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Trivedi Global Inc., 10624 S Eastern Avenue Suite A-969, Henderson, NV 89052, USA
Trivedi Science Research Laboratory Pvt. Ltd., Hall-A, Chinar Mega Mall, Chinar Fortune City, Hoshangabad Rd., Bhopal- 462026, Madhya Pradesh, India
Abstract
Indium has gained significant attention in the semiconductor industries due to its unique thermal and optical
properties. The objective of this research was to investigate the influence of the biofield energy treatment on the
atomic, physical and thermal properties of the indium. The study was performed in two groups (control and treated).
The control group remained as untreated, and treated group received Mr. Trivedis biofield energy treatment.
Subsequently, the control and treated indium samples were characterized by the X-ray diffraction (XRD), Differential
scanning calorimetry (DSC), Thermogravimetric analysis (TGA), and Fourier transform infrared (FT-IR) spectroscopy.
The XRD diffractogram showed the shifting of peaks toward higher Braggs angles in the treated indium sample
as compared to the control. The crystallite size of treated indium sample were substantially changed from -80% to
150.2% after biofield energy treatment, as compared to control. In addition, the biofield energy treatment has altered
the lattice parameter (-0.56%), unit cell volume (-0.23%), density (0.23%), atomic weight (-0.23), and nuclear charge
per unit volume (1.69%) of the treated indium sample with respect to the control. The DSC showed an increase in
the latent heat of fusion up to 3.23% in the treated indium sample with respect to control. Overall, results suggest
that biofield energy treatment has substantially altered the atomic, physical, and thermal properties of treated indium
powder. Therefore, the treated indium could be utilized in thermal interface material in semiconductor industries.
Citation: Trivedi MK, Tallapragada RM, Branton A, Trivedi D, Nayak G, et al. (2015) Potential Impact of Biofield Energy Treatment on the Atomic,
Physical and Thermal Properties Indium Powder. J Material Sci Eng 4: 198. doi:10.4172/2169-0022.1000198
Page 2 of 6
metals and ceramics, this work was undertaken to evaluate the impact
of this on the atomic, physical, and thermal properties of the indium
using x-ray diffraction (XRD), differential scanning calorimetry (DSC),
thermogravimetric analysis (TGA), and Fourier transform infrared
(FT-IR) spectroscopy.
XRD study
XRD analysis of control and treated indium was performed on
Phillips, Holland PW 1710 X-ray diffractometer system, which had a
copper anode with nickel filter. The radiation of wavelength used by
the XRD system was 1.54056 . The data obtained from this XRD were
in the form of a chart of 2 vs. intensity and a detailed table containing
peak intensity counts, d value (), full width half maximum (FWHM)
(), relative intensity (%) etc. The crystallite size (G) was calculated by
using formula:
G = k/(bCos)
Here, is the wavelength of radiation used, b is FWHM of peaks
and k is the equipment constant (=0.94). Percentage change in
crystallite size was calculated using following formula:
Percentage change in crystallite size = [(Gt-Gc)/Gc] 100
Where, Gc and Gt are crystallite size of control and treated powder
samples respectively.
Further, crystal structure parameters such as lattice parameter,
unit cell volume of control and treated were computed using PowderX
software.
Thermal analysis
The thermal analysis of indium powder was performed using
DSC and TGA-DTA. The DSC was used to investigate the melting
temperature and latent heat of fusion (H) of samples. The control and
treated indium samples were analyzed using a Pyris-6 Perkin Elmer
DSC at a heating rate of 10C/min under air atmosphere and the air was
flushed at a flow rate of 5 mL/min. Predetermined amount of sample
was kept in an aluminum pan and closed with a lid. A blank aluminum
pan was used as a reference. Percentage change in latent heat of fusion
was calculated using following equations:
% change in Latent
=
heat of fusion
Where, H Control and H Treated are the latent heat of fusion of control
and treated samples, respectively. For TGA-DTA analysis, Mettler
Toledo simultaneous TGA-DTA was used to analyze the thermal
characteristics of indium powder. The samples were heated from
room temperature to 400C with a heating rate of 5C/min under air
atmosphere.
J Material Sci Eng
ISSN: 2169-0022 JME, an open access journal
FT-IR spectroscopy
FT-IR spectra were recorded on Shimadzus Fourier transform
infrared spectrometer (Japan) with frequency range of 4000-500
cm-1. The analysis was accomplished to evaluate the effect of biofield
treatment on dipole moment, force constant and bond strength in
chemical structure [23].
Citation: Trivedi MK, Tallapragada RM, Branton A, Trivedi D, Nayak G, et al. (2015) Potential Impact of Biofield Energy Treatment on the Atomic,
Physical and Thermal Properties Indium Powder. J Material Sci Eng 4: 198. doi:10.4172/2169-0022.1000198
Page 3 of 6
Control
Treated (T1)
2 (degree)
Plane (hkl)
2 (degree)
Relative
Intensity
FWHM
(degree)
Crystallite size
(nm)
2 (degree)
Relative
Intensity
FWHM
(degree)
Crystallite size
(nm)
32.965
101
32.95
100
0.1
107.9
33.08
36.32
36.29
11
0.06
217.8
36.44
100
0.1
107.9
51.2
0.06
39.17
110
39.15
21.1
0.1
109.8
39.29
47.1
0.12
217.8
87.9
54.47
112
54.44
6.5
0.12
93.1
54.6
26.1
0.06
232.9
56.56
200
56.58
21.6
0.06
235.1
56.73
16.1
0.08
156.8
63.204
103
63.21
23.5
0.06
243.2
63.33
13.9
0.06
243.2
67.034
211
67.04
35.6
0.08
165.6
67.19
5.8
0.32
33.1
69.115
202
69.11
4.4
0.06
251.5
69.24
9.4
0.08
167.8
Table 1: Effect of biofield energy treatment on relative peak intensity, Braggs angle, and crystallite size of indium powder.
Group
Lattice
parameter
()
Control
Unit cell
Density
volume
(g/cc)
( 10-23 cm3)
Atomic
weight
(g/mol)
Nuclear
charge per
unit volume
( C/m3)
3.250
5.2280
7.36745
115.993
436233
5.2161
7.38425
115.729
443612
Percent
Change
-0.23
0.23
-0.23
1.69
-0.56
Table 2: Effect of biofield energy treatment on lattice parameter, unit cell volume
density atomic weight, nuclear charge per unit volume of indium powder.
Thermal analysis
200.0
Percent change in
crystallite size
150.0
100.0
50.0
0.0
-50.0
-100.0
101
002
110
112
200
103
211
202
Crystalline Plane
substitution of small radii atoms, the lattice constant of unit cell decrease
and that results into higher Braggs angle. Thus, based on shifting of
XRD peaks and reduction in the lattice parameter, it is assumed that
biofield treatment might induce compressive stress in treated indium
powder and that might be responsible for internal strain in treated
J Material Sci Eng
ISSN: 2169-0022 JME, an open access journal
Citation: Trivedi MK, Tallapragada RM, Branton A, Trivedi D, Nayak G, et al. (2015) Potential Impact of Biofield Energy Treatment on the Atomic,
Physical and Thermal Properties Indium Powder. J Material Sci Eng 4: 198. doi:10.4172/2169-0022.1000198
Page 4 of 6
FT-IR spectroscopy
FT-IR spectra of the control and treated indium samples are
presented in Figure 4. FT-IR spectra showed absorption peak at 3768
and 3730 cm-1 in control and treated indium sample, which could be
due to O-H stretching vibration. The absorption peak found at 3028
and 2997 cm-1 in control and treated indium sample respectively,
due to CO2 absorption from atmosphere. In addition, the absorption
peaks observed in control sample at 569 and 416 cm-1 attributing to
indium-oxide bonding vibrations were changed to 565 and 435 cm-1 in
Parameter
Control
T1
T2
T3
159.94
157.61
157.72
157.50
-1.45
-1.38
-1.52
26.92
27.70
27.79
27.60
2.89
3.23
2.52
Percent change in H
Control
T1
T4
18.13
16.69
11.64
155.94
156.11
156.23
26.83
27.44
25.64
-9.041
-3.31
3.07
Citation: Trivedi MK, Tallapragada RM, Branton A, Trivedi D, Nayak G, et al. (2015) Potential Impact of Biofield Energy Treatment on the Atomic,
Physical and Thermal Properties Indium Powder. J Material Sci Eng 4: 198. doi:10.4172/2169-0022.1000198
Page 5 of 6
7. Yu JK, Kang SG, Jung KC, Han JS, Kim DH (2007) Fabrication of nano-sized
ITO powder from waste ITO target by spray pyrolysis process. Mater Trans
48: 249-257.
Conclusion
8. Choi D, Hong SJ, Son Y (2014) Characteristics of indium tin oxide (ITO)
nanoparticles recovered by lift-off method from TFT-LCD panel scraps.
Materials 7: 7662-7669.
The XRD analysis showed that the alteration in crystallite size from
-80% to 150.2% in the treated indium as compared to control. The
lattice parameter, unit cell volume, density, atomic weight, and nuclear
charge per unit volume of the treated powder were altered after biofield
treatment. In addition, a significant alteration in relative intensities of
all XRD peaks suggested the modification in crystal morphology of
treated indium after biofield energy treatment. Besides, the thermal
analysis results indicated the increase in latent heat of fusion (upto
3.23%), which could be due to increase in interatomic attractive force
in treated sample. Overall, the result demonstrated that Mr. Trivedis
biofield energy treatment could be applied to modify the thermal and
physical properties of indium for semiconductor industries.
Acknowledgement
Authors thank Dr. Cheng Dong of NLSC, Institute of Physics, and Chinese
academy of sciences for permitting us to use Powder-X software for analyzing
XRD results. The authors would also like to thank Trivedi Science, Trivedi Master
Wellness and Trivedi Testimonials for their support during the work.
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Citation: Trivedi MK, Tallapragada RM, Branton A, Trivedi D, Nayak G, et al. (2015) Potential Impact of Biofield Energy Treatment on the Atomic,
Physical and Thermal Properties Indium Powder. J Material Sci Eng 4: 198. doi:10.4172/2169-0022.1000198
Page 6 of 6
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