Académique Documents
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Syllabus
Design of heat exchangers; mechanical and fabrication aspects. Design
of condenser, reboiler, and evaporator
Texts:
1. D. Q. Kern, Process Heat Transfer, McGraw-Hill Book Company, Int. ed. 1965.
2. Dutta B.K., Heat Transfer-Principles and Applications, PHI Pvt. Ltd., New Delhi, 1st ed,
2006.
3. R. K. Sinnott, Coulson & Richardsons Chemical Engineering: Chemical Engineering
Design (volume 6), Butterworth-Heinemann, 3rd ed, 1999.
4. Indian Standard (IS: 4503-1967): Specification for Shell and Tube Type Heat
Exchangers, BIS 2007, New Delhi.
Exchangers recovers heat between two process streams. Steam and cooling
water are utilities and are NOT considered in the same sense as recoverable
process streams
Heaters are used primarily to heat process fluids and, steam is usually employed for
this purpose. Although oil refineries hot recirculated oil serves the same purpose
Coolers are employed to cool process fluids. Water is the main cooling medium.
Condensers are coolers whose primary propose is removal of latent heat instead
of sensible heat
Reboilers supplies heat requirement of a distillation process as latent heat
Evaporators are used to concentrate a solution by evaporation of water. If any other
fluid is vaporized besides water, the unit is a vaporizer
Unit Conversion
Figure - A
Fixed tubesheet
Flow
U-tube
Parallel
Counter
Removable bundle
Tubular
Spiral tube
Double pipe
Finned tube
Indirect
contact-type
Extended surface
Finned plate
Gasketed plate
Recuperative
Plate
Lamella
Direct
contact-type
Heat
Exchanger
Disk type
Rotary
regenerator
Regenerative
Drum type
Fixed-matrix
regenerator
Spiral plate
Floating head
Blast-furnace stove
Hot fluid in
Diagram of a metallic
radiation recuperator
Gasket
Mechanical seal used to fill the space between two or more surfaces to prevent the
leakage of the flowing fluid
Gasket materials:
Asbestos
Composites (typical made from asbestos or graphite
Metals
Rubbers
Plastics
Corks etc.
Cooling Tower
Inner pipe is supported within outer pipe by packing glands. Tees have nozzles or
screwed connection to permit entry and exit of annulus fluid
Two lengths of inner pipe are connected by return bend which is usually exposed
and does NOT provide effective heat transfer surface. When arranged in two legs
(as in Figure below), the unit is hairpin
Double pipe exchangers are usually assembled in 12, 15 or 20 ft effective length
(distance over each leg over which heat transfer occurs)
5/4
5/2
5/4
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Design Calculations
When a hot fluid stream and a cold fluid stream, separated by a conducting wall, the rate of
heat transfer across the separating wall is expressed by Fouriers law :
=
(1)
+
+
0
[Neglect wall resistance on tube site resistance is small]
=
+ +
Coefficient (W.m-2.C-1)
Resistance (m2.C.W-1)
River water
Sea water
Cooling water (towers)
Towns water (soft)
Towns water (hard)
Steam condensate
Steam (oil free)
Steam (oil traces)
Refrigerated brine
Air and industrial gases
Flue gases
Organic vapors
Organic liquids
Light hydrocarbons
Heavy hydrocarbons
Boiling organics
Condensing organics
Heat transfer fluids
Aqueous salt solutions
3000-12000
1000-3000
3000-6000
3000-5000
1000-2000
1500-5000
4000- 10000
2000-5000
3000-5000
5000-10000
2000-5000
5000
5000
5000
2000
2500
5000
5000
3000-5000
0.0003-0.0001
0.001-0.0003
0.0003-0.00017
0.0003-0.0002
0.001-0.0005
0.00067-0.0002
0.0025-0.0001
0.0005-0.0002
0.0003-0.0002
0.0002-0.000-1
0.0005-0.0002
0.0002
0.0002
0.0002
0.0005
0.0004
0.0002
0.0002
0.0003-0.0002
= .
,
<
/
L = Pipe length
d = Pipe diameter
Equivalent diameter (dH) for annular section should be used:
=
=
, =
= Average heat transfer coefficient over the pipe length L including the entrance length
(
)
( )
i.
0.48<Pr <16700
ii.
0.0044 < < 9.75, =Viscosity at bulk fluid temperature, w=at wall temperature (Tw)
iii.
( = . )
Conditions:
i.
0.7 Pr 16,700
ii. d/L 0.1
iii. Re 10,000
tcc t1 FC (t2 t1 )
Caloric Temperature, Fc
Fc
tc T2 t1
t h T1 t 2
= .
= =
T cavg Cold fluid (outer side)
T w hot fluid
Now, =
do
Di
, =
=
Series-Parallel arrangement
( )
( )
=
( )
( )
( )
( )
=
( )
( )
+
( )
= and =
( )
( = )
Where
= Number of parallel branches
and =Intel and outlet temperature of series stream
and =Intel and outlet temperature of parallel stream
Th1
Tc2
Step #3: Calculate LMTD assuming counter-current flow if there is no specific reason
Step #4: Select the diameters of the inner and outer pipes. There are no rules for this
purpose. It primarily depends on flow rates of streams
Smaller diameter :
high velocity, Re will be high, larger will be heat transfer coefficient
It will give larger pressure drop
If the allowable pressure drops of the individual streams are given, this may provide a
basis of reflection of tube/pipe diameters
Step #5: Calculate Re number for both tube side and fluid flowing through annulus.
Calculate hi and ho from Sieder-Tate or proper correlation or from JH -chart assuming
.
= .
.
=
. ]
0.14
at Tw
Step #8: Recalculate hi and ho from Nusselt number correlation or using JH -factor.
Convert hi to hio =
Step #9: Choose suitable dirt factor and calculate overall heat transfer coefficient
considering dirt factor
Step #10: Calculate LMTD correction factor (FT) and calculate heat transfer area (A)
Step #11: Use a number of hairpin in series if length is large
Step #12: Calculate pressure drop for both annulus fluid and tube fluid
If pressure drops does not matches allowable pressure drops, then- Select different diameters of inner and outer pipes
- Switch the fluids (interchange fluid arrangement)
- Split flow stream (tube side fluid & annulus fluid)
Allowable Pressure drop of 5 to 10 psi is customary except where the flow is by
gravity. For each pumped stream 10 psi is fairly standard
For gravity flow, pressure drop is determined by the elevation of final fluid outlet
from the storage vessel
=
()
.
L=Tube length or length of straight section, (ft)
G =Mass velocity
lbm
hr.ft2
/ft3)];
[Laminar flow
+ +()/
in annulus]
For commercial pipe and turbulent flow (Re 3,000), for both inner pipe and the annulus:
= . .
Friction factor, f
A = Actual heat transfer area in the exchanger (calculated from tube length and diameter.
Consider number of hair pins also)
Ac = Calculated heat-transfer area based on clean overall heat transfer co-efficient Uc
Over-surface depends on the relative magnitudes of total fouling allowances & the film and
wall resistances
Typical value: 20-40 %, however higher values are not unusual
Over design represents extra surface area required beyond to compensate for fouling
% =
Problem: 5000 lb/h of benzene will be heated from 60 to 120F by exchanging heat with
an aniline stream, that will be cooled from 150 to 100F. A number of 12 ft hairpins
consisting of 2-inch by 1.25 inch schedule stainless steel (type 316, kw=9.4 Btu/h.ft.F)
are available and will be used for this purpose. Maximum allowable pressure drop is 5
psi for each stream. Design the configuration and determine the number of hair-pins
required.
Fluid Property
(cP)
0.55
2.0
Cp (Btu/lbm.F)
0.42
0.52
k (Btu/h ft.F)
0.092
0.1
s (Specific gravity)
0.879
1.022
Rd (h.ft2.F/Btu)
0.001
0.001
2 inch schedule 40 : ID= 2.067 inch, OD=2.375 inch, thickness =0.154 inch
1.25 inch schedule 40: ID=1.38 inch, OD=1.66 inch, thickness =0.140 inch
Nozzle: 1.0 inch schedule 40 (flow area= 0.006 ft2)
http://www.rexheatexchanger.com/
2. Removable tube bundle (Floating-head and U-tube exchanger: Tube bundle may be
removed for ease of cleaning and replacement
2a. Floating-head exchanger: Consists of a stationery tube sheet which is clamped with the shell
flange
Advantages
Tubes may expand into a freely riding floating-head at opposite end of the bundle
A floating head cover is bolted to the tube sheet and the entire bundle can be removed for cleaning
and inspection of the interior
Limitations
Tube side passes limited to single or two pass design
All tubes are attached to two tubesheets. Tubes cannot expand independently
2b. U-tube exchanger: Consists of tubes which are bent in the form of a U and rolled back
into the tube sheet
Advantages
Tubes can expand freely towards the U bend end
Shell circuit can be inspected and steam or mechanically cleaned
Provides multi-pass tube circuit arrangement
Limitations
Some tubes are omitted at the centre of tube bundle depending on the tube arrangement
Less surface per given shell and tube diameter than other removable designs
Due to U-tube nesting, individual tube is difficult to replace
Tube wall thickness at the U-bend is thinner than at straight portion of the tubes
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Tubular Exchanger
Manufacturers
Association
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Tube
Tube OD of and 1 are very common to design a compact heat
exchanger
Most efficient condition for heat transfer is to have the maximum number
of tubes in the shell to increase turbulence
Tube thickness should be enough to withstand the internal pressure along
with the adequate corrosion allowance. Tube thickness is expressed in
terms of BWG (Birmingham Wire Gauge) and true outside diameter (OD)
Tube length of 6, 8, 12, 16, 20 and 24 ft are preferably used. Longer tube
reduces shell diameter at the expense of higher shell pressure drop.
Finned tubes are also used when fluid with low heat transfer coefficient
flows in the shell side
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Number of tubes that can be accommodated in a given shell ID is called Tube Count
Tube count depends on the factors like shell ID, OD of tube, tube pitch, tube layout,
number of tube passes, type of heat exchanger and design pressure
Common tube layouts
Tube OD, in
Pitch type
Tube pitch,
in
3/4
Square
1
1
5/4
3/4
Triangular
15/16
3/4
1
+
+
Flow
Flow
Flow
Pitch
Pitch
Square
Triangular
Pitch
+
+
Rotated square
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Tube Passes
Number of passes is chosen to get the required tube side fluid velocity to obtain greater
heat transfer co-efficient and also to reduce scale formation
Tube passes vary from 1 to 16. The tube passes of 1, 2 and 4 are common in
application
Partition built into exchanger head known as partition plate (also called pass
partition) is used to direct the tube side flow
for alloy
Tube Sheet
Tubes are fixed with tube sheet that form the barrier between the tube and shell fluids
Tubes can be fixed with the tube sheet using ferrule and a soft metal packing ring
Tubes are attached to tube sheet with two or more grooves in the tube sheet wall by
tube rolling. Tube metal is forced to move into the grooves forming an excellent tight
seal
Tube sheet thickness should be greater than the tube outside diameter to make a good
seal
Recommended standards (IS:4503 or TEMA) should be followed to select the minimum
tube sheet thickness
shell
channel
channel
(a)
tube
tube sheet
shell
shell
channel
tube
(b)
tube sheet
tube
(c)
tube sheet
Tube sheet connections: a) Integral construction on both sides, b). one side integral
construction and other side gasketed construction, c). both side gasketed construction
Tube Sheets
Baffles
Baffles are used to increase the fluid velocity by diverting the flow across the tube
bundle to obtain higher transfer co-efficient
Distance between adjacent baffles is called baffle-spacing or baffle pitch. Baffle
spacing of 0.2 to 1 times of the inside shell diameter is commonly used
Baffles are held in positioned by means of baffle spacers
Closer baffle spacing gives greater transfer co-efficient by inducing higher turbulence.
Pressure drop is more with closer baffle spacing
In case of cut-segmental baffle, a segment (called baffle cut) is removed to form the
baffle expressed as a percentage of the baffle diameter. Baffle cuts from 15 to 45% are
normally used. A baffle cut of 20 to 25% provide a good heat-transfer with the
reasonable pressure drop. The % cut for segmental baffle refers to the cut away
diameter of the baffle.
Shell
Doughnut
Disc
Orifice
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Fouling Considerations
Material deposited reduces the effective heat transfer rate due to relatively low thermal
conductivity
Net heat transfer with clean surface should be higher to compensate the reduction in
performance during operation
Fouling of exchanger increases the cost of (i) construction due to oversizing, (ii)
additional energy due to poor exchanger performance and (iii) cleaning to remove
deposited materials
Coefficient (W.m-2.C-1)
Resistance (m2.C.W-1)
River water
Sea water
Cooling water (towers)
Towns water (soft)
Towns water (hard)
Steam condensate
Steam (oil free)
Steam (oil traces)
Refrigerated brine
Air and industrial gases
Flue gases
Organic vapors
Organic liquids
Light hydrocarbons
Heavy hydrocarbons
Boiling organics
Condensing organics
Heat transfer fluids
Aqueous salt solutions
3000-12,000
1000-3000
3000-6000
3000-5000
1000-2000
1500-5000
4000- 10,000
2000-5000
3000-5000
5000-10,000
2000-5000
5000
5000
5000
2000
2500
5000
5000
3000-5000
0.0003-0.0001
0.001-0.0003
0.0003-0.00017
0.0003-0.0002
0.001-0.0005
0.00067-0.0002
0.0025-0.0001
0.0005-0.0002
0.0003-0.0002
0.0002-0.000-1
0.0005-0.0002
0.0002
0.0002
0.0002
0.0005
0.0004
0.0002
0.0002
0.0003-0.0002
Shell-side fluid
Corrosive fluid
Cooling water
Fouling fluid
Less viscous fluid
High-pressure steam
Hotter fluid
+ +
Where,
Ud= Overall heat transfer coefficient that includes fouling factor (kcal/h.m2.C)
ho =Outside heat transfer coefficient (kcal/h.m2.C)
hi =Inside heat transfer coefficient (kcal/h.m2.C)
Ao =Outside heat transfer area (m2)
Ai = Inside heat transfer area (m2)
kw = Thermal conductivity of wall (kcal/h.m.C)
Where,
DH =Hydraulic diameter or equivalent diameter of the shell side
ko =Thermal conductivity of the shell-side (or outside) fluid
Gs =Mass flow rate (kg/m2s) of the shell fluid
ho =Outside heat transfer coefficient
=Viscosity of fluid at the bulk temperature
w =Viscosity of wall at the wall temperature
cp =Specific heat of the fluid
Equivalent diameter (DH) for tubes on square pitch:
/
=
Flow
+
Pitch (PT)
Flow
+
Pitch (PT)
. . /
=
/
= ; and =
Where,
W =Flow rate of the shell fluid, kg/s
as = Shell side flow area, m2
c =Clearance between two adjacent tubes, m
B =Baffle spacing, m
Ds =Inside diameter of the shell, m
Colburn factor (jH) for shell-side heat transfer with segmental baffles
Reynolds number, =
ln
Cocurrent flow
Cross
Approach
Temperature correction factor: 1 shell pass; two or more even tube passes
FT
Temperature correction factor: 2 shell passes; four or multiples of four tube passes
FT
Where,
f = Friction factor
Gt =Mass velocity of the tube fluid, kg/m2s
L =Tube length, m
np =Number of tube passes
g =Gravitational acceleration, 9.8 m/s2
t=Density of tube fluid, kg/m3
di =Inside diameter of the tube
t =Dimensionless viscosity ratio
Where,
V =Linear velocity of tube fluid, m/s
np =Number of tube passes
g =Gravitational acceleration, 9.8 m/s2
t =Density of tube fluid, kg/m3
Friction factor, f
0.14
Friction factor, f
Reynolds number, =
0.14
4 2 /4 2
=
+
Where,
do=Outside diameter of the tube, m
Ds=Inside diameter of the shell, m
nt =Number of the tubes in the shell
Step #3: Assume a reasonable value of overall heat transfer coefficient (Uo,assm)
Step #4: Decide tentative number of shell and tube passes (np). Determine the LMTD and
the correction factor FT. FT normally should be greater than 0.75 for the steady operation
of the exchangers
Step #5: Calculate heat transfer area (A) required:
Q
U o ,assm . LMTD . FT
Step #6: Select tube material, decide the tube diameter (ID=di , OD =do ), its wall
thickness (in terms of BWG or SWG) and tube length (L). Calculate the number of tubes
(nt) required to provide the heat transfer area
nt
A
do L
.
Fix np so that
Re
4 m(n p / nt )
di
104
4m(n p / nt )
di 2
and u1 m/s
Where, m, and are mass flow rate, density and viscosity of tube side fluid. However,
this is subject to allowable pressure drop in the tube side of the heat exchanger
Step #7: Decide type of shell and tube exchanger (fixed tubesheet, U-tube etc). Select the
tube pitch (PT), determine inside shell diameter (Ds) that can accommodate the calculated
number of tubes (nt). Use the standard tube counts table for this purpose
Step #9: Assign fluid to shell side or tube side . Select the type of baffle (segmental,
doughnut etc.), its size (i.e. percentage cut, 25% baffles are widely used), spacing (B) and
number. The baffle spacing is usually chosen to be within 0.2Ds to Ds
Step #10: Determine the tube side film heat transfer coefficient (hi) and shell side film heat
transfer coefficient (ho)
Select the shell side dirt factor (Rdo) and tube side) dirt factor (Rdi)
Calculate overall heat transfer coefficient (Uo,cal) based on the outside tube area (you may
neglect the tube-wall resistance) including dirt factors
U o ,cal
1
A0 d 0 di
Rdo
Ai 2k w
ho
A0 1 A0
Rdi
Ai hi Ai
Step #11: If , 0
U o ,cal U o ,assm
U o ,assm
30%
go the next step # 12. Otherwise go to step #5, calculate heat transfer area (A) required
using Uo,cal and repeat the calculations starting from step #5
If the calculated shell side heat transfer coefficient (ho) is too low, assume closer baffle
spacing (B) up to 0.2Ds and recalculate shell side heat transfer coefficient. However, this is
subject to allowable pressure drop across the heat exchanger
Step #12: Calculate % overdesign. Overdesign represents extra surface area provided
beyond that required to compensate for fouling. Typical value of 10% or less is acceptable
Step #13: Calculate the tube-side pressure drop (PT): (i) pressure drop in the straight
section of the tube (frictional loss) (Pt ) and (ii) return loss (Prt) due to change of direction
of fluid in a multi-pass exchanger
Total tube side pressure drop: PT = Pt + Prt
Step #14: Calculate shell side pressure drop (PS ): (i) pressure drop for flow across the
tube bundle (frictional loss) (Ps ) and (ii) return loss (Prs ) due to change of direction of
fluid
Total shell side pressure drop: PS = Ps + Prs
If the tube-side pressure drop exceeds the allowable pressure drop for the process
system, decrease the number of tube passes or increase number of tubes per pass. Go
back to step #6 and repeat the calculations steps
If the shell-side pressure drop exceeds the allowable pressure drop, go back to step #7
and repeat the calculations steps
Step #15: Upon fulfillment of pressure drop criteria, go mechanical design
Design Problem
150000 lb per hour of kerosene will be heated from 75 to 120F by cooling a gasoline
stream from 160 to 120F
Inlet pressure will be 50 psia for each stream and the maximum pressure drop of 7 psi
for gasoline and 10 psi for kerosene are permissible
Published fouling factors for oil refinery streams should be used for this application
Design a shell and tube heat exchanger for this service
DESIGN OF CONDENSER
[Condensation of single vapor]
CONDENSER
Change from liquid phase to vapor phase is called vaporization and the reverse phase
transfer is condensation
Change from liquid to vapor or vapor to liquid occurs at one temperature (called
saturation or equilibrium temperature) for a pure fluid compound at a given pressure.
Industrial practice of vaporization and condensation occurs at almost constant pressure;
therefore the phase change occurs isothermally
Condensation occurs by two different physical mechanisms i.e. drop-wise
condensation and film condensation
Heat transfer coefficient is about 4 to 8 times higher for drop wise condensation
Condensers are coolers whose primary propose is removal of latent heat instead of
sensible heat
Types of Condensers
1. Vertical condenser
Downflow vertical condenser: The vapor enters
at the top of condenser and flows down inside
tubes. Condensate drains from the tubes by
gravity and vapor induced shear
Upflow vertical condenser: Vapor enters at the
bottom and flows upwards inside the tubes.
Condensate drains down the tubes by gravity
only
2. Horizontal condenser
When the allowable pressure drop is difficult to meet through a 1-2 condenser, a lower
pressure drop can be obtained by using a double flow or divided flow condenser
Condenser Design
Design of condenser is similar to a typical shell and tube exchangers
Condenser must have a vent for removal of non-condensable gas
Non-condensable gas decreases the heat transfer rate
Condenser usually use a wider baffle spacing of (ID of shell) as the allowable
pressure drop in shell side vapor is usually less
Vertical cut-segmental baffles are generally used in condensers for side-to-side
vapor flow and not for top to bottom
An opening at the bottom of the baffles is provided to allow draining of condensate
(Tsat t1 ) (Tsat t2 )
(t2 t1 )
LMTD
(Tsat t1 )
(Tsat t1 )
ln
ln
(Tsat t2 )
(Tsat t2 )
Where,
Tsat = Saturation vapor temperature
t1 = Coolant inlet temperature
t2 = Coolant outlet temperature
Calculation of heat transfer co-efficient for the cold fluid (coolant) can be performed
similarly as discussed in design of shell and tube heat exchanger (heat transfer without
phase change)
It is assumed that the coolant flows in tube side and the condensing saturated vapor
flows in the shell side
If the condensation occurs in the tube side, follow the procedure discussed in
next section for shell side calculation
Assume, ho,(assm) in the range from 100 (500) to 300 (1500) BTU/h.ft2.F
(kcal/h.m2.C). Film coefficient of condensing hydrocarbons generally varies in this
range. Air-free condensing steam has a coefficient of 1500 BTU/h.ft2.F
ii.
ho (Tv TC ( avg ) )
(hio ho )
Or
ho (Tv Tcc )
Tw Tcc
(hio ho )
Where, hio hi
di
do
(Tw Tv )
2
=
2. Shell side pressure drop
Similarly for condensation in the shell-side condensation (with segmental baffles)
+
=
Tsuperheat
Temperature
Tsat
Tsub-cool
Desuper
-heating
Condensation
LMTDdesuperh
LMTDcondensatio
LMTDsubcooli
eat
ng
Heat transfer
Subcooling
DESIGN OF REBOILER
REBOILER
Classification of reboilers
There are three major types of reboilers:
Limitations: not suitable for heavily viscous fluid; high construction cost for the
installation of the column base at suitable elevation to get thermosyphon effect; not
suitable for low temperature difference processes due to boiling point elevation imposed
by static head
3. Kettle reboiler
Tube bundle is immerged in a pool of liquid at the base of the column in an oversize
shell
Kettle reboiler is also called a submerged bundle reboiler. Height of the tube
bundle is usually 40-60% of the shell ID. Submergence of the tube bundle is
assured by an overflow weir at height of typically 5-15 cm from the upper surface of
topmost tubes
Advantage: suitable for vacuum operation and high vaporization rate up to about 80%
of the feed
Limitations: low heat transfer rate than other types as there is no liquid circulation
(low velocity); not appropriate for fouling fluids; Kettle reboiler is not suitable for heat
sensitive materials as it has higher residence time
nt
Db d o
K1
Where,
Constants
Triangular
(PT = 1.25do)
K1
0.319
0.249
0.175
0.0743
0.0365
n1
2.142
2.207
2.285
2.499
2.675
Square
(PT = 1.25do)
K1
0.215
0.156
0.158
0.0402
0.0331
n1
2.207
2.291
2.263
2.617
2.643
ii.
iii.
Follow the same guideline and design requirements for shell containing the vaporizing
liquid
iv.
- 1000 Btu/h.ft2 F for natural or forced circulation vaporizing aqueous solution of low
concentration
Maximum allowable heat flux:
- 20,000 Btu/(h)ft2) for forced circulation reboilers and 12000 Btu/(h)ft2) for natural
Assume that h(assm) = 300 Btu/h.ft2 F for organics or 1000 Btu/h.ft2 F for water. With
this assumed value, calculate the tube wall temperature (Tw):
Tw Th ( avg )
If the calculated hcal is greater than the maximum heat transfer co-efficient of 300
Btu/h.ft2 F for organics and 1000 Btu/h.ft2 F for water, take hcal = 300 Btu/h.ft2 F for
organics and hcal =1000 Btu/h.ft2 F for water
Calculate the overall heat transfer-coefficient (Ud) including the dirt factors
Maximum for water
500
t tr
an
s fe
nt
he
a
100
ion
La
te
1000
ible
Sens
hea
sfer
n
a
r
t
t
e
by fr
t
nvec
e co
20
4
10
50
100
200
(Tw-t), F
Temperature difference between tube wall and boiling liquid
v. Decide type of exchanger i.e. fixed tube sheet or U- shell (use U-tube reboiler for large
temperature difference), tube size (diameter, length, tube pitch), layout, effective tube length.
A tube pitch of between 1.5 to 2 times the tubes OD should be used to avoid
vapor blanketing
vi. Calculate exchanger area (A =
)
.
Number of tubes should be calculated based on the effective tube length for U-tube
reboilers. Effective tube length is less than physical tube length due to U-bend
It should be less than the maximum heat flux of 20000 Btu/(h)ft2) for forced
circulation reboilers vaporizing organics and 30000 Btu/(h)ft2) for both forced or
natural circulation reboilers vaporizing aqueous solution
Otherwise, go to step # v, repeat the calculation until within the allowable limits
l v
uv 0.2
3
3600
Vapor density (kg/m ) Liquid surface area (m 2 )
DESIGN OF EVAPORATOR
EVAPORATOR
Evaporation is the removal of solvent as vapor from a solution, slurry or suspension of
solid in a liquid
Aim is to concentrate a non-volatile solute, such as organic compounds, inorganic salts,
acids or bases from a solvent
Common solutes are caustic soda, caustic potash, sodium sulfate, sodium chloride,
phosphoric acid, and urea
Most common solvent in most of the evaporation systems is water
Invention of evaporators: Norbert Rillieux is famous for his invention of the multiple
effect pan evaporator for sugar refining process in 1881. Rillieux born in New Orleans,
Louisiana in 1806. He used the steam generated from one pan to heat the sugar juice in
the next pan for energy efficient means of water evaporation
TYPE OF EVAPORATORS
1.
2.
3.
4.
5.
6.
7.
8.
Calandria evaporator
Long vertical tube bundle is fixed with a shell that extends into a
larger diameter vapor chamber at the top
Liquid flows as a thin film (both rising and falling film) on the
walls of long and vertical heated tube
Feed enters at the bottom and the liquid starts boiling at lower
part of the tube
Liquid is allowed to flow down through the inner wall of the tubes as a
film. As the liquid travels down the tubes the solvent vaporizes and
the concentration gradually increases
Vapor and liquid are usually separated at the bottom of the tubes and
the thick liquor is taken out
Distribution of liquid in the inner wall of the tubes greatly affects the
performance of this type of evaporator
Solution is heated in the heat exchanger without boiling and the superheated solution
flashes off (partially evaporated) at a lower pressure are reduced in the flash chamber
Pump pumps feed and liquor from the flash chamber and forces it through the heat
exchanger tubes back to the flash chamber
Forced circulation evaporator is commonly used for concentration of caustic and brine
solutions and also in evaporation of corrosive solution
Pumps, interconnecting pipes and valves are required for transfer of liquid from one
effect to another effect that increases both equipment and operating costs
Both feed and steam are introduced in the first effect and the feed passed from effect to effect
parallel to the vapor from the earlier effect. Concentration increases from the first effect to the last
Forward feeding operation is helpful when the concentrated product may degenerate if exposed
to high temperature
It requires a pump for feeding of dilute solution to the first effect. A pump removes thick liquor from
the last effect
Liquid from one effect to the next effect also can be transferred without a pump as the flow occurs
in the direction of decreasing pressure
Backward Feed
Feed enters at the last effect (coldest effect) and is pumped through the successive effects
Product is withdrawn from the first effect (hottest) where the steam is introduced
Feeding requires a pump between each pair of effects to transfer liquid from lower pressure effects
to higher pressure effects
It is advantageous when cold feed entering needs to be heated to a lower temperature than in
forward feed operation
Backward feed is commonly used when products are viscous and exposure to higher
temperature increases the rate of heat transfer due to reduction in viscosity of the liquid
Mixed Feed
Dilute feed liquid enters at an intermediate effect and flows in the next higher effect till it
reaches the last effect of the series. In this section, liquid flows in the forward feed
mode
Partly concentrated liquor is then pumped back to the effect before the one to which the
fresh feed was introduced for further concentration
Mixed feed arrangement eliminates some of the pumps needed in backward
configuration as flow occurs due to pressure difference whenever applicable
Parallel Feed
Fresh feed is introduced to each effect and product is withdrawn of from the same effect
in parallel feed operation
Overall heat transfer coefficient should be either known/ calculated from the
performance data of an operating evaporator of the same type and processing the
same solution
Typical overall heat transfer coefficients in evaporators
Type of evaporator
Long-tube vertical evaporator
Natural circulation
Forced circulation
Short-tube vertical or calandria evaporators
Agitated-film evaporators
Low to medium viscosity (<1 P)
High viscosity (> 1 P)
Falling film evaporators (viscosity <0.1 P)
Rising film evaporators
200-550
400-1500
150-500
1800-2700
1500
500-2500
2000-5000
300-500
300
100-500
100-1000
Boiling point of the solution is a straight line against boiling point of pure water at the
same pressure
Different lines are obtained if such plots made for solution of different concentrations
Dhring lines can be drawn if boiling points of a solution and water (read from steam
table) at two different pressures are known
This line can be used to predict boiling point of a solution at any pressure
m f H f ms s (m f ms1 ) H1 ms1H s1
Effect III:
(m f ms1 ms 2 ) H 2 ms 2 s 2 (m f ms1 ms 2 ms 3 ) H 3 ms 3 H s 3
Effect II:
(A1)
(A2)
(A3)
(A4)
Where,
msk = Rate of vapor generated in the kth effect
mf and ms = Feed and steam flow rate
Hk = Enthalpy of solution leaving kth effect at Ts and Ps
UD1, UD2 and UD3 : Overall heat transfer coefficients in 1st, 2nd and 3rd effects
A1, A2 and A3 are the corresponding heat transfer area required. Then Effect I:
(A5)
Effect II:
Q2 ms1s1 U D 2 A2 (Tw1 Tb 2 ) U D 2 A2 T2
(A6)
Effect III:
(A7)
Where,
Qk =Quantity of heat transferred in kth effect
Tbk =Boiling point of the solution in kth effect at the prevailing pressure
Ts =Steam temperature condensing in the 1st effect
(Tbk Twk) = Boiling point elevation in the kth effect, where Twk is the boiling point of pure
solvent (water) in kth effect at the prevailing pressure
Eqs. A2 to A7 are solved to calculate heat transfer area by trial-and-error calculations
U D1 A1T1 U D 2 A2 T2 U D 3 A3 T3
(A8)
Determine overall temperature drop between the steam in 1st effect and saturation
temperature of last effect (considering the BPE in all effects):
(A9)
Where,
(A10)
Step 2#: Calculate the total amount of solvent vaporized from the feed and product
concentration and feed flow rate. Total Ttot is distributed among all effects to have equal
heat transfer areas
Step 3#: Redistribute the overall temperature drop (Ttot ) among all the effects. Since
areas are same (A1=A2=A3). Temperature difference in each effect is roughly proportional to
the overall heat transfer coefficients:
U D1T1 U D 2 T2 U D 3T3
(11)
U
U
T2 T1 D1 , T3 T1 D1
U D2
U D3
U D1 U D1
Ttot T1 T2 T3 T1 1
U
U
D2
D3
Step 5#: Use heat transfer equations to calculate the heat transfer area for each effect.
(A12)
ms s
ms1s1
ms 2 s 2
A1
, A2
, A1
U D1T1
U D 2 T2
U D 3 T3
Step 6#: Compare the areas calculated. If they are not equal, repeat the calculation. Using
the areas obtained to revise the temperature estimates
Recommended approach is to use ratio of the calculated heat transfer area for an effect
to the arithmetic mean of the calculated areas as shown:
(A13)
A1
T1,new T1
A
mean
Repeat the calculations until the area of each effect is equal
Procedure above is for forward feed evaporators. Energy balance equation can
developed accordingly for backward feed system. The area for each effect is also
considered to be equal
Design Problem
A 5% aqueous solution (specific heat ~ 1 kcal.kg-1C-1) of a high molecular weight solute
has to be concentrated to 40% in a forward-feed double effect evaporators at the rate
of 8000 kg.h-1
Feed temperature is 40C. Saturated steam at 3.5 kg.cm-2 is available for heating
A vacuum of 600 mm Hg is maintained in the second effect
Calculate the area requirements, if calandria of equal area are used
Overall heat transfer coefficients are 550 and 370 kcal.h-1m-2 C-1 in the first and second
effect, respectively
Specific heat of the concentrated liquor is 0.87 kcal.kg-1C-1
Solution
? Pressure in effect I to be decided
Pressure in effect II = 760 - 600 = 160 mm Hg
Effect II: Boiling point at this pressure (160 mm Hg) = 60 C (from steam table)
(high molecular wt. solute, BPE is neglected)
Effect II: Latent heat vapor generated at 160 mm Hg (0.2133 bar) = 563 kcal.kg-1 (s2)
Water out with the product = 1000 (1-0.40) kg.h-1 = 600 kg.h-1
Total evaporation rate in two effects (ms1 +ms2) = 7600- 600 = 7000 kg.h-1
(A14)
Allow equal areas and heat transfer rates to two effects, i.e.: U D1T1 U D 2 T2
Ttot= T1 + T2 = 148-60 = 88 C
UD1= 550, UD2= 370 kcal.h-1m-2 C-1 T1 = 35.4 C & T2 = 52.6 C
Temperature of the vapor leaving effect I (Tb1) =148 35.4 = 112.6 C
Latent heat vapor generated in effect I at 112.6 C = 531 kcal.kg-1 (s1)
[evaporator drum pressure ~ 1.2116 bar]
(ref. A11)
m f H f ms s (m f ms1 ) H1 ms1H s1
(ref. A.2)
(8000)(-72.6)
ms = 1.05ms1 + 1148
(A15)
(ref. A3)
1 0.87
0.94)
= 0 kcal/ kg
(w.r.t. the reference temperature of 60 C)
= 531 kcal/ kg
= 563 kcal/ kg
(8000 - ms1)(49.4)
(A16)
ms s
m
(4713)(506)
(3395)(531)
122.5 m 2 and A2 s1 s1
92.6 m 2
U D1T1 (550)(35.4)
U D 2 T2 (370)(52.6)
? The areas in the two effects are not equal. Revision needed
Revised temperature difference in 1st effect, T1 40 o C and T2 48 o C taken for the
calculation
(ref. A.13)
o
38.84
C
You may also continue the calculation with this revised value:
1, new
(8000)(1)(40-108)
(Ref.A.2)
(A.17)
Areas: A1
(ref.A.3)
(A.18)
ms= 4652
ms1= 3417 and
ms2 = 3583 kg/h
ms s
(4652)(506)
m
(3417)(530)
107 m 2 and A2 s1 s1
102 m 2
U D1T1
(550)(40)
U D 2 T2
(370)(48)
Areas are fairly close, use A1 = A2 = 104 m2 plus overdesign. About 10% excess
area will provide a reasonable overdesign
Tube details:
Let us select 1 inch nominal diameter, 80 schedule, brass tubes of 12 ft in length
Outer tube diameter (do) = 42.16 mm
Inner tube diameter (di) = 32.46 mm
(where = 60)
Thank You