/Sec %Err

2.72E-02
1.02E-01
5.08E-02
2.30E+OO
3.57E-01
6.55E-02
2.85E-01
1.19E-01
3.83E-02
9.65E-01
1. 60E-02
1.73E-01
5.57E-02
2.39E-02
2.00E-02
4.18E-02
1.0lE-01
1.02E-01
3.06E-02
1.24E-02
8.lOE-02
4.79E-01
6.38E-02
4.40E-02
7.09E-02
3.0lE-02
3.16E-02

40.1
19.3
31. 5
2.4
9.0
32.5
7.4
15.5
27.3
3.5
57.1
14.4
25.3
41. 0
41. 0
19.2
12.4
11. 2
25.3
59.3
13.6
4.9
19.8
27.1
20.5
30.7
30.2

Fit
1.27E+OO
2.18E+OO
2.30E+OO

9.52E-01

6.75E-01
4.78E+OO
3.21E+OO

2.15E+OO

fliJ51

Summary of Nuclide Activity


Sample ID : 1307154-01

Acquisition date

Total number of lines in spectrum


Number of unidentified lines
Number of lines tentatively identified by NID
Nuclide Type
Nuclide
BA-133

Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
4.383E+02

Total Activity
:

---------

4.383E+02

Grand Total Activity :

=
=

Wtd Mean
Decay Corr
pCi/filter
4.384E+02

2-Sigma
Decay Corr
2-Sigma Error %Error Flags
16.77
0.735E+02

---------

4.384E+02

NATURAL

Wtd Mean
Uncorrected
Nuclide
Hlif e
Decay pCi/filter
TH-234 4.47E+09Y
2.314E+02
1. 00
--------Total Activity
2.314E+02

Flags: "K"
"E"

18.52%

FISSION

Hlife
10.50Y

Nuclide Type

27
22
5

Page :
2
8-AUG-2013 17:04:36

6.697E+02

Keyline not found


Manually edited

Wtd Mean
Decay Corr
pCi/filter
2.314E+02

2-Sigma
Decay Corr
%Error Flags
Error
2-Sigma
15.37
0.356E+02

---------

2.314E+02
6.698E+02
"M"
"A"

Manually accepted
Nuclide specific abn. limit

Nuclide Line Activity Report


Sample ID : 1307154-01

Acquisition date

Page :
3
8-AUG-2013 17:04:36

Nuclide Type: FISSION


Nuclide
BA-133

Energy
81.00
302.84
356.01

%Abn
33.00*
17.80
60.00

Final Mean for

Uncorrected Decay Corr 2-Sigma


%Ef f
pCi/filter pCi/filter %Error
1.802E+Ol 4.383E+02
4.384E+02 16.77
2.575E+OO 5.990E+02
5.991E+02 34.56
4.312E+OO 5.005E+02
5.006E+02 17.45

3 Valid Peaks

Status
OK
OK
OK

4.384E+02+/ 7.353E+Ol ( 16.77%)

Nuclide Type: NATURAL


Nuclide
TH-234

Energy
63.29

%Abn
3.80*

Final Mean for


Flag:

11

* 11

Uncorrected Decay Corr 2-Sigma


%Eff
pCi/filter pCi/filter %Error
8.750E+Ol 2.314E+02
2.314E+02 15.37

1 Valid Peaks

Status
OK

2.314E+02+/ 3.556E+Ol ( 15.37%)

Keyline

:!1353

Combined Activity-MDA Report


Sample ID : 1307154-01

Acquisition date

Page :
4
8-AUG-2013 17:04:36

Identified Nuclides
Nuclide
BA-133
TH-234

Activity
(pCi/filter)

Act error

4.384E+02
2.314E+02

7.353E+Ol
3.556E+Ol

MDA
(p,Ci/filter)
1.235E+Ol
3.063E+Ol

MDA error

Act/MDA

1.818E+OO
3.940E-01

35.495
7.555

MDA error

Act/MDA

8.667E+OO
1.746E+Ol
1.732E-02
2.577E-02
3.752E+OO
2.734E-02

-0.142
0.246
-0.021
1. 847
-0.155
-0.231

Non-Identified Nuclides

Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241

Key-Line
Activity K.L.
(pCi/filter)Ided
-3.619E+OO
4.468E+Ol
-3.260E-02
4.228E+OO
-6.580E+OO
-5.619E-01

Act error
l.441E+Ol
9.296E+Ol
8.351E-01
1.644E+OO
2.512E+Ol
l.704E+OO

MDA
(pCi/filter)
2.557E+Ol
l.815E+02
1.539E+OO
2.289E+OO
4.253E+Ol
2.429E+OO

~j!\l?

VAX/VMS Peak Search Report Generated


Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level

DK,AlOO: [GAMMA.SCUSR.ARCHIVE]SMP_130715402 GE5 BAFIL 194504.CN


PEAK V16.9 PEAKEFF V2.2
BLANK
8-AUG-2013 00:00:00.
1307154-02
FILTER
GE5
0 00:15:00.00
25
3.00000
No

Pk It

Energy

Area

Bkgnd

1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31

5.41
10.56
21. 26
25.84
28.73
30.97
35.12
36.02
52.78
61.74
66.01
70.01
81.00
111.56
115.85
275.72
301.17
302.14
306.62
332.51
333.65
355.12
382.53
383.15
385.67
386.28
389.40
389.93
390.36
412.88
413.58

20
20
95
13
9
1919
446
99
86
245
109
19
780
230
56
31
21
100
22
77
10
401
59
14
86
132
12
44
14
19
25

13
9
15
14
54
143
26
11
14
46
41
11
58
18
29
11
3
7
5
5
1
19
13
10
12
8
0
0
0
6
12

0
0
0
0
0
0
2
2
0
0
0
0
0
0
0
0
3
3
0
6
6
0
1
1
6
6
5
5
5
1
1

8-AUG-2013 17:35:36.41

Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian

8-AUG-2013 17:20:19.
1.00000E+OO filter
0
BAFIL
0 00:15:01.17 0.1%
4096
10.00000

FWHM Channel

Left

Pw

Cts/Sec %Err

0.99
0.30
0.81
0.91
0.88
0.72
0.68
0.57
1. 60
1. 20
0.34
0.43
0.65
0.59
0.95
0.90
1.17
0.85
Q.53
1. 21
0.58
0.86
1.16
1.16
1.18
1.16
1.16
1.16
0.69
1. 31
1.19

49
102
203
247
268
291
330
330
496
583
627
668
772
1061
1101
2636
2889
2889
2931
3182
3182
3396
3662
3662
3694
3694
3733
3733
3733
3960
3960

14
11
15
13
17
23
30
30
27
27
27
13
20
25
29
21
26
26
25
28
28
31
29
29
26
26
27
27
27
20
20

2.17E-02 46.3
2.17E-02 36.5
1.06E-01 13.6
1.44E-02 73.1
1.02E-02187.3
2.13E+OO 2.8
4.95E-01 5.8
1.llE-01 20.0
9.50E-02 16.1
2.72E-01 9.1
1.21E-01 16.7
2.09E-02 38.8
8.67E-01 4.1
2.56E-01 7.7
6.22E-02 26.8
3.50E-02 27.8
2.35E-02 34.4
1.12E-01 12.0
2.44E-02 28.6
8.60E-02 12.0
l.17E-02 26.1
4.46E-01 5.4
6.52E-02 19.3
1.60E-02 71.4
9.60E-02 15.8
1.46E-01 9.4
1. 31E-02 43.1
4.91E-02 15.5
1.60E-02 46.2
2.15E-02 30.0
2.78E-02 24.1

57.31
106.70
209.38
253.31
281.06
302.57
342.36
351. 00
511.88
597.85
638.80
677.17
782.61
1075.86
1117.09
2651.15
2895.35
2904.62
2947.64
3196.05
3206.97
3413.04
3676.00
3682.00
3706.17
3712.00
3742.00
3747.00
3751.18
3967.28
3974.00

Fit

9.58E-01

1.12E+OO
1.43E+OO
9.56E-01
4.72E+OO
2.09E+OO
1. 02E+OO

Summary of Nuclide Activity


Sample ID : 1307154-02

Acquisition date

Total number of lines in spectrum


Number of unidentified lines
Number of lines tentatively identified by NID

31
24
7

Page :
2
8-AUG-2013 17:20:19

22.58%

Nuclide Type : FISSION


Nuclide
BA-133

Hlife
10.50Y

Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
3.939E+02

Total Activity

--------

Wtd Mean
Decay Corr
pCi/filter
3.939E+02

2-Sigma
Decay Corr
2-Sigma Error %Error Flags
17.33
0.683E+02

--------

3.939E+02

3.939E+02

Wtd Mean
Uncorrected
pCi/f ilter
l.394E+OO
4.396E+OO
2.214E+02

Wtd Mean
Decay Corr
pCi/filter
1.394E+OO
4.396E+OO
2.214E+02

Nuclide Type : NATURAL


Nuclide
Hlife
PA-231 3.28E+04Y
PA-234 4.47E+09Y
TH-234 4.47E+09Y

Decay
1. 00
1. 00
1. 00

Total Activity
Grand Total Activity :

--------

--------

2.272E+02

2.272E+02

6.211E+02

6.211E+02

Flags: "K" = Key line not found


"E" = Manually edited

2-Sigma
Decay Corr
2-Sigma Error %Error Flags
73.14
1.020E+OO
27.46
1.207E+OO
0.412E+02
18.60

"M" = Manually accepted


"A" = Nuclide specific abn. limit

Nuclide Line Activity Report


Sample ID : 1307154-02

Acquisition date

Page :
3
8-AUG-2013 17:20:19

Nuclide Type: FISSION


Nuclide
BA-133

Energy
81.00
302.84
356.01

%Abn
33.00*
17.80
60.00

Final Mean for

Uncorrected Decay Corr 2-Sigma


%Ef f
pCi/filter pCi/f ilter %Error
1.802E+Ol 3.939E+02
3.939E+02 17.33
2.575E+OO 6.582E+02
6.583E+02 35.69
4.312E+OO 4.659E+02
4.660E+02 18.10

3 Valid Peaks

Status
OK
OK
OK

3.939E+02+/- 6.826E+Ol ( 17.33%)

Nuclide Type: NATURAL


Nuclide
PA-231

Energy
9.28
10.11
283.67
302.67

%Abn
42.00*
20.20
1. 60
2.30

Final Mean for


PA-234

9.89
21.72
37.93
131.42

TH-234

63.29

"*"

1.000E+02
1.000E+02
1.000E+02
2.473E+OO

3 Valid Peaks

3.80*

Final Mean for


Flag:

3 Valid Peaks

89.00
64.90*
23.75
20.40

Final Mean for

Uncorrected Decay Corr 2-Sigma


%Ef f
pCi/f ilter pCi/filter %Error
1.000E+02 l.394E+OO
1.394E+OO 73.14
1.000E+02 2.899E+OO
2.899E+OO 73.14
2.191E+OO - - - - - Line Not Found - - - - 2.572E+OO 5.102E+03
5.102E+03 34.26

8.750E+Ol

1 Valid Peaks

1.394E+OO+/- 1.020E+OO ( 73 .14%)

6.580E-01
4.396E+OO
l.258E+Ol
- - - - - Line

6.580E-01
4.396E+OO
l.258E+Ol
Not Found

73.14
27.46
40.17

-----

OK

OK

OK

Absent

4.396E+OO+/- 1.207E+OO ( 27.46%)

2.214E+02

Status
OK
OK
Absent
OK

2.214E+02

18.60

OK

2.214E+02+/- 4.119E+Ol ( 18.60%)

Key line

f!J357

Combined Activity-MDA Report


Sample ID : 1307154-02

Acquisition date

4
Page :
8-AUG-2013 17:20:19

Identified Nuclides
Nuclide
BA-133
PA-231
PA-234
TH-234

Activity
(pCi/filter)
3.939E+02
l.394E+OO
4.396E+OO
2.214E+02

Act error
6.826E+Ol
l.020E+OO
1.207E+OO
4.119E+Ol

MDA
(pCi/filter)
1.280E+Ol
1.192E+OO
9.485E-01
2.545E+Ol

MDA error

Act/MDA

l.885E+OO
1.342E-02
1.068E-02
3.275E-01

30.775
1.170
4.634
8.700

MDA error

Act/MDA

9.625E+OO
1.676E+Ol
3.406E+OO
2.728E-02

0.063
0.499
-1.088
-0.301

Non-Identified Nuclides

Nuclide
C0-57
CD-109
NP-237
AM-241

Key-Line
Activity K.L.
(pCi/filter)Ided
l.777E+OO
8.695E+Ol
-4.200E+Ol
-7.289E-01

Act error
l.522E+Ol
8.132E+Ol
2.759E+Ol
1.730E+OO

MDA
(pCi/filter)
2.839E+Ol
1.741E+02
3.862E+Ol
2.423E+OO

5358

\c{(fJ.\r)

VAX/VMS Peak Search Report Generated


Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level

DKAlOO: [GAMMA.SCUSR.ARCHIVE]SMP_130715403 GE5 BAFIL 194505.CN


PEAK Vl6.9 PEAKEFF V2.2
PZ-107-SS TOT
8-AUG-2013 00:00:00.
1307154-03
FILTER
GE5
0 00:15:00.00
25
3.00000
No

Pk It

Energy

Area

Bkgnd

1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24

21.11
30.97
35.06
36.26
61. 72
62.38
66.15
79.37
79.79
80.98
111. 70
115.79
186.26
275.97
301. 87
302.60
332.82
354.38
355.19
382.06
382.84
383.45
385.55
386.33

70
1605
306
15
137
49
90
33
26
615
152
48
10
22
33
77
28
54
172
32
17
29
105
33

32
84
80
54
31
7
42
14
19
16
34
14
19
17
0
0
16
3
9
4
9
6
13
4

0
0
0
0
1
1
0
6
6
6
0
0
0
0
1
1
0
6
6
3
3
3
4
4

8-AUG-2013 17:51:21.26

Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian

8-AUG-2013 17:36:05.
l.OOOOOE+OO filter
0
BAFIL
0 00:15:01.10 0.1%
4096
10.00000

FWHM Channel

Left

Pw

Cts/Sec %Err

0.99
0.81
0.63
0.22
0.71
0.65
0.37
1.17
0.69
0.65
0.73
0.86
0.26
0.77
1. 06
1. 06
0.87
1.11
0.82
1. 04
1.16
0.84
1.16
0.76

195
290
328
348
583
583
629
760
760
760
1065
1104
1777
2639
2888
2888
3186
3396
3396
3664
3664
3664
3692
3692

20
28
21
10
25
25
22
39
39
39
23
20
19
22
27
27
21
28
28
26
26
26
26
26

7.78E-02 22.7
1.78E+OO 3.0
3.40E-01 9.8
1.64E-02105.8
1.53E-01 12.9
5.40E-02 16.1
1. OOE-01 19.0
3.69E-02 27.2
2.87E-02 64.2
6.83E-01 4.3
1. 69E-01 11. 7
5.29E-02 21. 7
1.lOE-02 87.1
2.48E-02 41. 2
3.67E-02 25.7
8.61E-02 7.9
3.12E-02 31.7
6.04E-02 29.0
l.91E-01 10.2
3.61E-02 22.3
1.89E-02 58.3
3.26E-02 21. 3
1.16E-01 12.1
3.71E-02 24.3

207.94
302.60
341. 82
353.35
597.64
604.00
640.12
767.00
771. 00
782.42
1077.18
1116.45
1792.65
2653.53
2902.00
2909.00
3199.08
3405.89
3413.72
3671.56
3679.00
3684.83
3705.00
3712.46

Fit

1.66E+OO
1.00E+OO

5.47E+OO
1.87E+OO
2.23E+OO
4.98E+OO

Summary of Nuclide Activity


Sample ID : 1307154-03

Acquisition date

Total number of lines in spectrum


Number of unidentified lines
Number of lines tentatively identified by NID

24
18
6

Page :
2
8-AUG-2013 17:36:05

25.00%

Nuclide Type : FISSION


Nuclide
BA-133

Hlife
10.50Y

Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
3.104E+02

Total Activity

--------

3.104E+02

Wtd Mean
Decay Corr
pCi/filter
3.104E+02

Decay Corr
2-Sigma
2-Sigma Error %Error Flags
17.51
0.544E+02

--------

3.104E+02

Nuclide Type : NATURAL


Nuclide
Hlif e
TH-234 4.47E+09Y

Wtd Mean
Uncorrected
Decay pCi/f ilter
1. 00
4.386E+Ol

Total Activity
Grand Total Activity :
Flags: "K"
"E"

--------

Wtd Mean
Decay Corr
pCi/filter
4.386E+Ol

--------

4.386E+Ol

4.386E+Ol

3.542E+02

3.543E+02

= Keyline not found


= Manually edited

2-Sigma
Decay Corr
2-Sigma Error %Error Flags
32.51
1.426E+Ol

"M"
"A"

= Manually accepted
= Nuclide specific abn. limit

Nuclide Line Activity Report


Sample ID : 1307154-03

Acquisition date

Page :
3
8-AUG-2013 17:36:05

Nuclide Type: FISSION


Nuclide
BA-133

Energy
81.00
302.84
356.01

%Abn
33.00*
17.80
60.00

Final Mean for

Uncorrected Decay Corr 2-Sigma


%Ef f
pCi/f ilter pCi/filter %Error
l.802E+Ol 3.104E+02
3.104E+02 17.51
2.575E+OO 5.074E+02
5.075E+02 30.72
4.312E+OO 1.994E+02
1.995E+02 25.09

3 Valid Peaks =

Status
OK
OK
OK

3.104E+02+/- 5.437E+Ol ( 17.51%)

Nuclide Type: NATURAL


Nuclide
TH-234

Energy
63.29

%Abn
3.80*

Final Mean for


Flag:

11

* 11 = Keyline

Uncorrected Decay Corr 2-Sigma


%Ef f
pCi/filter pCi/f ilter %Error
8.750E+Ol 4.386E+Ol
4.386E+Ol 32.51

1 Valid Peaks

Statl,lS
OK

4.386E+Ol+/- 1.426E+Ol ( 32.51%)

Combined Activity-MDA Report


Sample ID : 1307154-03

Acquisition date

4
Page :
8-AUG-2013 17:36:05

Identified Nuclides
Nuclide
BA-133
TH-234

Activity
(pCi/filter)

Act error

3.104E+02
4.386E+Ol

5.437E+Ol
1.426E+Ol

MDA
(pCi/filter)
1.134E+Ol
2.817E+Ol

MDA error

Act/MDA

1.670E+OO
3.624E-01

27.366
1. 557

Non-Identified Nuclides

Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241

Key-Line
Activity K.L.
(pCi/filter)Ided
-8.348E+OO
6.846E+Ol
l.180E-01
3.241E+OO
4.610E+OO
7.681E-01

Act error

MDA
(pCi/filter)

MDA error

Act/MDA

l.070E+Ol
8.296E+Ol
6.567E-01
1.475E+OO
2.185E+Ol
1.258E+OO

1.645E+Ol
1.721E+02
l.302E+OO
l.827E+OO
4.213E+Ol
2.202E+OO

5.577E+OO
1.657E+Ol
l.466E-02
2.057E-02
3.716E+OO
2.479E-02

-0.507
0.398
0.091
1.774
0.109
0.349

8362

fl~L~

VAX/VMS Peak Search Report Generated


Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level

DKAlOO: [GAMMA.SCUSR.ARCHIVE]SMP_130715404 GE5 BAFIL 194506.CN


PEAK V16.9 PEAKEFF V2.2
PZ-200-SS TOT
8-AUG-2013 00:00:00.
1307154-04
FILTER
GE5
0 00:15:00.00
25
3.00000
No

Pk It

Energy

Area

Bkgnd

1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25

10.09
21.07
25.49
30.97
35.24
39.34
53.55
61.74
65.58

66.45
67.11
79.40
80.96
111.65

112.20
275.30
275.83
301.87
302.49
332.85
355.08
382.75
383.26
385.85
386.28

16
69
12
1499
385
9
20
206
70
31
32
26
627
97
46
23
35
86
52
39
301
77
32
109
12

8
32
16
80
55
5
27
13
9
4
0
0
0
29
5
0
0
0
0
3
8
5
5
13
9

0
0
0
0
0
0
0
0
1
1
1
2
2
1
1
5
5
1
1
0
0
1
1
5
5

8-AUG-2013 18:06:54.42

Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian

FWHM Channel

Left

Pw

0.90
0.17
0.23
0.78
0.64
0.39
0.18
0.90
0.72
0.66
0.73
0.71
0.72
0.84
0.77
1.49
1. 01
1. 06
0.96
0.81
1. 05
1. 27
1.16
1. 26
1.16

94
195
239
291
333
377
506
585
619
619
619
764
764
1065
1065
2638
2638
2887
2887
3184
3396
3663
3663
3693
3693

15
21
16
23
26
10
18
27
35
35
35
29
29
21
21
24
24
27
27
25
28
29
29
26
26

102.19
207.52
250.00
302.52
343.55
382.83
519.19
597.84
634.63
643.00
649.36
767.31
782.25
1076.73
1082.00
2647.08
2652.20
2902.00
2908.02
3199.30
3412.59
3678.11
3683.00
3707.87
3712.00

8-AUG-2013 17:51:33.
l.OOOOOE+OO filter
0
BAFIL
0 00:15:01.13 0.1%
4096
10.00000
Cts/Sec %Err

1.72E-02
7.68E-02
1. 33E-02
1.67E+OO
4.28E-01
1.00E-02
2.26E-02
2.29E-01
7.74E-02
3.47E-02
3.58E-02
2.92E-02
6.97E-01
1.07E-01
5.13E-02
2.51E-02
3.88E-02
9.55E-02
5.75E-02
4.34E-02
3.35E-01
8.57E-02
3.55E-02
1.21E-01
1. 31E-02

46.1
23.6
79.9
3.0
7.4
57.2
63.7
8.1
16.4
36.5
16.0
18.7
4.0
16.4
20.7
26.2
16.9
11. 2
16.9
17.8
6.1
12.1
27.2
11. 3
88.3

Fit

3.00E+OO
1.63E+OO

1.66E+OO
9.66E-01
2.49E+OO

4.26E+OO
1.90E+OO

!363

Summary of Nuclide Activity


Sample ID : 1307154-04

Acquisition date

Total number of lines in spectrum


Number of unidentified lines
Number of lines tentatively identified by NID

25
18
7

Page :
2
8-AUG-2013 17:51:33

28.00%

Nuclide Type : FISSION


Nuclide
BA-133

Hlife
10.50Y

Wtd Mean
Uncorrected
Decay pCi/filter
1.00 3.167E+02

Total Activity

Wtd Mean
Decay Corr
pCi/filter
3.168E+02

3.167E+02

3.168E+02

Wtd Mean
Uncorrected
pCi/filter
1.108E+OO
3.198E+OO
l.858E+02

Wtd Mean
Decay Corr
pCi/filter
1.108E+OO
3.198E+OO
1.858E+02

l.902E+02

1.902E+02

5.069E+02

5.069E+02

2-Sigma
Decay Corr
2-Sigma Error %Error Flags
17.23
0.546E+02

Nuclide Type : NATURAL


Nuclide
Hlife
PA-231 3.28E+04Y
PA-234 4.47E+09Y
TH-234 4.47E+09Y

Decay
1. 00
1. 00
1. 00

Total Activity
Grand Total Activity :
Flags: "K"
"E"

=
=

Keyline not found


Manually edited

"M"
"A"

=
=

2-Sigma
Decay Corr
2-Sigma Error %Error Flags
92.35

1.024E+OO
1.516E+OO
47.41

16.79

0.312E+02

Manually accepted
Nuclide specific abn. limit

8364

Nuclide Line Activity Report


Sample ID : 1307154-04

Acquisition date

Page :
3
8-AUG-2013 17:51:33

Nuclide Type: FISSION


Nuclide
BA-133

Energy
81.00
302.84
356.01

%Abn
33.00*
17.80
60.00

Final Mean for

Uncorrected Decay Corr 2-Sigma


%Ef f
pCi/filter pCi/filter %Error
1.802E+Ol 3.167E+02
3.168E+02 17.23
3.389E+02 42.81
2.575E+OO 3.389E+02
4.312E+OO 3.495E+02
3.496E+02 18.86

3 Valid Peaks =

Status
OK
OK
OK

3.168E+02+/- 5.459E+Ol ( 17.23%)

Nuclide Type: NATURAL


Nuclide
PA-231

Energy
9.28
10.11
283.67
302.67

%Abn
42.00*
20.20
1.60
2.30

Final Mean for


PA-234

9.89
21.72
37.93
131.42

TH-234

63.29

11

l.OOOE+02
1.000E+02
l.OOOE+02
2.473E+OO

8.750E+Ol

1 Valid Peaks

5.230E-01 92.35
3.198E+OO 47.41
1.138E+OO 114.47
Not Found - - - - -

OK

OK

OK

Absent

3.198E+OO+/- 1.516E+OO ( 47.41%)

1.858E+02

Status
OK
OK
Absent
OK

1.108E+OO+/- 1.024E+OO ( 92. 35%)

5.230E-01
3.198E+OO
l.138E+OO
- - - - - Line

3 Valid Peaks =

3.80*

Final Mean for


Flag:

3 Valid Peaks =

89.00
64.90*
23.75
20.40

Final Mean for

Uncorrected Decay Corr 2-Sigma


%Ef f
pCi/filter pCi/filter %Error
1.000E+02 1.108E+OO
1.108E+OO 92.35
1.000E+02 2.304E+OO
2.304E+OO 92.35
2.191E+OO - - - - - Line Not Found - - - - 2.572E+OO 2.627E+03
2.627E+03 41.63

1.858E+02

16.79

OK

1.858E+02+/- 3.121E+Ol ( 16.79%)

* 11 = Keyline

1!3S5

Combined Activity-MDA Report


Sample ID : 1307154-04
- - - -

Acquisition date

Page :
4
8-AUG-2013 17:51:33

Identified Nuclides

Nuclide
BA-133
PA-231
PA-234
TH-234

Activity
(pCi/filter)

Act error

MDA
(pCi/filter)

MDA error

Act/MDA

3.168E+02
1.108E+OO
3.198E+OO
1.858E+02

5.459E+Ol
1.024E+OO
1.516E+OO
3.121E+Ol

9.133E+OO
1.375E+OO
8.382E-01
1.531E+Ol

1.345E+OO
1.548E-02
9.435E-03
l.969E-01

34.683
0.806
3.815
12.143

Non-Identified Nuclides

Nuclide
C0-57
CD-109
NP-237
AM-241

Key-Line
Activity K.L.
(pCi/filter)Ided
4.539E+OO
-2.333E+Ol
-l.632E-02
4.199E-01

Act error

MDA
(pCi/filter)

MDA error

Act/MDA

l.297E+Ol
6.529E+Ol
l.958E+Ol
l.270E+OO

2.548E+Ol
1.167E+02
3.711E+Ol
2.lllE+OO

8.636E+OO
1.123E+Ol
3.273E+OO
2.376E-02

0.178
-0.200
0.000
0.199

6366

c.
VAX/VMS Peak Search Report Generated
Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level

DK.AlOO: [GAMMA.SCUSR.ARCHIVE]SMP_130715405 GE5 BAFIL 194509.CN


PEAK V16.9 PEAKEFF V2.2
PZ-200-SS DIS
9-AUG-2013 00:00:00.
1307154-05
FILTER
GE5
0 00:15:00.00
25
3.00000
No

Pk It

Energy

Area

Bkgnd

1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29

8.11
18.55
20.33
21. 05
24.21
25.01
30.97
35.12
36.02
53.33
61. 70
65.83
66.66
79.64
80.95
92.83
111.64
115.90
158.34
275.50
276.21
301.87
302.70
306.39
332.83
355.16
382.32
382.87
385.87

15
12
23
59
9
18
1967
450
92
42
242
90
29
46
777
9
160
72
6
62
24
160
22
39
51
423
12
77
141

4
7
18
24
3
11
132
16
3
17
26
14
13
22
13
10
35
7
7
0
0
7
4
0
10
3
1
4
14

0
0
1
1
3
3
0
2
2
0
0
3
3
2
2
0
0
0
0
1
1
1
1
0
0
0
6
6
0

~f'i/r'J

9-AUG-2013 06:44:48.84

Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian

FWHM Channel

Left

Pw

83.17
183.39
200.48
207.37
237.72
245.33
302.58
342.39
351.00
517.08
597.40
637.09
645.00
769.62
782.20
896.19
1076.62
1117.54
1524.75
2649.00
2655.78
2902.00
2910.02
2945.38
3199.14
3413.39
3674.00
3679.31
3708.05

79
176
195
195
236
236
283
330
330
509
584
626
626
755
755
887
1064
1107
1516
2637
2637
2887
2887
2928
3182
3397
3667
3667
3692

9
13
22
22
23
23
35
30
30
15
25
29
29
38
38
14
21
22
13
24
24
28
28
29
28
31
23
23
29

0.37
0.84
0.55
0.56
0.38
0.63
0.79
0.68
0.57
0.53
0.96
0.88
0.66
0.81
0.71
0. 47
0.85
0.92
0.11
1. 03
0.93
1. 06
0.96
0.35
0.45
0.93
1.16
0.98
0.94

9-AUG-2013 06:29:33.
1.00000E+OO filter
0
BAFIL
0 00:15:01.16 0.1%
4096
10.00000
Cts/Sec %Err

l.70E-02
1. 28E-02
2.51E-02
6.56E-02
9.75E-03
1.99E-02
2.19E+OO
5.00E-01
1.02E-01
4.70E-02
2.69E-01
1.00E-01
3.23E-02
5.09E-02
8.63E-01
1. 05E-02
1. 78E-01
7.95E-02
7.03E-03
6.94E-02
2.69E-02
1.78E-01
2.50E-02
4.33E-02
5.65E-02
4.70E-01
l.31E-02
8.55E-02
1.57E-01

35.4
54.4
45.1
24.3
30.4
47.8
2.9
5.6
20.6
23.9
8.0
14.5
42.0
40.0
3.7
67.8
11.1
14.4
76.7
11. 3
23.0
7.3
32.7
16.0
18.9
4.9
57.3
12.4
9.9

Fit

2.44E+OO
1.27E+OO
1.12E+OO

9.29E-01
1.33E+OO

7.93E-01
6.84E+OO

1.33E+OO

S367

Summary of Nuclide Activity


Sample ID : 1307154-05

Acquisition date

Total number of lines in spectrum


Number of unidentified lines
Number of lines tentatively identified by NID

29
22
7

Page :
2
9-AUG-2013 06:29:33

24.14%

Nuclide Type : FISSION


Nuclide
BA-133

Hlife
10.50Y

Wtd Mean
Uncorrected
Decay pCi/filter
1.00 3.922E+02

Total Activity

3.922E+02

Wtd Mean
Decay Corr
pCi/f ilter
3.922E+02

2-Sigma
Decay Corr
2-Sigma Error %Error Flags
16.97
0.665E+02

3.922E+02

Nuclide Type : NATURAL


Nuclide
Hlife
PA-234 4.47E+09Y
TH-234 4.47E+09Y

Wtd Mean
Uncorrected
Decay pCi/f ilter
1. 00
2.731E+OO
1. 00
2.190E+02

Wtd Mean
Decay Corr
pCi/f ilter
2.731E+OO
2.190E+02

Total Activity :

2.217E+02

2.217E+02

Grand Total Activity :

6.139E+02

6.139E+02

Flags: "K"
"E"

=
=

Keyline not found


Manually edited

"M"
"A"

=
=

Decay Corr
2-Sigma
2-Sigma Error %Error Flags
1.330E+OO
48.70
16.46
0.360E+02

Manually accepted
Nuclide specific abn. limit

8368

Nuclide Line Activity Report


Sample ID : 1307154-05

Acquisition date

Page :
3
9-AUG-2013 06:29:33

Nuclide Type: FISSION


Nuclide
BA-133

Energy
81.00
302.84
356.01

%Abn
33.00*
17.80
60.00

Final Mean for

Uncorrected Decay Corr 2-Sigma


%Ef f
pCi/f ilter pCi/filter %Error
3.922E+02 16.97
l.802E+Ol 3.922E+02
l.474E+02 70.46
2.575E+OO 1.474E+02
4.907E+02 17.51
4.312E+OO 4.907E+02

3 Valid Peaks =

Status
OK
OK
OK

3.922E+02+/- 6.654E+Ol ( 16.97%)

Nuclide Type: NATURAL


Nuclide
PA-234

Energy
9.89
21.72
37.93
131.42

%Abn
89.00
64.90*
23.75
20.40

Final Mean for


TH-234

63.29

Flag:

11

* 11

Keyline

3 Valid Peaks

3.80*

Final Mean for

Uncorrected Decay Corr 2-Sigma


%Ef f
pCi/filter pCi/filter %Error
5.150E-01 70.84
l.OOOE+02 5.150E-01
2.731E+OO 48.70
l.OOOE+02 2.731E+OO
1.158E+Ol 41.48
1.000E+02 1.158E+Ol
2.473E+OO - - - - - Line Not Found - - - - -

8.750E+Ol

1 Valid Peaks

2.731E+OO+/- 1.330E+OO ( 48.70%)

2.190E+02

Status
OK
OK
OK
Absent

2.190E+02

16.46

OK

2.190E+02+/- 3.604E+Ol ( 16.46%)

Combined Activity-MDA Report


Sample ID : 1307154-05

Acquisition date

Page :
4
9-AUG-2013 06:29:33

Identified Nuclides
Nuclide
BA-133
PA-234
TH-234

Activity
(pCi/filter)

Act error

3.922E+02
2.731E+OO
2.190E+02

6.654E+Ol
1.330E+OO
3.604E+Ol

MDA
(pCi/filter)
1.139E+Ol
1.134E+OO
2.063E+Ol

MDA error

Act/MDA

1.677E+OO
1.276E-02
2.655E-01

34.424
2.409
10.613

Non-Identified Nuclides

Nuclide
C0-57
CD-109
PA-231
NP-237
AM-241

Key-Line
Activity K.L.
(pCi/filter)Ided
-4.628E+OO
1.551E+Ol
1.091E+OO
-4.130E+OO
2.965E-01

Act error

MDA
(pCi/filter)

MDA error

Act/MDA

1.261E+Ol
8.594E+Ol
7.731E-01
2.426E+Ol
1.469E+OO

2.206E+Ol
1.634E+02
1.426E+OO
4.367E+Ol
2.335E+OO

7.478E+OO
1.573E+Ol
1.605E-02
3.852E+OO
2.628E-02

-0.210
0.095
0.766
-0.095
0.127

CY

VAX/VMS Peak Search Report Generated


Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level

cg( llt:J

DKAlOO: [GAMMA.SCUSR.ARCHIVE]SMP_130715406 GE5 BAFIL 194511. CN


PEAK V16.9 PEAKEFF V2.2
PZ-102-SS TOT
9-AUG-2013 00:00:00.
1307154-06
FILTER
GE5
0 00:15:00.00
25
3.00000
No

Pk It

Energy

Area

Bkgnd

1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19

3.54
8.44
17.61
21. 21
30.95
35.14
35.91
53.42
61. 65
62.18
65.74
81. 00
111.79
301.97
302.49
333.20
355.09
382.94
386.03

15
6
15
26
733
151
48
14
52
35
36
255
52
14
34
19
174
20
49

20
6
0
7
29
24
10
12
3
2
14
33
15
2
2
6
7
8
13

0
0
0
0
0
1
1
0
1
1
0
0
0
1
1
0
0
0
0

9-AUG-2013 07:06:25.68

Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian

FWHM Channel

Left

Pw

39.40
86.37
174.33
208.94
302.41
342.54
350.00
518.00
597.00
602.00
636.17
782.63
1078.13
2903.00
2908.00
3202.66
3412.75
3679.94
3709.65

38
81
169
201
290
334
334
508
587
587
627
773
1065
2890
2890
3192
3396
3666
3695

5
9
11
14
22
23
23
17
19
19
20
18
20
25
25
19
28
25
26

0.14
0.27
0.13
0.54
0.74
0.62
0.57
0.48
0.65
0.65
0.60
0.66
0.50
1. 06
1. 06
0.63
0.47
0.87
0.76

9-AUG-2013 06:51:07.
1.00000E+OO filter
0
BAFIL
0.1%
0 00:15:01.03
4096
10.00000
Cts/Sec %Err

1. 68E-02
6.39E-03
1.67E-02
2.89E-02
8.14E-01
1.68E-01
5.31E-02
1.51E-02
5.80E-02
3.93E-02
4.03E-02
2.83E-01
5.76E-02
1.55E-02
3.80E-02
2.16E-02
1. 94E-01
2.27E-02
5.43E-02

Fit

59.7
90.7
25.8
29.2
4.1
11. 0 3.13E+OO
26.6
65.9
19.4 1.58E+OO
17.3
26.8
7.7
20.4
52.4 1.25E+OO
17.9
30.8
8.2
33.5
20.0

5371

Summary of Nuclide Activity


Sample ID : 1307154-06

Acquisition date

Total number of lines in spectrum


Number of unictentif ied lines
Number of lines tentatively identified by NID

19
13
6

Page :
2
9-AUG-2013 06:51:07

31. 58%

Nuclide Type : FISSION


Nuclide
BA-133

Hlif e
10.50Y

Wtd Mean
Uncorrected
Decay pCi/filter
1.00 l.286E+02

Total Activity

l.286E+02

Wtd Mean
Decay Corr
pCi/filter
l.286E+02

2-Sigma
Decay Corr
2-Sigma Error %Error Flags
21. 71
0.279E+02

1.286E+02

Nuclide Type : NATURAL


Nuclide
Hlife
PA-231 3.28E+04Y
PA-234 4.47E+09Y
TH-234 4.47E+09Y

Decay
1. 00
1. 00
1. 00

Total Activity
Grand Total Activity :
Flags: "K"
"E"

=
=

Wtd Mean
Uncorrected
pCi/filter
4.lllE-01
1.202E+OO
3.195E+Ol

Wtd Mean
Decay Corr
pCi/filter
4.lllE-01
1.202E+OO
3.195E+Ol

3.356E+Ol

3.356E+Ol

1.621E+02

1.621E+02

Keyline not found


Manually edited

"M"
"A"

Decay Corr
2-Sigma
2-Sigma Error %Error Flags
181.41

7.458E-01
0.704E+OO
58.55

1.112E+Ol
34.81

Manually accepted
specific abn. limit

= Nuclide

mJ72

Nuclide Line Activity Report


Sample ID : 1307154-06

Acquisition date

Page :
3
9-AUG-2013 06:51:07

Nuclide Type: FISSION


Nuclide
BA-133

Energy
81.00
302.84
356.01

%Abn
33.00*
17.80
60.00

Final Mean for

Uncorrected Decay Corr 2-Sigma


%Ef f
pCi/filter pCi/filter %Error
1.286E+02 21. 71
1.802E+Ol 1.286E+02
2.243E+02 44.54
2.575E+OO 2.242E+02
2.023E+02 21. 87
4.312E+OO 2.023E+02

3 Valid Peaks =

Status
OK
OK
OK

1.286E+02+/ 2.792E+Ol ( 21. 71%)

Nuclide Type: NATURAL


Nuclide
PA-231

Energy
9.28
10.11
283.67
302.67

%Abn
42.00*
20.20
1. 60
2.30

Final Mean for


PA-234

9.89
21. 72
37.93
131.42

TH-234

63.29

Flag:

11

2 Valid Peaks

3.80*

Final Mean for

1.000E+02
1.000E+02
l.OOOE+02
2.473E+OO

8.750E+Ol

1 Valid Peaks

Status
OK
OK
Absent
OK

4.lllE-01+/ 7.458E-01 (181.41%)

3 Valid Peaks

89.00
64.90*
23.75
20.40

Final Mean for

Uncorrected Decay Corr 2-Sigma


%Ef f
pCi/filter pCi/filter %Error
4.lllE-01 181. 41
l.OOOE+02 4.lllE-01
l.OOOE+02 8.548E-01
8.548E-01 181.41
2.191E+OO - - - - Line Not Found - - - -
2.572E+OO l.738E+03
1.738E+03 43.40

1.940E-01
1.202E+OO
- - - - Line
- - - - Line

OK
OK
Absent
Absent

l.202E+OO+/ 7.035E-01 ( 58.55%)

3.195E+Ol

l.940E-01 181.41
l.202E+OO 58.55
Not Found - - - -
Not Found - - - -

3.195E+Ol

34.81

OK

3.195E+Ol+/ 1.112E+Ol ( 34.81%)

* 11 = Key line

~373

Combined Activity-MDA Report


Sample ID : 1307154-06
- - - -

Acquisition date

Page :
4
9-AUG-2013 06:51:07

Identified Nuclides

Nuclide
BA-133
PA-231
PA-234
TH-234

Activity
(pCi/ filter)
l.286E+02
4.lllE-01
l.202E+OO
3.195E+Ol

Act error

MDA
(pCi/filter)

MDA error

Act/MDA

2.792E+Ol
7.458E-01
7.035E-01
l.112E+Ol

1.359E+Ol
1.287E+OO
7.761E-01
1.653E+Ol

2.000E+OO
1.449E-02
8.736E-03
2.127E-01

9.464
0.319
1. 548
1. 933

Act error

MDA
(pCi/ filter)

MDA error

Act/MDA

6.035E+OO
1.355E+Ol
3.243E+OO
2.006E-02

-0.182
0.185
0.090
0.318

Non-Identified Nuclides

Nuclide
C0-57
CD-109
NP-237
AM-241

Key-Line
Activity K.L.
(pCi/filter)Ided
-3.239E+OO
2.610E+Ol
3.314E+OO
5.661E-01

9.874E+OO
6.947E+Ol
l.870E+Ol
9.621E-01

1.780E+Ol
1.408E+02
3.677E+Ol
l.782E+OO

a...
VAX/VMS Peak Search Report Generated
Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level

B(~ ti/

DKAlOO: [GAMMA.SCUSR.ARCHIVE]SMP_130715407 GE5 BAFIL 194514.CN


PEAK V16.9 PEAKEFF V2.2
PZ-102-SS DIS
9-AUG-2013 00:00:00.
1307154-07
FILTER
GE5
0 00:15:00.00
25
3.00000
No

Pk It

Energy

Area

Bkgnd

1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23

21.04
30.98
35.10
36.02
45.73
53.22
55.69
61.69
65.62
66.27
79.62
81.00
83.73
111.74
275.77
302.18
333.03
333.55
355.17
382.53
383.15
385.88
386.07

95
1856
350
77
16
45
22
275
78
47
57
818
33
187
41
102
98
11
380
28
66
162
12

23
137
19
10
0
0
7
18
13
21
8
7
7
56
5
8
6
3
3
4
5
9
8

0
0
1
1
0
0
0
0
2
2
2
2
0
0
0
0
1
1
0
1
1
9
9

9-AUG-2013 07:28:38.44

Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian

9-AUG-2013 07:13:24.
1.00000E+OO filter
0
BAFIL
0 00:15:01.10 0.1%
4096
10.00000

FWHM Channel

Left

Pw

Cts/Sec %Err

0.56
0.84
0.62
0.57
0.26
0.41
0.38
0.76
0.80
0.80
0.84
0.68
1. 44
0.96
1.27
0.79
1.10
1.10
0.83
1.16
1.16
1. 27
1.16

198
292
329
329
435
510
531
586
626
626
756
756
798
1065
2637
2890
3185
3185
3396
3661
3661
3693
3693

18
28
33
33
19
13
15
22
29
29
37
37
20
22
24
26
27
27
37
32
32
25
25

1.06E-01 15.5
2.06E+OO 3.0
3.89E-01 6.5
8.58E-02 23.6
l.78E-02 25.0
5.00E-02 14.9
2.42E-02 31. 8
3.05E-01 6.9
8.65E-02 17.3
5.24E-02 32.0
6.35E-02 29.9
9.09E-01 3.6
3.72E-02 23.6
2.08E-01 11. 3
4.58E-02 19.4
l.13E-01 11.2
1. 09E-01 9.3
1.24E-02 60.2
4.22E-01 5.2
3.14E-02 35.2
7.38E-02 14.4
1. 80E-01 8.4
1.31E-02111.0

207.32
302.71
342.22
351. 00
444.19
516.11
539.80
597.31
635.01
641.33
769.40
782.62
808.83
1077.63
2651.63
2905.06
3201.00
3206.00
3413.47
3676.00
3682.00
3708.13
3710.00

Fit

9.19E-01

6.45E-01
7.22E-01

2.23E+OO
5.36E-01
9.40E-01

!1375

Summary of Nuclide Activity


Sample ID : 1307154-07

Acquisition date

Total number of lines in spectrum


Number of unidentified lines
Number of lines tentatively identified by NID

23
17
6

Page :
2
9-AUG-2013 07:13:24

26.09%

Nuclide Type : FISSION


Nuclide
BA-133

Hlife
10.50Y

Wtd Mean
Uncorrected
Decay pCi/filter
1.00 4.132E+02

Total Activity

4.132E+02

Wtd Mean
Decay Corr
pCi/filter
4.132E+02

2-Sigma
Decay Corr
2-Sigma Error %Error Flags
16.87
0.697E+02

4.132E+02

Nuclide Type : NATURAL


Nuclide
Hlife
TH-234 4.47E+09Y

Wtd Mean
Uncorrected
Decay pCi/filter
1.00 2.480E+02

Wtd Mean
Decay Corr
pCi/filter
2.480E+02

Total Activity :

2.480E+02

2.480E+02

Grand Total Activity :

6.613E+02

6.613E+02

Flags: "K"
"E"

=
=

Keyline not found


Manually edited

"M"
"A"

=
=

Decay Corr
2-Sigma
2-Sigma Error %Error Flags
14.45
0.358E+02

Manually accepted
Nuclide specific abn. limit

Nuclide Line Activity Report


Sample ID : 1307154-07

Acquisition date

Page :
3
9-AUG-2013 07:13:24

Nuclide Type: FISSION


Nuclide
BA-133

Energy
81. 00
302.84
356.01

%Abn
33.00*
17.80
60.00

Final Mean for

Uncorrected Decay Corr 2-Sigma


%Ef f
pCi/filter pCi/filter %Error
1.802E+Ol 4.132E+02
4.132E+02 16.87
2.575E+OO 6.674E+02
6.674E+02 34.63
4.312E+OO 4.405E+02
4.406E+02 17.87

3 Valid Peaks

Status
OK
OK
OK

4.132E+02+/- 6.971E+Ol ( 16.87%)

Nuclide Type: NATURAL


Nuclide
TH-234

Energy
63.29

%Abn
3.80*

Final Mean for


Flag:

11

* 11

Uncorrected Decay Corr 2-Sigma


%Ef f
pCi/filter pCi/filter %Error
8.750E+Ol 2.480E+02
2.480E+02 14.45

1 Valid Peaks

Status
OK

2.480E+02+/- 3.583E+Ol ( 14.45%)

Keyline

1377

Combined Activity-MDA Report


Sample ID : 1307154-07

Acquisition date

4
Page :
9-AUG-2013 07:13:24

Identified Nuclides
Nuclide
BA-133
TH-234

Activity
(pCi/filter)

Act error

MDA
(pCi/filter)

MDA error

Act/MDA

4.132E+02
2.480E+02

6.971E+Ol
3.583E+Ol

l.188E+Ol
1.820E+Ol

1.749E+OO
2.341E-01

34.778
13.631

Act error

MDA

(pCi/ filter)

MDA error

Act/MDA

l.530E+Ol
9.524E+Ol
8.984E-01
l.383E+OO
2.389E+Ol
1.657E+OO

2.942E+Ol
l.636E+02
l.663E+OO
l.962E+OO
4.115E+Ol
2.791E+OO

9.973E+OO
1.575E+Ol
l.872E-02
2.209E-02
3.629E+OO
3.142E-02

0.215
-0.255
0.025
2.252
-0.110
0.418

Non-Identified Nuclides

Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241

Key-Line
Activity K.L.
(pCi/filter)Ided
6.332E+OO
-4.166E+Ol
4.196E-02
4.419E+OO
-4.532E+OO
1.166E+OO

8378

VAX/VMS Peak Search Report Generated


Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level

<-,

~thJ

DKAlOO: [GAMMA.SCUSR.ARCHIVE]SMP_130715408 GE5 BAFIL 1945 8.CN


PEAK V16.9 PEAKEFF V2.2
PZ-107-SS TOT
9-AUG-2013 00:00:00.
1307154-08
FILTER
GE5
0 00:15:00.00
25
3.00000
No

Pk It

Energy

Area

Bkgnd

1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19

13.31
21.15
30.97
35.12
36.12
53.27
61. 70
66.03
79.61
80.97
111. 77
160.92
275.96
302.22
332.83
355.09
382.74
383.36
385.87

8
60
1447
275
75
42
189
67
45
596
119
29
26
86
44
286
56
26
82

3
37
105
23
17
3
31
35
5
7
34
17
7
9
3
13
5
8
17

0
0
0
1
1
0
0
0
6
6
0
0
0
0
0
0
1
1
0

9-AUG-2013 07:50:24.34

Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian

FWHM Channel

Left

Pw

0.70
0.22
0.72
0.62
0.57
0.43
0.86
0.79
0.60
0.72
0.84
0.30
0.67
0.41
0.63
0.59
1.16
1.16
1. 20

127
196
290
332
332
510
583
623
762
762
1065
1533
2636
2889
3182
3395
3668
3668
3696

12
21
25
29
29
14
27
26
31
31
22
27
23
28
28
29
23
23
21

133.11
208.34
302.57
342.43
352.00
516.59
597.41
638.99
769.28
782.38
1077.90
1549.55
2653.46
2905.44
3199.15
3412.75
3678.00
3684.00
3708.12

9-AUG-2013 07:34:55.
1.00000E+OO filter
0
BAFIL
0 00:15:01.11 Q.1%
4096
10.00000
Cts/Sec %Err

8.64E-03
6.69E-02
1.61E+OO
3.06E-01
8.31E-02
4.65E-02
2.lOE-01
7.41E-02
5.03E-02
6.62E-01
1.32E-01
3.21E-02
2.86E-02
9.53E-02
4.86E-02
3.17E-01
6.24E-02
2.91E-02
9.09E-02

Fit

57.5
28.3
3.3
7.7 1.65E+OO
21. 6
18.1
10.1
23.8
18.0 1.13E+OO
4.2
13.9
35.1
27.4
12.7
16.9
6.5
14.2 1.30E+OO
29.3
14.2

!379

Summary of Nuclide Activity


Sample ID : 1307154-08

Acquisition date

Total number of lines in spectrum


Number of unidentified lines
Number of lines tentatively identified by NID

19
13
6

Page :
2
9-AUG-2013 07:34:55

31. 58%

Nuclide Type : FISSION


Nuclide
BA-133

Hlif e
10.50Y

Wtd Mean
Uncorrected
Decay pCi/filter
1. 00 3.007E+02

Total Activity

---------

3.007E+02

Wtd Mean
Decay Corr
pCi/filter
3.007E+02

Decay Corr
2-Sigma
2-Sigma Error %Error Flags
0.524E+02
17.42

---------

3.007E+02

Nuclide Type : NATURAL


Nuclide
Hlife
TH-234 4.47E+09Y

Wtd Mean
Uncorrected
Decay pCi/f ilter
1. 00 1.705E+02

Total Activity
Grand Total Activity :
Flags: "K"
"E"

---------

Wtd Mean
Decay Corr
pCi/f ilter
1.705E+02

---------

1.705E+02

1.705E+02

4.711E+02

4.711E+02

Keyline not found


Manually edited

Decay Corr
2-Sigma
2-Sigma Error %Error Flags
0.351E+02
20.59

"M"
"A"

=
=

Manually accepted
Nuclide specific abn. limit

Nuclide Line Activity Report


Sample ID : 1307154-08

Acquisition date

Page :
3
9-AUG-2013 07:34:55

Nuclide Type: FISSION


Nuclide
BA-133

Energy
81. 00
302.84
356.01

%Abn
33.00*
17.80
60.00

Final Mean for

Uncorrected Decay Corr 2-Sigma


%Ef f
pCi/filter pCi/filter %Error
l.802E+Ol 3.007E+02
3.007E+02 17.42
2.575E+OO 5.616E+02
5.617E+02 36.63
4.312E+OO 3.315E+02
3.316E+02 19.51

3 Valid Peaks

Status
OK
OK
OK

3.007E+02+/- 5.237E+Ol ( 17.42%)

Nuclide Type: NATURAL


Nuclide
TH-234

Energy
63.29

%Abn
3.80*

Final Mean for


Flag:

11

* 11

Keyline

Uncorrected Decay Corr 2-Sigma


%Eff
pCi/filter pCi/filter %Error
8.750E+Ol l.705E+02
1.705E+02 20.59

1 Valid Peaks

Status
OK

1.705E+02+/- 3.510E+Ol ( 20.59%)

Combined Activity-MDA Report


Sample ID : 1307154-08

Acquisition date

Page :
4
9-AUG-2013 07:34:55

Identified Nuclides
Nuclide
BA-133
TH-234

Activity
(pCi/filter)

Act error

MDA
(pCi/filter)

MDA error

Act/MDA

3.007E+02
1.705E+02

5.237E+Ol
3.510E+Ol

l.033E+Ol
2.063E+Ol

l.522E+OO
2.655E-01

29.095
8.261

Non-Identified Nuclides

Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241

Key-Line
Activity K.L.
(pCi/filter)Ided
-5.213E+OO
6.935E+Ol
-2.456E-01
2.786E+OO
-2.104E+Ol
7.914E-01

Act error

MDA
(pCi/filter)

MDA error

Act/MDA

l.339E+Ol
8.785E+Ol
7.lOOE-01
l.580E+OO
2.156E+Ol
1.476E+OO

2.321E+Ol
1.794E+02
1.258E+OO
1.752E+OO
3.333E+Ol
2.476E+OO

7.867E+OO
1.727E+Ol
1.416E-02
1.973E-02
2.940E+OO
2.787E-02

-0.225
0.386
-0.195
1.590
-0.631
0.320

8382

VAX/VMS Peak Search Report Generated


Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level

9-AUG-2013 08:15:00.33

DKAlOO: [GAMMA.SCUSR.ARCHIVE]SMP_130715409 GE5 BAFIL 194522.CN


PEAK Vl6.9 PEAKEFF V2.2
PZ-107-SS DIS
9-AUG-2013 00:00:00.
1307154-09
FILTER
GE5
0 00:15:00.00
25
3.00000
No

Pk It

Energy

Area

Bkgnd

1 0
2 0
3 3
4 3
5 0
6 0
7 0
8 4
9 4
10 0
11 0
12 2
13 2
14 0
15 0
16 0
17 0
18 10
19 10
20 10
21 0
22 0
23 4
24 4
25 0
26 0
27 0

21.23
30.96
35.09
35.97
53.35
56.63
61. 72
65.29
65.82
81.00
111.81
115.32
115.85
117.49
175.94
182.59
275.70
301.98
302.23
302.78
332.88
355.12
382.53
383.70
385.75
389.96
413.53

80
2012
387
87
33
13
250
50
108
808
150
25
49
5
17
16
43
103
67
12
41
384
124
13
131
28
11

31
92
34
10
28
6
33
4
9
74
49
17
15
8
8
16
5
4
3
1
10
13
5
0
5
10
8

Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian

9-AUG-2013 07:59:41.
1.00000E+OO filter
0
BAFIL
0 00:15:01.13 0.1%
4096
10.00000

FWHM Channel

Left

Pw

Cts/Sec %Err

0.37
0.71
0.60
0.59
0.48
0.34
0.66
0.64
0.66
0.71
0.65
0.93
0.77
0.24
1. 23
0.50
0.59
1. 25
0.66
0.46
0.50
0.93
1.16
0.76
1.12
0.50
0.61

201
289
331
331
506
541
587
627
627
771
1068
1102
1102
1125
1680
1745
2637
2888
2888
2888
3185
3398
3667
3667
3693
3733
3961

15
25
26
26
17
13
22
27
27
21
22
24
24
10
21
21
24
26
26
26
25
27
23
23
26
24
19

8.90E-02 19.2
2.24E+OO 2.5
4.30E-01 6.2
9.64E-02 19.5
3.64E-02 41.8
1.40E-02 45.7
2.78E-01 8.0
5.55E-02 19.0
1.20E-01 12.4
8.98E-01 4.2
1.67E-01 13.3
2.83E-02 41. 2
5.49E-02 20.9
5.73E-03105.7
1.89E-02 39.8
1.78E-02 53.4
4.78E-02 18.9
1.15E-01 11. 0
7.46E-02 16.3
1.34E-02 46.8
4.56E-02 21. 3
4.27E-01 5.4
1.38E-01 6.4
1.46E-02 29.2
l.46E-01 9.3
3.16E-02 28.7
l.27E-02 50.7

209.12
302.50
342.07
350.58
517.33
548.78
597.67
631.87
637.00
782.65
1078.23
1111.93
1117.00
1132.78
1693.70
1757.42
2650.93
2903.05
2905.54
2910.80
3199.58
3413.00
3676.00
3687.25
3706.91
3747.30
3973.51

Fit

1. 20E+OO

3.65E+OO

1.97E+OO

4.97E+OO

6.08E+OO

li383

Summary of Nuclide Activity


Sample ID : 1307154-09

Acquisition date

Total number of lines in spectrum


Number of unidentified lines
Number of lines tentatively identified by NID

27
21
6

Page :
2
9 -AUG-2 O13 O7 : 5 9 : 4 1

22.22%

Nuclide Type : FISSION


Nuclide
BA-133

Hlife
10.SOY

Wtd Mean
Uncorrected
Decay pCi/f ilter
1.00 4.079E+02

Total Activity

4.079E+02

Wtd Mean
Decay Corr
pCi/filter
4.079E+02

2-Sigma
Decay Corr
2-Sigma Error %Error Flags
0.709E+02
17.37

4.079E+02

Nuclide Type : NATURAL


Nuclide
Hlife
TH-234 4.47E+09Y

Wtd Mean
Uncorrected
Decay pCi/filter
1.00 2.257E+02

Total Activity
Grand Total Activity :
Flags: "K"
"E"

=
=

Wtd Mean
Decay Corr
pCi/f ilter
2.257E+02

2.257E+02

2.257E+02

6.335E+02

6.335E+02

Keyline not found


Manually edited

"M"
"A"

=
=

Decay Corr
2-Sigma
2-Sigma Error %Error Flags
0.375E+02
16.63

Manually accepted
Nuclide specific abn. limit

Nuclide Line Activity Report


Sample ID : 1307154-09

Acquisition date

Page :
3
9-AUG-2013 07:59:41

Nuclide Type: FISSION


Nuclide
BA-133

Energy
81.00
302.84
356.01

%Abn
33.00*
17.80
60.00

Final Mean for

Uncorrected Decay Corr 2-Sigma


%Ef f
pCi/filter pCi/filter %Error
4.079E+02 17.37
l.802E+Ol 4.079E+02
2.575E+OO 7.908E+Ol
7.908E+Ol 97.34
4.462E+02 18.07
4.312E+OO 4.462E+02

3 Valid Peaks

Status
OK
OK
OK

4.079E+02+/- 7.087E+Ol ( 17.37%)

Nuclide Type: NATURAL


Nuclide
TH-234

Energy
63.29

%Abn
3.80*

Final Mean for


Flag:

11

* 11

Keyline

Uncorrected Decay Corr 2-Sigma


%Eff
pCi/filter pCi/filter %Error
8.750E+Ol 2.257E+02
2.257E+02 16.63

1 Valid Peaks

Status
OK

2.257E+02+/- 3.753E+Ol ( 16.63%)

Combined Activity-MDA Report


Sample ID : 1307154-09

Acquisition date

4
Page :
9-AUG-2013 07:59:41

Identified Nuclides
Nuclide
BA-133
TH-234

Activity
(pCi/filter)

Act error

MDA

(pCi/filter)

MDA error

Act/MDA

4.079E+02
2.257E+02

7.087E+Ol
3.753E+Ol

1.405E+Ol

2.397E+Ol

2.069E+OO
3.083E-01

29.032
9.415

Act error

MDA

(pCi/ filter)

MDA error

Act/MDA

l.444E+Ol
8.683E+Ol
8.182E-01
1.435E+OO
2.432E+Ol
1.392E+OO

2.798E+Ol
1.452E+02
l.528E+OO
2.096E+OO
4.778E+Ol
2.634E+OO

9.485E+OO
1.398E+Ol
1.720E-02
2.359E-02
4.214E+OO
2.966E-02

0.206
-0.365
0.016
1.768
0.246
0.690

Non-Identified Nuclides

Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241

Key-Line
Activity K.L.
(pCi/filter)Ided
5.753E+OO
-5.298E+Ol
2.399E-02
3.707E+OO
1.177E+Ol
1.817E+OO

E386

VAX/VMS Peak Search Report Generated


Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level

Sl9//:J

DK,AlOO: [GAMMA.SCUSR.ARCHIVE]SMP_130715410 GE5 BAFIL 194526.CN


PEAK V16.9 PEAKEFF V2.2
PZ-106-KS TOT
9-AUG-2013 00:00:00.
1307154-10
FILTER
GE5
0 00:15:00.00
25
3.00000
No

Pk It

Energy

Area

Bkgnd

1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22

10.43
20.85
30.98
35.07
36.07
61. 72
66.29
80.99
110.29
111. 65
115.74
116.47
275.97
302.07
302.77
306.56
332.97
354.39
355.20
382.53
383.27
385.86

7
76
1937
397
66
213
92
774
48
211
25
26
29
100
13
27
60
11
340
41
49
133

11
35
74
9
8
52
57
37
41
22
12
10
12
4
2
5
12
5
14
7
4
11

0
0
0
1
1
0
0
0
1
1
1
1
0
6
6
0
0
2
2
1
1
0

9-AUG-2013 08:36:25.92

Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian

9-AUG-2013 08:21:07.
1.00000E+OO filter
0
BAFIL
0 00:15:01.10 0.1%
4096
10.00000

FWHM Channel

Left

Pw

Cts/Sec %Err

0.28
0.80
0.76
0.62
0.62
0.70
1. 01
0.57
0.84
0.83
0.77
0.77
0.56
0.78
0.86
0.31
0.88
1.12
0.91
1.16
1. 04
1.20

99
194
293
330
330
587
624
773
1049
1049
1104
1104
2638
2891
2891
2930
3183
3397
3397
3660
3660
3693

10
20
20
29
29
22
29
22
39
39
30
30
23
24
24
25
27
30
30
28
28
28

7.78E-03100.3
8.42E-02 22.3
2.15E+OO 2.5
4.41E-01 5.5
7.37E-02 25.4
2.37E-01 10.0
l.02E-01 22.5
8.60E-01 4.0
5.31E-02 31. 5
2.34E-01 8.5
2.76E-02 42.7
2.91E-02 40.3
3.17E-02 30.0
1.llE-01 11. 3
1.43E-02 53.7
3.00E-02 24.7
6.68E-02 16.7
1.27E-02137.8
3.78E-01 6.0
4.53E-02 25.0
5.39E-02 13.8
1.48E-01 9.9

105.43
205.41
302.64
341. 92
351.46
597.63
641.44
782.52
1063.73
1076.73
1116.00
1123.00
2653.47
2903.94
2910.64
2947.01
3200.49
3406.00
3413.76
3676.00
3683.11
3708.02

Fit

9.96E-01

l.82E+OO
7.07E-01
5.93E-01

1.09E+OO
1.03E+OO

i387

Summary of Nuclide Activity


Sample ID : 1307154-10

Acquisition date

Total number of lines in spectrum


Number of unidentified lines
Number of lines tentatively identified by NID

22
15
7

Page :
2
9-AUG-2013 08:21:07

31.82%

Nuclide Type : FISSION


Nuclide
BA-133

Hlife
10.50Y

Wtd Mean
Uncorrected
Decay pCi/filter
1.00 3.907E+02

Total Activity

Wtd Mean
Decay Corr
pCi/filter
3.907E+02

3.907E+02

3.907E+02

Wtd Mean
Uncorrected
pCi/filter
5.005E-01
3.505E+OO
1.925E+02

Wtd Mean
Decay Corr
pCi/f ilter
5.005E-01
3.505E+OO
l.925E+02

1.965E+02

1.965E+02

5.872E+02

5.872E+02

2-Sigma
Decay Corr
2-Sigma Error %Error Flags
17.25
Q.674E+02

Nuclide Type : NATURAL


Nuclide
Hlife
PA-231 3.28E+04Y
PA-234 4.47E+09Y
TH-234 4.47E+09Y

Decay
1. 00
1. 00
1. 00

Total Activity
Grand Total Activity :
Flags: "K"
"E"

=
=

Keyline not found


Manually edited

"M"
"A"

=
=

2-Sigma
Decay Corr
2-Sigma Error %Error Flags
10.04E-01
200.55
44.84
1.572E+OO
20.42
0.393E+02

Manually accepted
Nuclide specific abn. limit

8388

Nuclide Line Activity Report


Sample ID : 1307154-10

Acquisition date

Page :
3
9-AUG-2013 08:21:07

Nuclide Type: FISSION


Nuclide
BA-133

Energy
81.00
302.84
356.01

%Abn
33.00*
17.80
60.00

Final Mean for

Uncorrected Decay Corr 2-Sigma


%Ef f
pCi/filter pCi/filter %Error
1.802E+Ol 3.907E+02
3.907E+02 17.25
2.575E+OO 8.414E+Ol
8.415E+Ol 110.65
3.945E+02 18.75
4.312E+OO 3.945E+02

3 Valid Peaks =

Status
OK
OK
OK

3.907E+02+/- 6.741E+Ol ( 17.25%)

Nuclide Type: NATURAL


Nuclide
PA-231

Energy
9.28
10.11
283.67
302.67

%Abn
42.00*
20.20
1. 60
2.30

Final Mean for


PA-234

9.89
21.72
37.93
131.42

TH-234

63.29

11

* 11 = Keyline

l.OOOE+02
l.OOOE+02
1.000E+02
2.473E+OO

8.750E+Ol

1 Valid Peaks

----110.19

Status
OK
OK
Absent
OK

2.362E-01 200.55
3.505E+OO 44.84
8.385E+OO 50.92
Not Found - - - - -

OK
OK
OK
Absent

3.505E+OO+/- 1.572E+OO ( 44.84%)

1.925E+02

2-Sigma
%Error
200.55
200.55

5.005E-01+/- 1.004E+OO (200.55%)

2.362E-01
3.505E+OO
8.385E+OO
----Line

3 Valid Peaks =

3.80*

Final Mean for


Flag:

3 Valid Peaks =

89.00
64.90*
23.75
20.40

Final Mean for

Uncorrected Decay Corr


%Ef f
pCi/f ilter pCi/filter
1.000E+02 5.005E-01
5.005E-01
1.000E+02 1.041E+OO
l.041E+OO
2.191E+OO - - - - - Line Not Found
2.572E+OO 6.522E+02
6.522E+02

1.925E+02

20.42

OK

1.925E+02+/- 3.930E+Ol ( 20.42%)

Combined Activity-MDA Report


Sample ID : 1307154-10

Acquisition date

Page :
4
9-AUG-2013 08:21:07

Identified Nuclides
Nuclide
BA-133
PA-231
PA-234
TH-234

Activity
(pCi/filter)
3.907E+02
5.005E-01
3.505E+OO
l.925E+02

Act error

MDA
(pCi/filter)

MDA error

Act/MDA

6.741E+Ol
1.004E+OO
1.572E+OO
3.930E+Ol

1.732E+Ol
1.923E+OO
1.175E+OO
4.103E+Ol

2.549E+OO
2.164E-02
1.322E-02
5.279E-01

22.563
0.260
2.984
4.691

Non-Identified Nuclides

Nuclide
C0-57
CD-109
NP-237
AM-241

Key-Line
Activity K.L.
(pCi/filter)Ided
-4.240E+OO
l.002E+Ol
-8.085E+OO
2.368E-01

Act error

MDA
(pCi/f il ter)

MDA error

Act/MDA

1.470E+Ol
8.260E+Ol
2.301E+Ol
1.560E+OO

2.585E+Ol
1.566E+02
4.041E+Ol
2.439E+OO

8.764E+OO
1.507E+Ol
3.565E+OO
2.746E-02

-0.164
0.064
-0.200
0.097

VAX/VMS Peak Search Report Generated


Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
Pk It
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32

3
3
0
1
1
0
0
4
4
0
0
0
6
6
1
1
1
1
1
0
0
3
3
0
1
1
0
0
0
0
0
0

9-AUG-2013 07:28:06.95

Cd(///>

DKAlOO: [GAMMA.SCUSR.ARCHIVE]SMP_130715411 GE2 BAFIL 194513.CN


PEAK V16.9 PEAKEFF V2.2
PZ-106-KS DIS
9-AUG-2013 00:00:00.
1307154-11
FILTER
GE2
0 00:15:00.00
25
3.00000
No

Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian

Energy

Area

Bkgnd

FWHM Channel

Left

Pw

30.98
35.26
52.89
61.92
65.75
81.12
94.73
111.92
116.23
160.75
167.60
185.76
276.12
281.13
299.05
303.00
306.94
333.86
338.05
356.09
364.86
383.91

386.95
391. 35
414.72
418.07
437.45
468.02
511. 23
583.36
697.78

1002.28

2013
481
60
191
82
826
29
193
31
51
21
31
40
13
8
158
30
69
27
517
11
101
160
40
29
16
76
18
24
13
14
8

116
101
57
60
61
116
86
53
61
57
46
70
19
18
3
8
12
15
9
33
25
11
10
14
10
11
18
7
8
0
2
0

1.35
31.10
1. 56
35.38
2.25
53.00
1.46
62.03
1.47
65.87
1. 52
81. 23
1. 74
94.84
1. 60 112.03
2.07 116.34
1. 41 160.87
2.93 167.71
3.10 185.87
2.04 276.23
2.83 281.23
1. 78 299.16
1. 78 303.10
1. 79 307.05
1. 74 333.96
1. 82 338.16
1. 52 356.20
1. 64 364.97
2.06 384.02
1.49 387.06
1. 99 391.46
1. 88
414.83
1.89 418.17
1.70 437.55
1.74 468.12
1. 35 511. 34
1. 90 583.46
4.42 697.88
2.98 1002.38

27
27
50
57
57
77
90
108
108
157
165
182
270
270
297
297
297
328
328
351
361
380
380
390
411
411
433
464
509
580
694
998

14
14
6
14
14
9
9
13
13
8
7
8
15
15
21
21
21
14
14
9
9
10
10
6
14
14
9
7
7
8
8
8

9-AUG-2013 07:12:50.
1.00000E+OO filter
0
BAFIL
0 00:15:00.29 0.0%
4096
10.00000
Cts/Sec %Err

2.24E+OO
5.34E-01
6.63E-02
2.12E-01
9.15E-02
9.18E-01
3.25E-02
2.14E-01
3.49E-02
5.64E-02
2.28E-02
3.41E-02
4.45E-02
1.48E-02
9.28E-03
1.76E-01
3.30E-02
7.70E-02
2.96E-02
5.75E-01
1.22E-02
l.12E-01
1.77E-01
4.48E-02
3.25E-02
1.83E-02
8.44E-02
2.02E-02
2.64E-02
1.44E-02
1.58E-02
8.89E-03

Fit

2.3 3.78E+OO
5.7
23.9
9.7 l.87E+OO
17.8
4.2
60.4
9.0 2.52E+OO
49.0
29.5

58.9

50.5

25.8 3.62E+OO
63.5
45.6 2.52E+OO
8.2
31. 7
14.5 1.38E+OO
28.9
4.8
87.2

12.9 l.86E+OO
9.0
21. 7

24.8 1.58E+OO
48.1
15.3
33.5
28.9

27.7

31. 5

35.4

Summary of Nuclide Activity


Sample ID : 1307154-11

Acquisition date

Total number of lines in spectrum


Number of unidentified lines
Number of lines tentatively identified by NID

32
28
4

Page :
2
9-AUG-2013 07:12:50

12.50%

Nuclide Type : FISSION


Nuclide
BA-133

Hlife
10.50Y

Wtd Mean
Uncorrected
Decay pCi/filter
1. 00 4.180E+02

Total Activity

--------4.180E+02

Wtd Mean
Decay Corr
pCi/filter
4.180E+02

Decay Corr
2-Sigma
2-Sigma Error %Error Flags
0.811E+02
19.40

---------

4.180E+02

Nuclide Type : NATURAL


Nuclide
Hlife
TH-234 4.47E+09Y

Wtd Mean
Uncorrected
Decay pCi/filter
1. 00 6.543E+02

Total Activity
Grand Total Activity :
Flags: "K"
"E"

=
=

---------

Wtd Mean
Decay Corr
pCi/filter
6.543E+02

---------

6.543E+02

6.543E+02

1.072E+03

1.072E+03

Keyline not found


Manually edited

"M"
"A"

=
=

Decay Corr
2-Sigma
2-Sigma Error %Error Flags
1.400E+02
21. 40

Manually accepted
Nuclide specific abn. limit

ili392

Nuclide Line Activity Report


Sample ID : 1307154-11

Acquisition date

Page :
3
9-AUG-2013 07:12:50

Nuclide Type: FISSION


Nuclide
BA-133

Energy
81. 00
302.84
356.01

%Abn
33.00*
17.80
60.00

Final Mean for

Uncorrected Decay Corr 2-Sigma


%Ef f
pCi/filter pCi/filter %Error
1.799E+Ol 4.180E+02
4.180E+02 19.40
7.560E+OO 3.527E+02
3.527E+02 34.07
7.170E+OO 3.611E+02
3.612E+02 17.95

3 Valid Peaks

Status
OK
OK
OK

4.180E+02+/- 8.108E+Ol ( 19.40%)

Nuclide Type: NATURAL


Nuclide
TH-234

Energy
63.29

%Abn
3.80*

Final Mean for


Flag:

11

* 11

Keyline

uncorrected Decay Corr 2-Sigma


%Eff
pCi/filter pCi/filter %Error
2.305E+Ol 6.543E+02
6.543E+02 21.40

1 Valid Peaks

Status
OK

6.543E+02+/- 1.400E+02 ( 21.40%)

Combined Activity-MDA Report


Sample ID : 1307154-11
- -

Acquisition date

Page :
4
9-AUG-2013 07:12:50

- - Identified Nuclides

Nuclide
BA-133
TH-234

Activity
(pCi/filter)

Act error

4.180E+02
6.543E+02

8.108E+Ol
1.400E+02

MDA
(pCi/filter)
1.713E+Ol
1.269E+02

MDA error

Act/MDA

2.917E+OO
1.049E+Ol

24.401
5.156

MDA error

Act/MDA

1.305E+OO
1.887E+Ol
1.462E-01
6.706E-02
5.836E+OO
1.420E+OO

-0.362
-0.801
3.150
1. 254
0.447
1. 249

Non-Identified Nuclides

Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241

Key-Line
Activity K.L.
(pCi/filter)Ided
-3.074E+OO
-l.316E+02
2.418E+Ol
4.076E+OO
2.312E+Ol
2.292E+Ol

Act error
5.658E+OO
1.358E+02
3.813E+OO
l.652E+OO
3.217E+Ol
9.654E+OO

MDA
(pCi/filter)
8.499E+OO
1.643E+02
7.676E+OO
3.251E+OO
5.169E+Ol
l.834E+Ol

8393

VAX/VMS Peak Search Report Generated


Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
Pk It
1

2
3

4
5
6

7
8
9

10
11

12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28

3
3
3
0
0
1
1

0
0
4
4
0
0
0
4
4
3
3
2
2
1
1
1
1
0
0
0
0

9-AUG-2013 07:49:30.10

C::...-

DKAlOO: [GAMMA.SCUSR.ARCHIVE]SMP_130715412 GE2 BAFIL


PEAK V16.9 PEAKEFF V2.2
DUP 08 TOT
9-AUG-2013 00:00:00.
1307154-12
FILTER
GE2
0 00:15:00.00
25
3.00000
No

Energy

Area

Bkgnd

28.03
31. 02
35.03
47.03
52.46
61. 84
65.87
81. 09
92.24