Vietsovpetro Experiment PDF

EURONAVY PAINTS A REVOLUTION IN COATING INDUSTRY
REPORT
ON
TESTS ASSESSMENTS
OF EURONAVY PAINTS
AT
VIETSOVPETRO JOINT-STOCK
ENTERPRISE
JUNE 2009
HIGH TECHNOLOGY PETROCHEMICAL JOINT-STOCK COMPANY (HI-PEC)
Add: 26- 34 Le Van Linh st., ward 12, district 4, Ho Chi Minh city, Vietnam
Tel: +84.8.39434480
+84.8.39434482
Fax: + 84.8.39434481
Email: info@hi-pec.com.vn
Website: http://www.hi-pec.com.vn
TABLE OF CONTENTS
EXECUTIVE SUMMARY
TESTING PROCESS AND RESULTS
I.
General introduction
II.
Testing process
1.
Surface preparations
2.
Euronavy paint system
3.
Tests and assessments

a.
Film thickness tests
b.
Holiday tests
c.
Pull-off tests
III. Photo reports

APPENDICES

Address: 26- 34 Le Van Linh st., ward 12, district 4, Ho Chi Minh city, Vietnam
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Fax: + 84.8.39434481
page 1
EXECUTIVE SUMMARY
Vietsovpetro Joint-Venture Enterprise
(VSP), under the Vietnam National
Oil and Gas Group (Petrovietnam), was founded by the governments of Vietnam
and former Soviet Union in proportion of 50:50.
VSP whose headquarter is located at 105 Le Loi st., Vung Tau city was
established in 1981. It is the biggest and most effective enterprise in Vietnam with
its yearly oil and gas export capacity of about 10 million tons.
During 28 years operation, VSP has exploited over 150 million tons of oil
equivalent bringing nearly US$ 38 billion profit to both parties and contributing
some 15%-22% income of Vietnams state budget.
During its construction and development, VSP has invested billions US
dollars in construction of a strong material basis: 12 fixed oil exploitation platforms,
2 central technology platforms, 9 light frame-works, 4 water pressure pumping
frame-works, 3 floating oil storage tanks, 2 mobile drilling platform, 2 air pressing
frame-works, over 400 kilometers of internal pipelines and 17 floating facilities
including bulk boats, service vessels, diving ships, fire-fighting ships and a shore
infrastructure complex. The enterprise is now joining with Petrovietnam to expand
their operations to more countries.
With its capability and long-term development strategy, VSP yearly invests
hundreds of millions of US dollars in maintaining, repairing its huge material basis
and in building new ships, drilling platforms, ect.
Due to the specific marine environment, most structures are highly
corrosively affected. On the other hand, oil and gas are inflammable so
technologies, equipments and materials must be in high quality according to strict
standards. The enterprise has its own Nipi research institute which has an anticorrosion research division.
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Relying on actual demands, the institute has researched and issued technical
specifications for anti-corrosive coats and surface preparation methods. Basing on
the research results, VSP promulgated standards and processes for tests and
evaluations on materials and paints in the whole enterprise.
As the enterprises processes, new paint applications to its structures must be
carried out in accordance with the following steps:
1.
Permission from VSPs leader
2.
A seminar representing new paints to paint using units, anti-corrosive

departments and Nipi institute
3.
Paint firms study VSPs procedures and offer technical diagrams as per
VSPs stipulations
4.
Tests and evaluations on paints at the laboratory as per VSPs stipulations
5.
Tests at the platforms, VSPs production bases
6.
Overall evaluations
7.
Acceptance for new paint applications at VSP
Hi-Pec and Euronavy International carried out the following steps in an attempt to
apply Euronavy paints to VSP:
1. Guideline
According to Hi-Pecs official document no. 0705/CV-HIPEC dated May
12th, 2009, VSPs general director approved tests and assigned Nipi Institute
the leadership.
2. Seminars
Hi-Pec/Euronavy organized 2 seminars:
-
In the first seminar (2006), Mr. Joao, Euronavys Technical Director,

presented Euronavy paints to about 30 experts from VSP.

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In the second seminar (2008), Doctor Nguyen Thanh Hai, Chairman of

Hi-Pecs Management Board, presented to about 20 experts from VSP.
The seminars achieved great success. Hi-Pec/Euronavy got permission from

VSPs leader to carry out Euronavy paint tests.
3. Paint application diagrams and technical procedures
The diagrams and processes are designed for:
-
Projects of building new ships, platforms.
Projects of repairing platforms, ships and other structures.
Hi-Pec/Euronavy sent technical proposals and paint diagrams for ships and
platforms to VSP. The number of 27 paint diagrams issued by VSP was
reduced to 7 due to Euronavy paints preeminent and versatile properties.
The number of 28 paint types for ship coating was also reduced to 8.
4. Tests in the laboratory
The tests comprised of 2 steps:
Surface preparation and paint applications as per stipulated processes
Tests at the laboratory, including:
-
Film thickness tests
Holiday tests
Pull-off tests
Tests on safety properties (testing toxicant content in the product) in

accordance with the standard applied to fresh water storage tanks
On June 8th, 2009, Hi-Pec brought its ultra high pressure water injecting machine
and relevant equipments to VSP for tests.
The concrete testing process is described as follows:

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TESTING PROCESS
AND
RESULTS

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I. General introduction
With the permission from VSPs chief engineer, on June 1st, 2009, Hi-Pec
carried out Euronavy paint tests as per VSPs process ITT-FSO-AKP-05 (refer to
appendix 1).
1. Applied standards:
Standards and specification tables used in the tests comprised of:
- Standard for surface preparation by grit blasting: ISO 8501-1
- Standard for surface preparation by ultra high pressure water injection:
SSPC SP 12
- Standard for surface preparation by power tools before paint application:
SSPC SP 03
- Standard for sweeping oil and grease from the surface before paint
application: SSPC SP - 01
- Standard for holiday tests: NACE RP 0188
- Standard for pull-off tests: ASTM D 4541
- VSPs coating technology: No. BC-MSP (BK)-AZ-07.1999
- Paint application guides of the paint producer
2. Assessment committee
Science Research and Design Institute (NIPI) leader
VSPs Offshore Structure Exploration and Repair Division
Offshore Structure Engineering and Repair Enterprise
Exploitation Enterprise
Marine Transport and Diving Service Enterprise
Euronavy Internationals representative
High Technology Petrochemical Joint-Stock Company (Hi-Pec),

Euronavys exclusive representative in Vietnam.

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3. Place and time:

Euronavy paint tests were carried out as follows:
- Surface preparation and applications of Euronavy coating samples (samples
1, 2, 5, 6, 7, 8, 9) at the Engineering Enterprises shot blasting workshop
from 9th to 12th June, 2009.
- Surface preparation and applications of Euronavy coating samples (samples
3 and 4) at the Anti-corrosive Laboratory of VSP from 18th to 19th June,
2009.
- Gauges, tests and evaluations of tested paint films at the Anti-corrosive
Laboratory from 23rd to 25th June, 2009.
4. Euronavy coating systems

a. Sample list
Sample 1: Underwater part of ship hull (below load line)
Sample 2:
Topside part of ship hull (above load line)
Sample 3:
Non-insulated facilities operating at the temperature from 400

600C
Sample 4:
Galvanized steel surface on atmospheric zone
Sample 5:
Fresh water tanks
Sample 6:
Ballast tanks (Grit blasting to standard SA2.0; after washing with

fresh water)
Sample 7:
Ballast tanks (Ultra high pressure water injection to standard Wj2)
Sample 8:
Ballast tanks (Power tool cleaning to standard St3; after washing

with fresh water)
Sample 9:
Recovering of holes, pitting and corroded steel surfaces on

offshore structures
b. Euronavy paint systems (refer to appendix 2)
5. Criteria for assessments

According to VSPs procedures and stipulations (refer to appendix 1)
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II. Testing process

1. Surface preparations:
Ultra high pressure water injection (UHP) to standard Wj2
Carried out by Hi-Pec
Performance place: VSP Port Vung Tau
Time: June 9th, 2009
Monitored and inspected by Assessment Committee led by VSPs
Nipi Institute (VSP Committee)
Grit-blasting to standard SA2.5 and AS2.0

Carried out by VSP Port Exploitation Enterprise
Monitored and inspected by VSP Committee
Power tool cleaning to standard St3

Steel samples used for tests were provided by VSP. After prepared by HiPec, all the samples were inspected and approved of paint application by
VSP Committee.

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2.
Euronavy paint systems
a.
Technical requirements (refer to appendix 1)
b.
Euronavy paint systems for tests at VSPs laboratory (refer to

appendix 2)
Sample 1:
Underwater part of ship hull (below load line)

Performance schedule:
Dates
Coats
Product names
June 9th, 2009
1st
Euro Basic ES301K62
June 10th, 2009
2nd
Euro Basic ES301K10
June 11th, 2009
3rd
Euro Basic ES301K62
June 11th, 2009
4th
Euro Sealer TE08
June 12th, 2009
5th
Euro antifouling AF2160
Sample 2:
Topside part of ship hull (above load line)

Dates
Coats
Product name
June 9th, 2009
1st
Euro Basic ES301K62
June 10th, 2009
2nd
Euro Basic ES301K10
June 11th, 2009
3rd
Euro urethan3PU16

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Sample 3:
Non-insulated facilities operating at the temperature from

400 600C

Performance place: VSP Anti-corrosion Laboratory (Nipi Institute)
Monitored and inspected by Nipi Institute
Dates
Coats
June 18th, 2009
1st
Euro Alt 600 AT02
June 18th, 2009
2nd
Euro Alt 600 AT02
June 19th, 2009
3rd
Euro Alt 600 AT02
Sample 4:
Product name
Galvanized steel surface on atmospheric zone

Performance place: VSP Anti-corrosion Laboratory (Nipi Institute)
Dates
Coats
June 18th, 2009
1st
Euro Shop WP04
June 18th, 2009
2nd
Euro urethan3 PU16
June 19th, 2009
3rd
Euro urethan3 PU16
Sample 5:
Product name
Fresh water tanks

Dates
Coats
Product name
June 9th, 2009
1st
Euro Basic ES301K62
June 10th, 2009
2nd
Euro Wall ES303W
June 11th, 2009
3rd
Euro Wall ES303W

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Sample 6:
Ballast tanks (Grit blasting to standard SA2.0; after washing

with fresh water)

Dates
Coats
Product name
June 9th, 2009
1st
Euro Basic ES301K62
June 10th, 2009
2nd
Euro Basic ES301K10
Sample 7:
Ballast tanks (Ultra high pressure water injection to standard Wj2)

Dates
Coats
Product name
June 9th, 2009
1st
Euro Basic ES301K62
June 10th, 2009
2nd
Euro Basic ES301K10
Sample 8:
Ballast tanks (Power tool cleaning to standard St3; after

washing with fresh water)

Dates
Coats
Product name
June 9th, 2009
1st
Euro Basic ES301K62
June 10th, 2009
2nd
Euro Basic ES301K10

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Sample 9:
Recovering of holes, pitting and corroded steel surfaces

on offshore structures

Dates
Coats
Product name
June 9th, 2009
1st
Euro Basic ES301K62
June 10th, 2009
2nd
ES307 + glass fiber
June 10th, 2009
3rd
ES307 + glass fiber
June 11th, 2009
4th
ES307 + glass fiber
June 12th, 2009
5th
Euro urethan3 PU16

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III. Tests and assessments

1. Film thickness tests
Performance steps
-
Wet film thickness test: VSP directly inspected the painting processes,
measured and recorded exactly the results with specialized meters.
Dry film thickness test: VSP measured all dry film thickness of 8
samples (except sample 9) with Elecometer 415.
Conclusion
All samples met VSPs standards and VSP approved for next testing
steps.
2. Holiday tests (NACE RP 0188-88)

Performance steps
- Film thickness tests
- Selection of appropriate electric current
- Holiday tests
Results (refer to appendix 3)
Sample 1: OK
Sample 2: OK
Sample 3: (no action)
Sample 5: OK
Sample 6: OK
Sample 7: OK
Sample 8: OK
Conclusion
All tested samples got satisfactory results, no error of the paint films was
found. This proves the solvent free paints preeminence.
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3. Pull-off tests (ASTM D 4541)

Performance steps
- Preparing the surface with glass-paper
- Gluing dollies onto the prepared surface with epoxy adhesive
- Keeping the dollies fixed for about 24 hours with adhesive tape
- Cropping paint coat (to the steel surface) around the dollies
- Pul-off tests
Because results of pull-off tests depend on applied testers and standards, VSP
Committee used 3 following testers to measure:
1.
Mechanical tester, provided by VSP with the maximum

measurement limit of 7.0 MPA
2.
Hydraulic twisting tester, provided by Hi-Pec with the maximum

measurement limit of 25 MPA
3.
Hydraulic pressing tester, provided by an intermediary company

with the maximum measurement limit of 25 MPA
Among above equipments, hydraulic pressing tester is considered most

accurate.
According to Standard ASTM D 4541-02, the value of adhesive strength of
tested coatings measured with mechanical testers and hydraulic testers can be in
difference of 1.77 times.
Results (refer to appendix 3)
-
The minimum result required by VSP: 2.5 MPA (with mechanical

testers)
The measurement results of all sample paint coats were much higher
than VSPs requirement.
Some samples could not be recorded because they exceeded the

maximum measurement limit of the testers (more than 7 MPA with Fixed
Alignment Pull-off Tester; more than 25 MPA with Self-Alignment Tester)
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IV. Conclusion
-
The results of the laboratory tests show that Euronavy paints not only met
but also exceeded the standards required by VSP with many prominent advantages
such as:
Solvent free, non-flammable
Non-toxic, general-purpose
Compatible with surfaces prepared by grit blasting, power tools or
high pressure water injection
Simple and easy to apply
Independent of climatic conditions and humidity
Compatible with wet, damp and flash-rusted surfaces
No profile required
Glossy, regular, non-void and very hard paint film
Very high results of all samples in pull-off tests
In brief, Euronavy paints have preeminent, general-purpose properties, easy to
use and safe for the users and the environment.
-
VSP approved of the testing results and agreed for Hi-Pec/Euronavy to
perform next tests on VSPs field according to Euronavy paint systems.

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PHOTO REPORT

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I.
Seminar
Photo No.1: Hi-Pecs representative is presenting at the seminar
Photo No.2: VSPs officals are studying documents of Euronavy paints

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Photo No.3: Discussions at the seminar
Photo No.4: Discussions at the seminar

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II. Preparations before tests
Photo No.5: Hi-Pecs presentation of testing program
Photo No.6: Hi-Pecs ultra high pressure water injecting machine (2,000 bars)
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Photo No.7: Nipi Institutes official is writing down technical information of

Euronavy paints

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III. Surface preparations

1. Cleaning by ultra high pressure water injection
Photo No.8: Preparation for ultra high pressure water injection (2,000 bars)
Photo No.9: Ultra high pressure water injection (2,000 bars)

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Photo No.10: Surfaces condition after Ultra high pressure water injection
Photo No.11: Surfaces condition after Ultra high pressure water injection

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2. Cleaning by grit blasting
Photo No.12: Surfaces condition after grit blasting
Photo No.13: Surfaces condition after grit blasting

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3. Cleaning by power tools
Photo No.14: Power tool cleaning
Photo No.15: Surfaces condition after power tool cleaning

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IV. Paint application
Photo No.16: 1st coat application with ES301K62
Photo No.17: Wet film thickness test

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Photo No.18: Wet film thickness test
Photo No.19: Completion of 1st coat

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Photo No. 20: 2nd coat application with ES301K10
Photo No.21: Completion of 2nd coat

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Photo No.22: Gluing fiberglass onto the surface
Photo No.23: Coating special adhesive on the fiberglass

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Photo No.24: Paint application to high temperature surface area (400 - 600C)
Photo No.25: Paint application to galvanized steel surface

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Photo No.26: Ultraviolet resistant coating
Photo No.27: Completion of all processes before tests

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Photo No.28: A completed paint sample

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V. Testing process
1. Checks on testing equipments
Photo No.29: VSP Committees checks of testing equipments
Photo No.30: Checks on testing equipments before tests

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2. Dry film thickness test
Photo No.31: Testing dry film thickness
Photo No.32: Recording results of dry film thickness tests

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3. Holiday test
Photo No. 33: VSP Committee is carrying out holiday test
Photo No. 34: VSP Committee is carrying out holiday test

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4. Pull-off test
Photo No.35: Euronavys expert is preparing the surface before gluing dollies
Photo No.36: The expert is applying glue on a dolly

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Photo No.37: The expert is attaching dollies onto the sample paint coat
Photo No.38: The expert is making the dollies fixed

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Photo No.39: Completion of dolly attachment

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5. Measurement with a mechanical tester
More
than
7 MPA
Photo No.40: Measurement with Fixed Alignment Pull-off Tester,

type II (D4541-02). The dolly could not be pulled off.
Fixed Alignment Pull-off Tester, type II

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6. Measurement with a twisting hydraulic tester
22.18
MPA
Photo No.41: Measurement with Self - Alignment Tester, type III (D4541-02)
Self - Alignment Tester, type III

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7. Measurement with a pressing hydraulic tester
More
than
25 MPA
Photo No.42: Measurement with Self - Aligning Tester, type V (D4541-02)
Self - Aligning Tester, type V

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More
than
25 MPA
Photo No.43: Exceeding the maximum limit of the tester,

the dolly is still not pulled off
Paint
forever!
Photo No.46: All parties rejoice on the result of over 25 MPA.

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APPENDICES

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Appendix 1

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Appendix 2

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Appendix 3

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EURONAVY PAINTS A REVOLUTION IN COATING INDUSTRY

Euronavy paint system

Tests and assessments

Film thickness tests

III. Photo reports

HIGH TECHNOLOGY PETROCHEMICAL JOINT-STOCK COMPANY (HI-PEC)

(VSP), under the Vietnam National

Permission from VSPs leader

A seminar representing new paints to paint using units, anti-corrosive

Tests and evaluations on paints at the laboratory as per VSPs stipulations

Tests at the platforms, VSPs production bases

Acceptance for new paint applications at VSP

In the first seminar (2006), Mr. Joao, Euronavys Technical Director,

HIGH TECHNOLOGY PETROCHEMICAL JOINT-STOCK COMPANY (HI-PEC)

In the second seminar (2008), Doctor Nguyen Thanh Hai, Chairman of

The seminars achieved great success. Hi-Pec/Euronavy got permission from

Projects of building new ships, platforms.

Projects of repairing platforms, ships and other structures.

Film thickness tests

Tests on safety properties (testing toxicant content in the product) in

The concrete testing process is described as follows:

HIGH TECHNOLOGY PETROCHEMICAL JOINT-STOCK COMPANY (HI-PEC)

HIGH TECHNOLOGY PETROCHEMICAL JOINT-STOCK COMPANY (HI-PEC)

Science Research and Design Institute (NIPI) leader

VSPs Offshore Structure Exploration and Repair Division

Offshore Structure Engineering and Repair Enterprise

Marine Transport and Diving Service Enterprise

Euronavy Internationals representative

High Technology Petrochemical Joint-Stock Company (Hi-Pec),

HIGH TECHNOLOGY PETROCHEMICAL JOINT-STOCK COMPANY (HI-PEC)

3. Place and time:

4. Euronavy coating systems

Topside part of ship hull (above load line)

Non-insulated facilities operating at the temperature from 400

Galvanized steel surface on atmospheric zone

Fresh water tanks

Ballast tanks (Grit blasting to standard SA2.0; after washing with

Ballast tanks (Ultra high pressure water injection to standard Wj2)

Ballast tanks (Power tool cleaning to standard St3; after washing

Recovering of holes, pitting and corroded steel surfaces on

b. Euronavy paint systems (refer to appendix 2)

5. Criteria for assessments

II. Testing process

Grit-blasting to standard SA2.5 and AS2.0

Power tool cleaning to standard St3

HIGH TECHNOLOGY PETROCHEMICAL JOINT-STOCK COMPANY (HI-PEC)

Euronavy paint systems

Technical requirements (refer to appendix 1)

Euronavy paint systems for tests at VSPs laboratory (refer to

Underwater part of ship hull (below load line)

Carried out by Hi-Pec

June 9th, 2009

Euro Basic ES301K62

June 10th, 2009

Euro Basic ES301K10

June 11th, 2009

Euro Basic ES301K62

June 11th, 2009

Euro Sealer TE08

June 12th, 2009

Euro antifouling AF2160

Topside part of ship hull (above load line)

Carried out by Hi-Pec