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ABSTRACT
A study was undertaken to optimize the parameters for particle size analysis through laser diffraction
techniques. Fifty soil samples with varying soil texture, organic matter, sesquioxide content and
calcareousness were collected and analyzed for soil texture by conventional (International Pipette
Method-IPm) and Instrumental (Particle Size Analyser-PSA) methods. The study reveals that PSA is
more accurate and preferable compared to IPm in determining the soil particle sizes. The clay content
of the different samples estimated by International Pipette method and by Particle size analyzer varied
from 0.9 to 48.4% and 0.35 to 41.2 %, respectively. PSA showed a good agreement (72% samples)
for silt size fractions, and a slight shift in the upper limit of clay from conventional size of 2 m could
help in analysis of soil texture by PSA.
Keywords: Soil texture, international pipette method, particle size analyser
INTRODUCTION
Soil texture is a qualitative classification tool
used in both field and laboratory to determine
classes for agricultural soils. The classes are
distinguished in the field by the textural feel which
can be further clarified by separating the relative
proportions of sand, silt and clay using grading
sieves. The class is then used to determine crop
suitability and to approximate the soils responses
to irrigation and management practices. Traditional
particle size determination techniques include
sieves for the larger size ranges, usually above
63m (230 mesh size). Sieves are limited in
resolution (number of sieves = number of data
channels), they are slow and operator intensive, and
has limitation for determining the smaller size
classes. Pipette or sedimentation method is
generally used for the finer fractions; however, this
technique is slow and is affected by particle shape.
Modern automated analytical techniques are
used for sizing sediments which includes laser
Original aticle
78
79
X 100
Where,
a = per cent of clay / silt / sand determined
through International Pipette method.
b = per cent of clay / silt / sand determined
through Particle Size Analyzer.
80
1
18.4
2
23.4
3
48.4
4
5.9
5
35.9
6
48.4
7
23.4
8
20.9
9
20.9
10
3.4
11
25.9
12
5.9
13
5.9
14
18.4
15
23.4
16
0.9
17
10.9
18
20.9
19
5.9
20
10.9
21
35.9
22
20.9
23
20.9
24
25.9
25
43.4
26
45.9
27
10.9
28
20.9
29
15.9
30
3.4
31
28.4
32
8.4
33
10.9
34
15.9
35
5.9
36
10.9
37
20.9
38
15.9
39
10.9
40
18.4
41
15.9
42
10.9
43
23.4
44
5.9
45
20.9
46
8.4
47
13.4
48
18.4
49
13.4
50
15.9
Mean 18.3
S.D.
11.5
C.V. 130.5
% Silt
% Sand
7.5
17.5
17.5
17.5
15.0
10.0
7.5
17.5
10.0
7.5
2.5
2.5
5.0
20.0
10.0
10.0
5.0
10.0
5.0
10.0
15.0
5.0
5.0
20.0
10.0
10.0
10.0
7.5
5.0
4.0
10.0
5.0
2.5
17.5
2.5
5.0
2.5
2.5
7.5
2.5
15.0
7.5
10.0
10.0
15.0
10.0
17.5
17.5
2.5
15.0
9.5
5.4
28.6
70.6
57.6
32.2
76.5
44.9
37.3
65.1
59.5
63.9
85.3
70.6
90.7
85.8
54.2
62.0
87.7
82.6
64.4
88.2
76.6
43.3
71.2
70.4
53.1
46.0
44.0
72.7
65.5
78.6
89.0
57.1
84.6
82.4
59.2
89.0
77.4
73.2
78.3
78.3
78.4
65.6
77.4
64.6
79.4
63.5
73.1
64.7
59.5
83.6
68.7
68.9
14.4
202.3
81
% Clay
% Silt
% Sand
10.5
25.9
35.3
6.7
25.8
37.7
10.4
11.5
9.9
1.6
11.1
2.5
1.8
2.0
10.0
6.9
6.8
11.4
0.4
6.1
41.2
11.8
15.7
10.0
9.2
23.2
8.7
13.2
6.6
2.5
20.5
3.8
6.3
11.8
6.5
5.5
9.4
9.3
7.7
7.9
21.1
5.8
14.3
4.9
8.3
10.7
13.7
5.2
2.2
5.3
11.1
9.1
80.6
23.5
21.9
33.5
15.9
25.5
30.1
15.6
18.2
14.3
5.8
23.3
11.0
9.8
22.8
27.1
16.6
16.6
22.8
8.3
14.5
21.7
26.2
25.3
20.3
29.0
32.5
22.3
20.8
16.3
10.1
26.6
11.0
13.3
26.6
14.8
18.3
16.3
22.1
20.3
11.6
23.5
23.7
20.2
13.1
16.7
17.2
23.5
14.0
9.7
14.7
19.2
6.5
41.0
65.9
52.2
31.2
77.4
48.7
32.2
74.0
70.3
75.8
92.6
65.6
86.5
88.5
75.2
62.9
76.4
76.6
65.8
91.3
79.4
37.1
62.0
59.0
69.7
61.8
44.3
69.0
66.1
77.1
87.5
53.0
85.2
80.5
61.6
78.7
76.2
74.3
68.7
72.0
80.6
55.5
70.5
65.5
82.0
75.0
72.1
62.8
80.8
88.1
80.0
69.7
14.3
200.1
12
12
19
7
6
2
7
2
50
17
37
29
CONCLUSIONS
ACKNOWLEDGEMENT
The authors sincerely thank M/s Metrohm India
Limited, Chennai for providing technical assistance
and laboratory facilities to carry out the study.
REFERENCES
Cooper LR, Haverland RL, Vendricks DM, Knisel WG (1984).
Microtac particle-size analyzer: An alternative particlesize determination method for sediment and soils. Soil
Sci 138:138146
Eshel G, Levyb GJ, Mingelgrinb U, Singera MJ (2004). Critical
evaluation of the use of laser diffraction for particlesize distribution analysis. Soil Sci Soc Am J 68(3):
736-743
Hesse PR (1971). A Text Book of Soil Chemical Analysis.
John Murray Ltd 10362
ISSS (International Society of Soil Science) (1929). Minutes
of the First Commission Meetings. International
Congress of Soil Science, Washington 1927.
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83