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Document No: UOG-ENG-SPC-45-011

Revision No.: 01
SPECIFICATION FOR TITANIUM
01 Issued for Comment I. McInnes 6/07/04 J. Wells 6/07/04
Issue
Rev
Issue or Revision
Description
Origin By Date Chkd By Date Appd
By
Date Appd
By
Date
AMEC CLIENT
Specification for Titanium
UOG-ENG-SPC-45-011 Page 2 of 9 Revision 01
CONTENTS
1.0 INTRODUCTION ......................................................................................................................... 3
2.0 SUPPLIER QUALIFICATION...................................................................................................... 3
3.0 CERTIFICATION......................................................................................................................... 3
4.0 PACKING & MARKING............................................................................................................... 3
5.0 DOCUMENTATION..................................................................................................................... 4
DATA SHEETS.................................................................................................................................... 5
MATERIAL DATA SHEET 1 .............................................................................................................. 6
Flanges, Hubs, Spacers, Spades, Weldolets, Flangeolets, Nippolets and Sweepolets .................. 6
MATERIAL DATA SHEET 2 .............................................................................................................. 7
Fittings ............................................................................................................................................. 7
MATERIAL DATA SHEET 3 .............................................................................................................. 8
Pipe and Bends................................................................................................................................ 8
MATERIAL DATA SHEET 4 .............................................................................................................. 9
Sheet and Plate ............................................................................................................................... 9
Specification for Titanium
UOG-ENG-SPC-45-011 Page 3 of 9 Revision 01
1.0 INTRODUCTION
This specification defines the requirements for titanium components complying with UNS
R50400 for pressure systems manufactured in accordance with ASME B31.3, ASME B16.34,
API 510, ASME VIII and PD5500. It is required to address deficiencies in the commonly
utilised ASTM standards, which have been identified through practical field experience.
The selected options in the referred standards and additional requirements shall be added or
supersede the corresponding requirements in the referred standard.
The latest revision of the specified design codes/ specifications at the time of contract award
shall be used.
2.0 SUPPLIER QUALIFICATION
Suppliers shall be able to demonstrate their ability to meet the minimum requirements of the
applicable material specification and the additional requirements of this specification.
Material suppliers, in addition to operating a BS EN ISO 9001 or equivalent accredited
Quality Assurance system, shall:
Qualify to NORSOK M-650 Rev. 2 for titanium.
Display a knowledge and relevant experience in the type of material(s) to be
manufactured. Experience may be demonstrated via statistical data or relevant test
records for the types of materials to be supplied.
Maintain and operate acceptable facilities and equipment, which shall be calibrated at
prescribed intervals. This should be undertaken in accordance with the suppliers
calibration procedure.
Be subject to a full audit by AMEC QA and Metallurgy unless the supplier can
demonstrate an adequate system of control in the pre-qualification data submitted.
However, if the criticality rating of the scope of supply dictates, a full system audit will be
undertaken.
3.0 CERTIFICATION
Unless specified otherwise in the item description or Purchase Order, certification is to be in
accordance with BS EN 10204 Type 3.1.B with independent witness at the final mechanical
testing stages. Specified certificates are to be supplied with the order.
4.0 PACKING & MARKING
Packing is to be the responsibility of the supplier and shall be such as to ensure that the
items are not damaged during transportation to AMEC. Particular attention should be paid to
the adequate protection of bevelled ends and sealing faces using plastic caps.
Items shall be palletised and shrink-wrapped. In addition further protection such as end
protectors and wooden blocks shall be used. Titanium items shall be packed separately from
all other items to avoid contamination. Titanium items (including pipe and plate) shall be
packed utilising plastic banding and shrink-wrapping. Carbon steel banding shall not be
used.
In addition to the standard marking required by the relevant code and/ or standard each
piece shall be marked with the item number. Where it is not possible to place this
information on the individual piece, due to size, tagging or bagging & tagging may be
utilised. Any tags used must be securely attached and be of sufficient strength to minimise
the risk of loss and/ or damage.
Specification for Titanium
UOG-ENG-SPC-45-011 Page 4 of 9 Revision 01
5.0 DOCUMENTATION
Purchase orders may require the submittal of documentation for certain items or commodities
over and above those documentation requirements stated in this specification. Should this
be the case the documents required will be clearly stated in the Purchase Order.
Specification for Titanium
UOG-ENG-SPC-45-011 Page 5 of 9 Revision 01
DATA SHEETS
Material Data Sheet 1 - Flanges, Hubs, Spacers, Spades, Weldolets, Flangeolets, Nippolets and
Sweepolets
Material Data Sheet 2 Fittings
Material Data Sheet 3 Pipe and Bends
Material Data Sheet 4 Sheet and Plate
Specification for Titanium
UOG-ENG-SPC-45-011 Page 6 of 9 Revision 01
MATERIAL DATA SHEET 1
PRODUCT
Flanges, Hubs, Spacers, Spades, Weldolets, Flangeolets, Nippolets and Sweepolets
MANUFACTURING
PROCESS
Forging
SPECIFIC
REQUIREMENTS
Minimum reduction ratio 4:1
Forged bodies, end adapters, extended bonnets or other flanged components shall be forged close to final shape. Forging shall have
achieved at least 2/3 of the change in diameter in a flanged component, thereby limiting machining to 1/3 of the diameter change.
GRADE ASTM B381 Grade F-2 Supplementary Requirement None
DESIGN Non-standard/ special piping components must comply with ASME B31.3 sect. 304. Manufacturers calculations demonstrating compliance
with above requirements shall be made available free of charge to AMEC if requested.
Drawings for weldolets, flangeolets, nippolets, sweepolets and hubs must be submitted for review/ acceptance by AMEC prior to
manufacture.
Burst test data shall be made available for review where applicable (e.g. for flangeolets)
FINISHING Bevelled ends are to be bevelled in accordance with ANSI B16.25
Orifice flanges are to be supplied complete with Jack Screws.
Flange face finish shall be 3.2 - 6.4 m unless specified otherwise.
HEAT TREATMENT The components shall be annealed and air cooled. All parts should be cleaned carefully prior to heating using non-chlorinated solvents or a
detergent wash, followed by a thorough water rinse. Handling following cleaning should be minimized to avoid potential surface
contamination.
CHEMISTRY Chemical composition shall be determined by product analysis. At least two samples shall be tested to determine chemical composition.
Samples shall be taken from the extremes of the product.
HARDNESS TESTING The hardness shall be less than 23 HRC (100HRB or 254 HV10).
TENSILE TESTING Elevated temperature tensile tests shall be carried out at maximum design temperature when wall thickness exceeds 30mm and maximum
design temperature exceeds 150C.
IMPACT TESTING No impact testing is required.
EXTENT OF TESTING One set of tests shall be carried out for each heat and heat treatment load. A test lot shall not exceed 2000 kg for components with as
forged/ HIPed weight 50kg, and 5000kg for components with as forged/ HIPed weight > 50kg.
TEST SAMPLING Samples for production testing shall realistically reflect the properties in the actual components.
Test samples shall be from prolongations on actual component except for die-forged components and tees.
Sacrificial forgings shall be used for die forged components and for tees. Special agreements may be made for die forged components with
as forged weight exceeding 50 kg. Integrated test blocks shall be used for HIP.
Test specimens shall be cut at the 1/4 T location from the surface near the weld preparation area, where T is the thickness of the test
samples. Additional test specimens shall be taken from the crotch region of tees for a second full set of tests. Sketches shall be
established showing type, size and location of test specimens.
NON-DESTRUCTIVE
TESTING
Final inspection shall take place after heat treatment, and final machining.
Visual inspection
Method: ASME V
Extent: 100% of all surfaces
Acceptance criteria: MSS SP55 (No discolouration is acceptable)
Dye penetrant inspection
Method: ASME V after final machining.
Extent: 100% of all accessible surfaces.
Acceptance criteria: ASME VIII, Div. 1, Appendix 8.
Ultrasonic inspection
Method: ASME V
Extent: 3 and over & class 900lb or 65barg design pressure and above: 100% of entire pressure containing surface.
Acceptance criteria: Shear Wave: Any imperfection that produces a signal greater than the reference standard shall be
cause for rejection.
Compression Wave: Multiple indications with an amplitude exceeding 50% of the indication from a 3mm flat
bottom hole, accompanied by a loss of back wall echo exceeding 50% shall be cause for
rejection. Any indication with complete loss in back wall echo shall be cause for rejection.
For thicknesses greater than 30mm the test procedure to be used shall be shown to be
able to detect surface embedded flaws of dimensions no greater than 50mm length by
3mm depth.
SURFACE TREATMENT Annealed surfaces shall be supplied descaled.
DEFECT REPAIRS Weld repairs are not acceptable.
MARKING The component shall be marked to ensure full traceability.
Specification for Titanium
UOG-ENG-SPC-45-011 Page 7 of 9 Revision 01
MATERIAL DATA SHEET 2
PRODUCT
FITTINGS
MANUFACTURING
PROCESS
Forming
GRADE ASTM B363 Grade WPT2 B861/ B862
Grade 2 (Pipe) or B381 Grade F-2
(Forgings)
Supplementary Requirement None
FINISHING Bevelled ends are to be in accordance with ANSI B16.25.
HEAT TREATMENT The components shall be annealed and air cooled. All parts should be cleaned carefully prior to heating using non-chlorinated solvents or
a detergent wash, followed by a thorough water rinse. Handling following cleaning should be minimised to avoid potential surface
contamination.
CHEMISTRY Chemical composition shall be determined by product analysis. At least two samples shall be tested to determine chemical composition.
Samples shall be taken from the extremes of the product.
WELDING Weld procedures for seam welds shall be qualified in accordance with UOG-ENG-SPC-45-001.
HARDNESS TESTING The hardness shall be less than 23 HRC (100HRB or 254 HV10).
TENSILE TESTING Elevated temperature tensile tests shall be carried out at maximum design temperature when wall thickness exceeds 30mm and
maximum design temperature exceeds 150C.
IMPACT TESTING No impact testing is required.
EXTENT OF TESTING One set of tests shall be carried out for each heat and heat treatment load. A test lot shall not exceed 2000 kg.
TEST SAMPLING Samples for production testing shall realistically reflect the properties in the actual components.
Sacrificial fittings shall be used.
Test specimens shall be cut at the 1/4 T location from the surface where T is the thickness of the test samples as heat-treated. Sketches
shall be established showing type, size and location of test samples and extraction of test specimens.
DIMENSIONAL
TOLERANCES
As per ASTM B363
In addition the difference between major and minor outside diameters, with one measurement taken at a weld location, shall not exceed
5%. Excessive cold working or use of heat is not permitted.
NON-DESTRUCTIVE
TESTING
Final inspection shall take place after heat treatment, and final machining.
Visual inspection
Method: ASME V
Extent: 100% of all surfaces
Acceptance criteria: MSS SP55 (No discolouration is acceptable)
Dye penetrant inspection
Method: ASME V after final machining.
Extent: 100% of all accessible surfaces.
Acceptance criteria: ASME VIII, Div. 1, Appendix 8.
Radiographic inspection
Method: ASME VIII UW-51
Extent: 100% of seam weld
Acceptance criteria: ASME VIII, Div. 1 Appendix 7.
Ultrasonic inspection
Method: ASME V with 5% reference notch.
Extent: 100% of fittings thicker than 10mm.
Acceptance criteria: As per ASME VIII Div. 1 Appendix 12 except any imperfection that produces a signal greater than the reference
standard shall be cause for rejection. For thicknesses greater than 30mm the test procedure to be used shall be
shown to be able to detect surface embedded flaws of dimensions no greater than 50mm length by 3mm depth.
SURFACE TREATMENT Annealed surfaces shall be supplied descaled.
DEFECT REPAIRS Weld repair to areas other than welds is not acceptable.
MARKING The component shall be marked to ensure full traceability to melt and heat treatment batch.
Specification for Titanium
UOG-ENG-SPC-45-011 Page 8 of 9 Revision 01
MATERIAL DATA SHEET 3
PRODUCT
PIPE AND BENDS
MANUFACTURING
PROCESS
Seamless or Seam Welded.
Spiral welded pipe shall not be used
GRADE ASTM B861 Grade 2 (seamless) B862 Grade 2 (seam welded) Supplementary Requirement None
FINISHING Pipe with a wall thickness of 6.0mm and below may be supplied with plain ends.
Bevelled ends are to be in accordance with ANSI B16.25.
Pipe lengths shall be Single Random (6m +/- 10%) or Double Random (12m +/- 10%) as agreed with AMEC. Overall order quantity
shall be 0 / + 1 Random Length.
BENDS For Induction and forged bends, test bends shall be manufactured to the smallest radius for each NPS. The mechanical testing required
for the test bend will be subject to agreement between the supplier and AMEC. A drawing showing the location and orientation of all
mechanical test pieces will be submitted to AMEC for approval prior to manufacture of the test bend.
If the results of mechanical testing from the test bend are considered acceptable then no further destructive testing of the production
bends will be required.
HEAT TREATMENT The components shall be annealed and air cooled. All parts should be cleaned carefully prior to heating using non-chlorinated solvents
or a detergent wash, followed by a thorough water rinse. Handling following cleaning should be minimised to avoid potential surface
contamination.
CHEMISTRY Chemical composition shall be determined by product analysis. For seam welded pipe at least two samples shall be tested to determine
chemical composition. Samples shall be taken from the extremes of the product.
WELDING Weld procedures for seam welds shall be qualified in accordance with UOG-ENG-SPC-45-001.
HARDNESS TESTING The hardness shall be less than 23 HRC (100HRB or 254 HV10).
TENSILE TESTING Elevated temperature tensile tests shall be carried out at maximum design temperature when wall thickness exceeds 30mm and
maximum design temperature exceeds 150C.
IMPACT TESTING No impact testing is required.
EXTENT OF TESTING One set of tests shall be carried out for each heat and heat treatment load. A test lot shall not exceed 2000 kg for components with as
forged/ HIPed weight 50 kg, and 5000 kg for components with as forged/ HIPed weight > 50 kg.
TEST SAMPLING Samples for production testing shall realistically reflect the properties in the actual components.
Test samples shall be from prolongations on actual component. Sacrificial forgings shall be used for die forged components.
Test specimens shall be cut at the 1/4 T location from the surface where T is the thickness of the test samples as heat-treated. Sketches
shall be established showing type, size and location of test samples and extraction of test specimens.
DIMENSIONAL TOLERANCES As per ASTM B861 & B862. In addition the difference between major and minor outside diameters at ends and at the middle of each
length, with one measurement taken at a weld location, shall not exceed 5%. Excessive cold working or use of heat to achieve this
tolerance is not permitted.
NON-DESTRUCTIVE
TESTING
Final inspection shall take place after heat treatment, and final machining.
Visual inspection
Method: ASME V
Extent: 100% of all surfaces
Acceptance criteria: MSS SP55 (No discolouration is acceptable)
Dye penetrant inspection
Method: ASME V after final machining.
Extent: 100% of all accessible surfaces after any final forming
Acceptance criteria: ASME VIII, Div. 1, Appendix 8.
Radiographic inspection
Method: ASME VIII UW-51
Extent: 100% of seam welds
Acceptance criteria: ASME VIII, Div. 1 Appendix 7.
Ultrasonic inspection
Method: ASME V with 5% reference notch.
Extent: 100% of fittings thicker than 10mm.
Acceptance criteria: As per ASME VIII Div. 1 Appendix 12 except any imperfection that produces a signal greater than the reference
standard shall be cause for rejection. For thicknesses greater than 30mm the test procedure to be used shall be
shown to be able to detect surface embedded flaws of dimensions no greater than 50mm length by 3mm depth.
SURFACE TREATMENT Annealed surfaces shall be supplied descaled.
DEFECT REPAIRS Weld repair to areas other than welds is not acceptable.
MARKING The component shall be marked to ensure full traceability.
Specification for Titanium
UOG-ENG-SPC-45-011 Page 9 of 9 Revision 01
MATERIAL DATA SHEET 4
PRODUCT
SHEET AND PLATE
MANUFACTURING
PROCESS
Rolling
GRADE ASTM B265 Grade 2 Supplementary Requirement S1
HEAT TREATMENT The components shall be annealed and air cooled. All parts should be cleaned carefully prior to heating using non-chlorinated
solvents or a detergent wash, followed by a thorough water rinse. Handling following cleaning should be minimised to avoid potential
surface contamination.
CHEMISTRY Chemical composition shall be determined by product analysis. At least two samples shall be tested to determine chemical
composition. Samples shall be taken from the extremes of the product.
HARDNESS TESTING The hardness shall be less than 23 HRC (100HRB or 254 HV10).
TENSILE TESTING Elevated temperature tensile tests shall be carried out at maximum design temperature when wall thickness exceeds 30mm and
maximum design temperature exceeds 150C.
IMPACT TESTING No impact testing is required.
EXTENT OF TESTING One set of tests shall be carried out for each heat and heat treatment load. A test lot shall not exceed 2000 kg for components with
weight 50 kg, and 5000 kg for components with weight > 50 kg.
TEST SAMPLING Samples for production testing shall realistically reflect the properties in the actual components.
Test samples shall be from prolongations on actual component.
Test specimens shall be cut at the T location from the surface where T is the thickness of the test samples as heat-treated. Sketches
shall be established showing type, size and location of test samples and extraction of test specimens.
DIMENSIONAL
TOLERANCES
As per ASTM B265
NON-DESTRUCTIVE
TESTING
Final inspection shall take place after heat treatment, and final machining.
Visual inspection
Method: ASME V
Extent: 100% of all surfaces
Acceptance criteria: MSS SP55 (No discolouration is acceptable)
Dye penetrant inspection
Method: ASME V after final machining.
Extent: 100% of all accessible surfaces.
Acceptance criteria: ASME VIII, Div. 1, Appendix 8.
Ultrasonic inspection
Method: S
3
E
4
Extent: 100% of plate thicker than 10mm and all rolled heads.
Acceptance criteria: EN 10160
SURFACE TREATMENT Annealed surfaces shall be supplied descaled.
DEFECT REPAIRS Weld repairs are not acceptable.
MARKING The component shall be marked to ensure full traceability.

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