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of ceramics
and glasses
G. F. Raisera)
Division of Engineering, Brown University, Providence, Rhode Island 02912
J. L. Wise
Organization 1433, Sandia National Laboratories, Albuquerque, New Mexico 87185
R. J. Clifton
Division of Engineering, Brown Vniversity, Providence, Rhode Island 02912
11 January 1994)
Soft-recovery plate impact experiments have been conducted to study the evolution of damage
in polycrystalline Al,O, samples. Examination of the recovered samples by means of scanning
electron microscopy and transmission electron microscopy has revealed that microcracking
occurs along grain boundaries; the cracks appear to emanate from grain-boundary triple points.
Velocity-time profiles measured at the rear surface of the momentum trap indicate that the
compressive pulse is not fully elastic even when the maximum amplitude of the pulse is
significantly less than the Hugoniot elastic limit. Attempts to explain this seemingly anomalous
behavior are summarized. Primary attention is given to the role of the intergranular glassy phase
which arises from sintering aids and which is ultimately forced into the interfaces and voids
between the ceramic grains. Experiments are reported on the effects of grain size and glass
content on the resistance of the sample to damage during the initial compressive pulse. To
further understand the role of the glass, plate impact experiments were conducted on glass with
chemical composition comparable to that which is present in the ceramic. These experiments
were designed to gain further insight into the possibility of failure waves in glasses under
compressive loading.
I. INTRODUCTlON
The dynamic recovery plate impact experiment has
been considered an attractive method for evaluating the
brittle behavior of ceramics for two main reasons. First,
since microdamage in ceramic materials takes place at very
rapid rates, these experiments provide a means of initiating
microcracks but removing the loads before the microcracks
coalesce into large-scale cracks and rupture the material.
Second, if the plate thicknesses and geometries are chosen
correctly, it is possible to subject the central region of the
specimen to a well-known stress history and still recover it
for microscopy studies.
Several studies have utilized some of these ideas in
plate impact experiments designed to study damage mechanisms in ceramics and ceramic-related materials. Yaziv
used a double-impact technique which led him to characterize tensile damage as comprising a spa11 zone. Longy
and Cagnoux used spa11 and recovery experiments to
study how certain microstructures of alumina ceramics affect their spa11properties and their Hugoniot elastic limit
(HEL). Louro3 tested different aluminas under various
stress pulse durations and magnitudes to highlight how
porosity and grain size alter their dynamic damage properties. Stress histories in the ceramic were unfortunately
indeterminate, and post-test analyses were limited to gross
effects on recovered fragments. This is because these invesakurrent
3882
0021-8979/94/75(8)/3862/8/$6.00
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experiments
on A1203
3863
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Beam
Second Pulse
M2
Photodiodes
rl3lT
Lens
To Monitoring
FIG. 2. Lagrangian
f-X
source (a = 587.6 mn), and subsequently cleaned ultrasonically. The ceramic specimens are prepared for vapor deposition in a solution of hydrogen peroxide and sulfuric
acid.8 An aluminum layer < 0.1 ym thick is then vapor
deposited in the pattern of four tabs surrounding a central
cross, each tab being electrically isolated on the nonconducting alumina specimen. These conductive tabs and the
cross provide a means of measuring tilt as well as a reflective surface for pm-impact alignment of the star flyer and
specimen. The projectile is assembled and a Delrin key is
inserted in a piston at the back of the projectile. This key
fits into a slot in the gun barrel and prevents rotation of the
projectile during its acceleration toward the target. The
specimen and momentum trap are assembled with four
small drops of epoxy between them at the corners. For
production of extensive tensile damage a sputtered layer of
material several micrometers thick is deposited on the four
corners of the momentum trap prior to assembly to provide
a prescribed gap between the plates. The assembly is then
bonded inside the aluminum holder at the precise location
to make projectile-anvil
impact coincide with flyerspecimen impact. The disposable brass nose, which protects the anvil from damage during numerous impacts, is
then applied with epoxy. Tilt wires are attached outside the
impact area to each of the vapor deposited tabs and to the
central cross on the specimen. These wires are fed into a
logic box and the output is monitored on an oscilloscope
used for tilt measurement. Tilts of less than 1 x 10e3 rad
are routine. The target assembly is aligned with the star
flyer using a technique developed by Kumar and Clifton,15
which renders respective faces parallel to an accuracy of
2.0~ 10m5 rad. After alignment the projectile is pulled
back to the breech end of the gun barrel and a velocity
system similar to the one described by Fowles et al. l6 is
installed at the muzzle. The accuracy of this system is
better than 1%. A disposable mirror is suspended behind
the momentum trap and the laser system is set up to monitor surface motion caused by the stress waves in the experiment. For these experiments, all interferometer data is
confined to a 4 mm square region in the center of the
3864
Surface
on glass
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NosepieceIlmpactor
from this surface will be weak, and will return to the glass
rear surface through region 6 causing little or no reduction
in free surface particle velocity. The dotted line maps the
path of a reported recompression wavei1-13 arising from
the release wave interaction with the failure wave. The
occurrence of such a wave is explained on the basis of the
failed material having a lower impedance than the unfailed
material.
The 6061-T6 aluminum flyer plate is lapped and polished on both sides to a roughness of 0.02 pm rms. The
Corning aluminosilicate glass is cut, lapped, and polished
by Precision Glass Products Co. of Oreland, PA. Its flatness is measured as in Sec. II A and is better than four
rings. The 60-40 polish has an average roughness of 0.04
pm rms. A thin ( -500 nm) coating of aluminum is applied to the rear surface of the glass to give it the necessary
reflectivity for laserinterferometry measurements. In shots
requiring a rough glass impact face, the glass is lapped
for 0.5 h using 15 pm B&! powder, giving a surface roughness of 0.52 pm rms. An epoxy bond around the targetplate periphery holds the glass concentricially within a
standard aluminum support ring. The impact surface of
the glass is flush with the front face of this ring. Impact
velocity and tilt are measured using coaxial shorting pins
mounted in this ring. The particle velocity history is measured using a VISAR.~ The fringe constants are 0.4028
mm/,&fringe
for shots GLASS1 and GLASS2 and 0.1988
mm/,&fringe
for shots GLASS3 and GLASS4. The two
quadrature records and the beam intensity variation are
recorded on LeCroy digitizers (previously described).
Data reduction is carried out using VISARSS, a program
developed at Sandia.2*
experiments
3865
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SHOT 92-08
0.07
Exp. Data
SHOT 89-05
- - - Elastic Prediction
0.07
1-1 ElasticP
1500 T
1500
0.06
0.06
0.05
loo0
0.04
0.03
0.02
IWO
0.04
0.05
0.03
0.02
500
0.01
8
500
0.01
0.00
-250
260
500
Tlms[me]
Time [nsoc]
SHOT 92-l 1
m,....,--..,-...,-.-.,.~..,--.*,
SHOT 92-09
0.06~.,....,....,....,....,....,...~
-
0.07
0.05
0.06
f7
0.03
0.04
0.02
- - - Elastic Prediction
.Data
250
---
500
ElasticF
750
lool
Time [nut]
Time [nsoc]
FIG. 6. Experimental particle velocity vs time data for shots 92-08 (elastic shot: steel specimen), 89-05 (Coors Vista1 specimen), 92-09 (Coors AD-995
specimen), and 92-11 (Coors AD-999 specimen).
Results from tests run on three different sintered aluminas from Coors Porcelain Co. of Boulder, CO, are also
presented in Fig. 6. Test parameters and ceramic material
properties are summarized in Table I. All shots were conducted at nearly the same stress level, using the same star
flyer and momentum trap materials (Ti6Al4V and Hampden steel, respectively). Comparisons between certain
shots where specimens differ primarily in only one microstructural feature allow conclusions to be made about that
features effect.
Shots 89-05 and 92-09 were performed using Coors
Vista1 and Coors AD-995, respectively. As shown in Table
I, AD-995 has an average grain size similar to Vista1 (17
pm for AD-995,20 pm for Vistal), but more intergranular
Shot
No.
Impact
stress
WI%)
89-05
92-09
92-l 1
92-14
1291
1372
1473
1476
Material
Specific
gravity
Average
grain size
(pm)
wt % Al,O,
(preprocessing)
Longitudinal
wave speed
(mm/w)
Porosity
(%b)
Coors Vista1
Coors AD-995
Coors AD-999
Browna HP Al,O,
3.99
3.89
3.96
3.96
20
17
3
2.4
99.9
99.5
99.9
99.99
10.8
10.45
10.2
10.9
0.0
2.3
0.7
0.8
Raiser et a/.
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SHOT 92-14
XT
3
2
!i.a
0.06
0.07
1500
z
z
0.05
0.04
1000
0
R
8yg
0.03
0.02
500
P(D
E
tj
z
0.01
0.00
-250
250
500
750
1000
1250
150;
Time [nsec]
FIG. 7. Experimental particle velocity vs time data for shot 92-14 (hotpressed alumina).
examination
3867
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PI
(4
FIG. 8. SEM micrographs of (a) compression-dominated region in Coors AD-995; (b) tension-dominated region in Coors AD-995; (c) compressiondominated region in hot-pressed alumina; (d) tension-dominated region in hot-pressed alumina.
. . . . . .......(..~~.
--Smooth - 0.04~ rms
- - - -Rough - 0.52~ rms
Estimated Recompression
EstimatedUnloading
2 1.00
.E.
*is8 0-. 75
z
a 0.50
g
g
Shot
No.
Impact
velocity
b-44
Shock
stress
(GW
Impact surface
roughness
(8, ms)
Nonzero
spa11
strength
GLASS 1
GLASS2
GLASS3
GLASS4
0.961
0.965
0.450
0.443
7.88
7.51
3.42
3.33
100
5300
700
5100
no
no
yes
yes
3868
q.25
0.00
0.0
0.5
1.0
1.5
2.0
2.5
3.0
Time(psec)
FIG. 4. Experimental particle velocity vs time data for spall experiments
on glass.
Raiser et
a/.
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Raiser et a/.
3869
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