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COURSE OUTCOMES
CO
RECOGNIZE
all
the
piping
and
instrumentation symbols, CHOOSE suitable
symbols and DEVELOP the piping systems and
the
specification
of
the
process
instrumentation, equipment, piping, valves,
fittings; and their arrangement in P&ID for the
bioprocess plant design.
OUTLINES
TYPES of piping and
instrumentation symbols.
How to CHOOSE the suitable
symbols in control system?
How to DEVELOP the piping
systems and the specification of the
process instrumentation,
equipment, piping, valves, fittings.
The ARRANGEMENT in P&ID
for the bioprocess plant design.
Block Flow
Diagram (BFD)
Process Flow
Diagram (PFD)
PROCESS
DIAGRAMS
Process equipments
symbol and
numbering
Piping and
Instrumentation
Diagram (P&ID)
Block Flow
Diagram (BFD)
Process Flow
Diagram (PFD)
PROCESS
DIAGRAMS
Process equipments
symbol and
numbering
Piping and
Instrumentation
Diagram (P&ID)
Toluene, C7H8
10,000 kg/hr
Reactor
Hydrogen H2
820 kg/hr
C6H6
Gas Separator
Benzene, C6H6
8,210 kg/hr
CH4
C7H8
Mixed Liquid
75% Conversion of
Toluene
Reaction : C7H8 + H2
C6H6 + CH4
Example 2:
Production of Ethane from Ethanol
Ethanol is feed to continuous reactor with presence of Acid Sulphuric catalyzer
to produce ethylene. Distillation process then will be applied to separate
ethylene-H2O mixture. Ethylene as a top product is then condensate with
condenser to perform liquid ethylene. Hydrogenation of ethylene applies in
another reactor with presence of Nickel catalyzer to produce ethane as a final
product. Develop BFD for these processes.
CH3CH2OH
CH2=CH2 + H2
H2SO4
Ni
Answer:
CH2=CH2 + H2O
CH3CH3
Hot water
out
Ethylene,
CH2CH2 (g)
Ethylene liq.
CH2CH2 (l)
Ethanol,
C2H5OH
H2SO4
Reactor 1
CH2CH2
H2 O
Cold
water in
Distillation
column
H2O
Reactor 2
Hydrogen,
H2 Ni
Ethane,
CH3CH3
Example 3:
Ammonia-air mixture is feed to the bottom stream of an absorber with flow rate of 10L/min.
Water then feed to the upper stream of the same absorber with desired flow rate of 5L/min.
There are two outputs from the absorber where upper stream is insoluble NH3 and bottom
stream is NH3-Water mixture. This NH3-water mixture then feed up to a batch distillation
column. The column produces ammonia gas as a top product which this product then will be
condensate with a condenser to produce liquid ammonia. Develop Block Flow Diagram (BFD)
for this process.
Hot water
out
Insoluble
ammonia
Water 5 L/min
Ammonia
liquid
Ammonia gas
Condenser
Batch
Distillation
Absorber
Cold water
in
Ammonia-water mixture
Ammonia-air mixture 10 L/min
Block Flow
Diagram (BFD)
Process Flow
Diagram (PFD)
PROCESS
DIAGRAMS
Process equipments
symbol and
numbering
Piping and
Instrumentation
Diagram (P&ID)
2. Utility
Streams
1. Major Pieces Of
Equipment
PFD
4. Basic Control
Loops
3. Process Flow
Streams
2. Utility
Streams
1. Major Pieces Of
Equipment
PFD
4. Basic Control
Loops
3. Process Flow
Streams
PFD will contains the following information:1. All major pieces of equipment (descriptive
name, unique equipment no.), pumps and valves.
2. All the utility streams supplied to major
equipments such as steam lines, compressed air
lines, electricity, etc.
Description
Heat exchanger
H2O
Water cooler
Steam heater
Cooling coil
Description
Heater coil
Centrifugal pump
Pressure gauge
Name
Description
Stripper
A
separator
unit
used
commonly to liquid mixture
into gas phase.
Absorber
A
separator unit used
commonly to extract mixture
gas into liquid phase.
Name
Description
Distillation
A
separator
unit
used
commonly to crack liquid
contains
miscellaneous
component fractions.
column
or
Liquid mixer
Name
Description
Reaction
chamber
Horizontal tank
or cylinder
Name
Description
Boiler
Centrifuge
Name
Gate Valve
Globe Valve
Ball Valve
Check Valve
Butterfly Valve
Name
Relief Valve
Needle Valve
3-Way Valve
Angle Valve
Butterfly Valve
E XAMPLE 4
Production of Ethane from Ethanol
Ethanol is feed to continuous reactor with presence of Acid Sulphuric catalyzer to produce ethylene.
Distillation process then will be applied to separate ethylene-H2O mixture. Ethylene as a top product
is then condensate with condenser to perform liquid ethylene. Hydrogenation of ethylene applies in
another reactor with presence of Nickel catalyzer to produce ethane as a final product. Develop PFD
for these processes.
H2SO4
CH3CH2OH
CH2=CH2 + H2
CH2=CH2 + H2O
CH3CH3
Ni
R-100
P-100
T-100
E-100
P-101
R-101
Reactor
Pump
Distillation Column
Condenser
Pump
Reactor
Ethylene
E-100
V-104
Ethylene
liq.
Cold water in
CV-100
Ethanol
V-100
H2SO4
V-101
V-103
R-100
P-100
T-100
V-106
CV-101
V-105
Hydrogen
V-102
V-107
H2O
Ni
P-101
R-101
Ethane
E XAMPLE 5
Ammonia-air mixture is feed to the bottom stream of an absorber with flow rate of
10L/min. Water then feed to the upper stream of the same absorber with desired
flow rate of 5L/min. There are two outputs from the absorber where upper stream
is insoluble NH3 and bottom stream is NH3-Water mixture. This NH3-water mixture
then feed up to a batch distillation column. The column produces ammonia gas as a
top product which this product then will be condensate with a condenser to
produce liquid ammonia. Develop Process Flow Diagram (PFD) for this process.
T-100
T-101
E-100
Absorber Column
Condenser
Insoluble ammonia
gas
Ammonia liquid
Water 5 L/min
Cold water in
Ammonia-air
mixture 10 L/min
Ammonia-water mixture
Supplemental Information
Hot water
out
Ethylene
Ethylene
Cold
water in
Ethylene liq.
Ethanol
Cold
water in
Ethanol
H2SO4
Hydrogen
Ni
H2O
Ethane
H2SO4
Ethylene liq.
Hydrogen
Ni
H2O
P-100 A
P-100 A/B
P-100 B
In PFD
In Real Plant
Ethane
2. Utility
Streams
1. Major Pieces Of
Equipment
PFD
4. Basic Control
Loops
3. Process Flow
Streams
PFD will contains the following information:All process flow streams: identification by a
number, process condition, chemical composition.
Yes
No
No
E XAMPLE 4 - CONT
R-100
P-100
T-100
E-100
P-101
R-101
Reactor
Pump
Distillation Column
Condenser
Pump
Reactor
Hot water
out
Ethylene
Ethylene liq.
E-100
6
V-104
T-100
Cold water
in
CV-101
V-106
CV-100
V-105
Ethanol
1
H2SO4
V-101
V-100
5
V-102
4
V-103
R-100
V-107
9
R-101
8
7
P-100
Hydrogen
Ni
Ethane
10
H2O
P-101
24
8
6
9
7
Pressure
10.3
Mass Flowrate
108
Molar Flowrate
10
600
24
12
11
4
24
13
Gas Flowrate
Liquid
Flowrate
E XAMPLE 4 - CONT
R-100
P-100
T-100
E-100
P-101
R-101
Reactor
Pump
Distillation Column
Condenser
Pump
Reactor
Hot water
out
Ethylene
Ethylene liq.
E-100
6
V-104
T-100
25
28
Ethanol
H2SO4
Cold
water in CV-101
V-106
CV-100
V-105
V-101
V-100
V-102
V-103
R-100
2
35
32.2
P-100
35
31.0
20
38
Hydrogen
Ni
V-107
R-101
8
7
9
Ethane
10
H2O
P-101
10
Temperature
(oC)
25.0
35.0
35.0
35.0
35.0
60.3
41
38
54.0
45.1
Pressure (psi)
28
32.2
31.0
31.0
30.2
45.1
31.3
24.0
39.0
2.6
Mass flow
(tonne/hr)
10.3
13.3
0.82
20.5
6.41
20.5
0.36
9.2
20.9
11.6
Mole flow
(kmol/hr)
108
114.2
301.0
1204.0
758.8
1204.4
42.6
1100.8
142.2
244.0
Vapor fraction
E XAMPLE 4 - CONT
R-100
P-100
T-100
E-100
P-101
R-101
Reactor
Pump
Distillation Column
Condenser
Pump
Reactor
Hot water
out
Ethylene
Ethylene liq.
E-100
6
V-104
25
28
Ethanol
H2SO4
T-100
CV-100
1
V-100
V-101
V-106
CV-101
V-105
20
38
V-103
R-100
35
32.2
V-102
Cold
water in
Hydrogen
Ni
V-107
35
31.0
H2O
Ethane
R-101
10
P-101
P-100
Stream Number
10
Temperature (oC)
25.0
35.0
35.0
35.0
35.0
60.3
41
38
54
45.1
28
32.2
31.0
31.0
30.2
45.1
31.3
24.0
39
2.6
10.3
13.3
0.82
20.5
6.41
20.5
0.36
9.2
20.9
11.6
108
114.2
301.0
1204.0
758.8
1204.4
42.6
1100.8
142.2
244.0
Pressure (psi)
Vapor fraction
1. Major Pieces Of
Equipment
2. Utility
Streams
PFD
4. Basic Control
Loops
3. Process Flow
Streams
E XAMPLE 4 - CONT
R-100
P-100
T-100
E-100
P-101
R-101
Reactor
Pump
Distillation Column
Condenser
Pump
Reactor
Hot water
out
Ethylene
Ethylene liq.
E-100
6
V-104
25
28
Ethanol
H2SO4
Cold water in
LIC
V-106
T-100
CV-101
CV-100
V-101
20
V-103
R-100
35
32.2
38
V-100
V-102
V-105
Hydrogen
Ni
V-107
35
31.0
H2O
Ethane
R-101
10
LIC
P-101
P-100
Stream Number
10
Temperature (oC)
25.0
35.0
35.0
35.0
35.0
60.3
41
38
54
45.1
28
32.2
31.0
31.0
30.2
45.1
31.3
24.0
39
2.6
10.3
13.3
0.82
20.5
6.41
20.5
0.36
9.2
20.9
11.6
108
114.2
301.0
1204.0
758.8
1204.4
42.6
1100.8
142.2
244.0
Pressure (psi)
Vapor fraction
R-100
P-100
T-100
E-100
P-101
R-101
Reactor
Pump
Distillation Column
Condenser
Pump
Reactor
NOTE:
GATE VALVE
GLOBE VALVE
CHECK VALVE
Ethylene liq.
Ethylene E-100
PNEUMATIC DIAPHRAGM
VALVE
6
V-104
Cold water in
LIC
V-106
T-100
25
28
CV-101
CV-100
V-105
Ethanol
1
H2SO4
20
V-102
V-101
V-103
R-100
V-107
R-101
35
31.0
35
32.2
Hydrogen
9
Ni
38
V-100
Ethane
10
H2O
LIC
P-101
P-100
FLYSIS CHEMICAL
(M) SDN. BHD
Stream Number
10
Temperature (oC)
25.0
35.0
35.0
35.0
35.0
60.3
41
38
54
45.1
28
32.2
31.0
31.0
30.2
45.1
31.3
24.0
39
2.6
Pressure (psi)
Vapor fraction
Mass flow (tonne/hr)
10.3
13.3
0.82
20.5
6.41
20.5
0.36
9.2
20.9
11.6
108
114.2
301.0
1204.0
758.8
1204.4
42.6
1100.8
142.2
244.0
PROCESS FLOW
DIAGRAM
PRODUCTION OF
ETHANE FROM
ETHANOL
DRAWN BY :
APPROVED BY :
fs
ISSUED :
PAGE : 1 OF 1
Block Flow
Diagram (BFD)
Process Flow
Diagram (PFD)
PROCESS
DIAGRAMS
Process equipments
symbol and
numbering
Piping and
Instrumentation
Diagram (P&ID)
PFD
P&ID
Sensing Element
Final Control
Element
Measuring
Element
Transmit
Element
Control Element
Transmitter
Set point
Controller
Transmitter
Fluid
Fluid
Orifice (Flow
Sensor)
Resistance Temperature Detectors (RTD), as the name implies, are sensors used to
measure temperature by correlating the resistance of the RTD element with
temperature.
Most RTD elements consist of a length of fine coiled wire wrapped around a ceramic
or glass core. The element is usually quite fragile, so it is often placed inside a
sheathed probe to protect it.
The RTD element is made from a pure material whose resistance at various
temperatures has been documented. The material has a predictable change in
resistance as the temperature changes; it is this predictable change that is used to
determine temperature.
Temperature
C
Ohms
-200
056
1.3
-100
0.32
0.8
0.12
0.3
100
0.30
0.8
200
0.48
1.3
300
0.64
1.8
400
0.79
2.3
500
0.93
2.8
600
1.06
3.3
650
1.13
3.6
FLOW
SENSOR
FLOW SENSOR
4. Venturi Meter
A device for measuring flow of a fluid in terms of
the drop in pressure when the fluid flows into
the constriction of a Venturi tube.
TRANSMITTER
Transmitter is a transducer* that responds to a measurement variable and
converts that input into a standardized transmission signal.
*Transducer is a device that receives output signal from sensors.
Pressure Level
Transmitter
Differential Pressure
Transmitter
Pressure Transmitter
CONTROLLER
Controller is a device which monitors and affects the operational conditions of a
given dynamical system.
The operational conditions are typically referred to as output variables of the system
which can be affected by adjusting certain input variables.
Indicating Controller
Recording Controller
Pump
Control Valve
Heater
Block Flow
Diagram (BFD)
Process Flow
Diagram (PFD)
PROCESS
DIAGRAMS
Process equipments
symbol and
numbering
Piping and
Instrumentation
Diagram (P&ID)
Field
mounted on
pipeline
Flow Controller
PT
Pressure Transmitter
FE
Flow Element
PTD
Pressure Transducer
FI
Flow Indicator
FT
Flow Transmitter
LC
Level Controller
FS
Flow Switch
LG
Level Gauge
FIC
LR
Level Recorder
FCV
LT
Level Transmitter
FRC
LS
Level Switch
LIC
PC
Pressure Controller
LCV
PG
Pressure Gauge
LRC
PI
Pressure Indicator
PR
Pressure Recorder
TE
Temperature Element
Pressure Switch
TI
Temperature Indicator
PIC
TR
Temperature Recorder
PCV
TS
Temperature Switch
PRC
TC
Temperature Controller
PDI
TT
Temperature Transmitter
PDR
PDS
PDT
LC
LV 100
LC
V-100
LT
Complete control loop for LCV 101
LCV 101
PIPINGSometimes
AND also
INSTRUMENTATION
DIAGRAM (P&ID)
known as Process & Instrumentation Diagram
Example 2
With using these following symbology;
PRV-100
PE
V-100
PIC
PE
PT
PIC
PT
CV-102
TK-102
CV-101
pHT 1
pHE 2
pHT 2
pHIC 1
pHIC 2
TK-100
pHE 1
TK-101
(acid feed tank)
CV-102
TK-102
pHT 2
pHE 2
pHIC 1
pHE 1
TK-100
(pH adjustment tank)
CV-101
pHT 1
pHTE
2
pHT 2
pHIC 1
pHIC 2
pHE 1
TK-101
(acid feed tank)
LT 1
FC
L3
L2
PCV-100
TK-100
LIC 1
L1
PCV-101
LT 2
V-100
L4
LIC 2
FC
LT 1
L3
L2
PRV-100
TK-100
LIC 1
LT 1
L1
LIC 2
FC
PRV-101
L5
LT 2
V-100
L4
LT 2
LIC 2
Block Flow
Diagram (BFD)
Process Flow
Diagram (PFD)
PROCESS
DIAGRAMS
Process equipments
symbol and
numbering
Piping and
Instrumentation
Diagram (P&ID)
Instrumentation Numbering
XYY CZZLL
X represents a process variable to be measured.
(T=temperature, F=flow, P=pressure, L=level)
YY represents type of instruments.
Instrumentation Numbering
LIC 10003
L
IC
= Indicating controller.
100
03
= Loop number 3
Instrumentation Numbering
FRC 82516
F
RC
= Recording controller
825
16
= Loop number 16
Block Flow
Diagram (BFD)
Process Flow
Diagram (PFD)
PROCESS
DIAGRAMS
Process equipments
symbol and
numbering
Piping and
Instrumentation
Diagram (P&ID)
P&ID
PROCESS
CONTROL
VARIETY
Ratio Control
Split Range Control
Cascade Control
Differential Control
The advantage of this control scheme is that it is simple using single transmitter.
This control scheme does not take into consideration any of the other variables in
the process.
Y
LC
Fluid in
LCV-100
V-100
LT
Fluid out
V-100
The advantage of a feedback loop is that directly controls the desired process variable.
The disadvantage of feedback loops is that the process variable must leave set
point for action to be taken.
Y
LC
Fluid in
LCV-100
V-100
LT
Fluid out
V-100
Fluid in
V-100
TT
Fluid out
V 100
Feedforward loop is a control system that anticipates load disturbances and controls
them before they can impact the process variable.
For feedforward control to work, the user must have a mathematical understanding of how
the manipulated variables will impact the process variable.
FC
FT
Fluid in
Y
Steam
LCV-100
TI
Fluid out
In general, feedforward system should be used in case where the controlled variable has the
potential of being a major load disturbance on the process variable ultimately being
controlled.
FC
FT
Fluid in
Steam
LCV-100
TI
Fluid out
Y
FC
FT
V-100
PI
Controller with summing functions are used in these combined systems to total the
input from both the feedforward loop and the feedback loop, and send a unified
signal to the final control element.
FC
TC
FT
Fluid in
TT
Steam
LCV-100
Fluid out
PIC
Y
PT
FC
FT
V-100
Hot steam
Water
BOILER
TIC
PIC
Y
TT
PT
Hot steam
Water
BOILER
Ratio control is used to ensure that two or more flows are kept at
the same ratio even if the flows are changing.
FIC
FF
FT
FT
Water
Acid
2 part of water
1 part of acid
FIC
FF
FT
FT
Water
Acid
2 part of water
1 part of acid
FIC
Remote Ratio
Adjustment
FT
Water
FT
AIC
Physical Property
Measurement
2 part of water
1 part of acid
Acid
Waste, pH 4.5
NaOH Tank
pH 6.5
pH Adjustment Tank
pHC
FT
pHT
Waste, pH 4.5
NaOH Tank
pH 6.5
pH Adjustment Tank
FC
FT
Valve A
Valve B
CV-102
pHIC
TK-102
(base feed tank)
pHT 1
TK-100
(pH adjustment tank)
CV-101
TK-101
(acid feed tank)
T HANK YOU
Prepared by,
MISS RAHIMAH OTHMAN