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ICDF (International Centre for Diffraction Data)

Powder Diffraction Pattern for Mordenite


Composition:
|Na8(H2O)24| [Si40Al8O96]
Refined composition:

|Na8(H2O)25| [Si40Al8O96]

Space group:

Cmcm

Cell parameters:

a = 18.11

b = 20.53

c = 7.528

= 90

= 90

= 90

Reference:

(# )

Setting:

Gramlich, V. Ph.D. Thesis, ETH, Zrich, Switzerland, , (1971)


Mordenite (MOR)

HKL
h
1
0
4
1
3
4
0
3
2
1
5
2
3
0
4
3
2
4
5

list:
k
l
3
0
2
1
2
0
5
0
3
1
2
1
2
2
5
0
2
2
3
2
1
1
6
0
1
2
6
1
4
1
5
1
4
2
2
2
5
0

2-Theta
13.456
14.194
20.862
21.590
22.293
23.853
24.506
25.525
26.337
26.729
26.909
27.103
27.495
27.864
28.047
28.049
30.212
31.236
32.057

d
I (rel)
h
k
l 2-Theta
6.4015 34.18
3
7
1
35.066
6.0705 16.86
7
3
0
36.109
4.1425
6.58
4
6
2
39.680
4.0044 56.22
6
6
1
40.485
3.8796
1.31
8
4
0
42.459
3.6293
5.44
2
8
2
42.604
3.5339
5.19
7
7
0
45.482
3.3951 53.29
4
8
2
45.982
3.2921
5.84
9
1
2
50.202
3.2447 16.06
2
8
3
50.447
3.2234 57.82
3
9
3
54.952
3.2008
0.16
2
3 10 57.269
3.1560
5.07
7
9
2
57.567
3.1150 13.15
0 12 2
57.572
3.0950
4.20
10 4
2
57.665
3.0949
0.62
3 13 0
58.799
2.8779
0.26
4 10 3
60.031
2.7858
0.13
9 11 1
67.707
2.7162
0.71
5
3
6
79.888
Powder pattern generated for Mordenite (MOR)

Profile parameters
Wave length: 1.5 Ang
Profile: Start = 10.0, End = 80.0, Step = 0.02

d
I (rel)
2.4896
1.43
2.4200
0.13
2.2098
0.10
2.1677
1.65
2.0712
0.08
2.0645
3.60
1.9402
0.01
1.9202
4.38
1.7680
3.18
1.7599 .3.11
1.6256
2.02
1.5650
0.06
1.5576
0.42
1.5575
0.88
1.5552
0.01
1.5278
2.95
1.4993
0.14
1.3463
0.16
1.1682
2.60

Powder Diffraction Pattern for Clinoptilolite


Composition:
|Na1.84K1.76Mg0.2Ca1.24(H2O)21.36| [Si29.84Al6.16O72]
Refined composition:

|Na1.84K1.76Mg0.2Ca1.24(H2O)21.36| [Si29.84Al6.16O72]

Space group:

C12/m1

Cell parameters:

a = 17.662

b = 17.911

c = 7.407

= 90

= 116.40

= 90

Reference:
HKL list:
h k l
2 2 0
1 3 0
-4 0 1
2 0 1
-3 3 1
2 4 0
4 2 0
-1 1 2
1 5 0
-1 5 1
-4 2 2
-4 4 1
5 1 0
-3 3 2
2 4 1
-2 4 2
5 3 0
2 6 1
5 1 1

(# )

Setting:

Koyama, K. and Takeuchi, Y. Z. Kristallogr., 145, 216-239 (1977)


Clinoptilolite (HEU)
2-Theta
14.535
15.433
19.839
20.381
21.406
22.194
23.929
24.656
24.792
26.899
27.368
27.805
27.857
28.001
28.202
30.480
31.123
35.791
35.816

d
I (rel)
h k l
2-Theta
5.9286
5.88
4 6
0
36.694
5.5858
1.96
5 5
0
36.874
4.3537
5.85
0 6
2
39.509
4.2392
0.01
0 0
3
39.648
4.0384
0.08
-1 3
3
40.314
3.8967 27.81
-5 7
1
42.448
3.6179
0.38
4 2
2
42.645
3.5127
3.58
-9 1
2
45.434
3.4938
1.33
-1 9
1
45.939
3.2246
0.17
2 0
3
45.988
3.1703 31.24
3 1
3
50.291
3.1215 15.89
-8 6
1
50.851
3.1158
0.23
-9 5
3
54.861
3.1001
3.18
-8 8
2
57.442
3.0784
1.20
7 7
1
58.961
2.8532
0.10
-11 3
1
59.747
2.7957 26.81
1 7
4
67.876
2.4407
7.18
2 6
4
68.248
2.4391
1.54
-2 0
6
79.846
Powder pattern generated for Clinoptilolite (HEU)

Profile parameters
Wave length: 1.5 Ang
Profile: Start = 10.0, End = 80.0, Step = 0.02

d
I
2.3827
2.3714
2.2190
2.2115
2.1765
2.0717
2.0626
1.9421
1.9219
1.9199
1.7683
1.7959
1.6280
1.5607
1.5240
1.5058
1.3434
1.3369
1.1687

(rel)
6.72
0.20
0.03
5.22
1.69
0.27
0.30
2.98
3.68
0.44
4.21
9.00
0.07
0.03
0.76
0.10
0.33
0.20
0.77

Powder Diffraction Pattern for Natrolite


Composition:
|Na16(H2O)16| [Si24Al16O80]
Refined composition:

|Na16(H2O)16| [Si24Al16O80]

Space group:

Fdd2

Cell parameters:

a = 18.30

b = 18.63

c = 6.60

= 90

= 90

= 90

Reference:
HKL
h
2
1
3
2
4
3
4
1
5
0
2
3
5
2

list:
k
l
2
0
1
1
1
1
4
0
2
0
3
1
4
0
5
1
1
1
2
2
6
0
5
1
3
1
4
2

(# )

Setting:

Meier, W.M.Z. Kristallogr., 113, 430-444 (1960)


Natrolite (NAT)
2-Theta
13.195
14.631
19.831
20.820
21.047
23.827
26.570
27.154
27.508
27.905
29.556
30.356
30.569
33.758

d
I (rel)
h
k
l 2-Theta
6.5276 57.59
4
2
2
33.903
5.8901 100.00
1
7
1
35.709
4.3555 47.31
7
1
1
36.262
4.1507 25.02
8
2
0
39.463
4.1064 15.45
2
6
2
39.953
3.6331
1.56
6
2
2
40.289
3.2638
3.33
1
5
3
46.908
3.1948 34.65
3
9
1
47.048
3.1546 40.29
2
8
2
47.483
3.1106 12.15
6
6
2
48.771
2.9403
2.56
3
5
3
48.982
2.8646 65.36
5
3
3
49.125
2.8451 58.11
10 2
0
49.375
2.5831
7.81
7
7
1
49.403
Powder pattern generated for Natrolite (NAT)

Profile parameters
Wave length: 1.5 Ang
Profile: Start = 0.0, End = 50.0, Step = 0.02

d
I (rel)
2.5723 12.80
2.4462 16.32
2.4101 15.87
2.2215
1.84
2.1953 13.21
2.1778 10.96
1.8844
4.59
1.8791
0.85
1.8628
0.80
1.8165
0.24
1.8092
7.51
1.8042
8.68
1.7957
6.16
1.7947
4.98

Powder Diffraction Pattern for AlPO-8


Composition:

[Al36P36O144]

Refined composition:

[Si72O144]

Space group:

Cmcm

Cell parameters:

a = 33.2900

b = 14.7036

c = 8.3863

= 90

= 90

= 90

Reference:
HKL
h
3
6
6
8
2
6
0
8
2
4
2
9
1
7
4
7
10
11
4

list:
k
l
1
1
0
0
2
0
0
0
0
2
2
1
2
2
2
0
2
2
4
0
4
1
1
1
3
2
3
1
4
1
1
2
2
1
1
1
2
3

(# )

Setting:

Richardson Jr., J.W. and Vogt, E.T.C. Zeolites, 12, 13-19 (1992)
AlPO-8 (AET)
2-Theta
14.149
15.538
19.500
20.767
21.258
22.082
23.766
23.905
24.337
25.776
26.274
26.289
27.356
27.448
27.809
28.228
30.495
31.133
35.017

d
I (rel)
h
k
l 2-Theta
6.0897
0.10
0
6
0
35.642
5.5483
0.51
7
5
1
36.470
4.4287
6.09
7
1
3
36.766
4.1613
0.44
12 4
0
39.596
4.0661
2.57
8
2
3
39.623
3.9162 10.08
6
6
1
40.524
3.6424
0.18
14 0
2
42.519
3.6214
0.81
6
4
3
42.588
3.5582
0.10
3
7
0
42.618
3.3625
3.68
14 4
1
45.430
3.2999
0.08
17 1
0
45.459
3.2981
0.30
7
7
0
45.950
3.1717
1.13
16 4
1
50.143
3.1613
0.67
17 1
2
50.399
3.1210
0.18
14 3
2
50.487
3.0756
0.83
17 4
3
58.947
2.8519
0.01
15 5
4
59.960
2.7948
0.17
10 10 0
67.782
2.4929
0.02
Powder pattern generated for AlPO-8 (AET)

Profile parameters
Wave length: 1.5 Ang
Profile: Start = 10.0, End = 80.0, Step = 0.02

d
I (rel)
2.4506
0.60
2.3968
0.15
2.3782
1.60
2.2143
0.01
2.2128
0.03
2.1656
0.05
2.0684
0.01
2.0652
0.09
2.0639
0.20
1.9423
0.18
1.9411
0.30
1.9214
0.09
1.7699
0.37
1.7615
0.14
1.7586
0.08
1.5243
0.07
1.5009
0.05
1.3450
0.11

Powder Diffraction Pattern for AlPO-18


Composition:
[Al24P24O96]
Refined composition:

[Al24P24O96]

Space group:

C12/c1

Cell parameters:

a = 13.7114

b = 12.7315

c = 18.5706

= 90

= 90.01

= 90

Reference:
HKL
h
0
1
1
-3
3
1
3
1
-2
4
0
-3
3
0
3
0
2
3
0

list:
k
l
2
3
1
4
3
0
1
2
1
2
3
2
1
3
3
3
2
4
0
2
4
0
1
4
1
4
4
1
3
0
0
6
4
1
1
5
2
6

(# )

Setting:

Simmen, A., McCusker, L.B., Baerlocher, Ch. and Meier, W.M. Zeolites (1991)
AlPO-18 (AEI)
2-Theta
19.459
20.792
21.322
22.155
22.158
23.292
24.518
25.553
26.347
26.976
27.258
27.498
27.502
27.664
27.911
28.047
30.486
30.949
31.262

d
I (rel)
h
k
l 2-Theta
4.4379
6.59
0
2
7
35.670
4.1563
0.55
-3 3
5
36.664
4.0541
0.70
3
3
5
36.669
3.9034
3.29
0
4
6
39.510
3.9029
0.08
6
0
2
39.510
3.7153
3.56
-5 1
5
40.364
3.5322
0.88
5
1
5
40.371
3.3914
2.76
2
2
8
42.311
3.2909
0.42
0
6
2
42.516
3.1829
0.43
-5 3
4
42.627
3.1557
0.83
5
3
4
42.633
3.1552
0.18
1
5
6
45.327
3.1371
0.12
-4 0
8
45.931
3.1099
0.04
4
0
8
45.938
3.0951
0.04
1
7
2
50.143
2.8526
0.02
-6 2
6
50.250
2.8110
0.24
6
2
6
50.259
2.7835
0.02
-5 1
8
50.599
2.4811
4.23
-7 3
2
50.854
Powder pattern generated for AlPO-18 (AEI)

Profile parameters
Wave length: 1.5 Ang
Profile: Start = 10.0, End = 80.0, Step = 0.02

d
I (rel)
2.4488
0.32
2.3846
0.24
2.3843
0.12
2.2189
0.13
2.2189
0.02
2.1739
0.02
2.1735
0.02
2.0781
0.04
2.0686
0.15
2.0634
0.11
2.0632
0.21
1.9464
0.03
1.9222
0.02
1.9219
0.04
1.7699
0.08
1.7664
0.06
1.7661
0.11
1.7550
0.04
1.7468
0.11

Powder Diffraction Pattern for Tetrapropylammonium ZSM-5


Composition:
|((C3H7)4NOH)4| [Si95.7Al0.3O192]
Refined composition:

|(C12N)4| [Si96O192]

Space group:

Pnma

Cell parameters:

a = 20.022

b = 19.899

c = 13.383

= 90

= 90

= 90

Reference:
HKL
h
1
0
3
2
1
0
2
3
5
1
3
1
1
1
3
2
4
1
2

list:
k
l
0
2
6
4
8
1
0
2
0
3
1
3
0
3
3
2
0
1
3
3
2
3
5
2
0
4
4
3
3
3
5
2
0
3
6
1
0
4

(# )

Setting:

Van Koningsveld, H., van Bekkum, H. and Jansen, J.C. Acta Crystallogr. (1987)
Tetrapropylammonium ZSM-5 (MFI)
2-Theta
d
I (rel)
h
k
l 2-Theta
d
I (rel)
13.574 6.3464 17.34
2 6
0
27.564
3.1482
0.26
13.674 2.3554
3.34
4
4
2
27.808
3.1212
0.09
14.028 2.2962
2.39
6
2
1
28.197
3.0789
0.38
15.496 5.5632
6.19
2
6
2
30.529
2.8487
3.04
19.837 4.3542
4.67
1 18 4
31.031
1.0482
1.15
19.843 4.3530
7.11
6
5
2
36.600
2.3886
2.07
21.213 4.0747
3.03
1
7
3
36.731
2.3803
1.61
22.475 3.8486
4.02
39.550
2.2168
0.36
1
0
6
23.224 3.8363 100.00
5
6
3
39.553
2.2166
0.09
23.751 3.6400 39.76
5
1
5
39.649
2.2115
0.03
24.927 3.4752
3.03
8
3
2
39.673
2.2102
0.06
25.705 3.3717
1.63
7
0
4
40.360
2.1741
0.25
26.273 3.3000
9.57
8
1
3
40.446
2.1697
0.30
26.465 3.2765
3.24
1
9
1
40.467
2.1686
0.21
26.793 3.2371
1.56
1
2
6
40.562
2.1637
0.41
26.795 3.2368
2.06
5 10 1
50.249
1.7664
1.24
26.814 3.3303
5.91
7
0
6
50.479
1.7589
0.70
27.298 3.1783
0.68
8
8
4
57.448
1.5606
0.46
27.343 3.1732
1.34
12 5
2
60.017
1.4996
8.28
Powder pattern generated for Tetrapropylammonium ZSM-5 (MFI)

Profile parameters
Wave length: 1.5 Ang
Profile: Start = 10.0, End = 80.0, Step = 0.02

Powder Diffraction Pattern for ZSM-5, Calcined


Composition:
|H0.32| [Si95.68Al0.32O192]
Refined composition:

[Si96O192]

Space group:

P121/n1

Cell parameters:

a = 19.879

b = 20.107

c = 13.369

= 90

= 90.67

= 90

Reference:

HKL
h
1
2
2
4
2
4
1
1
1
2
3
-1
5
1
6
-3
6
0
-4

list:
k
l
0
2
2
1
0
2
2
0
4
1
3
0
2
3
5
1
3
3
3
3
2
3
5
2
1
2
5
2
0
0
5
1
1
0
7
1
0
4

(# )

Setting:

van Koningsveld, H., Jansen, J.C. and van Bekkum, H.


Zeolites, 10, 235-242 (1990)
ZSM-5, Calcined (MFI)
2-Theta
13.977
14.212
15.496
19.889
21.052
22.257
22.324
23.784
24.496
25.701
25.794
26.221
26.365
26.479
26.759
26.781
27.281
30.979
31.207

d
I (rel)
h
k
l 2-Theta
d
I (rel)
6.3464 17.38
4 2
1
36.633
2.3865
0.35
6.2423
0.35
5 6
2
36.703
2.3821
0.01
5.5632
6.19
7 0
3
39.601
2.2140
0.01
4.4715
0.51
5 6
3
40.350
2.1746
0.16
4.2270 10.04
1 8
3
40.477
2.1687
0.17
3.9955
5.64
2 0
6
42.326
2.1353
0.01
3.9890
1.75
2 8
3
45.541
1.9378
0.04
3.7473 30.97
4 3
6
50.231
1.7670
0.31
3.6400 39.75
8 8
0
53.699
1.6606
0.07
3.4720
0.62
-10 5
3
54.988
1.6246
0.03
3.4539
0.99
6 2
7
54.992
1.6245
0.02
3.3986
1.17
9 7
3
57.462
1.5602
0.02
3.3860
1.35
-7 6
6
60.068
1.5402
0.09
3.3717
1.63
-12 2
3
67.850
1.3813
0.02
3.3370
2.73
-11 3
6
68.309
1.3731
0.02
3.3343
0.87
-16 1
4
79.983
1.1670
0.05
3.2689
0.07
-6 6 10 79.995
1.1669
0.01
2.8083
0.25
2.7884
0.11
Powder pattern generated for ZSM-5, Calcined (MFI)

Profile parameters
Wave length: CuA2
Profile: Start = 0.0, End = 50.0, Step = 0.02

Powder Diffraction Pattern for SSZ-26/SSZ-33 family, Polymorph A SiO2 framework


Composition:
[Si56O112]
Refined composition:

[Si56O112]

Space group:

Pmna

Cell parameters:

a = 13.26

b = 12.33

c = 21.08

= 90

= 90

= 90

(# )

Reference:

Setting:

Lobo, R.F., Pan, M., Chan, I., Li, H.X., Medrud, R.C., Zones, S.I.,
Crozier, P.A. and Davis, M.E. Science (1993).
SSZ-26/SSZ-33 family, Polymorph A SiO2 framework (SSZ-26/SSZ-33 family, Polymorph A SiO2 framework)
HKL list:
h
k
l 2-Theta
d
I (rel)
h
k
l 2-Theta
d
I (rel)
1 0
3 13.876 6.2088
1.50
1 3
7
36.587
2.3894
0.71
0 2
1 14.564 5.9171
2.99
0 3
8
39.523
2.2183
0.07
1 2
3 19.743 4.3747
0.28
2 1
9
40.365
2.1739
0.03
2 2
2 20.823 4.1501
0.01
6 2
1
42.479
2.0703
0.11
2 0
4 20.949 4.1255
3.07
3 0
9
42.494
2.0696
0.01
0 3
0 21.029 4.1100
0.26
4 5
2
45.372
1.9446
0.01
3 1
2 22.348 3.8701
0.02
6 4
2
50.123
1.7706
0.04
1 3
1 22.411 3.8594
6.26
6 5
2
54.933
1.6261
0.04
1 3
2 23.526 3.6789
0.10
4 4
9
54.959
1.6254
0.01
1 2
5 25.748 3.3661
0.28
8 3
3
59.926
1.5017
0.01
1 1
6 26.484 3.2742
0.97
8 0
6
60.042
1.4991
0.62
0 3
4 26.761 3.2409
0.03
4 6 10 67.786
1.3449
0.00
1 3
4 27.564 3.1483
1.00
8 1
9
67.788
1.3449
0.00
2 0
6 27.961 3.1044
1.43
1 9
3
68.197
1.3378
0.01
2 2
5 28.174 3.0814
1.23
3 6 11 68.304
1.3360
0.02
4 1
2 28.346 3.0631
0.48
10 5
0
79.911
1.1679
0.01
4 2
2 30.918 2.8137
0.07
4 0
4 31.005 2.8060
1.82
3 0
7 35.079 2.4887
0.02
Powder pattern generated for SSZ-26/SSZ-33 family, Polymorph A SiO2 framework (SSZ-26/SSZ-33 family,
Polymorph A SiO2 framework)

Profile parameters
Wave length: 1.5 Ang
Profile: Start = 10.0, End = 80.0, Step = 0.02