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Metallurgy and Materials Engineering Division, Sistan & Baluchestan University, Zahedan, Iran
School of Metallurgy and Materials Engineering, University College of Engineering, University of Tehran, P.O. Box: 11365-4563, Tehran, Iran
a r t i c l e
i n f o
Article history:
Received 26 October 2010
Accepted 3 March 2011
Available online 10 March 2011
Keywords:
A. Ferrous metals and alloys
D. Welding
E. Mechanical
F. Microstructure
a b s t r a c t
Resistance upset welding (UW) is a widely used process for joining metal parts. In this process, current,
time and upset pressure are three parameters that affect the quality of welded products. In the present
research, resistance upset butt welding of 304 austenitic stainless steel and effect of welding power and
upset pressure on microstructure, tensile strength and fatigue life of the joint were investigated. Microstructure of welds were studied using scanning electron microscopy (SEM). X-ray diffraction (XRD) analysis was used to distinguish the phase(s) that formed at the joint interface and in heat affected zone
(HAZ). Energy dispersive spectroscopy (EDS) linked to the SEM was used to determine chemical composition of phases formed at the joint interface. Fatigue tests were performed using a pullpush fatigue test
machine and the fatigue properties were analyzed drawing stress-number of cycles to failure (SN)
curves. Also tensile strength tests were performed. Finally tensile and fatigue fracture surfaces were studied by SEM. Results showed that there were three different microstructural zones at different distances
from the joint interface and delta ferrite phase has formed in these regions. There was no precipitation of
chromium carbide at the joint interface and in the HAZ. Tensile and fatigue strengths of the joint
decreased with welding power. Increasing of upset pressure has also considerable inuence on tensile
strength of the joint. Fractography of fractured samples showed that formation of hot spots at high welding powers is the most important factor in decreasing tensile and fatigue strengths.
2011 Elsevier Ltd. All rights reserved.
1. Introduction
Resistance upset welding is a solid-state welding process which
involves the interaction of electrical, thermal, mechanical and metallurgical phenomena. In this process, the joining surfaces are kept
at a forced contact; followed by a high electric current passing
through the workpieces. Due to the contact resistance and Joule
heating, a vast amount of heat is generated at the faying surfaces.
Before, during and after applying the electric current, force is
applied to maintain the electric current continuity and to provide
the pressure necessary to form the weld zone. The metal at the
joint is heated to a temperature where recrystallization can rapidly
occur across the heated surfaces. In this process, similar to other
resistance welding processes, there is no requirement to any extraneous material such as ller material or shielding gas [1]. In this
welding process there are two types of resistances namely contact
resistance and bulk resistance. At the earlier stages of the welding,
contact resistance plays the main role but gradually it decreases
and the role of bulk resistance becomes more important [2,3].
Kanne expressed that in comparison with fusion welding processes, the chemical composition and metallurgical properties are
not signicantly changed leading to better mechanical properties.
Simplicity, welding speed, capability of remote control and independence of welding quality from the operator skill are the other
advantages of this process [4]. Miyazaki et al., Kang, Kanne and
Sharitabar and Halvaee stated that resistance upset welding is a
suitable welding process for applications such as sealing of atomic
waste containers, welding of automotive parts and joining of stainless steels, low carbon steels, super alloys, aluminum alloys and
parts made of dissimilar materials [47]. The general conguration
of parts and equipments in upset welding is shown in Fig. 1.
Stainless steels play an important role in the modern world.
Austenitic stainless steels represent more than 2/3 of the total
stainless steel production. These stainless steels are preferred more
than other stainless steel types due to their good weldability [8].
But there are some negative metallurgical changes during welding
of these steels which should be considered. They are [9,10]:
(a) formation of delta ferrite phase, (b) formation of sigma phase,
(c) stress corrosion cracking, (d) precipitation of chromium carbide
at grain boundaries and (e) formation of hot cracks.
Nikitin et al. and Nikitin and Bses stated that fatigue behavior of
austenitic stainless steel welds is strongly affected by stress ampli-
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that two samples penetrate into each other during welding) for
producing a high quality weld. Also they reported that the required
upset length can be reduced using lower welding forces [5]. Kanne
also reported applicability of the UW process to weld a variety of
stainless steels (including A-286), super alloys (including TD nickel), refractory metals (including tungsten) and aluminum alloys
(including 2024) [4]. Shieh and Chang presented a study of upset
welding process in wire drawing; obtaining the optimum parameters of the operation for a better distribution of hardness in the
wire [21]. Further, Cannel et al. wrote on the optimization and reliability of UW process [22]. In a study by Kang et al. the upset weldability and formability of a particular kind of material (SPCC) was
investigated. The results showed that the formability of upset
welded SPCC steel sheets were slightly lower than that of the parent material [11]. Applications of upset welding processes were recently extended to cast iron parts by Shakhmatov and Shakhmatov
and dissimilar austenitic to martensitic stainless steels by Sharitabar and Halvaee [7,23]. They found that a good metallurgical bond
can be produced between austenitic and martensitic stainless
steels by resistance upset welding. Also in the past decade some
work has been carried out on numerical simulation of resistance
upset welding. Recently, Kerstens and Richardson reported an
experimental study of weld development during resistance upset
butt welding process. They also made a simplied thermal nite
element model to explore the inuence of welding conditions on
heating [2]. In a very recent study Hamedi et al. considered numerical simulation and experimental investigation of UW process
parameters including heating and post-weld heating current and
their corresponding duration as well as interference of the part features that form the joint and effect of these parameters on tensile
strength of a low carbon low alloy oil pressure sensor. They found
that both numerical and experimental results suggest an optimum
set of welding parameters, i.e. time and electrical current that yield
a maximum value for the tensile strength of the joint. Also the effects of post-weld heating time and current on the tensile strength
showed that these parameters had a remarkable effect on improving tensile strength of the weldment [24].
In this research, resistance upset butt welding of 304 austenitic
stainless steel and effect of welding power and upset pressure on
microstructure, tensile and fatigue life of the joint were investigated in order to correlate the weld quality to the variation of these
two parameters and introducing optimum welding conditions.
2. Experimental procedure
Chemical composition of AISI 304 stainless steel used in this research was 0.04%C, 0.48%Si, 1.75%Mn, 18.15%Cr, 8.2%Ni, 0.045%P,
0.016%S, 0.7%Cu and 0.11Mo. Also yield and tensile strengths of
the steel used were 242 and 658 MPa respectively.
Start material was heated 10 min at 1060 C and cooled in air to
diminish cold work effects due to mechanical processing prior to
welding. The welding machine used in this research had been manufactured by Electro-TechnoTak Company (Tehran, Iran) and its
maximum power was 25 KVA. Then surfaces of samples were
ground by 1000 mesh grinding paper to remove oxide layer formed
during heat treatment. Two rods of 50 mm length and diameter of
8 mm were clamped in upset welding machine for each state of
welding. Table 1 shows welding conditions and measured parameters during welding. Primary and upset pressures were the same
and were applied by a mechanical system. Firstly, heating pressure
was applied on the faying surfaces. Then electrical current was
passed through the bars in contact. During welding, the electrical
potential was measured by an AVO meter and welding power
was calculated using following equation
P VI
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Table 1
Selected conditions and measured parameters during welding.
Sample
name
Welding
current (A)
Welding
pressure (MPa)
Welding
time (S)
Heat input
(V.A.S)
A1B1
A2B1
A3B1
A4B1
A1B2
A2B2
A3B2
A4B2
A1B3
A2B3
A3B3
A4B3
A1B4
A2B4
A3B4
A4B4
1500
2000
2500
3000
1500
2000
2500
3000
1500
2000
2500
3000
1500
2000
2500
3000
1.01
1.01
1.01
1.01
1.15
1.15
1.15
1.15
1.27
1.27
1.27
1.27
1.41
1.41
1.41
1.41
1.5
1.42
1.33
1.21
1.51
1.41
1.33
1.19
1.5
1.40
1.31
1.20
1.49
1.42
1.32
1.21
4500
5680
6650
7260
4530
5640
6650
7140
4500
5600
6550
7200
4470
5680
6600
7260
where P is the welding power (VoltAmpere), I is the current intensity (Ampere) and V is the electrical voltage (Volt) [2]. Also, welding
time which is the passing time of electrical current was measured
by the AVO meter.
Tensile test was carried out by MST30/MH machine at 2 mm/
min displacement rate on welded samples. This test was performed according to ASTM-E8 standard [25] while the joint interface was held in the middle of the tension samples and the ash
was removed. The examination method in fatigue investigation
was the single factor method, i.e. for each series of experiments
one factor was varying while the other parameter was kept constant at previously optimized levels of tensile strength. The aim
of the authors was to investigate the effect of UW process parameters on fatigue properties of 304 austenitic stainless steel joints. In
other words, the authors wanted to see how variations in welding
parameters can affect the fatigue life of the joint. For this purpose,
three different stress amplitudes were selected higher than yield
strength of the alloy to represent the results of the tests as SN
curves. The Pullpush fatigue test was performed according to
ASTM-E60692 standard [26] while the joint interfaces were held
in the middle of the samples. These test was carried out by INSTRON 8502 fatigue testing machine at R = 1, frequency of 2 Hz
and 320, 370 and 430 MPa stress amplitudes. The metallographic
samples were cut longitudinally and the interfaces were studied
by SEM Cam Scan MV2300 and Energy dispersive X-ray lined up
to the SEM after preparation and etching with Kalling No. 2 agent
(5 g CuCl2, 100 ml HCl and 100 ml Ethanol). XRD test was fullled
by wave length of Coka 1:7889 nm: Finally fracture surfaces were
studied by SEM.
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Fig. 2. Microstructure of base metal (a): before and (b): after annealing heat treatment.
Fig. 3. (a): Macrostructure of resistance upset butt welding joint of 304 stainless steel. (b)(d): different microstructural zones formed in the joint.
temperature. This caused residual ferrite to transform to Widmansttten austenite by displacive mechanism. Compressive stresses during transformation in this welding process also encouraged
ferrite to Widmansttten austenite transformation (Fig. 3b).
Joining surfaces have the highest temperature during welding
and with increasing distance from the weld interface, temperature
decreases [2,28]. Around the interface, temperature rose up to austenite + delta ferrite in FeCrNi phase diagram resulting to the
formation of ferrite at austenite grain boundaries (Fig. 3c). Because
of high cooling rate of the joint, the possibility of ferrite to austenite transformation was low and some ferrite was remained in grain
boundaries. So microstructure of this region consisted of austenite
and delta ferrite [27]. Fuller et al. concluded that presence of d-ferrite in grain boundaries prohibits grain growth and so the grains
are ne. Also this phase acts as a crack growth inhibitor and reduces the possibility of intergranular fracture [32]. But Lippold
and Kotecki expressed that presence of delta ferrite decreases
formability of austenitic stainless steels and increases probability
3858
Z e0 expQ =RT
between the joint interface and bulk of the samples. This reduced
the cooling rate leading to decreasing the amount of grain boundary
ferrite near the interface and grain growth in this region.
By using higher welding pressure at constant welding powers
(e.g. samples A2B1A2B4), width of the WAZ decreased. But it
caused widening DRZ and PRZ. Higher welding pressures lower
the interface resistance according to Eq. (3) and increase the roll
of bulk resistance on heat generation during welding and formation of lower amount of liquid at the interface.
Z C 1 sinhC 2 rn
where C1, C2 and n are constants and r is stress exerted during hot
deformation [33]. According to this equation, higher welding pressures increased the possibility of dynamic recrystallization and
widening DRZ and PRZ.
3.2. Phase analysis
Fig. 4 shows the result of XRD analysis for weld metal and HAZ.
Only there are austenite and delta ferrite phases in these regions
and no precipitation of chromium carbides (Cr23C6) phase is observed. This is because of high cooling rate of weld interfaces from
the temperature range of chromium carbide precipitation (450
850 C).
Fig. 5a and b shows EDX analysis of the black phase in Fig. 3c.
Also chemical composition of this phase is shown in Table 2. It
can be seen that the amount of Cr increased and Ni decreased in
this phase and its chemical composition is in the ferrite region of
the FeCrNi phase diagram at room temperature [28].
where Z is ZenerHolloman parameter, e is strain rate, Q is activation energy, R is gas constant and T is temperature. According to this
equation, higher temperature during hot deformation reduces Z and
increases the possibility of dynamic recrystallization and therefore
widening DRZ and PRZ [33]. On the other hand, higher heat generated by bulk resistance of samples decreased temperature gradient
3859
Fig. 5. (a): Black phase formed in the microstructure and (b): EDX line scan analysis of the black phase in the microstructure.
Table 2
EDX Chemical composition of black phase in the microstructure.
Element
Cr
Ni
Si
Mn
Fe
Wt%
23.93
4.71
0.46
1.61
Bal
can be formed by in-homogeneities in the material and local variations in the interface resistance resulting from contaminations,
non-uniform deformation or surface imperfections. A non-uniform
upsetting pressure distribution over the joint may also play a role.
If the upsetting pressure is not uniform, then according to Eq. (3)
there will be a difference in contact resistance over the joint area.
Non-uniformity in current distribution also may arise as a result
of contact resistance variations at the electrode/sample interface
due to the electrode surface condition and contaminations or variations of the clamping force. With increasing of welding power, the
probability of hot spot formation rises due to increase in the heat
input to the joint interface.
Fracture surface of sample A4B2 (welded at high welding power)
is shown in Fig. 8. The fracture mode is completely ductile in this
steel. It can be seen that formation of hot spot at the interface of
this sample caused crack initiation and reduced the joint strength.
Fig. 9 shows that with increasing of the upset pressure, strength
of the joint increases rstly and then decreases. Contact resistance
rises with decrease in upset pressure according Eq. (3). Experimental investigations of Song et al. [3] also showed that contact resistance increases with decreasing of welding pressure. So, low
welding pressures leads to widening the area for formation of Widmansttten austenite and decreasing joint strength [35]. Also at
3860
Fig. 7. SEM macrostructure of a hot spot in sample A4B1 and formation of cracks in
this region.
of liquid was rejected in upsetting stage due to high welding pressure. This caused thinning the area for formation of Widmansttten austenite and increasing joint strength (sample A1B3). Also
increase in upset pressure led to formation of good metallurgical
joint. By using welding pressure higher than 1.27 MPa; all liquid
and mushy metals were rejected from the joint interface as ash
and an incomplete joint was formed which reduced the joint
strength (sample A1B4). On the other hand, effect of welding pressure on tensile strength decreased with increasing of welding
power (Fig. 9). This may be due to the formation of hot spots at
high welding powers. Because of the presence of welding defect
at the joint area, effect of microstructure on mechanical properties
was reduced led to decreasing the effect of welding pressure on
tensile strength at high welding powers.
Fig. 10 shows fracture surface of sample A3B1 (welded at low
welding pressure). In Fig. 10a there are different crack initiation
sites at the fracture surface. The higher magnications of zones
13 are shown in Fig. 10bd respectively. It is observed that presence of plate form Widmansttten austenite phase at the joint
interface caused formation of large voids due to stress concentration and reduced the joint strength at low welding pressures.
3.3.2. Fatigue properties
Fig. 11 show the effect of welding power on fatigue life of the
joint at different stress amplitudes in samples welded with
1.27 MPa welding pressure. It is observed that fatigue life of
welded samples is lower than base metal and decreases slightly
Fig. 8. Fracture surface of sample A4B2, a: lower magnication b: higher magnication showing hot spot on this surface.
3861
Fig. 10. (a): Fracture surface of sample A3B1 (b)(d) higher magnication of crack initiation sites on the fracture surface.
3862
Fig. 12. Fatigue fracture surface of the sample welded at high welding power.
Fig. 13. Fatigue fracture surface of the sample A2B3 tested at two different stress amplitudes (a): 320 MPa and (b): 430 MPa.
steel after a true tensile strain of 30%) [8]. This relatively high temperature in sample tested at 430 MPa stress amplitude inhibited
martensite transformation. In addition, plastic deformation by
migration of dislocations was facilitated at these relatively high
temperatures (thermal activation).
Fig. 14 shows the sub-surface fatigue crack formed in the Widmansttten austenite formation zone. Fatigue process and its
mechanisms are largely inuenced by the presence of the material
in-homogeneities. Since d-ferrite is basically different from austenite matrix in crystallography and chemical composition, it is likely
to provide crack nucleation sites. Goyal et al. [13] conducted a
Fig. 14. Fatigue sub-surface crack formed in the Widmanstatten austenite formation zone in sample A2B1 tested at 320 MPa stress amplitude.
3863
Acknowledgments
The authors gratefully acknowledge the extensive support of
the Electro-Techno Tak Company and University of Tehran for
experimental and nancial supports.
References
Fig. 15. Fatigue crack growth mode in the dynamic recrystallization zone in sample
A3B2 tested at 320 MPa stress amplitude.
no fatigue crack deection by d-ferrite phase in this region. Therefore it can be concluded that presence of d-ferrite in austenitic
stainless steel welds causes fatigue crack initiation and does not
have any considerable effect on crack path at high stress
amplitudes.
4. Conclusions
In the present investigation, resistance upset butt welding of
304 austenitic stainless steel and effect of welding power and upset pressure on microstructure, tensile strength and fatigue properties of the joint were investigated. The obtained results can be
summarized as follows:
1. In resistance upset butt welding of 304 stainless steel, three different microstructural zones were formed at the joint interface
due to thermal gradient between the joining faces and electrodes. These zones are: Widmansttten austenite formation
zone, dynamic recrystallization zone and partially recrystallized
zone. Also delta ferrite phase formed in these regions.
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