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High-Performance
Random Packing
2
An Overview of Intalox High-Performance Systems.
IMTP High-Performance
Random Packing
3
IMTP Packing Performance.
Flo
od
Po
int
Eff
ici
en
tC
ap
ac
Vapor Rate
Carbon steel
Stainless steel
Sy
ste
Ba
se
Materials of Construction
IMTP packing can be fabricated
from almost any metal. Examples
of available metals are:
ity
HE
TP
High-alloy steels
Duplex steels
Nickel and nickel alloys
Copper
Aluminum
Titanium
Zirconium
4
IMTP Packing Capacity.
Efficient Capacity, CSC = Co
20
0.2
0.16
0.11
Capacity Correlation
No. 70
No. 60
No. 15
No. 50
No. 40
No. 25
1.00
0.90
0.80
0.70
0.20
0.60
0.50
0.10
0.09
0.08
0.30
Co - m/s
Co - ft/s
0.40
0.07
0.20
0.06
0.05
0.04
0.10
0.01
0.02
0.03
0.04
0.05 0.06
0.08 0.10
0.20
0.30
0.40
0.50 0.60
0.80
1.00
0.03
Flow Parameter, X
G
L
G
L G
ng
a
aR
Da
5 73
0.07 1.1
Flow parameter
m/s or ft/s
5
IMTP Packing Pressure Drop.
1.5 (1
25)
1.0 (83)
0.50 (42)
0.25 (21)
Y = F Cs2 0.1
1.0
0.10 (8)
0.05 (4)
0.1
0.01
0.001
0.01
0.1
1.0
10.0
Flow Parameter, X
n.
0i
1.
Value of Packing Factor F
(Average Values) ze No. 15
i
g S s 549
n
i
ck
m/
51
Pa
in s
P
s
T
C
ft/
IM hen
in
s
F w en C
h
ion
34
tat 2
i
Fw
im m
L
14
2
te 3 /h
Ra m m/ft
d
i
u
gp
Liq
r/f
No. 25
441
41
No. 40
258
24
No. 50
194
18
No. 60
172
16
No. 70
129
12
73
30
122
50
122
50
122
50
122
50
te
wa
= 1.87 mm Hg/ft
= 6.15 mm Hg/m
= 817 Pa/m
6
IMTP Packing Efficiency.
7
Comparison of IMTP Packing to Other Mass Transfer Devices.
14
No. 40
(18)
12
457
No. 50
No. 60
(24)
10
610
kin
P
MT
c
Pa
(30)
No. 70
762
(36)
914
4
e
iev
tss
n
)2
e
ici iou in.
eff var m (
m
% t
60 ys angs,
tra aci
sp
0.03
0.10
0.06
0.20
0.09
0.30
0.12
0.40
0.15 m/s
0.50 ft/s
kin
Capacity Cs
TP
c
Pa
No. 25
16
14
No. 40
(18)
457
12
762
No. 60
(24)
610
No. 50
(21)
533
10
No. 70
(30)
IM
lve
va
t
en s )
ici iou in.
eff var m (
m
% t
60 ys angs,
a
i
r
t ac
sp
4
2
0.015
0.05
Typical Pressure
Drop Relationship
0.045
0.15
Capacity Cs
50 mm (2 in.) Packings
25 mm (1 in.) Packings
CIS = Ceramic
Intalox Saddle
0.030
0.10
Typical Capacity
Relationship
Typical Pressure
Drop Relationship
1.47
Typical Capacity
Relationship
1.0
1.0
1.39
MPR = Metal
Pall Ring
1.14
1.10
1.0
1.0
0.85
0.82
0.61
No. 25
16
0.58
IMTP
MPR
CIS
IMTP
MPR
CIS
IMTP
MPR
CIS
IMTP
MPR
CIS
8
Design Example.
Statement of Problem:
A deep bed of No. 50 IMTP packing
is to be used in a 2438 mm (96 in.) ID
11.0 bar ga (160 psig) hydrocarbon
stripper. Rate the packing capacity
and estimate its pressure drop
under the following hydraulic loadings.
Metric
English
A = (0.7854)(2.438)2
= 4.668 m2
A = (0.7854)(8.0)2
= 50.27 ft2
76200
V =
(22.4)(4.668)(3600)
= 0.2024 m/s
168000
V =
(1.40)(50.27)(3600)
= 0.6631 ft/s
3. Capacity Factor, Cs
(see pg. 4)
22.4
Cs = 0.2024
544.6-22.4
= 0.0419 m/s
4. Flow Parameter, X
(see pg. 4)
244940 22.4
X =
76200 544.6
= 0.652
5. Kinematic Viscosity
= 0.25
= / (L, g/cm3)
1.40
Cs = 0.6631
34.0-1.40
= 0.1374 ft/s
0.5
540000 1.40
X =
168000 34.0
= 0.652
0.5
544.6
/
1000
= 0.25
= 0.46 cs
0.5
0.5
/ 3642..04
= 0.46 cs
Capacity Rating:
From the capacity chart on page 4, Co = 0.061 m/s (0.20 ft/s) for No. 50 IMTP packing at X = 0.65.
6. Efficient Capacity, Csc
(see pg. 4)
7. Capacity Rating
Cs
Csc
0.2
10.5
Csc = (0.061)
20
= 0.0537 m/s
0.16
0.25
0.11
= 78% Capacity
0.0537
0.0419
0.2
10.5
Csc = (0.20)
20
= 0.1760 ft/s
0.16
0.25
0.11
= 78% Capacity
0.1760
0.1374
P = 14 mm H2O/m
9
Case Study.
Question:
A gas plant deethanizer contains
three beds of IMTP packing and
Intalox distributors. Five sets of
operating data were analyzed to
obtain measured HETP values as
tabulated below. Is the deethanizer
packing performing as it should?
Operating Data
on
cti
e
r S mm
we
To ths - ft
p
e
hs
d D pt
e
Be d De Siz
P
e
T
B IM
/cm
ne p
y
-d -c
ion osity nt
s
c
en
ou
e T d Vis ge C m
c
m
rfa iqui Sta
P - in.
Su
L
T
HE P red HET
u
as ed
Me asur
Me
Analysis:
The average surface tension value in
the rectifying section is 3.0 dyne/cm,
and the average viscosity is 0.065 cp.
By the correlation on page 6, the
System Base HETP of No. 25 IMTP
packing in the rectifying section is:
(1.78)0.065 = 464 mm
3.0
System Base HETP = 330
20
or
3.0
System Base HETP = 13.0
20
Rectifying
4140
13'7"
No. 25
2.5 - 3.5
0.06 - 0.07
8.6
481
19.0
Stripping
7087 & 7772
23'3" & 25'6"
No. 50
1.2 - 4.0
0.05 - 0.08
19.6
758
29.8
0.16
0.16
(1.78)0.065 = 757 mm
2.6
System Base HETP = 526
20
or
2.6
System Base HETP = 20.7
20
0.16
0.16
Data Summary
on
cti
e
rS
m
we - m
o
T
P
T
E
mm
dH Pe
r
T
u
.
HE
as
- in
Me ase
P
T
B
HE - in.
m
e
d
t
s
ure ETP
Sy
as
H
e
M
se
a
B
m
ste
y
S
Rectifying
Stripping
481
758
464
757
19.0
29.8
18.3
29.8
Conclusion:
Measured HETP values should be
equal to, or slightly above, the
System Base HETP values estimated
by the correlation. Because the
deethanizer HETP values are very
close to the correlation values, we
conclude that the deethanizers
packing is achieving the best
efficiency that can be expected.
10
Liquid Distribution for Intalox Systems.
ipe
P
ed
Fe
id
iqu
r
uto
b
i
r
t
r
Dis mite
i
id
L
u
Liq Bed
ing
ck
a
P
L
flu
Re
te
Pla
t
r
o
s)
ed
pp
Su se fe
ha
tor
o-p
w
ibu
t
r
(
t
dis
ery
ter
all
Re Limi
G
d
h
ui
d
las
Be
Liq
ing
ck
Pa
ed
Fe
te
rt
po
Pla
Su
or
p
Va
r
ile
bo r
e
R po
Va
Di
uto
ib
str
11
When is distribution quality important?
90-100% quality
generally 30-85% quality
20
18
16
14
20
Stages per Bed with System Base HETP
16
12
10
12
8
8
6
4
4
2
10
20
30
40
50
60
70
Distribution Quality, Percent
80
90
100
12
Norton Services.
Pilot Plant.
Nortons pilot plant distillation
columns located in Ohio are available
for testing with customer-supplied
test systems. These towers provide
information on packing efficiency,
capacity and pressure drop in the
customers specific system. Nortons
387 mm (15.25 in.) ID column can
hold up to 6 m (20 ft) of random
packing, structured packing or cartridge trays. This tower is constructed
of 316L stainless steel and is rated for
full vacuum to 400 psia. Norton also
offers the use of its 762 mm (30 in.)
atmospheric absorber/stripper tower
of 304 stainless steel.
13
Installation Services.
Norton provides field consultants to
assist customers with the installation
of Norton trays and packings anywhere in the world. Many customers
have averted major problems and
saved significant time by requesting
on-site supervision of their projects.
In the U.S., Norton Process Services,
Inc., a wholly-owned subsidiary of
Norton Chemical Process Products
Corporation, offers full-service contracting for tower modifications and
internal equipment installation.
Scanning Services.
Norton Tower SolutionsSM Scanning
Analysis provides gamma scans of
operating towers and interpretation of
the results. A Tower Solutions scan
can diagnose problems that cannot
be seen when the tower is not
operating. A scan is an effective tool
to diagnose problems and prepare
solutions in advance of a shutdown
for repairs or modification.
14
Quality Policy Statement.
15
Worldwide Office Locations.
Worldwide Headquarters
Norton Chemical Process Products
Corporation
P.O. Box 350
Akron, OH 44309-0350
Telephone: 330-673-5860
U.S. Toll Free: 1-888-NORTON-1
Fax: 330-677-7245
Sales Offices
Australia
Norton Engineering Materials
Division of Norton Pty. Ltd.
Nyrang Street, P.O. Box 44
Lidcombe, NSW, Australia 2141
Telephone: (61) 2-649-0161
Fax: (61) 2-643-2926
Mexico
Norton International, Inc.
Alejandro Dumas #103 2 Do Piso
Colonia Polanco
Mexico, D.F., C.P. 11590
Mexico
Telephone: (52) 5-280-05-22
Fax: (52) 5-280-06-47
France
Norton Chemical Process Products
BP No. 148
Rue de LAmbassadeur
F-78702 Conflans
St. Honorine, France
Telephone: (33) 1-3490-4000
Fax: (33) 1-3490-0788
Russia
Norton Russia
Office 440
1 Gagarina Avenue
Saint Petersburg 196105 Russia
Telephone: (7) 812-294-8530
Fax: (7) 812-294-8572
Germany
Norton Chemical Process Products
Theodor-Heuss-Platz 11
Postfach 10 11 51
D-4040 Neuss 1
Germany
Telephone: (49) 2131-15 74-0
Fax: (49) 2131-27 56 69
Holland
Norton Chemical Process Products
Dadelgaarde 71
2723 BJ Zoetermeer
Netherlands
Telephone: (31) 79 342 89 55
Fax: (31) 79 341 02 37
United States
Norton Chemical Process Products
Corporation
4501 East La Palma Avenue
Suite 250
Anaheim, CA 92807-1904
Telephone: 714-970-3000
Fax: 714-970-3001
Norton Chemical Process Products
Corporation
P.O. Box 350
Akron, OH 44309-0350
Telephone: 330-673-5860
Fax: 330-677-7245
Norton Process Services, Inc.
4137 S. Sherwood Forest Blvd.
Suite 220
Baton Rouge, LA 70816
Telephone 504-292-1895
Fax 504-292-1519
Norton Chemical Process Products
Corporation
5120 Woodway, Suite 9000
Houston, TX 77056-1724
Telephone: 713-627-7667
Fax: 713-627-7567
A Saint-Gobain Company