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Department of Materials Science and Engineering, The Pennsyl6ania State Uni6ersity, Uni6ersity Park, PA 16802 -5006, USA
b
Na6al Surface Warfare Center, Indian Head, MD 20903, USA
c
Na6al Surface Warfare Center, Carderock, MD, USA
Received 27 June 2000; received in revised form 10 October 2000
Abstract
The influence of temperature and strain rate on the deformation and failure behavior of HY-100 steel has been examined as a
function of stress state using notched and un-notched axisymmetric tensile specimens. Behavior over the range of temperatures/
strain rates from 85C and 1 s 1 to 27C and 10 3 s 1 shows an equivalence of decreasing test temperature or increasing
strain rate on deformation behavior in a manner that can be predicted by the thermally activated flow theory. Over the entire
range of temperatures/strain rates, the influence of stress state on failure is such that two void coalescence mechanisms control
failure; at low stress triaxialities, relatively equiaxed voids grow to impingement, while at high triaxialities, a void-sheet process
intervenes linking elongated MnS-initiated voids by a shear instability. The failure strains decrease rapidly with increasing stress
triaxiality ratio in a similar manner for all temperatures and strain rates except for an intermediate stress triaxiality condition
where the void-sheet mode of failure extends to lower stress triaxialities under cryogenic test conditions. 2001 Elsevier Science
B.V. All rights reserved.
Keywords: Fracture; Temperature; Strain rate; Stress state; Failure behavior; HY-100 steel
1. Introduction
An accurate description of the deformation and failure response of structural materials over a wide range
of loading conditions is critical to the success of computational models that predict material failure under inservice conditions. To that end, several constitutive
models have been developed to describe the deformation
behavior of materials as a function of temperature and
strain rate. Prominent examples of such models include
the mechanical threshold model (MTS) [1 4], the Johnson Cook model [5], and the Zerilli Armstrong model
[6]. Utilizing a number of constants, these models are
able to link the flow stress to temperature, strain rate,
and strain by fitting the constants to stress strain data
over a range of temperatures and strain rates. In addi* Corresponding author. Tel.: +1-814-8655447; fax: + 1-8148652917.
E-mail address: koss@ems.psu.edu (D.A. Koss).
1
Present address: Siemens Westinghouse Power Corp., Orlando,
FL 32826, USA.
0921-5093/01/$ - see front matter 2001 Elsevier Science B.V. All rights reserved.
PII: S 0 9 2 1 - 5 0 9 3 ( 0 0 ) 0 1 8 3 2 - 3
198
Table 1
Composition of HY-100 steel base plate used in the study
Element
Mn
Si
Ni
Cr
Mo
Cu
Wt.%
0.16
0.26
0.008
0.009
0.22
2.62
1.32
0.25
0.14
Tensile testing at cryogenic temperatures was performed at 85 and 40C and at strain rates of
either 10 3 or 1 s 1. To calculate the cross-head speed
required to produce the desired initial strain-rate, the
effective gauge length of the notched specimen was
assumed to be roughly equal to the radius of curvature,
z. This assumption is based on finite element analysis
that showed that the axial strain in the notch decreases
rapidly at distances of approximately 9 0.5z from the
minimum diameter section for all specimen geometries
[10].
Material failure in this study is defined as that condition in which the material damage is sufficiently severe
such that the stress-carrying capacity is measurably
degraded. Thus, using the procedure described elsewhere [7,8], failure initiation was determined experimentally as that point at which the load-diametric
contraction curve showed an abrupt drop during the
tensile test. This test procedure had the sensitivity to
detect roughly a 2% load loss due to damage accumulation, which is consistent with a 3% area fraction of
microvoids present on the fracture surfaces of specimens that were strained to failure and subsequently
fractured by cleavage at liquid nitrogen temperatures
[8]. In addition to the determination of failure strains,
fracture strains, mf, were also calculated using initial, do,
and final diameter, df, measurements taken from the
broken tensile specimens and using the expression: mf =
2 ln(do/df).
Fig. 1. Elongated MnS inclusion present within the tempered martensite microstructure of the HY-100 steel.
199
Fig. 2. Stress strain behavior of HY-100 steel under five test conditions. Data at 25C and 4700 s 1 is from Ref. [4].
200
in failure strains with decreasing temperature. In addition, at a given temperature, the results in Fig. 3a show
no effect of strain rate on failure; the failure strains at
10 3 s 1 strain rate are the same as those at 1 s 1 for
a given specimen geometry.
The fracture strains, as determined from the initial
and final diameters of the specimens, are shown in Fig.
3b for quasi-static strain rates over a range of temperatures as well as for dynamic strain-rate tests of notched
specimens at 25C. As in the case of the failure strains,
the fracture data in Fig. 3b reveal that at intermediate
(A-notch) to high (D-notch) stress triaxialities the fracture strains are not sensitive to temperature or strainrate, even at high strain rates of :103 s 1. At low
stress triaxialities (B-notch), however, there is a slight
decrease of the fracture strains with decreasing temperature, as was observed in the case of the failure strain
data.
In summary, these ductility data show that, except
for the intermediate stress triaxiality (B-Notch) specimens, both the failure and the fracture strains show no
sensitivity to temperature or strain rate for a given
notch geometry over the range of conditions from 10 3
s 1 and 25C to 1 s 1 and 85C. In the case of the
Fig. 4. A failure limit diagram showing the equivalent plastic strainto-failure and average stress triaxiality ratio combinations at failure
initiation for HY-100 steel.
3.3. Fractography
Fig. 3. The dependence of (a) the fracture strain and (b) the failure
strain on test temperature and strain-rate. See text for definitions of
fracture and failure strains.
Based on failure at room temperature under quasistatic strain rates [7,8], previous research has identified
void coalescence by the void-sheet mechanism as the
process controlling the Region II failure in Fig. 4. In
the present study, fractography performed for a wide
range of temperatures/strain rate conditions (Fig. 5),
indicates that the fracture process for Region II continues to involve the void-sheet linking of elongated voids
nucleated at large MnS ( 15 75 mm long) stringers.
For example, fractographs taken in the failure initiation
regions of the high stress triaxiality (D-Notch) specimens tested over a wide range of conditions, such as at
the 85C and 1 s 1 and 25C and 10 3 s 1 cases
shown in Fig. 6(a,b), indicate failure due to void linking
by a void-sheet mechanism. Fig. 6 as well as profile
views of the fracture surface depict shear planes connecting the large, elongated MnS-stringer-nucleated
voids and forming a ridge trough profile [7,8].
As analyzed by Bandstra et al., void-sheet failure is a
result of a localized shear instability that develops
between the two neighboring, elongated primary voids
[12,13]. The void-sheet deformation localization process
also results in the eventual nucleation of secondary
microvoids within the deformation localization band
joining the primary voids. Thus, Fig. 5 also shows the
presence of (a) secondary microvoids of a few microns
in size nucleated at equiaxed MnS particles near the
primary voids and (b) even smaller microvoids ( 1 mm
in diameter) nucleated at smaller, equiaxed (presumably) carbide particles.
201
202
Fig. 6. Fractographs from the failure initiation region revealing extensive void-sheeting in the failure initiation region of a high stress triaxiality
specimen (D-notch) tested at (a) 25C and 10 3 s 1, (b) 85C and 1 s 1. In contrast (c) shows coalescence of equiaxed voids in a low
triaxiality specimen (B-notch) tested at 25C and 10 3 s 1, but (d) extensive void-sheeting between elongated voids in the same B-Notch specimen
configuration when tested at 85C and 1 s 1.
(1)
Table 2
A summary of the fractography for all of the test conditions
Room temperature
(103 s1 and 103 s1)
40C
(1 s1)
85C
(103 s1 and 1 s1)
Extensive void-sheeting; no
cleavage
|m
(A-Notch); mf
|
unaffected
|m
(B-Notch); mf decreased at
|
low m; and temperature
Medium
Low
Eq. (1) has the form similar to the void growth model
of Rice and Tracey [16] and has been used previously in
similar forms to correlate the tensile ductile fracture
data for many different materials [5,8,14,19,20]. It will
be recalled that the Rice Tracey void growth analysis
assumes an isolated spherical void and neglects void
interactions, and that the analysis predicts a value of
the exponent D of 1.5 [16].
Fig. 7 shows that the stress-state dependence of the
failure of HY-100 steel can indeed be predicted for a
wide range of temperature/strain rates by a relationship
of the form given by Eq. (1), pro6ided that the data are
separated into Regions I and II. However, as is observed for this steel at room temperature [8], the D-values obtained when fitting Eq. (1) to the experimental
data are significantly higher than that predicted by the
Rice Tracey analysis (experimentally, D = 2.7 for Region I and D =2.3 for Region II, which compares to
the D = 1.5 predicted [16]).
There are several possible causes for the difference in
D-values between the Rice Tracey prediction of 1.5
and the observed values of 2.3 2.7. It is possible that,
despite the small volume fraction of voids (51 2%)
just prior to failure [18], significant void void interactions occur and accelerate void growth, increasing the
D-value. However, given the small inclusion content of
this steel (volume fraction:0.00015) the inclusion-nucleated voids would have to interact at distances in
excess of 10 void diameters. Recent computational
modeling of void-sheet mode of failure indicates strong
void interactions can in fact occur between cylindrical
voids 2.5 mm in diameter but spaced 70 mm apart
(approximately 28 void diameters) [11,12]. In addition,
recent experimental measurements of damage accumulation during ductile fracture of HY-100 steel show the
presence of a rapid void growth stage initiating at 5 1
vol.% voids, which also suggests stronger than predicted interactions between widely separated voids [18].
Thus, we conclude that the use of a relationship such as
Eq. (1) is a reasonable approach to predicting the
stress-state dependence of failure of steels such at HY100 even though significant void interaction effects
appear to be present.
203
The tensile failure behavior (i.e. the mechanical conditions at failure at different stress states as well as the
underlying void coalescence mechanisms) of HY-100
steel is, for the most part, insensitive to strain-rates
over six orders of magnitude in strain rate and to
temperatures ranging from 25 to 85C. The only
significant effect on ductility occurs at an intermediate
stress triaxiality ratio in which there is a small decrease
in failure strains at high strain rates/low temperatures.
That ductility decrease is associated with void coalescence as a result of a void-sheet process in which the
high strain-rate/cryogenic temperature condition favors
a deformation localization between elongated inclusioninitiated voids.
When the failure data are taken as a whole, the
dependence of the failure strains on stress state can be
adequately predicted by a relationship of the form
previously developed by Rice and Tracey for void
growth [16]. Such a relationship is consistent with void
nucleation occurring at sulfide particles at small strains
in this steel, and, although the form of the relationship
suggests the presence of void interaction effects, its use
implies a critical void volume fraction or critical void
growth rate as a failure criterion.
Acknowledgements
The authors are very grateful to Carl Cady, Rusty
Gray, Rich Thissel, Shuh-Rong Chen, Mike Lopez, and
Manny Lovato at the Los Alamos National Laboratory
for their generous assistance in performing the mechanical tests at cryogenic temperatures. We also wish to
acknowledge many discussions with Dongchul Chae.
This research was supported by the Office of Naval
Research.
4. Summary
Relying on constants developed based on room temperature deformation behavior, the MTS model predicts the cryogenic stress strain response of HY-100
steel with reasonable accuracy. Specifically the model
predicts that the stress strain behavior at 40C and
1 s 1 and 85C and 10 3 s 1 should be equivalent
as should that at 85C and 1 s 1 and 25C and 7290
s 1; our experimental observation agree fairly well with
these predictions.
204
Table 3
HY-100 steel MTS model parameters used for determining the appropriate cryogenic temperature to emulate a dynamic test at 100 s1
Parameter
Value
Units
Sj (m; , T)=
|a
vo
k/b 3
m; oi
goi
qi
pi
| i
m; om
gom
qm
pm
qo
a
goms
| mso
m; oms
50
7.146104
0.9047
1109
0.698423
3/2
1/2
1338
1107
1.6
1
2/3
20 000
6
1.6
1000
1107
MPa
MPa
MPa K1
s1
MPa
s1
MPa
MPa
s1
m=
Appendix A
| |a
| i
|
= + Si (m; , T)
+Sm (m; , T) m
v v
vo
vo
(A.1)
2910 MPa
(A.2)
204 K
exp
1
T
where vo is the shear modulus at 0 K. The correction
factors that account for the thermal effects, Si and Sm
(essentially the ratios between the component of flow
stress attributable to a particular obstacle type at any
v [MPa] = vo
n "
tanh(h)
| m tanh(h)
qo(tanh2(h) 1)
+
!
|j /v
kT
m; oj
= 1
ln
3
| j /vo
gojvb
m;
1/qj
| ms = | mso exp
kT
m;
ln
3
vb goms
m; oms
(A.3)
n)
h| m
h| m
| ms
ln tanh(h) cosh
sinh
h
| ms
| ms
where
1/pj
|
m
|
m
(A.4)
(A.5)
The stress interval, | mi B | m B | mf, is assumed to correspond to a constant deformation path, i.e. constant
strain-rate, temperature, stress-state, etc.
Determination of the stress strain behavior requires
that the appropriate model parameters are inserted into
Eqs. (A.1), (A.2) and (A.3) to calculate the initial flow
stress at zero-plastic strain. In the present study, these
parameters as listed in Table 3 have been determined
based on the room temperature response of HY-100
steel. Plastic strain is then determined by applying the
model parameters, given in Table 3 to Eqs. (A.3), (A.4)
and (A.5), and incrementally increasing | m.
Predicting corresponding temperature/strain-rate
conditions using the MTS model relies primarily on
evaluating the thermally-activated component associated with short-range obstacles, Si and | i. The rate-sensitivity of long-range obstacles, in the current HY-100
MTS model description, is secondary in comparison to
short-range obstacles. In other words, yielding behavior
is markedly more sensitive to temperature and strainrate than is strain-hardening. In short, an Arrheniuslike diagram is constructed to illustrate the dependence
of
|y |a
v
on
Pi
n
kT
m; oj
ln
3
m;
vb
1/qj
|y |a
v
Pi
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