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Magnetic anisotropy works as a petrofabric tool because individual grains of most minerals are magnetically anisotropic, i.e. Easier to magnetize. AMS and related techniques are now routinely applied to characterizing fabrics in a wide variety of geological materials.
Magnetic anisotropy works as a petrofabric tool because individual grains of most minerals are magnetically anisotropic, i.e. Easier to magnetize. AMS and related techniques are now routinely applied to characterizing fabrics in a wide variety of geological materials.
Magnetic anisotropy works as a petrofabric tool because individual grains of most minerals are magnetically anisotropic, i.e. Easier to magnetize. AMS and related techniques are now routinely applied to characterizing fabrics in a wide variety of geological materials.
01 2004; v. 238; p. 1-7 Geological Society, London, Special Publications
F. Martn-Hernndez, C. M. Lneburg, C. Aubourg and M. Jackson
Magnetic fabric: methods and applications an introduction
Geological Society, London, Special Publications
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Downloaded by on 4 December 2007 London 2004 Geological Society of Magnetic fabric: methods and appl i cat i ons- an introduction F. MARTI N- HERNANDEZ 1, C. M. LONEBURG 2, C. AUBOURG 3 & M. J ACKS ON 4 1paleomagnetic Laboratory 'Fort Hoofddijk', Faculty of Geosciences, Utrecht University, 3584 CD Utrecht, The Netherlands 2Department of Geology and Geophysics, University of New Orleans, 2000 Lake Shore Drive, New Orleans, LA 70148, USA 3Laboratoire de Tectonique, UMR 7072, UniversitO de Cergy-Pontoise, 95031, Cergy Cedes, France 4Institute for Rock Magnetism, University of Minnesota, Minneapolis MN 55455, USA Fifty years have now passed since Graham (1954) published his seminal paper advocating the use of anisotropy of magnetic susceptibility (AMS) as a rapid and sensitive petrofabric tool. During these five decades, Graham' s ' under- exploited' method has become standard, and AMS and related techniques are now routinely applied to characterizing fabrics in a wide variety of geological materials (e.g. the GEOREF data- base lists over 500 journal publications with ' magnetic anisotropy' as keywords). Magnetic anisotropy works as a petrofabric tool because individual grains of most minerals are magnetically anisotropic, i.e. easier to mag- netize in certain orientations, which are governed primarily by crystallography and/or grain shape. Magnetic anisotropy at the bulk rock scale results from the preferred crystallographic orien- tation (PCO) and/or preferred dimensional orientation (PDO) of anisotropic mineral grains. AMS can also result from magnetostatic interactions among closely spaced, strongly mag- netic grains that are heterogeneously distributed in a matrix of more weakly magnetic minerals. In either case, magnetic anisotropy is directly related to some aspects of rock fabric, and thus it provides a quick, simple and effective charac- terization tool, even though the relationship between magnetic fabric and petrofabric is quite complex in detail. The present collection of papers originated, in part, at a special session on magnetic fabrics at the Joint Assembly of the EGS-AGU-EUG (April 2003) in Nice, which highlighted recent methodological advances, theoretical and experi- mental studies, and characterization of flow and deformation fabrics in rocks and sediments. A similar session at the AGU Fall Meeting (December 2003) in San Francisco underscored the continuing breadth of interest in magnetic fabric research, and suggested that the time was ripe for a comprehensive critical assessment of the field on this golden anniversary of Graham' s influential publication. It is our goal in this volume to present a view of the current state of the art in magnetic fabric analysis, from the physical foundations to the geological applica- tions, and to illustrate as well some of the important limitations, unresolved problems and directions for future research. The first observations of AMS in natural samples were presented before 1954 (e.g. Ising 1943). The early works focused on establishing correlations between the AMS principal direc- tions and the structural features in sediments (Rees 1961, 1965; Graham 1966), igneous and metamorphic rocks (Stacey 1960; Stacey et al. 1960; Khan 1962; Stone 1962). Contemporary advances in palaeomagnetism led to a need for methods to assess the fidelity of the stable rema- nence, increasing the interest in AMS and other techniques for measuring magnetic anisotropy (Fuller 1960, 1963; Rees 1961). The technique was refined with the appearance of rigorous measurement schemes (Girdler 1961) and mathe- matical theories to explain the origin of AMS (Nagata 1961; Stacey 1963; Uyeda et al. 1963; Bathal 1971). The ultimate goals of magnetic fabric research in the geosciences have remained essentially unchanged since these early studies: determining flow/emplacement directions in sediments, intru- sive and extrusive rocks; establishing principal orientations (as well as estimating magnitudes) of finite or incremental strains; and ascertaining the extent of possible deviations of NRM vectors from the palaeofield orientation due to aniso- tropic acquisition and/or subsequent deforma- tion. With these consistent goals, the field has evolved primarily in its recognition of the From: MARTiN-HERNANDEZ, F., LONEBURG, C. M., AUBOURG, C. JACKSON, M. (eds) 2004. Magnetic Fabric: Methods and Applications. Geological Society, London, Special Publications, 238, 1-7. 0305-8719/04/$15.00 9 The Geological Society of London 2004. 2 F. MARTiN-HERNANDEZ ET AL. complexity of natural magnetic fabrics and in the development of increasingly sophisticated methods for extracting meaningful information from them. This evolution may be traced through a series of excellent reviews (Bhathal 1971; Hrouda 1982; MacDonal d & Ellwood 1987; Rochette et al. 1992; Tarling & Hrouda 1993; Kodama 1995; Borradaile & Henry 1997). Magnet i c fabric characteri zati on methods and mi neral sources The first measurements of AMS were performed using low-field torque magnetometers (Ising 1943; Granar 1958; Stone 1962; King & Rees 1966). The crystalline anisotropy can also be determined by means of high-field torque magne- tometry in natural samples (Stacey 1960; Bane- rjee & Stacey 1967) and ferromagnetic single crystals such as pyrrhotite (Mikami et al. 1959; Bin & Pauthenet 1963; Sato et al. 1964) or hema- tite (Townsend 1916; Townsend 1920; Lin 1959). Measurements are tedious and time-consuming and for this reason an alternative was found, with measurements based on astatic magnet- ometers (Johnson & Steiner 1937; Collinson 1967; Deutsch et al. 1967; Roy 1971; Fujiwara & Yoshida 1981) or spinner magnetometers (Jeli- nek 1966; Noltimier 1971; Schmidt et al. 1988). The technique became a standard measurement with the appearance of a.c. susceptibility bridges (Fuller 1960; Girdler 1961; Graham 1964; Jelinek 1973), which are relatively fast, inexpensive, simple to use and very precise (Pokorny et aL, this volume). Parallel to the development of the instrumentation, the measurement technique became more refined and additional work helped to evaluate accurately the magnetic sus- ceptibility tensor and analytical uncertainty, for individual specimens and for groups of samples (Owens 2000a; Owens 2000b; Borradaile 2003 and references therein). The statistical treatment of the AMS data requires analysis of the shape of the ellipsoid, degree of anisotropy and their correlation with bulk properties as the magnetic susceptibility (Nakamura & Borradaile, this volume). The AMS measures the anisotropy of all minerals present in the samples, weighted according to their specific susceptibilities (which vary by roughly six orders of magnitude), con- centrations, grain-scale anisotropies (controlled by crystallography, grain shape and/or stress) and degrees of preferred orientation. In most rocks and sediments, AMS is mainly due to the heavily weighted trace ferromagnetic phases, and often it reflects a single dominant event or process. In such favourable cases it is possible to quantify the orientation distribution of the magnetic minerals (Jezek & Hrouda, this volume). But in many cases the AMS has been proved to consist of multiple superposed compo- nents, carried by different mixtures of ferro-, para- and even diamagnetic minerals (Hrouda; Just et al. , this volume), with different preferred orientations imposed by different mechanisms (e.g. Daly 1967). It has become necessary, in order to unravel the history of deformation and alteration of natural samples, to separate these individual magnetic subfabrics. Several tech- niques are now available for this purpose, based on measurements at different temperatures (Richter & van der Pluijm 1994; Hrouda et al. 1997; Lfineburg et al. 1999; Par6s & van der Pluijm 2002), measurements at different fields (Hrouda & Jelinek 1990; Martin-Hernfindez & Hirt 2001; Kelso et al. 2002; Martin-Hern/mdez & Hirt 2004) or a combination (Rochette & Fillion 1988; Richter & van der Pluijm 1994). Comparison between magnetic fabrics or sub- fabrics and the results of other techniques such as neutron texture goniometry (Chadima et al. , this volume), acoustic waves (Louis et al. 2003), or X-ray texture goniometry (Debacker et aL, Hirt et aL, this volume) allow a better under- standing of the nature, origin and significance of measured magnetic fabrics. The separation of superposed magnetic sub- fabrics can also be achieved through measure- ments of the anisotropy of magnetic remanence (AMR) alone (reviewed by Potter, this volume). The AMR is a measurement of the anisotropy of ferromagnetic minerals that can be evaluated using different types of magnetization, including anhysteretic remanence (ARM) (McCabe et al. 1985; Jackson et al. 1988; Jackson 1991), iso- thermal remanence (IRM) (Daly & Zinsser 1973; Stephenson et al. 1986; Borradaile & Dehls 1993; Jelinek 1993), thermoremanence (TRM) (Cogn~ 1987) and gyroremanence (GRM) (Stephenson 1981). In some cases the ferromagnetic mineral anisotropy can be isolated without recourse to laborious AMR measure- ments, by analysing the variation of AMS with mean susceptibility (e.g. Henry & Daly 1983; Hamilton et aL, this volume). The results from AMS and AMR measurements can be combined in order to effectively compute the different sub- fabrics (Hrouda 2002). One as-yet poorly under- stood aspect of AMR is its sensitivity to magnetostatic interactions between neighbour- ing grains (Muxworthy & Williams, this volume). In samples with weak anisotropy, it has in some cases proven effective to ' enhance' the ferro- magnetic fabric (i.e. increase the susceptibility INTRODUCTION 3 and/or its anisotropy) by thermal treatment of the samples. In many cases the new ferromagnetic phases that appear while heating mimic the pre- existing fabric of the rocks (Dunlop 1974; Henry et al. 2003; de Wall & Warr, this volume). From sedi mentary fabrics to tectonic fabrics in sedi mentary rocks In the five decades since the seminal paper of Graham (1954), numerous studies have docu- mented a general consistency between magnetic fabric and petrofabric in sedimentary rocks (see Borradaile & Jackson, this volume). This con- sistency is essentially qual i t at i v e , i.e. a parallelism between magnetic fabric axes and sedimentary or tectonic structures or finite strain axes. Addition- ally, the shape of the magnetic fabric ellipsoid (oblate, triaxial or prolate) often generally corresponds in a qualitative way with the shape of the petrofabric ellipsoid. However, few successful q u a n t i t a t i v e correlations (involving direct correlation of axial ratios) have been docu- mented. This is due in essence to the variable intrinsic properties of magnetic carriers, the vari- able proportions of different carriers in different samples, and the bulk (non-mineral-specific) sensitivity of magnetic fabric. In sedimentary rocks, the magnetic foliation results from a combination of depositional pro- cesses and diagenetic compaction. The magnetic lineation can result from sedimentary currents in marine conditions or wind in continental con- dition (see Matasova & Kazansky, this volume). When subjected to strain, the magnetic fabric of sedimentary rocks rapidly starts to record an imprint (see Parks, this volume). Studies of the palaeomagnetic remanence and AMS can help in the understanding of the magnetic fabric acquisition process at early stages of deformation (Larrasoafia e t al . , this volume). The magnetic lineation carries the first imprint of shortening or extension. This imprint seems to resist sub- sequent deformation and can behave therefore as a passive marker. The magnetic foliation is more resistant to early strain. However, the development of magnetic foliation strongly obli- que to bedding has been documented in clastic rocks and carbonates during horizontal shorten- ing (the so called layer parallel shortening). Inter- estingly, this tectonic magnetic foliation is cryptic and it is not necessarily accompanied by its macroscopic equivalent plane in the field (Sun et al. 1993). In low-grade metamorphic rocks (e.g. Ander- son & Morris; Aubourg et aL; Debacker et aL, this volume), the consistency between magnetic fabric and petrofabric is observed either at the scale of the macroscopic elements (cleavage, lineation) or thin section. Magnetic foliation, i f carried by phyllosilicates, is closely parallel to macroscopic cleavage. Magnetic lineation is often the result of microfolding of phyllosilicates and therefore reflects the fold axis or intersection lineation (Hirt e t al . , this volume). The plunge- attitude of magnetic lineation (strike-parallel to down-dip) with respect to magnetic foliation can be a useful indicator of the degree of defor- mation (Aubourg e t aL this volume). In flysch- derived metamorphic rocks, Debacker e t al. (this volume) suggest that a sedimentary linea- tion carried by coarse ferromagnetic grains is preserved. While magnetic fabric is generally very well defined in metamorphic rocks, the fre- quent mixture of several ferromagnetic phases (pyrrhotite, magnetite, hematite) interplaying with paramagnetic phyllosilicates is the cause of complex magnetic fabric (Aubourg et al., this volume), rendering difficult a quantitative char- acterization of strain. In addition, different deformation mechanisms on the microscale are domi nant with increasing strain and strongly influence magnetic - and petrofabric - ellipsoids, hampering correlations with finite strain (Hirt e t aL, this volume) or macroscopic structures. However, examples exist where, despite a com- plex tectonic history, the magnetic fabric is rather consistent with macroscopic structures (Ka, dzialko-Hofmokl e t al . , this volume). Pl utoni c & igneous fabrics Magnetic fabric analysis is a powerful approach for studying granites because it provides mag- matic to strain patterns at a regional scale, in rocks where fabric is difficult to characterize (e.g. Bouchez 2002). We present in this volume a view of the current state of the art in magnetic fabric applications, together with other tech- niques (Gil-Imaz & Barbero-Gonz~ilez, L6pez de Luchi e t al., Pueyo e t al., this volume). Similarly to extensive studies performed in granites, there is a growing interest in magnetic fabric studies of igneous rocks, which allow definition at differ- ent scales of the direction and the sense of magma flows (trapp, dyke swarm). Khan (1962) presented the first interpretation of AMS in igneous rocks and dykes and the technique has been used since then in order to understand lava flow and emplacement mechanism of igneous rocks (Hargraves e t a / . 1991; Tauxe et al. 1998). Cafi6n-Tapia (this volume) provides a historical review of AMS applications in volcanic rocks. 4 F. MARTIN-HERN,~NDEZ E T A L . The i nt erpret at i on of AMS analysis in igneous rocks is based on the devel opment of the pre- ferred or i ent at i on of magnet i c particles duri ng the flow of mat eri al (Cafi6n-Tapia & Chfivez- Alvarez, this volume). Ferromagnet i c minerals, in part i cul ar t i t anomagnet i t es, are the mai n carriers of AMS in volcanic rocks, and due to the high intrinsic susceptibility of t i t anomagne- tite with respect to paramagnet i c phases, it typi- cally overwhelms the signal from ot her sources (Tarling & Hr ouda 1993; Raposo 1997). Optical observat i ons of the mi neral fabrics in lava flows have revealed t hat the mi neral fabric of paramag- netic phases such as plagioclase correlates with the principal directions given by AMS as well (Archanj o e t al . 2002; Ferr~ e t al . 2002; Arehanjo & Launeau, this volume). The met hodol ogy to retrieve the magma flow has changed consider- abl y duri ng the last decade (Cafi6n-Tapia, this volume). Fr om the early i nt erpret at i on of mag- netic l i neat i on parallel to the flow (Ellwood 1978), it appears t hat i mbri cat i on of magnetic lineations provides in addi t i on the sense of flow (Kni ght & Wal ker 1988). To account for the large occurrence of inverse magnet i c fabrics in volcanic rocks, Geoffroy e t al . (2002) proposed to use in addi t i on t he i mbri cat i on of magnet i c fol i at i on to retrieve the sense of flow. Addi t i on- ally to the empl acement mechani sm, the combi- nat i on of AMS studies and pal aeomagnet i c directions provi de i nf or mat i on on the post- empl acement def or mat i on (Petronis e t al . , this volume). O u t l o o k The papers in this volume collectively por t r ay the current state of research on magnetic fabric analysis, its physical basis and its geological applications. In practice, the terms magnetic fabric and AMS remai n nearly synonymous. AMS cont i nues to be by far the most widely applied magnetic met hod for characterizing fabrics because AMS measurement s are fast, nondest ruct i ve and extremely precise, enabl i ng regional mappi ng of sedi ment ary features, strain and magma flow in al most all rock types. We ant i ci pat e t hat this will cont i nue to be the case in the comi ng decades, but t hat more comprehensi ve met hods, including field- and t emperat ure-dependent measurement s and remanence ani sot ropy at higher applied fields, will play an ever-increasing role in magnet i c fabric charact eri zat i on. Toget her with growing i nt egrat i on of magnet i c and nonmagnet i c approaches (e.g. neut r on and X-ray goni omet ry, Scanni ng El ect ron Mi croscopy with EBSD), these more detailed approaches will enabl e more accurate identification and characteriza- t i on of the separate component s of composi t e fabrics, their mi neral sources and geological significance. On the geophysical side, two of the i mpor t ant research frontiers where we ant i ci pat e maj or advances concern inverse fabrics and magnet o- static interactions. Inverse magnet i c fabrics involve a t ransposi t i on or per mut at i on of princi- pal axes with respect to pet rofabri c (e.g. magnetic l i neat i on normal to bedding in undeformed sedi- ments), arising from the magnet ocryst al l i ne and magnet ost at i c peculiarities of a relatively small number of magnet i c phases (e.g. si ngl e-domai n magnetite). When ' expected' ori ent at i ons are unknown, inverse magnet i c fabrics cannot be recognized a p r i o r i and they provi de misleading i ndi cat ors of petrofabric. Yet it is precisely when ' expected' ori ent at i ons are unknown t hat magnetic fabrics have the greatest pot ent i al i mport ance, and more reliable met hods of estab- lishing mi neral PDOs and PCOs from a combi na- t i on of remanence ani sot ropy, t emperat ure- and field-dependent AMS measurement s will be of considerable value. Similarly, i nt eract i on aniso- t ropy (also known as ' di st ri but i on ani sot ropy' ) is generally underst ood t heoret i cal l y and experi- mentally, but remains a significant compl i cat i ng fact or in some geological applications. An i mpor- t ant challenge for the future will be the develop- ment of met hods for part i t i oni ng the AMS of nat ural materials i nt o component s related to PCO, PDO and interactions, The scope of magnet i c fabric applications, which already comprises all nat ur al materials, cannot expand, but we may expect a cont i nui ng shift from qual i t at i ve to more quant i t at i ve appli- cations. We would like to thank all the people who have con- tributed to this volume, authors, reviewers and collea- gues. The following people were asked to review one or more of the submitted papers, they are all kindly acknowledged: I. Abad, C. Archanjo, J. Bascou, J. Becker, K. Benn, G. J. Borradaile, J. P. Callot, E. Cafi6n-Tapia, D. Czeck, L. Geoffroy, H. de Wall, B. B. Ellwood, E. C. FerrY, M. Fuller, B. Henry, A. M. Hirt, J. Hodych, B. Housen, M. Hounslow, F. Hrouda, J. Jesek, P. Kelso, K. Kodama, F. Lagroix, P. Launeau, W. Lowrie, M. Mattei, J. M. Miranda, B. Moskowitz, M. Ort, Averbuch, J. 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