Viscometer Manual

Instruction Manual
AMVn
Automated Microviscometer
Firmware Version: 1.7x
'ALILEO'ALILEI
-EASURE
WHATISMEASURABLE
ANDMAKEMEASURABLE
THATWHICHISNOT
Instruction Manual
AMVn
Automated Microviscometer
Firmware Version: 1.7x
Anton Paar GmbH assumes no liability for technical or printing errors or omissions in this document.
Nor is any liability assumed for damages resulting from information contained in the document.
Anton Paar GmbH reserves the right to content changes. This also extends to changes to delivery
volumes or any features of delivered parts.
All rights reserved (including translation). This document, or any part of it, may not be reproduced,
changed, copied, or distributed by means of electronic systems in any form (print, photocopy, microfilm
or any other process) without prior written permission by Anton Paar GmbH.
Trademarks, registered trademarks, trade names, etc. may be used in this manual without being marked
as such. They are the property of their respective owner.
Published by Anton Paar
Printed: Anton Paar, Austria
Copyright 2008 Anton Paar GmbH, Graz, Austria
Address:
Anton Paar GmbH

Anton-Paar-Str. 20
A-8054 Graz / Austria Europe
Tel: +43 316 257-0
Fax: +43 316 257-257
E-Mail: rheology@anton-paar.com
Web: www.anton-paar.com
Date:
July 2008
Document no.: B80IB01O.fm
Contents
1 About the Instruction Manual ......................................................................................................... 8
2 Safety Instructions........................................................................................................................... 9
2.1
2.2
General Safety Instructions ..................................................................................................... 9

2.1.1
Liability ..................................................................................................................... 9
2.1.2
Installation and Use .................................................................................................. 9
2.1.3
Maintenance and Service......................................................................................... 9
2.1.4
Disposal.................................................................................................................. 10
2.1.5
Returns................................................................................................................... 10
2.1.6
Precautions for Highly Inflammable Samples and Cleaning Agents ...................... 10
Warning Symbols on the AMVn Instrument............................................................................11
3 AMVn - An Overview...................................................................................................................... 12
4 Unpacking and Checking the Supplied Items ............................................................................. 13
4.1
Unpacking Supplied Items ..................................................................................................... 13
4.2
Checking of Supplied Items ................................................................................................... 13

4.2.1
Supplied Parts ....................................................................................................... 13
4.2.2
Accessories in the Measuring System Set ............................................................. 14
4.2.3
4.2.2.1
Available Measuring System Sets .......................................................... 14
4.2.2.2
Content of a Measuring System Set ....................................................... 15
Optional Accessories ............................................................................................. 16
5 Functional Components................................................................................................................ 17
5.1
Front of AMVn........................................................................................................................ 17
5.2
Rear Side of AMVn ............................................................................................................... 17
5.3
Measuring System ................................................................................................................ 18
5.4
Monitor and Function Keys .................................................................................................... 18
6 Putting AMVn into Operation........................................................................................................ 19
6.1
Activating AMVn .................................................................................................................... 19
6.2
Preparing the Measurement .................................................................................................. 20

6.2.1
Introducing the Ball to the Capillary ....................................................................... 20
6.2.2
Attaching the Filling Adapter .................................................................................. 20
6.2.3
Filling the Capillary ................................................................................................. 21
6.2.4
Attaching Temperature Tube .................................................................................. 21
6.2.5
Mounting the Capillary into the AMVn Instrument .................................................. 22
6.2.6
Attaching Protective Cap........................................................................................ 22
Measurement................................................................................................................................. 23
7.1
Setting up AMVn.................................................................................................................... 23
7.2
Starting the Measurement...................................................................................................... 24
B80IB01
7.2.1
Thermostatting the Capillary Block......................................................................... 24
7.2.2
Sample Thermostatting .......................................................................................... 24
7.2.3
Measuring the Sample ........................................................................................... 25
7.3
Displaying the Measured Values ........................................................................................... 25
7.4
Printing the Measured Values................................................................................................ 26
7.5
Cleaning the Measuring System............................................................................................ 27
8 AMVn Firmware Update................................................................................................................. 28

8.1
8.2
8.3
Menu "SETUP Instrument" ................................................................................................. 28

8.1.1
Date and Time ........................................................................................................ 28
8.1.2
Temperature Equilibration ...................................................................................... 29

8.1.2.1
Temperature Equilibration in "constant mode" ........................................ 29
8.1.2.2
Temperature Equilibration in "auto mode"............................................... 29
8.1.3
Default Settings ...................................................................................................... 30
8.1.4
Printer Configuration .............................................................................................. 30
8.1.5
Software Update..................................................................................................... 31
8.1.6
Zero Point Adjustment............................................................................................ 31
Menu "SETUP Measurement" ............................................................................................ 32

8.2.1
Method ................................................................................................................... 32
8.2.2
Measuring System.................................................................................................. 34
Menu "Print Configuration" ................................................................................................. 35
9 Calibration of Measuring Systems ............................................................................................... 36

9.1
Calibrated and Uncalibrated Capillaries ................................................................................ 36
9.2
Menu Calibration.................................................................................................................... 36
9.3
Calibrating a New Measuring System.................................................................................... 37
10 Maintenance ................................................................................................................................... 38
10.1 Cleaning the Measuring System............................................................................................ 38
10.2 Cleaning the Filling Adapter................................................................................................... 38
10.3 Cleaning AMVn...................................................................................................................... 39
10.4 Wetted Parts of AMVn ........................................................................................................... 39
10.5 Replacing O-rings in the Filling Adapter ................................................................................ 40
10.5.1
Filling Adapter Without Engraved Marking Ring .................................................... 40
10.5.2
Filling Adapter With Engraved Marking Ring ......................................................... 40
10.5.3
Exchanging the O-rings.......................................................................................... 40
11 Technical Data ................................................................................................................................ 41

Appendix A:
Viscosity..................................................................................................................... 42
A.1 Viscosity Standard Fluids .................................................................................... 42
A.2 Calibration Constant K1 ...................................................................................... 43
A.3 Determining the Viscosity.................................................................................... 43
Appendix B:
Extension of the Measuring Range.......................................................................... 44

B.1 Quadrupling the Maximum Measuring Range..................................................... 44
B.2 Doubling the Maximum Measuring Range .......................................................... 45
Appendix C:
Menu Tree Firmware Structure.............................................................................. 46
B80IB01
B80IB01
1 About the Instruction Manual
1 About the Instruction Manual

This instruction manual informs you about the installation and the safe handling
and use of the instrument. Make sure that the instruction manual is easily
accessible to all personnel involved with the instrument. Pay special attention to
the safety instructions and warnings in the manual and on the instrument.
Symbols in this Instruction Manual
This instruction manual features the following symbols:
Warning:
This symbol calls attention to the risk of accidental injuries or damage to
goods. Do not proceed until the indicated conditions for averting this threat
are fully understood and met.
Caution:
This symbol calls attention to the risk of instrument damage or
measurement errors. Do not proceed until the indicated conditions for
averting this threat are fully understood and met.
Information:
This symbol calls attention to any additional information of use to the
operator.
Warning! Hot surface:

This symbol calls attention to the fact that the respective surface can get
very hot. Do not touch this surface without adequate protective measures.
B80IB01
2 Safety Instructions
Read the instruction manual at hand before using AMVn.
Follow all hints and instructions contained in this instruction manual to

ensure the correct use and safe functioning of AMVn.
2.1
2.1.1
Liability
The instruction manual at hand does not claim to address all safety issues
associated with the use of the instrument and samples. It is your
responsibility to establish health and safety practices and determine the
applicability of regulatory limitations.
Anton Paar GmbH only warrants the proper functioning of AMVn if no

adjustments have been made to the mechanics, electronics and firmware.
Only use AMVn for the purpose described in this instruction manual. Anton
Paar GmbH is not liable for damages caused by incorrect use of AMVn.
2.1.2
Installation and Use
AMVn is not an explosion-proof instrument and therefore must not be

operated in areas with risk of explosion.
The installation procedure should only be carried out by authorized

personnel who are familiar with the installation instructions.
Do not use any accessories or wearing parts other than those supplied or
approved by Anton Paar GmbH.
Make sure all operators are trained to use the instrument safely and correctly
before starting any applicable operations.
In case of damage or malfunction, do not continue operating AMVn. Do not

operate the instrument under conditions which could result in damage to
goods and/or injuries and loss of life.
Check AMVn for chemical resistance to the samples and cleaning agents.
2.1.3
B80IB01
General Safety Instructions
Maintenance and Service
The results delivered by AMVn not only depend on the correct function of the
instrument, but also on various other factors. We therefore recommend to
have the results checked (e.g. plausibility tested) by skilled personnel before
consequential actions are taken based on the results.
Service and repair procedures may only be carried out by authorized

personnel or by Anton Paar GmbH.
2.1.4
Concerning the disposal of AMVn, observe the legal requirements in your

country.
2.1.5
Returns
For repairs send the cleaned AMVn instrument to your Anton Paar
representative. Only return the instrument together with the filled out
"Maintenance/Error Report" and the "Standard Maintenance Contract". Find
the applicable forms on the Anton Paar homepage (www.anton-paar.com).
2.1.6
10
Disposal
Precautions for Highly Inflammable Samples and

Cleaning Agents
Observe and adhere to your national safety regulations for handling the
measured samples (e.g. use of safety goggles, gloves, respiratory protection
etc.).
Only store the minimum required amount of sample, cleaning agents and
other inflammable materials near the AMVn.
Do not spill sample/cleaning agents or leave their containers uncovered.

Immediately remove spilled sample/cleaning agents.
Make sure that the setup location is sufficiently ventilated. The environment
of AMVn must be kept free of inflammable gases and vapors.
Connect AMVn to the mains via a safety switch located at a safe distance
from the instrument. In an emergency, turn off the power using this switch
instead of the power switch on AMVn.
Supply a fire extinction unit.
Ensure the sufficient supervision of AMVn during operation.
B80IB01
2.2
Warning Symbols on the AMVn Instrument
Warning symbol Hazard on capillary block:

When handling caustic fluids, acids, easily inflammable fluids etc. use the
required protective clothing (protective gloves, safety goggles). If the samples in
the capillary are heated up to measuring temperatures of over 70 C after filling,
the thermal expansion of the fluid in the glass capillary may result in the
unintentional opening of the capillarys sealing caps.
During the activation of the AMVn instrument, the capillary block moves into the
physical end position (initialization). The capillary block should not be touched
during this movement, in order to avoid possible clamping or displacement of the
zero position. The capillary block should only be moved by hand when the
instrument is inactive.
Warning symbol Hot surface on capillary block:

At measuring temperatures of over 70 C there is risk of burning at
various parts of the capillary block. Therefore, the capillary block and the used
capillary should only be touched with adequate safety gloves at these
temperatures.
Keep in mind that at measurement temperatures of over 70 C the glass capillary
has the same temperature when extracted, therefore it might cause burns. It is
recommendable to cool down AMVn to temperatures lower than 70 C before the
capillary is touched with bare hands.
Warning symbol on the rear side of AMVn:
B80IB01
Service should only be carried out by qualified personnel.

Before service, the mains plug should be disconnected.
The instrument needs to be earthed.
11
3 AMVn - An Overview
3 AMVn - An Overview
Anton Paar GmbH thanks you for buying AMVn, the global vanguard measuring
instrument for the automatic, high-precision viscosity determination of low viscous
substances. It provides you with measurement solutions of utmost precision in a
very broad viscosity and temperature measurement range.
The measurement principle of AMVn is the rolling ball/falling ball principle in
accordance with DIN 53015 and ISO 12058. It consists of the measurement of a
balls rolling time in a diagonally mounted glass capillary filled with sample. The
shear rate is influenced by changing the inclination angle of the capillary.
In this way, investigations are implemented on whether the measured samples
are Newtonian or non-Newtonian (pseudoplastic or dilatant) fluids.
A built-in Pt100 temperature sensor is used for precise temperature
measurements and temperature regulation.
Choose various measurement methods and systems that accord with your
measurement applications.
You can print and display measurement results with sample names and
measurement system data. Only the most recent measurement result is saved in
the AMVn instrument.
In the case of multiple measurement results, it is recommendable to immediately
print or note the data.
With the optional VisioLab Windows Software, all results can be saved and
evaluated in Excel.
The optionally delivered, fully automatic sample changers of Anton Paar GmbH
automatically fill the AMVn capillaries with samples. Between measurements the
capillaries are automatically cleaned with two cleaning agents, and consecutively
dried in air.
Our trained Anton Paar GmbH personnel always welcome your requests and will
gladly provide you with additional offers.
12
B80IB01
4 Unpacking and Checking the Supplied Items
4 Unpacking and Checking the Supplied

Items
4.1
Unpacking Supplied Items
AMVn was tested and packed carefully before shipment. However, damage may
occur during transport.
Keep the packaging material (box, foam piece, transport protection) for
possible returns and further questions from the transport- and insurance
company.
Compare the supplied parts to those noted in the table to check the delivery
for completion.
If a part is missing, contact your Anton Paar representative.
If a part is damaged, contact the transport company and your Anton Paar
representative.
4.2
Checking of Supplied Items
The following tables list all supplied items contained in your order. Every
instrument is delivered as a unit.
4.2.1
Symbol
B80IB01
Supplied Parts
Pcs.
Article Description
Mat. No.
AMVn Automated Microviscometer
1569
Instruction manual
German or English
Mains cable:
Euro- or
GB- or
US- or
PRC
52112
61865
52656
27011
Temperature tube
22109
Protective cap
22252
Measuring system set, dependent on

your application and order
in a box (288 x 157 x 38 mm)
see
Chapter
4.2.2.
13
4.2.2
Accessories in the Measuring System Set
A measuring system set is delivered in a box, including all necessary parts for
a measurement with AMVn. Every measuring system set includes the measuring
system that accords with your order.
The measuring system is a combination of a capillary and a diametrically
matching ball.
The identification is determined by the internal diameter of the capillary:
e.g. the measuring system (set) 1.6 which is comprised of:
a capillary (diameter 1.6 mm) and balls (diameter 1.5 mm).
Find a listing of all measuring system sets and all parts contained in the box in the
tables below. You can order all registered parts either in a set (Chapter 4.2.2.1)
or separately, in reference to the material number listed on the right (Chapter
4.2.2.2).
4.2.2.1
Symbol
14
Available Measuring System Sets

Pcs.
Article Description
Mat. No.
Measuring system set 1.6

Capillary diameter: 1.6 mm
Volume:
400 L
Ball diameter:
1.5 mm
Measuring range: 0.3-10 mPa.s
67603

Volume:
510 L
Ball diameter:
1.5 mm
63875

Volume:
400 L
Ball diameter:
2.5 mm
Measuring range: 20-230 mPa.s
63877

Volume:
2500 L
Ball diameter:
3.0 mm
Measuring range: 80-2500 mPa.s
63878
Measuring
system
set
uncalibrated
Volume:
400 L
Ball diameter:
1.5 mm
1.6
19570
B80IB01
4.2.2.2
Content of a Measuring System Set
The measuring system contained in the box depends on your order

Symbol
Pcs.
Article Description
Calibrated capillary
with data medium and calibration
certificate
Capillary 1.6 mm calibrated or
Capillary 4.0 mm calibrated
74273
74275
74276
74277
Uncalibrated capillary
Capillary 1.6 mm uncalibrated
67605
Balls
d = 1.5 mm for 1.6
d = 1.5 mm for 1.8
d = 2.5 mm for 3.0
d = 3.0 mm for 4.0
73109
63869
63870
63871
300
300
500
500
B80IB01
mm capillaries or
mm capillaries or
mm capillaries or
mm capillaries
Mat. No.
Plastic tweezers
63132
Syringe, 5 mL
63130
Funnel
for 1.5 mm balls or
for 2.5 mm and 3.0 mm balls
20743
20742
Filling adapter incl. O-rings
63390
Replacement-O-ring silicone 10x1.5 mm
12760
Replacement-O-rings Viton
(Chapter 10.5)
O-ring viton 6.4x1.9 mm FPM 75
(for filling adapter with engraved
marking ring)
oder
O-ring viton 6.5x1.5 mm FPM 80
(for filling adapter without engraved
marking ring)
23726
65555
O-ring tool
24943
LUER sealing cap PCTFE
63388
LUER plug PTFE
63865
15
4.2.3
Symbol
Optional Accessories
Pcs.
Article Description
Filling adapter "KALREZ"

(incl. 1 silicone and 2 KALREZ O-rings)
69079
O-ring (KALREZ) 6.4 x 1.9 mm
69578
Ball dispenser
for 1.5 mm balls or
for 2.5 mm and 3.0 mm balls
63604
63605
10
Tungsten carbide-cobalt balls 3.0 mm

for the viscosity measuring range
extension of the 4.0 mm capillary
Mat. No.
70116
Balls 4m-gold plated

for high chemical resistance
d = 1.5 mm
d = 2.5 mm
d = 3.0 mm
20659
20660
20661
Keyboard
German
English
77143
77144
Printer
9423
Printer paper
59149
Ribbon cartridge black for Citizen printer
8139
Uncalibrated capillary:
1.6 mm
1.8 mm
3.0 mm
4.0 mm
67605
63180
63181
63182
Disposable syringes:
1 mL Luer
2 mL Luer
5 mL Luer
68015
6771
6772
VisioLab Windows software
5034
300
500
500
1
1
100
100
1
Viscosity standard fluids see Chapter

A.1
16
B80IB01
5 Functional Components
5.1
Front of AMVn
A
B
C
D
E
... Capillary block

... Drip plate
... Bubble level
... Display with function keys
... Housing ventilation
The functions of the function keys F1 F5, which

have different meanings in different menu levels,
are featured in the footer on the display.
Fig. 5. 1
AMVn front side
B
D
5.2
Rear Side of AMVn
A
B
C
D
A
E
B F
C
D G
E H
F
G
H
J I
K
L
I
J
K
L
... Interface for sample changer SPV or

SP3-V (COM 3)
... Serial printer interface (COM 2)
... Interface for density meters (COM 1)
... Computer interface (PC)
... Contrast regulation display
... S-BUS interface for sample changer SP-1m
or SP-3m
... Keyboard connection
... Type plate
... Data plate (power supply)
... Power switch
... Mains connection
... Warning
Fig. 5. 2
AMVn rear side
Information:
The interfaces COM 1, COM 3, PC and S-Bus are only necessary if the
VisioLab Windows software is used.
Density meters are connected to COM 1.
Sample changers are either connected to COM 3 (SPV and SP3-V) or to
the S-BUS interface (SP-1m and SP-3m).
B80IB01
17
5.3
Measuring System
A
B
C
D
E
F
G
D
C
B
F
... Sealing cap

... Capillary
... Glass knob
... Filling adapter
... Plug
... 8-digit serial number of capillary
... Ball
G
A
Fig. 5. 3
5.4
Measuring system set
Monitor and Function Keys
Title of the indicated menu or submenu
Time
actual SETTINGS
Sample
Method
Meas. System
Instr. Settings
10:48:12
Name
Remark
Temp.
Dens.
Menu
:
:
:
:
Sample 1
Testlauf 1
20.00C
0.9982g/cm3
Eval
NewRun
Reference to the function keys

Indicating range for settings;
Data of the active menu line
Items of the menu:

active menu line highlit
Function keys and monitor display:
ESC
Back
Edit
Cont
.....
.....
.....
.....
......
.....
.....
.....
further submenus (down)

further submenus (up)
<Enter> to confirm and/or go to next
to go back one step or to abort a current action, all changes are lost
to go back one step, changes are saved
to edit data
to skip through the possible values
to go to the next step and continue
Keyboard use:
The keyboards function keys (F1 F5) accord with the function keys of AMVn.
Use these to choose the menu and/or input field you wish to access. An external
keyboard enables a much faster and easier input.
18
B80IB01
6 Putting AMVn into Operation

AMVn needs to be set up on a stable, level surface. To ensure temperature
stability, never locate AMVn:
6.1
next to a heating facility

near an air conditioning or ventilation system
in direct sunlight.
Activating AMVn
1. Set up AMVn on the lab desk and level it off with the adjustable feet and the
built-in bubble level. Make sure all four feet touch the lab desk.
Caution:
Before activating the AMVn instrument make sure that the correct line voltage
is applied (85 V to 264 V, 50 Hz to 60 Hz). If large voltage fluctuations are to
be expected, we recommend using a constant-voltage source (UPS).
2. Connect the power inlet of the AMVn instrument to the mains using the
delivered power cord.
3. Activate AMVn with the power switch located on its rear side. The green
display light signals that the power is on.
Warning:
After its activation, AMVn independently runs through the coil- and zero
position initialization. In the course of this the capillary block first moves to its
final position before it remains in its home position leaning backwards at
20 . The capillary block should not be touched during this movement, in order
to avoid possible clamping or displacement of the zero position. The capillary
block should only be moved by hand when the power of the instrument is
switched off.
4. After the successful initialization you will see the following reading on the
display:
actual SETTINGS
Sample
Method
Meas. System
Instr. Settings
Menu
10:48:12
Name
Remark
Temp.
Dens.
:
:
:
:
Sample 1
Testlauf 1
20.00C
0.9982g/cm3
Eval
NewRun
"actual SETTINGS" displays the settings of the last measurement. Browse with
F3 or the down button to check the following:
Sample:
sample name, remark, temperature, density
Method:
the last method used
Meas. system: the measuring system used for the last measurement
Instr. Settings: instrument constant K2, temperature equilibration mode
F4 <Eval> displays/prints the results of the last measurement.
B80IB01
19
6.2
Preparing the Measurement
Before starting a measurement, fill the capillary and mount the measuring system
in the capillary block.
6.2.1
Introducing the Ball to the Capillary
1. Hold the capillary (B) vertically and place the funnel (A) on
the capillary opening (Fig. 6. 1).
2. Use the delivered plastic tweezers to introduce a ball into the
funnel.
(B)
Fig. 6. 1
Introduction of the ball
Information:
Never touch the balls with your fingers, as these need to be completely
clean to function correctly. Only use clean capillaries and clean or new
balls.
You can also use an optionally available ball dispenser to introduce the
ball.
6.2.2
Attaching the Filling Adapter
1. Close the capillary by attaching the filling adapter to it.
Fig. 6. 2
Attaching the filling adapter
2. Check the mobility of the ball by swiveling the capillary.

Caution:
Make sure the capillary is completely inserted into the filling adapter. Handle
the capillary with care, it is made of glass and can easily break.
20
B80IB01
6.2.3
Filling the Capillary
1. Introduce a syringe into the cone of the filling adapter.

2. Immerse the tip of the capillary in the sample.
3. Draw up the sample with the syringe until it is visible in the
lower end of the syringe. The capillary should be completely
free of air bubbles, otherwise the filling procedure needs to be
repeated.
4. Dry the tip of the capillary with a cloth and close it with a LUER
cap.
5. Now extract the syringe from the filling adapter and dry the
adapter if necessary. Close the filling adapter with the LUER
plug.
6. Make sure that the capillarys exterior is clean and dry.
7. Again check the mobility of the ball by swiveling the capillary.
Fig. 6. 3 Filling the capillary
Warning:
When handling caustic fluids, acids, easily inflammable fluids etc., use the
required protective clothing (protective gloves, safety goggles).
6.2.4
Attaching Temperature Tube
Always mount the temperature tube and the protective cap (Chapter 6.2.6) before
you start a measurement.
1
2
Fig. 6. 4
... Temperature
tube
... Protective cap
Attaching the temperature tube and the protection cap
Screw the temperature tube on to the rear side of the capillary block. For
functionality reasons it should always stay attached to the capillary block and
should only be unscrewed for cleaning.
B80IB01
21
6.2.5
Mounting the Capillary into the AMVn Instrument
Before mounting the filled capillary, you need to activate AMVn and wait until the
self-test is concluded (Chapter 6.1).
Caution:
Make sure that the self-test is concluded and no measurement program has
started, so that the capillary block does not start any surprising movements.
Do not push too hard when mounting the capillary, because the glass could
break. Do not use excessive force!
1. Carefully insert the capillary into the capillary block, starting from the front.
2. Turn the capillary so that the glass knob easily slips into the corresponding
recess of the capillary block opening.
As soon as the glass knob has slid into the opening, completely insert the capillary
into the capillary block until the red silicone O-ring of the adapter is no longer
visible and you meet a resistance.
6.2.6
Attaching Protective Cap
1. After mounting a capillary, attach the protective cap (2, Fig. 6. 4) in a straight
position in the front of the capillary block.
2. Fix the protective cap by turning it clockwise.
Leave the protective cap on the capillary block during the measurement and only
remove it once you change the capillary.
Hot surface:
When attaching or removing the temperature tube and the protective cap at
high measuring temperatures you might be operating in the direct vicinity of
hot surfaces. Therefore only touch the capillary block and the capillary with
adequate protective gloves (Chapter 2.2) or wait until the capillary block has
cooled down.
Warning:
If the samples in the capillary are heated up to measuring temperatures up to
135 C, the thermal expansion of the fluid in the glass capillary may result in
the unintentional opening of the capillarys sealing caps. It is imperative to use
the temperature tube and the protective cap.
22
B80IB01
7 Measurement
Measurement
Before starting a measurement, set up AMVn according to your wishes.
7.1
Setting up AMVn
To prepare a measurement, press F5 <New Run> in the main menu "Actual

Settings" which appears after activation.
The following screen appears "MEASURE PREPARE":
MEASURE PREPARE
Sample Name
Remark
Density
Temperature
11:18:26
Sample 1
Back
Scroll through all items with the F3 <down button> and make sure all settings
always listed on the right are correct before starting the measurement:
Sample Name: sample name

Remark:
remark or hint concerning the sample (optional)
Density:
sample density at measuring temperature
Temperature: measuring temperature between +5 and +135 C
Temp. Equi:
temperature equilibration mode
Method:
choose a stored measuring method
Meas. System: choose a stored measuring system for the method
F5 <Enter>:
F2, F3, F4:
F1 <Back>:
to change a setting
enter values
to return to "Actual SETTINGS" menu
Information:
A new method or measuring system can only be entered in the submenu
"Setup Measurement" in "MENU".
Individual settings of the temperature equilibration mode are only possible
in the submenu "Setup Instrument" - "Temperature equilibration" .
Keep in mind that only measuring systems that apply to the chosen
method are displayed.
B80IB01
23
7 Measurement
7.2
Starting the Measurement
*** Start *** starts the measurement, for this option press F5 <ENTER>.
MEASURE PREPARE
11:19:23
Temp. Equi.
Method
Measuring System
*** Start ***
Press ENTER to Start
Back
Every measuring procedure consists of three consecutive steps:
1. Thermostatting of capillary block
2. Sample thermostatting
3. Sample measurement
7.2.1
Thermostatting the Capillary Block
If the set temperature ("set T:") does not accord with the actual temperature ("act
T:"), the instrument holds up the temperature equilibration of the sample until the
display reading "!Temp. diff >!" disappears. This occurs at differences smaller
than 0.05 C.
7.2.2
Sample Thermostatting
The sample thermostatting takes place immediately after the thermostatting of the
capillary block. You can find settings for this in Chapter 8.1.2.
RUN - TempEqui
Time (s)
to Start: 2.65
Runtime : 11.34
to End : 0.63
var Coef: min.rep = 4
Skip
F2 <Show>:
F1 <Skip>:
Show
*auto
set
act
set
act
10:55:02
T
:
T
:
ang.:
ang.:
rep :
20.00C
20.00C
70
70.0
2/4
Strtd
displays the individual run times of the measurement

displays the samples temperature equilibration,
e.g. at repeated measurements with the same sample
Every start and stop signal is accompanied by a beeping sound. After the second
measurement the actual and desired deviation ("var Coef:") is displayed. After a
successful temperature equilibration, the measuring instrument starts the actual
measurement.
24
B80IB01
7 Measurement
7.2.3
Measuring the Sample
The display shows the actual measuring angle, the current number of actual
repetition, and, from the third measurement onwards, the determined viscosity.
RUN
11:25:12
Time (s)
to Start: 2.65
Runtime : 11.34
to End : 0.63
Visc.
: 1.002 mPa.s
Stop
F2 <Show>:
F1 <Stop>:
Esc:
Enter:
set
act
set
act
T
:
T
:
ang.:
ang.:
rep :
Show
20.00C
20.00C
70
70.0
Strtd
displays the single run times of the measurement

interrupts the measurement
continues the measurement
stops the measurement
Caution:
Choose the angle of your measurement in such a way that the ball rolling
times do not drop below 10 sec. Otherwise turbulence is caused in the
capillary and a seemingly higher viscosity is read.
In this case choose another measuring method (Chapter 8.2.1).
Information:
Always enter an even number of repetitions, because viscosity is always
determined from two repetitions.
For the viscosity calculation a maximum of 20 repetition periods is used. If you
want more than 20 repetitions, you have the further option of connecting
AMVn to a PC. The AMVn Visiolab Windows software allows a nearly
unlimited amount of repetitions, which is only one of its many benefits.
7.3
Displaying the Measured Values
When a measurement is finished, its evaluation is automatically displayed under

"EVALUATION".
The result of the highlit value is displayed on the right side of the screen. The
sample name and remark are displayed on each screen. Scroll with the cursor
keys F2, F3 and F4
.
EVALUATION
Sample:Sample1
dyn. Visco
kin. Visco
Infos
Rep.times
ESC
B80IB01
11:23:56
Testlauf1
Mean
: 1.0019 mPa.s
Time
: 11.35 s
St.Dev :0.00006 mPa.s
Var.Co : 0.01 %
Print
25
7 Measurement
"Infos": angle of capillary block during measurement, number of measurement

repetitions, temperature, density, starting time and date, serial number of
capillary, calibration constant K1 and the measuring system used for the
measurement.
"Rep. times": display of all repetitions runtimes
7.4
Printing the Measured Values
F5 <Print>: prints the last stored values

Example for a printout:
----- A M V n Microviscometer
SNo: 409247
----------
-----
SW_Ver: V1.70
EVALUATION
-----------
Sample: Water
Remark:
Method: Standard 1.6
Angle:
70 deg
Repetitions: 4
CapSys: 1.6/1.500 mm
Density :
0.9982 g/cm3
act. Temp:
20.00 C
MeasSystem: 15844194-70A
K1
: 0.984e-02
dyn. Viscosity: 1.0020 mPa.s
kin. Viscosity: 1.0038 mm2/s
mean Time:
15.27 s
Var. Coeff.:
0.00 %
Started on 2010-03-10 at 08:38
26
B80IB01
7 Measurement
7.5
Cleaning the Measuring System
A thorough cleaning of the AMVn measuring system after measurement

conclusion is imperative.
Caution:
Do not leave any samples in the measuring system after you have
finished the measurement.
Rinse the measuring system with a suitable cleaning agent.
Only use cleaning agents that are compatible with the materials (Chapter
10.4).
Before you dry the capillary with compressed air, remove the ball.
1. Remove the protective cap.
2. Remove the capillary from the the capillary block. Take care not to twist the
capillary.
3. Remove the LUER plug and insert a syringe into the filling adapter.
4. Now remove the LUER cap and rinse the capillary with cleaning agent.
Repeat the rinsing procedure several times by drawing up and flushing out
cleaning agent.
5. After the cleaning procedure remove the syringe and the filling adapter.
6. Use a volatile solvent, e.g. highly concentrated alcohol or acetone, to
accelerate the drying procedure after cleaning.
7. Dry the measuring system e.g. with compressed air (max. 0.5 bar).
8. Check that the ball moves easily when the capillary is swiveled. If this is the
case, the cleaning procedure is concluded.
B80IB01
27
8 AMVn Firmware Update

This description extends to the Firmware Version V1.7x. If your AMVn features
another Firmware Version, minor differences to the description in this manual
could occur.
Through the main menu "MENU" you access the submenus:
"Setup Instrument" for setting up AMVn,

"SETUP Measurement" to enter measurement settings and
"Print Configuration" to print out the configuration of AMVn.
8.1
Menu "SETUP Instrument"
In "Setup Instrument" you can view or change all settings concerning AMVn.
With F5 <Enter> you can access each of the following submenus, with F1 <Back
or <ESC> you return to the menu.
"Date" Date
"Time" Time
"Zero adjust" Zero adjustment
"Temperature equilibration" Temperature equilibration
"Instrument Constant K2" Instrument constant: preset
"Default Settings" Default settings
"Configuration Printer" Printer configuration
"Info" Information on Firmware Version, serial number of AMVn and your
Anton Paar GmbH contact address
"Service Utilities" password-protected service menu for authorized
service personnel of Anton Paar GmbH
"Software Update" Update instrument software
8.1.1
Date and Time
Change date and time with the arrow keys and confirm the entry with <Enter>.
SETUP Date
Date :
10:49:37
2000-09-23 Saturday
YYYY-MM-DD Day
ESC
28
B80IB01
8.1.2
Temperature Equilibration
You can choose between two different modes: constant oder auto mode. The
active mode is highlit and marked with an asterisk (*).
F2, F3:
F5 <Enter>:
F4 <Edit>:
8.1.2.1
to select the desired mode

activate the desired mode
edit the selected mode
Temperature Equilibration in "constant mode"
Choose "constant mode" if you know how long your sample will take to reach
measuring temperature.
F2, F3, F4 arrow keys: adjust waiting periods until measurement start
F5 <Enter>:
accept changes
F1 <ESC>:
discard changes
SETUP Temp. equilibration

Mode:
* constant
auto
waiting time:
ESC
8.1.2.2
10:55:24
60s
Edit
Temperature Equilibration in "auto mode"
Standard setting of parameters:
SETUP Temp. equilibration

Mode:
constant
* auto
ESC
angle:
var.coeff:
rep. to fit:
max.rep.:
:
:
:
:
70
0.1%
4
20
Edit
measurement angle
variation coefficient to reach temperature equilibration
number of repetitions to calculate the variation coefficient
max. number of repetitions to reach temperature equilibration
F5 <Enter>:
F2, F3, F4 arrow keys:
F5 <Enter>:
F1 <ESC>:
B80IB01
angle
var. coeff.
rep. to fit
max. rep.
10:55:31
choose parameters with values you wish to change

change values
accept changes
discard changes
29
8.1.3
Default Settings
In the submenu "Default Settings" you can reset user-defined settings to factory
default values.
SETUP Default Settings

F2
F3
F4
Prnt
F2 <Prnt>:
F3 <Meth>:
F4 <Meth>:
8.1.4
10:55:56
Reset Printer Configuration

Delete user defined Methods
Delete user defined MeasSystem
Back
1-2
Meth
Meas
to reset the printer configuration

to delete user-defined measuring methods
to delete user-defined measuring systems
Printer Configuration
In the submenu "Configuration Printer" you can change your printer settings.
SETUP Configuration Printer

Printer on
Delay Char/Char
Delay Line/Line
:
:
:
11:48:42
COM2
OFF
1.0 s
ESC
Press F4
to select the serial interface COM 2 or COM 3

to activate a delay between the single characters
to activate the delay time of 0.0 to 1.5 s between two printed lines
F5 <Enter>:
F1 <ESC>:
confirm changes
discard changes
Delays are necessary for printers without a receive buffer. In case characters are
missing in your printout, increase the delay times.
The parameters of the printer interface on the AMVn instrument are pre-adjusted
and cannot be changed:
baudrate 9600, 7 data bits, even parity, 1 stop bit, no handshake
30
B80IB01
8.1.5
Software Update
In the submenu "Software Update" you can install new instrument software
versions. Further information will be included with your update.
Whenever applicable, contact your local Anton Paar representative for possible
firmware updates.
8.1.6
Zero Point Adjustment
AMVn is already delivered pre-adjusted. In case you observe evident run time
differences between even and uneven repetitions, you can compensate these
with the zero point adjustment.
Before starting a zero point adjustment, make sure that the instrument is placed
on a level, stable surface. If necessary, level AMVn using the adjustable feet and
the built-in bubble level.
Follow the submenu instructions on the screen.
SETUP Zero Adjust

1st
2nd
3rd
4th
Step:
Step:
Step:
Step:
Back
F3 <Meas>:
F5 <Edit>:
F5
F3
F4
F3
Show
to
to
to
to
1-2
10:55:02
edit method
start Run
adjust 0-Position
control adjustment
Meas
Zero
Edit
starts the zero point adjustment with the method "Zero Adjust"
changes the zero point adjustment method
After the selected angle is measured, AMVn automatically raises the angle by 1
degree and starts a new run. This second run substantially raises the accuracy of
the zero point adjustment.
B80IB01
31
8.2
Menu "SETUP Measurement"
In the second submenu of "MENU" "SETUP Measurement", you can create

or edit measuring methods and measuring systems and calibrate the latter.
SETUP Measurement
10:59:35
Method
Measuring System
Measuring System: Calibrate
Menu
Print
A measuring system is the combination of a capillary and the suitable ball

calibrated for a certain angle.
There can be different measuring systems that still feature the same
capillary serial number if they have different angles. Seeing as there are
various different measuring systems, always choose the one most suitable to
your individual application.
In the menu "Measuring System: Calibrate" you can calibrate capillaries.

See Kapitel 9.
With F4 <Print> you can print the content of the highlit menu.
With F5 <Enter> you can enter the selected submenu.
8.2.1
Method
A method involves the measuring angle, the number of repetitions, and the
measuring system used for a measurement.
In the menu "Method" you can create, revise or delete a method.
Information:
When using more than one method it is advisable to assign slightly different
names. This might prove helpful later in matching them to the applications.
32
B80IB01
SETUP: Measure-Method
->
2/05
Name
Angle
Rep.
CapSys
:
:
:
:
Standard 1.6
70
04
1.6/1.500 mm
Back
F2, F3 arrow keys:
e.g. 2/05:
F1 <Back>:
F5 <Enter>:
F5 <Edit>:
F3 <Delete>:
F1 <Back>:
F4 <Enter>:
11:01:37
New
display all stored methods
the second of five stored methods is displayed
back to the menu
choose the displayed method to then press:
to edit or
to delete or
to return
enter a new method:
SETUP: EDIT Method

Name
Angle
Rep
CapSys
.......
ESC
F5 <Enter>:
11:00:44
Save
choose a parameter
arrow keys or external keyboard: change parameters:

Name:
an individual name for this method
Angle:
measurement angle
Rep:
number of repetitions
CapSys:
measuring system used for this method
F4 <Save>:
F3 <Insert>:
F5 <Overw.>:
F1 <Back>:
displays your entries

includes the new method
overwrites an existing method
skips back in case you want to change the entries again
The option F5 <Overw.> (Overwrite) is only available after you edited a previously
existing method.
B80IB01
33
8.2.2
Measuring System
In the submenu "Measuring System" you can create, revise or delete a

measuring system.
SETUP: Measure-MeasSystem
->
1/05
11:04:31
Cap
:11118183-70A
K1
:1.28800e-02
CapSys
:1.6/1.500
Ball Dens:7.8500e+00
Back
1999-07-22
14:41:00
New
1/05:
F4 <Enter>:
F2, F3 arrow keys:
F5 <Enter>:
F5 <Edit>:
F3 <Delete>:
F1 <Back>:
the first of five stored measuring systems is displayed

enter a new measuring system
browse all stored measuring systems
choose the preferred measuring system to then press:
to make changes
to delete or
to go back
Entering a measuring system:
SETUP: EDIT MeasSystem
SerNo
Angle
K1
CapSys
ESC
11:04:46
.......
Save
F5 <Enter>:
choose a parameter
arrow keys or external keyboard: change parameters:
SerNo:
8 digit serial number (engraved in the capillary)
Angle:
measurement angle
K1:
calibration constant K1
CapSys:
measuring system (capillary-/ball diameter)
B-Dens:
density of the ball
Date:
date of calibration
Time:
time of calibration
F4 <Save>:
F3 <Insert>:
F5 <Overw.>:
F1 <Back>:
displays your entries

inserts the new measuring system
overwrites an existing measuring system
skips back in case you want to change the entries again
The option F5 <Overw.> (Overwrite) is only available after you edited a previously
existing measuring system.
34
B80IB01
8.3
Menu "Print Configuration"
In the third submenu of "MENU" "Print Configuration", you can print the
configuration of AMVn.
The printer has to be attached to the selected connection
(default selection: COM 2).
PRINT: Configuration
11:12:02
Printing on COM2
Please wait
ESC
F5 <Enter>:
<ESC>:
starts the print

cancels the print job
You can find the settings for the printer interface in Chapter 8.1.4.
Example of a printout
(numbers and values are different on every instrument):
AMVn Microviscometer
SNo: 409247
SW_Ver: V1.70
---------- CONFIGURATION ----------SW-Version V1.70

Date: 2006-06-10, Time: 09:12:05
Serial Number: 409247
Zero adjust: 27592
Runtime-Limit: 250 s
Instrument-Constant: 1.000
ADC
: A = 0.9928
Pt100-factors: KA= 0. 0568
KB= 0.0035
Coil 1: Ampl= 25, Phase= 37, U= 138
Printer on COM2
DelayChar/Char: OFF; Line/Line: 1.0s
Settings: 9600 / 7 / even / 1
B80IB01
35
9 Calibration of Measuring Systems

For a precise viscosity determination, the calibration of the capillary is necessary.
The calibration constant is different at every angle and with every capillary.
9.1
Calibrated and Uncalibrated Capillaries
There are calibrated and uncalibrated measuring system sets (Chapter 4.2.2) and
calibrated and uncalibrated capillaries:
Calibrated capillary: calibrated at certain angles and a certain temperature

before delivery. The data is stored on a data medium and on the calibration
certificate. Both is delivered. Manually enter the calibration constant data
stated on the calibration certificate in the firmware, menu "Setup
Measurement" (also see Chapter 8.2). Import the calibration constant from
the data medium in the Visiolab software.
Uncalibrated capillary: determine the calibration constant acc. to

calibration procedure and store this value in the menu "Setup
Measurement" (Chapter 8.2).
When using a new or alternative ball set the calibration constant only needs to
be redefined in case the measuring deviation is above tolerance limit (0.3 %) and/
or the ball set features a different batch number. Read the batch number on the
sticker attached to your ball set.
When calibrating a measuring system, choose the viscosity standard in such a
way that it falls within the viscosity range of the measurement at the usual
measuring temperature (Chapter A.1).
9.2
Menu Calibration
Calibrate or recalibrate a measuring system in the menu "Setup Measurement"

"Measuring System: Calibrate".
SETUP: Measure-MeasSystem-Calib
->
1/05
Back
F2, F3:
F4 <New>:
F5 <Enter>:
1/05:
36
Cap
:11118183-70A
K1
:1.28800e-02
CapSys
:1.6/1.500
Ball Dens:7.8500e+00
11:04:31
1999-07-22
14:41:00
New
browse all stored measuring systems and check all values
calibrate a new measuring system
choose the measuring system you wish to recalibrate
the first of five stored measuring systems is displayed
B80IB01
9.3
Calibrating a New Measuring System
1. Press F4 <New>.
2. Enter all values:
SETUP: EDIT MeasSystem Calib
SerNo
Angle
K1
B-Dens
ESC
SerNo:
Angle:
CapSys:
B-Dens:
S-Name:
S-Rem:
S-Visc:
S-Dens:
Temp:
Rep:
11:06:39
.......
Cont
8-digit serial number (engraved in the capillary)
measurement angle
measuring system (capillary-/ball diameter)
density of the ball (e.g. steel ball = 7.85 g/cm3)
name of calibration medium
remark on calibration medium
dyn. viscosity of calibration medium at the chosen temperature
density of calibration medium at the chosen temperature
temperature for the calibration medium values
number of repetitions for the calibration
F5 <Enter>:
F2, F3, F4 arrow keys:
F4 <Cont>:
F3 <Insert>:
F5 <Overw.>:
F1 <ESC>:
edit a value
make entries
continue
insert measuring system
overwrite an existing measuring system
return to previous screen
3. Fill the capillary with the suitable viscosity standard fluid (Chapter A.1).
4. Press F5 <Start> to start the calibration.
The calibration procedure runs automatically.
5. After measurement conclusion press:
F2, F3:
view the detailed evaluations
F5 <Print>:
print the result
F4 <Save>:
save to use the calibration constant in measurements.
Information:
If you do not save the calibration constant K1, you lose all calibration results.
B80IB01
37
10 Maintenance
10 Maintenance
Clean AMVn and its accessories regularly.
We recommend regular maintenance of your measuring instrument by authorized
Anton Paar GmbH personnel.
10.1 Cleaning the Measuring System

A thorough cleaning of the AMVn measuring system after each measurement or
measurement series is imperative.
Caution:
Do not leave any samples in the measuring system after finishing the
measurement.
Rinse the measuring system with a suitable cleaning agent.
Only use cleaning agents that are compatible with the materials (Chapter
10.4).
Before you dry the capillary with compressed air, remove the ball.
1. Remove the protective cap and clean it if necessary.
2. Remove the capillary from the the capillary block. Take care not to twist the
capillary.
3. Remove the LUER plug and insert a syringe into the filling adapter.
4. Now remove the LUER cap and rinse the capillary with cleaning agent.
Repeat the rinsing procedure several times by flushing out and drawing up
the cleaning agent.
5. After the cleaning procedure remove the syringe and the filling adapter.
6. Use a volatile solvent, e.g. highly concentrated alcohol or acetone, to
accelerate the drying procedure after cleaning.
7. Dry the measuring system e.g. with compressed air (max. 0.5 bar).
8. Check that the ball moves easily when the capillary is swiveled. This
concludes the cleaning procedure.
10.2 Cleaning the Filling Adapter

Clean the filling adapter regularly to avoid clotting or the ball getting stuck.
1. Detach the filling adapter from the capillary with gentle turns. Do not use
excessive force as this could break the capillary.
2. Rinse the filling adapter with a cleaning agent.
3. Rinse the filling adapter with a volatile solvent, e.g. highly concentrated
alcohol, to accelerate the drying procedure after cleaning.
4. Afterwards dry the filling adapter, e.g. with compressed air (max. 0.5 bar).
38
B80IB01
10 Maintenance
10.3 Cleaning AMVn
Use a soft cloth and warm water to clean the casing and display.
Dry the AMVn instrument with a soft, dry cloth.
Wash the drip plate regularly with a suitable cleaning agent.
Regularly unscrew the thermostat and rinse it with cleaning agent.
Check the capillary block for pollution and clean it regularly, especially at the
thermostat and protective cap fixations.
Never remove the warning signs on the capillary block. If these come loose,
they need to be attached again.
10.4 Wetted Parts of AMVn

The following items have contact to the measured samples and cleaning agents:
Item
B80IB01
Material
Capillary
Borosilicate glass
Ball
Steel 1.4125 (AISI 440C)
Filling adapter
PCTFE
O-ring
Viton
O-ring
Kalrez
LUER cap
PCTFE
LUER plug
PCTFE
39
10 Maintenance
10.5 Replacing O-rings in the Filling Adapter

The filling adapter already contains the O-rings at delivery. Always replace both
interior O-rings at the same time.
10.5.1
Filling Adapter Without Engraved Marking Ring

Viton
Silicone
Fig. 10. 5
O-rings for the filling adapter without engraved marking ring
The O-rings on the inside are made of viton and have the dimension
6.5 x 1.5 mm FPM 80. They have contact to the sample and have a sealing
function.
10.5.2
Filling Adapter With Engraved Marking Ring

Viton or
Kalrez
O-rings
Engraved
marking ring
Silicon e
Fig. 10. 6
O-rings for the filling adapter with engraved marking ring
The filling adapter with engraved marking ring contains O-rings of the dimension
6.4 x 1.9 mm FPM 75. In this filling adapter with engraved marking ring O-rings
made of viton and made of Kalrez can be used.
Kalrez-O-rings should be used if viton is not resistant against the measured
sample. You can optionally order it (Chapter 4.2.3).
10.5.3
Exchanging the O-rings
Caution:
The filling adapter without engraved marking ring and the filling adapter with
engraved marking ring are NOT compatible.
The O-rings have another dimension (see Chapter 4.2.2 and Chapter 4.2.3).
The red, outer O-ring is made of silicone and does not usually need to be
exchanged. The inner O-rings are sealing rings. If the O-rings need to be
replaced, first remove them from the adapter using the O-ring tool. Then carefully
insert the new O-rings.
40
B80IB01
11 Technical Data
Time measuring range:
Resolution:
Accuracy:
0 - 250 s (999 s *)
0.001 sec
<0.002 sec
Viscosity range:
Repeatability:
Reproducibility:
0.3 - 2500 mPa.s (20000 mPa.s *)

<0.1 %**
<0.5 %***
Temperature range:
Resolution:
Accuracy:
+5 C to +135 C
0.01 C
<0.05 C
Mains connection:
85 to 264 VAC, 50 to 60 Hz, 75 VA
Dimensions (W x H x D): 290 x 340 x 330 mm

Weight:
15 kg (150 N)
Ambient temperature:
15 to 35 C
Air humidity:
10 to 80 % relative humidity for temperatures

up to 31 C, decreasing linearly to
67 % relative humidity at 35 C
More detailed information about AMVn specifications are available on request.
41
*)
with measuring range extension (see Chapter Appendix B:)
**)
typical value, provided the ball is not changed
***)
typical value for the range, where the calibration constant was determined
B80IB01
Appendix A: Viscosity
For a precise viscosity determination, a suitable calibration standard fluid is
required for the calibration of the capillaries. A calibration constant needs to be
determined and/or entered for every capillary (Chapter 9).
Information:
The calibration procedure has to be repeated periodically, depending on the
specific accuracy requirements of your laboratory.
A.1
Viscosity Standard Fluids
Due to the different measuring ranges of the capillaries, you need different
viscosity standard fluids. You can order these viscosity standard fluids at Anton
Paar GmbH.
The table below shows general values for the different measuring systems.
The best results are achieved if you calibrate a measuring system at the usual
measuring temperature and in its viscosity range.
(e.g. if you measure approx. 50 mPa.s with a 3.0 measuring system at 100 C,
use e.g. the viscosity standard fluid DKD 10000. At 100 C this standard has
approx. 57 mPa.s).
For measuring aqueous samples we recommend bidistilled water as a viscosity
standard fluid.
Viscosity value for calibration [mPa.s]
20 C
40 C
100 C
Capillary [mm]
Capillary [mm]
Capillary [mm]
1.002
0.9 / 1.6
0.6529
0.9 / 1.6
---
33
1,8 / 3,0
15
1.8
100
3.0 / 4.0
Viscosity standard fluid
Mat. No.
Bidistilled water
26750
3.1
1.6 / 1.8
Viscosity standard fluid SH M
12935
38
1.8 / 3.0
6.2
1.6 / 1.8
Viscosity standard fluid SH C
9754
1100
4.0 / 4.0 WK/KO*
330
4.0
32
1.8 / 3.0 / 4.0
Viscosity standard fluid SH H
12936
7900
4.0 WK/KO*
1500
4.0 / 4.0 WK/KO*
57
1.8 / 3.0 / 4.0
DKD 10000AW
301364
* for extended measuring range

Choose the appropriate temperature (according to the calibration certificate) to
reach the recommended viscosity for calibration.
A custom-tailored calibration is possible. You can use any stable sample with
known dynamic viscosity and density as a viscosity standard fluid.
B80IB01
42
A.2
Calibration Constant K1
For every measuring angle you plan to use, first determine the calibration
constant K1.
N
K 1 = ----------------------------------t1(K N )
K1
N
t1
K
N
calibration constant of the measuring system [mPa.cm3/g]

dynamic viscosity of the viscosity standard fluid [mPa.s]
Rolling time of ball [s]
Density of ball [ 7.85 g/cm3 ]
Density of the viscosity standard fluid [ g/cm3 ]
Information:
The calibration constant is different at every angle and with every
capillary.
A calibration datasheet with pre-determined calibration constants for the
stated angles is enclosed with every calibrated capillary.
If a ball is exchanged, K1 only needs to be readjusted if the measuring
deviation is above the tolerance limit (0.3 %). Readjust the constant if you
use balls with different batch numbers. The batch number is written on the
ball vessel.
The viscosity of the standard fluid should fall within the viscosity range of
the measured samples.
A.3
Determining the Viscosity
The dynamic viscosity of the sample is calculated from the calibration constant
K1 of the measuring system, the rolling time t1 and the density difference
between ball and sample.
= K1 * (K - P) * t1
K1
K
P
t1
...
...
...
...
...
dynamic viscosity of sample [mPa.s]

calibration constant of the measuring system [mPa.cm3/g]
ball density [ g/cm3] (steel ball = 7.85 g/cm3)
density of the measured sample [ g/cm3]
ball rolling time [s]
The serial number and the ball density of the measuring system are known (steel
ball: K = 7.85 g/cm3, tungsten carbide-cobalt ball: K = 15 g/cm3). The density of
the sample, often a known number, must also be entered.
If there is no information on the density of the sample to be measured, you can
order a manual density meter DMA 35N from Anton Paar GmbH, which measures
the density with an accuracy of +/- 0.001 g/cm3.
Caution:
Choose the angle of your measurement in such a way that the ball rolling
times do not drop below 10 sec. Otherwise turbulence is caused in the
capillary and a seemingly higher viscosity is read.
43
B80IB01
Appendix B: Extension of the Measuring Range
Appendix B: Extension of the Measuring

Range
B.1
Quadrupling the Maximum Measuring Range
A measuring range extension through an increase in run time from 250 to 999 sec
quadruples the maximum measuring range.
The run time increase can only be defined by means of a "remote" command from
the PC.
Proceed as follows:
1. Connect AMVn and PC with the interface cable.
2. Switch on your AMVn and the PC.
3. Start the Windows Terminal Program
PC port: 9600, 8 databit, no parity, 1 stop bit, no handshake.
4. The following commands, which need to be typed using capital and small
letters, define the max. runtime to 999 sec:
<REM
<STATUS 00000>
<setrlim = 999>
Runtime-Limit = 999
<LOC
OK
5. End the Terminal Program.
6. Check with the printer in menu Print Configuration.
7. Check the print:
AMVn Microviscometer
SNo: 80074021
SW_Ver: V1.70
---------- CONFIGURATION ----------SW-Version V1.70

Date: 07/21/2006, Time: 11:12:05
Serial Number: 80074021
Zero adjust: 27471
Runtime-Limit: 999 s
Instrument-Constant: 1.000
ADC
: A = 0.9928
Pt100-factors: KA= 0. 0568
KB= 0.0035
Printer on COM2
DelayChar/Char: OFF; Line/Line: 0.5s
Settings: 9600 / 7 / even / 1
B80IB01
44
Appendix B: Extension of the Measuring Range
B.2
Doubling the Maximum Measuring Range
A measuring range extension through the use of tungsten carbide-cobalt balls

doubles the maximum measuring range, as they have approx. twice the density
(15 g/cm) and therefore half the runtime.
Before calibrating the measuring system 4.0 with tungsten carbide-cobalt balls,
read Chapter 9 and proceed accordingly.
Proceed as follows:
1. Select capillary 4.0 mm.
2. Insert 3 mm tungsten carbide-cobalt balls.
3. Fill the capillary with viscosity standard fluid and start the calibration.
Save the calculated calibration constant for the measuring system 4.0.
45
B80IB01
B80IB01
F1
F1
Menu
F5
F1
Capillary Ser. No.

K1
Calibration Date
Capillary System
Instrument Constant K2
Temp. Equi-Mode
Meas. System:
Instr. Settings:
F5
Date
Time
Zero adjust
Temperature equilibration
Instrument Constant K2
Default Settings
Configuration Printer
Info
Service Utilities
Software Update
Name
Angle
Repetitions
Capillary System
Method:
F2
Name
Remark
Temperature
Density
Sample:
Setup Instrument
F2 F3
actual SETTINGS
Initialization
Start
F5
F1
Setup Temp. Equilibration
Appendix C: Menu Tree Firmware Structure
Appendix C: Menu Tree Firmware

Structure
46
47
F5
F1
F4
F1
New Run
Evaluation
F5
F1
F5
F1
F2 F3
F2 F3
F5
Sample Name
Remark
Density
Temperature
Temp. Equi
Method
Measuring System
Start
RUN - Temp Equi
Repetition Times: discrete run times
Angle / Method
Repetitions
Temperature
Density
Mean
Time
St.Dev.
Var. Co.
Kin. Visco.:
1/2
2/2
F1
F1
Meas. System: Calibrate
Mean
Time
St.Dev.
Var. Co.
Infos:
F1
Measuring System
Method
Dyn. Visco.:
Print Configuration
F2 F3
Setup Measurement
F1
F2
F1
Start Time
Capillary SerNo.
K1
Capillary System
Stop measurement
Show runtimes
Setup: Measure-MeasSystem-Calib
Setup Temp. Equilibration

Print Measuring Systems
Setup: Measure-Method
Print Methods
RUN
F5
F4
F1
F4
F5
F5
Appendix C: Menu Tree Firmware Structure
B80IB01

Viscometer Manual

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Instruction Manual

Firmware Version: 1.7x

Anton Paar GmbH

Document no.: B80IB01O.fm

General Safety Instructions ..................................................................................................... 9

Installation and Use .................................................................................................. 9

Maintenance and Service......................................................................................... 9

Precautions for Highly Inflammable Samples and Cleaning Agents ...................... 10

Warning Symbols on the AMVn Instrument............................................................................11

Unpacking Supplied Items ..................................................................................................... 13

Checking of Supplied Items ................................................................................................... 13

Supplied Parts ....................................................................................................... 13

Accessories in the Measuring System Set ............................................................. 14

Available Measuring System Sets .......................................................... 14

Content of a Measuring System Set ....................................................... 15

Optional Accessories ............................................................................................. 16

Rear Side of AMVn ............................................................................................................... 17

Measuring System ................................................................................................................ 18

Monitor and Function Keys .................................................................................................... 18

6 Putting AMVn into Operation........................................................................................................ 19

Activating AMVn .................................................................................................................... 19

Preparing the Measurement .................................................................................................. 20

Introducing the Ball to the Capillary ....................................................................... 20

Attaching the Filling Adapter .................................................................................. 20

Filling the Capillary ................................................................................................. 21

Attaching Temperature Tube .................................................................................. 21

Mounting the Capillary into the AMVn Instrument .................................................. 22

Attaching Protective Cap........................................................................................ 22

Starting the Measurement...................................................................................................... 24

Thermostatting the Capillary Block......................................................................... 24

Sample Thermostatting .......................................................................................... 24

Measuring the Sample ........................................................................................... 25

Displaying the Measured Values ........................................................................................... 25

Printing the Measured Values................................................................................................ 26

Cleaning the Measuring System............................................................................................ 27

8 AMVn Firmware Update................................................................................................................. 28

Menu "SETUP Instrument" ................................................................................................. 28

Date and Time ........................................................................................................ 28

Temperature Equilibration ...................................................................................... 29

Temperature Equilibration in "constant mode" ........................................ 29

Temperature Equilibration in "auto mode"............................................... 29

Default Settings ...................................................................................................... 30

Printer Configuration .............................................................................................. 30

Zero Point Adjustment............................................................................................ 31

Menu "SETUP Measurement" ............................................................................................ 32

Menu "Print Configuration" ................................................................................................. 35

9 Calibration of Measuring Systems ............................................................................................... 36

Calibrated and Uncalibrated Capillaries ................................................................................ 36

Calibrating a New Measuring System.................................................................................... 37

Filling Adapter Without Engraved Marking Ring .................................................... 40

Filling Adapter With Engraved Marking Ring ......................................................... 40

Exchanging the O-rings.......................................................................................... 40

11 Technical Data ................................................................................................................................ 41

Extension of the Measuring Range.......................................................................... 44

Menu Tree Firmware Structure.............................................................................. 46

1 About the Instruction Manual

1 About the Instruction Manual

Warning! Hot surface:

Read the instruction manual at hand before using AMVn.

Follow all hints and instructions contained in this instruction manual to

Anton Paar GmbH only warrants the proper functioning of AMVn if no

Installation and Use

AMVn is not an explosion-proof instrument and therefore must not be

The installation procedure should only be carried out by authorized