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J O U R N A L O F M A T E R I A L S S C I E N C E 4 0 (2 0 0 5 ) 5 3 4 1 –5 3 4 7
This paper describes the bundle strengths of PET filaments from a statistical point of view.
A bundle is an arrangement of a number of filaments. We applied the weakest-link theory
and probabilistic load-sharing rules to estimate the bundle strength from the breaking
strength data of PET filaments. We analyzed the breaking behavior of 12 filament bundles
according to their length and number of filaments and compared the breaking behavior of
a prepared specimen yarn with that of a commercial PET filament yarn. The breaking
strength of the PET filaments, which we tested using a MANTIS R
tester, was compared with
that of the actual yarn. We compared the actual tested values obtained by INSTRON R
with
R
the expected values, which we calculated from the MANTIS data by using Peirce’s theory
and Knox’s hazard function. The key effects that determine the actual random breakage
behavior of a bundle include not only the load-sharing rules in the constituent filaments but
also the slippage and friction between adjacent filaments, the appearance of which we
distinguished especially in the bundle consisting of a large number of filaments and in
small-denier filaments. The PET filaments were better approximated when using the
Peirce’s weakest-link theory than they were by Knox’s hazard function. In a series-parallel
model, we found that the number of parallel filaments and their load-sharing behavior had
larger effects on the bundle strength than did the weakest-link effects of continuous
elements. C 2005 Springer Science + Business Media, Inc.
2. Experimental
2.1. Materials
To study the random breakage behavior of bundles, we
prepared bundles from a different number of filaments
of 262 denier(d)/12 filament(f) PET yarn provided by
Kanebo Co. Ltd. Filaments having large denier could
be separated readily from the yarn. All filament yarns
were drawn from relatively restricted sections of the
package, to avoid any large effects that might be en-
countered through the packages. Single filaments were
separated from the raw filament yarn and artificially Figure 1 The series-parallel combination model of bundle strength: (a)
bundle and filaments; (b) series-parallel combination.
prepared into 1–12-filament bundles. We considered
bundles to be parallel arrangements of component fil-
aments that might behave independently from one an-
the breaking strength of single filaments and bundles,
other and filaments to be continuous chains of com-
we prepared four partially drawn yarns (DPY) that were
ponents of unit length. We selected lengths of 10, 20,
75d/36f and 50d/24f PET yarns. We performed single-
30, 40, 60, and 80 mm from twelve filament bundles.
filament tensile tests using a MANTIS R
single-fiber
For the tensile tests of the bundles that were arranged
tensile tester. The information achieved was stored in a
in a series-parallel combination of filaments, we glued
computer database for subsequent analysis. The tensile
the specimens to a paper tab using a polyamide-epoxy
tests of bundles were performed using an INSTRON R
resin. We considered N-filament bundles to be an ar-
tester (Table I).
rangement of component filaments of PET yarn, as
illustrated in Fig. 1, which exists in a continuous chain
of components of unit length. We made the following
basic assumptions for the series-parallel combination 2.2. Measurements
model: 2.2.1. Tensile test of N-filament bundle
The tensile tests of N-filament bundles were performed
on an INSTRON R
(model 4468, UK) tensile tester by
1. No inter-filament friction exists in a bundle.
using a 100-N load cell. Lengths of 10, 20, 30, 40, 60,
2. All filaments within a clamped bundle have equal
and 80 mm were selected from each of twelve filament
length.
bundles, i.e., from a single-filament bundle to a twelve-
3. Filament axes are parallel to the extension and
filament bundle (Table I). The specimens were then
direction when the filament was clamped between the
mounted in clamps and tested at a cross-head speed of
upper and lower gripper.
60 mm/min. We performed a total of 720 tensile tests,
4. Filaments within a bundle are ideally clamped,
which we repeated 20 times for twelve N-bundles of
permitting no filament slippage or damage at clamping
each gauge length. The data obtained from each test
points as a result of load concentration.
were treated as a set of breaking strengths and breaking
In a well-combed and brushed filament bundle, as-
sumptions 1 and 3 should hold; assumption 2 is satisfied TABLE I The classification of PET samples
when bundles are glued at the same tension; assumption
Sample name Denier/filament Company Instrument
4 should hold when a default specimen is checked after
testing, which is a safeguard against the usual experi- PET-A 262/12 Kanebo InstronR
mental errors that stem from the flowed clamping con- PET-B 75/36 Kolon
Instron R & MantisR
ditions. These assumptions provide a great simplifica- PET-C 75/36 Hyosung InstronR
& MantisR
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POLYMER FIBRES 2004
strains and were compared with those sample properties yarns provided by Kolon Co. and Hyosung Co., Ko-
from other sets for filaments of the same PET yarns. rea. Lengths of 10, 20, 30, 40, 60, and 80 mm were
selected from each PET yarn. Paper tabs were glued
2.2.2. Tensile testing of a single filament to the ends of the specimen using a polyamide-epoxy
Single-filament tensile tests were performed using a resin. The prepared specimen was then tested on an
MANTIS R
single-fiber tensile tester (Zellweger Uster INSTRON R
(model 4468, UK) tensile tester by using
Inc.) having a 3.175-mm gauge length at a 60 mm/min a 10-N load cell. The specimen were then mounted in
extension rate, as given in Table I. We performed a to- clamps and tested at a cross-head speed of 60 mm/min.
tal of 225 or 150 single-filament tests, which were re- Data obtained from each test were treated as a set and
peated three times for each filament, on the MANTIS R
the breaking strengths, breaking elongations, and mod-
for each filament type. The information was stored in uli were compared with those sample properties ob-
a computer database for subsequent analysis. We ac- tained from the data obtained using the MANTIS R
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POLYMER FIBRES 2004
0.8 0.8
Load (kgf)
Load (kgf)
0.6 0.6
0.4 0.4
0.2 0.2
0.0 0.0
0 1 2 3 4 5 6 7 8 9 10 11 12 0 1 2 3 4 5
Extension (mm) Extension (mm)
1.2
1.2 60mm 80mm
1.0
1.0
0.8
Load (kgf)
Load (kgf)
0.8
0.6 0.6
0.4 0.4
0.2 0.2
0.0 0.0
0 5 10 15 0 5 10 15 20 25
Extension (mm) Extension (mm)
Figure 3 The load-extension curves of the 1–12-filament bundles for the 262d/12f PET yarn at different gauge length.
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POLYMER FIBRES 2004
0. 16
at maximum load 1. 00
(a)
0. 99
0. 12 0. 97
0. 96
0. 10 0. 95
0. 94
1f 2f 3f 4f
0. 08 5f 6f 7f 8f
0. 93
9f 10 f 11 f 12 f
0. 92
0. 06 20 30 40 50 60 70 80
0 2 4 6 8 10 12
Gauge length(mm)
Number of Filament
(a)
0. 11
at breaking load 1200
0. 10
0. 08 800
0. 07
600
10 mm
0. 06
400
20 mm
0. 05 30 mm
40 mm
200 60 mm
0. 04
80 mm
0. 03 0
0 2 4 6 8 10 12 0 2 4 6 8 10 12
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POLYMER FIBRES 2004
12 390
The tested DPY1
The expected I DPY3
360
The expected II DPY8
330
300
270
4
240
2 210
180
0
0 10 20 30 40 50 60 70 80 0 10 20 30 40 50 60 70 80 90
Gauge Length (mm) Gauge Length (mm)
(a) (a)
12
The tested DP Y1
The expected I 10.0
DP Y3
Breaking Strength (gf )
10 The expected II DP Y8
9.5 DP Y9
Efficiency (gf )
8
9.0
4
8.5
2
8.0
0 7.5
0 10 20 30 40 50 60 70 80 0 10 20 30 40 50 60 70 80 90
Gauge Length (mm) Gauge Length (mm)
(b) (b)
Figure 8 Comparisons between the tested values obtained using Figure 9 The effects that length and bundle size have on the break-
INSTRON R
and the expected values obtained using MANTIS
R
for ing strength of commercial PET yarn: (a) the breaking load; (b) the
the 50d/24f PET single filaments: (a) PET-D; (b) PET-E. efficiency.
The results are presented in Figs 7 and 8, which indi- pared these results with those obtained using a com-
cate that the expected values obtained using Peirce’s mercial PET filament yarn. We compared the breaking
theory are better approximations of the tested values strengths determined by MANTIS R
tests with those
than are those predicted by the hazard function. The
R
from INSTRON tests. In addition, we evaluated the
expected values obtained using Peirce’s theory, how- strength of both filaments and bundles by using the
ever, also present a number of differences in relation MINITAB statistic package. The normality tests for
to the tested plots. Consequently, we conclude that the PET filaments indicated that commercial PET single
PET filaments followed a normal distribution because filaments and prepared N-filament bundles followed
Peirce assumed the breaking strength of a filament to normal distributions and that the bundle strength could
be normally distributed. Fig. 9 illustrates the effects be predicted from the distribution function of each sin-
that the length and bundle size have on the breaking gle filament of PET yarn. The results of N-filament
strength of commercial PET yarn. Fig. 9a indicates bundles are explained by the weakest-link effect and the
that the breaking load of the PET filaments decreased bundle size effect of the N-filament bundles. That is to
as the gauge length increased, i.e., the weakest link say, although when the length of a specimen increases,
theory. Fig. 9b displays a plot of the efficiency of com- the probability of the existence of defects should also
mercial PET filament yarn. For PET-B, PET-C, PET-E increase, but we found that the major effects that deter-
was appeared the similar scale with the exception of mining the bundle strength are the number of filaments
PET-D. Despite having the same denier, the filaments and the load sharing behavior of each single filament.
displayed different behavior. This finding indicates that In a comparison between the expected and tested val-
the difference is due to the load sharing breakage. The ues in the PET filaments and bundles, Peirce’s theory
load sharing behavior on the random breakage of PET provided a better fit than did a simple hazard function.
bundles is very complicated because of the effects of Consequently, in both series and parallel effects, we
slippage and friction between adjacent filaments; these found that the breaking strength of a bundle was in-
effects are more significant in small-denier filament fluenced by the length effect (the weakest link theory),
bundles. but the load-sharing behavior of the component fila-
ments in a bundle had a greater effect on the bundle
strength. We implicate that the load sharing behavior
4. Conclusions has an effect on the random breakage of a polyester
In this study, we prepared N-filament bundles from bundle because slippage and friction between adjacent
262d/12f PET filament yarn to investigate the behav- filaments have more significant effects in small-denier
ior of the random breakage of a bundle; we com- filament bundles. For further study, it is worthwhile
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POLYMER FIBRES 2004
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