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Department of Grain Science and Technology, Central Food Technological Research Institute, Mysore 570 020, Karnataka, India
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Department of Food Engineering, Central Food Technological Research Institute, Mysore 570 020, Karnataka, India
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Received 15 June 2006; received in revised form 20 January 2007; accepted 23 January 2007
Available online 4 February 2007
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Abstract
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The decorticated nger millet was subjected to high temperature short time treatment to prepare expanded millet, a ready-to-eat new
generation product. It was observed that, attening the grains to the desired shape factor and the moisture content were critical factors
for obtaining the millet with maximum expansion ratio. Accordingly, the eect of moisture content of the millet prior to attening, the
shape factor and drying time and their complex interaction on the expansion ratio of the millet were determined. Besides, the bulk density, sphericity, hardness and overall acceptability of the expanded millet were also evaluated using a central composite rotatable experimental design. Based on the design, the optimal conditions for obtaining fully expanded millet were, moisture content of about 40%
prior to attening, shape factor ranging from 0.52 to 0.58 and drying time varying from 136 to 150 min. The product prepared under
these conditions had an expansion ratio (Y1) P 4.6, bulk density (Y2) 6 0.17 g/cm3, sphericity (Y3) P 0.90, hardness/texture
(Y4) 6 5.0 N and the overall acceptability (Y5) P 7.2.
2007 Published by Elsevier Ltd.
Keywords: Decorticated nger millet; Expanded millet; Expansion ratio; Shape factor; Central composite rotatable design
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1. Introduction
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Corresponding author. Tel.: +91 821 2510843; fax: +91 821 2517233.
E-mail addresses: malleshi@yahoo.com, gst@cftri.res.in (N.G. Malleshi).
0260-8774/$ - see front matter 2007 Published by Elsevier Ltd.
doi:10.1016/j.jfoodeng.2007.01.012
36
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of interest to examine its potential for dierent food products, exploratory studies on its expansion characteristics
were conducted and it was observed that, the decorticated
millet could be readily used for the preparation of
expanded millet (Malleshi & Ushakumari, 2004). However,
it was observed that, attening the decorticated millet to
near ellipsoid by a mild mechanical impact improves the
expansion capability of the grains and also the moisture
content of the kernels prior to attening and prior to
expansion inuences the expansion ratio. Since, expansion
ratio of the product is the main determinant of its food and
market value, the process parameters, namely, moisture
content of the millet before attening, shape factor and
also the moisture content before expansion, on the expansion characteristics of the millet were determined. For this
purpose, response surface methodology (RSM), using a
Central Composite Rotatable Design (CCRD) to t a second order polynomial by a least square technique was utilized (Hunter, 1959; Rastogi, Rajesh, & Shamala, 1998).
2. Material and methods
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2.1. Material
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The pericarp (glumes) covering the kernels was separated (deglumed) in a Engleburg huller (Sri Ganesha Engineering Works, Chennai, India) and the same was used for
the preparation of expanded millet. It was soaked in water
maintained at 68 2 C for 4 h, excess water was drained
o and the material was steamed at atmospheric pressure
(98 1 C) for 30 min and dried in an air drier at
38 1 C to 15 1% moisture content. The dried material
was decorticated in a horizontal corborandum disc mill as
per Shobana and Malleshi (2007), and the decorticated millet was used to study the expansion characteristics.
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A known weight of the decorticated millet placed in different glass containers and then individually sprayed with
4, 10, 21, 35 and 46 ml of additional water to raise the
moisture content of the samples from 15% to 40% and left
for equilibration for about 12 h with occasional mixing.
Followed by that, the samples were passed through a
heavy-duty roller aker (Aktiebolsget, Malmo, Germany)
to atten the grains to dierent degree of thickness. The
shape of the attened grains was quantied by measuring
the three main axes, a, b and c, perpendicular to each
other, using a dial calipers (Model 537, Mitutoyo, Japan)
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2.7. Sphericity
A second order polynomial equation was used to t the
experimental data given in Table 1. The model proposed
for the response (Yi) was,
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where a is the longest intercept, b the longest intercept normal to a, and c is the longest intercept normal to a and b.
The average of 10 independent determinations of sphericity was reported.
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abc1=3
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Y i a0 a1 X 1 a2 X 2 a3 X 3 a11 X 21 a22 X 22
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2.8. Hardness
The hardness of the expanded millet was measured using
the universal texture analyzer (Stable Microsystems, Model
TA-HDi, Surrey, UK). For this purpose the maximum
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Table 1
Treatment schedule for ve-factor CCRD and responses
Moisture content
(%, X1)
Shape factor
(X2)
Drying time
(min, X3)
Expansion ratio
(Y1)
Bulk density
(g/cm3, Y2)
Sphericity
(Y3)
Texture
(N,Y4)
Overall
acceptability (Y5)
20.07 (1)
34.93 (+1)
20.07 (1)
34.93 (+1)
20.07 (1)
34.93 (+1)
20.07 (1)
34.93 (+1)
15.0 (1.682)
40.0 (+1.682)
27.50 (0)
27.50 (0)
27.50 (0)
27.50 (0)
27.50 (0)
27.50 (0)
27.50 (0)
27.50 (0)
27.50 (0)
27.50 (0)
0.44
0.44
0.86
0.86
0.44
0.44
0.86
0.86
0.65
0.65
0.30
1.00
0.65
0.65
0.65
0.65
0.65
0.65
0.65
0.65
30.41 (1)
30.41 (1)
30.41 (1)
30.41 (1)
119.59 (+1)
119.59 (+1)
119.59 (+1)
119.59 (+1)
75 (0)
75 (0)
75 (0)
75 (0)
0 (1.682)
150 (1.682)
75 (0)
75 (0)
75 (0)
75 (0)
75 (0)
75 (0)
3.330
3.560
3.042
2.100
3.268
4.486
3.349
4.252
3.227
3.463
4.496
2.800
2.200
3.628
3.737
3.713
3.639
3.596
3.710
3.741
0.231
0.230
0.290
0.327
0.235
0.171
0.230
0.199
0.238
0.222
0.171
0.298
0.350
0.212
0.206
0.207
0.211
0.214
0.207
0.206
0.863
0.900
0.952
0.920
0.898
0.904
0.930
0.960
0.916
0.915
0.840
0.960
0.949
0.935
0.955
0.955
0.953
0.967
0.956
0.967
19.08
18.21
26.29
30.16
27.87
7.13
20.28
11.69
22.87
17.45
19.97
28.04
32.91
13.2
13.42
13.52
13.96
14.15
13.8
13.5
5.430
4.860
5.380
1.800
3.630
6.630
5.890
6.000
6.330
4.500
6.750
4.000
2.970
6.000
6.000
5.400
5.500
5.300
5.400
5.400
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(1)
(1)
(+1)
(+1)
(1)
(1)
(+1)
(+1)
(0)
(0)
(1.682)
(+1.682)
(0)
(0)
(0)
(0)
(0)
(0)
(0)
(0)
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The appearance, colour, texture, taste and overall quality of the expanded millet were evaluated by a trained panel
of 10 members on a nine point hedonic scale, ranking 1 for
dislike extremely and 9 for like extremely (Watts, Ylimaki, Jeery, & Elias, 1989). The average and the mean
values of the scores for each of the attributes were computed and analyzed statistically (Snedecor & Cochran,
1962).
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Five responses, namely, expansion ratio (Y1), bulk density (Y2), sphericity (Y3), texture (Y4) and overall acceptability (Y5), which describe the quality characteristics of
the expanded millet, were measured. The coecients for
the actual functional relations for predicting Yi are presented in Table 2. The non-signicant terms from the
model were omitted based on Students t-ratio (Khuri &
Cornell, 1987) and the polynomial was recalculated and
reported with the recalculated coecient of determination
(R2). All the ve responses under dierent combinations
as dened in the design (Table 1) were analyzed using the
analysis of variance (ANOVA) appropriate to the experimental design. The ANOVA for the data obtained using
CCRD presented in Table 3, indicates that, the sum of
squares due to regression (rst and second order terms)
was signicant. However, the lack of t was not signicant
for the expansion ratio as well as for the sphericity and also
for the overall acceptability, but it was signicant for bulk
density and texture. The high values of coecient of determination (R2) also suggest that the model is a good t. R2 is
the proportion of variability in response values explained
R2 values
*
**
Original
equation
Recalculated
equation
Original
equation
3.685
0.132*
0.348**
0.419**
0.091
0.016
0.244**
0.186*
0.354**
0.199*
3.628
0.132
0.348
0.419
0.209
0.006
0.029**
0.035**
0.005
0.007
0.023**
0.009
0.016**
0.017**
0.237
0.186
0.354
0.199
0.938
0.920
Signicant at 5% level.
Signicant at 1% level.
0.960
Sphericity (Y3)
Texture (N,Y4)
Original
equation
Original
equation
Recalculated
equation
Original
equation
0.959
0.003
0.029**
0.002
0.015**
0.021**
0.006
0.006
0.004
0.003
13.816
2.595**
2.175**
4.387**
1.675*
3.034**
2.698**
2.111*
4.041**
2.774*
13.816
2.595
2.175
4.387
1.675
3.034
2.698
2.111
4.041
2.774
5.504
0.302
0.447**
0.716**
0.054
0.068
0.383*
0.738**
0.908**
0.593**
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Recalculated
equation
0.218
0.029
0.035
0.022
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a0
a1
a2
a3
a11
a22
a33
a12
a13
a23
0.016
0.017
0.911
0.910
Recalculated
equation
0.954
0.029
0.015
0.020
0.855
0.933
0.933
0.912
Recalculated
equation
5.412
0.447
0.716
0.372
0.738
0.907
0.593
0.866
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Coecients
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Table 2
Estimated coecients of the tted second order polynomial representing the relationship between the responses and the process variables
Table 3
Analysis of variance for the tted second order polynomial model as per CCRD
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Sum of squares
Sphericity (Y3)
Texture (N,Y4)
3
6
9
4.292a
2.550a
6.842
0.028a
0.013a
0.041
0.012a
0.009a
0.021
419.485a
463.855a
883.340
10.969a
15.878a
26.847
Residual
Lack of t
Pure error
Total error
5
5
10
0.431b
0.017
0.448
0.0019a
5.64 105
0.002
0.0018b
0.0002
0.002
63.389a
0.478
63.867
2.268b
0.320
2.588
Grand total
19
7.290
0.043
0.024
df
Regression
First order terms
Second order terms
Total
a
b
Signicant at p 6 0.001.
Not signicant at p 6 0.001.
947.207
29.435
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40
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Fig. 2. Response surfaces showing the eect of shape factor and drying time on (a) expansion ratio; (b) bulk density; (c) sphericity; (d) overall
acceptability; (e) hardness. For all the experiments moisture content was constant at 40%. Levels are as shown in Table 1.
with the drying time for all the levels of shape factor
(Fig. 2e). The interaction term of shape factor and drying
time was found to be signicant (p 6 0.05, Table 2). The
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(A)
(B)
Hardness 5.0 N
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0.00
-0.42
0.42
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Drying
Dryingtime
time
0.84
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(C)
1.26
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(D)
1.68
41
-0.84
Sphericity 0.90
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-1.26
-1.68
-1.68
-1.26
-0.84
-0.42
0.00
0.42
0.84
1.26
1.68
Shape factor
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Fig. 3. Superimposed contour plots showing the shaded overlapping area for which expansion ratio P4.6, bulk density 60.17, sphericity P0.90.
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Table 4
Feasible and optimum conditions and also predicted (Pred.) and experimental (Exp.) values of the responses at optimum conditions
Optimum condition
Conditions A
Conditions B
Conditions C
Conditions D
Coded
Actual
Coded
Actual
Coded
Actual
Coded
Actual
Moisture (X1, %)
Shape factor (X2)
Drying time (X3, min)
1.68
0.70
1.09
40
0.50
126.57
1.68
0.47
1.01
40
0.55
120.49
1.68
0.10
1.34
40
0.63
144.78
1.68
0.45
1.68
40
0.55
170.59
Responses
Pred. value
Exp. valuea
Pred. value
Exp. valuea
Pred. value
Exp. valuea
Pred. value
Exp. valuea
4.78
0.16
0.90
4.79
7.53
4.70
0.15
0.91
4.50
7.40
4.64
0.16
0.91
4.93
7.21
4.55
0.15
0.90
4.85
7.12
4.61
0.17
0.92
3.89
7.25
4.58
0.16
0.91
3.79
7.15
4.82
0.17
0.91
3.15
7.83
4.77
0.16
0.90
3.25
7.60
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Acknowledgement
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4. Conclusion
Exploration of the response surfaces to optimize the
parameters inuencing the expansion of decorticated nger
millet were carried out and it was found that there exists a
complex interaction between the variables such as moisture
content, drying time and shape factor. The optimum conditions for preparing a product with highest expansion ratio
were found to be about 40% moisture content prior to attening, shape factor ranging from 0.52 to 0.58 and drying
time varying from 136 to 150 min. The expanded millet
obtained following these conditions will have expansion
ratio P4.6 with bulk density 60.17 g/cm3, sphericity
P0.90, hardness/texture 65.0 N and overall acceptability
P7.2.
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Thanks are due to Dr. Ravi, for the help towards the
measurement of the texture and to Mr. Jayaprakashan,
for the assistance in the attening experiments. The nancial support from ICAR, New Delhi, under AICRP on
Small Millets, for under taking this work is gratefully
acknowledged.
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