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C

N TA IN
S

2014

TH

A N N I V E R S A R Y

TED
RA

ACE G

S
A

C
N
O
I
R
S

1936 2011

NE

N
,
LAND

VI

USA

Reactors Catalog
Bench & Kilo Class

G
RI
CIN

General Information
Specifications
The products in this catalog represent what we believe to be
the most advanced design and construction. However, design
improvements are constantly being made, and we reserve the
right to modify specifications where we feel that a change is
warranted.
Apparatus fabricated in accordance with ASTM, API, AOAC and
other technical organization specifications such as USP, NIST,
and NIOSH, are subject to modification by these organizations.
All precision-grade ware is warranted to be within the tolerance
prescribed in ASTM Specifications. All laboratory-grade ware
is twice precision-grade tolerances.

In case of Shortage:
1. Notify ACE immediately.
2. A replacement will be issued upon confirming
inventory d iscrepancy.
In case of Loss:
1. First, please verify with all your receiving departments
that delivery was not made.
2. Notify ACE immediately.
3. ACE will contact the carrier for tracking information
as a pplicable.
4. A replacement will be issued upon verification that the
shipment was not delivered and upon confirmation
that the carrier cannot locate shipment.

Special Apparatus

PLEASE NOTE:

Orders or inquiries for special apparatus should be


accomp anied by prints or drawings, if possible. To prevent
delay, and to enable us to more intelligently quote on your
specials, all necessary dimensions and tolerances should
be noted. For technical information, design assistance
and help please visit www.aceglass.com.
The following information should also be furnished where
applicable: joint sizes, AceThred sizes, capacity, whether to
contain or to deliver, porosity of filter, and any abnormal
operating conditions, such as extremely high pressure or
temperature, to which the apparatus may be subjected.
We reserve the right to overrun or under run by 10% on orders
for special items and to ship and invoice for amounts within
this variation.
NOTE: Special items are not returnable.
Our research and drafting departments are always available to
assist you in designing special apparatus. Your special will be
assigned a permanent drawing number for future reference,
duplication or change. You will be sent a drawing of your special
for your approval/sign off before manufacturing begins.

Types of Glass
All ACE-manufactured glassware items listed in this catalog
are, unless otherwise noted, fabricated from 33 expansion
borosilicate glass, such as Pyrex Brand Glass, a product of
Corning Incorporated; KG-33 Glass, a product of Kimble Glass
Company; Duran Glass, a product of Schott Glaswerke; Simax,
a product of Kavalier Glaswork.

Breakage or Loss
In case of Breakage:
1. Notify ACE immediately.
2. Please retain all inner and outer cartons and
packing material.
3. ACE will advise you whether the carrier will
report to your location for inspection or if item(s)
are to be returned for inspection.

All breakages and shortages must be


reported within two weeks of receipt.

Returns and Repairs


Incoming material (returns or repairs) must be pre-approved
by our Product Return Specialist. Please follow these steps to
ensure our Receiving Department does not refuse your shipment.

Contact ACE for an RA# (Return Authorization Number).


1-800-223-4524 (Vineland, NJ, USA)
E-mail: returns@aceglass.com

2. Once an RA# is given, properly pack the item(s) in an inner


and outer box/carton and write the RA# on the outside of
the box. All used items are to be thoroughly cleaned and
defined in the assignment of an RA#.
3. A 20% restocking fee will be assessed for authorized
returns. ACE cannot accept responsibility for damage or
destruction of glassware that occurs in your shipment to
us. We strongly advise you to purchase additional insurance
with your carrier.
4. For Returns that are the result of your receiving the item(s)
broken, ACE cannot accept responsibility for further
damage or destruction of glassware that occurs in the
return shipment due to improper packing.
5. Repairs will be evaluated by our technicians. You will
be advised if any pieces are beyond repair or cannot be
salvaged economically. ACE cannot accept responsibility
for further damage or destruction of any glassware that is
damaged during return shipment.
PLEASE NOTE:

ACE cannot accept responsibility


for material returned without proper
authorization.

Specifications are subject to change without prior notice. Although they are represented to be
accurate, it is best to verify product specifications with ACE prior to purchase in the event they have
been changed since publication of this catalog.

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

General Information
Order by Code

ACE Glassware Discounts

Each item in this catalog has a two- or three-digit code in


addition to the four- or five-digit number. No other ordering
information is needed since each individual size, capacity, etc.
has its own code. Example: 5000 10/30 top 14/35 bottom
would be ordered as 5000-05.
The majority of items listed in this catalog are normally available
from stock at our plant in Vineland, NJ.
In the event your entire order cannot be filled immediately,
a partial shipment will be sent, with the back-ordered items
following shortly. If you should desire the entire order to be sent
in one shipment, please so specify on your purchase order.
Unless otherwise specified on the order, we will ship material
by what we consider the best way.

All ACE-manufactured glassware, identified with a spade (),


listed in this catalog is subject to the following dollar value
discounts. Items marked by a star () or that have no designation
whatsoever are not subject to this discount.

.10% on purchases of $500.00 and over

.12% on purchases of $1000.00 and over

.15% on purchases of $1500.00 and over
Terms: Net 30 days (Domestic only)
Minimum Order: $25.00

Ways to Order

All quantities in this catalog are each


unless otherwise noted.

Contact ACE for current price list/pricing CD


or visit our website, www.aceglass.com.

Ace Glass products are also available from our many lab
distribution partners, particularly VWR International and
Sigma Aldrich.
PHONE 856-692-3333

800-223-4524
FAX 856-692-8919

800-543-6752
CREDIT CARD VISA

MasterCard
American Express
MAIL P.O. Box 688

Vineland, NJ 08362
WEB SITE www.aceglass.com
E-MAIL sales@aceglass.com
INTERNATIONAL export@aceglass.com

Shipments are F.O.B. our factory


in Vineland, NJ, USA.

INTERNATIONAL SALES
Ways to Order
Methods of Payment
Mail: Ace Glass Incorporated
International Sales Dept.
1430 N. West Blvd P.O. Box 688
Vineland, NJ 08360-0688 USA
Phone: 856-692-3333
Fax: 856-692-8919
E-mail: export@aceglass.com

Wire Transfer
Irrevocable, payable on-sight,
and confirmed letter of credit
Payment in advance by check or
money order, in US Funds only
Credit Card: Amex, Visa, MasterCard, etc.

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Technical Information
Reference Guide to AceThred Sizes
Accepts
Use Bushing
Size
Tube O.D., mm
Number
#7
6-7
5029-10
Mini

Fraction Conversion

Use With
ORing No.
7855-704

Optional
Ferrule
11710-07

Suggested
Uses
A, B, I

Midi

#11

9-10.5

7506-02

7855-708

11710-11

D, E, F, G

Maxi

#15
#18

12.5-14
16-17

7506-06
7506-08

7855-716
7855-720

11710-15
11710-18

C, H
H, L

Giant

#25
#36

24-25
34-35

7506-10
7506-12

7855-734
7855-740

11710-25

K, R
K, L, R

Jumbo

#50
#80

47-48
80

7506-14
7506-20

7855-744
7855-782

11710-50

K, L, R
R

Length,
Fractional Inches
1/16
1/8
3/16
1/4
5/16
38
7/16
1/2
9/16
5/8
11/16
3/4
13/16
7/8
15/16
1

AThermometers, BBleed Tubes, CElectrodes, DSensing Probes, EThermowells,


FGas Dispersion Tubes, GVacuum Take-Offs, HInlet and Outlet Tubes,
IMiniature Electrodes, KManifolds, LImmersion Wells, RReactors

Millimeters
1.6
3.2
4.8
6.4
7.9
9.5
11.1
12.7
14.3
15.9
17.5
19.1
20.6
22.1
23.8
25.4

Hose Connection Size Guide

Dimensions in Millimeters
3.0

3.5

3.0

4.0

5.0

7.7

6.5

7.1

6.0

8.9

8.4

12.5

10.5

10.4

12.5

11.5

12.9

10.0

7.3
13.8

16.2

Use with
7.9mm (5/16-in.)
I.D. Tubing

Use with
7.9mm (5/16-in.)
or 9.5mm (3/8-in.)
I.D. Tubing

Use with
7.9mm (5/16-in.)
or 9.5mm (3/8-in.)
I.D. Tubing

Specifications for Joints,


Threads, and Stopcocks
Standard Taper

Symbol used to designate


interchangeable joints, stoppers
and stopcocks that comply with
the requirements of Commercial
Standard CS-21 published by
N.I.S.T.

JS

Use with
9.5mm (3/8-in.)
I.D. Tubing

24/40
Inner Joint

Product Standard

Symbol designates stopcock


plugs made of PTFE that meet
requirements of N.I.S.T. Voluntary
Product Standard PS 28-70.

24/40
Outer Joint

24
mm

40
mm

#25
AceThred

Use with
11.1mm (7/16-in.)
or 12.7mm (1/2-in.)
I.D. Tubing

35/25
Ball Joint

24
mm
40
mm

#25 Bushing
for
AceThred

35/25
Socket Joint

#25 ORing
Joint

35
mm

25
mm

25
mm

25
mm
35
mm

0-5 mm Hi-Vac
Stopcock

Use with
15.9mm (5/8-in.)
I.D. Tubing

12/30 Glass
Stopcock Plug
Straight Bore

12
mm
30
mm

25
mm

Spherical Joint

Symbol designates spherical joints


that comply with CS-21.

Use with
9.5mm (3/8-in.)
or 11.1mm (7/16-in.)
I.D. Tubing

25
mm

0-5 mm Orifice
Maximum Flow

16.2/56
Glass
Double
Oblique
Stopcock Plug

1 1:5 Taper
Size 11/25 PTFE
Stopcock Plug

16.2
mm
56
mm

2 mm
BORE
11
mm

25
mm

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Technical Information

Plastic Properties

Low Density
Polyethylene
(LDPE)

High Density
Polyethylene
(HDPE)

Polypropylene
(PP)

PTFE/FEP

Polycarbonate
(PC)

Polymethylpentene
(PMP)

Temperature Limit, C
Specific Gravity
Tensile Strength, psi
Brittleness Temperature, C
Water Absorption, %
Flexibility
Transparency

80
0.92
2000
100
<0.01
excellent
translucent

120
0.95
4000
100
<0.01
rigid
translucent

135
0.90
5000
0
<0.02
rigid
translucent

205
2.15
3000
270
<0.01
excellent
translucent

135
1.20
8000
135
0.35
rigid
clear

175
0.83
4000
20
<0.01
rigid
clear

ORing Compatibility Chart


Key: 1=Recommended; 2=Satistfactory; 3=Poor; 4=Marginal; 5=Not Recommended; A=Acceptable; NA=Not Acceptable
Temperature Range C
Compression set
Durometer
Steam < 120 C
Acetone
Toluene
Tetrachloroethane
THF
Methyl Ethyl Ketone
Acetonitrile
Hydrochloric Acid (conc)
Ammonia Gas (cold)
Tetrachloroethylene
Sulfuric Acid (dilute)
Nitric Acid (conc)
Calcium Carbonate
Xylene
Mineral Oils
Sodium Carbonate
Vacuum
FDA

Viton
26 to 204
2

Silicone
62 to 204
2

Buna-N
37 to 121
2

EPDM
54 to 149
2

75
3
4
2
1
4
5
5
2
4
3
2
2
2
2
1
1
1
A

70
4
3
3
3
4
5
5
5
1
5
5
5
5
4
2
1
4
A

70
4
3
3
3
4
5
5
4
2
3
1
4
1
4
1
1
2
A

70
4
2
3
3
4
2
5
5
2
3
5
5
1
3
4
1
4
A

Chemraz 514 Kalrez 4079


30 to 220
15 to 316
2
2
70
1
1
1
1
1
1
1
1
1
1
2
1
1
1
1
1
4
NA

75
1
1
1
1
1
1
1
1
1
1
2
1
1
1
1
1
4
NA

FETFE
18 to 204
2

CAPFE
60 to 204
3

70
1
5
2
1
5
5
5
2
4
3
2
2
2
2
1
1
1
NA

70
5
1
2
2
3
2
2
4
2
2
2
4
2
2
1
2
2
A

Chemical compatibility information courtesy of the respective manufacturers of each o-ring type. Ace is not responsible for errors.

Conversion Factors
Length

Volume

Power

1 millimeter (mm)............. 0.1 centimeter (cm)


1 centimeter............................0.01 meter (M)
1 centimeter.................................. 0.394 inch
1 inch................................. 2.540 centimeters
1 meter......................................... 3.2808 feet

1 cubic centimeter..................... 0.001 liter (L)


1 cubic inch........... 16.3872 cubic centimeter

1 watt...............................0.73756 foot pound


per second
1 foot pound
per second................................ 1.3582 watts

1 cubic meter..................... 35.314 cubic feet

1 watt.....................0.056884 BTU per minute

1 cubic foot................... 0.02832 cubic meter

1 BTU per minute...................... 17.580 watts

1 foot...........................................0.305 meter

Area
1 square centimeter (cm).0.1550 square inch
1 square inch......... 6.452 square centimeters
1 square meter (M)........... 10.764 square feet
1 square foot...............0.09290 square meter

Mass
1 gram.............. 0.03527 ounce (Avoirdupois)
1 ounce (Avoirdupois)............. 28.3495 grams
1 kilogram.........2.20462 pound (Avoirdupois)
1 pound (Avoirdupois)........ 0.45359 kilogram

1 cubic centimeter..............0.0610 cubic inch

Capacity
1 milliliter (mL)........................ 0.03382 ounce
(U.S. Liquid)
1 ounce (U.S. Liquid)............ 29.573 milliliters
1 liter (L)..................................1.05671 quarts
(U.S. Liquid)
1 quart (U.S. Liquid)................... 0.94633 liter
1 liter....................................... 0.26418 gallon
(U.S. Liquid)
1 gallon (U.S. Liquid)................ 3.78533 liters
1 lambda.......................0.001 cc / 1 microliter

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

1 watt................. 0.001341 horsepower (U.S.)


1 horsepower (U.S.)..................... 754.7 watts
1 watt.......................0.01433 kilogram-calorie
per minute
1 kilogram-calorie
per minute................................. 69.767 watts

Temperature
C = (F32) 5/9
F = 9/5 C +32

Technical Information

Glass Properties
Unless otherwise specified, ACE GLASS brand glassware
is fabricated from Corning 7740, Kimble KG-33, Kavalier/
Simax, or Schott-Duran glass and conforms to federal
specifications DD-G-541B and ASTM E-438. Also meets
the U.S. Pharmacopoeia specs for Type I Borosilicate
Glass. Glass properties are those represented by the
aforementioned companies.

Composition (approximate percent)


Corning 7740

Duran

Kavalier/Simax

Si02

80.6%

81%

80.4%

B203

13.0%

13%

13.0%

Na20/K20

4.1%

4%

4.2%

Al203

2.3%

2%

2.4%

Properties
Coefficient of Expansion
Strain Point
Annealing Point
Softening Point
Density
Temperature Limits
Maximum Thermal Shock
Refractive Index
1
At Sodium D Line

Corning 7740

Schott-Duran

Kavalier/Simax

32.5 x 10-7 cm/cm/C


510C
560C
821C
2.53 g/cm3
230C (Normal use)
400C (Extreme, short-term use only)
160C
1.4741

3.3 x 10-6 cm/cm/K


510C
560C
815C
2.23 g/cm3
230C (Normal use)

3.3.1 x 10-6 cm/cm/K


510C
560C
820C
2.23 g/cm3
240C (Normal use)
400C (Extreme, short-term use only)
160C
1.4721

400C (Extreme, short-term use only)


160C
1.4741

Flask Stoppers

ACE Glass Fiber Filter Discs

Approximate
Length
Diameter
Stopper Diameter at
of Ground at Large
Number Small End, mm Zone, mm End, mm
8
9
13
16
19
22
27
32
38

7.25
8
12
15
18
20
25
30
35

10 1.0
14 1.0
14 1.0
15 1.0
17 1.0
20.5 1.0
21.5 1.0
21.5 1.0
30 1.0

8.25
9.40
13.40
16.50
19.70
22.05
27.15
32.15
38.00

Porosity
Maximum Pore
Diameter
ACE Porosity
Range
Designation
(micron)
A
B
C
D
E

145-174
70-100
25-50
10-20
4-8

ACE

Corning, Kimble
and ChemGlass
Equivalents/
Porosities

Uses

EC (170-220)

C (40-60)
M (10-15)
F (4-5.5)

Coarse Filtration
Coarse Filtration
Gas Dispersion
Extraction
Extraction

Pressure Conversions
Absolute
cm
of Hg
76
70
60
50
40
30
20
10
5
1
0.1
0

Torr
or mm
of Hg

Micron

Atmosphere

760
700
600
500
400
300
200
100
50
10
1
0

760000
700000
600000
500000
400000
300000
200000
100000
50000
10000
1000
0

1
0.921
0.79
0.659
0.526
0.395
0.263
0.132
0.006
0.013
0.001
0

lb/
in.2
14.7
13.53
11.6
9.67
7.74
5.8
3.87
1.94
0.967
0.194
0.019
0

Gauge Pressure
ton/
ft.2

gram/
cm2

ft. of
H20

in. of
Hg

1.06
0.975
0.835
0.696
0.557
0.417
0.278
0.139
0.07
0.014
0.001
0

1033
952
816
680
545
408
272
136
68
13.6
1.36
0

33.9
31.2
26.8
22.3
17.8
13.4
8.92
4.46
2.23
0.446
0.045
0

29.9
27.6
23.6
19.7
15.7
11.8
7.87
3.94
1.97
0.394
0.039
0

lb. in.
0.00
1.16
3.10
5.03
6.97
8.90
10.8
12.8
13.7
14.5
14.68
14.7

in. of
Hg
0.00
2.36
6.30
10.2
14.2
18.1
22.0
26.0
27.9
29.5
29.88
29.92

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Technical Information

Reference Guide to ACE Boiling Flasks


Capacity,
mL
5
10
15
20
25
50
100

Approx.
O.D. mm
25
31
35
38
42
50
58

Approx.
O.D. Inches
1.0
1.24
1.4
1.5
1.68
2.0
2.25

Capacity,
mL
200
250
300
500
1000
2000
3000
5000

Approx.
O.D. mm
75
82
86
100
125
160
180
225

Approx.
O.D. Inches
3.0
3.25
3.385
4.0
5.0
6.3
7.0
8.86

Capacity,
mL
12000
22000
500001
500002
500003
72000
100000
2000002
2000003

Approx.
O.D. mm
285
350
457
488
508
508
610
750
762

Approx.
O.D. Inches
11.22
13.78
18.0
19.3
20.0
20.0
24.0
29.5
30.0

Corning flask; 2Schott flask; 3QVF flask.

Guide to Flange Styles


Flat Flange

I.D.

(with or without o-ring groove)

O.D.

Thickness

100 mm (4-inch)

138 mm (5.4-inch)

10 mm (0.4-inch)

130 mm (5.1-inch)

168 mm (6.6-inch)

10 mm (0.4-inch)

Uses Clamp: 6508, 6509, 6510 Flat clamp

Conical Flange

I.D.

O.D.

102mm (4-inch)

135mm (5.3-inch)

Thickness
30mm (1.2-inch)

Uses Clamp: 6496 Standard clamp

Schott-Duran Flange

I.D.

(with or without o-ring groove)

O.D.

Thickness

60mm (2.4-inch)

100mm (4-inch)

20mm (0.8-inch)

100mm (4-inch)

138mm (5.4-inch)

20mm (0.8-inch)

150mm (6-inch)

184mm (7.2-inch)

20mm (0.8-inch)

200mm (8-inch)

242mm (9.5-inch)

20mm (0.8-inch)

Uses Clamp: 6517 Quick release clamp

KF Plane Flange

I.D.

O.D.

Thickness

200mm (8-Inch)

230mm (9-Inch)

24mm (0.95-Inch)

300mm (12-Inch)

338mm (13.3-inch)

24mm (0.95-inch)

Uses Clamp: 6525 Coupling

Beaded Process Beaded Process Pipe flanges range 1/2-inch thru 6-inch I.D.
Pipe Flange
Example: 2-inch pipe = 2-inch I.D.

2-9/16 inch bead O.D.


Tube O.D. = 2-5/16-inch
See page 270 for dimensions for all sizes of beaded pipe
Uses Clamp: 8856 Coupling

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Technical Information

Standard Pipe Thread Fittings

The illustrations are


actual size. If you have
any questions as to
the size of fitting you
require, simply compare
the threads per inch, the
diameter and length of
the threading, and the
taper of the threading of
your existing fittings to
these drawings.

Sterilization Reference Guide


Method

Procedure

Autoclave:
Dry Heat:
Gas:
Microwave:
Gamma Irradiation:
Chemical Disinfectants:

Cycle is 121C, 15 psig (1bar) 20 min


170C for 60 min
Ethylene Oxide for formaldehyde
Transmission of microwaves
High energy ionizing gamma radiation from a Cobolt 60 source
Quaternay Ammonim Compounds, Iodophors, Formalin, Benzalkonium
Chloride, Ethanol, etc.

Viscosity Conversion Factors


Viscosity is the resistance to flow due to the internal friction within a fluid. This is generally expressed as the
force required to move one unit area one unit distance. Kinematic and absolute viscosity are related by the
density of the fluid.

92903.04
0.092903
10.7639
1000000.0
0.000001
0.0000107639

Absolute to Kinematic Viscosity


to get
Divide
centistokes
sq. meters/sec
ft2/sec
centistokes
sq. meters/sec
ft2/sec

Absolute or Dynamic Viscosity

Multiply
to get
lbf-sec/ft2
lbf-sec/ft2
centipoises
centipoises
Pascal-sec
Pascal-sec

47880.26
47.8803
0.000102
0.001
0.0208854
1000

to get
Divide
centipoises
Pascal-sec
kg-sec/sq. meter
lbf-sec/ft*
Pascal-sec
centipoises

*Sometimes absolute viscosity is given in terms of pounds


mass. In this casecentipoises x 0.000672 = lbm/ft sec.

Multiply
to get
centipoises
centipoises
lbf-sec/ft2
kg-sec/m2
Pascal-sec

1/density (g/cm )
0.00067197/density (lb/ft3)
32.174/density (lb/ft3)
9.80665/density (kg/m3)
1000/density (g/cm3)
3

to get
Divide
centistokes
ft2/sec
ft2/sec
sq. meters/sec
centistokes

Kimematic to Absolute Viscosity


Multiply
to get
centistokes
sq. meters/sec
ft2/sec
ft2/sec
centistokes
sq. meters/sec

Multiply
to get
ft2/sec
ft2/sec
sq. meters/sec
sq. meters/sec
centistokes
centistokes

Kinematic Viscosity

density (g/cm )
0.10197 x density (kg/m3)
0.03108 x density (lb/ft3)
1488.16 x density (lb/ft3)
0.001 x density (g/cm3)
1000/density (g/cm3)
3

to get
Divide
centipoises
kg-sec/m2
lbf-sec/ft2
centipoises
Pascal-sec
Pascal-sec

Dilatant Liquids viscosity increases


as shear rate increases. Mixers can bog
down and stall after initially mixing such
liquids. Dilatant liquids include slurries,
clay, and candy compounds.
Newtonian Liquids viscosity
remains constant regardless of
shear rate or agitation. As mixer
speed increases, flow increases
proportionately. Newtonian liquids
include water, mineral oils, and
hydrocarbons.
Pseudoplastic Liquids viscosity
decreases as shear rate increases, but
initial viscosity may be sufficiently great
to prevent mixing. Typical pseudoplastic
liquids are gels, latex paints, and lotions.
Thixotropic Liquids as with
pseudoplastic
liquids,
viscosity
decreases as shear rate or agitation
increases. When agitation is stopped or
reduced, hysteresis occurs and viscosity
increases. Often the viscosity will not
return to its initial value. Thixotropic
liquids include soaps, tars, shortening,
glue, inks, and peanut butter.

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Technical Information

10

Chemical Resistance for Plastic Resins @ 20C


Classes of Substances

ACL

Acids,
dilute
or
weak

Acids,
strong
& conc.

Alcohols,
aliphatic

Aldehydes

Bases

Esters

Hydrocarbons,
aliphatic

Hydrocarbons,
aromatic

Hydrocarbons,
haloge
nated

Ketones

Oxidizing
agents,
strong

ECTFE/ETFE

FEP/TFE/PFA

FLPE

XLPE

HDPE/XLPE

DLPE

PC

PCT

PTE

PMMA

PMP

PP/PPCO

PS

PSF

PUR

PVC Bottles

Flexible PVC Tubing

PVDF

TPE

Resin Codes
ACL
ECTFE
ETFE
FEP
FLPE
HDPE
LDPE
PC
PCT
PET
PFA
PMMA
PMP
PP
PPCO
PS
PSF
PUR
PVC
PVDF
TFE
TPE
XLPE

Acetal (Polyoxymethylene)
Halar ECTFE (Ethylene-Chlorotrifluoroethylene Copolymer)
Tefzel ETFE (Ethylene-Tetrafluoroethylene)
Teflon FEP (Fluorinated Ethylene Propylene)
Fluorinated High-Density Polyethylene
High-Density Polyethylene
Low-Density Polyethylene
Polycarbonate
Poly (1,4 Cyclohexylene Dimethylene Terephthalate)
Polyethylene Terephthalate
Teflon PFA (Perfluoroalkoxy)
Polymethyl Methacrylate (Acrylic)
Polymethylpentene (TPX)
Polypropylene
Polypropylene Copolymer
Polystyrene
Polysulfone
Polyurethane
Polyvinyl Chloride
Polyvinyllidene Fluoride
TeflonTFE (Tetrafluoroethylene)
Thermoplastic Elastomer
Cross-Linked High-Density Polyethylene

Chemical Resistance Classifications

30 days of constant exposure causes no damage.


Plastic may even tolerate for years.

Little or no damage after 30 days of constant


exposure to the reagent.

Some effect after seven days of constant exposure


to the reagent. Depending on the plastic, the
effect may be crazing, cracking, loss of strength
or discoloration. Solvents may cause softening,
swelling and permeation losses with LDPE, HDPE,
PP, PPCO and PMP. The solvent effect on these five
resins are normally reversible; the part will usually
return to its normal condition after evaporation.

Not recommended for continuous use. Immediate


damage may occur. Depending on the plastic, the
effect will be a more severe crazing, cracking, loss
of strength, discoloration, deformation, dissolution
or permeating loss.

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Bench Reactors/Filter

11

ACE Filter Reactors allow single


or multi-step reactions and
filtrations in the same vessel.
Stirrer Motors
13500 series or
13566 series

Major Design
Features

100 mL to 6000 mL
standard

Unjacketed or jacketed

All inert materials

Reactions at ambient
or pressure conditions
Filtering by vacuum
and/or pressure
Removable/changeable
filters, poly screen or
glass, wide choice of
porosities

Mechanical agitation

Inert bottom drain valve

Easy assembly/
disassembly for cleaning

Typical
Assembly

Chuck

8124, 8126

Shaft
8075

Bearing

8050, 8066

Head

6527/6528/6529

Clamp
6517

Reactor Body
6384, 6386

Clamp Holder
13550-25

PTFE Agitator
8089

Chain Clamp

PTFE Adapter

11079-24

5857, 5838, 5861

Filter Support
5848

Valve
5839

w/5844 Adapter

Support Stands

12840, 13550, 13586

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

12

Bench Reactors/Filter

6384

UNJACKETED FILTER REACTOR

8075
Stirring
Shaft

8066
Bearing

6527/6528/6529
Head

6517
Clamp

7855
CAPFE
ORing
6384-15
Reactor
Body

Rugged heavy wall reactor with 60mm (2.4inch), 100mm (4inch), or 150mm (6inch)
Schott style top flange with oring groove at top, for connection to 6527, 6528 or 6529
heads, with 6517 quick release clamp. Bottom has an AceThred (internal glass thread)
for installing 5838-83 (size 50) or 5857-86 (size 80) bottom adapter with filter support
and drain valve. Head has three 24/40 joints on 60mm size; four 24/40 joints on
100mm and 150mm sizes.
Complete item consists of: reactor body with CAPFE oring, head with joints, 6517
clamp, PTFE bottom adapter with CAPFE oring (with perforated plate#80 thread only),
retainer ring, 350 micron polypropylene screen support and 100 micron polyethylene
support, 5844 adapter, 5839 shutoff valve (optional larger valve is available), 8066 bearing,
8075 stirring rod, and 8089 multipaddle agitator.
For replacement glass fritted support, polyethylene support or polypropylene screen,
see 5848 or 5814. For condenser and funnel, see 6029 and 7298; stoppers with 24/40
joints, see 8250. For stirring motor, see 13511 or 13566 motor; for chuck, see 8124 or
8126. Use 7855-829 CAPFE o-ring for #50 adapter, 7855-864 for #80 bottom adapter.
Flange
Bottom
Body
Approx.
Top
Cap.,
I.D.,
Thread
I.D.,
Height*,
CAPFE
Order
mL
mm (in.)
Size
mm
mm
ORing
Code
Each
150
60 (2.4)
#50
60
100
7855-878
6384-115 1240.55
600
60 (2.4)
#50
79
205
7855-878
6384-121 1284.35
1000
100 (4)
#80
100
180
7855-880
6384-125 1457.18
2000
100 (4)
#80
126
210
7855-880
6384-129 1624.11
3000
150 (6)
#80
150
205
7855-881
6384-133 2012.91
6000
150 (6)
#80
150
395
7855-881
6384-137 2103.95
*Height measurements are measured from top of flask flange to seal on top thread.
Note: 150mL and 600mL heads have angled side necks.

8089
Agitator

#50/5838 or/#80 5857


Bottom Adapter
w/Filter Support
(with 3/8" FNPT
outlet)

Stand (13550), Clamp


(11079) and Clamp Holder
(13550-25) not included.

5844/12770 Adapter
3/8" MNTP 1/4" FNPT/
3/8" MNTP 3/8" MNTP

5839
Bottom Valve

See page 51 for stands.

(For #80, bottom also available with 1/2" MNPT.)

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Subject to Ace Discount (Page 4)

Net

Bench Reactors/Filter

6384

UNJACKETED FILTER REACTOR, PRESSURE VERSION

Heavy wall glass reactor available with 60mm (2.4-inch), 100mm (4-inch), or 150mm
(6inch) diameter Schott style flange with o-ring groove at top. Connects to #6433
head with a #6517 quick release clamp. Reactor bottom has an AceThred for installing
a 5838-83 (size 80) or 5857-86 (size 50) adapter with a filter support and bottom drain
valve. The 60mm reactor head has a #15 AceThred center neck, (2) #15 and (1) #7
AceThred side necks. The 100mm head has a #15 AceThred center neck, (3) #15 and
(1) #7 AceThred side necks. The 150mm head has a #15 AceThred center neck, (4)
#15 and (1) #7 AceThred side necks. The AceThreds allow for vacuum or pressure
applications and for easy draining of material out of the reactor. The main bearing, funnel
and condenser are designed to connect to the threads on the head via compression
bushing connections. The #7 AceThred is used for connecting a 1/4inch O.D. tubing
fitting to allow for a direct connection to a pressure source or a #6448 pressure manifold.
Complete item consists of: reactor body with 60mm CAPFE o-ring, head with
AceThreds, 6517 clamp, PTFE bottom threaded adapter and valve with CAPFE o-ring,
retainer ring, 350 micron polypropylene screen support, 100 micron polyethylene
support, 5844 adapter, 8044 bearing, 8075 stir rod, 8089 paddle agitator, 6024
condenser, 7299 addition funnel and #7 AceThred bushing. Size 80 bottom adapter
also comes with a perforated glass plate support.
Pressure manifold (page 20), stand and clamps are optional. For replacement glass
fritted discs and supports see 5848 or 5814. See 13511 or 13566 motor; for chuck,
see 8124 or 8126. Use 7855-829 CAPFE o-ring for #50 adapter, 7855-864 for #80
bottom adapter.
Flange
Bottom Body Approx.
Top
Cap.,
I.D.,
Thread
I.D.,
Height*,
CAPFE
Order
mL
mm (in.)
Size
mm
mm
ORing
Code
Each
150 60 (2.4)
#50
60
100
7855-878
6384-225
1751.53
600 60 (2.4)
#50
99
205
7855-878
6384-231
1802.37
1000 100 (4)
#80
100
180
7855-880
6384-235
2009.44
2000 100 (4)
#80
126
210
7855-880
6384-239
2195.92
3000 150 (6)
#80
150
205
7855-881
6384-243
2635.79
6000 150 (6)
#80
150
395
7855-881
6384-247
2753.61
*Height measurements are measured from top of flask flange to seal on top thread.
Note: 150mL and 600mL heads have angled side necks.

13

35 PSIG
@100C
8075
Stirring
Shaft
8044
Bearing

6433
Head

6517
Clamp
7855
CAPFE
ORing

6384-19
Reactor
Body

8089
Agitator

Stand (13586) and Support


Shelf (11173) not included.
#50/5838 or/#80 5857
Bottom Adapter
w/Filter Support
(with 3/8" FNPT
outlet)
5844/12770 Adapter
3/8" MNPT 1/4" FNPT/
3/8" MNPT 3/8" MNPT

Glass Filter Discs

5839
Bottom
Valve

(For #80, bottom also available with 1/2inch MNPT.)

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

14

Bench Reactors/Filter

6386

JACKETED FILTER REACTOR

Rugged heavy wall reactor, jacketed for cooling and/or heating of reaction material. With 60mm
(2.4inch), 100mm (4inch), or 150mm (6inch) Schott style flange with oring groove at top,
for connection to 6527, 6528 or 6529 heads, with 6517 quick release clamp. Bottom has an
AceThred (internal glass thread) for installing 5838-83 (size 50) or 5857-86 (size 80) bottom
adapter with filter support and drain valve. Body is jacketed with size 28/15 oring ball joints
on inlet/outlet, sealed tangentially for more efficient circulation. Head has three 24/40 joints
on 60mm size; four 24/40 joints on 100mm and 150mm sizes.
8075
Stirring
Shaft

8066
Bearing

6527/6528/
6529 Head

6517
Clamp
7855
CAPFE
ORing

Complete item consists of: reactor body with 60mm CAPFE oring, head with joints, 6517
clamp, PTFE bottom adapter with CAPFE oring (with perforated plate #80 thread only),
retainer ring, 350 micron polypropylene screen support and 100 micron polyethylene support,
5844 adapter, 5839 shutoff valve (optional larger valve is available), non-flaking 8066 bearing,
8075 stirring rod, 8089 multipaddle agitator.
For replacement glass fritted support, polyethylene support or polypropylene screen, see 5848
or 5814. For condenser and funnel, see 6029 and 7298; stoppers with 24/40 joints, see 8250.
For stirring motor, see 13511 or 13566 motor; for chuck, see 8124 or 8126. Use 7855-829
CAPFE o-ring for #50 adapter, 7855-864 for #80 bottom adapter.
Flange
Bottom Body Approx.
Top
Cap.,
I.D.,
Thread
I.D., Height*,
CAPFE
Order
mL
mm (in.)
Size
mm
mm
ORing
Code
Each
150
60 (2.4)
#50
60
100
7855-878
6386-40
1965.54
600
60 (2.4)
#50
79
205
7855-878
6386-45
2232.07
1000
100 (4)
#80
100
180
7855-880
6386-50
2731.96
2000
100 (4)
#80
126
210
7855-880
6386-55
3072.39
3000
150 (6)
#80
150
205
7855-881
6386-60
3691.26
6000
150 (6)
#80
150
395
7855-881
6386-65
4011.93
*Height measurements are measured from top of flask flange to seal on top thread.
Note: 150mL and 600mL heads have angled side necks.

6386-16
Jacketed
Reactor
Body
8089
Agitator

Stand (13586) and Support


Shelf (11173) not included.
28/15 ORing
Ball Joint
Connectors

#50/5838 or/#80 5857


Bottom Adapter
w/Filter Support
(with 3/8 FNPT
outlet)

5844/12770
Adapter
3/8" MNPT 1/4" FNPT/
3/8" MNPT 3/8" MNPT

For a complete catalog of


recirculating chillers, please
contact Ace Glass.

5839
Bottom
Valve

(For #80, bottom also available with 1/2inch MNPT.)

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Subject to Ace Discount (Page 4)

Net

Bench Reactors/Filter

6386

JACKETED FILTER REACTOR, PRESSURE VERSION

Heavy wall glass reactor, jacketed version for cooling or heating of reactor. Available with 60mm
(2.4-inch), 100mm (4-inch), or 150mm (6-inch) diameter Schott flange with o-ring grove at top.
Connects to #6433 head with a #6517 quick release clamp. Reactor bottom has an AceThred
for installing a 5838-83 (size 50) or 5857-86 (size 80) adapter with a filter support and bottom
drain valve. Jacket inlet/outlet are size 28/15 o-ring ball joint connections, sealed tangentially for
more efficient circulation. The 60mm reactor head has a #15 AceThred center neck, (2) #15 and
(1) #7 AceThred side necks. The 100mm head has a #15 AceThred center neck, (3) #15 and
(1) #7 AceThred side necks. The 150mm head has a #15 AceThred center neck, (4) #15 and
(1) #7 AceThred side necks. The AceThreds allow for vacuum or pressure applications and
for draining material out of the reactor. The main bearing, funnel and condenser are designed to
connect to the threds on the head via compression bushing connections. The #7 AceThred is
used for connecting a 1/4-inch O.D. tubing fitting to allow for a direct connection to a pressure
source or a #6448 pressure manifold.
Complete item consists of: reactor body with 60mm CAPFE o-ring, head with
AceThreds, 6517 clamp, PTFE bottom threaded adapter and valve with CAPFE
o-ring, retainer ring, 350 micron polypropylene screen support, 100 micron
polyethylene support, 5844 adapter , 8044 bearing, 8075 stir rod, 8089 paddle
agitator, 6024 condenser, 7299 addition funnel and #7 AceThred bushing.
Size 80 bottom adapter also comes with a perforated glass plate support.

15

35 PSIG
@100C
8075
Stirring
Shaft

8044
Bearing

6433
Head

Pressure manifold (page 20), stand and clamps are optional. For replacement
glass fritted discs and supports see 5848 or 5814. For motor, see 13511 or
13566; for chucks see 8124 or 8126. Use 7855-829 CAPFE o-ring for #50
adapter, 7855-864 for #80 bottom adapter

6517
Clamp

Flange Bottom Body Approx.


Top
Cap.,
I.D.,
Thread I.D., Height*, CAPFE
Order
mL
mm (in.)
Size
mm
mm
ORing
Code
Each
150 60 (2.4) #50
60
100
7855-878 6386-107 2476.52
6386-16
600 60 (2.4) #50
79
205
7855-878 6386-110 2750.09
Jacketed
1000 100 (4)
#80
100
180
7855-880 6386-115 3284.22
Reactor
2000 100 (4)
#80
126
210
7855-880 6386-120 3644.20
Body
3000 150 (6)
#80
150
205
7855-881 6386-124 4314.14
6000 150 (6)
#80
150
395
7855-881 6386-128 4661.59
*Height measurements are measured from top of flask flange to seal on top thread.
Note: 150mL and 600mL heads have angled side necks.

7855
CAPFE
ORing

28/15 ORing
Ball Joint
Connectors

8089
Agitator

#50/5838 or/#80 5857


Bottom Adapter
w/Filter Support
(with 3/8 FNPT outlet)

E-SA

OR

ON

See page 219 for stands.

5844/12770
Adapter
3/8" MNPT 1/4"
FNPT/3/8" MNPT
3/8" MNPT

FE

AC

Stand (13586) and Support


Shelf (11173) not included.

N ECT

5839
Bottom
Valve

(For #80, bottom also available with 1/2inch MNPT.)

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Bench Reactors/Filter

16

Small
Volume

9534
Stirring
Shaft

6381

UNJACKETED FILTER REACTOR

Small-volume filter reactor with 45/50 joint at top and #50 AceThred (internal glass thread)
at bottom that accepts a 5838-83 (size 50) PTFE bottom adapter with filter support and drain
valve. Head has a 19/38 center neck and three 14/20 side necks. Complete item consists
of: reactor body, head with joints, clamp, #50 PTFE bottom adapter with size 136 CAPFE
oring, 350 micron polypropylene screen support, 100 micron polyethylene support, 5844
adapter, 5839-42 shutoff valve, 8066-120 non-flaking bearing, 9534-40 stirring rod, 9542-20
blade. For glass fritted support replacements for polypropylene screen and polyethylene support, see 5848 or 5814; for condensers see 6024; for addition funnel see 7299. For stirring
motor, see 13523; for chuck, see 8124 or 8126.

Complete:
Cap., mL
100
150

Top Joint
45/50
45/50

Bottom Thread
Size
#50
#50

Head, only
8066
Bearing

Cap., mL Order Code


100
9443-10
150
9443-10

Components:

9443
Head

6381-05
Body

Description
Adapter, PTFE,
3
8" mpt" FNPT, only
Bottom Adapter,
#5038" FNPT, only
Bottom Shutoff Valve,
" MNPT" Tube, PTFE
Clamp, Plastic, 45/50
Bearing, 19/22, 6mm
Stopper, 14/20

Each
188.78
188.78
Order
Code

5844-120
5838-83
5839-42
7598-45
8066-120
9543-04

Body I.D.,
mm
51
51

Body, only
Order Code
6381-05
6381-10

Approx.
Height, mm
65
125

Use
Joint Clamp
7598-45
7598-45

Complete

Each
114.95
119.18

Order Code
6381-25
6381-30

Description
Stirring Shaft, 6mm x 318mm
88.91
long, with button
Stirring Blade, PTFE
232.72
Each

Optional Accessories
PTFE Sleeves 14/20/Pkg. 3
50.48 PTFE Sleeves 19/38/Pkg. 3
111.21 PTFE Sleeves 45/50/Pkg. 3
14.30 Thermometer Adpt., 14/20
CAPFE o-ring
110.20

Each
836.60
840.83
Order
Code

Each

9534-40

42.71

9542-20
Order
Code
7642-07
7643-06
7642-23
5028-26
7855-829

9.45

10.00
5.73
27.14
27.55
23.39

9542
Blade

#50/5838
Bottom Adapter
w/Filter Support
(3/8" FNPT outlet)

Stand (13550), Clamp


(11079) and Clamp Holder
(13550-25) not included.

See page 51 for stands.

5844-120
Adapter
3/8" MNPT 1/4" FNPT
5839
Valve

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Subject to Ace Discount (Page 4)

Net

Bench Reactor Accessories

17

Filter Reactor Accessories and Replacement Parts

Instatherm Heated Filter Reactor

Use with either regular or pressure version head and accessories.


6388 FILTER REACTOR, UNJACKETED Instatherm, Body only
Same rugged, heavy-wall reactor flask as 6384, except Instatherm coated for
safer, rapid heating. Instatherm is an integral noble metal alloy fused permanently
to the glass and covered with a tough silicone rubber-treated glass cloth insulation
which serves as a thermal barrier as well as protection against physical shock. Heat
response is rapid and thermal lag low typical heating rates are approximately 5 per
minute. Instatherm can be operated at 120v or 40v with ACE or J-Kem temperature
controllers. Flange at top is Schott-Duran style 60mm (2.4inch), 100mm (4inch),
or 150mm (6inch) with shallow oring groove, for connection to 6527, 6528, 6529
or 6533 head, with 6517 quick release clamp. Bottom has a #50 or #80 AceThred
(internal glass thread) for installing 5838, 5857, or 5861 bottom adapter with filter
support and drain valve. For head, bottom adapter, and other accessory items,
order separately. Supplied with cord and CAPFE o-ring. Maximum temperature
(with no vacuum or pressure) is 200C.
Cap.,
mL
150
600
1000
2000
3000
6000

Flange Bottom
I.D., Thread
mm (in.) Size
60 (2.4) #50
60 (2.4) #50
100 (4) #80
100 (4) #80
150 (6) #80
150 (6) #80

Body Approx.
I.D., Height,
mm
mm
50
100
50
205
96
180
126
210
150
205
150
395

Top
CAPFE
ORing
7855-878
7855-878
7855-880
7855-880
7855-881
7855-881

Order
Volts Amps Watts Code
Each
40 6 240 6388-15 988.47
40 8 320 6388-20 1052.27
120 5 600 6388-25 1139.96
120 8 960 6388-30 1331.27
120 9 1080 6388-35 1674.05
120 10 1200 6388-40 1785.64

6388

ACE Custom Glass


Design Service
www.aceglass.com
ACE Scientific Glass Repair Service
www.aceglass.com

1-800-223-4524
Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Bench Reactor Accessories

18

Filter Reactor Accessories and Replacement Parts


6384 FILTER REACTOR Unjacketed, Body only
Reactor body, only, with Schott-style flange with oring groove at top and ACE #50 or
#80 internal thread at bottom. Pressure rating is 35 psi. Supplied with CAPFE oring.
6384

Cap.,
mL
150
600
1000
2000
3000
6000

6386

Flange
Bottom
I.D.,
Thread
mm (in.)
Size
60 (2.4)
#50
60 (2.4)
#50
100 (4)
#80
100 (4)
#80
150 (6)
#80
150 (6)
#80

Body
O.D.,
mm
70
89
110
140
165
165

Body
I.D.,
mm
60
79
100
126
150
150

Approx.
Height,
mm
100
205
180
210
205
395

Top
CAPFE
ORing
7855-878
7855-878
7855-880
7855-880
7855-881
7855-881

Order
Code
6384-05
6384-11
6384-15
6384-19
6384-23
6384-27

Each
257.21
301.01
369.42
536.35
827.76
913.96

6386 FILTER REACTOR Jacketed, Body only


Reactor body, only, with Schott-style flange with oring groove at top and ACE #50 or
#80 internal thread at bottom. Body is jacketed for heating/cooling. Inlet/outlet of jacket
are 28/15 oring ball joints, sealed tangentially, for more efficient circulation. Pressure
rating is 35 psi. Supplied with CAPFE oring.
Cap.,
mL
150
600
1000
2000
3000
6000

Flange
I.D.,
mm (in.)
60 (2.4)
60 (2.4)
100 (4)
100 (4)
150 (6)
150 (6)

Bottom
Thread
Size
#50
#50
#80
#80
#80
#80

Body
O.D.,
mm
100
120
140
180
190
190

Body
I.D.,
mm
60
79
100
126
150
150

Approx.
Height,
mm
100
205
180
210
205
395

Top
CAPFE
ORing
7855-878
7855-878
7855-880
7855-880
7855-881
7855-881

Order
Code
6386-06
6386-12
6386-16
6386-20
6386-24
6386-28

Each
982.20
1248.73
1644.20
1984.63
2506.11
2821.94

5839 VALVE PTFE, Bottom Shut Off


PTFE valve for bottom of 5838, 5857, or 5861 bottom adapter to control flow from reactor.
Code -42 has an male NPT thread at one end for attaching to 5844 adapter, other end is
a 1/4-inch O.D. tubing compression fitting; codes -47 and -55 have female NPT threads
on both ends, for connecting to 5844 adapter using 12770 nipple. Must use 5844-120
adapter (3/8-inch male NPT 1/4-inch female NPT) when connecting 5839-42; 12770-54
(3/8-inch male NPT 3/8-inch male NPT) when connecting 5839-47.

5839-42

5839-47, -55

5857-68

5839-55

5857-85

5839-42

5857-85

5838-80

12770-54

12770-54

5839-47

5839-47

12770-38

12770-38

Order Code
5839-42
5839-47
5839-55
12770-38

Each
110.20
505.36
532.33
24.21

PTFE adapter used to connect 5839-47 or -55 valve to 5838 or 5857 bottom adapter.
Order
NPT Size
Code
3/8" MNPT3/8" MNPT 12770-54

5844-120 12770-59 5844-120


5839-42

NPT Size
1/4" Male NPT1/4" Tube
3/8" Female NPT3/8" Female NPT
1/2" Female NPT1/2" Female NPT
3/8" Male NPT3/8" I.D. Tube

12770 ADAPTERPTFE

Reactor Bottom
Combinations
5838-80

For Bottom
Adapter Size
50
80
80
Barb (for use with 5839-47)

12770

Order
Each
NPT Size
Code
19.40 1/2" MNPT1/2" MNPT 12770-59

Each
29.49

5844 ADAPTERPTFE
Used to connect 5839 valve to 5838 or 5857 bottom adapter.

5844

Order
NPT Size
Code
3/8" MNPT1/4" FNPT 5844-120

Each
88.91

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Order
NPT Size
Code
Each
1/2" MNPT1/2" FNPT 5844-125 107.15

Subject to Ace Discount (Page 4)

Net

Bench Reactor Accessories

19

Filter Reactor Accessories and Replacement Parts


5848 PLATEGlass

5848-60

Perforated glass plate for #80 thread size 5857 or 5861 adapters.
Order Code
5848-60

Each
86.83

5838/5857 ADAPTER PTFE, Bottom Outlet


Bottom adapter for use with 6384, 6386 or 6388 reactor bodies and 6390 PTFE reactor.
Fabricated from PTFE, #50 and #80 have a 3/8-inch female NPT for connecting bottom
valve. Both have a CAPFE oring to seal adapter in AceThred. #50 size supplied with 100
micron polyethylene support disc (see 5848, above, for replacement or glass substitute).
Can also be replaced with screen support using retainer ring. #80 size supplied with
dual filter supports; a 100 micron polyethylene filter (see 5848, above) and/or perforated
support plate with retainer ring for use with 350 micron polypropylene screen (for other
screen sizes, see 5814).
For Thread Size
50
80
(Optional) 80
CAPFE oring, replacement for #50, Pkg/1
CAPFE oring, replacement for #80, Pkg/1

Bottom Opening
3/8-inch FNPT
3/8-inch FNPT
1/2-inch FNPT

Order Code
5838-83
5857-86
5857-89
7855-829
7855-864

Each
232.72
326.41
326.41
23.39
28.62

5857-86, -89
(Size 80)

5857 RETAINER RINGPTFE

5857-38

PTFE rings for size #50 & #80 adapters. Slide in to hold screens, filter paper, etc.
Adapter Size Thickness, mm
#50
0.125
#80
0.127

Dimensions
O.D., mm
1.955
2.950

I.D., mm
1.750
2.656

Order Code
5857-38
5857-52

5838
(Size 50)

Each
13.39
15.30

5814 SCREEN SUPPORTPolypropylene


For use with 5838, 5857, or 5861 bottom adapters. It is necessary to use a PTFE retainer
ring (above) to hold support in adapter. See page 265 for additional sizes.
Thread Size
50
80
50
80
50
80
50
80
50

Micron
350
350
295
295
210
210
105
105
74

Pkg. Quantity
12
12
12
6
12
6
12
6
12

Order Code
5814-348
5814-350
5814-358
5814-60
5814-368
5814-70
5814-88
5814-90
5814-378

Each
35.76
46.80
35.76
54.39
35.76
54.39
36.45
54.39
35.76

5861 ADAPTER PTFE, with Side Outlet

5814

5861

Same adapter as 5838/5857 except with 3/8-inch NPT side discharge port. Fits 6384,
6386, 6388 reactor flask bodies. Comes with 7855-800 series CAPFE o-rings. See 5814
screen support and 5857 retainer ring (above).
For Thread Size
50
80
CAPFE oring, replacement for #50, Pkg/1
CAPFE oring, replacement for #80, Pkg/1

Order Code
5861-03
5861-07
7855-829
7855-864

Each
234.71
323.51
23.39
28.62

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Bench Reactor Accessories

20

Filter Reactor Accessories and Replacement Parts


13385-44
5844-176

5844-74

5844-62
12517-14

8767-20

5844-74

5844-74

6448-24

6445-12

6448 MANIFOLD Pressure, Epoxy Coated


Complete glass manifold, fitted with a pressure gauge, primary
adjustable pressure relief valve, and secondary rupture disc to allow
for safer operation of pressure and filter reactors.
13385 Pressure Gauge is a 0-60 psi stainless steel internal, with
1-1/2inch face and 1/8-inch npt male connection for use with
5844-74 adapter in #15 AceThred.
8767 Pressure Relief Valve is adjustable from 3-50 psig by adjusting
set screws to desired cracking pressure. Ends are 1/4-inch npt for
connecting to #15 AceThred on manifold with 5844-74 adapter.

To 5844-58 #7 AceThred and 12517-08, -40

6445 Rupture Disc is a secondary safety device that, in the event of an overpressure (one that cannot be handled by the 8767
relief valve) will rupture at a predetermined burst rating; 55 psig (3 psig) for -12 version, 65 psig (3 psig) for -41 version. Disc is
manufactured from high-purity carbon with a PTFE coating on the underside. No springs or moving parts, disc is secured directly
in #25 AceThred of manifold with 5844176 adapter.
Manifold is connected to #7 AceThred on 6433 head using 584458 adapter (must be ordered separately) and 12517 tubing
connectors with 1/4inch tubing.
For Two-Piece
Pressure Reactors (55
psig) and Filter Reactors
Order Code
5844-62
5844-74
5844-176
6445-12

Each
67.75
67.75
88.93
133.39

6448-24
8767-20
12517-08
12517-14
12517-40
12681-110
13385-44
6448-54*

Replacement o-rings
Size 110 for #15 adapters (shelf-pack of 12)
Size 212 for #25 adapters (shelf-pack of 6)
Additional Items
Adapter, PTFE, #71/8-inch NPT

Adapter, PTFE, #151/8-inch NPT


Adapter, PTFE, #151/4-inch NPT (3)
Adapter, PTFE, #251/4-inch NPT, w/o oring
Rupture Disc, Graphite, 55 psig
Rupture Disc, Graphite, 65 psig (for pressure version only)
Manifold, Glass, (4) #15, (1) #25, Epoxy Coated
Valve, Pressure Relief, 1/4-inch NPT, 350 psig
Coupling Body, 1/8-inch MPT
Coupling Body, 1/4-inch MPT
Coupling Insert, for 1/4-inch O.D. tubing (2)
Tubing, PP, 1/4-inch O.D. x .170-inch I.D., 10 feet
Gauge, Pressure, 060 psi, 1/8-inch MPT
Complete

For One-Piece
Pressure R
eactors
(65 psig)
Order Code
5844-62
5844-74
5844-176

Each
67.75
67.75
88.93

197.03
86.02
11.42
12.07
12.25
13.22
171.92
989.82

6445-41
6448-24
8767-20
12517-08
12517-14
12517-40
12681-110
13385-44
6448-68**

133.39
197.03
86.02
11.42
12.07
12.25
13.22
171.92
989.82

7855-716
7855-734

19.78
20.14

7855-716
7855-734

19.78
20.14

5844-58

40.02

5844-58

40.02

*6448-54 is for use with two-piece pressure and filter style reactors.
**6448-68 is for use with one-piece pressure reactors only.

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Subject to Ace Discount (Page 4)

Net

Bench Reactors
A complete, general purpose
benchtop cylindrical reactor.
Self-supported and portable,
with a small footprint.

All-in-One
Benchtop Reactor

Electric heating mantle with digital


temperature controller and Type
J PTFE-covered thermoprobe for
operation from room temperature
to 200C

1 or 2 liter Cylindrical
Large 4-in. diameter flange on flask and head with
CAPFE (PTFE encapsulated silicone rubber) oring and
Quick Release clamp facilitate assembly/disassembly
and removal of contents.

125 mL pressure equalizing addition


funnel
Reflux condenser
Support stand, clamps, clamp
holders and joint clips

All glass and PTFE wetted components.


PTFE joint sleeves and valves and FETFE orings for
high-purity, grease-free system with high chemical
resistance.

Note: This re
ac
available with tor is
bo
outlet on flask ttom
; call or
e-mail for pric
e.

Suitable for high-vacuum situations.


Overhead mechanical stirring with 10 mm diameter glass
stirring shaft, PTFE multi-paddle agitator, flexible shaft
and variable speed motor with controller.

1 LITER

2 LITER
Order
Code

FLASK, 1-liter, Cylindrical, 4-inch (100mm) Grooved


Flange with CAPFE oring
HEAD, 4-inch (100mm) 24/40 Center Neck,
(3) 24/40 Side Necks
CLAMP, Quick Release, 4-inch
CONDENSER, 24/40, 300mm Jacket Length with
Ace-Safe Connectors
FUNNEL, Addition, 125mL, Pressure Equalizing,
24/40 Joints
STIRRING SHAFT, 10mm, Polished with Ring, 44cm
AGITATOR, PTFE, 4-Blade Multipaddle, 64 mm dia.
BEARING, 10mm, PTFE, 24/40, Complete
CHUCK, Flex-Grip, for 10mm Rod, 5/16-in. Motor Shaft
STIRRING MOTOR & CONTROLLER, Reversible, Variable
Speed, Complete
FLEXIBLE SHAFT, 91.4cm (36-inch)
HEATING MANTLE, Aluminum Housed, 335w, 115v
TEMP. CONTROLLER, Digital, Type J, 120 volts
THERMOPROBE, Type J, 1/4-in. O.D. x 12 in. long,
PTFE covered
THERMOPROBE, Lead Only, Detachable, Type J
ADAPTER, Offset, 24/40#7, Complete
ADAPTER, 24/40, 2mm Bore PTFE Stopcock
ADAPTER, Offset, 24/40 24/40
STOPPER, Glass 24/40 (3)
SLEEVES, PTFE 24/40, Pkg/3 (2)
JOINT CLIPS, Plastic 24/40, Pkg/10
SUPPORT STAND, 29 in. High x 5/8-in. Dia. Rod, U Base
CLAMP, Three-jaw, Medium
CLAMP HOLDER, Regular (3)
COMPLETE

21

Order
Code

Each

6521-10

152.00

6528-31

281.42

6517-25

98.23

5946-118

152.29

7298-05

231.90

8075-32
8089-06
8066-43
8124-10

57.11
111.43
111.75
43.92

13649-19

1265.18

8081-30
12058-12
12125-14

187.03
325.00
797.11

12141-25

118.70

12141-80
5032-22
5202-12
5268-10
8250-12
7642-11
7598-24
13586-10
11067-14
11080-19
6542-12

69.68
34.31
80.01
36.56
19.79
10.70
39.32
274.82
39.73
18.82
3953.86

FLASK, 2-liter, Cylindrical, 4-in. (100mm) Grooved Flange


with CAPFE oring
HEAD, 4-in. (100mm) 24/40 Center Neck,
(3) 24/40 Side Necks
CLAMP, Quick Release, 4-inch
CONDENSER, 24/40, 300mm Jacket Length with
Ace-Safe Connectors
FUNNEL, Addition, 125mL, Pressure Equalizing,
24/40 Joints
STIRRING SHAFT, 10mm, Polished with Ring, 58 cm
AGITATOR, PTFE, 4-Blade Multipaddle, 64mm dia.
BEARING, 10mm, PTFE, 24/40, Complete
CHUCK, Flex-Grip, for 10mm Rod, 5/16-in. Motor Shaft
STIRRING MOTOR & CONTROLLER, Reversible, Variable
Speed, Complete
FLEXIBLE SHAFT, 91.4cm (36")
HEATING MANTLE, Aluminum Housed, 450w, 115v
TEMP. CONTROLLER, Digital, Type J, 120 volts
THERMOPROBE, Type J, 1/4-in. O.D. x 12" long,
PTFE covered
THERMOPROBE, Lead Only, Detachable, Type J
ADAPTER, Offset, 24/40#7, Complete
ADAPTER, 24/40, 2mm Bore PTFE Stopcock
ADAPTER, Offset, 24/40 24/40
STOPPER, Glass 24/40 (3)
SLEEVES, PTFE 24/40, Pkg/3 (2)
JOINT CLIPS, Plastic 24/40, Pkg/10
SUPPORT STAND, 36 in. High x 5/8-in. Dia. Rod, U Base
CLAMP, Three-jaw, Medium
CLAMP HOLDER, Regular (3)
COMPLETE

Each

6521-12

161.73

6528-31

281.42

6517-25

98.23

5946-118

152.29

7298-05

231.90

8075-34
8089-06
8066-43
8124-10

60.33
111.43
111.75
43.92

13649-19

1265.18

8081-30
6478-51
12125-14

187.03
356.00
797.11

12141-25

118.70

12141-80
5032-22
5202-12
5268-10
8250-12
7642-11
7598-24
13586-13
11067-14
11080-19
6542-25

69.68
34.31
80.01
36.56
19.79
10.70
39.32
313.93
39.73
18.82
4120.32

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

22

Bench Reactors
A complete, general purpose
benchtop cylindrical reactor.
Self-supported and portable,
with a small footprint.

All-in-One Jacketed
Benchtop Reactor

Temperature controller and Type


J PTFE-covered thermoprobe for
operation from room temperature
to 200C

1 or 2 liter Cylindrical
Large 4-in. diameter flange on jacketed flask and
head with CAPFE (PTFE encapsulated silicone rubber)
oring and Quick Release clamp facilitate assembly/
disassembly and removal of contents.

125 mL pressure equalizing addition


funnel
Reflux condenser
Support stand, clamps, clamp
holders and joint clips

All glass and PTFE wetted components.


PTFE joint sleeves and valves and FETFE orings for
high-purity, grease-free system with high chemical
resistance.

Pressure manifold optional

Mechanical stirring with 10 mm diameter glass stirring


shaft, PTFE multi-paddle agitator, flexible shaft and
variable speed motor with controller.
Includes temperature controller and probe

1 LITER

2 LITER
Order
Code

FLASK, Jacketed, 1-liter, Cylindrical, 4-inch (100mm)


Grooved Flange with CAPFE oring, Bottom Outlet
HEAD, 4-inch (100mm) 24/40 Center Neck,
(3) 24/40 Side Necks
CLAMP, Quick Release, 4-inch
CONDENSER, 24/40, 300mm Jacket Length with
Ace-Safe Connectors
FUNNEL, Addition, 125mL, Pressure Equalizing,
24/40 Joints
STIRRING SHAFT, 10mm, Polished with Ring, 44cm
AGITATOR, PTFE, 4-Blade Multipaddle, 64 mm dia.
BEARING, 10mm, PTFE, 24/40, Complete
CHUCK, Flex-Grip, for 10mm Rod, 5/16-in. Motor Shaft
STIRRING MOTOR & CONTROLLER, Reversible, Variable
Speed, Complete
FLEXIBLE SHAFT, 91.4cm (36-inch)
ADAPTER, Offset, 24/40#7, Complete
ADAPTER, 24/40, 2mm Bore PTFE Stopcock
ADAPTER, Offset, 24/40 24/40
STOPPER, Glass 24/40 (3)
SLEEVES, PTFE 24/40, Pkg/3 (2)
JOINT CLIPS, Plastic 24/40, Pkg/10
SUPPORT STAND, 29 in. High x 5/8-in. Dia. Rod, U Base
CLAMP, Three-jaw, Medium
CLAMP HOLDER, Regular (4)
CLAMP, Chain Clamp
PLATE SUPPORT SHELF, w/102mm center hole
STAINLESS STEEL SUPPORT ROD, 28 inches high
COMPLETE

Order
Code

Each

6524-13

883.96

6528-31

281.42

6517-25

98.23

5946-118

152.29

7298-05

231.90

8075-32
8089-06
8066-43
8124-10

57.11
111.43
111.75
43.92

13649-19

1265.18

8081-30
5032-22
5202-12
5268-10
8250-12
7642-11
7598-24
13586-10
11067-14
11080-19
11079-24
11173-17
13586-25
6539-05

187.03
34.31
80.01
36.56
19.79
10.70
39.32
274.82
39.73
18.82
51.23
111.28
104.64
4203.00

FLASK, Jacketed, 2-liter, Cylindrical, 4-in. (100mm)


Grooved Flange with CAPFE oring, Bottom Outlet
HEAD, 4-in. (100mm) 24/40 Center Neck,
(3) 24/40 Side Necks
CLAMP, Quick Release, 4-inch
CONDENSER, 24/40, 300mm Jacket Length with
Ace-Safe Connectors
FUNNEL, Addition, 125mL, Pressure Equalizing,
24/40 Joints
STIRRING SHAFT, 10mm, Polished with Ring, 58 cm
AGITATOR, PTFE, 4-Blade Multipaddle, 64mm dia.
BEARING, 10mm, PTFE, 24/40, Complete
CHUCK, Flex-Grip, for 10mm Rod, 5/16-in. Motor Shaft
STIRRING MOTOR & CONTROLLER, Reversible, Variable
Speed, Complete
FLEXIBLE SHAFT, 91.4cm (36")
ADAPTER, Offset, 24/40#7, Complete
ADAPTER, 24/40, 2mm Bore PTFE Stopcock
ADAPTER, Offset, 24/40 24/40
STOPPER, Glass 24/40 (3)
SLEEVES, PTFE 24/40, Pkg/3 (2)
JOINT CLIPS, Plastic 24/40, Pkg/10
SUPPORT STAND, 36 in. High x 5/8-in. Dia. Rod, U Base
CLAMP, Three-jaw, Medium
CLAMP HOLDER, Regular (4)
CLAMP, Chain Clamp
PLATE SUPPORT SHELF, w/102mm center hole
STAINLESS STEEL SUPPORT ROD, 28 inches high
COMPLETE

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Each

6524-15

995.14

6528-31

281.42

6517-25

98.23

5946-118

152.29

7298-05

231.90

8075-34
8089-06
8066-43
8124-10

60.33
111.43
111.75
43.92

13649-19

1265.18

8081-30
5032-22
5202-12
5268-10
8250-12
7642-11
7598-24
13586-13
11067-14
11080-19
11079-24
11173-17
13586-25
6539-10

187.03
34.31
80.01
36.56
19.79
10.70
39.32
313.93
39.73
18.82
51.23
111.28
104.64
4355.59

Subject to Ace Discount (Page 4)

Net

Bench Reactors/Pressure

23

Pressure Reactors
T

he following ACE heavy wall borosilicate glass Pressure


Reactors have been designed and tested to provide the
chemist with a system to perform low to moderate positive
pressure reactions, synthesis, and catalysis, or simply to
run reactions under inert gas conditions. Reactor capacities
range from 500 mL to 5000mL, and use AceThreds to
achieve a leak-tight system.
Two types of Pressure Reactors are available:
1 Two-Piece System, with a maximum
pressure limit of 35 psig @ 100C.

Typical
Assembly

2 One-Piece System, with a maximum


pressure limit of 45 psig @ 100C
The Two-Piece System consists of a flanged flask and
head with a shallow oring groove, oring and quick release
clamp. Flange sizes range from 60mm to 150mm inside
diameter, allowing the use of large a
gitators and facilitating
product removal and clean-out.
The One-Piece System provides a 25mm center opening,
with smaller openings as side necks, and has a higher
allowable operating pressure.
Both systems offer vessels with or without bottom outlet
valves and with or without heating/cooling jackets. These
jackets are heat sealed.
Complete systems and their components are listed on the
following pages. Systems are available with:
Mechanical Stirring, using stirring shaft with
agitator, and a unique bearing designed with internal
oring seals.

Due to varying conditions, ACE cannot


guarantee glassware against breakage
caused by pressure or vacuum.

Safety is the foremost concern when operating


pressurized glass reactors. With this in mind, ACE
offers a separate manifold, 6448 (see photo), which
MUST be used in conjunction with all pressure systems
listed in this catalog. It consists of a glass manifold
with AceThreds, PTFE adapters, a pressure gauge,
a primary adjustable pressure release valve, and a
secondary fixed pressure rupture disc. In addition,
approved safety shields, eye and body protection
should be used to avoid personal injury.
For all complete systems the following accessories have
been included:
Liquid addition funnel
Stirring motor, controller and flexible shaft
Heating mantle and temperature control system
Thermowell
Temperature controller with thermocouple
Pressure relief manifold

IMPORTANT General Warnings for Pressurized Glassware


Due to varying conditions, ACE cannot guarantee glass vessels from breakage under pressure.
ALL LABORATORY SAFETY PROCEDURES SHOULD BE OBSERVED. ALWAYS WORK BEHIND A SHIELD.
Do not use with materials
which solidify on standing
and create excessive stress
on glass.

Before applying pressure,


examine glassware carefully
for surface scratches which
may weaken its strength.

Questions regarding the safe


operating conditions of a
particular glass vessel under
pressure may be directed to
ACE GLASS INCORPORATED.

Safety coatings: epoxy and


plastic coating help prevent
scratching and shattering and
reduce spills; however, they
do not prevent breakage

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Bench Reactors/Pressure

24

6423

Complete ACE
Two-Piece Unjacketed
Pressure Reactors

SERIES ONE

8081

Pressure Reactor
Manifold, Complete, 6448
(See page 20 for a complete
listing of parts in this assembly)

5846

Tubing
12681

8075

8124
7299

6024

13530

8044
12110
7506
6433
6471
6423

6517

12111

13649
12058

8648-19

8082-04

8116

14120

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Does NOT include stand, base or clamps.


Subject to Ace Discount (Page 4)

Net

Bench Reactors/Pressure

6423

25

Complete Unjacketed Two-Piece Pressure Reactor


Two-piece systems with a maximum pressure limit of 35 psig @ 100C.

SERIES ONE

6423-200 Complete System


(contains all items listed below)

500mL, 60mm Flange


#15 PTFE Plug (Complete contains TWO)
West Condenser w/AceThreds
Flask, 500 mL, 60mm flange top
Head, 60mm, #15 center neck, three side necks
Pressure Reactor Manifold, complete
Thermowell
Clamp, 60mm, Quick Release
Addition Funnel, 60mL
#15 PTFE Bushing (Complete contains TWO)
Bearing, complete, with AceThreds
Stir Shaft, 10mm
Flexible Shaft, complete, 91.4cm
Stirrer Blade, PTFE, 19mm
Krytox High Vacuum Grease
Flex-Grip Chuck
Bushing, PTFE, #15 with oring
Aluminum Heating Mantle
Type J Thermocouple Sensor, PTFE-clad
Digital Temperature Controller, J output
Polypropylene Tubing, 1/4-inch OD x 0.170-in. ID
Stirrer Motor Controller, Solid State
Stirrer Motor with Mounting Rod, Solid State
PTFE Sealing Tape, 1/2-inch Width

6423-205 Complete System


(contains all items listed below)

500mL, 100mm Flange


#15 PTFE Plug (Complete contains TWO)
West Condenser w/AceThreds
Flask, 500 mL, 100mm flange top
Head, 100mm, #15 center neck, four side necks
Pressure Reactor Manifold, complete
Thermowell
Clamp, 100mm, Quick Release
Addition Funnel, 60mL
#15 PTFE Bushing (Complete contains TWO)
Bearing, complete, with AceThreds
Stir Shaft, 10mm
Flexible Shaft, complete, 91.4cm
Stirrer Blade, PTFE, 19mm
Krytox High Vacuum Grease
Flex-Grip Chuck
Bushing, PTFE, #15 with oring
Aluminum Heating Mantle
Type J Thermocouple Sensor, PTFE-clad
Digital Temperature Controller, J output
Polypropylene Tubing, 1/4-inch OD x 0.170-in. ID
Stirrer Motor Controller, Solid State
Stirrer Motor with Mounting Rod, Solid State
PTFE Sealing Tape, 1/2-inch Width

6423-210 Complete System


(contains all items listed below)

1000mL, 100mm Flange


#15 PTFE Plug (Complete contains TWO)
West Condenser w/AceThreds
Flask, 1000 mL, 100mm flange top
Head, 100mm, #15 center neck, four side necks
Pressure Reactor Manifold, complete
Thermowell
Clamp, 100mm, Quick Release
Addition Funnel, 125mL
#15 PTFE Bushing (Complete contains TWO)
Bearing, complete, with AceThreds
Stir Shaft, 10mm
Flexible Shaft, complete, 91.4cm
Stirrer Blade, PTFE, 19mm
Krytox High Vacuum Grease
Flex-Grip Chuck
Bushing, PTFE, #15 with oring
Aluminum Heating Mantle
Type J Thermocouple Sensor, PTFE-clad
Digital Temperature Controller, J output
Polypropylene Tubing, 1/4-inch OD x 0.170-in. ID
Stirrer Motor Controller, Solid State
Stirrer Motor with Mounting Rod, Solid State
PTFE Sealing Tape, 1/2-inch Width

Order Code
6423-200

Each
5962.58

Order Code
5846-48
6024-20
6423-05
6433-23
6448-54
6471-04
6517-22
7299-06
7506-27
8044-24
8075-12
8081-30
8082-02
8116-10
8124-10
8648-19
12058-03
12110-25
12111-15
12681-110
13530-10
13649-09
14120-18

Each
38.41
129.75
170.98
295.48
989.82
36.76
87.08
305.29
40.65
233.08
55.65
187.03
8.39
105.04
43.92
31.37
622.85
50.88
1424.21
13.22
523.17
742.01
11.91

Order Code
6423-205

Each
6304.63

Order Code
5846-48
6024-20
6423-07
6433-35
6448-54
6471-10
6517-25
7299-06
7506-27
8044-24
8075-12
8081-30
8082-04
8116-10
8124-10
8648-19
12058-07
12110-25
12111-15
12681-110
13530-10
13649-09
14120-18

Each
38.41
129.75
218.67
396.77
989.82
36.76
98.23
305.29
40.65
233.08
55.65
187.03
10.03
105.04
43.92
31.37
825.72
50.88
1424.21
13.22
523.17
742.01
11.91

Order Code
6423-210

Each
5831.71

Order Code
5846-48
6024-20
6423-10
6433-35
6448-54
6471-14
6517-25
7299-12
7506-27
8044-24
8075-12
8081-30
8082-04
8116-10
8124-10
8648-19
12058-12
12110-25
12111-15
12681-110
13530-10
13649-09
14120-18

Each
38.41
129.75
242.49
396.77
989.82
37.64
98.23
313.29
40.65
233.08
55.65
187.03
10.03
105.04
43.92
31.37
325.00
50.88
1424.21
13.22
523.17
742.01
11.91

6423-215 Complete System


(contains all items listed below)

2000mL, 100mm Flange


#15 PTFE Plug (Complete contains TWO)
West Condenser w/AceThreds
Flask, 2000 mL, 100mm flange top
Head, 100mm, #15 center neck, four side necks
Pressure Reactor Manifold, complete
Thermowell
Clamp, 100mm, Quick Release
Addition Funnel, 250mL
#15 PTFE Bushing (Complete contains TWO)
Bearing, complete, with AceThreds
Stir Shaft, 10mm
Flexible Shaft, complete, 91.4cm
Stirrer Blade, PTFE, 19mm
Krytox High Vacuum Grease
Flex-Grip Chuck
Bushing, PTFE, #15 with oring
Aluminum Heating Mantle
Type J Thermocouple Sensor, PTFE-clad
Digital Temperature Controller, J output
Polypropylene Tubing, 1/4-inch OD x 0.170-in. ID
Stirrer Motor Controller, Solid State
Stirrer Motor with Mounting Rod, Solid State
PTFE Sealing Tape, 1/2-inch Width

6423-220 Complete System


(contains all items listed below)

3000mL, 150mm Flange


#15 PTFE Plug (Complete contains THREE)
West Condenser w/AceThreds
Flask, 3000 mL, 150mm flange top
Head, 150mm, #15 center neck, five side necks
Pressure Reactor Manifold, complete
Thermowell
Clamp, 150mm, Quick Release
Addition Funnel, 250mL
#15 PTFE Bushing (Complete contains TWO)
Bearing, complete, with AceThreds
Stir Shaft, 10mm
Flexible Shaft, complete, 91.4cm
Stirrer Blade, PTFE, 19mm
Krytox High Vacuum Grease
Flex-Grip Chuck
Bushing, PTFE, #15 with oring
Aluminum Heating Mantle
Type J Thermocouple Sensor, PTFE-clad
Digital Temperature Controller, J output
Polypropylene Tubing, 1/4-inch OD x 0.170-in. ID
Stirrer Motor Controller, Solid State
Stirrer Motor with Mounting Rod, Solid State
PTFE Sealing Tape, 1/2-inch Width

6423-225 Complete System


(contains all items listed below)

5000mL, 150mm Flange


#15 PTFE Plug (Complete contains THREE)
West Condenser w/AceThreds
Flask, 5000 mL, 100mm flange top
Head, 150mm, #15 center neck, five side necks
Pressure Reactor Manifold, complete
Thermowell
Clamp, 150mm, Quick Release
Addition Funnel, 500mL
#15 PTFE Bushing (Complete contains TWO)
Bearing, complete, with AceThreds
Stir Shaft, 10mm
Flexible Shaft, complete, 91.4cm
Stirrer Blade, PTFE, 19mm
Krytox High Vacuum Grease
Flex-Grip Chuck
Bushing, PTFE, #15 with oring
Aluminum Heating Mantle
Type J Thermocouple Sensor, PTFE-clad
Digital Temperature Controller, J output
Polypropylene Tubing, 1/4-inch OD x 0.170-in. ID
Stirrer Motor Controller, Solid State
Stirrer Motor with Mounting Rod, Solid State
PTFE Sealing Tape, 1/2-inch Width

Order Code
6423-215

Each
6145.75

Order Code
5846-48
6024-20
6423-20
6433-35
6448-54
6471-14
6517-25
7299-25
7506-27
8044-24
8075-12
8081-30
8082-04
8116-10
8124-10
8648-19
12058-16
12110-25
12111-15
12681-110
13530-10
13649-09
14120-18

Each
38.41
129.75
497.34
396.77
989.82
37.64
98.23
336.29
40.65
233.08
55.65
187.03
10.03
105.04
43.92
31.37
335.00
50.88
1424.21
13.22
523.17
742.01
11.91

Order Code
6423-220

Each
6785.85

Order Code
5846-48
6024-20
6423-30
6433-44
6448-54
6471-22
6517-27
7299-25
7506-27
8044-24
8075-12
8081-30
8082-06
8116-10
8124-10
8648-19
12058-30
12110-25
12111-15
12681-110
13530-10
13649-09
14120-18

Each
38.41
129.75
745.21
544.04
989.82
38.07
117.67
336.29
40.65
233.08
55.65
187.03
12.60
105.04
43.92
31.37
652.46
50.88
1424.21
13.22
523.17
742.01
11.91

Order Code
6423-225

Each
7114.32

Order Code
5846-48
6024-20
6423-35
6433-44
6448-54
6471-24
6517-27
7299-34
7506-27
8044-24
8075-14
8081-30
8082-06
8116-10
8124-10
8648-19
12058-33
12110-25
12111-15
12681-110
13530-10
13649-09
14120-18

Each
38.41
129.75
847.86
544.04
989.82
38.51
117.67
367.99
40.65
233.08
57.59
187.03
12.60
105.04
43.92
31.37
864.71
50.88
1424.21
13.22
523.17
742.01
11.91

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

26

Bench Reactors/Pressure

6425

Complete ACE
Two-Piece Unjacketed
Pressure Reactors

SERIES TWO

Bottom Outlet

8081
Pressure Reactor
Manifold, Complete, 6448

5846

(See page 20 for a complete


listing of parts in this assembly)

7299

12681
8124
8044
6024

8075

13530

12110

7506
6433
6471

6517
6425

12111

12058
13649

8648-19

8082-04

8116

14120
Does NOT include stand, base or clamps

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Subject to Ace Discount (Page 4)

Net

Bench Reactors/Pressure

6425

27

Complete Unjacketed Two-Piece Pressure Reactor


Two-piece systems with a maximum pressure limit of 35 psig @ 100C. Flask has bottom outlet.

SERIES TWO

6425-201 Complete System


(contains all items listed below)

500mL, 60mm Flange


#15 PTFE Plug (Complete contains TWO)
West Condenser w/AceThreds
Flask, 500mL, 60mm flange top w/bottom outlet
Head, 60mm, #15 center neck, three side necks
Pressure Reactor Manifold, complete
Thermowell
Clamp, 60mm, Quick Release
Addition Funnel, 60mL
#15 PTFE Bushing (Complete contains TWO)
Bearing, complete, with AceThreds
Stir Shaft, 10mm
Flexible Shaft, complete, 91.4cm
Stirrer Blade, PTFE, 19mm wide
Krytox High Vacuum Grease
Flex-Grip Chuck
Bushing, PTFE, #15 with oring
Aluminum Heating Mantle
Type J Thermocouple Sensor, PTFE-clad
Digital Temperature Controller, J output
Polypropylene Tubing, 1/4-inch OD x 0.170-in. ID
Stirrer Motor Controller, Solid State
Stirrer Motor with Mounting Rod, Solid State
PTFE Sealing Tape, 1/2-inch Width

6425-206 Complete System


(contains all items listed below)

500mL, 100mm Flange


#15 PTFE Plug (Complete contains TWO)
West Condenser w/AceThreds
Flask, 500mL, 100mm flange top w/bottom outlet
Head, 100mm, #15 center neck, four side necks
Pressure Reactor Manifold, complete
Thermowell
Clamp, 100mm, Quick Release
Addition Funnel, 60mL
#15 PTFE Bushing (Complete contains TWO)
Bearing, complete, with AceThreds
Stir Shaft, 10mm
Flexible Shaft, complete, 91.4cm
Stirrer Blade, PTFE, 19mm wide
Krytox High Vacuum Grease
Flex-Grip Chuck
Bushing, PTFE, #15 with oring
Aluminum Heating Mantle
Type J Thermocouple Sensor, PTFE-clad
Digital Temperature Controller, J output
Polypropylene Tubing, 1/4-inch OD x 0.170-in. ID
Stirrer Motor Controller, Solid State
Stirrer Motor with Mounting Rod, Solid State
PTFE Sealing Tape, 1/2-inch Width

6425-211 Complete System


(contains all items listed below)

1000mL, 100mm Flange


#15 PTFE Plug (Complete contains TWO)
West Condenser w/AceThreds
Flask, 1000mL, 100mm flange top w/bottom outlet
Head, 100mm, #15 center neck, four side necks
Pressure Reactor Manifold, complete
Thermowell
Clamp, 100mm, Quick Release
Addition Funnel, 125mL
#15 PTFE Bushing (Complete contains TWO)
Bearing, complete, with AceThreds
Stir Shaft, 10mm
Flexible Shaft, complete, 91.4cm
Stirrer Blade, PTFE, 19mm wide
Krytox High Vacuum Grease
Flex-Grip Chuck
Bushing, PTFE, #15 with oring
Aluminum Heating Mantle
Type J Thermocouple Sensor, PTFE-clad
Digital Temperature Controller, J output
Polypropylene Tubing, 1/4-inch OD x 0.170-in. ID
Stirrer Motor Controller, Solid State
Stirrer Motor with Mounting Rod, Solid State
PTFE Sealing Tape, 1/2-inch Width

Order Code
6425-201

Each
6126.56

Order Code
5846-48
6024-20
6425-04
6433-23
6448-54
6471-04
6517-22
7299-06
7506-27
8044-24
8075-12
8081-30
8082-02
8116-10
8124-10
8648-19
12058-44
12110-25
12111-15
12681-110
13530-10
13649-09
14120-18

Each
38.41
129.75
300.71
295.48
989.82
36.76
87.08
305.29
40.65
233.08
55.65
187.03
8.39
105.04
43.92
31.37
676.56
50.88
1424.21
13.22
523.17
742.01
11.91

Order Code
6425-206

Each
6188.89

Order Code
5846-48
6024-20
6425-06
6433-35
6448-54
6471-10
6517-25
7299-06
7506-27
8044-24
8075-12
8081-30
8082-04
8116-10
8124-10
8648-19
12058-47
12110-25
12111-15
12681-110
13530-10
13649-09
14120-18

Each
38.41
129.75
354.34
396.77
989.82
36.76
98.23
305.29
40.65
233.08
55.65
187.03
10.03
105.04
43.92
31.37
594.66
50.88
1424.21
13.22
523.17
742.01
11.91

Order Code
6425-211

Each
6223.42

Order Code
5846-48
6024-20
6425-12
6433-35
6448-54
6471-14
6517-25
7299-12
7506-27
8044-24
8075-12
8081-30
8082-04
8116-10
8124-10
8648-19
12058-49
12110-25
12111-15
12681-110
13530-10
13649-09
14120-18

Each
38.41
129.75
376.20
396.77
989.82
37.64
98.23
313.29
40.65
233.08
55.65
187.03
10.03
105.04
43.92
31.37
603.06
50.88
1424.21
13.22
523.17
742.01
11.91

6425-214 Complete System


(contains all items listed below)

2000mL, 100mm Flange


#15 PTFE Plug (Complete contains TWO)
West Condenser w/AceThreds
Flask, 2000mL, 100mm flange top w/bottom outlet
Head, 100mm, #15 center neck, four side necks
Pressure Reactor Manifold, complete
Thermowell
Clamp, 100mm, Quick Release
Addition Funnel, 250mL
#15 PTFE Bushing (Complete contains TWO)
Bearing, complete, with AceThreds
Stir Shaft, 10mm
Flexible Shaft, complete, 91.4cm
Stirrer Blade, PTFE, 19mm wide
Krytox High Vacuum Grease
Flex-Grip Chuck
Bushing, PTFE, #15 with oring
Aluminum Heating Mantle
Type J Thermocouple Sensor, PTFE-clad
Digital Temperature Controller, J output
Polypropylene Tubing, 1/4-inch OD x 0.170-in. ID
Stirrer Motor Controller, Solid State
Stirrer Motor with Mounting Rod, Solid State
PTFE Sealing Tape, 1/2-inch Width

6425-221 Complete System


(contains all items listed below)

3000mL, 150mm Flange


#15 PTFE Plug (Complete contains THREE)
West Condenser w/AceThreds
Flask, 3000mL, 150mm flange top w/bottom outlet
Head, 150mm, #15 center neck, five side necks
Pressure Reactor Manifold, complete
Thermowell
Clamp, 150mm, Quick Release
Addition Funnel, 250mL
#15 PTFE Bushing (Complete contains TWO)
Bearing, complete, with AceThreds
Stir Shaft, 10mm
Flexible Shaft, complete, 91.4cm
Stirrer Blade, PTFE, 24mm wide
Krytox High Vacuum Grease
Flex-Grip Chuck
Bushing, PTFE, #15 with oring
Aluminum Heating Mantle
Type J Thermocouple Sensor, PTFE-clad
Digital Temperature Controller, J output
Polypropylene Tubing, 1/4-inch OD x 0.170-in. ID
Stirrer Motor Controller, Solid State
Stirrer Motor with Mounting Rod, Solid State
PTFE Sealing Tape, 1/2-inch Width

6425-226 Complete System


(contains all items listed below)

5000mL, 150mm Flange


#15 PTFE Plug (Complete contains THREE)
West Condenser w/AceThreds
Flask, 5000mL, 150mm flange top w/bottom outlet
Head, 150mm, #15 center neck, five side necks
Pressure Reactor Manifold, complete
Thermowell
Clamp, 150mm, Quick Release
Addition Funnel, 500mL
#15 PTFE Bushing (Complete contains TWO)
Bearing, complete, with AceThreds
Stir Shaft, 10mm
Flexible Shaft, complete, 91.4cm
Stirrer Blade, PTFE, 24mm wide
Krytox High Vacuum Grease
Flex-Grip Chuck
Bushing, PTFE, #15 with oring
Aluminum Heating Mantle
Type J Thermocouple Sensor, PTFE-clad
Digital Temperature Controller, J output
Polypropylene Tubing, 1/4-inch OD x 0.170-in. ID
Stirrer Motor Controller, Solid State
Stirrer Motor with Mounting Rod, Solid State
PTFE Sealing Tape, 1/2-inch Width

Order Code
6425-214

Each
6503.89

Order Code
5846-48
6024-20
6425-15
6433-35
6448-54
6471-14
6517-25
7299-25
7506-27
8044-24
8075-12
8081-30
8082-04
8116-10
8124-10
8648-19
12058-51
12110-25
12111-15
12681-110
13530-10
13649-09
14120-18

Each
38.41
129.75
651.79
396.77
989.82
37.64
98.23
336.29
40.65
233.08
55.65
187.03
10.03
105.04
43.92
31.37
561.86
50.88
1424.21
13.22
523.17
742.01
11.91

Order Code
6425-221

Each
7007.57

Order Code
5846-48
6024-20
6425-19
6433-44
6448-54
6471-22
6517-27
7299-25
7506-27
8044-24
8075-12
8081-30
8082-06
8116-10
8124-10
8648-19
12058-53
12110-25
12111-15
12681-110
13530-10
13649-09
14120-18

Each
38.41
129.75
890.27
544.04
989.82
38.07
117.67
336.29
40.65
233.08
55.65
187.03
12.60
105.04
43.92
31.37
750.88
50.88
1424.21
13.22
523.17
742.01
11.91

Order Code
6425-226

Each
7255.22

Order Code
5846-48
6024-20
6425-23
6433-44
6448-54
6471-24
6517-27
7299-34
7506-27
8044-24
8075-14
8081-30
8082-06
8116-10
8124-10
8648-19
12058-55
12110-25
12111-15
12681-110
13530-10
13649-09
14120-18

Each
38.41
129.75
990.44
544.04
989.82
38.51
117.67
367.99
40.65
233.08
57.59
187.03
12.60
105.04
43.92
31.37
884.42
50.88
1424.21
13.22
523.17
742.01
11.91

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

28

Bench Reactors/Pressure

6427

Complete ACE
Two-Piece Jacketed
Pressure Reactors

SERIES ONE

8081

5846

Pressure Reactor
Manifold, Complete, 6448
(See page 20 for a complete
listing of parts in this assembly)

7299
12681
8124

6024

8075
8044
13530
7506

6433

6517

6471

6427

8648-19

8082-04

8116

13649

14120

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Does NOT include stand, base or clamps.


Shown without clamps for better visibility.
Subject to Ace Discount (Page 4)

Net

Bench Reactors/Pressure

6427

29

Complete Jacketed Two-Piece Pressure Reactor


Two-piece systems with a maximum pressure limit of 35 psig @ 100C.

SERIES ONE

6427-207 Complete System


(contains all items listed below)

500mL, 60mm Flange


#15 PTFE Plug (Complete contains TWO)
West Condenser w/AceThreds
Flask, 500mL, 60mm flange top
Head, 60mm, #15 center neck, three side necks
Pressure Reactor Manifold, complete
Thermowell
Clamp, 60mm, Quick Release
Addition Funnel, 60mL
#15 PTFE Bushing (Complete contains TWO)
Bearing, complete, with AceThreds
Stir Shaft, 10mm
Flexible Shaft, complete, 91.4cm
Stirrer Blade, PTFE, 19mm wide
Krytox High Vacuum Grease
Flex-Grip Chuck
Bushing, PTFE, #15 with oring
Polypropylene Tubing, 1/4-inch OD x 0.170-in. ID
Stirrer Motor Controller, Solid State
Stirrer Motor with Mounting Rod, Solid State
PTFE Sealing Tape, 1/2-inch Width

6427-209 Complete System


(contains all items listed below)

500mL, 100mm Flange


#15 PTFE Plug (Complete contains TWO)
West Condenser w/AceThreds
Flask, 500mL, 100mm flange top
Head, 100mm, #15 center neck, four side necks
Pressure Reactor Manifold, complete
Thermowell
Clamp, 100mm, Quick Release
Addition Funnel, 60mL
#15 PTFE Bushing (Complete contains TWO)
Bearing, complete, with AceThreds
Stir Shaft, 10mm
Flexible Shaft, complete, 91.4cm
Stirrer Blade, PTFE, 19mm wide
Krytox High Vacuum Grease
Flex-Grip Chuck
Bushing, PTFE, #15 with oring
Polypropylene Tubing, 1/4-inch OD x 0.170-in. ID
Stirrer Motor Controller, Solid State
Stirrer Motor with Mounting Rod, Solid State
PTFE Sealing Tape, 1/2-inch Width

6427-212 Complete System


(contains all items listed below)

1000mL, 100mm Flange


#15 PTFE Plug (Complete contains TWO)
West Condenser w/AceThreds
Flask, 1000mL, 100mm flange top
Head, 100mm, #15 center neck, four side necks
Pressure Reactor Manifold, complete
Thermowell
Clamp, 100mm, Quick Release
Addition Funnel, 125mL
#15 PTFE Bushing (Complete contains TWO)
Bearing, complete, with AceThreds
Stir Shaft, 10mm
Flexible Shaft, complete, 91.4cm
Stirrer Blade, PTFE, 19mm wide
Krytox High Vacuum Grease
Flex-Grip Chuck
Bushing, PTFE, #15 with oring
Polypropylene Tubing, 1/4-inch OD x 0.170-in. ID
Stirrer Motor Controller, Solid State
Stirrer Motor with Mounting Rod, Solid State
PTFE Sealing Tape, 1/2-inch Width

Order Code
6427-207
Order Code
5846-48
6024-20
6427-09
6433-23
6448-54
6471-04
6517-22
7299-06
7506-27
8044-24
8075-12
8081-30
8082-02
8116-10
8124-10
8648-19
12681-110
13530-10
13649-09
14120-18
Order Code
6427-209
Order Code
5846-48
6024-20
6427-13
6433-35
6448-54
6471-10
6517-25
7299-06
7506-27
8044-24
8075-12
8081-30
8082-04
8116-10
8124-10
8648-19
12681-110
13530-10
13649-09
14120-18
Order Code
6427-212
Order Code
5846-48
6024-20
6427-16
6433-35
6448-54
6471-14
6517-25
7299-12
7506-27
8044-24
8075-12
8081-30
8082-04
8116-10
8124-10
8648-19
12681-110
13530-10
13649-09
14120-18

Each
4397.46
Each
38.41
129.75
797.82
295.48
989.82
36.76
87.08
305.29
40.65
233.08
55.65
187.03
8.39
105.04
43.92
31.37
13.22
523.17
742.01
11.91
Each
4483.60
Each
38.41
129.75
783.11
396.77
989.82
36.76
98.23
305.29
40.65
233.08
55.65
187.03
10.03
105.04
43.92
31.37
13.22
523.17
742.01
11.91
Each
4506.53
Each
38.41
129.75
801.21
396.77
989.82
37.64
98.23
313.29
40.65
233.08
55.65
187.03
10.03
105.04
43.92
31.37
13.22
523.17
742.01
11.91

6427-217 Complete System


(contains all items listed below)

2000mL, 100 Flange


#15 PTFE Plug (Complete contains TWO)
West Condenser w/AceThreds
Flask, 2000mL, 100mm flange top
Head, 100mm, #15 center neck, four side necks
Pressure Reactor Manifold, complete
Thermowell
Clamp, 100mm, Quick Release
Addition Funnel, 150mL
#15 PTFE Bushing (Complete contains TWO)
Bearing, complete, with AceThreds
Stir Shaft, 10mm
Flexible Shaft, complete, 91.4cm
Stirrer Blade, PTFE, 19mm wide
Krytox High Vacuum Grease
Flex-Grip Chuck
Bushing, PTFE, #15 with oring
Polypropylene Tubing, 1/4-inch OD x 0.170-in. ID
Stirrer Motor Controller, Solid State
Stirrer Motor with Mounting Rod, Solid State
PTFE Sealing Tape, 1/2-inch Width

6427-223 Complete System


(contains all items listed below)

3000mL, 150mm Flange


#15 PTFE Plug (Complete contains THREE)
West Condenser w/AceThreds
Flask, 3000mL, 150mm flange top
Head, 150mm, #15 center neck, five side necks
Pressure Reactor Manifold, complete
Thermowell
Clamp, 150mm, Quick Release
Addition Funnel, 150mL
#15 PTFE Bushing (Complete contains TWO)
Bearing, complete, with AceThreds
Stir Shaft, 10mm
Flexible Shaft, complete, 91.4cm
Stirrer Blade, PTFE, 24mm wide
Krytox High Vacuum Grease
Flex-Grip Chuck
Bushing, PTFE, #15 with oring
Polypropylene Tubing, 1/4-inch OD x 0.170-in. ID
Stirrer Motor Controller, Solid State
Stirrer Motor with Mounting Rod, Solid State
PTFE Sealing Tape, 1/2-inch Width

6427-228 Complete System


(contains all items listed below)

5000mL, 150mm Flange


#15 PTFE Plug (Complete contains THREE)
West Condenser w/AceThreds
Flask, 5000mL, 150mm flange top
Head, 150mm, #15 center neck, five side necks
Pressure Reactor Manifold, complete
Thermowell
Clamp, 150mm, Quick Release
Addition Funnel, 500mL
#15 PTFE Bushing (Complete contains TWO)
Bearing, complete, with AceThreds
Stir Shaft, 10mm
Flexible Shaft, complete, 91.4cm
Stirrer Blade, PTFE, 24mm wide
Krytox High Vacuum Grease
Flex-Grip Chuck
Bushing, PTFE, #15 with oring
Polypropylene Tubing, 1/4-inch OD x 0.170-in. ID
Stirrer Motor Controller, Solid State
Stirrer Motor with Mounting Rod, Solid State
PTFE Sealing Tape, 1/2-inch Width

Order Code
6427-217

Each
4975.84

Order Code
5846-48
6024-20
6427-18
6433-35
6448-54
6471-14
6517-25
7299-25
7506-27
8044-24
8075-12
8081-30
8082-04
8116-10
8124-10
8648-19
12681-110
13530-10
13649-09
14120-18

Each
38.41
129.75
1250.49
396.77
989.82
37.64
98.23
336.29
40.65
233.08
55.65
187.03
10.03
105.04
43.92
31.37
13.22
523.17
742.01
11.91

Order Code
6427-223

Each
6944.97

Order Code
5846-48
6024-20
6427-23
6433-44
6448-54
6471-22
6517-27
7299-25
7506-27
8044-24
8075-12
8081-30
8082-06
8116-10
8124-10
8648-19
12681-110
13530-10
13649-09
14120-18

Each
38.41
129.75
3435.42
544.04
989.82
38.07
117.67
336.29
40.65
233.08
55.65
187.03
12.60
105.04
43.92
31.37
13.22
523.17
742.01
11.91

Order Code
6427-228

Each
7062.60

Order Code
5846-48
6024-20
6427-26
6433-44
6448-54
6471-24
6517-27
7299-34
7506-27
8044-24
8075-14
8081-30
8082-06
8116-10
8124-10
8648-19
12681-110
13530-10
13649-09
14120-18

Each
38.41
129.75
3539.72
544.04
989.82
38.51
117.67
367.99
40.65
233.08
57.59
187.03
12.60
105.04
43.92
31.37
13.22
523.17
742.01
11.91

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

30

Bench Reactors/Pressure

6429

Complete ACE
Two-Piece Jacketed
Pressure Reactors

SERIES TWO

Bottom Outlet

8081

5846
Pressure Reactor
Manifold, Complete, 6448
(See page 20 for a complete
listing of parts in this assembly)

7299
8124
8075
12681
8044
6024

13530

7506

6433
6471
6517
6429

13649

8648-19

8082-04

8116

14120

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Does NOT include stand, base or clamps.


Shown without clamps for better visibility.
Subject to Ace Discount (Page 4)

Net

Bench Reactors/Pressure

6429

31

Complete Jacketed Two-Piece Pressure Reactor


Two-piece systems with a maximum pressure limit of 35 psig @ 100C. Flask has bottom outlet.

SERIES TWO

6429-229 Complete System


(contains all items listed below)

500mL, 60mm Flange


#15 PTFE Plug (Complete contains TWO)
West Condenser w/AceThreds
Flask, 500mL, 60mm flange top, bottom outlet
Head, 60mm, #15 center neck, three side necks
Pressure Reactor Manifold, complete
Thermowell
Clamp, 60mm, Quick Release
Addition Funnel, 60mL
#15 PTFE Bushing (Complete contains TWO)
Bearing, complete, with AceThreds
Stir Shaft, 10mm
Flexible Shaft, complete, 91.4cm
Stirrer Blade, PTFE, 19mm wide
Krytox High Vacuum Grease
Flex-Grip Chuck
Bushing, PTFE, #15 with oring
Polypropylene Tubing, 1/4-inch OD x 0.170-in. ID
Stirrer Motor Controller, Solid State
Stirrer Motor with Mounting Rod, Solid State
PTFE Sealing Tape, 1/2-inch Width

6429-232 Complete System


(contains all items listed below)

500mL, 100mm Flange


#15 PTFE Plug (Complete contains TWO)
West Condenser w/AceThreds
Flask, 500mL, 100mm flange top, bottom outlet
Head, 100mm, #15 center neck, four side necks
Pressure Reactor Manifold, complete
Thermowell
Clamp, 100mm, Quick Release
Addition Funnel, 60mL
#15 PTFE Bushing (Complete contains TWO)
Bearing, complete, with AceThreds
Stir Shaft, 10mm
Flexible Shaft, complete, 91.4cm
Stirrer Blade, PTFE, 19mm wide
Krytox High Vacuum Grease
Flex-Grip Chuck
Bushing, PTFE, #15 with oring
Polypropylene Tubing, 1/4-inch OD x 0.170-in. ID
Stirrer Motor Controller, Solid State
Stirrer Motor with Mounting Rod, Solid State
PTFE Sealing Tape, 1/2-inch Width

6429-235 Complete System


(contains all items listed below)

1000mL, 100mm Flange


#15 PTFE Plug (Complete contains TWO)
West Condenser w/AceThreds
Flask, 1000mL, 100mm flange top, bottom outlet
Head, 100mm, #15 center neck, four side necks
Pressure Reactor Manifold, complete
Thermowell
Clamp, 100mm, Quick Release
Addition Funnel, 125mL
#15 PTFE Bushing (Complete contains TWO)
Bearing, complete, with AceThreds
Stir Shaft, 10mm
Flexible Shaft, complete, 91.4cm
Stirrer Blade, PTFE, 19mm wide
Krytox High Vacuum Grease
Flex-Grip Chuck
Bushing, PTFE, #15 with oring
Polypropylene Tubing, 1/4-inch OD x 0.170-in. ID
Stirrer Motor Controller, Solid State
Stirrer Motor with Mounting Rod, Solid State
PTFE Sealing Tape, 1/2-inch Width

Order Code
6429-229
Order Code
5846-48
6024-20
6429-09
6433-23
6448-54
6471-04
6517-22
7299-06
7506-27
8044-24
8075-12
8081-30
8082-02
8116-10
8124-10
8648-19
12681-110
13530-10
13649-09
14120-18
Order Code
6429-232
Order Code
5846-48
6024-20
6429-14
6433-35
6448-54
6471-10
6517-25
7299-06
7506-27
8044-24
8075-12
8081-30
8082-04
8116-10
8124-10
8648-19
12681-110
13530-10
13649-09
14120-18
Order Code
6429-235
Order Code
5846-48
6024-20
6429-20
6433-35
6448-54
6471-14
6517-25
7299-12
7506-27
8044-24
8075-12
8081-30
8082-04
8116-10
8124-10
8648-19
12681-110
13530-10
13649-09
14120-18

Each
4465.31
Each
38.41
129.75
877.65
295.48
989.82
36.76
87.08
305.29
40.65
233.08
55.65
187.03
8.39
105.04
43.92
31.37
13.22
523.17
742.01
11.91
Each
4628.76
Each
38.41
129.75
953.89
396.77
989.82
36.76
98.23
305.29
40.65
233.08
55.65
187.03
10.03
105.04
43.92
31.37
13.22
523.17
742.01
11.91
Each
4644.19
Each
38.41
129.75
963.17
396.77
989.82
37.64
98.23
313.29
40.65
233.08
55.65
187.03
10.03
105.04
43.92
31.37
13.22
523.17
742.01
11.91

6429-237 Complete System


(contains all items listed below)

2000mL, 100mm Flange


#15 PTFE Plug (Complete contains TWO)
West Condenser w/AceThreds
Flask, 2000mL, 100mm flange top, bottom outlet
Head, 100mm, #15 center neck, four side necks
Pressure Reactor Manifold, complete
Thermowell
Clamp, 100mm, Quick Release
Addition Funnel, 150mL
#15 PTFE Bushing (Complete contains TWO)
Bearing, complete, with AceThreds
Stir Shaft, 10mm
Flexible Shaft, complete, 91.4cm
Stirrer Blade, PTFE, 19mm wide
Krytox High Vacuum Grease
Flex-Grip Chuck
Bushing, PTFE, #15 with oring
Polypropylene Tubing, 1/4-inch OD x 0.170-in. ID
Stirrer Motor Controller, Solid State
Stirrer Motor with Mounting Rod, Solid State
PTFE Sealing Tape, 1/2-inch Width

6429-242 Complete System


(contains all items listed below)

3000mL, 150mm Flange


#15 PTFE Plug (Complete contains THREE)
West Condenser w/AceThreds
Flask, 3000mL, 150mm flange top, bottom outlet
Head, 150mm, #15 center neck, five side necks
Pressure Reactor Manifold, complete
Thermowell
Clamp, 150mm, Quick Release
Addition Funnel, 150mL
#15 PTFE Bushing (Complete contains TWO)
Bearing, complete, with AceThreds
Stir Shaft, 10mm
Flexible Shaft, complete, 91.4cm
Stirrer Blade, PTFE, 24mm wide
Krytox High Vacuum Grease
Flex-Grip Chuck
Bushing, PTFE, #15 with oring
Polypropylene Tubing, 1/4-inch OD x 0.170-in. ID
Stirrer Motor Controller, Solid State
Stirrer Motor with Mounting Rod, Solid State
PTFE Sealing Tape, 1/2-inch Width

6429-245 Complete System


(contains all items listed below)

5000mL, 150mm Flange


#15 PTFE Plug (Complete contains THREE)
West Condenser w/AceThreds
Flask, 5000mL, 150mm flange top, bottom outlet
Head, 150mm, #15 center neck, five side necks
Pressure Reactor Manifold, complete
Thermowell
Clamp, 150mm, Quick Release
Addition Funnel, 500mL
#15 PTFE Bushing (Complete contains TWO)
Bearing, complete, with AceThreds
Stir Shaft, 10mm
Flexible Shaft, complete, 91.4cm
Stirrer Blade, PTFE, 24mm wide
Krytox High Vacuum Grease
Flex-Grip Chuck
Bushing, PTFE, #15 with oring
Polypropylene Tubing, 1/4-inch OD x 0.170-in. ID
Stirrer Motor Controller, Solid State
Stirrer Motor with Mounting Rod, Solid State
PTFE Sealing Tape, 1/2-inch Width

Order Code
6429-237

Each
5124.18

Order Code
5846-48
6024-20
6429-24
6433-35
6448-54
6471-14
6517-25
7299-25
7506-27
8044-24
8075-12
8081-30
8082-04
8116-10
8124-10
8648-19
12681-110
13530-10
13649-09
14120-18

Each
38.41
129.75
1425.01
396.77
989.82
37.64
98.23
336.29
40.65
233.08
55.65
187.03
10.03
105.04
43.92
31.37
13.22
523.17
742.01
11.91

Order Code
6429-242

Each
7058.33

Order Code
5846-48
6024-20
6429-28
6433-44
6448-54
6471-22
6517-27
7299-25
7506-27
8044-24
8075-12
8081-30
8082-06
8116-10
8124-10
8648-19
12681-110
13530-10
13649-09
14120-18

Each
38.41
129.75
3568.78
544.04
989.82
38.07
117.67
336.29
40.65
233.08
55.65
187.03
12.60
105.04
43.92
31.37
13.22
523.17
742.01
11.91

Order Code
6429-245

Each
7254.82

Order Code
5846-48
6024-20
6429-33
6433-44
6448-54
6471-24
6517-27
7299-34
7506-27
8044-24
8075-14
8081-30
8082-06
8116-10
8124-10
8648-19
12681-110
13530-10
13649-09
14120-18

Each
38.41
129.75
3765.86
544.04
989.82
38.51
117.67
367.99
40.65
233.08
57.59
187.03
12.60
105.04
43.92
31.37
13.22
523.17
742.01
11.91

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

32

Bench Reactors/Pressure

6436

Complete ACE
One-Piece Unjacketed
Pressure Reactors
8081

SERIES FOUR
Pressure Reactor
Manifold, Complete, 6448
(See page 20 for a complete
listing of parts in this assembly)

8124

5846

Tubing
12681

8075
7299
8044

13530

6024
12110
7506
6436
12111

6471

13649

12058

8082-04
8648-19

8116

14120
Does NOT include stand, base or clamps

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Subject to Ace Discount (Page 4)

Net

Bench Reactors/Pressure

6436

33

Complete Unjacketed One-Piece Pressure Reactor


One-piece systems with a maximum pressure limit of 45 psig @ 100C.

SERIES FOUR
6436-233 Complete System
(contains all items listed below)

500mL
#15 PTFE Plug (Complete contains TWO)
West Condenser w/AceThreds
Flask, 500mL
Pressure Reactor Manifold, complete
Thermowell
Addition Funnel, 60mL
#15 PTFE Bushing (Complete contains TWO)
Bearing, complete, with AceThreds
Stir Shaft, 10mm
Flexible Shaft, complete, 91.4cm
Stirrer Blade, PTFE, 19mm
Krytox High Vacuum Grease
Flex-Grip Chuck
Bushing, PTFE, #15 with oring
Aluminum Heating Mantle
Type J Thermocouple Sensor, PTFE-clad
Digital Temperature Controller, J output
Polypropylene Tubing, 1/4-inch OD x 0.170-in. ID
Stirrer Motor Controller, Solid State
Stirrer Motor with Mounting Rod, Solid State
PTFE Sealing Tape, 1/2-inch Width

6436-236 Complete System


(contains all items listed below)

1000mL
#15 PTFE Plug (Complete contains TWO)
West Condenser w/AceThreds
Flask, 1000mL
Pressure Reactor Manifold, complete
Thermowell
Addition Funnel, 125mL
#15 PTFE Bushing (Complete contains TWO)
Bearing, complete, with AceThreds
Stir Shaft, 10mm
Flexible Shaft, complete, 91.4cm
Stirrer Blade, PTFE, 19mm
Krytox High Vacuum Grease
Flex-Grip Chuck
Bushing, PTFE, #15 with oring
Aluminum Heating Mantle
Type J Thermocouple Sensor, PTFE-clad
Digital Temperature Controller, J output
Polypropylene Tubing, 1/4-inch OD x 0.170-in. ID
Stirrer Motor Controller, Solid State
Stirrer Motor with Mounting Rod, Solid State
PTFE Sealing Tape, 1/2-inch Width

6436-239 Complete System


(contains all items listed below)

2000mL
#15 PTFE Plug (Complete contains TWO)
West Condenser w/AceThreds
Flask, 2000mL
Pressure Reactor Manifold, complete
Thermowell
Addition Funnel, 150mL
#15 PTFE Bushing (Complete contains TWO)
Bearing, complete, with AceThreds
Stir Shaft, 10mm
Flexible Shaft, complete, 91.4cm
Stirrer Blade, PTFE, 19mm
Krytox High Vacuum Grease
Flex-Grip Chuck
Bushing, PTFE, #15 with oring
Aluminum Heating Mantle
Type J Thermocouple Sensor, PTFE-clad
Digital Temperature Controller, J output
Polypropylene Tubing, 1/4-inch OD x 0.170-in. ID
Stirrer Motor Controller, Solid State
Stirrer Motor with Mounting Rod, Solid State
PTFE Sealing Tape, 1/2-inch Width

Order Code
6436-233

Each
6085.40

Order Code
5846-48
6024-20
6436-06
6448-68
6471-41
7299-06
7506-27
8044-55
8075-12
8081-30
8082-04
8116-10
8124-10
8648-19
12058-07
12110-25
12111-15
12681-110
13530-10
13649-09
14120-18

Each
38.41
129.75
458.51
989.82
36.76
305.29
40.65
247.66
55.65
187.03
10.03
105.04
43.92
31.37
825.72
50.88
1424.21
13.22
523.17
742.01
11.91

Order Code
6436-236

Each
5622.87

Order Code
5846-48
6024-20
6436-09
6448-68
6471-43
7299-12
7506-27
8044-55
8075-12
8081-30
8082-04
8116-10
8124-10
8648-19
12058-12
12110-25
12111-15
12681-110
13530-10
13649-09
14120-18

Each
38.41
129.75
495.44
989.82
36.76
313.29
40.65
247.66
55.65
187.03
10.03
105.04
43.92
31.37
325.00
50.88
1424.21
13.22
523.17
742.01
11.91

Order Code
6436-239

Each
5771.68

Order Code
5846-48
6024-20
6436-22
6448-68
6471-43
7299-25
7506-27
8044-55
8075-12
8081-30
8082-04
8116-10
8124-10
8648-19
12058-16
12110-25
12111-15
12681-110
13530-10
13649-09
14120-18

Each
38.41
129.75
555.89
989.82
36.76
336.29
40.65
247.66
55.65
187.03
10.03
105.04
43.92
31.37
335.00
50.88
1424.21
13.22
523.17
742.01
11.91

6436-243 Complete System


(contains all items listed below)

3000mL
#15 PTFE Plug (Complete contains THREE)
West Condenser w/AceThreds
Flask, 3000mL
Pressure Reactor Manifold, complete
Thermowell
Addition Funnel, 150mL
#15 PTFE Bushing (Complete contains TWO)
Bearing, complete, with AceThreds
Stir Shaft, 10mm
Flexible Shaft, complete, 91.4cm
Stirrer Blade, PTFE, 19mm
Krytox High Vacuum Grease
Flex-Grip Chuck
Bushing, PTFE, #15 with oring
Aluminum Heating Mantle
Type J Thermocouple Sensor, PTFE-clad
Digital Temperature Controller, J output
Polypropylene Tubing, 1/4-inch OD x 0.170-in. ID
Stirrer Motor Controller, Solid State
Stirrer Motor with Mounting Rod, Solid State
PTFE Sealing Tape, 1/2-inch Width

6436-245 Complete System


(contains all items listed below)

5000mL
#15 PTFE Plug (Complete contains THREE)
West Condenser w/AceThreds
Flask, 5000mL
Pressure Reactor Manifold, complete
Thermowell
Addition Funnel, 500mL
#15 PTFE Bushing (Complete contains TWO)
Bearing, complete, with AceThreds
Stir Shaft, 10mm
Flexible Shaft, complete, 91.4cm
Stirrer Blade, PTFE, 19mm
Krytox High Vacuum Grease
Flex-Grip Chuck
Bushing, PTFE, #15 with oring
Aluminum Heating Mantle
Type J Thermocouple Sensor, PTFE-clad
Digital Temperature Controller, J output
Polypropylene Tubing, 1/4-inch OD x 0.170-in. ID
Stirrer Motor Controller, Solid State
Stirrer Motor with Mounting Rod, Solid State
PTFE Sealing Tape, 1/2-inch Width

Order Code
6436-243

Each
6091.12

Order Code
5846-48
6024-20
6436-31
6448-68
6471-47
7299-25
7506-27
8044-55
8075-12
8081-30
8082-04
8116-10
8124-10
8648-19
12058-30
12110-25
12111-15
12681-110
13530-10
13649-09
14120-18

Each
38.41
129.75
598.78
989.82
37.64
336.29
40.65
247.66
55.65
187.03
10.03
105.04
43.92
31.37
652.46
50.88
1424.21
13.22
523.17
742.01
11.91

Order Code
6436-245

Each
6373.93

Order Code
5846-48
6024-20
6436-37
6448-68
6471-49
7299-34
7506-27
8044-55
8075-14
8081-30
8082-04
8116-10
8124-10
8648-19
12058-33
12110-25
12111-15
12681-110
13530-10
13649-09
14120-18

Each
38.41
129.75
647.28
989.82
38.51
367.99
40.65
247.66
57.59
187.03
10.03
105.04
43.92
31.37
864.71
50.88
1424.21
13.22
523.17
742.01
11.91

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

34

Bench Reactors/Pressure
Complete ACE
One-Piece Unjacketed
Pressure Reactors

8081

with Bottom Outlet

6437
SERIES SIX

Pressure Reactor
Manifold, Complete, 6448
(See page 20 for a complete
listing of parts in this assembly)

5846

7299

8124
8075
8044
12681
6024
7506
13530
6437

6471

12110

12058
12111

13649

8082-04
8648-19

8116

14120
Does NOT include stand, base or clamps

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Subject to Ace Discount (Page 4)

Net

Bench Reactors/Pressure

6437

35

Complete Unjacketed One-Piece Pressure Reactor


One-piece systems with a maximum pressure limit of 45 psig @ 100C. Flask has bottom outlet.

SERIES SIX

6437-235 Complete System


(contains all items listed below)

500mL
#15 PTFE Plug (Complete contains TWO)
West Condenser w/AceThreds
Flask, 500mL
Pressure Reactor Manifold, complete
Thermowell
Addition Funnel, 60mL
#15 PTFE Bushing (Complete contains TWO)
Bearing, complete, with AceThreds
Stir Shaft, 10mm
Flexible Shaft, complete, 91.4cm
Stirrer Blade, 19mm
Krytox High Vacuum Grease
Flex-Grip Chuck
Bushing, PTFE, #15 with oring
Aluminum Heating Mantle
Type J Thermocouple Sensor, PTFE-clad
Digital Temperature Controller, J output
Polypropylene Tubing, 1/4-inch OD x 0.170-in. ID
Stirrer Motor Controller, Solid State
Stirrer Motor with Mounting Rod, Solid State
PTFE Sealing Tape, 1/2-inch Width

6437-238 Complete System


(contains all items listed below)

1000mL
#15 PTFE Plug (Complete contains TWO)
West Condenser w/AceThreds
Flask, 1000mL
Pressure Reactor Manifold, complete
Thermowell
Addition Funnel, 125mL
#15 PTFE Bushing (Complete contains TWO)
Bearing, complete, with AceThreds
Stir Shaft, 10mm
Flexible Shaft, complete, 91.4cm
Stirrer Blade, 19mm
Krytox High Vacuum Grease
Flex-Grip Chuck
Bushing, PTFE, #15 with oring
Aluminum Heating Mantle
Type J Thermocouple Sensor, PTFE-clad
Digital Temperature Controller, J output
Polypropylene Tubing, 1/4-inch OD x 0.170-in. ID
Stirrer Motor Controller, Solid State
Stirrer Motor with Mounting Rod, Solid State
PTFE Sealing Tape, 1/2-inch Width

6437-241 Complete System


(contains all items listed below)

2000mL
#15 PTFE Plug (Complete contains TWO)
West Condenser w/AceThreds
Flask, 2000mL
Pressure Reactor Manifold, complete
Thermowell
Addition Funnel, 150mL
#15 PTFE Bushing (Complete contains TWO)
Bearing, complete, with AceThreds
Stir Shaft, 10mm
Flexible Shaft, complete, 91.4cm
Stirrer Blade, 19mm
Krytox High Vacuum Grease
Flex-Grip Chuck
Bushing, PTFE, #15 with oring
Aluminum Heating Mantle
Type J Thermocouple Sensor, PTFE-clad
Digital Temperature Controller, J output
Polypropylene Tubing, 1/4-inch OD x 0.170-in. ID
Stirrer Motor Controller, Solid State
Stirrer Motor with Mounting Rod, Solid State
PTFE Sealing Tape, 1/2-inch Width

Order Code
6437-235

Each
5965.67

Order Code
5846-48
6024-20
6437-07
6448-68
6471-41
7299-06
7506-27
8044-55
8075-12
8081-30
8082-04
8116-10
8124-10
8648-19
12058-47
12110-25
12111-15
12681-110
13530-10
13649-09
14120-18

Each
38.41
129.75
589.48
989.82
36.76
305.29
40.65
247.66
55.65
187.03
10.03
105.04
43.92
31.37
594.66
50.88
1424.21
13.22
523.17
742.01
11.91

Order Code
6437-238

Each
6003.33

Order Code
5846-48
6024-20
6437-13
6448-68
6471-43
7299-12
7506-27
8044-55
8075-12
8081-30
8082-04
8116-10
8124-10
8648-19
12058-49
12110-25
12111-15
12681-110
13530-10
13649-09
14120-18

Each
38.41
129.75
615.91
989.82
36.76
313.29
40.65
247.66
55.65
187.03
10.03
105.04
43.92
31.37
603.06
50.88
1424.21
13.22
523.17
742.01
11.91

Order Code
6437-241

Each
6053.43

Order Code
5846-48
6024-20
6437-16
6448-68
6471-43
7299-25
7506-27
8044-55
8075-12
8081-30
8082-04
8116-10
8124-10
8648-19
12058-51
12110-25
12111-15
12681-110
13530-10
13649-09
14120-18

Each
38.41
129.75
700.32
989.82
36.76
336.29
40.65
247.66
55.65
187.03
10.03
105.04
43.92
31.37
561.86
50.88
1424.21
13.22
523.17
742.01
11.91

6437-244 Complete System


(contains all items listed below)

3000mL
#15 PTFE Plug (Complete contains THREE)
West Condenser w/AceThreds
Flask, 3000mL
Pressure Reactor Manifold, complete
Thermowell
Addition Funnel, 150mL
#15 PTFE Bushing (Complete contains TWO)
Bearing, complete, with AceThreds
Stir Shaft, 10mm
Flexible Shaft, complete, 91.4cm
Stirrer Blade, 19mm
Krytox High Vacuum Grease
Flex-Grip Chuck
Bushing, PTFE, #15 with oring
Aluminum Heating Mantle
Type J Thermocouple Sensor, PTFE-clad
Digital Temperature Controller, J output
Polypropylene Tubing, 1/4-inch OD x 0.170-in. ID
Stirrer Motor Controller, Solid State
Stirrer Motor with Mounting Rod, Solid State
PTFE Sealing Tape, 1/2-inch Width

6437-246 Complete System


(contains all items listed below)

5000mL
#15 PTFE Plug (Complete contains THREE)
West Condenser w/AceThreds
Flask, 5000mL
Pressure Reactor Manifold, complete
Thermowell
Addition Funnel, 500mL
#15 PTFE Bushing (Complete contains TWO)
Bearing, complete, with AceThreds
Stir Shaft, 10mm
Flexible Shaft, complete, 91.4cm
Stirrer Blade, 19mm
Krytox High Vacuum Grease
Flex-Grip Chuck
Bushing, PTFE, #15 with oring
Aluminum Heating Mantle
Type J Thermocouple Sensor, PTFE-clad
Digital Temperature Controller, J output
Polypropylene Tubing, 1/4-inch OD x 0.170-in. ID
Stirrer Motor Controller, Solid State
Stirrer Motor with Mounting Rod, Solid State
PTFE Sealing Tape, 1/2-inch Width

Order Code
6437-244

Each
6326.87

Order Code
5846-48
6024-20
6437-20
6448-68
6471-47
7299-25
7506-27
8044-55
8075-12
8081-30
8082-04
8116-10
8124-10
8648-19
12058-53
12110-25
12111-15
12681-110
13530-10
13649-09
14120-18

Each
38.41
129.75
760.35
989.82
37.64
336.29
40.65
247.66
55.65
187.03
10.03
105.04
43.92
31.37
750.88
50.88
1424.21
13.22
523.17
742.01
11.91

Order Code
6437-246

Each
6560.27

Order Code
5846-48
6024-20
6437-24
6448-68
6471-49
7299-34
7506-27
8044-55
8075-14
8081-30
8082-04
8116-10
8124-10
8648-19
12058-55
12110-25
12111-15
12681-110
13530-10
13649-09
14120-18

Each
38.41
129.75
700.32
989.82
38.51
367.99
40.65
247.66
57.59
187.03
10.03
105.04
43.92
31.37
884.42
50.88
1424.21
13.22
523.17
742.01
11.91

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

36

Bench Reactors/Pressure

6438

Complete ACE
One-Piece Jacketed
Pressure Reactors

8081

SERIES FOUR
Pressure Reactor
Manifold, Complete, 6448

5846

(See page 20 for a complete


listing of parts in this assembly)

8124
7299
12681
8075

13530

8044
6024

7506

6471
6438

13649

8082-04
8648-19

8116

14120

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Does NOT include stand, base or clamps.


Shown without clamps for better visibility.
Subject to Ace Discount (Page 4)

Net

Bench Reactors/Pressure

6438

37

Complete Jacketed One-Piece Pressure Reactor


One-piece systems with a maximum pressure limit of 45 psig @ 100C.

SERIES FOUR
6438-240 Complete System
(contains all items listed below)

500mL
#15 PTFE Plug (Complete contains TWO)
West Condenser w/AceThreds
Flask, 500mL
Pressure Reactor Manifold, complete
Thermowell
Addition Funnel, 60mL
#15 PTFE Bushing (Complete contains TWO)
Bearing, complete, with AceThreds
Stir Shaft, 10mm
Flexible Shaft, complete, 91.4cm
Stirrer Blade, PTFE, 19mm
Krytox High Vacuum Grease
Flex-Grip Chuck
Bushing, PTFE, #15 with oring
Polypropylene Tubing, 1/4-inch OD x 0.170-in. ID
Stirrer Motor Controller, Solid State
Stirrer Motor with Mounting Rod, Solid State
PTFE Sealing Tape, 1/2-inch Width

6438-247 Complete System


(contains all items listed below)

1000mL
#15 PTFE Plug (Complete contains TWO)
West Condenser w/AceThreds
Flask, 1000mL
Pressure Reactor Manifold, complete
Thermowell
Addition Funnel, 125mL
#15 PTFE Bushing (Complete contains TWO)
Bearing, complete, with AceThreds
Stir Shaft, 10mm
Flexible Shaft, complete, 91.4cm
Stirrer Blade, PTFE, 19mm
Krytox High Vacuum Grease
Flex-Grip Chuck
Bushing, PTFE, #15 with oring
Polypropylene Tubing, 1/4-inch OD x 0.170-in. ID
Stirrer Motor Controller, Solid State
Stirrer Motor with Mounting Rod, Solid State
PTFE Sealing Tape, 1/2-inch Width

6438-250 Complete System


(contains all items listed below)

2000mL
#15 PTFE Plug (Complete contains TWO)
West Condenser w/AceThreds
Flask, 2000mL
Pressure Reactor Manifold, complete
Thermowell
Addition Funnel, 150mL
#15 PTFE Bushing (Complete contains TWO)
Bearing, complete, with AceThreds
Stir Shaft, 10mm
Flexible Shaft, complete, 91.4cm
Stirrer Blade, PTFE, 19mm
Krytox High Vacuum Grease
Flex-Grip Chuck
Bushing, PTFE, #15 with oring
Polypropylene Tubing, 1/4-inch OD x 0.170-in. ID
Stirrer Motor Controller, Solid State
Stirrer Motor with Mounting Rod, Solid State
PTFE Sealing Tape, 1/2-inch Width

Order Code
6438-240

Each
4335.74

Order Code
5846-48
6024-20
6438-14
6448-68
6471-41
7299-06
7506-27
8044-55
8075-12
8081-30
8082-04
8116-10
8124-10
8648-19
12681-110
13530-10
13649-09
14120-18

Each
38.41
129.75
1106.92
989.82
36.76
305.29
40.65
247.66
55.65
187.03
10.03
105.04
43.92
31.37
13.22
523.17
742.01
11.91

Order Code
6438-247

Each
4381.43

Order Code
5846-48
6024-20
6438-17
6448-68
6471-43
7299-12
7506-27
8044-55
8075-12
8081-30
8082-04
8116-10
8124-10
8648-19
12681-110
13530-10
13649-09
14120-18

Each
38.41
129.75
1152.67
989.82
36.76
313.29
40.65
247.66
55.65
187.03
10.03
105.04
43.92
31.37
13.22
523.17
742.01
11.91

Order Code
6438-250

Each
4491.69

Order Code
5846-48
6024-20
6438-19
6448-68
6471-43
7299-25
7506-27
8044-55
8075-12
8081-30
8082-04
8116-10
8124-10
8648-19
12681-110
13530-10
13649-09
14120-18

Each
38.41
129.75
1259.39
989.82
36.76
336.29
40.65
247.66
55.65
187.03
10.03
105.04
43.92
31.37
13.22
523.17
742.01
11.91

6438-253 Complete System


(contains all items listed below)

3000mL
#15 PTFE Plug (Complete contains THREE)
West Condenser w/AceThreds
Flask, 3000mL
Pressure Reactor Manifold, complete
Thermowell
Addition Funnel, 150mL
#15 PTFE Bushing (Complete contains TWO)
Bearing, complete, with AceThreds
Stir Shaft, 10mm
Flexible Shaft, complete, 91.4cm
Stirrer Blade, PTFE, 19mm
Krytox High Vacuum Grease
Flex-Grip Chuck
Bushing, PTFE, #15 with oring
Polypropylene Tubing, 1/4-inch OD x 0.170-in. ID
Stirrer Motor Controller, Solid State
Stirrer Motor with Mounting Rod, Solid State
PTFE Sealing Tape, 1/2-inch Width

6438-255 Complete System


(contains all items listed below)

5000mL
#15 PTFE Plug (Complete contains THREE)
West Condenser w/AceThreds
Flask, 5000mL
Pressure Reactor Manifold, complete
Thermowell
Addition Funnel, 500mL
#15 PTFE Bushing (Complete contains TWO)
Bearing, complete, with AceThreds
Stir Shaft, 10mm
Flexible Shaft, complete, 91.4cm
Stirrer Blade, PTFE, 19mm
Krytox High Vacuum Grease
Flex-Grip Chuck
Bushing, PTFE, #15 with oring
Polypropylene Tubing, 1/4-inch OD x 0.170-in. ID
Stirrer Motor Controller, Solid State
Stirrer Motor with Mounting Rod, Solid State
PTFE Sealing Tape, 1/2-inch Width

Order Code
6438-253

Each
6081.12

Order Code
5846-48
6024-20
6438-24
6448-68
6471-47
7299-25
7506-27
8044-55
8075-12
8081-30
8082-04
8116-10
8124-10
8648-19
12681-110
13530-10
13649-09
14120-18

Each
38.41
129.75
3090.02
989.82
37.64
336.29
40.65
247.66
55.65
187.03
10.03
105.04
43.92
31.37
13.22
523.17
742.01
11.91

Order Code
6438-255

Each
6260.14

Order Code
5846-48
6024-20
6438-29
6448-68
6471-49
7299-34
7506-27
8044-55
8075-14
8081-30
8082-04
8116-10
8124-10
8648-19
12681-110
13530-10
13649-09
14120-18

Each
38.41
129.75
3266.12
989.82
38.51
367.99
40.65
247.66
57.59
187.03
10.03
105.04
43.92
31.37
13.22
523.17
742.01
11.91

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

38

Bench Reactors/Pressure

6439

Complete ACE
One-Piece Jacketed
Pressure Reactors

SERIES SIX

with Bottom Outlet

8081

Pressure Reactor
Manifold, Complete, 6448
(See page 20 for a complete
listing of parts in this assembly)

5846
12681
7299

8124

8075
6024

8081
7506

13530
6471

6439

13649

8082-04
8648-19

8116

14120

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Does NOT include stand, base or clamps.


Shown without clamps for better visibility.
Subject to Ace Discount (Page 4)

Net

Bench Reactors/Pressure

6439

39

Complete Jacketed One-Piece Pressure Reactor


One-piece systems with a maximum pressure limit of 45 psig @ 100C. Flask has bottom outlet.

SERIES SIX

6439-243 Complete System


(contains all items listed below)

500mL
#15 PTFE Plug (Complete contains TWO)
West Condenser w/AceThreds
Flask, 500mL with bottom outlet
Pressure Reactor Manifold, complete
Thermowell
Addition Funnel, 60mL
#15 PTFE Bushing (Complete contains TWO)
Bearing, complete, with AceThreds
Stir Shaft, 10mm
Flexible Shaft, complete, 91.4cm
Stirrer Blade, PTFE, 19mm
Krytox High Vacuum Grease
Flex-Grip Chuck
Bushing, PTFE, #15 with oring
Polypropylene Tubing, 1/4-inch OD x 0.170-in. ID
Stirrer Motor Controller, Solid State
Stirrer Motor with Mounting Rod, Solid State
PTFE Sealing Tape, 1/2-inch Width

6439-248 Complete System


(contains all items listed below)

1000mL
#15 PTFE Plug (Complete contains TWO)
West Condenser w/AceThreds
Flask, 1000mL with bottom outlet
Pressure Reactor Manifold, complete
Thermowell
Addition Funnel, 125mL
#15 PTFE Bushing (Complete contains TWO)
Bearing, complete, with AceThreds
Stir Shaft, 10mm
Flexible Shaft, complete, 91.4cm
Stirrer Blade, PTFE, 19mm
Krytox High Vacuum Grease
Flex-Grip Chuck
Bushing, PTFE, #15 with oring
Polypropylene Tubing, 1/4-inch OD x 0.170-in. ID
Stirrer Motor Controller, Solid State
Stirrer Motor with Mounting Rod, Solid State
PTFE Sealing Tape, 1/2-inch Width

6439-252 Complete System


(contains all items listed below)

2000mL
#15 PTFE Plug (Complete contains TWO)
West Condenser w/AceThreds
Flask, 2000mL with bottom outlet
Pressure Reactor Manifold, complete
Thermowell
Addition Funnel, 150mL
#15 PTFE Bushing (Complete contains TWO)
Bearing, complete, with AceThreds
Stir Shaft, 10mm
Flexible Shaft, complete, 91.4cm
Stirrer Blade, PTFE, 19mm
Krytox High Vacuum Grease
Flex-Grip Chuck
Bushing, PTFE, #15 with oring
Polypropylene Tubing, 1/4-inch OD x 0.170-in. ID
Stirrer Motor Controller, Solid State
Stirrer Motor with Mounting Rod, Solid State
PTFE Sealing Tape, 1/2-inch Width

Order Code
6439-243

Each
4413.43

Order Code
5846-48
6024-20
6439-15
6448-68
6471-41
7299-06
7506-27
8044-55
8075-12
8081-30
8082-04
8116-10
8124-10
8648-19
12681-110
13530-10
13649-09
14120-18

Each
38.41
129.75
1198.32
989.82
36.76
305.29
40.65
247.66
55.65
187.03
10.03
105.04
43.92
31.37
13.22
523.17
742.01
11.91

Order Code
6439-248

Each
4465.70

Order Code
5846-48
6024-20
6439-21
6448-68
6471-43
7299-12
7506-27
8044-55
8075-12
8081-30
8082-04
8116-10
8124-10
8648-19
12681-110
13530-10
13649-09
14120-18

Each
38.41
129.75
1251.81
989.82
36.76
313.29
40.65
247.66
55.65
187.03
10.03
105.04
43.92
31.37
13.22
523.17
742.01
11.91

Order Code
6439-252

Each
4590.10

Order Code
5846-48
6024-20
6439-25
6448-68
6471-43
7299-25
7506-27
8044-55
8075-12
8081-30
8082-04
8116-10
8124-10
8648-19
12681-110
13530-10
13649-09
14120-18

Each
38.41
129.75
1375.16
989.82
36.76
336.29
40.65
247.66
55.65
187.03
10.03
105.04
43.92
31.37
13.22
523.17
742.01
11.91

6439-254 Complete System


(contains all items listed below)

3000mL
#15 PTFE Plug (Complete contains THREE)
West Condenser w/AceThreds
Flask, 3000mL with bottom outlet
Pressure Reactor Manifold, complete
Thermowell
Addition Funnel, 150mL
#15 PTFE Bushing (Complete contains TWO)
Bearing, complete, with AceThreds
Stir Shaft, 10mm
Flexible Shaft, complete, 91.4cm
Stirrer Blade, PTFE, 19mm
Krytox High Vacuum Grease
Flex-Grip Chuck
Bushing, PTFE, #15 with oring
Polypropylene Tubing, 1/4-inch OD x 0.170-in. ID
Stirrer Motor Controller, Solid State
Stirrer Motor with Mounting Rod, Solid State
PTFE Sealing Tape, 1/2-inch Width

6439-257 Complete System


(contains all items listed below)

5000mL
#15 PTFE Plug (Complete contains THREE)
West Condenser w/AceThreds
Flask, 5000mL with bottom outlet
Pressure Reactor Manifold, complete
Thermowell
Addition Funnel, 500mL
#15 PTFE Bushing (Complete contains TWO)
Bearing, complete, with AceThreds
Stir Shaft, 10mm
Flexible Shaft, complete, 91.4cm
Stirrer Blade, PTFE, 19mm
Krytox High Vacuum Grease
Flex-Grip Chuck
Bushing, PTFE, #15 with oring
Polypropylene Tubing, 1/4-inch OD x 0.170-in. ID
Stirrer Motor Controller, Solid State
Stirrer Motor with Mounting Rod, Solid State
PTFE Sealing Tape, 1/2-inch Width

Order Code
6439-254

Each
6211.17

Order Code
5846-48
6024-20
6439-29
6448-68
6471-47
7299-25
7506-27
8044-55
8075-12
8081-30
8082-04
8116-10
8124-10
8648-19
12681-110
13530-10
13649-09
14120-18

Each
38.41
129.75
3243.02
989.82
37.64
336.29
40.65
247.66
55.65
187.03
10.03
105.04
43.92
31.37
13.22
523.17
742.01
11.91

Order Code
6439-257

Each
6530.27

Order Code
5846-48
6024-20
6439-34
6448-68
6471-49
7299-34
7506-27
8044-55
8075-14
8081-30
8082-04
8116-10
8124-10
8648-19
12681-110
13530-10
13649-09
14120-18

Each
38.41
129.75
3583.92
989.82
38.51
367.99
40.65
247.66
57.59
187.03
10.03
105.04
43.92
31.37
13.22
523.17
742.01
11.91

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Bench Reactor Accessories

40

6423 FLASK Pressure Reaction, Unjacketed


Heavy wall unjacketed reaction flask, part of the two-piece pressure reactor, for use at
elevated pressures*. Schott-Duran type top flange supplied with oring groove for use
with heads 6433, 6527, 6528 or 6529. Supplied with CAPFE oring (silicone optional).
For heating mantle, see 12058. Uses 6517 quick release clamp.

Capacity,
mL
500
500
1000
2000
3000
5000

6423

O.D.,
mm
70
110
110
140
165
165

I.D.,
mm
60
100
100
130
155
155

Height,
mm (A)
210
100
180
230
210
310

Flange Size,
mm (In.)
60 (2.4)
100 (4)
100 (4)
100 (4)
150 (6)
150 (6)

Top
ORing
7855-878
7855-880
7855-880
7855-880
7855-881
7855-881

Order
Code
6423-05
6423-07
6423-10
6423-20
6423-30
6423-35

Each
170.98
218.67
242.49
497.34
745.21
847.86

6425 FLASK Pressure Reaction, Unjacketed, with Bottom Outlet


Heavy wall reaction flask with threaded bottom outlet, part of the two-piece pressure
reactor, for use at elevated pressures*. Schott-Duran type top flange supplied with oring
groove for use with heads 6433, 6527, 6528 or 6529. Supplied with CAPFE oring (silicone
optional). For heating mantle, see 12058. Bottom outlet tube has 28/15 oring ball joint
connection with size 116 FETFE o-rings. Uses 6517 quick release clamp.

Capacity,
mL
500
500
1000
2000
3000
5000

6425

O.D.,
mm
70
110
110
140
165
165

I.D.,
mm
60
100
100
130
155
155

Height,
mm (A)
210
100
180
230
210
310

Flange Size,
mm (In.)
60 (2.4)
100 (4)
100 (4)
100 (4)
150 (6)
150 (6)

Bottom
Outlet, mm
0-8
0-8
0-8
0-8
0-10
0-10

Top
ORing
7855-878
7855-880
7855-880
7855-880
7855-881
7855-881

Order
Code
6425-04
6425-06
6425-12
6425-15
6425-19
6425-23

Each
300.71
354.34
376.20
651.79
890.27
990.44

6427 FLASK Pressure Reaction, J acketed


Heavy wall reaction flask with jacket, part of the two-piece pressure reactor, for use at
elevated pressures*. Schott-Duran type top flange supplied with oring groove for use
with heads 6433, 6527, 6528 or 6529. Supplied with CAPFE oring (silicone optional).
Cooling/heating jacket is heat sealed. Inlet/outlet on jacket has size 28/15 oring ball
joints with size 116 FETFE o-rings. Uses 6517 quick release clamp.

6427

Capacity,
mL
500
500
1000
2000
3000
5000

O.D.,
mm
110
130
150
180
215
215

I.D.,
mm
60
96
96
126
151
151

Height,
mm (A)
210
100
180
230
210
310

Flange Size,
mm (In.)
60 (2.4)
100 (4)
100 (4)
100 (4)
150 (6)
150 (6)

Top
ORing
7855-878
7855-880
7855-880
7855-880
7855-881
7855-881

Order
Code
6427-09
6427-13
6427-16
6427-18
6427-23
6427-26

Each
797.82
783.11
801.21
1250.49
3435.42
3539.72

6429 FLASK Pressure Reaction, Jacketed, with Bottom Outlet


Heavy wall reaction flask with jacket and threaded bottom outlet, part of the two-piece
pressure reactor, for use at elevated pressures. Schott-Duran type top flange supplied
with a shallow oring groove for use with heads 6433, 6527, 6528 or 6529. Supplied
with CAPFE oring (silicone optional). Cooling/heating jacket is heat sealed. Inlet/outlet
on jacket and bottom valve have size 28/15 oring ball joint connections with size 116
FETFE o-rings. Uses 6517 quick release clamp.

6429

Capacity,
mL
500
500
1000
2000
3000
5000

O.D.,
mm
110
130
150
180
215
214

I.D.,
mm
60
96
96
126
151
151

Height,
mm (A)
210
100
180
230
210
310

Flange Size,
mm (In.)
60 (2.4)
100 (4)
100 (4)
100 (4)
150 (6)
150 (6)

Bottom
Outlet, mm
0-8
0-8
0-8
0-8
0-10
0-10

Top
ORing
7855-878
7855-880
7855-880
7855-880
7855-881
7855-881

Order
Code
6429-09
6429-14
6429-20
6429-24
6429-28
6429-33

Each
877.65
953.89
963.17
1425.01
3568.78
3765.86

*One-piece systems have maximum pressure limit of 45 psig @ 100C;


Two-piece systems have maximum pressure limit of 35 psig @ 100C.

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Subject to Ace Discount (Page 4)

Net

Bench Reactor Accessories

41

6518 FLASK Reaction, Cylindrical, with ZDS Valve


Cylindrical, heavy wall flask with round bottom. Flask has Schott-Duran top type flange
supplied with oring groove for use with heads 6433, 6527, 6528 or 6529. Comes with
one CAPFE oring (silicone optional). Bottom outlet is ZDS (Zero Dead Space) PTFE
valve with Chemraz o-rings. Uses 6517 quick release clamp.
Capacity,
mL
1000
2000
2000
3000
3000
4000

O.D.,
mm
110
110
155
110
150
155

I.D.,
mm
100
100
145
100
140
145

Height,
mm (A)
180
265
200
400
250
300

Flange Size.
mm (in.)
100 (4)
100 (4)
150 (6)
100 (4)
150 (6)
150 (6)

Bottom
Outlet, mm
0-10
0-10
0-20
0-10
0-20
0-20

Top
ORing
7855-880
7855-880
7855-881
7855-880
7855-881
7855-881

Order
Code
6518-10
6518-12
6518-14
6518-16
6518-18
6518-20

Each
538.44
622.60
627.86
644.69
651.37
758.94

6518

6436 FLASK Pressure Reaction, Unjacketed


Heavy wall unjacketed reaction flask, part of the one-piece pressure reactor system, for
use at elevated pressures*. With vertical AceThred necks for positive connection of
stirrer, funnel, thermowell, condenser, etc.
Capacity,
mL
500
1000
2000
3000
5000

O.D.,
mm
110
110
140
165
165

I.D.,
mm
96
96
126
151
151

Height,
mm (A)
100
180
180
195
310

Center
Neck
#25
#25
#25
#25
#25

Side Necks
(1) #7; (3) #15
(1) #7; (3) #15
(1) #7; (3) #15
(1) #7; (4) #15
(1) #7; (4) #15

Order
Code
6436-06
6436-09
6436-22
6436-31
6436-37

Each
458.51
495.44
555.89
598.78
647.28

6436

500mL and 1000mL sizes have necks angled at 5.

6433 HEAD For Pressure or Filter Reactors, AceThreds


Reactor head, only, with Schott-Duran style flange and AceThreds for use with 6384,
6386, 6388, or 6518 reactor bodies. Also fits 6423, 6425, 6427, and 6429 flasks. Pressure
rating is 35 psi. 6433-23 (only) has angled side joints. Uses 6517 quick release clamp.
For Flask
Cap., mL
150-600
1000-2000
3000-6000

Flange I.D.,
mm (in.)
60 (2.4)
100 (4)
150 (6)

Center
Neck
#15
#15
#15

Side Necks
(2)#15-(1)#7
(3)#15-(1)#7
(4)#15-(1)#7

Order Code
6433-23
6433-35
6433-44

6433-23

Each
295.48
396.77
544.04

6433-35
*One-piece systems have maximum pressure limit of 45 psig @ 100C;
Two-piece systems have maximum pressure limit of 35 psig @ 100C.

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

42

Bench Reactor Accessories

6527-26

6527/6528/6529 HEAD For Filter Reactors,  Joints


Reactor head, only, with Schott-Duran style flange and joints for use with 6384, 6386
or 6388 reactor bodies. 6527-26 has three 24/40 joints (two side joints are angled);
6528-31 and 6529-32 have four 24/40 joints.
For Flask
Cap., mL
150-600
1000-2000
3000-6000

Flange I.D., mm (in.)


60 (2.4)
100 (4)
150 (6)

# of 24/40
Joints
3
4
4

Order Code
6527-26
6528-31
6529-32

Each
278.81
281.42
387.69

6528-31/6529-32

6471 THERMOWELL
For use with two-piece pressure reactors in #15 AceThred. Well has a shoulder that rides
against bottom of bushing to prevent blowout. oring groove makes thermowell suitable
for full vacuum as well as pressure use. Inner diameter of well at top is approximately
5mm. Order thermowell and bushing separately.

6471

8648-19

For Reactor
Cap., mL
Length, mm
500
205
500
170
1000-2000
220
3000
235
5000
360
500
115
1000-2000
180
3000
210
5000
290
Bushing with FETFE oring, only

Order Code
6471-04
6471-10
6471-14
6471-22
6471-24
6471-41
6471-43
6471-47
6471-49
8648-19

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Each
36.76
36.76
37.64
38.07
38.51
36.76
36.76
37.64
38.51
31.37

Subject to Ace Discount (Page 4)

Net

Bench Reactor Accessories

43

6437 FLASK Pressure Reaction, with Bottom Outlet


Heavy wall reaction flask with threaded bottom outlet valve, part of the one-piece pressure
reactor, for use at elevated pressures*. With vertical AceThred necks for positive connection
of stirrer, funnel, thermowell, condenser, etc. Bottom outlet is a 28/15 oring ball joint (with
size 116 FETFE o-rings, 7855-726) and a threaded valve for retrieving contents of flask.
Capacity, O.D.,
mL
mm
500
110
1000
110
2000
140
3000
165
5000
165

I.D.,
mm
96
96
126
151
151

Height,
mm (A)
100
180
180
185
310

Bottom
Outlet, mm
0-8
0-8
0-8
0-10
0-10

Center
Neck
#25
#25
#25
#25
#25

Side Necks
(1) #7; (3) #15
(1) #7; (3) #15
(1) #7; (3) #15
(1) #7; (4) #15
(1) #7; (4) #15

Order
Code
6437-07
6437-13
6437-16
6437-20
6437-24

Each
589.48
615.91
700.32
760.35
843.32

6437

500mL and 1000mL sizes have necks angled at 5.

6438 FLASK Pressure Reaction, J acketed

6438

Heavy wall reaction flask with jacket, part of the one-piece pressure reactor, for use at
elevated pressures*. With vertical AceThred necks for positive connection of stirrer,
funnel, thermowell, condenser, etc. Cooling/heating jacket is heat sealed. Inlet/outlet on
jacket has easy connect/disconnect size 28/15 oring ball joints with size 116 FETFE
o-rings, 7855-726.
Capacity, O.D.,
mL
mm
500
140
1000
150
2000
180
3000
215
5000
215

I.D.,
mm
96
96
126
151
151

Height,
mm (A)
108
195
195
205
325

Center
Neck
#25
#25
#25
#25
#25

Side Necks
(1) #7; (3) #15
(1) #7; (3) #15
(1) #7; (3) #15
(1) #7; (4) #15
(1) #7; (4) #15

Order
Code
6438-14
6438-17
6438-19
6438-24
6438-29

Each
1106.92
1152.67
1259.39
3090.02
3266.12

500mL and 1000mL sizes have necks angled at 5.

6439 FLASK Pressure Reaction, Jacketed, with Bottom Outlet


Heavy wall reaction flask with jacket, part of the one-piece pressure reactor, for use at
elevated pressures*. With vertical AceThred necks for positive connection of stirrer,
funnel, thermowell, condenser, etc. Cooling/heating jacket is heat sealed. Inlet/outlet
on jacket has easy connect/disconnect size 28/15 oring ball joints. Bottom outlet is a
28/15 oring ball joint (with size 116 FETFE o-rings, 7855-726) and a threaded valve for
retrieving contents of flask.
Capacity, O.D.,
mL
mm
500
130
1000
150
2000
180
3000
215
5000
215

I.D.,
mm
96
96
126
151
151

Height,
mm (A)
108
195
195
205
325

Center
Neck
#25
#25
#25
#25
#25

Side Necks
(1) #7; (3) #15
(1) #7; (3) #15
(1) #7; (3) #15
(1) #7; (4) #15
(1) #7; (4) #15

Bottom
Outlet, mm
0-8
0-8
0-8
0-10
0-10

Order
Code
6439-15
6439-21
6439-25
6439-29
6439-34

Each
1198.32
1251.81
1375.16
3243.02
3583.92

6439

500mL and 1000mL sizes have necks angled at 5.

*One-piece systems have maximum pressure limit of 45 psig @ 100C;


Two-piece systems have maximum pressure limit of 35 psig @ 100C.

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

44

Bench Reactor Accessories


7701 MOISTURE TEST RECEIVERPressure
Used to determine heavier-than-water, co-distilling solvent component content of reaction
mixture. For use with ACE pressure reactors with #15 AceThred. Side arm is connected to
#15 AceThred on pressure reactor head with 7506 bushing and size 110 FETFE oring,
7855-716. The 6024-20 pressure condenser, with #15 top plug, is attached to #15 thread
at top of receiver with bushing and oring. Receiver capacity is 60mL, graduated in 1mL
subdivisions. Bottom outlet stopcock is a 0-3mm with FETFE orings. Pressure rating,
45 psig @100C. Complete consists of receiver and bushing with oring. Condenser and
#15 Plug NOT supplied order separately.

7701-20

Receiver, only, 60 mL, #15


Bushing, Nylon, #15, w/FETFE oring (2)
Complete

Order Code
7701-04
7506-06
7701-20

Each
585.23
12.35
609.93

7506 BUSHING Nylon or PTFE


B

Used with oring and AceThred to make a compression seal between thread and glass
like 6024 condenser or 7299 funnel. Supplied with one 7855-716 size 110 FETFE oring.

7506
AceThred
Size
15

NYLON
I.D.
(B), mm Order Code Each
14
7506-06
12.35

PTFE
Order Code Each
7506-27
40.65

5844 ADAPTER Swagelok, PTFE


PTFE adapter with male AceThred to NPT female for connecting pressure gauge,
pressure relief valve or connection from pressure tank to AceThred on head of pressure
reactor Supplied with one FETFE oring (see size and Order Code below) except -176.

5844

AceThred Size
7
15
15
25 (w/o oring)

NPT Thread O-Ring Size/


Size (In.)
Order Code
1/8
009/7855-707
1/8
110/7855-716
1/4
110/7855-716
1/4

Order Code
5844-58
5844-62
5844-74
5844-176

Each
40.02
67.75
67.75
88.93

5846 PLUG Nylon or PTFE


Solid plug for sealing top of 6024 condenser or AceThreds on 6433 head. Supplied with
one FETFE oring (see size and Order Code below).

5846

AceThred
Size
7
15
25

NYLON
O-Ring Size/
Order Code
Order Code
009/7855-707
5846-04
110/7855-716
5846-12
212/7855-734
5846-16

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

PTFE
Each
9.21
21.56
36.14

Order Code Each


5846-44
22.15
5846-48
38.41
5846-50
59.54

Subject to Ace Discount (Page 4)

Net

Bench Reactor Accessories

45

12681 TUBINGPolypropylene
Polypropylene tubing used to make connection between pressure source and 12517
quick disconnect on side of pressure manifold and between other side of manifold the
pressure reactor.
Size (Inches)
1/4 O.D. x 0.170 I.D.
1/4 O.D. x 0.170 I.D.
3/8 O.D. x 75mm length

Order Code
12681-10
12861-110
12861-812

Quanity
100-foot box
10-foot length
Pkg. of 12 lengths

12681

Each
45.20
13.22
28.38

8767 VALVE Pressure Relief, Adjustable


The primary protection to personnel and equipment involved with static and dynamic
pressurized systems. This one-piece pressure relief valve is adjustable from 3 to 50
psig (for use with ACE pressure reactors) by simply adjusting set screws to desired
cracking pressure. When pressure exceeds set cracking pressure, valve bleeds; when
safe lower pressure is realized, valve will reseal. Fabricated from 316 stainless steel
with a Viton oring. Ends are 1/4-inch MPT for connecting to AceThred with a 5844
adapter. Combining this valve with the 6445 rupture disc in the same pressure manifold
offers fail-safe protection against runaway pressure situations.
Order Code
8767-20

8767

Each
86.02

6444 SPARGER TUBE for Pressure Reactor, PTFE


Sparger tube for use in #15 AceThred with either one- or two-piece reactors. Consists
of a closed bottom, 1/2-inch O.D. tube with a 1/8-inch I.D. bore. Bottom of tube has two
3/64inch holes, 90 apart; top has a 5/16-inch male thread for connecting to bottom
of #15 adapter. Adapter has a female thread in handle for tubing connection. Simply
thread tube into bottom of #15 adapter. Thread into #15 AceThred on reactor. Attach
appropriate size tubing to top of adapter. Adapter and tube are fabricated from PTFE.
oring on adapter is FETFE. For replacement FETFE orings, order 7855-716. Order tube
and adapter separately.
TUBE ONLY
Tube Length,
mm (in.)
Order Code
140 (5.5)
6444-04
190 (7.5)
6444-09
343 (13.5)
6444-16

Each
156.95
156.95
156.95

ADAPTER ONLY
Thread Size,
Top of Adapter Order Code
1/4-in.-28 UNF
6444-30
1/4-in. NPT
6444-38

6444

Each
56.19
56.19

6445 RUPTURE DISC Pressure, Graphite

Installation
Direction

For use in 6448 pressure manifold, these rupture discs provide extra protection to
personnel and equipment involved with static and dynamic pressurized systems. In
the event of an overpressure one that cannot be handled by the 8767-20 pressure
relief valve this disc will rupture at a predetermined burst rating; 55 psig (3 psig)
for two-piece units, 65 psig (3 psig) for one-piece units. Manufactured from a single
piece of a high-purity carbon, these discs have a PTFE coating on underside, are
tamper-proof, have no springs or moving parts and mount directly in a #25 AceThred.
Simply place the FETFE oring (7855-734) supplied with disc, on the underside to make
the seal, drop into the #25 AceThred and hold in place using a 5844-176 adapter.
Disc Burst Pressure
55 psig
65 psig

Use With
TWO-PIECE Reactor
ONE-PIECE Reactor

Order Code
6445-12
6445-41

Each
133.39
133.39

Disc

6445

ORing

Flow
Direction

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Bench Reactor Accessories

46

13385-44

5844-74

5844-62
12517-14

6448 MANIFOLD Pressure, Epoxy Coated

8767-20

5844-176

5844-74

5844-74

6448-24

Complete glass manifold, fitted with a pressure gauge, primary


adjustable pressure relief valve, and secondary rupture disc to allow
for safer operation of pressure and filter reactors.
13385 Pressure Gauge is a 0-60 psi stainless steel internal, with
1-1/2inch face and 1/8-inch npt male connection for use with
5844-74 adapter in #15 AceThred.
8767 Pressure Relief Valve is adjustable from 3-50 psig by adjusting
set screws to desired cracking pressure. Ends are 1/4-inch npt for
connecting to #15 AceThred on manifold with 5844-74 adapter.

6445-12

To 5844-58 #7 AceThred and 12517-08, -40

6445 Rupture Disc is a secondary safety device that, in the event of an overpressure (one that cannot be handled by the 8767
relief valve) will rupture at a predetermined burst rating; 55 psig (3 psig) for -12 version, 65 psig (3 psig) for -41 version. Disc is
manufactured from high-purity carbon with a PTFE coating on the underside. No springs or moving parts, disc is secured directly
in #25 AceThred of manifold with 5844176 adapter.
Manifold is connected to #7 AceThred on 6433 head using 584458 adapter and 12517 tubing connectors with 1/4inch tubing.
For Two-Piece
Pressure Reactors (55
psig) and Filter Reactors
Adapter, PTFE, #71/8-inch NPT
Adapter, PTFE, #151/8-inch NPT
Adapter, PTFE, #151/4-inch NPT (3)
Adapter, PTFE, #251/4-inch NPT, w/o oring
Rupture Disc, Graphite, 55 psig
Rupture Disc, Graphite, 65 psig (for pressure version only)
Manifold, Glass, (4) #15, (1) #25, Epoxy Coated
Valve, Pressure Relief, 1/4-inch NPT, 350 psig
Coupling Body, 1/8-inch MPT
Coupling Body, 1/4-inch MPT
Coupling Insert, for 1/4-inch O.D. tubing (2)
Tubing, PP, 1/4-inch O.D. x .170-inch I.D., 10 feet
Gauge, Pressure, 060 psi, 1/8-inch MPT
Complete
Replacement o-rings
Size 110 for #15 adapters (shelf-pack of 12)
Size 212 for #25 adapters (shelf-pack of 6)

Order Code
5844-58
5844-62
5844-74
5844-176
6445-12

Each
40.02
67.75
67.75
88.93
133.39

6448-24
8767-20
12517-08
12517-14
12517-40
12681-110
13385-44
6448-54*
7855-716
7855-734

For One-Piece
Pressure R
eactors
(65 psig)
Order Code
5844-58
5844-62
5844-74
5844-176

Each
40.02
67.75
67.75
88.93

197.03
86.02
11.42
12.07
12.25
13.22
171.92
989.82

6445-41
6448-24
8767-20
12517-08
12517-14
12517-40
12681-110
13385-44
6448-68**

133.39
197.03
86.02
11.42
12.07
12.25
13.22
171.92
989.82

19.78
20.14

7855-716
7855-734

19.78
20.14

*6448-54 is for use with two-piece pressure and filter style reactors.
**6448-68 is for use with one-piece pressure reactors only.

Tubing
Connection
Coupling
Insert

Coupling
Body

12517 TUBING CONNECTOR Quick Connect/Disconnect


12517

Two-piece tubing connector, used to connect tubing from a pressure source to the
manifold of the ACE pressure reactor. Offers the convenience of a quick connect/
disconnect coupling. Body has MPT thread for connecting to a 5844 adapter at end of
ACE pressure manifold. Coupling insert is connected to tubing from pressure source.
Push coupling insert into coupling body for leak-tight connection; press thumb latch
to quick disconnect. Fabricated of polypropylene. Order body and insert separately.
Coupling Body, 1/8-inch MPT
Coupling Body, 1/4-inch MPT
Coupling Insert, for 1/4-inch OD x 0.170 ID Tubing

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Order Code
12517-08
12517-14
12517-40

Each
11.42
12.07
12.25

Subject to Ace Discount (Page 4)

Net

Bench Reactor Accessories

47

13270 SAFETY SHIELD Self Supporting


Weighted, all-transparent safety shield for laboratory worker protection. Polycarbonate
shield is 4.7mm (3/16-inch) thick. Three-sided construction provides stability and
protects personnel from front and sides. Heavy steel perimeter base is 25mm x 48mm
(1-inch x 1-1/2-inch), coated with green epoxy. Outside width is 50cm (19-1/2-inch),
17cm (61/2-inch) front to back.
Height, cm
76
91

Weight, Kg
8.4 (18.5 lbs)
8.9 (19.6 lbs)

Order Code
13270-07
13270-10

13270

Each
430.20
476.70

9655 REACTION FLASKInstatherm Heated, Schott-Duran Flange


Rugged cylindrical reaction flask with Schott-Duran, flat, ground 4-inch flange with
oring groove for use with 6517-25 quick release clamp and integral heating element
that eliminates the local superheating commonly associated with more conventional
heating methods and eliminates cumbersome oil baths. The heating response is rapid
and accurate. Supplied with silicone coating for insulation and protection. O-Ring
(supplied with flask) is CAPFE (PTFE encapsulated silicone). Flask is coated to within
approximately 38mm of the flange for 250C operation. Interchangeable with ACE
4-inch reactor heads with Schott-Duran flange. Three-pronged plug for insertion into
ACE temperature controllers. Integral six-foot controller cord.
Capacity, O.D.,
Liters
mm
1
110
2
110

I.D.,
mm
100
100

Height,
mm (A)
180
200

Volt/Amp
Rating
40/8
120/5

Watts
400
600

Order
Code
9655-17
9655-22

Each
766.76
869.89

9655

9656 REACTION FLASKInstatherm Heated, Conical, 4-Inch Flange


Same flask as listed under 6476, except with Instatherm coating. Has flat-ground, 4-inch
conical flange. This integral heating element eliminates the local super-heating commonly
associated with more conventional heating methods. Eliminates cumbersome and
dangerous oil baths. The heating response is rapid and accurate. Supplied with 969820 cord for connection to variable voltage or termperature controller. Flask is coated
to within 38mm of the flange for 200C operation, 360C maximum on special order.
Interchangeable with ACE 4-inch reactor heads with Schott-Duran flange. For controllers,
see ACE or J-Kem temperature controllers with voltage limiting output, such as 12125,
12324. Use 6496 clamp for securing head to flask.
Capacity, O.D.,
Liters
mm
1
110
2
114

I.D.,
mm
100
104

Height,
mm (A)
180
260

Volt/Amp
Rating
40/8
120/5

Watts
400
500

Order
Code
9656-08
9656-12

Each
758.58
864.03

9656

6526 FLASK Reaction, Cylindrical, Indented Style


Rugged cylindrical reaction flask with Schott-Duran flat flange with oring groove, for
use with 6517 quick release clamp but with indents for greater agitation. Each flask
is supplied with one CAPFE oring (PTFE encapsulated silicone oring). Plain silicone
orings are also available. For reaction heads, see 6528. For cooling/heating coils, see
12067. NOT suitable for vacuum or pressure operation. Uses 6517 quick release clamp.
Capacity, O.D.,
Liters
mm
1
110
2
110

I.D.,
mm
100
100

Height,
mm (A)
180
265

Flange Size.
mm (in.)
100 (4)
100 (4)

Top
ORing
7855-880
7855-880

Order
Code
6526-10
6526-12

Each
200.17
223.10

6526

ted

Inden

New

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

48

Bench Reactor Accessories

8044-24

8044 BEARING Pressure, with AceThreds, 1 0mm


Glass bearing with #15 AceThred at each end and glass tubing between for use
with 10mm O.D. 8075 stirring shafts. PTFE coupling, with internal FETFE oring seal,
connects bottom of bearing to either #15 or #25 AceThred on vessels such as 6433
pressure reactor head or one-piece pressure reactors. Top bushing also has an internal
oring seal for additional seal on shaft to allow pressure reactions. Maximum operating
speed 600rpm. Coupling and bushing supplied with orings. For replacement orings
(the bearings take two o-rings, one internal and one external): for #15#15 coupling,
7855730 external, 7855-716 internal; for #15#25 coupling, 7855-730 and 7855-742
external, 7855-716 internal; for #15 bushing, 7855-730 external, 7855-716 internal.

8044-55

For Coupling to #15 AceThred


Order
Code
Each
Glass Bearing, only, #15-#15 8044-07 39.14
Coupling, PTFE, #15-#15
5840-60 113.73
Bushing, PTFE, #15
8044-13 80.21
Complete
8044-24 233.08

5848 FILTER DISC

5848

Filter disc for use with 5837 and 5838 adapters. Available in polyethylene (100 micron
pore size), and borosilicate glass Porosity A (145-174 microns), B (70-100 microns),
C (25-50 microns) and D (10-20 microns). Sold in packages. (Caution: These discs are
intended to be removable. However, because of the tight fit, the glass disc may break
when being removed.)
Polyethylene
100 microns

For
Adapter Pkg.
Size,mm Qty.
11
6
15
6
25
6
50
6
80
1

For Coupling to #25 AceThred


Order
Code
Each
Glass Bearing, only, #15-#15 8044-07 39.14
Coupling, PTFE, #15-#25
5843-62 128.31
Bushing, PTFE, #15
8044-13 80.21
Complete
8044-55 247.66

Order
Code
5848-07
5848-10
5848-14
5848-17
5848-19

Per.
Pkg.
14.44
14.44
16.58
34.99
9.03

Borosilicate Glass
Porosity B
Porosity C
70-100 microns
25-50 microns

Porosity A
145-174 microns
Order
Code
5848-43
5848-44
5848-47
5848-49
5848-100

Per
Pkg.
58.53
58.53
66.12
130.80
126.50

Order
Code
5848-52
5848-54
5848-56
5848-58
5848-120

Per
Pkg.
58.53
58.53
66.12
130.80
129.55

Order
Code
5848-21
5848-23
5848-25
5848-28
5848-122

Per
Pkg.
58.53
58.53
66.12
130.80
147.23

Porosity D
10-20 microns
Order
Code
5848-31
5848-33
5848-35
5848-38
5848-124

Per
Pkg.
58.53
58.53
66.12
130.80
161.95

5021 ADAPTER Bushing, Thermometer


For thermometers having a 10/30 joint.

5021

Inner
10/30
10/30
10/30

Outer
14/35
24/40
29/42

Order Code
5021-05
5021-09
5021-12

Each
36.10
41.53
45.16

5028 ADAPTER Thermometer, Mini #7 AceThred


With ground joint at bottom and threaded bushing at top which tightens into #7 AceThred
to form an oring compression seal with thermometers, bleed tubes, etc. Nylon bushing
comes complete with FETFE oring. 10/18 size will accommodate thermometers up
to 6.5mm diameter, all others will accommodate 7mm diameters. Suitable for vacuum
work. Supplied complete with 5029-10 nylon bushing. For extra orings, see 7855-704.

5028

Joint
10/18
14/20
19/22
24/40

Order Code
5028-24
5028-26
5028-28
5028-30

Each
27.51
27.55
27.38
27.61

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Joint
24/20
29/42
18/9
35/25

Order Code
5028-30
5028-32
5028-38
5028-42

Each
27.61
32.61
33.42
35.95

Subject to Ace Discount (Page 4)

Net

Bench Reactor Accessories

49

5269 ADAPTER Offset, with AceThred


Offset adapter with #15 AceThred offset to a 14mm OD tube with oring groove. For use
with ACE pressure reactors to locate condenser, etc., away from stirrer. NOT supplied
with bushing or oring. Order 7506-06 for bushing and FETFE oring.
Order Code
5269-12

Each
39.20

5269

6024/6029 CONDENSERWest

6029

West style condenser for use with 6433 threaded or 6527, 6528 or 6529 jointed heads.
6024-20 supplied with #15 AceThred at top for 5846 plug (not supplied) and drip stem
with groove, and long enough to be secured in #15 AceThred with 7506-06 bushing
and FETFE oring (not supplied) to restrict blowout. With #7 AceThred on inlet/outlet
for use with Ace-Safe 5853 tubing connectors. Supplied with bushing and connectors
for 1/4inch I.D. tubing.
6029-13 supplied with 24/40 joint at top and bottom and D size (see page 5 for sizing)
barbed hose connection on inlet/outlet for inch I.D. tubing.
Use with Head No.
6433
6527,6528,6529

Jacket Length, mm
200
250

Order Code
6024-20
6029-13

Each
129.75
105.87

6024

7234 FUNNEL Powder Dispensing


Side operated screw feed funnel for addition of powders and solids, up to 25 mesh, to
reactions without problems of seizing or binding.
Features a flexible PTFE screw thread wrapped on a precision PTFE-ceramic shaft and
contained within a precision bore housing. This offers a unique flexibility in that the thread
can move aside temporarily; as one spacing increases, the adjacent spacing decreases,
thereby maintaining an average feed rate.
Completely inert materials allow flushing with solvents without fear of contamination.
#15 AceThred offers easy disassembly for cleaning. Large 1inch knob makes turning
T24/40. S
T14/20 outer joint atop
smooth and easy. Top outer and bottom inner joints are S
inner joint is for easier flushing.
Capacity, mL
100
250

Order Code
7234-25
7234-35

Each
331.84
358.50

7234

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

50

Bench Reactor Accessories


7298/7299 FUNNEL Addition, Pressure Equalizing
Funnel for use with 6433 threaded or 6527, 6528 or 6529 jointed heads.
7298

7298 (use with 6527,6528, or 6529 head) supplied 24/40 joint at top and bottom, with
threaded PTFE stopcock shutoff.
7299 (use with 6433 head) supplied with #15 AceThred at top for 5846 plug (not
supplied) and drip stem with groove and long enough to be secured in a #15 AceThred
with 7506-06 bushing and FETFE oring (not supplied) to restrict blowout. With threaded
PTFE stopcock shutoff.
Replacement Plugs

7299

Cap.,
mL
60
125
250
500
1000

Stopcock
Orifice,
mm
0-3
0-3
0-3
0-3
0-5

Order
Code

7298-05
7298-10
7298-15
7298-24

Each
231.90
249.35
278.92
326.09

Order
Code
7299-06
7299-12
7299-25
7299-34

Each
305.29
313.29
336.29
367.99

Order
For 7298
Code
0-3 mm 8192-261
0-5 mm 8192-263

Each
37.87
52.16

For 7299
0-3 mm 8189-43

38.16

7233 FUNNEL Powder Dispensing, Vertical


A vertical, compact, screw feed funnel for addition of powders and solids, up to 25
mesh, into reactions without seizing or binding. Features a flexible PTFE screw thread
wrapped on a precision PTFE-ceramic shaft and contained within a precision bore
housing. This offers a unique flexibility in that the thread can move aside temporarily;
as one spacing increases, the adjacent spacing decreases, thereby maintaining an
average feed rate. Completely inert materials allow flushing with solvents without fear
of contamination. #15 AceThred at top offers easy disassembly for cleaning. Large
T14/20 outer joint,
1inch knob makes turning smooth and easy. Top side port is S
T24/40. Overall height, 9 inches.
bottom inner joint is S

7233

Capacity, mL
50
100

Order Code
7233-20
7233-30

Each
250.88
282.08

9485 FUNNEL Powder Dispensing


A vertical, compact, screw feed funnel for addition of powders and solids, up to 25 mesh,
into reactions without seizing or binding. Features a flexible PTFE screw thread wrapped
on a precision PTFE-ceramic shaft and contained within a precision bore housing. This
offers a unique flexibility in that the thread can move aside temporarily; as one spacing
increases, the adjacent spacing decreases, thereby maintaining an average feed rate.
Completely inert materials allow flushing with solvents without fear of contamination. #7
T14/20.
AceThred offers easy disassembly for cleaning. Top outer and bottom inner joints are S
Approximate capacity, 15mL.

9485

Order Code
9485-15

Each
238.41

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Subject to Ace Discount (Page 4)

Net

Bench Reactor Accessories

51

6517 CLAMP Quick Release


Stainless steel quick release clamp for use with two-piece pressure reaction flasks
and heads with Schott-Duran flanges. Available with or without extension rod for
clamping to support frame. Note: Welded extension rod is 5/8inch O.D. x 12 inches
long for stabilizing reactor only. Reactors should be supported from below in usual
manner, namely cork rings, mantle, etc.
WITHOUT EXTENSION
For Flange
Size, mm (in.)
60 (2.5)
100 (4)
150 (6)

Order Code
6517-22
6517-25
6517-27

WITH EXTENSION
Order Code

6517-54
6517-56

Each
87.08
98.23
117.67

6517-22, -25, -27

Each
158.10
172.33

6517-54, -56

7669 CLAMP Pinch Type, Stainless Steel


Spherical joint clamps made of stainless steel. With strong spring-closed, forked jaws.
Size
No.
12

18
28
35

For
Joint
12/5
18/9
12/5
18/9
28/15
35/25

Order
Code
7669-03
7669-05
7669-08
7669-10
7669-12
7669-14

Each
7.79
8.64
14.30
14.33
16.57
18.51

Size
No.
40
50
65
75
100

For
Joint
50/30
65/40
75/50
102/75

Order
Code
7669-16
7669-18
7669-20
7669-22
7669-26

Each
41.45
32.03
35.90
72.92
246.61

7669

13550 SUPPORT STAND/CLAMP HOLDER

Stand: Rugged, with H shaped base for use with filter reaction flasks. Stainless steel
vertical rod available 25mm O.D. x 70cm (27 inches) long; 25mm O.D. x 92cm (36 inches);
or 25mm O.D. x 122cm (48 inches). Base is 17 inches wide x 16 inches deep. Clamp
Holder: For connecting up to 13mm O.D. mounting rod to 25mm O.D. support rod.

Stand, only, 25mm O.D. x 70cm


Stand, only, 25mm O.D. x 92cm
Stand, only, 25mm O.D. x 122cm

Order
Code
13550-21
13550-23
13550-24

Each
305.91 Clamp Holder, only
314.96
314.96

Order
Code
Each
13550-25 139.05

13550

11079 CHAIN CLAMP


Use code -24, for connecting up to 170mm O.D. vessels. Code -38 & -40, for connecting
up to 280mm O.D. vessels. Code -40 has extended 12-inch (305mm) arm.
For Vessel O.D.
Up to 170 mm
Up to 280 mm
Up to 280 mm (with 12-inch extension arm)

Order Code
11079-24
11079-38
11079-40

Each
51.23
75.28
79.46

11080 CLAMP HOLDERRegular


Normally used to hold the Nos. 11065 through 11072 clamps to rods and lab frame
supports. Made of heavily nickel-plated zinc. Will grip rods up to and including 19mm
diameter. Attaches clamp at right angle.
Order Code
11080-19

11079
11080

Each
18.82

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

52

Bench Reactor Accessories

12840 BENCH REACTOR STAND


Ace Glass is pleased to introduce a new bench
reactor stand assembly to accommodate all types
of glass bench filter and pressure reactors. The
stand is compatible with reactors from 1-Liter up to
6-Liters having overhead drive motors, and in both
jacketed and non-jacketed flask versions. The bottom
plate, motor mount and middle flask supports are all
adjustable to fit any small reactor, and the stand will
fit into most laboratory hoods. It comes completely
assembled, but it is very easy to take apart for
cleaning. The open bottom accommodates roundbottom and flat-bottom flasks, and even flasks with
bottom valves. Will accept either IKA or Heidolph
overhead stir motors. All stand components are
either anodized or powder coated aluminum. The
flasks sit on an attached rubber base plate.

New

12840
Dimensions, Inches
43 H x 24 W x 24 D

Order Code
12840-10

Each
2665.13

13586 SUPPORT STAND

13586

All-stainless-steel support stand. Heavy base, six pounds, can accommodate vessels
up to 18 inches in diameter within its U shape. Support rod is 5/8-inch diameter,
approximately 29 or 36 inches high, fastened to base with stainless steel lock nuts. Two
additional threaded holes in base legs to accommodate extra support rods. Complete
item consists of one base and one rod. For extra rods, order 29 inch, 13586-25; 36 inch,
13586-27. Base is 19 inches wide by 11 inches deep.
Rod Height, in
29
36

Order Code
13586-10
13586-13

Each
274.82
313.93

13586-25
13586-27
13586-15

104.64
133.18
181.78

Additional Support Rods:


28
36
60

11086

New

11086 CLAMP HOLDER 13mm Grip, Stainless Steel


Lab frame hook connector allow one-handed assembly of two components with one
adjustment screw.
Order Code
11086-01

Each
27.18

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Subject to Ace Discount (Page 4)

Net

Bench Reactor Accessories

53

11173 PLATE SUPPORT SHELF


Adjustable cast alloy, black epoxy coated support shelf. With knob, measures 7 inches
x 10 inches. Fits up to 5/8-inch O.D. rod. Plain or with 4inch diameter hole and with
1inch rubber around perimeter.
Order Code
11173-08
11173-17

Style/Size
Solid, No Hole
4-inch Hole

Each
111.57
111.28

11173-17

11057 CLAMP Stainless Steel, Three-Prong


Multi-purpose, three-prong clamps manufactured from electropolished stainless steel
for improved corrosion resistance and autoclave sterilization. Features include dual
screw adjustments and vinyl sleeved prongs. See our 11074 product family for vinyl
or fiberglass (high temperature) replacement sleeves. See our 11083 & 11086 product
families for stainless clamp holders.
Size
Small
Medium
Large

Maximum
Grip Size (cm)
4.8
6.9
10.2

Arm Length (in.)


4
5
5

Order Code
11057-01
11057-03
11057-05

11057

Each
70.05
80.51
89.91

11065/11067/11069 CLAMP Versatile, Vinylized Jaws


Three-prong grip clamp. Because both jaws are adjustable, with double screws that
operate independently, large or small objects can be held easily. Comes with an extra
set of fiberglass prong covers for temperatures above 100C.
Clamp
Size
Large
Large
Medium
Small

Overall
Length, cm
27
30
22
17

Will Hold Objects


up to mm diameter
89
89
57
25

Order Code
11065-16
11065-17
11067-14
11069-18

Each
41.82
51.23
39.73
37.64

11066 CLAMP Versatile, Vinylized Jaws


Three-prong grip clamp. Because both jaws are adjustable, with double screws that
operate independently, large or small objects can be held easily. Comes with an extra
set of fiberglass prong covers for temperatures above 100C. Has 12-inch (305mm)
extended arm.
Clamp
Size
Medium
Large

Overall
Length, cm
40.6
45.1

Will Hold Objects


up to mm diameter
69
105

Order Code
11066-10
11066-12

Each
Call
Call

11081 CLAMP HOLDER Pilot Plant


Used with 11065 versatile jaw-type clamp to secure condenser, etc., on 6472 pilot plant
reactor support frame. Holder clamps to 1-inch bar on frame of reactor; 11065 clamp
is held in clamp holder with thumb screw. Fabricated of aluminum, painted black. For
clamps, see 11065.
Order Code
11081-21

11065/67/69

New

11066

11081

Each
84.80

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Bench Reactor ROBO

54

ROBO
INTRODUCING

ROMASZEWSKI OIL BENCH OXIDATION

Reactor and Components for ASTM D7528-09 procedure for


simulation and test of auto engine oils

ll new components and reactor for testing


and simulation of automobile engine oil
aging as per ASTM D7320 sequence
IIIG method.

T h i s p ro c e d u re w a s d e v e l o p e d b y R .
omaszewski, B. Kinker and P. Palmer of
R
Evonik (RohMax) USA.
Before auto engine oils are made available for
the global market for use in auto engines, they
must pass rigorous testing and meet tough
specifications for performance. ASTM and the
International Lubricant Standardization and
Approval Committee, (ILSAC) set the standards
for US and Japanese auto manufacturers. This
revised, updated method is part of D7320 IIIG
engine oil test method. The new revised method
reduces the costs and test times substantially
from the old method.
Ace Glass is pleased to be part of this effort and
this new protocol. Our proprietary Instatherm
coating on the flask body allows for very
precise control of the heating in one complete
vessel. ACE offers all the glass and stainless
steel components, as well as accessories for
the reactor system with the appropriate part
numbers from the ASTM D7528-09 document.
Components:
1000mL Instatherm flask
Dual chamber trap/condenser
Inner condenser (two required)
12mL V bottom tube with side tab
Stainless steel head
Bearing
Squash cap
Stainless steel shaft, 8mm
Stainless steel turbine blade
ACE clamp
PTFE ring seal
Head gasket
Rack assembly
Gas drying tube
Heidolph RZR motor
Stainless steel fittings, tubing
Stainless steel valves
Stainless steel vacuum/pressure gauge
Flow Meter
Complete

Order Code
D120676
D127507
D127590
D120677
RMI-1002-DH
RMI-1004-DH
RMI-1005-DH
RMI-1003-DH
RMI-1001-DH
D124780
RMI-1007-DH
6495-43
11162-08
10165-10
13507-51
6650-10
6650-20
6650-30
6650-40
6650-01

Each
Call
Call
Call
Call
Call
Call
Call
Call
Call
Call
Call
19.53
500.80
106.81
2363.71
Call
Call
Call
Call
Call

New
Accessories:
Stainless steel extension arms for head
(two required, not needed if using D124780
clamp)
Water flow monitor (J-Kem)
Valve for WFM (J-Kem)
Temperature controller with J thermocouple Model 410 (J-Kem)
Vacuum regulator (J-Kem)
Vacuum regulator valve

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

RMI-1006-DH

Call

12168-120
12168-03

354.20
240.00

12324-25

823.40

14061-08
14066-01

1127.00
485.00

Subject to Ace Discount (Page 4)

Net

Bench Reactor PTFE


6390 REACTORPTFE, Filter, Complete

55

New

All PTFE filter reactor. An extension of the famous ACE borosilicate glass filter reactor
product line. The head, head joints, body, stir-bearing, bottom filter assembly with valve,
and stir shaft with agitator are all PTFE. Even the o-rings are PTFE encapsulated. The filter
supports are polypropylene. The bottom filter assembly is either #50 or #80 AceThred
and threads in/out for easy capture of filtrate, or for cleaning. Unit is excellent for fluorine
chemistry work as well as any work using strong alkalis where glass cant be used. Halar
coated stainless steel internal coil can be used for heating or cooling the contents. Three
sizes are available as standard. Other sizes are available on request. Support stand
(13586 or 13550-21) and chain clamp (11079) not included. We recommend Caframo
BDC2010 stirmotor (13566-05). Recommend Julabo circulator (12254-33) for heating/
cooling and Ace/JKem 260T temperature controller (12318-05) with a 12-inch PTFE
coated T temperature sensor (1231825).

6390

250mL Reactor
Order Code
6391-02
12858-15
7855-878
6517-22
5838-83
5839-42
5844-120
5814-348
13443-12

Component
Reactor Body (A = 5.8 in.; O.D. = 3.5 in.)
PTFE Head (60mm, 4 openings, 24/40)
CAPFE o-ring (60mm)
Quick Release Clamp (60mm)
Bottom Filter Assembly (#50)
Bottom Valve (1/4-inch/3/8-inch)
Adapter
Polypropylene Filter Supports (#50) (Pkg. of 12)
Stirrer Bearing (10mm)
PTFE Coated Stainless Steel Shaft
with Agitator (10mm)
Complete

Each
1184.49
193.24
28.10
87.08
232.72
110.20
88.91
35.76
428.93

13852-10

335.81

6390-02

2874.94

500mL Reactor
Order Code
6391-05
12858-15
7855-878
6517-22
5838-83
5839-42
5844-120
5814-348
13443-12

Component
Reactor Body (A = 8.88 in.; O.D. = 3.5 in.)
PTFE Head (60mm, 4 openings, 24/40)
CAPFE o-ring (60mm)
Quick Release Clamp (60mm)
Bottom Filter Assembly (#50)
Bottom Valve (1/4-inch/3/8-inch)
Adapter
Polypropylene Filter Supports (#50) (Pkg. of 12)
Stirrer Bearing (10mm)
PTFE Coated Stainless Steel Shaft
with Agitator (10mm)
Complete

Each
1443.03
193.24
28.10
87.08
232.72
110.20
88.91
35.76
428.93

13852-10

335.81

6390-05

3133.48

1,000mL Reactor
Component
Reactor Body (A = 7.84 in.; O.D. = 4.33 in.)
PTFE Head (100mm, 7 openings, 5x24/40, 2x#7)
CAPFE o-ring (100mm)
Quick Release Clamp (100mm)
Bottom Filter Assembly (#80)
Bottom Valve (1/4-inch/3/8-inch)
Adapter
Polypropylene Filter Supports (#80) (Pkg. of 12)
Stirrer Bearing (10mm)
PTFE Coated Stainless Steel Shaft
with Agitator (10mm)
Halar Coated Heating Coil
Complete

Order Code
6391-10
12860-12
7855-880
6517-25
5857-86
5839-42
5844-120
5814-350
13443-12

Each
1863.92
348.95
28.63
98.23
326.41
110.20
88.91
46.80
428.93

13852-15

335.81

12069-06
6390-10

835.14
4809.74

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

56

Reactors/Large-Scale Pilot Plants

ACE Pilot Plant Reactors


ACE cylindrical and spherical pilot plant reactors have been field tested and improved to
provide a portable, self-contained reaction system for research and production purposes.

Standard Design Specifications:

Complete listing of domed as well as flat head reactor assemblies.


Cylindrical, jacketed, and spherical type flasks.
Various bottom outlet valve versions available.
Stainless steel support frame with reactor support platform/ring, and stirring m
otor
mount.
Three-point adjustable top bracing system that provides greater stability
of flask and head on four-post stands.
Large, locking wheels on support frame for easier movement and greater stability.
Unique design for securing bottom and upper agitators on shaft.
New pinned valve/agitator assemblies for reduced vibration/flexing.
Digital temperature control systems for added safety.
Numerous stirring motor types
Clear safety shields for support frame available, call or email for details.

LIMITATIONS
AND PRECAUTIONS

MAXIMUM ALLOWABLE
TEMPERATURES

The strength of glass is primarily


determined by its surface condition,
thickness, and uniformity. Mechanical
stress applied to glass contributes to
strain, which results in breakage when the
total strain exceeds its allowable limit (i.e.,
tensile strength). Thus, careful handling
and use of glassware are important to
avoid scratching and mechanical shock
to outside and inside surfaces.
Thermal stress may produce the
same result catastrophic breakage.
It is important to avoid rapid or uneven
temperature changes across any glass
wall. This refers to temperature increases
from externally applied heat (mantles)
or internally generated heat (exothermic
reactions), as well as temperature
decreases such as rapidly introducing large
quantities of cold liquids to hot reactants,
etc. Remember: Mechanical and Thermal
Stresses are additive.

The standard reactors have a maximum


operating temperature of 160C. The
maximum allowable temperature difference
(T) across the glass wall for units with
domed head is 80C; 30C for flat head.
Also, these values limit the rate at
which a reactor may heat up or cool
down. ACE recommends continuous
monitoring of internal and external
temperatures to avoid exceeding
allowable temperature differences.
Caution must be used when heating a
reactor vessel with mantles since they
produce local temperatures in excess
of 350C. When using variable voltage
controllers, we suggest 3/4 voltage
(i.e., half power) during warm-up and
gradually increasing voltage until
desired internal temperature is reached,
never exceeding the maximum T.

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

MAXIMUM PRESSURE
Maximum pressure for reactors is 5 psi
with standard taper joints (domed head)
using clips. Flat head NOT recommended
for use with pressure.

MAXIMUM VACUUM
Maximum permissible operating vacuum
for spherical and cylindrical vessels with
50C max. T:
10 liter = Full Vacuum (i.e., 5 mm Hg)

}
}

30 & 50 liter Cylindrical


50mm Hg
50, 72 & 100 liter Spherical
100 & 200 liter Cylindrical
200 liter Spherical

200mm Hg

Flat head NOT recommended


for use under vacuum.

Subject to Ace Discount (Page 4)

Net

Reactors/Large-Scale Pilot Plants

57

A Guide to Ordering Custom Pilot Plants


Its easy to customize one of our standard listings with a Pilot Plant Reactor
design that will meet your specific application needs. Here are some key points
to consider when specifying a Pilot Plant that will work for you:

Overall Height Limit

3- or 4-Post Stand

Door or Hood Clearance

Motor Size & Type


Air-Driven
Electric
Digital
Analog

Accessories

Condensers
Powder Funnel
Liquid Addition Funnel
Sample Ports
Temperature Sensors
Baffles

Coupling

Temperature
Controller
Addition or Sample Port
Needed?

Bearing Type/Size
Head

Flat or Domed; number


of ports, sizes

Flask Type & Size


Spherical
Cylindrical
Jacketed
Unjacketed

Heating/Cooling Coil
Safety Shields

Heating/Cooling Circulator
needed?

Total Capacity
& Reaction
Volume

If so, what capacity?

Heating Girdle/Mantle

Bottom
Heating
Mantle

Jacketed or
Unjacketed
Flask

Agitators
Bottom Valve Type

Bottom
Clearance
Required

Easy Action
Sink Type
ZDS Valve

Piston Type
Beaded
Flush Seal

Number & Type


Pin or no pin

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

58

Reactors/Large-Scale Pilot Plants


Complete 12 & 22 liter
Elevated mantle support
Temperature controlled heating mantle
Bottom outlet
6469 REACTION ASSEMBLY Complete, 12 and 22 Liter
Complete self-supporting pilot plant assembly. Needs only to be located near
electrical outlet. When not in use, entire assembly can be moved, intact, without
breakdown.

Features
Flask with 4 inch (10.2 cm) center opening, Flat-sided powder funnel offers easier
two 45/50 side necks, one #7 AceThred
additions.
thermometer opening and one 28/15 Rugged steel-reinforced PTFE stirring rod
ball joint take-off at bottom.
needs no lubrication. Turns in a precision
Electric stirring motor, Cat. No. 13649-07,
Trubore economy bearing. The PTFE
is self-standing on flask-mounted motor
paddle agitator is removable for cleaning.
mount (air motor also available).
Mantle supports raise the mantle about
With PID Digital readout temperature
91.4 cm (36 inches) to allow easy access
controller and PFA coated J thermo
to bottom of flask.
probe for better temperature control.
Approximate overall height: 12 L and 22L,
Bottom heating mantle
71 inches; Base width: 28 inches
12 Liter
Order Code

6469

Flask with
Sink Valve
or Zero D
ead Spac
e Va
available
upon requ lve
est.

Temperature range:
Ambient +5 to 200C

ACE Reaction Assemblies are


available as listed. If you require a
design change or just a modification,
well fabricate to order.
Email, phone or fax for a quotation.

22 Liter
Each

Order Code

Each

FLASK, Center Neck 10.2cm


Flange, Two 45/50 Side Necks,
One #7 AceThred and One
28/15 Ball Outlet At Bottom
6469-16

763.28

6469-18

1062.02

HEAD, 45/50

6469-26

199.64

6469-26

199.64

GASKET, PTFE

6495-10

11.28

6495-10

11.28

CHUCK, Flex-Grip

8124-10

43.92

8124-15

152.25

ROD, PTFE with Stainless Steel


Core

8071-07

264.62

8079-03

477.57

AGITATOR, PTFE Paddle

8089-08

112.73

8091-10

226.34

MOTOR, only

13649-07

509.07

13649-07

509.07

MOTOR MOUNT

6469-30

487.00

6469-32

487.00

MOTOR CONTROLLER, only

13530-10

523.17

13530-10

523.17

BEARING, Economy, 45/50

8042-121

105.74

8065-64

169.59

6468-13

503.79

CLAMP, Head, Aluminum

6468-13

503.79

ADAPTER, Stopcock, 28/15,


PTFE, 6mm Bore

6469-40

173.03

6469-40

173.03

TEMPERATURE CONTROLLER

12126-24

874.72

12126-24

874.72

SENSOR, PFA Coated, 12 inch


x 1/4 inch

12141-25

118.70

12141-25

118.70

SENSOR LEAD, only, Type J

12141-80

69.68

12141-80

69.68

FUNNEL, Powder, 45/50

6469-52

228.81

6469-52

228.81

STOPPER, 45/50

8250-20

44.68

8250-20

44.68

CLAMP, 28/15

7666-15

40.04

7666-15

40.04

CLAMP Holder, Regular

11080-19

18.82

11080-19

18.82

MANTLE, Heating, with Hole

12044-28

1091.72

12044-30

1207.35

MANTLE, Support

12097-45

467.00

12097-47

492.00

COMPLETE

6469-62

6358.09

6469-67

7248.21

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Subject to Ace Discount (Page 4)

Net

Reactors/Large-Scale Pilot Plants

59

Full range of pilot size flasks


Rugged, steel-reinforced PTFE stirring rod
Heavy duty mechanical lab stirrer
Temperature controlled heating mantle
6470 REACTION ASSEMBLY 12 thru 72 Liter
Complete reaction assembly using standard ACE reaction equipment.
The 12 thru 72 liter flasks have three 65/40 in-line spherical joints
and two 29/42 standard taper joints.

Features
Full range of pilot-size flasks from 12 liter to 72 liter with spherical
and standard taper joints.
Rugged 19mm diameter, steel-reinforced PTFE stirring rod needs no
lubrication. Runs in a precision Trubore bearing. The PTFE paddle is
removable and other interchangeable agitators, available from ACE,
may be substituted.
The 12 liter assembly has a 10 mm diameter, steel-reinforced PTFE
rod as well as a 10 mm bearing, chuck, and paddle.
Highly efficient 6016 condenser is attached directly to 65/40 side joint.
Thermowell depth is completely adjustable via an AceThred adapter.
Unit as supplied has a heavy-duty mechanical lab stirrer; for situations
that call for non-electric motors, ACE can supply a compact air-driven
motor and support. Call or email for a quotation.
Heavy-duty bottom heating mantle.

6470

Approximate overall height: 12 L and 22L 59 inches; 50 L and


72L63 inches.
12 Liter
Order
Code

22 Liter
Each

50 Liter

72 Liter

Order
Code

Each

Order
Code

Each

Order
Code

Each

FLASK, Center and Two Side


65/40, Two 29/42
CONDENSER, Pilot Plant

6470-20
6016-75

892.05
972.51

6470-24
6016-77

1034.76
1048.01

6470-26
6016-79

1673.33
1328.76

6470-28
6016-79

2162.67
1328.76

BEARING, 65/40, WaterCooled

8040-55

217.99

8060-10

299.67

8060-10

299.67

8060-10

299.67

ROD, PTFE with SSteel Core

8071-10

267.94

8079-05

484.69

8079-10

528.19

8079-10

528.19

AGITATOR, PTFE, Single Blade

8088-10

222.39

8092-10

256.36

8092-10

256.36

8092-10

256.36

CHUCK, Flex-Grip
FUNNEL, Pressure Equalizing,
24/40, 1000 mL

8124-10

43.92

8124-15

152.25

8124-15

152.25

8124-15

152.25

7297-37

332.65

7297-37

332.65

7297-37

332.65

7297-37

332.65

STOPPER, 24/40

8250-12

19.79

8250-12

19.79

8250-12

19.79

8250-12

19.79

ADAPTER, 24/40 - 65/40

5025-24

118.29

5025-24

118.29

5025-24

118.29

5025-24

118.29

ADAPTER, Maxi 29/42

5030-42

45.73

5030-42

45.73

5030-42

45.73

5030-42

45.73

ADAPTER, Midi 29/42

5030-24

44.98

5030-24

44.98

5030-24

44.98

5030-24

44.98

THERMOWELL, 10 mm O.D.
6470-42
STIRRER MOTOR & CONTROLLER 13649-19

16.99
1265.18

6470-44
13647-35

16.99
1269.00

6470-46
13647-35

18.53
1269.00

6470-46
13647-35

18.53
1269.00

CLAMPS, 65/40 Union Type (3) 7666-30


HEATING MANTLE, Alum.
Housing
12043-27
MANTLE SUPPORT
12097-08
VOLTAGE CONTROLLER (2)
12087-10
VOLTAGE CONTROLLER (3)

COMPLETE
6470-60

170.88

7666-30

170.88

7666-30

170.88

7666-30

170.88

871.00
139.00
621.30

6841.45

12043-29
12097-10
12087-10

6470-64

984.00
186.00
621.30

7649.40

12043-31
12097-12

12087-10
6470-68

1624.37
201.00

621.30

12043-33
12097-14
12082-10

6470-72

1784.00
233.00
1119.76

11098.18

10041.59

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

60

Reactors/Large-Scale Pilot Plants

6472 Cylindrical Pilot Plants

10 & 20 Liter Reactors

Domed Head

Unjacketed

With Stainless Steel Support

10 & 20 liter flasks with


bottom outlet
Large side
port on head
for material
addition
Internal heat
exchange coil*

6472-284

6472-282

Rugged stainless steel


support frame on casters for
mobility
Adjustable height flask
support
Available with Lexan safety
shields
*Supplied with PTFE-coated copper
tubing; also available in Hastalloy C-276
or 316 stainless steel.

Order
Code
6465-405

13549.56

10-Liter COMPLETE, Unjacketed Flask, with Electric ANALOG Motor 6465-401

12480.33

10-Liter COMPLETE, Unjacketed Flask, with Electric DIGITAL Motor

Each

10-Liter COMPLETE, Unjacketed Flask, with AIR DRIVEN Motor

6472-47

11835.62

20-Liter COMPLETE, Unjacketed Flask, with Electric DIGITAL Motor

6472-280

16526.01

20-Liter COMPLETE, Unjacketed Flask, with Electric ANALOG Motor 6472-282

15143.18

6472-284

15206.51

20-Liter COMPLETE, Unjacketed Flask, with AIR DRIVEN Motor

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

6472-280

20L shown above

Subject to Ace Discount (Page 4)

Net

Reactors/Large-Scale Pilot Plants

61

6472 PILOT PLANT REACTOR Cylindrical, 10 & 20 Liter Unjacketed Flask, D


 omed Head
Complete cylindrical pilot plant reactor
on oneinch stainless steel tubing mobile
support frame: measures 60 inches high,
15 inches wide, 15 inches deep. Note:
Frame shipped assembled.
Flask opening is 200 mm (8 inches),
Schott style flange with oring groove.
Bottom outlet is 0-14 mm Easy Action
adjustable threaded valve opening or flush
seal valve. ORings supplied on valves
are Chemraz (PTFE elastomeric material)
f o r e x c e l l e n t c h e m i c a l re s i s t a n c e .
Flasks with other bottom outlet types
are available.

Head is traditional domed style, with


seven openings. One 45/50 center
neck, one 45/50, two 29/42 and
two 24/40 openings plus a 60 mm I.D.
side port. Motor is secured on an epoxy
coated mounting plate over center 45/50
opening; other openings are for condenser,
thermop robe, cooling coil, etc. Head is
secured to flask with a quick release clamp.
Stirring motor can be air-driven or
electric, either digital or analog.
Stirring rod is a 19 mm (3/4 inch) O.D.,
precision ground and polished glass
stirring shaft with a pinned multi-

10 LITER
STIRRING MOTOR, Air Driven, 1-1/2 HP with 1/2 inch Motor Shaft
SUPPORT ASSEMBLY, Complete
CHUCK, Flex-Grip, 12.7mm 19mm
FILTER/REGULATOR/LUBRICATOR for Air Motor
COMPLETE AIR DRIVEN MOTOR SYSTEM
STIRRING MOTOR, Analog
SUPPORT ASSEMBLY, Complete
CHUCK, Flex-Grip, 9.5mm 19mm
COMPLETE ANALOG MOTOR SYSTEM
STIRRING MOTOR, Digital
SUPPORT ASSEMBLY, Complete
CHUCK, Flex-Grip, 13mm 19mm
COMPLETE DIGITAL MOTOR SYSTEM

Order Code
13370-10
6472-27
8124-20
13372-45
6472-47
13544-20
6472-362
8124-17
6465-401
13504-41
6472-360
8124-22
6465-405

All the above COMPLETE items contain these components:

Order Code

FLASK, with CAPFE ORing and 0-14 E-Z Action Bottom Valve
FLASK, with 200mm Flange, ORing groove
HEAD, Domed, with seven (7) openings
GLASS CAP, Side Port
CAPFE ORing, Side Port
CLAMP, Side Port, Quick Release
CLAMP, Head, 200mm, Quick Release
DRAIN VALVE, only, Flush Seal
CLAMP, Drain Valve, 1 inch
CLAMP, Drain Valve, 2 inch
SWEEP ELBOW, 60, 1 inch Beaded Pipe
MANTLE, Bottom, Aluminum, with hole, 1180w115v
MANTLE, Bottom, Aluminum, with hole, 1250w115v
MANTLE, #2 & #3, Fabric, Removable 1495w115v
MANTLE, #2 & #3, Fabric, Removable 1770w115v (2)
HEAT EXCHANGE COIL, Cooling, Copper/PTFE
TEMPERATURE CONTROL SYSTEM, Complete
AGITATOR, Lower, PTFE, Multipaddle
AGITATOR, Upper, PTFE, Turbine, 102mm
STIRRING SHAFT, 19mm Polished Glass
BEARING, PTFE, 45/50
COLLAR, with PTFE Gasket
ADAPTER, #7 24/40 (2)
ADAPTER, #7 29/42
ADAPTER, #11 29/42
ADAPTER, #11 24/40
ADAPTER, Offset 24/40
ADAPTER, Offset 29/42
ADAPTER, with 2mm bore PTFE stopcock
CONDENSER, 300mm, 29/42
CONDENSER, 300mm, 24/40
STOPPER, 24/40 (2)
STOPPER, 29/42 (2)
CLAMP HOLDER, Large Scale
ROD, 6 inch x 1/2 inch for Temperature Controller
GREASE, Krytox GPL

6522-21

6530-37
15312-30
7855-878
6517-22
6517-31

12053-50

12041-10

12067-39
6472-67
8091-10
8093-12
8076-40
8067-30
8127-20
5028-30
5028-32
5030-24

5945-24

8250-12
8250-14
11081-21
11166-22
8115-08

paddle PTFE agitator at bottom and a


pinned turbine blade PTFE agitator
higher on shaft for grease-free operation
with 8067 PTFE bearing. Note: Steel
reinforced PTFE shafts or ground glass
shafts can be supplied along with other
bearings.
Cooling coil is copper tubing
encapsulated with PTFE; also available
in 316 stainless steel or Hastalloy C-276.
A digital temperature control system is
supplied to control heating mantles. This
prevents overheating, overshoot and
gives an instant readout of temperature.

20 LITER
411.74
2563.97
152.25
237.98
11835.62
582.32
3269.29
152.25
12480.33
1948.46
3276.44
152.25
13549.56

Order Code
13370-10
6472-364
8124-20
13372-45
6472-284
13544-20
6472-362
8124-17
6472-282
13504-41
6472-360
8124-22
6472-280

411.74
3265.22
152.25
237.98
15206.51
582.32
3269.29
152.25
15143.18
1948.46
3276.44
152.25
16526.01

Each

Order Code

Each

Each

1131.71

1095.60
60.05
28.10
87.08
145.09

676.91

860.65

547.05
1745.08
226.34
186.56
248.02
269.05
36.68
27.61
32.61
44.98

137.68

19.79
25.05
84.80
8.36
59.40

6472-02
6530-37
15312-30
7855-878
6517-22
6517-31
6472-245
8856-07
8856-11
8830-207

12053-64

12041-12
12067-48
6472-67
8091-10
8093-12
8076-40
8067-30
8127-20
5028-30
5028-32
5030-24
5030-06
5268-10
5268-15
5202-12

5946-18
8250-12
8250-14
11081-21
11166-22
8115-08

Each

2242.57
1095.60
60.05
28.10
87.08
145.09
1010.52
112.13
150.55
65.97

874.66

777.15
600.74
1745.08
226.34
186.56
248.02
269.05
36.68
27.61
32.61
44.98
28.65
36.56
40.74
80.01

125.23
19.79
25.05
84.80
8.36
59.40

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

62

Reactors/Large-Scale Pilot Plants

6472 Cylindrical Pilot Plants

Domed Head

Unjacketed

30 & 50 Liter Reactors


With Stainless Steel Support

30 & 50 liter reactors with bottom


outlet
Domed glass head with large side
port opening
Internal heat exchange coil*
Rugged stainless steel pipe
support frame on casters for
mobility
Adjustable height flask support
Available with Lexan safety
shields

*Supplied with PTFE-coated copper


tubing; also available in Hastalloy C-276
or 316 stainless steel.
6472-56
Order Code

Each

30 Liter COMPLETE, Unjacketed Flask, with AIR DRIVEN Motor

6472-56

19978.81

50 Liter COMPLETE, Unjacketed Flask, with AIR DRIVEN Motor

6472-60

22534.06

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Subject to Ace Discount (Page 4)

Net

Reactors/Large-Scale Pilot Plants

63

6472 PILOT PLANT REACTOR Cylindrical, 30 & 50 Liter Unjacketed Flask, D


 omed Head
Complete cylindrical pilot plant reactor
on oneinch pipe, self-supporting, stainless
steel mobile support frame: 30 liter size
measures 76 inches high, 26 inches wide,
26 inches deep; 50 liter size measures 84
inches high, 26 inches wide, 26 inches
deep. Note: Frame shipped assembled.
Flask opening is 300 mm (12 inch),
flat-ground plane flange. Bottom outlet is
0-20mm Easy Action adjustable threaded
valve opening with oring ball joint outlet
tube. ORings supplied on valves are
Chemraz (PTFE elastomeric material)
f o r e x c e l l e n t c h e m i c a l re s i s t a n c e .
Flasks with other bottom outlet types
are available.
Black epoxy coated aluminum flask
support plate is adjustable, vertically,

to allow room under flask for various


outlet configurations.
Head is traditional domed style, with
eight openings. One 45/50 center neck,
four 45/50 and two 29/42 openings plus
a 100 mm I.D. side port. Motor is secured
on an epoxy coated mounting plate over
center 45/50 opening; other openings are
for condenser, thermop robe, cooling coil,
etc. Head is secured to flask with a PTFE
gasket and two-piece polymer coupling.
Maximum bolt-tightening torque for plastic
coupling (cold state) is 30 in-lbs. In place
of domed head, ACE also offers a flat glass
or flat stainless steel head (see page 113).
Stirring motor is a compact, air
driven motor that develops 1.5 HP at 90
lbs. air pressure. As an optional item,

30 LITER
FLASK, with 300mm Plane Flange and Bottom Valve
HEAD, Domed, with eight (8) openings
GLASS CAP, Side Port
CAPFE ORing, Side Port
CLAMP, Side Port, Quick Release
GASKET, Head, PTFE
COUPLING, Head, with Inserts and Hardware
WRENCH, Torque, 30 in-lbs.
SOCKET, 1/4 inch
MANTLE, Bottom, Aluminum, with hole, 1370w115v
MANTLE, #2, Fabric, Removable 2880w115v
MANTLE, #3, Fabric, Removable 2-725w115v
HEAT EXCHANGE COIL, Cooling, Copper/PTFE
SUPPORT ASSEMBLY, Complete
TEMPERATURE CONTROL SYSTEM, Complete
AIR MOTOR, 1-1/2 Hp with 1/2 inch Motor Shaft
FILTER/REGULATOR/LUBRICATOR for Air Motor
AGITATOR, Lower, PTFE, Multipaddle
AGITATOR, Upper, PTFE, with four Pitched Blades, 152mm
STIRRING SHAFT, Polished Glass
BEARING, PTFE, 45/50
CONNECTOR, Beam Connects 1/2 inch Motor Shaft to Chuck
CHUCK, 28mm Connects Beam Connection to Stirring Shaft
COLLAR, with PTFE Gasket
ADAPTER, #7 24/40
ADAPTER, #15 29/42, (2)
ADAPTER, #11 45/50
ADAPTER, #15 45/50
ADAPTER, #15 45/50, with 4mm PTFE Stopcock
ADAPTER, #11 and #15 45/50
ADAPTER, Side Arm, 45/50 45/50 24/40
ADAPTER, Angle, 45/50 45/50
BUSHING, Nylon, #11
BUSHING, Nylon, #15, (4)
CONDENSER, 500mm, 45/50
CONDENSER, Cold Finger, 14mm O.D., 625mm
STOPPER, 45/50, (4)
CLAMP HOLDER, Large Scale
ROD, 6 inch x 1/2 inch for Temperature Controller
GREASE, Krytox GPL
COMPLETE

ACE also o
ffers electric stirrer motors
(see 13554, page 216).
Stirring rod is a 28mm (1-1/8 inch)
O.D., precision ground and polished
glass stirring shaft with a pinned multipaddle PTFE agitator at bottom and a
turbine blade PTFE agitator higher on
shaft for grease-free operation with 8067
PTFE bearing. Note: Steel reinforced
PTFE shafts or ground glass shafts can be
supplied along with other bearing types.
Cooling coil is copper tubing
encapsulated with PTFE; available in
316 stainless steel or Hastalloy C-276.
A digital temperature control system is
supplied to control heating mantles. This
prevents overheating, overshoot and
gives an instant readout of temperature.

50 LITER

Order Code

Each

Order Code

Each

6472-03
6530-45
15312-33
7855-880
6517-25
6525-51
6525-30
6525-60
6525-61
12053-54
12041-16

12067-40
6472-31
6472-77
13370-10
13372-45
8091-36
8093-35
8080-14
8067-105
6472-155
6472-157
8127-28
5028-30
5030-42
5030-60
8042-17
5274-22
5031-86
5040-96
5075-45
7506-02
7506-06
5945-76
5958-99
8250-20
11081-21
11166-22
8115-08
6472-56

2583.56
2562.18
107.78
28.63
98.23
326.26
1056.54
144.09
10.69
697.89
1201.84

6472-05
6530-45
15312-33
7855-880
6517-25
6525-51
6525-30
6525-60
6525-61
12053-54
12041-18
12041-35
12067-44
6472-32
6472-79
13370-10
13372-45
8091-36
8093-35
8080-18
8067-105
6472-155
6472-157
8127-28
5028-30
5030-42
5030-60
8042-21
5274-22
5031-86
5040-96
5075-45
7506-02
7506-06
5945-76
5958-99
8250-20
11081-21
11166-22
8115-08
6472-60

3046.63
2562.18
107.78
28.63
98.23
326.26
1056.54
144.09
10.69
697.89
1090.99
1236.96
1692.90
3103.43
2988.82
411.74
237.98
613.84
628.06
446.02

1134.78
2790.68
2937.00
411.74
237.98
613.84
628.06
402.64
320.08
55.71
89.89
73.09
27.61
45.73
51.58
33.38
117.64
119.50
169.62
123.30
11.39
12.35
382.96
92.87
12.35
84.80
8.36
59.40
19978.81

320.08
55.71
89.89
73.09
27.61
45.73
51.58
33.38
117.64
119.50
169.62
123.30
11.39
12.35
382.96
92.87
12.35
84.80
8.36
59.40
22534.06

Custom variations and other stirring motors are available via


special order. Contact ACE Engineering and Technical Staff.

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

64

Reactors/Large-Scale Pilot Plants

6472 Cylindrical Pilot Plants

Flat Head

Unjacketed

30 & 50 Liter Reactors


With Stainless Steel Support

30 & 50 liter reactors with bottom


outlet
Stainless steel flat head
Internal heat exchange coil*
Rugged stainless steel pipe support
frame on casters for mobility
Adjustable height top and
bottom flask supports
Available with Lexan safety shields

*Supplied with PTFE-coated


copper tubing; also available
in Hastalloy C-276 or 316
stainless steel.

6472-51

30 Liter COMPLETE, Unjacketed Flask, with AIR DRIVEN Motor

Order Code
6472-51

Each
18892.72

50 Liter COMPLETE, Unjacketed Flask, with AIR DRIVEN Motor

6472-54

21447.97

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Subject to Ace Discount (Page 4)

Net

Reactors/Large-Scale Pilot Plants

65

6472 PILOT PLANT REACTOR Cylindrical, 30 & 50 Liter Unjacketed Flask, F lat Head
Complete cylindrical pilot plant reactor on
self-supporting, mobile support frame: 30
liter size on oneinch stainless steel pipe,
measures 70 inches high, 26 inches wide,
26 inches deep; 50 liter size on oneinch
stainless steel pipe, measures 78 inches
high, 26 inches wide, 26 inches deep. Note:
Frame shipped assembled.
Flask opening on 30 and 50 liter is 300 mm
(12 inch) flat-ground plane flange. Bottom
outlet on 30 and 50 liter is 0-20 mm valve.
ORings supplied on valves are Chemraz
(PTFE elastomeric material) for excellent
chemical resistance. Flasks with other bottom
outlet valves are available.
Black epoxy coated aluminum flask
support plate is adjustable, vertically, to

allow room under flask for various outlet


configurations.
Unique flat 316 stainless steel head is
0.250 inches (6.4mm) thick, with seven
openings. Head has 45/50 PTFE center
joint insert, four 45/50 PTFE joint inserts,
and two 29/42 PTFE joint inserts. Stainless
steel head has a PTFE cover. Maximum
bolt-tightening torque of head clamp (cold
state) is 30 in-lbs. Motor is secured on an
epoxy coated mounting plate over center
45/50 PTFE insert; other openings are for
condenser, thermoprobe, cooling coil, etc.
Head is secured to flask with PTFE gasket
and two-piece polymer coupling. In place of
flat head, ACE offers a domed glass head with
traditional raised joints.

30 LITER
Order Code

Stirring motor is a compact, air driven m


otor
that develops 1.5 HP at 90 lbs. air pressure.
As an optional item, ACE also offers electric
stirrer motors: see 13554.
Stirring rod is a 28 mm (1-1/8 inch),
precision ground and polished glass stirring
shaft with a pinned multi-paddle PTFE
agitator at bottom and a turbine blade PTFE
agitator higher on shaft for grease-free
operation with 8067 PTFE bearing.
Cooling coil is copper tubing encapsulated
with PTFE; available in 316 stainless steel
or Hastalloy C-276.
A digital temperature control system is
supplied to control heating mantles. This
prevents overheating, overshoot and gives
an instant readout of temperature.

50 LITER
Each

Order Code

Each

FLASK, with 300mm Plane Flange and Bottom Valve

6472-03

2583.56

6472-05

3046.63

HEAD, Flat, Stainless Steel, with 7 openings

6472-26

835.47

6472-26

835.47

HEAD COVER, 300mm, PTFE

6472-30

219.16

6472-30

219.16

JOINT INSERTS, PTFE 29/42 (2)

6413-07

90.78

6413-07

90.78

JOINT INSERTS, PTFE 45/50 (5)

6413-09

111.18

6413-09

111.18

GASKET, Head, PTFE

6525-51

326.26

6525-51

326.26

COUPLING, Head, with Inserts and Hardware

6525-30

1056.54

6525-30

1056.54

WRENCH, TORQUE, 30 in-lbs.

6525-60

144.09

6525-60

144.09

SOCKET, 1/4 inch

6525-61

10.69

6525-61

MANTLE, Bottom, Aluminum, with hole, 1370w-115v

12053-54

697.89

MANTLE, #2, Fabric, Removable 2880w-115v

12041-16

1201.84

MANTLE, #3, Fabric, Removable 2725-w115v

10.69

12053-54

697.89

12041-18

1090.99

12041-35

1236.96

COIL, Cooling, Copper/PTFE, 1/2 inch

12067-40

1134.78

12067-44

1692.90

SUPPORT ASSEMBLY, Complete

6472-31

2790.68

6472-32

3103.43

TEMPERATURE CONTROL SYSTEM, Complete

6472-77

2937.00

6472-79

2988.82

AIR MOTOR, 1-1/2 HP with 1/2 inch Motor Shaft

13370-10

411.74

13370-10

411.74

FILTER/REGULATOR/LUBRICATOR for Air Motor

13372-45

237.98

13372-45

237.98

AGITATOR, Lower, PTFE, Multipaddle, 178mm

8091-36

613.84

8091-36

613.84

AGITATOR, Upper, PTFE, with 4 Pitched Blades, 152mm

8093-35

628.06

8093-35

628.06

STIRRING SHAFT, Polished Glass

8080-14

402.64

8080-18

446.02

BEARING, PTFE, 45/50

8067-105

320.08

8067-105

320.08

CONNECTOR, Beam, Connects 1/2 inch Motor Shaft to Chuck

6472-155

55.71

6472-155

55.71

CHUCK, 28mm, Connects Beam Connector to Stirring Shaft

6472-157

89.89

6472-157

89.89

COLLAR, with PTFE Gasket

8127-28

73.09

8127-28

73.09

ADAPTER, #15 29/42 (2)

5030-42

45.73

5030-42

45.73

ADAPTER, #11 45/50

5030-60

51.58

5030-60

51.58

ADAPTER, #15 45/50

8042-21

50.57

8042-21

50.57

ADAPTER, #15 45/50, with 4mm PTFE Stopcock

5274-22

117.64

5274-22

117.64

ADAPTER, #11 & #15 45/50

5031-86

119.50

5031-86

119.50

ADAPTER, Side Arm, 45/50 45/50 24/40

5040-96

169.62

5040-96

169.62

ADAPTER, Angle, 45/50 45/50

5075-45

123.30

5075-45

123.30

BUSHING, Nylon, #11

7506-02

11.39

7506-02

11.39

BUSHING, Nylon, #15 (4)

7506-06

12.35

7506-06

12.35

CONDENSER, 500mm, 45/50

5945-76

382.96

5945-76

382.96

CONDENSER, Cold Finger, 14mm O.D., 625mm

5958-99

92.87

5958-99

92.87

STOPPER, 45/50 (4)

8250-20

44.68

8250-20

44.68

ROD, 6 inch x 1/2 inch for Temperature Controller

11166-22

GREASE, Krytox GPL

8115-08

59.40

8115-08

59.40

COMPLETE

6472-51

18892.72

6472-54

21447.97

8.36

11166-22

8.36

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

66

Reactors/Large-Scale Pilot Plants

6473 Cylindrical Pilot Plants



Jacketed or Unjacketed Flask

3-Post Stand

30 Liter Reactors

New 3-post support stand


with open top offers easier
access to head and/or
placement of condensers,
probes, etc.
Portable 30 liter reactor
with bottom outlet
Internal heat exchange
coil (unjacketed flask)*
Rugged user-friendly
support frame has
flanges with captive
hardware
PTFE-covered bottom
flask support shelf

For heating/cooling
circulators, see
listing starting on
page 240.

6473-150

*Supplied with PTFE-coated


copper tubing; also available
in Hastalloy C-276 or 316
stainless steel.

6473-275

Adapter and side drive motors are available.


Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Subject to Ace Discount (Page 4)

Net

Reactors/Large-Scale Pilot Plants

67

6473 PILOT PLANT REACTOR Cylindrical, 30 Liter Jacketed or Unjacketed Flask, D


 omed Head
Complete cylindrical pilot plant
reactor on self-supporting 3-post, mobile
support frame. Frame is fabricated
from stainless steel and powder coated
aluminum: measures 74 inches high, 24
inches wide, 20 inches deep. Note: Frame
shipped assembled.
Flask can be jacketed or unjacketed
with 300mm (12 inch) opening, flat
ground plane flange. Bottom outlet
is a 0-20mm Easy Action adjustable
opening threaded valve with C hemraz
(PTFE elastomeric material) orings
for excellent chemical resistance on
unjacketed flask; a flush seal drain with
oneinch beaded drain discharge with
CAPFE and Kalrez orings on jacketed
flask. Flasks with other bottom valves
are available.

Jacket on flask is direct sealed to inner


vessel at top and silicone rubber sealed
at bottom. Jacket inlet/outlet 35/25
ORing ball joints sealed tangentially
Flask support is adjustable, vertically,
to allow room under flask for various
outlet configurations.
Head is traditional domed style, with
eight openings: 45/50 center neck,
four 45/50 and two 29/42 side necks,
plus a 100mm (4 inch) I.D. side port
with grooved flange. Head is secured
to flask with a new swing open front
flange clamp, torqued to 30 in-lbs (tools
supplied).
Stirring motor is a 1/2 HP, 120v,
50/60Hz electric motor, for hazardous
locations, mounted over center of
45/50 center neck.

30 LITER UNJACKETED

(12 inch Flange; 12 inch Body)


Order Code
FLASK, with 300mm Plane Flange and Valve or Valve Opening
HEAD, Domed, with Eight Openings
GLASS CAP, 100mm
CAPFE ORing, 100mm
CLAMP, Quick Release, 100mm
GASKET, PTFE
WRENCH, TORQUE, 30 in-lbs.
SOCKET, 1/2-inch, 1/4-inch
DRAIN VALVE, Flush Seal (Jacketed only)
CLAMP, Drain Valve, 1 inch
CLAMP, Drain Valve, 2 inch
SWEEP ELBOW, 60, 1 inch BP
MANTLE, Bottom, Aluminum, with hole, 1-370w-115v
MANTLE, #2, Fabric, Removable, 2-880w-115v
COIL, Cooling, Copper/PTFE, 1/2 inch
SUPPORT ASSEMBLY, 3-Post Complete
TEMPERATURE CONTROL SYSTEM, Complete
TEMPERATURE MONITORING SYSTEM, Complete
STIRRER MOTOR AND CONTROLLER, 1/2 HP
AGITATOR, Lower, PTFE, Multipaddle, 178mm
AGITATOR, Upper, PTFE, with 4 Pitched Blades, 152mm
STIRRING SHAFT, Polished Glass, 28mm
BEARING, PTFE, 45/50
CONNECTOR, Beam Coupling, 5/8 inch Motor Shaft to Chuck
CHUCK, 28mm, Connects Beam Connector to Stirring Shaft
COLLAR, with PTFE Gasket
ADAPTER, #7 24/40
ADAPTER, #15 29/42 (2)
ADAPTER, #11 45/50
ADAPTER, #15 45/50
ADAPTER, #15 45/50, with 4mm PTFE Stopcock
ADAPTER, #11 and #15 45/50
ADAPTER, Side Arm, 45/50 45/50 45/50
ADAPTER, Angle, 45/50 45/50
ADAPTER, Offset, 45/50 45/50
BUSHING, Nylon, #11
BUSHING, Nylon, #15 (4)
CONDENSER, 500mm, 45/50
CONDENSER, Cold Finger, 14mm O.D., 625m
STOPPER, 45/50 (4)
GREASE, Krytox GPL
COMPLETE

6472-03
6530-45
15312-33
7855-880
6517-25
6525-51
6525-60
6525-61

12053-54
12041-16
12067-40
6473-47
6472-77

13554-55
8091-36
8093-35
8080-14
8067-105
6472-156
6472-157
8127-28
5028-30
5030-42
5030-60
8042-21
5274-22
5031-86
5040-96
5075-45
5268-21
7506-02
7506-06
5945-76
5958-99
8250-20
8115-08
6473-150

Each
2583.56
2562.18
107.78
28.63
98.23
326.26
144.09
10.69

697.89
1201.84
1134.78
5188.31
2937.00

3369.54
613.84
628.06
402.64
320.08
54.09
89.89
73.09
27.61
45.73
51.58
50.57
117.64
119.50
169.62
123.30
109.58
11.39
12.35
382.96
92.87
44.68
59.40
23975.32

Stirring rod is a 28mm (1-1/8 inch)


O.D. precision ground and polished
solid glass stirring shaft with a pinned
multi-paddle PTFE agitator at bottom
and a turbine blade PTFE agitator higher
on shaft for grease-free operation with
8067 PTFE bearing.
Heat exchange coil for unjacketed
reactor is a 1/2 inch O.D. copper tubing
encapsulated with PTFE; available in
316 stainless steel or Hastalloy C-276.
A digital temperature control system
is supplied with unjacketed reactor
consisting of a type J digital controller
with a PFA covered thermoprobe to
control heating mantles.
A type J temperature monitoring
system is supplied with the jacketed
flask version.

30 LITER JACKETED

(12 inch Flange; 12 inch Body)


Order Code
6472-030
6530-45
15312-33
7855-880
6517-25
6525-51
6525-60
6525-61
6472-245
8856-07
8856-11
8830-207

6473-51

8318-207
13554-55
8091-36
8093-35
8080-14
8067-105
6472-156
6472-157
8127-28
5028-30
5030-42
5030-60
8042-21
5274-22
5031-86
5040-96
5075-45
5268-21
7506-02
7506-06
5945-76
5958-99
8250-20
8115-08
6473-275

Each
6038.75
2562.18
107.78
28.63
98.23
326.26
144.09
10.69
1010.52
112.13
150.55
65.97

5531.62

1028.28
3369.54
613.84
628.06
402.64
320.08
54.09
89.89
73.09
27.61
45.73
51.58
50.57
117.64
119.50
169.62
123.30
109.58
11.39
12.35
382.96
92.87
44.68
59.40
24274.92

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

68

Reactors/Large-Scale Pilot Plants

6473 Cylindrical Pilot Plants

100 Liter Reactor

Domed Head

Unjacketed

With Stainless Steel Support

100 liter reactor with bottom outlet


Domed glass head with large side
port opening
Internal heat exchange coil*
Rugged stainless steel pipe support
frame on casters for mobility
Adjustable height top and bottom
flask supports
Available with Lexan safety shields

*Supplied with PTFE-coated copper


tubing; also available in Hastalloy C-276
or 316 stainless steel.

6473-60
Order Code
100 Liter COMPLETE, Unjacketed Flask, with Motor

6473-60

Each
29452.59

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Subject to Ace Discount (Page 4)

Net

Reactors/Large-Scale Pilot Plants

69

6473 PILOT PLANT REACTOR Cylindrical, 100 Liter Unjacketed Flask, D


 omed Head
Complete cylindrical pilot plant reactor
on self-supporting, mobile support frame
on oneinch stainless steel pipe, measures
88 inches high, 28 inches wide, 28 inches
deep. Note: Frame shipped assembled.
Flask opening is 300 mm (12 inch) flatground plane flange. Flask body is 18 inch
outside diameter. Bottom outlet is 0-20
mm adjustable opening threaded valve
with Chemraz (PTFE elastomeric material)
ORings for excellent chemical resistance.
Other bottom valve types are available.
Black epoxy coated aluminum flask
support plate is adjustable, vertically, to
allow room under flask for various outlet
receptacles. Upper support brackets

supplied to stabilize flask.


Head is traditional domed style, with
eight openings; five 45/50 and two
29/42 plus one 100 mm I.D. side port.
Motor is secured on black epoxy coated
mounting plate over center 45/50 opening
on head; other openings are for condenser,
thermoprobe, cooling coil, etc. Head is
secured to flask with PTFE gasket and

two-piece polymer coupling. Maximum bolt


tightening torque for coupling (cold state)
is 30 in-lbs. In place of domed head, ACE
offers a flat glass or flat stainless steel head.
Stirring motor is heavy duty, 1/2 HP
electronic motor for hazardous area duty,
complete with controller. Motor shaft is

100 LITER (12 inch Flange; 18 inch Body)


FLASK, with 300mm Plane Flange and Valve
HEAD, Domed, with 8 Openings
GLASS CAP, 100mm
CAPFE ORing, 100mm
CLAMP, Quick Release, 100mm
GASKET, PTFE
COUPLING, with Inserts and Hardware
WRENCH, TORQUE, 30 in-lbs.
SOCKET
MANTLE, Bottom, Aluminum, with hole, 1-775w-115v
MANTLE, #2, Fabric, Removable, 4-1100w-115v
COIL, Cooling, Copper/PTFE, 1/2 inch
SUPPORT ASSEMBLY, Complete
TEMPERATURE CONTROL SYSTEM, Complete
STIRRER MOTOR AND CONTROLLER, 1/2 HP
AGITATOR, Lower, PTFE, Multipaddle, 178mm
AGITATOR, Upper, PTFE, with 4 Pitched Blades, 152mm
STIRRING SHAFT, Polished Glass, 28mm
BEARING, PTFE, 45/50
CONNECTOR, Beam, Connects 5/8 inch Motor Shaft to Chuck
CHUCK, 28mm, Connects Beam Connector to Stirring Shaft
COLLAR, with PTFE Gasket
ADAPTER, #7 24/40
ADAPTER, #15 29/42 (2)
ADAPTER, #11 45/50
ADAPTER, #15 45/50
ADAPTER, #15 45/50, with 4mm PTFE Stopcock
ADAPTER, #11 and #15 45/50
ADAPTER, Side Arm, 45/50 45/50 24/40
ADAPTER, Angle, 45/50 45/50
ADAPTER, Offset, 45/50 45/50
BUSHING, Nylon, #11
BUSHING, Nylon, #15 (4)
CONDENSER, 500mm, 45/50
CONDENSER, Cold Finger, 14mm O.D., 625mm
STOPPER, 45/50 (4)
CLAMP, Chain
CLAMP HOLDER, Pilot Plant (2)
SUPPORT ROD, 1/2 inch diameter, 12 inches long
END-TO-END ROD CONNECTOR
ROD, 6 inch x 1/2 inch for Temperature Controller
GREASE, Krytox GPL
COMPLETE

Order Code
6473-02
6530-45
15312-33
7855-880
6517-25
6525-51
6525-30
6525-60
6525-61
12053-74
12041-52
12067-79
6473-34
6472-79
13554-55
8091-36
8093-35
8080-22
8067-105
6472-156
6472-157
8127-28
5028-30
5030-42
5030-19
8042-21
5274-22
5031-86
5040-96
5075-45
5268-21
7506-02
7506-06
5945-76
5958-99
8250-20
11079-24
11081-21
11166-37
11175-23
11166-22
8115-08
6473-60

5/8 inch O.D. Controller operates on 120


volts 50/60 Hz (air motor available call
for quotation).
Features a 28 mm (1-1/8 inch) O.D.
precision ground and polished glass stirring
shaft with a pinned multi-paddle PTFE
agitator at bottom and a turbine blade PTFE
agitator higher on shaft for grease-free
operation with 8067 PTFE bearing.
Cooling coil is 1/2 inch O.D. copper tubing
encapsulated with PTFE; also available in
316 stainless steel or Hastalloy C-276.
A digital temperature control system is
supplied to control heating mantles. This
prevents overheating, overshoot and gives
an instant readout of temperature.

Each
5531.62
2562.18
107.78
28.63
98.23
326.26
1056.54
144.09
10.69
1462.92
2228.41
1773.43
3855.28
2988.82
3369.54
613.84
628.06
472.33
320.08
54.09
89.89
73.09
27.61
45.73
62.97
50.57
117.64
119.50
169.62
123.30
109.58
11.39
12.35
382.96
92.87
44.68
51.23
84.80
13.60
19.87
8.36
59.40
29452.59

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

70

Reactors/Large-Scale Pilot Plants

6473 Cylindrical Pilot Plants

200 Liter Reactor

Domed Head

Unjacketed

With Stainless Steel Support

200 liter reactor with bottom outlet


Domed glass head with large side
port opening
Internal heat exchange coil*
Rugged stainless steel pipe support
frame on casters for mobility
Adjustable height top and bottom
flask supports
Available with Lexan safety shields

*Supplied with PTFE-coated copper


tubing; also available in Hastalloy C-276
or 316 stainless steel.

Order Code
200 Liter COMPLETE, Unjacketed Flask, with Motor

6473-72

Each

6473-72

39583.21

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Subject to Ace Discount (Page 4)

Net

Reactors/Large-Scale Pilot Plants

71

6473 PILOT PLANT REACTOR Cylindrical, 200 Liter Unjacketed Flask, D


 omed Head
Complete cylindrical pilot plant reactor
on self-supporting, mobile support frame
on oneinch stainless steel pipe, measures
118 inches high, 32 inches wide, 32 inches
deep. Note: Frame shipped assembled.
Flask opening is 300 mm (12 inch) flatground plane flange. Flask body is 18 inch
outside diameter. Bottom outlet is a flush
seal drain valve with a oneinch beaded
drain discharge. ORing supplied on valve is
a CAPFE (silicone encapsulated with PTFE),
and Kalrez for excellent chemical resistance.
Black epoxy coated aluminum flask
support plate is adjustable, vertically,
to allow room under flask for various
outlet receptacles. Plate is supplied with
three adjustable braces to hold mantle in

place. Upper support brackets supplied


to stabilize flask.
Head is traditional domed style, with
eight openings; five 45/50, two 29/42,
plus one 100 mm I.D. side port.
Motor is secured on black epoxy coated
mounting plate over center 45/50 opening
on head; other openings are for condenser,
thermoprobe, cooling coil, etc. Head is
s ecured to flask with PTFE gasket and

two-piece plastic coupling. Maximum bolt


tightening torque for coupling (cold state)
is 30 in-lbs. In place of domed head, ACE
offers a flat glass or flat stainless steel head
that use PTFE joint inserts.
Stirring motor is heavy duty, 1/2 HP
electronic motor for hazardous area duty.

200 LITER (12 inch Flange; 18 inch Body)


FLASK with 300mm Plane Flange, 200L
HEAD, Domed, with 8 Openings
GLASS CAP, 100mm
CAPFE ORing, 100mm
CLAMP, Quick Release, 100mm
GASKET, PTFE
COUPLING, with Inserts and Hardware
WRENCH, TORQUE, 30 in-lbs.
SOCKET 1/4 inch
DRAIN VALVE, Flush Seal
CLAMP, Drain Seal 1 inch
CLAMP, Drain Seal 2 inch
SWEEP ELBOW, 60, 1 inch BP
MANTLE, Bottom, Aluminum, with hole, 1-775w-115v
MANTLE, #2, Fabric, Removable, 4-1100w-115v (2)
COIL, Cooling, Copper/PTFE, 1/2 inch
SUPPORT ASSEMBLY, Complete
TEMPERATURE CONTROL SYSTEM, Complete
STIRRER MOTOR AND CONTROLLER, 1/2 HP
AGITATOR, Lower, PTFE, Multipaddle, 178mm
AGITATOR, Upper, PTFE, with 4 Pitched Blades, 152mm (2)
STIRRING SHAFT, Polished Glass, 28mm
BEARING, PTFE, 45/50
CONNECTOR, Beam, Conn. 5/8 inch Motor Shaft to Chuck
CHUCK, 28mm, Connects Beam Conn. to Stirring Shaft
COLLAR, with PTFE Gasket
ADAPTER, #7 24/40
ADAPTER, #11 45/50
ADAPTER, #15 29/42
ADAPTER, #15 45/50
ADAPTER, #15 45/50, with 4mm PTFE stopcock
ADAPTER, #11 and #15 45/50
ADAPTER, Side Arm, 45/50 45/50 24/40
ADAPTER, Angle, 45/50 45/50
ADAPTER, Offset, 45/50 45/50
BUSHING, Nylon, #11
BUSHING, Nylon, #15 (4)
CONDENSER, 500mm, 45/50
CONDENSER, Cold Finger, 14mm O.D., 625mm
STOPPER, 45/50 (4)
CLAMP, Chain
CLAMP HOLDER, Pilot Plant (2)
SUPPORT ROD, 1/2 inch diameter, 12 inches long (2)
END-TO-END ROD CONNECTOR
GREASE, Krytox GPL
COMPLETE

Order Code
6473-11
6530-45
15312-33
7855-880
6517-25
6525-51
6525-30
6525-60
6525-61
6472-245
8856-07
8856-11
8830-207
12053-74
12041-52
12067-80
6473-37
6472-87
13554-55
8091-36
8093-35
8080-25
8067-105
6472-156
6472-157
8127-28
5028-30
5030-19
5030-42
8042-21
5274-22
5031-86
5040-96
5075-45
5268-21
7506-02
7506-06
5945-76
5958-99
8250-20
11079-24
11081-21
11166-37
11175-23
8115-08
6473-72

Motor shaft is 5/8 inch O.D. Controller


operates on 120 volts 50/60 Hz. (Air motor
available, call for quotation).
28 mm (1-1/8 inch) O.D. precision
ground and polished glass stirring shaft
with a pinned multi-paddle PTFE agitator
at bottom and two turbine blade PTFE
agitators higher on shaft for grease-free
operation with 8067 PTFE bearing.
Cooling coil is 1/2 inch O.D. copper
tubing encapsulated with PTFE; also
available in 316 stainless steel or Hastalloy
C-276.
A digital temperature control system
is supplied to control heating mantles. This
prevents over-heating and overshoot, and
gives an instant readout of temperature.

Each
10958.02
2562.18
107.78
28.63
98.23
326.26
1056.54
144.09
10.69
1010.52
112.13
150.55
65.97
1462.92
2228.41
2123.00
3940.86
3017.57
3369.54
613.84
628.06
634.97
320.08
54.09
89.89
73.09
27.61
62.97
45.73
50.57
117.64
119.50
169.62
123.30
109.58
11.39
12.35
382.96
92.87
44.68
51.23
84.80
13.60
19.87
59.40
39583.21

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

72

Reactors/Large-Scale Pilot Plants

6472/6465 C ylindrical Pilot Plants

Domed Head

Jacketed

10 & 20 Liter Reactors


With Stainless Steel Support

10 & 20 liter jacketed


reactors with bottom
outlet
Domed glass head
with large side
port
opening
Internal heat
exchange coil
available, not
supplied

6472-367

6472-365

Rugged stainless steel pipe


support frame on casters
for mobility
Adjustable height flask support
Available with Lexan safety
shields
For heating/cooling circulators,
see listing starting on page 240.
Order Code

Each

10-Liter COMPLETE, Jacketed Flask, with Electric ANALOG Motor

6465-501

10591.42

10-Liter COMPLETE, Jacketed Flask, with Electric DIGITAL Motor

6465-505

11977.03

10-Liter COMPLETE, Jacketed Flask, with AIR DRIVEN Motor

6472-147

9933.34

20-Liter COMPLETE, Jacketed Flask, with Electric DIGITAL Motor

6472-363

14738.20

20-Liter COMPLETE, Jacketed Flask, with Electric ANALOG Motor

6472-365

13344.23

20-Liter COMPLETE, Jacketed Flask, with AIR DRIVEN Motor

6472-367

13417.02

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

6472-363

Subject to Ace Discount (Page 4)

Net

Reactors/Large-Scale Pilot Plants

73

6472/6465 PILOT PLANT REACTOR Cylindrical, 10 & 20 Liter Jacketed Flask, D


 omed Head
Complete cylindrical pilot plant reactor
on 1-inch stainless steel tubing mobile
support frame: measures 60 inches high,
15 inches wide, 15 inches deep. Note:
Frame shipped assembled.
Jacketed flask opening is 200 mm
(8 inch), Schott style flange with oring
groove. Bottom outlet on 10L flask is
0-14 mm Easy Action adjustable threaded
valve opening; bottom outlet on 20L
flask is low dead space, flush seal valve.
ORings supplied on valves are Chemraz
(PTFE elastomeric material) for excellent
chemical resistance. Flasks with other
bottom outlet types are available. Jacket

on flask is direct sealed at the top and


silicone rubber sealed at bottom. 28/15 or
35/25 o-ring ball joint on inlet/outlet sealed
tangentially.
Head is traditional domed style, with
seven openings. One 45/50 center neck,
one 45/50 , two 29/42 and two 24/40
openings, plus a 60 mm I.D. side port. Motor
is secured on an epoxy coated mounting
plate over center 45/50 opening; other
openings are for condenser, thermop robe,
cooling coil, etc. Head is secured to flask
with a quick release clamp.
Stirring motor can be air-driven or
electric, either digital or analog.

Stirring rod is a 19 mm (3/4 inch) O.D.,


precision ground and polished glass
stirring shafts with a pinned multi-paddle
PTFE agitator at bottom and a turbine
blade PTFE agitator higher on shaft for
grease-free operation with 8067 PTFE
bearing. Note: Steel reinforced PTFE
shafts or ground glass shafts can be
supplied along with other bearings.
A temperature monitoring system, with
PTFE-covered Type J Thermocouple,
is supplied to give an instant readout of
temperature.
Jacket volume for 10L flask is six liters.
Jacket volume for 20L flask is 13.4 liters.

10 LITER
STIRRING MOTOR, Air Driven, 1-1/2 HP with 1/2 inch Motor Shaft
SUPPORT ASSEMBLY, Stainless Steel, Complete
CHUCK, Flex-Grip, 12.7mm 19mm
FILTER/REGULATOR/LUBRICATOR for Air Motor
COMPLETE AIR DRIVEN MOTOR SYSTEM
STIRRING MOTOR, Analog
SUPPORT ASSEMBLY, Stainless Steel, Complete
CHUCK, Flex-Grip, 9.5mm 19mm
COMPLETE ANALOG MOTOR SYSTEM
STIRRING MOTOR, Digital
SUPPORT ASSEMBLY, Stainless Steel, Complete
CHUCK, Flex-Grip, 13mm 19mm
COMPLETE DIGITAL MOTOR SYSTEM

Order Code
13370-10
6472-328
8124-20
13372-45
6472-147
13544-20
6472-335
8124-17
6465-501
13504-41
6472-329
8124-22
6465-505

All the above COMPLETE items contain these components:

Order Code

FLASK, Jacketed with ORing Groove and 0-14mm Bottom Valve, 10L
FLASK, Jacketed with 200mm Flange, ORing groove, 20L
HEAD, Domed, with seven (7) openings
GLASS CAP, Side Port
CAPFE ORing, Side Port
CLAMP, Side Port, Quick Release
CLAMP, Head, 200mm, Quick Release
DRAIN VALVE, only Flush Seal
CLAMP, Drain Valve, 1 inch
CLAMP, Drain Valve, 2 inch
SWEEP ELBOW, 60, 1 inch Beaded Pipe
TEMPERATURE MONITORING SYSTEM, Complete
AGITATOR, Lower, PTFE, Multipaddle
AGITATOR, Upper, PTFE, Turbine, 102mm
STIRRING SHAFT, 19mm Polished Glass
BEARING, PTFE, 45/50
COLLAR, with PTFE Gasket
ADAPTER, #7 29/42
ADAPTER, #11 29/42
ADAPTER, #11 24/40
ADAPTER, Offset 24/40
ADAPTER, Offset 29/42
ADAPTER, with 2mm bore PTFE stopcock
CONDENSER, 300mm, 29/42
CONDENSER, 300mm, 24/40
STOPPER, 24/40 (2)
STOPPER, 29/42 (2)
CLAMP HOLDER, Large Scale
ROD, 6 inch x 1/2 inch for Temperature Monitor
GREASE, Krytox GPL

6524-23

6530-37
15312-30
7855-878
6517-22
6517-31

8318-204
8091-10
8093-12
8076-40
8067-30
8127-20
5028-32
5030-24

5268-15

5945-24

8250-12
8250-14
11081-21
11166-22
8115-08

20 LITER
Each
411.74
2601.49
152.25
237.98
9933.34
582.32
3326.97
152.25
10591.42
1948.46
3336.90
152.25
11977.03

Each
3002.10

1095.60
60.05
28.10
87.08
145.09

865.12
226.34
186.56
248.02
269.05
36.68
32.61
44.98

40.74

137.68

19.79
25.05
84.80
8.36
59.40

Order Code
13370-10
6472-337
8124-20
13372-45
6472-367
13544-20
6472-335
8124-17
6472-365
13504-41
6472-329
8124-22
6472-363
Order Code

6472-16
6530-37
15312-30
7855-878
6517-22
6517-31
6472-245
8856-07
8856-11
8830-207
8318-204
8091-10
8093-12
8076-40
8067-30
8127-20
5028-32

5030-22
5268-10

5202-12

5946-18
8250-12
8250-14
11081-21
11166-22
8115-08

Each
411.74
3294.38
152.25
237.98
13417.02
582.32
3326.97
152.25
13344.23
1948.46
3336.90
152.25
14738.20

Each

4361.31
1095.60
60.05
28.10
87.08
145.09
1010.52
112.13
150.55
65.97
865.12
226.34
186.56
248.02
269.05
36.68
32.61

40.04
36.56

80.01

125.23
19.79
25.05
84.80
8.36
59.40

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

74

Reactors/Large-Scale Pilot Plants

7885 Pilot Plant Reactor

Photochemical

Jacketed

10 & 20 Liter Reactors


With Stainless Steel Support

New

10 & 20 liter jacketed reactors


with bottom outlet
Domed glass head with large
side port opening
Rugged stainless steel pipe
support frame on casters
for mobility
Adjustable height flask support
Large-scale photochemical
quartz immersion well
Large-scale photochemical U.V.
lamp & 1200 watt power supply
Available with Lexan safety
shields
6530-85
Head

7830-71

Order Code

Each

10 Liter COMPLETE, Unjacketed Flask, with DIGITAL Motor

7885-10

23009.90

20 Liter COMPLETE, Unjacketed Flask, with DIGITAL Motor

7885-20

24480.30

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

7885

Subject to Ace Discount (Page 4)

Net

Reactors/Large-Scale Pilot Plants

75

7885 PHOTOCHEMICAL REACTOR Pilot Plant, 10 & 20 Liter Jacketed Flask


Complete cylindrical pilot plant reactor
on 1-inch stainless steel tubing mobile
support frame: measures 60 inches high,
15 inches wide, 15 inches deep. Note:
Frame shipped assembled.
Jacketed flask opening is 200 mm
(8inch), Schott style flange with ORing
groove. Bottom outlet is low dead
space flush seal valve. ORings
supplied on valves are Chemraz (PTFE
elastomeric material) for excellent
chemical resistance. Flasks with other
bottom outlet types are available. Jacket
on flask is direct sealed at the top and
bottom. 35/25 o-ring ball joint on inlet/
outlet sealed tangentially.

stirring shaft with a pinned multipaddle PTFE agitator at bottom of shaft


with 8050 PTFE mechanical seal bearing.
Note: Steel reinforced PTFE shafts or
ground glass shafts can be supplied
along with other bearings.
A temperature monitoring system, with
PTFE-covered type J thermocouple,
is supplied to give an instant readout
of temperature. Also includes a 230V
power supply and a 120-watt U.V. lamp.
Includes Pyrex absorption sleeve for well.

Head is traditional domed style,


with six openings. One 45/50 center
neck, one 45/50, one 29/42 and one
24/40 side necks, a #50 AceThred
neck for immersion well, and a 60 mm
I.D. side port. Motor is secured on an
epoxy coated mounting plate over center
45/50 opening; other openings are for
condenser, thermoprobe, immersion well,
etc. Head is secured to flask with a quick
release clamp.
Stirring motor is 120V Heidolph
electric, digital. Other types are available
via special order.
Stirring rod is a 19 mm (3/4 inch) O.D.,
precision ground and polished glass

Jacket volume for 10L flask is six liters.


Jacket volume for 20L flask is 13.4 liters.

10 LITER

20 LITER

Order Code

Each

Order Code

Each

STIRRING MOTOR, Digital, Heidolph


SUPPORT ASSEMBLY, Stainless Steel
CHUCK, 19mm
RZR Stainless Steel Shaft and Coupling
FLASK, 10L Jacketed, 200mm Opening with ORing Groove
FLASK, 20L Jacketed, 200mm Opening with ORing Groove
Bottom Flush Seal Valve Assembly with Pin
HEAD, Domed, with six (6) openings
GLASS CAP, 60mm Side Port
CAPFE ORing, Side Port
CLAMP, 60mm, Side Port, Quick Release
CLAMP, Head, 200mm, Quick Release
CLAMP, Drain Valve, 1 inch
CLAMP, Drain Valve, 2 inch
SWEEP ELBOW, 60 x 1 inch Beaded Pipe
TEMPERATURE MONITORING SYSTEM, J-Kem, with J Thermocouple
24-in. PFA J Thermocouple
AGITATOR, Lower, PTFE, with Receptacle
STIRRING SHAFT, 19mm Polished Glass, 37 in. length
BEARING, PTFE, 45/50, Mechanical Seal
Stopcock Adapter for Condenser
ADAPTER, #7 24/40
ADAPTER, Offset 29/42
CONDENSER, 400mm, 29/42
STOPPER, 45/50 (1)
CLAMP HOLDER, for Temperature Monitor
ROD, 6 inch x 1/2 inch for Temperature Monitor
GREASE, Krytox
Immersion Well, Quartz, 48mm O.D. x 840mm Long
U.V. Lamp 1200w
#50 Bushing
Pyrex Absorption Sleeve, 30mm O.D. x 762mm Long
U.V. Power Supply 230v, 60hz
Pressure Relief Manifold
Circulator Hose Adapters (1)
Hose Clamps (1)

13504-41
6472-329
8126-19
8126-22
6524-73

6482-20
6530-85
15312-30
7855-878
6517-22
6517-31
8856-07
8856-11
8830-207
12327-05
12141-26
8100-19
8076-39
8050-06
5202-114
5028-30
5268-15
5945-25
8250-20
11081-21
11166-22
8115-08
7874-48
7825-40
7506-14
7835-45
7830-71
10015-10
12187-35
13010-01

1948.46
3336.90
113.26
276.11
2890.91

1032.42
1213.52
60.05
28.10
87.08
145.09
112.13
150.55
65.97
391.00
171.58
854.95
249.51
601.93
63.72
27.61
40.74
141.24
44.68
84.80
8.36
59.40
1100.65
897.10
854.52
56.98
3901.10
2741.31
135.20
112.28

13504-41
6472-329
8126-19
8126-22

6472-16
6482-20
6530-85
15312-30
7855-878
6517-22
6517-31
8856-07
8856-11
8830-207
12327-05
12141-26
8100-19
8076-39
8050-06
5202-114
5028-30
5268-15
5945-25
8250-20
11081-21
11166-22
8115-08
7874-48
7825-40
7506-14
7835-45
7830-71
10015-10
12187-35
13010-01

1948.46
3336.90
113.26
276.11

4361.31
1032.42
1213.52
60.05
28.10
87.08
145.09
112.13
150.55
65.97
391.00
171.58
854.95
249.51
601.93
63.72
27.61
40.74
141.24
44.68
84.80
8.36
59.40
1100.65
897.10
854.52
56.98
3901.10
2741.31
135.20
112.28

COMPLETE

7885-10

23009.90

7885-20

24480.30

For safety, either aluminum, stainless steel, or black


plastic shields should be added to the stand, or it should
be used in an enclosed hood.
Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

76

Reactors/Large-Scale Pilot Plants

6472 Cylindrical Pilot Plants

Domed Head

Jacketed

30 & 50 Liter Reactors


With Stainless Steel Support

30 & 50 liter jacketed reactors


with bottom outlet
Domed glass head with
large side port opening
Rugged stainless steel pipe
support frame on casters
for mobility
Adjustable height flask support
Available with Lexan safety
shields

For heating/cooling
circulators, see
listing starting on
page 240.
Contact ACE for full circulator catalog.

Order Code

Each

30-Liter COMPLETE, Jacketed Flask,


with AIR DRIVEN Motor

6472-153

19633.14

50-Liter COMPLETE, Jacketed Flask,


with AIR DRIVEN Motor

6472-160

20820.72

6472-153

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Subject to Ace Discount (Page 4)

Net

Reactors/Large-Scale Pilot Plants

77

6472 PILOT PLANT REACTOR Cylindrical, 30 & 50 Liter Jacketed Flask, D


 omed Head
Complete cylindrical pilot plant reactor
on oneinch self-supporting, stainless steel
pipe mobile support frame: 30 liter frame size
measures 76 inches high, 26 inches wide, 26
inches deep; 50 liter size measures 84 inches
high, 26 inches wide, 26 inches deep. Note:
Frame shipped assembled.
Flask opening is 300 mm (12 inch), flatground plane flange. Bottom outlet is a flush
seal drain valve with oneinch beaded pipe
outlet. ORings supplied on valves are CAPFE
(silicone encapsulated with PTFE) & Kalrez,
for excellent chemical resistance. Flasks
with other bottom outlet types are available.
Jacket on flask is direct sealed at the top and
silicone rubber sealed at bottom. 35/25 o-ring
ball joint on inlet/outlet sealed tangentially.
Flask support is adjustable, vertically, to
allow room under flask for various outlet
configurations. 30L and 50L flasks sit on

a padded metal alloy (coated) ring secured


directly to the oneinch pipe frame.
Head is traditional domed style, with
eight openings. Five 45/50 and two 29/42
openings plus a 100 mm I.D. side port with
cap, CAPFE ORing and clamp.
Motor is secured on an epoxy coated
mounting plate over center 45/50 opening;
other openings are for condenser, thermo
probe, etc. Head is secured to flask with a
PTFE gasket and two-piece plastic coupling.
Maximum bolt-tightening torque for plastic
coupling (cold state) is 30 in-lbs. In place of
domed head, ACE offers a flat glass head
with ground-in joints, or a stainless steel
flat head that uses PTFE joint inserts.
Standard stirring motor is a compact,
air driven motor that develops 1.5 HP at 90
lbs. air pressure. As an optional item, ACE
also offers electric stirring: see No. 13554.

30 LITER
Order Code
FLASK, Jacketed, with 300mm Plane Flange
HEAD, Domed, with eight (8) openings
GLASS CAP, Side Port
CAPFE ORing, Side Port
CLAMP, Side Port, Quick Release
GASKET, Head, PTFE
COUPLING, Head, with Inserts and Hardware
WRENCH, Torque, 30 in-lbs.
SOCKET, 1/4 inch
DRAIN VALVE, Flush Seal
CLAMP, Drain Valve, 1 inch
CLAMP, Drain Valve, 2 inch
SWEEP ELBOW, 60, 1 inch Beaded Pipe
SUPPORT ASSEMBLY, Complete
TEMPERATURE MONITORING SYSTEM, Complete
AIR MOTOR, 1-1/2 Hp with 1/2 inch Motor Shaft
FILTER/REGULATOR/LUBRICATOR for Air Motor
AGITATOR, Lower, PTFE, Multipaddle
AGITATOR, Upper, PTFE, with four Pitched Blades, 152mm
STIRRING SHAFT, Polished Glass
BEARING, PTFE, 45/50
CONNECTOR, Beam Connects 1/2 inch Motor Shaft to Chuck
CHUCK, 28mm Connects Beam Connector to Stirring Shaft
COLLAR, with PTFE Gasket
ADAPTER, #7 29/42
ADAPTER, #11 45/50
ADAPTER, #15 45/50
ADAPTER, #15 45/50, with 4mm PTFE Stopcock
ADAPTER, #11 and #15 45/50
ADAPTER, Side Arm, 45/50 45/50 24/40
ADAPTER, Angle, 45/50 45/50
BUSHING, Nylon, #11
BUSHING, Nylon, #15, (4)
CONDENSER, 500mm, 45/50
CONDENSER, Cold Finger, 14mm O.D., 625mm
STOPPER, 45/50, (4)
CLAMP HOLDER
ROD, 6 inch x 1/2 inch for Temperature Monitor
GREASE, Krytox GPL
COMPLETE

6472-030
6530-45
15312-33
7855-880
6517-25
6525-51
6525-30
6525-60
6525-61
6472-245
8856-07
8856-11
8830-207
6472-331
8318-207
13370-10
13372-45
8091-36
8093-35
8080-14
8067-105
6472-155
6472-157
8127-28
5028-32
5030-60
8042-21
5274-22
5031-86
5040-96
5075-45
7506-02
7506-06
5945-76
5958-99
8250-20
11081-21
11166-22
8115-08
6472-153

Stirring rod is a 28mm (1-1/8 inch) O.D.,


precision ground and polished glass stirring
shaft with a pinned multi-paddle PTFE
agitator at bottom and a turbine blade PTFE
agitator higher on shaft for grease-free
operation with 8067 PTFE bearing. Note:
Steel reinforced PTFE shafts or ground
glass shafts can be supplied along with
other bearings.
Cooling coil is NOT supplied, but
available in copper tubing encapsulated
with PTFE; also available in 316 Stainless
Steel or Hastalloy C-276.
A temperature monitoring system, with
PTFE-covered type J thermocouple,
is supplied to give an instant readout of
temperature.
Jacket volume for 30L flask is 6.5 liters.
Jacket volume for 50L flask is 9.7 liters.

50 LITER
Each
6038.75
2562.18
107.78
28.63
98.23
326.26
1056.54
144.09
10.69
1010.52
112.13
150.55
65.97
2763.12
1028.28
411.74
237.98
613.84
628.06
402.64
320.08
55.71
89.89
73.09
32.61
51.58
50.57
117.64
119.50
169.62
123.30
11.39
12.35
382.96
92.87
44.68
84.80
8.36
59.40
19633.14

Order Code
6472-050
6530-45
15312-33
7855-880
6517-25
6525-51
6525-30
6525-60
6525-61
6472-245
8856-07
8856-11
8830-207
6472-332
8318-209
13370-10
13372-45
8091-36
8093-35
8080-18
8067-105
6472-155
6472-157
8127-28
5028-32
5030-60
8042-21
5274-22
5031-86
5040-96
5075-45
7506-02
7506-06
5945-76
5958-99
8250-20
11081-21
11166-22
8115-08
6472-160

Each
6821.55
2562.18
107.78
28.63
98.23
326.26
1056.54
144.09
10.69
1010.52
112.13
150.55
65.97
3072.70
1080.10
411.74
237.98
613.84
628.06
446.02
320.08
55.71
89.89
73.09
32.61
51.58
50.57
117.64
119.50
169.62
123.30
11.39
12.35
382.96
92.87
44.68
84.80
8.36
59.40
20820.72

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

78

Reactors/Large-Scale Pilot Plants

6472 Cylindrical Pilot Plants

Flat Head

Jacketed

30 & 50 Liter Reactors


With Stainless Steel Support

30 & 50 liter jacketed reactors


with b
ottom outlet
Stainless steel flat head
Rugged pipe support frame
on casters for mobility
Adjustable height top flask
support
Available with Lexan safety
shields

For heating/cooling
circulators, see
listing starting on
page 240.

Order Code

Each

30-Liter COMPLETE, Jacketed Flask,


with AIR DRIVEN Motor

6472-151

18664.29

50-Liter COMPLETE, Jacketed Flask,


with AIR DRIVEN Motor

6472-154

19811.28

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

6472-151

Subject to Ace Discount (Page 4)

Net

Reactors/Large-Scale Pilot Plants

79

6472 PILOT PLANT REACTOR Cylindrical, 30 & 50 Liter Jacketed Flask, F lat Head
Complete cylindrical pilot plant reactor
on one-inch, self-supporting, stainless
steel pipe mobile support frame: 30
liter size, measures 70 inches high, 26
inches wide, 26 inches deep; 50 liter size
measures 78 inches high, 26 inches wide,
26 inches deep. Note: Frame shipped
assembled.
Jacketed flask opening on 30 and 50
liter is 300 mm (12 inch), flat ground plane
flange. Bottom outlet on 30 and 50 liter
is a Flush Seal drain valve with oneinch
b e a d e d p i p e d r a i n o u t l e t . O R i n g s
supplied on valve are CAPFE (silicone
encapsulated with PTFE) & Kalrez, for
excellent chemical resistance. Flasks with
other bottom outlet valves are available.
Jacket on flask is direct sealed at top
and silicone rubber sealed at bottom.
35/25 ORing ball joint on inlet/outlet
sealed tangentially.

Flask support is adjustable, vertically,


to allow room under flask for various outlet
configurations. 30L and 50L flasks sit on
a padded metal alloy (coated) ring secured
directly to the oneinch pipe frame.
Unique flat 316 stainless steel head is
0.250 inches (6.4mm) thick, with seven
openings. Head has 45/50 PTFE center
joint insert, four 45/50 PTFE joint inserts,
and two 29/42 PTFE joint inserts.
Stainless steel head has a PTFE cover.
Maximum bolt-tightening torque of head
clamp (cold state) is 30 in-lbs. Motor is
secured on an epoxy coated mounting
plate over center 45/50 PTFE insert;
o t h e r o p e n i n g s a re f o r c o n d e n s e r,
thermoprobe, cooling coil, etc. Head is
secured to flask with PTFE gasket and
two-piece polymer coupling. In place of
flat head, ACE offers a domed glass head
with traditional raised joints.
30 LITER
Order Code

Stirring motor is a compact, air driven


motor that develops 1.5 HP at 90 lbs. air
pressure. As an optional item, ACE also
offers electronic stirring; see 13554.
Stirring rod on 30 L and 50 L size is a
28 mm (1-1/8 inch) O.D. precision ground
and polished glass stirring shaft with a
pinned multi-paddle PTFE agitator at
bottom and a turbine blade PTFE agitator
higher on shaft for grease-free operation
with 8067 PTFE bearing.
Optional cooling coil is available in
copper tubing encapsulated with PTFE;
also available in 316 Stainless Steel or
Hastalloy C-276.
A temperature monitoring system, with
PTFE-covered type J thermocouple,
is supplied to give an instant readout of
temperature.
Jacket volume for 30L flask is 6.5 liters.
Jacket volume for 50L flask is 9.7 liters.
50 LITER

Each

Order Code

Each

FLASK, Jacketed, with 300mm Plane Flange

6472-030

6038.75

6472-050

6821.55

HEAD, Flat, Stainless Steel, with 7 openings

6472-26

835.47

6472-26

835.47

HEAD COVER, 300mm, PTFE

6472-30

219.16

6472-30

219.16

JOINT INSERTS, PTFE 29/42 (2)

6412-07

90.78

6412-07

90.78

JOINT INSERTS, PTFE 45/50 (5)

6412-09

111.18

6412-09

111.18

DRAIN VALVE, Flush Seal

6472-245

1010.52

6472-245

1010.52

CLAMP, Drain Valve, 1 inch

8856-07

112.13

8856-07

112.13

CLAMP, Drain Valve, 2 inch

8856-11

150.55

8856-11

150.55

SWEEP ELBOW, 60, 1 inch Beaded Pipe

8830-207

GASKET, PTFE

6525-51

326.26

6525-51

326.26

COUPLING, with Inserts and Hardware

6525-30

1056.54

6525-30

1056.54

WRENCH, TORQUE, 30 in-lbs.

6525-60

144.09

6525-60

144.09

SOCKET, 1/4 inch

6525-61

10.69

6525-61

10.69

SUPPORT ASSEMBLY, Complete

6472-38

2702.41

6472-42

2971.40

TEMPERATURE MONITORING SYSTEM, Complete

8318-207

1028.28

8318-209

1080.10

AIR MOTOR, 1-1/2 HP with 1/2 inch Motor Shaft

13370-10

411.74

13370-10

411.74

FILTER/REGULATOR/LUBRICATOR for Air Motor

13372-45

237.98

13372-45

237.98

AGITATOR, Lower, PTFE, Multipaddle (178mm)

8091-36

613.84

8091-36

613.84

AGITATOR, Upper, PTFE, with 4 Pitched Blades, 152mm

8093-35

628.06

8093-35

628.06

STIRRING SHAFT, Polished Glass, 28mm

8080-14

402.64

8080-18

446.02

BEARING, PTFE, 45/50

8067-105

320.08

8067-105

320.08

CONNECTOR, Beam, Connects 1/2 inch Motor Shaft to Chuck

6472-155

55.71

6472-155

55.71

CHUCK, 28mm, Connects Beam Connector to Stirring Shaft

6472-157

89.89

6472-157

89.89

COLLAR, w/PTFE Gasket

8127-28

73.09

8127-28

73.09

ADAPTER, #7 29/42

5028-32

32.61

5028-32

32.61

ADAPTER, #11 45/50

5030-60

51.58

5030-60

51.58

ADAPTER, #15 45/50

8042-21

66.87

8042-21

66.87

ADAPTER, #15 45/50, w/4mm PTFE Stopcock

5274-22

117.64

5274-22

117.64

ADAPTER, #11 and #15 45/50

5031-86

119.50

5031-86

119.50

ADAPTER, Side Arm, 45/50 45/50 24/40

5040-96

169.62

5040-96

169.62

ADAPTER, Angle, 45/50 45/50

5075-45

123.30

5075-45

123.30

BUSHING, Nylon, #11

7506-02

11.39

7506-02

11.39

BUSHING, Nylon, #15 (4)

7506-06

12.35

7506-06

12.35

CONDENSER, 500mm, 45/50

5945-76

382.96

5945-76

382.96

CONDENSER, Cold Finger, 14mm O.D., 625mm

5958-99

92.87

5958-99

92.87

STOPPER, 45/50 (4)

8250-20

44.68

8250-20

44.68

CLAMP HOLDER

11081-21

84.80

11081-21

84.80

ROD, 6 inch x 1/2 inch for Temperature Monitor

11166-22

8.36

11166-22

8.36

GREASE, Krytox, GPL

8115-08

59.40

8115-08

59.40

COMPLETE

6472-151

65.97

18664.29

8830-207

6472-154

65.97

19811.28

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

80

Reactors/Large-Scale Pilot Plants

6473 Cylindrical Pilot Plants

100 Liter Reactor

Domed Head

Jacketed

With Stainless Steel Support

100 Liter Reactor with bottom


outlet
Domed glass head with large
side port opening
Rugged stainless steel pipe
support frame on casters for
mobility
Adjustable height flask support
Available with Lexan safety
shields

For heating/cooling
circulators, see
listing starting on
page 240.

Order Code
100 Liter COMPLETE, Jacketed Flask, with Motor

6473-66

Each
32441.89

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

6473-66

Subject to Ace Discount (Page 4)

Net

Reactors/Large-Scale Pilot Plants

81

6473 PILOT PLANT REACTOR Cylindrical, 100 Liter Jacketed Flask (12 inch Flange), D
 omed Head
Complete cylindrical pilot plant
reactor on self-supporting, mobile
support frame on oneinch stainless
steel pipe, measures 94 inches high,
28 inches wide, 28 inches deep. Note:
Frame shipped assembled.
Flask opening is 300mm (12 inch)
flat-ground plane flange. Bottom outlet
is a flush seal drain valve with oneinch
beaded
drain
discharge.
ORings
supplied on valve are CAPFE (silicone
encapsulated with PTFE) & Kalrez, for
excellent chemical resistance.
Jacket on flask is direct sealed at
top and silicone sealed at bottom.
35/25 oring ball joints on inlet/outlet
ports sealed tangentially. Flask sits
on a padded metal alloy (coated) ring

secured directly to oneinch pipe, and is


adjustable, vertically, to allow room for
various outlet configurations.
Head is traditionally domed style, with
eight openings: five 45/50, two 29/42
plus one 100 mm I.D. side port.
Motor is secured on black epoxy
coated mounting plate over center
45/50 opening on head; other openings
are for condenser, thermoprobe, cooling
coil, etc. Head is secured to flask with
PTFE gasket and two-piece plastic
coupling. Maximum bolt tightening
torque for coupling (cold state) is 30 inlbs. In place of domed head, ACE offers
a flat glass or flat stainless steel head.
Stirring motor is heavy duty, 1/2 HP
electric motor for hazardous area duty.

Motor shaft is 5/8 inch O.D. Controller


operates on 120 volts 50/60 Hz. (Air
motor available, call for details).
28mm (1-1/8 inch) O.D. precision
ground and polished glass stirring shaft
with a pinned multi-paddle PTFE
agitator at bottom and a turbine blade
PTFE agitator higher on shaft for greasefree operation with 8067 PTFE bearing.
Optional cooling coil is 1/2 inch O.D.
copper tubing encapsulated with PTFE;
also available in 316 stainless steel or
Hastalloy C-276.
A temperature monitoring system, with
PTFE-covered type J thermocouple,
is supplied to give an instant readout of
temperature.
Jacket volume of flask is 26 liters.

100 LITER (12 inch Flange)

Order Code

Each

FLASK with 300mm Plane Flange, 100L


HEAD, Domed, with Eight Openings
GLASS CAP, 100mm
CAPFE ORing, 100mm
CLAMP, Quick Release, 100mm
GASKET, PTFE
COUPLING, with Inserts and Hardware
WRENCH, TORQUE, 62 in-lbs.
SOCKET 1/2 inch
DRAIN VALVE, Flush Seal
CLAMP, Drain Seal, 1 inch
CLAMP, Drain Seal, 2 inch
SWEEP ELBOW, 60, 1 inch BP
SUPPORT ASSEMBLY, Complete
TEMPERATURE MONITORING SYSTEM, Complete
STIRRER MOTOR AND CONTROLLER, 1/2 HP
AGITATOR, Lower, PTFE, Multipaddle, 178mm
AGITATOR, Upper, PTFE, with 4 Pitched Blades, 152mm (1)
STIRRING SHAFT, Polished Glass, 28mm
BEARING, PTFE, 45/50
CONNECTOR, Beam, Connects 5/8 inch Motor Shaft to Chuck
CHUCK, 28mm, Connects Beam Connector to Stirring Shaft
COLLAR, with PTFE Gasket
ADAPTER, #7 24/40
ADAPTER, #11 45/50
ADAPTER, #15 29/42 (2)
ADAPTER, #15 45/50
ADAPTER, #15 45/50, with 4mm PTFE Stopcock
ADAPTER, #11 and #15 45/50
ADAPTER, Side Arm, 45/50 45/50 24/40
ADAPTER, Angle, 45/50 45/50
ADAPTER, Offset, 45/50 45/50
BUSHING, Nylon, #11
BUSHING, Nylon, #15 (3)
CONDENSER, 500mm, 45/50
CONDENSER, Cold Finger, 14mm O.D., 625mm

6473-09
6530-45
15312-33
7855-880
6517-25
6525-51
6525-30
6525-60
6525-61
6472-245
8856-07
8856-11
8830-207
6473-35
8318-209
13554-55
8091-36
8093-35
8080-30
8067-105
6472-156
6472-157
8127-28
5028-30
5030-19
5030-42
8042-21
5274-22
5040-96
5031-86
5075-45
5268-21
7506-02
7506-06
5945-76
5958-99
8250-14
8250-20
11079-24
11081-21
11166-37
11175-23
8115-08
6473-66

14341.21

STOPPER, 29/42 (2)


STOPPER, 45/50 (4)
CLAMP, Chain
CLAMP HOLDER, Pilot Plant (2)
SUPPORT ROD, 1/2 inch diameter, 12 inch long (2)
END-TO-END ROD CONNECTOR
GREASE, Krytox GPL
COMPLETE

2562.18
107.78
28.63
98.23
326.26
1056.54
144.09
10.69
1010.52
112.13
150.55
65.97
3885.78
1080.10
3369.54
613.84
628.06
586.44
320.08
54.09
89.89
73.09
27.61
62.97
45.73
50.57
117.64
169.62
119.50
123.30
109.58
11.39
12.35
382.96
92.87
25.05
44.68
51.23
84.80
13.60
19.87
59.40
32441.89

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

82

Reactors/Large-Scale Pilot Plants

6559 Low-Profile Pilot Plant

50 Liter Reactor

Flat Head

Jacketed

With Stainless Steel Support

Portable 50 liter jacketed


reactor with bottom outlet
Low profile for walk-in hoods
Rugged pipe support frame
on casters for mobility
Also available with domed
head
Also available with threepost stand
Available with Lexan safety
shields
Stainless steel flat heads

For heating/cooling
circulators, see
listing starting on
page 240.

6559-10

Order Code
50 Liter COMPLETE, Jacketed Flask, with ELECTRIC Motor

6559-10

Each
24683.76

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Subject to Ace Discount (Page 4)

Net

Reactors/Large-Scale Pilot Plants

83

6559 PILOT PLANT REACTOR Low-Profile, 50 Liter Jacketed Flask, F lat Head
Complete cylindrical pilot plant reactor on
1inch stainless steel pipe, self supporting,
mobile support frame; measures 22 inches
wide by 22 inches deep x 68 inches high. Note:
Frame shipped assembled.
This system has the new low-profile 50L
jacketed flask which has a reduced height vs.
the standard 50L flask by 25%. The reactor
has the same capacity as the standard 50L
but the shorter frame and flask enable it to fit
into hoods easier. Jacketed flask has a 300mm
(12inch) opening, flat ground plane flange top.
Bottom outlet is a flush seal drain valve with
one-inch beaded pipe outlet. ORings provided
for valve are CAPFE, (silicone encapsulated
with PTFE) for excellent chemical resistance.
Flasks with other bottom outlet valves are

available. Jacket on flask is direct sealed at top


and silicone rubber sealed at bottom. 35/25
ORing ball joint inlet/outletconnections ae
sealed tangentially.
Bottom padded flask support is adjustable
to allow room under flask for various outlet
configurations.
Unique flat 316 stainless steel head is 0.250
inches (6.4mm) thick, with seven openings.
Head has 45/50 PTFE center joint insert, four
45/50 PTFE joint inserts, and two 29/42
PTFE joint inserts. Stainless steel head has a
PTFE cover. Maximum bolt-tightening torque
of head clamp (cold state) is 30 in-lbs. Motor
is secured on an epoxy coated mounting
plate over center 45/50 PTFE insert; other
openings are for condenser, thermoprobe,

50 LITER

Order Code

FLASK, Jacketed, with 300mm Plane Flange and 2 inch BP Bottom Opening
HEAD, Flat, Stainless Steel, with 7 openings
FLAT HEAD COVER, 300mm, PTFE
JOINT INSERTS, PTFE 29/42 (2)
JOINT INSERTS, PTFE 45/50 (5)
DRAIN VALVE, Flush Seal
CLAMP, Drain Valve, 1 inch
CLAMP, Drain Valve, 2 inch
SWEEP ELBOW, 60, 1 inch Beaded Pipe
GASKET, PTFE
COUPLING, with Inserts and Hardware
WRENCH, TORQUE, 30 in-lbs.
SOCKET, 1/4 inch
SUPPORT ASSEMBLY, Complete
J-KEM TEMPERATURE MONITORING SYSTEM, Complete
PROBE T 36 inch
EXTENSION CORD, 11-foot
1/2 HP ELECTRIC MOTOR
CONTROLLER
SIDE DRIVE GEAR BOX
AGITATOR, Lower, PTFE, Multipaddle (178mm)
AGITATOR, Upper, PTFE, with 4 Pitched Blades, 152mm
STIRRING SHAFT, Polished Glass, 28mm, 40 inch Length
BEARING, PTFE, Inner Body, 45/50
GLASS FILLED PTFE BUSHING
GLASS FILLED PTFE LOCK-NUT
SADDLE O-RING
GLASS BODY ONLY, 45/50-36
CONNECTOR, Beam, Connects 5/8-inch Motor Shaft to Chuck
CHUCK, 28mm, Connects Beam Connector to Stirring Shaft
COLLAR, w/PTFE Gasket
ADAPTER, #7 29/42
ADAPTER, #11 45/50
ADAPTER, #15 45/50
ADAPTER, #15 45/50, w/4mm PTFE Stopcock
ADAPTER, #11 and #15 45/50
ADAPTER, Side Arm, 45/50 45/50 24/40
ADAPTER, Angle, 45/50 45/50
BUSHING, Nylon, #11
BUSHING, Nylon, #15 (4)
CONDENSER, 500mm, 45/50
CONDENSER, Cold Finger, 14mm O.D., 625mm
STOPPER, 45/50 (4)
ADAPTER, Offset, 45/50 45/50
CLAMP, Chain
END-TO-END ROD CONNECTOR
CLAMP HOLDER (2)
ROD, 6 inch x 1/2 inch for Temperature Monitor (2)
GREASE, Krytox, GPL
COMPLETE

6543-30
6472-26
6472-30
6412-07
6412-09
6472-245
8856-07
8856-11
8830-207
6525-51
6525-30
6525-60
6525-61
6472-334
12327-03
12180-11
12190-11
13554-50
13554-26
13557-10
8091-36
8093-35
8080-12
8067-55
8067-58
8067-60
8067-65
5030-78
6472-156
6472-157
8127-28
5028-32
5030-60
8042-21
5274-22
5031-86
5040-96
5075-45
7506-02
7506-06
5945-76
5958-99
8250-20
5268-21
11079-24
11175-23
11081-21
11166-22
8115-08
6559-10

cooling coil, etc. Head is secured to flask with


PTFE gasket and two-piece polymer coupling.
In place of flat head, ACE offers a domed glass
head with traditional raised joints.
Stirring motor is high powered, 1/2HP
explosion proof motor complete with controller
box and with a side drive gear box to save even
more head space. Stir rod is 28mm (11/8inch)
O.D. precision ground and polished glass shaft
with a pinned multi-paddle PTFE agitator at
the bottom and a turbine blade PTFE agitator
in the middle of the shaft running through an
ACE Tru-Bore bearing.
A J-Kem temperature monitor and 36inch
T thermocouple is included to give an instant
readout of vessel temperature. Jacket volume
of flask is 14.25 liters.

Each
8228.25
835.47
219.16
90.78
111.18
1010.52
112.13
150.55
65.97
326.26
1056.54
144.09
10.69
2914.40
391.00
62.00
38.80
2276.62
1092.92
651.97
613.84
628.06
378.55
114.72
75.44
21.59
30.45
77.88
54.09
89.89
73.09
32.61
51.58
50.57
117.64
119.50
169.62
123.30
11.39
12.35
382.96
92.87
44.68
109.58
51.23
19.87
84.80
8.36
59.40
24683.76

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

84

Reactors/Large-Scale Pilot Plants

6474 Spherical Pilot Plants

Domed Head

50/72/100 Liter Reactors

Unjacketed

With Stainless Steel Support

50, 72 & 100 liter reactors with


bottom outlet
Internal heat exchange coil*
Rugged stainless steel pipe
support frame on casters for
mobility
Adjustable height flask supports
Available with Lexan safety
shields

*Supplied with PTFE-coated copper


tubing; also available in Hastalloy C-276
or 316 stainless steel.

Order Code

Each

50-Liter COMPLETE, Unjacketed Flask, with Motor

6474-60

17615.70

72-Liter COMPLETE, Unjacketed Flask, with Motor

6474-64

19224.40

100-Liter COMPLETE, Unjacketed Flask, with Motor

6474-68

24262.69

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

6474-60

Subject to Ace Discount (Page 4)

Net

Reactors/Large-Scale Pilot Plants

85

6474 PILOT PLANT REACTOR Spherical, 50/72/100 Liter Unjacketed Flask (8 inch Flange), D
 omed Head
Complete spherical pilot plant reactor on
self-supporting, mobile oneinch stainless steel
pipe support frame: 50 liter size measures 72
inches high, 26 inches wide, 26 inches deep;
72 liter size measures 85 inches high, 32 inches
wide, 32 inches deep; 100 liter size measures
85 inches high, 40 inches wide, 40 inches deep.
Note: Frame shipped assembled.
Flask opening is 200 mm (8 inches); Schottstyle flange with ORing groove as center neck
(supplied with 7855-884 CAPFE ORing); three
45/50 side necks on all capacities. Bottom
outlet is a 0-20 mm adjustable opening threaded
valve on all sizes. ORings supplied on valves
are Chemraz (PTFE elastomeric material) for
excellent chemical resistance. Other bottom
outlet valves available, contact Ace for options.

Black epoxy coated aluminum flask support


plate is adjustable, vertically, to allow room
under flask for various outlet configurations.
Domed style head has one 45/50 center
joint, two 29/42 side joints and connects
to flask head with 6517 quick release clamp.
Motor is secured on black epoxy coated
mounting plate over center 45/50 opening
on head; other openings are for condenser,
thermoprobe, cooling coil, etc.
Stirring motor is a heavy duty, 1/4 HP (50 L
and 72 L), 1/2 HP (100 L) electric motor for
hazardous area duty. Motor shaft is 5/8 inch
O.D. Controller operates on 120 volts, 50/60Hz.
(Air motor available, call for quotation).
Precision ground and polished glass stirring
shaft: 50 L Reactor has a 19 mm O.D. rod; 72 L

and 100 L have 28 mm (1-1/8 inch) O.D. rods,


with a pinned multi-paddle PTFE agitator
at bottom and a turbine blade PTFE agitator
higher on shaft for grease-free operation with
8067 PTFE bearing.
Cooling coil is 3/8-inch O.D. copper tubing
encapsulated with PTFE; also available in 316
stainless steel or Hastalloy C-276.
A digital temperature control system is
supplied to control heating mantles. This prevents
over-heating and overshoot, and gives an
instant readout of temperature.

50 LITER

72 LITER

100 LITER

(8 inch I.D. Flange)


Order Code
Each

(8 inch I.D. Flange)


Order Code
Each

(8 inch I.D. Flange)


Order Code
Each

FLASK, with Side Necks and Bottom Valve

6530-10

2917.90

6530-17

2883.44

6530-23

5066.97

HEAD, 45/50 Center Neck, 29/42 Side Necks


CLAMP, Quick Release

6530-33

594.98

6530-33

594.98

6530-33

594.98

145.09
6517-31
813.52
12050-41
(370w-115v)
1394.13
12041-40
(1-1200w-115v)
2793.00
6474-370
2908.50
6472-73
2670.40
13554-45

318.61
8091-26

290.38
8076-45

145.09
6517-31
1121.28
12050-43
(1300w-230v)
1771.47
12041-42
(2-1800w-230v)
3021.00
6474-371
2908.50
6472-75
2670.40
13554-45

616.11
8091-34

402.64
8080-14

145.09
6517-31
1586.14
12050-45
(1600w-230v)
2335.70
12041-44
(3-1400w-230v)
3534.01
6474-372
2908.50
6472-75

3369.54
13554-55

616.11
8091-34
583.27
8093-25

402.64
8080-14

BEARING, PTFE, 45/50


CHUCK, Flex-Grip, 19mm
CONNECTOR, Beam, Connects 5/8 inch Motor Shaft to Chuck
CHUCK, 28mm, Connects Beam Connector to Stirring Shaft
COLLAR, with PTFE Gasket
COIL, Cooling/Heating, Copper/PTFE, 3/8 inch

8067-30

269.05

8067-105

320.08

8067-105

320.08

8124-23

8127-20
12067-61

152.25

6472-156
6472-157
8127-28
12067-63

6472-156
6472-157
8127-28
12067-65

ADAPTER, #11 29/42 (2)

5030-24

44.98

5030-24

44.98

5030-24

ADAPTER, #15 45/50

8042-21

50.57

8042-21

50.57

8042-21

50.57

ADAPTER, #15 45/50, with 4mm PTFE Stopcock

5274-22

117.64

5274-22

117.64

5274-22

117.64

ADAPTER, #11 and #15 45/50

5031-86

119.50

5031-86

119.50

5031-86

119.50

ADAPTER, Side Arm, 45/50 45/50 24/40

5040-96

169.62

5040-96

169.62

5040-96

169.62

ADAPTER, Angle, 45/50 45/50

5075-45

123.30

5075-45

123.30

5075-45

123.30

ADAPTER, Offset, 45/50 45/50


BUSHING, Nylon, #11
BUSHING, Nylon, #15 (4)

5268-21

109.58

5268-21

109.58

5268-21

109.58

7506-02
7506-06

11.39

11.39
12.35

7506-02
7506-06

11.39

12.35

7506-02
7506-06

CONDENSER, 500mm, 45/50


CONDENSER, Cold Finger, 14mm O.D., 625mm

5945-76

382.96

5945-76

382.96

5945-76

382.96

5958-99

92.87

5958-99

92.87

5958-99

92.87

STOPPER, 45/50 (3)


CLAMP, Chain
CLAMP HOLDER, Pilot Plant (2)
SUPPORT ROD, 1/2 inch diameter, 12 inch long (2)
SUPPORT ROD, 1/2 inch diameter, 18 inch long (2)
END-TO-END CONNECTOR
GREASE, Krytox GPL
COMPLETE

8250-20

44.68

8250-20

44.68

8250-20

44.68

11079-24
11081-21
11166-37

11175-23
8115-08
6474-60

51.23

11079-24
11081-21

11166-25
11175-23
8115-08
6474-64

51.23

11079-24
11081-21

11166-25
11175-23
8115-08
6474-68

51.23

MANTLE, Bottom, Low Profile, w/Twist-Lock Connector


(Wattage-Voltage)
MANTLE, Girdle, Low Profile, w/Twist-Lock Connector
(Wattage-Voltage)
SUPPORT ASSEMBLY, Complete
TEMPERATURE CONTROL SYSTEM, Complete
STIRRING MOTOR AND CONTROLLER, 1/4 HP
STIRRING MOTOR AND CONTROLLER, 1/2 HP
AGITATOR, Lower, PTFE, Multipaddle, 140mm
AGITATOR, Lower, PTFE, Multipaddle, 140mm
AGITATOR, Upper, PTFE, with 4 Pitched Blades, 140mm
STIRRING SHAFT, Polished Glass, 19mm
STIRRING SHAFT, Polished Glass, 28mm

36.68
892.76

84.80
11.66

19.87
59.40
17615.70

54.09
89.89
73.09
995.02

84.80

14.69
19.87
59.40
19224.40

54.09
89.89
73.09
1045.32
44.98

12.35

84.80

14.69
19.87
59.40
24262.69

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

86

Reactors/Large-Scale Pilot Plants

6474 Spherical Pilot Plants

200 Liter Reactor

Domed Head

Unjacketed

With Stainless Steel Support

200 liter reactor with bottom


outlet
Internal heat exchange coil*
Rugged stainless steel pipe
support frame on casters for
mobility
Adjustable height flask support
Available with Lexan safety
shields

*Supplied with PTFE-coated copper


tubing; also available in Hastalloy C-276
or 316 stainless steel.

6474-75

Order Code
200 Liter COMPLETE, Unjacketed Flask, with ELECTRIC Motor

6474-75

Each
35282.07

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Subject to Ace Discount (Page 4)

Net

Reactors/Large-Scale Pilot Plants

87

6474 PILOT PLANT REACTOR Spherical, 200 Liter Unjacketed Flask (12 inch Flange), D
 omed Head
Complete cylindrical pilot plant reactor on
self-supporting, mobile support frame with
oneinch stainless steel pipe. Measures 90
inches high, 42 inches wide, 42 inches deep.
Note: Frame shipped assembled.
Flask opening is 300 mm (12 inch) flatground flange. Bottom outlet is a flush seal
drain valve with oneinch beaded drain
discharge. ORing supplied on valve is a
CAPFE (silicone encapsulated with PTFE),
and Kalrez for excellent chemical resistance.
Flask has 100mm I.D. side port, angled 45
degrees.
Black epoxy coated aluminum flask
support plate is adjustable, vertically, to
allow room under flask for various outlet

configurations. Upper support brackets


supplied to stabilize flask.
Head is traditional domed style, with
seven openings; five 45/50, two 29/42.
Motor is secured on black epoxy coated
mounting plate over center 45/50 opening
on head; other openings are for condenser,
thermoprobe, cooling coil, etc. Head is
secured to flask with PTFE gasket and
plastic coupling. Maximum bolt tightening
torque for coupling (cold state) is 30 in-lbs.
Stirring motor is heavy duty, 1/2 HP
electric motor for hazardous area duty.
Motor shaft is 5/8 inch O.D. Controller
operates on 120 volts 50/60Hz. (Air motor
available, call for details.)

Features a 28 mm (1-1/8 inch) O.D.


precision ground and polished glass stirring
shaft with a pinned multi-paddle PTFE
agitator at bottom and a turbine blade PTFE
agitator higher on shaft for grease-free
operation with 8067 PTFE bearing.
Cooling coil is 1/2 inch O.D. copper tubing
encapsulated with PTFE; also available in
316 stainless steel or Hastalloy C-276.
A digital temperature control system
is supplied to control heating mantles. This
prevents over-heating and overshoot, and gives
an instant readout of temperature.

200 LITER
(12 inch I.D. Flange)
Order Code
FLASK, with Side Necks and 2 inch Beaded Pipe Bottom Opening
HEAD, Domed, with Seven Openings
GASKET, PTFE
COUPLING, with inserts and hardware
WRENCH, Torque, 30 in-lbs
SOCKET, 1/4 inch
DRAIN VALVE, Flush Seal
CLAMP, Drain Valve, 1 inch
CLAMP, Drain Valve, 2 inch
SWEEP ELBOW, 60, 1 inch BP
CAP, 4 inch
ORing, CAPFE, for 4 inch Flange
CLAMP, Quick Release
MANTLE, Bottom, Aluminum, w/hole, 4-2000x-230v, wired w/plugs
SUPPORT ASSEMBLY, Complete
TEMPERATURE CONTROL SYSTEM, Complete
STIRRING MOTOR AND CONTROLLER, 1/2 HP
AGITATOR, Lower, PTFE, Multipaddle, 178mm
AGITATOR, Upper, PTFE, with 4 Pitched Blades, 152mm
STIRRING SHAFT, Polished Glass, 28mm
BEARING, PTFE, 45/50
CONNECTOR, Beam, Connects 5/8 inch Motor Shaft to Chuck
CHUCK, 28mm, Connects Beam Connector to Stirring Shaft
COLLAR, w/PTFE Gasket
COIL, Cooling/Heating, Copper/PTFE, 1/2 inch
ADAPTER, #15 29/42 (2)
ADAPTER, #15 45/50
ADAPTER, #15 45/50, with 4mm PTFE Stopcock
ADAPTER, #11 and #15 45/50
ADAPTER, Side Arm, 45/50 45/50 24/40
ADAPTER, Angle, 45/50 45/50
ADAPTER, Offset, 45/50 45/50
BUSHING, Nylon, #11
BUSHING, Nylon, #15 (4)
CONDENSER, 500mm, 45/50
CONDENSER, Cold Finger, 14mm O.D., 625mm
STOPPER, 45/50 (3)
CLAMP, Chain
CLAMP HOLDER, Pilot Plant (2)
SUPPORT ROD,1/2 inch diameter, 18 inch long
END-TO-END CONNECTOR
GREASE, Krytox GPL
COMPLETE

6474-29
6472-23
6525-51
6525-30
6525-60
6525-61
6472-245
8856-07
8856-11
8830-207
15312-33
7855-880
6517-25
12053-78
6474-373
6472-83
13554-55
8091-36
8093-35
8080-24
8067-105
6472-156
6472-157
8127-28
12067-68
5030-42
8042-21
5274-22
5031-86
5040-96
5075-45
5268-21
7506-02
7506-06
5945-76
5958-99
8250-20
11079-24
11081-21
11166-25
11175-23
8115-08
6474-75

Each
8410.93
2379.08
326.26
1056.54
144.09
10.69
1010.52
112.13
150.55
65.97
107.78
28.63
98.23
4360.53
4208.23
3514.35
3369.54
613.84
628.06
458.41
320.08
54.09
89.89
73.09
2011.00
45.73
50.57
117.64
119.50
169.62
123.30
109.58
11.39
12.35
382.96
92.87
44.68
51.23
84.80
14.69
19.87
59.40
35282.07

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

88

Reactors/Large-Scale Pilot Plants

The
Impresario I
Reactor
Controller
New
6458-10 Impresario I
Reactor Control System

Introducing the Impresario I, Ace Glasss new,


expandable reactor control system. The Impresario I
controls and monitors various reaction parameters via
an expandable hardware unit and highly configurable
Windows-based software (XP and Windows7).
The base configuration includes the ability to control
hardware from equipment manufacturers such as
JKem, Heidolph, IKA, and Julabo.
Users also have the option of creating reaction recipes
via an easy-to-use graphical interface.
Call Ace today to discuss a quotation for a new
reaction system, or for an Impresario I configuration to
work with your existing equipment.

SPECIFICATIONS (Base Configuration)


SYSTEM PC running Windows XP, Windows 7 or higher
REQUIREMENTS: 250 MB of disk space
Minimum 1 GB RAM
DRIVERS INCLUDED FOR: Julabo recirculators
Heidolph and IKA digital stirring motors
SOFTWARE FEATURES: Configurable emergency stop
Configurable safety alarm actions
Graph single parameter over time for each
monitored parameter
Creates CSV (comma-delimited file) data file
PARAMETERS pH via probe
MONITORED: Stirrer speed
Stirrer torque
Vacuum/pressure via onboard transducer
(35 psi maximum)
Temperature of circulator oil
Temperature of reaction via probe
PARAMETERS Temperature via chiller
CONTROLLED: Stirring speed
Pressure and vacuum via proportioning valve
(not included call for details)
ITEMS Impresario controller
INCLUDED: USB cable for connection to PC
Impresario software

Base system includes Impresario I


controller, USB cable, and all software
and
standard
drivers.
Reactor,
recirculator, computer, cables and other
peripherals must be ordered separately.

ITEMS PC not sold by Ace; Netbook is available,


NOT
however only the Impresario software is supINCLUDED:
ported
Cables for connection to peripherals
Proportioning valve (see Ace 14066 family)
Recirculator, stir motor, vacuum pump, liquid
pump, syringe pump, etc.
Drivers for equipment other than those listed
above (can be supplied as custom orders)

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Subject to Ace Discount (Page 4)

Net

Reactors/Large-Scale Pilot Plants

89

10/20L Pilot Plant Packages


A

ce Glass combines our expertise in


Pilot Plant-Kilo Scale Reactors with
Julabos expertise in recirculating
chillers to provide a total, convenient solu-

tion and package. Aces glass reactors and


Julabos Presto series chillers are a perfect
combination for your large scale, pilot or
production process needs.

Key Components for


10L Pilot Plant System

Key Components for


20L Pilot Plant System

Item Description
Order Code
10L Jacketed Flask
6524-73
Domed Head, 7 ports
6530-37
Stainless Steel Stand
6472-329
Digital Stirring Motor
13504-41
8091-10
PTFE Agitator (Lower)
PTFE Agitator (Upper)
8093-12
Stirring Shaft, 19mm
8076-43
Condenser, 300mm, 29/42 5945-24
Julabo LH85 Circulator
12262-38
Hose Clamps (2)
13010-01
Julabo Hoses (2)
12677-15
Julabo PT100 Sensor
12307-44
Julabo 2L Expansion Tank
12497-02

Item Description
Order Code
20L Jacketed Flask
6472-16
Domed Head, 7 ports
6530-37
Bottom Drain Valve
6472-245
Drain Valve Clamp 1-inch
8856-07
Drain Valve Clamp 2-inch
8856-11
Stainless Steel Stand
6472-329
Digital Stirring Motor
13504-41
PTFE Agitator (Lower)
8091-10
PTFE Agitator (Upper)
8093-12
Stirring Shaft, 19mm
8076-40
Condenser, 300mm, 24/40 5946-18
Julabo LH85 Circulator
12262-38
Hose Clamps (2)
13010-01
Julabo Hoses (2)
12677-15
Julabo PT100 Sensor
12307-48
Julabo 2L Expansion Tank
12497-02

47578.28

Complete 10L System


Order Code: 10000-10

50807.50

Complete 20L System


Order Code: 10000-20

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

90

Reactors/Large-Scale Pilot Plants

30/50L Pilot Plant Packages


66708.

99

Complete 30L System


Order Code: 10000-30

68328.91

Complete 50L System


Order Code: 10000-50

Key Components for


30L Pilot Plant System
Item Description
30L Jacketed Flask
Domed Head, 8 ports
PTFE Head Gasket, 300mm
Bottom Drain Valve
Drain Valve Clamp 1-inch
Drain Valve Clamp 2-inch
Three-Post Stand
Stirring Motor, 1/2-HP XP
Motor Controller
PTFE Agitator (Lower)
PTFE Agitator (Upper)
Stirring Shaft, 28mm
Connect Beam Coupling
Chuck, 28mm
Condenser, 500mm
Condenser, Cold Finger
Julabo LH50 Circulator
Hose Clamps (2)
Julabo Hoses (2)
Julabo PT100 Sensor
Julabo 5L Expansion Tank

Order Code
6472-030
6530-45
6525-51
6472-245
8856-07
8856-11
6473-51
13554-50
13554-26
8091-36
8093-35
8080-14
6472-156
6472-157
5945-76
5958-99
12262-40
13010-01
12677-15
12307-48
12497-05

Key Components for


50L Pilot Plant System
Item Description
50L Jacketed Flask
Domed Head, 8 ports
PTFE Head Gasket, 300mm
Bottom Drain Valve
Drain Valve Clamp 1-inch
Drain Valve Clamp 2-inch
Three-Post Stand
Stirring Motor, 1/2-HP XP
Motor Controller
PTFE Agitator (Lower)
PTFE Agitator (Upper)
Stirring Shaft, 28mm
Connect Beam Coupling
Chuck, 28mm
Condenser, 500mm
Condenser, Cold Finger
Julabo LH50 Circulator
Hose Clamps (2)
Julabo Hoses (2)
Julabo PT100 Sensor
Julabo 5L Expansion Tank

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Order Code
6472-050
6530-45
6525-51
6472-245
8856-07
8856-11
6473-51
13554-50
13554-26
8091-36
8093-35
8080-18
6472-156
6472-157
5945-76
5958-99
12262-40
13010-01
12677-15
12307-48
12497-05

Subject to Ace Discount (Page 4)

Net

Reactors/Large-Scale Filter Reactors

91

Process Scale
Filtration Apparatus
and Filter Reactors
Ace Glass fabricates bench scale filtration
apparatus and reactors as standard products.
ACE also fabricates kilo scale filter reactors such
as the one pictured here.
ACE has produced units from 150mL up to as
large as 200L custom units. ACE has typically
produced 20L, 30L and 50L filter apparatus as
well for various applications such as Nutsche
filters, etc. All filter reactors are built on corrosion
resistant stainless steel stands with locking, rolling
casters for portability. All borosilicate heavy-wall
glass bodies with either glass or PTFE bottom
units. Many bottom and side outlet valve styles
are available such as our flush seal or ZDS valves.
Various agitator styles exist in either stainless steel
or PTFE and custom fabrication is possible. Glass
vessels can be standard single wall or jacketed
double wall. Heads can be stainless steel or glass
domed or flat head style.
Filter apparatus stands can be fabricated from
anodized aluminum or stainless steel with
powder coated components. Various sizes and
types of stir motors are available, including UL
classified Hazardous duty motors that meet
either; Class I, Div 1, Group D and Class II, Div
I, Group F&G atmospheres.

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

92

Components / Flasks
Easy Action
Bottom Valve

ZDS Valve

Flush Seal

Beaded

Valve Types
for
Reaction Flasks

Sink Type

Piston Type

Easy Action Bottom Valve

Piston Type Valve

Flask has Easy Action Plug bottom outlet with Chemraz orings
for draining contents. Bottom outlet has size 35/25 oring ball joint
connection. Supplied with one 7855884 CAPFE oring (PTFE
encapsulated silicone oring). Plain silicone orings also available.

Flask has 35/25 or 28/15 oring ball joint on outlet and utilizes a sealedin
threaded stopcock assembly that rotates CLOSED into the bottom of
the flask thereby offering nearly zero dead space. Turn stopcock handle
counterclockwise and piston plunger retracts to allow contents to
drain. Drain opening is approximately 15mm. Piston plunger supplied
with FETFE orings (two 7855726, one 7855721); Chemraz orings
can be offered as replacements.

Sink Type Valve


Flask is fabricated with a #36 AceThred on bottom. The allPTFE valve
is inserted into the AceThred. A stainless steel handle is then secured
to the drain tube. By rotating the handle, plug rises into the flask and
contents drain through three (3) 1/2 inch wide x 1-1/2 inch long slit
openings. Rotate handle in opposite direction and plug seals at bottom
of flask, with NO dead space. Supplied with two Chemraz orings: one
7859540, to secure valve in #36 AceThred; the other, 7859542, on
bottom of plug to make seal at bottom of flask.

ZDS Valve
Flask has new Zero Dead Space (ZDS) valve. When in the full open
position, the ZDS valve allows for complete product drainage, and has
no hang-up where material can be trapped or suspended. The product
drains through openings in the valve stem, and will completely empty
including dissolved and small, solid particles. When closed, the valve
plug seals flush to the bottom of the flask. The valve is available in two
standard sizes. All wetted parts are borosilicate glass or inert PTFE.
The PTFE plug stem orings are made from Chemraz, so the valve can
handle almost any type of material or chemical.

Beaded
Flask is supplied with a one-inch beaded pipetype flange extension off
bottom for connection to a 020 mm threaded PTFE stopcock as the
outlet. Stopcock assembly has a mating one-inch beaded flange that
connects to extension off bottom via a Viton lined coupling. Takeoff on
stopcock is one-inch O.D. tubing. Drain assembly plug supplied with
FETFE orings; Chemraz orings can be offered as replacements. ACE
can supply the takeoff with beaded flange, AceThred, hose connection,
etc.; call or email for quotation.

Flush Seal Valve


Flask is fabricated with a two-inch beaded valve seat, for 30L and 50L.
The plug, with a CAPFE oring, is inserted into valve seat and s ecures
within a coupling. By rotating the handle, plug rises into the flask and
seals to afford zero dead space. Back thread out to drain through
oneinch beaded pipe angled side port. Supplied with CAPFE oring for
seal at flask, two Kalrez orings supplied on valve stem. Other oring
materials available.

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Subject to Ace Discount (Page 4)

Net

Components / Flasks

93

6472 FLASK Reaction, Pilot Plant, Cylindrical, with Piston Type Drain
Similar to flask supplied with 6472 pilot plant reactor systems except this flask has a
bottom outlet with oring ball joint and utilizes a sealed-in threaded PTFE stopcock
assembly that rotates CLOSED into the bottom of the flask thereby offering nearly zero
dead space. Turn stopcock handle counterclockwise and piston plunger retracts to
allow contents to drain. Drain opening is approximately 15mm. Piston plunger supplied
with FETFE orings (two 7855-726, one 7855-721); Chemraz orings can be offered as
replacements. Offered as flask only with drain assembly. Can also be substituted for
outlets on 6473 or 6474 assemblies, call for details.
FLASK with Drain Assembly, ONLY
Capacity, Liters
10
20
30
50

ORing Ball Joint Size


28/15
28/15
35/25
35/25

Order Code
6472-39
6472-45
6472-40
6472-41

Each
2236.22
Call
2483.33
2694.33

6472-41

6472 FLASK Reaction, Pilot Plant, Cylindrical, with Sink Type Drain
Similar to flask supplied with 6472 pilot plant reactor systems except this flask has a
sink type drain assembly as a bottom outlet. Flask is fabricated with a #36 AceThred
on bottom. The all-PTFE valve is inserted into the AceThred. A stainless steel handle
is then secured to the drain tube. By rotating the handle, plug rises into the flask and
contents drain through three (3) 1/2-inch wide x 1-1/2-inch long slit openings. Rotate
handle in opposite direction and plug seals at bottom of flask, with NO dead space.
Supplied with two Chemraz orings: one 7859-540, to secure valve in #36 AceThred; the
other, 7859542, on bottom of plug to make seal at bottom of flask. Offered as flask with
thread only, drain assembly only, or flask with drain assembly. Can also be substituted
for outlets on 6473 or 6474 assemblies, call for details.
FLASK, with
Thread, only
Cap., Order
Liters Code
Each
10
6472-64 2079.57
20
6472-68
Call
30
6472-65 2396.10
50
6472-66 2861.39

SINK DRAIN
ASSEMBLY, only
Cap.,
Order
Liters
Code
Each
10
6472-69 845.27
20
6472-69 845.27
30
6472-69 845.27
50
6472-69 845.27

FLASK COMPLETE
w/SINK DRAIN ASSY.
Cap.,
Order
Liters
Code
Each
10
6472-164 2924.84
20
6472-163
Call
30
6472-165 3241.37
50
6472-166 3706.66

6472-66

6472 FLASK Reaction, Pilot Plant, Cylindrical,


with Beaded Drain Assembly

Similar to flask supplied with 6472 pilot plant reactor systems except this flask is
supplied with a 1-inch beaded pipe-type flange extension off bottom for connection to
a 020mm threaded PTFE stopcock as the outlet. Stopcock assembly has a mating
1-inch beaded flange that connects to extension off bottom via a Viton lined coupling.
Takeoff on stopcock is 1-inch O.D. tubing. Drain assembly plug supplied with FETFE
orings; Chemraz orings can be offered as replacements. ACE can supply the takeoff
with beaded flange, AceThred, hose connection, etc.; phone for quotation. Listed as
flask with beaded pipe extension only, drain assembly only (includes 020 plug plus glass
thread with mating beaded pipe) or flask with drain assembly. Order coupling separately.
Can also be substituted for outlets on 6473 or 6474 assemblies, call for details.
FLASK, with
Bead, only
Cap., Order
Liters Code
Each
10 6472-96 2061.34
20 6472-94
Call
30 6472-97 2352.39
50 6472-98 2799.44
Coupling, only

BEADED VALVE
ASSEMBLY, only
Cap., Order
Liters Code
Each
10
6472-99 418.62
20
6472-99 418.62
30
6472-99 418.62
50
6472-99 418.62
8856-07

FLASK COMPLETE
w/BEADED VALVE ASSEM.
Cap.,
Order
Liters
Code
Each
10
6472-196 2592.09
20
6472-195
Call
30
6472-197 2883.14
50
6472-198 3330.19

6472-98

8856-07

6472-99

112.13

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Components / Flasks

94

6472 FLASK Reaction, Pilot Plant, Cylindrical, with


Flush Seal Drain Assembly

Similar to flask supplied with 6472 pilot plant reactor systems except this flask has a
Martin-style flush seal drain assembly as a bottom outlet. Flask is fabricated with a 2-inch
beaded valve seat, for 30L and 50L. The plug with a CAPFE oring is inserted into valve
seat and secures within a coupling. By rotating the handle, plug rises into the flask and
seals to afford zero dead space. Back thread out to drain through 1-inch beaded pipe
angled side port. Supplied with CAPFE oring for seal at flask, two Kalrez orings supplied
on valve stem. Other oring materials are available. Offered as flask with valve seat only,
drain assembly only, or flask with drain assembly. Can also be substituted for outlets on
6473 or 6474 assemblies, call for details.

8856-11

FLASK, with
Bead, only
Cap., Order
Liters Code
Each
20 6472-02 2242.57
30 6472-241 2325.19
50 6472-242 2772.68

6472-242

FLUSH SEAL DRAIN


ASSEMBLY, only
Cap., Order
Liters Code
Each
20 6472-245 1010.52
30 6472-245 1010.52
50 6472-245 1010.52

Coupling, only 8856-11

New

FLASK COMPLETE
w/FLUSH SEAL DRAIN ASSEM.
Cap.,
Liters Order Code
Each
20
6472-247
2,250.00
30
6472-248
3486.26
50
6472-249
3933.75

150.55

6482 VALVE ASSEMBLY PTFE, Flush Seal, with Top Pin


Redesigned flush-seal type valve similar to 6472-245 except that the top of the valve has
a 1-1/2-inch x 3/8-inch O.D. pin that extends upward. The pin fits into the receptacle on
the bottom of the 8100 and 8101 bottom agitators. This assembly is designed to reduce
shaft wobble or flexing on the larger reactors. Top opening is 2-inch beaded pipe and
the side drain port is 1-inch beaded pipe. Uses 8856-11 clamp.
Order Code
6482-20

Complete Valve Assembly

Each
1032.42

6482

6483

S INN O Necks, Heavy Wall, with ZDS Valve


6483 LFLASK
AS Three
V

Capacity,
A N N Nominal
I V E R S Nominal
A R Y
Liters
O.D., mm I.D., mm
1936 2011
1
125
115
2I
160
150
3 N E 180
D166,

ON

ACE

I
AT

Heavy wall, round-bottom flask with three 24/40 vertical necks and ZDS valve
TH joint sizes are available as special orders. Bottom outlet is Zero
attached. Other neck
Dead Space (ZDS) valve.

LAN

Height,
mm (A)
180
250
270

Neck
Height, Center
mm
Neck
100
24/40
100
24/40
100
24/40

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Side
Bottom
Order
Necks Outlet, mm
Code
24/40
0-10
6483-110
24/40
0-10
6483-112
24/40
0-10
6483-120

Each
306.44
364.07
421.27

Subject to Ace Discount (Page 4)

Net

Components / Flasks

95

6475 FLASKReaction, Jacketed, Conical 4-Inch Flange


Jacketed cylindrical flask with conical neck opening of four inches (100mm). Inlet and
outlet connections are size 28/15 oring ball joints, both sealed tangentially, one at top
and one at bottom of jacketed section. See 6495 for gaskets, 6496 for clamp.
Capacity,
mL
1000
1500
2000
3000

O.D.,
mm
150
150
150
150

I.D.,
mm
104
104
104
104

Height,
mm (A)
235
245
335
415

Top PTFE
Gasket
6495-10
6495-10
6495-10
6495-10

Order
Code
6475-10
6475-15
6475-20
6475-25

6475

Each
476.88
499.04
544.80
648.09

6476 FLASK Reaction, Conical 4-Inch Flange


Rugged cylindrical flask with conical neck opening of four inches (100mm). Uses 6496 clamp
for securing flask head to flask. See 6495 for gaskets.
Capacity,
mL
500
1000
1500
2000
3000

O.D.,
mm
114
114
114
114
114

I.D.,
mm
104
104
104
104
104

Height,
mm (A)
120
180
220
260
340

Top PTFE
Gasket
6495-10
6495-10
6495-10
6495-10
6495-10

Order
Code
6476-05
6476-10
6476-15
6476-20
6476-25

6476

Each
128.36
137.05
154.46
155.51
159.36

6477 FLASK Reaction, with Indents, Conical 4-Inch Flange


Same as 6476, except with side indents for improved stirring characteristics. Not suitable
for vacuum operation. Uses 6496 clamp for securing conical flask head to flask. See
6495 for gaskets.
Capacity,
mL
500
1000
1500
2000
3000

O.D.,
mm
114
114
114
114
114

I.D.,
mm
104
104
104
104
104

Height,
mm (A)
120
180
220
260
340

Top PTFE
Gasket
6495-10
6495-10
6495-10
6495-10
6495-10

Order Code
6477-05
6477-10
6477-15
6477-20
6477-25

Each
156.51
173.24
181.90
196.99
222.36

6477

ted

Inden

New
6479 FLASK Reaction, Conical 4-Inch Flange
Rugged spherical flask with conical neck opening of 4-inches (100mm). Standard size
flasks use regular Glas-Col heating mantles of equivalent capacity. Length of straight
section including flange, approximately 95mm (3-3/4 inches). Uses 6496 clamp for
securing flask head to flask. See 6495 for gaskets.
Capacity,
Liters
3
5
12
22
50
72

Nominal Nominal
O.D., mm I.D., mm
180
166
225
212
285
270
350
336
457
461
508
496

Height,
mm (A)
270
320
380
450
550
570

Neck
Height,
mm
100
100
100
100
100
100

Order
Code
6479-05
6479-10
6479-15
6479-20
6479-25
6479-30

6479

A
Each
181.94
210.00
334.21
557.04
1682.00
1555.59

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Components / Flasks

96

6540 FLASK Reaction, Spherical, with ZDS Valve


Heavy wall spherical reaction flask with Schott-Duran style flat grooved flange opening.
Flask uses 6517 quick release clamp. Takes all Schott-Duran style heads. Flask comes
with one CAPFE oring. Bottom outlet is Zero Dead Space (ZDS) valve.

6540

Neck Flange Bottom


Capacity, Nominal Nominal Height, Height,
I.D.,
Outlet,
Liters O.D., mm I.D., mm mm (A)
mm mm (In.) mm
2
160
150
250
100
100 (4) 0-10
3
180
166
270
100
100 (4) 0-20
5
226
212
320
100
100 (4) 0-20
5
226
212
320
100
150 (6) 0-20
12
285
270
380
100
150 (6) 0-20
22
350
336
450
100
150 (6) 0-20

Top CAPFE
ORing
7855-880
7855-880
7855-880
7855-881
7855-881
7855-881

Order
Code
6540-104
6540-106
6540-108
6540-110
6540-115
6540-120

Each
548.09
604.15
616.61
819.38
1107.41
1538.40

6469 FLASK Reaction, 4-Neck, Spherical, with Bottom Outlet,


Conical 4-inch Flange

Spherical reaction flask with flat, ground conical style flange with oring groove and
bottom outlet. Supplied with capacity reference gradations. Nominal flange I.D. is 100mm
(4 inches). With three side ports: one #7 AceThred and two 45/50 outer joints. Bottom
outlet is 28/15 spherical ball joint. Each flask is supplied with one 7855-880 CAPFE
(PTFE encapsulated silicone) oring.

Capacity, Nominal Nominal


Liters O.D., mm I.D., mm
12
285
270
22
350
336

Height,
mm (A)
380
450

Neck
Height,
mm
100
100

Flange
I.D.,
Order
mm (In.)
Code
100 (4) 6469-16
100 (4) 6469-18

Each
763.28
1062.02

6469-16

6474 FLASK Reaction, Spherical, 100mm Side Port, with Bottom Outlet
Spherical reaction flask with flat, ground KF flange and bottom outlet. Supplied with
capacity reference gradations. Nominal flange I.D. is 300mm (12 inches). Side sample port
is angled at 45 (Schott-Duran style flange 2.5 inches in diameter). Main flange opening
uses 6525-30 clamp and 6525-51 gasket. Each flask is supplied with one 7855-880
CAPFE (PTFE encapsulated silicone) oring for side port.

6474-29

Capacity, Nominal Nominal Height,


Liters O.D., mm I.D., mm mm (A)
200
750
736
960
200
750
736
960
200
750
736
960
200
750
736
960
200
750
736
960
Glass Cap for Side Port, 100mm
CAPFE ORing for Side Port, 100mm
Gasket for Main Flange, 300mm
Clamp for Main Flange, 300mm
Clamp for Side Port, 60mm, quick release

Neck
Height,
mm
210
210
210
210
210

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Flange
Nominal
I.D., mm
300
300
300
300
300

Bottom
Outlet
Style
0-20mm
Piston
Sink
Beaded
Flush

Order Code Each


6474-16
8521.67
6474-18
8521.67
6474-23
8521.67
6474-25
8399.85
6474-29
8410.93
15312-33
107.78
7855-880
28.63
6525-51
326.26
6525-30
1056.54
6517-22
87.08

Subject to Ace Discount (Page 4)

Net

Components / Flasks

97

6480 FLASKReaction, Jacketed, Conical 4-Inch Flange


Spherical flask with conical neck opening of 4 inches (100mm). Inlet and outlet
connections are size 28/15 oring ball joints, both sealed tangentially, on jacketed
section. Uses 6496 clamp for securing flask head to flask. See 6495 for gaskets.
Capacity, Nominal Nominal
Liters O.D., mm I.D., mm
3
220
170
5
285
211

Height,
mm (A)
370
450

Neck Height,
mm
95
95

Order
Code
6480-05
6480-10

6480

Each
703.82
1055.60

6481 FLASK Reaction, with Indents, Conical 4-Inch Flange

New

Same as 6479, except with side indents for improved stirring characteristics. Not suitable
for vacuum operation. Uses 6496 clamp for securing conical flask head to flask. See
6495 for gaskets.
Capacity, Nominal Nominal
Liters O.D., mm I.D., mm
3
180
166
5
226
212
12
285
270

Height,
mm (A)
270
320
380

Neck Height,
mm
100
100
100

Order
Code
6481-05
6481-10
6481-15

Each
249.01
292.80
490.01

6481

ted

Inden

6491 REACTION FLASKConical 4-Inch Flange


With 4mm bore stopcock for rapid removal of contents without disturbing the general
arrangement of the apparatus. Conical neck opening is 100mm (4-inches). Use 6496
clamp for securing head to flask. See 6495 for gaskets.
Capacity,
Liters
1
2

O.D., I.D.,
mm mm
114 104
114 104

Height,
mm (A)
180
260

Top PTFE
Gasket
6495-10
6495-10

Order Code
6491-10
6491-20

Each
266.46
279.54

6491

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Components / Flasks

98

6492 REACTION FLASK Conical 4-Inch Flange


With 4mm bore stopcock. Stopcock is separated from lower section by 28/15 joint.
Otherwise, identical to 6491. For bottom joint clamp, order 7669-12. Use 6496 Clamp
for securing head to flask. See 6495 for gaskets.

6492

Capacity,
Liters
1
2

O.D.,
mm
114
114

I.D., Height,
mm mm (A)
104 220
104 300

Flask, only
Order
Code
Each
6492-02 173.95
6492-06 194.10

Stopcock, only
Order
Code
Each
6492-10 117.28
6492-10 117.28

Complete
Order
Code
Each
6492-15 291.23
6492-25 311.38

6511 FLASK Reaction, Flat Flange


Cylindrical, heavy-wall reaction flask, round bottom, with flat, ground flange. Without
constriction at top to facilitate introduction/removal of material and allow for ease of
cleaning. For reaction heads, see 6512, 6513 and 6515. For clamp, see 6508 or 6510.

6511-06

Capacity, O.D.,
Liters
mm
1
110
2
140
3
140
4
140

I.D.,
mm
100
130
130
130

Height,
mm (A)
165
185
260
335

Flange
O.D., mm
137
168
168
168

Top FETFE
Gasket
6495-21
6495-23
6495-23
6495-23

Order
Code
6511-06
6511-08
6511-10
6511-12

Each
156.21
188.86
207.26
233.67

6511 FLASK Reaction, Flat Flange, with ORing Groove


Cylindrical, heavy-wall reaction flask, round bottom. Top has flat flange with an oring
groove for use with CAPFE (PTFE encapsulated silicone rubber) oring instead of gasket.
Without constriction at top to facilitate introduction/removal of material and allow for
ease of cleaning. For reaction heads, see 6512, 6513 and 6515. Flask is supplied with
one CAPFE oring. For clamp, see 6508 or 6510.

6511-42

Capacity, O.D.,
Liters
mm
1
110
2
140
3
140
4
140

I.D.,
mm
100
130
130
130

Height,
mm (A)
165
185
260
335

Flange
O.D., mm
137
168
168
168

Top CAPFE
ORing
7855-887
7855-889
7855-889
7855-889

Order
Code
6511-42
6511-45
6511-47
6511-49

Each
183.81
224.38
236.37
269.10

6511 FLASK Reaction, Flat Flange


Cylindrical heavy wall reaction flask, with flat bottom rounded into side wall, and flat,
ground flange top. Without constriction at top to facilitate introduction/removal of material
6511-24 and allow for ease of cleaning. For reaction heads, see 6512, 6513 and 6515. For clamp,
see 6508 or 6510.

Capacity, O.D.,
Liters
mm
1
110
2
140
3
140
4
140

I.D.,
mm
100
130
130
130

Height,
mm (A)
165
185
260
335

Flange
O.D., mm
137
168
168
168

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Top PTFE
Gasket
6495-21
6495-23
6495-23
6495-23

Order
Code
6511-24
6511-27
6511-29
6511-31

Each
158.45
188.31
208.78
233.67

Subject to Ace Discount (Page 4)

Net

Components / Flasks

99

6511 FLASK Reaction, Flat Flange, with ORing Groove


Cylindrical heavy-wall reaction flask, with flat bottom rounded inside wall, and flat flange.
Flange has an oring groove for use with CAPFE (PTFE encapsulated silicone rubber)
oring instead of gasket. Without constriction at top to facilitate introduction/removal of
material and allow for ease of cleaning. For reaction heads, see 6512, 6513 and 6515.
Flask is supplied with one CAPFE oring. For clamp, see 6508 or 6510.
Capacity, O.D.,
Liters
mm
1
110
2
140
3
140
4
140

I.D.,
mm
100
130
130
130

Height,
mm (A)
165
185
260
335

Flange
O.D., mm
137
168
168
168

Top CAPFE
ORing
7855-887
7855-889
7855-889
7855-889

Order Code
6511-53
6511-56
6511-58
6511-60

6511-53

Each
187.54
223.88
245.25
273.13

6516 FLASK Reaction, with Indents, Flat Flange


Cylindrical heavy wall reaction flask, with flat bottom rounded into side wall, and flat,
ground flat flange. Without constriction at top to facilitate introduction/removal of material
and allow for ease of cleaning. Indented sides for better mixing. For reaction heads, see
6512, 6513 and 6515. For clamp, see 6508 or 6510.
Capacity, O.D.,
Liters
mm
1
110
2
140
3
140
4
140

I.D.,
mm
100
130
130
130

Height,
Flange
mm (A) O.D., mm
165
137
185
168
260
168
335
168

Top PTFE
Gasket
6495-21
6495-23
6495-23
6495-23

Order
Code
6516-01
6516-03
6516-05
6516-07

6516

Each
190.13
225.99
246.85
280.21

ted

Inden

New
6518 FLASK Reaction, Cylindrical, with ZDS Valve
Cylindrical, heavy wall flask with round bottom. Flask has Schott-Duran style top flange
supplied with oring groove for use with heads 6433, 6527, 6528 or 6529. Comes with
one CAPFE oring (silicone optional). Bottom outlet is ZDS (Zero Dead Space) PTFE
valve with Chemraz orings. Uses 6517 quick release clamp.
Capacity,
mL
1000
2000
2000
3000
3000
4000

O.D.,
mm
110
110
155
110
150
155

I.D.,
mm
100
100
145
100
140
145

Height,
mm (A)
180
265
200
400
250
300

Flange Size.
mm (in.)
100 (4)
100 (4)
150 (6)
100 (4)
150 (6)
150 (6)

Bottom
Outlet, mm
0-10
0-10
0-20
0-10
0-20
0-20

Top
ORing
7855-880
7855-880
7855-881
7855-880
7855-881
7855-881

Order
Code
6518-10
6518-12
6518-14
6518-16
6518-18
6518-20

Each
538.44
622.60
627.86
644.69
651.37
758.94

6518

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Components / Flasks

100

6519 FLASK Reaction, Jacketed, Flat Flange, with ORing Groove


6519

Cylindrical, heavy-wall reaction flask, except flat flange has an oring groove for use
with CAPFE (PTFE encapsulated silicone rubber) oring instead of gasket. Without
constriction at top to facilitate introduction/removal of material and allow for ease of
cleaning. Flat bottom rounded into side wall. For reaction heads, see 6512, 6513 and
6515. Flask is supplied with one CAPFE oring. For clamp, see 6510. For replacement
orings, see 7855. With 28/15 oring ball joints for easy connect/disconnect from hoses.
Capacity, O.D.,
Liters
mm
1
140
2
170
3
170
4
170

I.D.,
mm
100
130
130
130

Height,
mm (A)
165
185
260
335

Flange
O.D., mm
137
168
168
168

Top CAPFE
ORing
7855-887
7855-889
7855-889
7855-889

Order
Code
6519-01
6519-02
6519-03
6519-04

Each
605.60
633.13
660.66
770.76

6521 FLASK Reaction, Cylindrical, Schott-Duran Flange


Rugged cylindrical reaction flask with Schott-Duran style ground flange with oring groove,
for use with 6517 quick release clamp. Ten liter and larger are supplied with capacity
reference graduations. Each flask is supplied with one CAPFE (PTFE encapsulated silicone)
oring. Plain silicone orings are also available. For reaction heads, see 6528 or 6530. For
cooling/heating coils, see 12067. Thirty (30) liter and above have reduced area to flange.

6521

Capacity, O.D.,
Liters
mm
1
110
2
110
3
110
6
215
10
215
15
250
20
250
30
315
50
315
100
457
200
450

I.D.,
mm
100
100
100
205
205
236
236
300
300
443
436

Height,
mm (A)
180
265
400
280
470
470
570
540
890
940
1575

Flange I.D.,
mm (In.)
100 (4)
100 (4)
100 (4)
200 (8)
200 (8)
200 (8)
200 (8)
200 (8)
200 (8)
200 (8)
200 (8)

Use
Clamp
6517-25
6517-25
6517-25
6517-31
6517-31
6517-31
6517-31
6517-31
6517-31
6517-31
6517-31

Top CAPFE
ORing
Order Code
Each
7855-880
6521-10
152.00
7855-880
6521-12
161.73
7855-880
6521-14
180.95
7855-884
6521-16
846.55
7855-884
6521-20
1189.70
7855-884
6521-25
1463.07
7855-884
6521-27
1636.17
7855-884
6521-30
1736.55
7855-884
6521-35
2194.61
7855-884
6521-40
Priced
7855-884
6521-44 upon request

6526 FLASK Reaction, Cylindrical, Indented Style

6526

ted

Rugged cylindrical reaction flask with Schott-Duran style flat flange with oring groove,
for use with 6517 quick release clamp but with indents for greater agitation. Each flask
is supplied with one CAPFE oring (PTFE encapsulated silicone oring). Plain silicone
orings are also available. For reaction heads, see 6528. For cooling/heating coils, see
12067. NOT suitable for vacuum or pressure operation. Uses 6517-25 quick release clamp.
Capacity, O.D.,
Liters
mm
1
110
2
110

I.D.,
mm
100
100

Height,
mm (A)
180
265

Flange Size.
mm (in.)
100 (4)
100 (4)

Top
ORing
7855-880
7855-880

Order
Code
6526-10
6526-12

Each
200.17
223.10

Inden

New

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Subject to Ace Discount (Page 4)

Net

Components / Flasks

101

6630 REACTION ASSEMBLY Spherical, 8-inch Schott-Duran Flange


Spherical reaction flask with 200mm (8-inch) Schott-Duran style flange with oring groove
as center neck and three (3) 45/50 side necks. Large center neck affords easy clean-out
and allows insertion of a heat exchange coil, 12067. Use 6530 head on center neck and
secure head to flask with 6517 quick release clamp. Flask is supplied with one 7855-288
silicone rubber oring. For replacement, use silicone oring or CAPFE oring. Also listed
are a low-profile, aluminum-housed heating mantle for bottom and a removable fabric
(girdle) mantle for the sides.
50 Liter
Order
Code
Each
Flask, 200mm Flange,
8-inch Center Neck and
(3) 45/50 Side Necks
Head, only, 45/50
Clamp, only
Coil, Cooling,
Copper/PTFE, 1/2-inch
Mantle, Bottom,
Low-Profile
(Wattage)
Mantle, Girdle
(Wattage)
Complete

72 Liter
Order
Code
Each

100 Liter
Order
Code
Each

6530-08
6530-32
6517-31

2807.79
425.01
145.09

6530-15
6530-32
6517-31

2643.93
425.01
145.09

6530-20
6530-32
6517-31

4893.78
425.01
145.09

12067-71

1110.49

12067-71

1110.49

12067-84

1446.60

909.03
12050-34
(1000w-115v)
12041-40
1394.13
(2-1200w-115v)
6630-10
Call

12050-36
1530.57
(1300w-230v)
12041-42
1771.47
(2-1800w-230v)
6630-20
Call

12050-38
2044.00
(1600w-230v)
12041-44
2335.70
(2-2200w-230v)
6630-30
Call

6630

6495 GASKETPTFE
PTFE gaskets, white in color, for mating ground flange surfaces on reactor flasks and
matching heads. Can be used with all conical style and flat flange style flask and heads.
PTFE makes a leak-free seal with slight clamp pressure. They also provide the added
chemical resistance and purity of PTFE.
Thickness,
inches/mm

O.D., Inches
(mm)

Fits Flask
Size, mL

Grooved

Order
Code

Each

0.03/0.8
0.03/0.8
0.03/0.8

5.250 (133.4)
5.375 (136.7)
6.625 (168.4)

500-3000mL
500-1000mL
2000-4000mL

No
Yes
Yes

6495-10
6495-21
6495-23

11.28
60.28
64.15

6495-10

6495-21

6495 GASKETFETFE
ACE FETFE gaskets, black in color, for mating ground flange surfaces on reactor flasks
and matching heads. Can be used with all conical style and flat flange style flask and
heads. FETFE makes a leak-free seal with clamp pressure. FETFE is an exclusive
ACE product made from TFE impregnated fluoroelastomers with good chemical and
temperature resistance.
Thickness,
inches/mm
0.02/0.5
0.02/0.5

O.D., Inches
(mm)
5.375 (136.7)
6.625 (168.4)

Fits Flask
Size, mL
500-1000mL
2000-1000mL

Grooved
Yes
Yes

Order
Code
6495-43
6495-47

6495-43

Each
19.53
20.12

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

102

Components / Flasks
6530 FLASK Reaction, Spherical, 3-Neck, Side Port, Flange Top

Cap, clamp, and


ORing for Side Port
(not included)

Rugged, spherical reaction flask with Schott-Duran style oring grooved side port, angled
45 for ease in adding material to flask. In addition to the side port, flask has three 45/50
side necks, all vertical. Center is a Schott-Duran style oring grooved flange supplied
with a CAPFE (PTFE encapsulated silicone) oring for use with 6517 quick release clamp.
Supplied with capacity reference gradations. Order cap, clamps, and extra orings (listed
below) separately.
Capacity, Nominal Nominal
Liters O.D., mm I.D., mm
50
457
443
50
457
443
50
457
443
50
457
443
50
457
443
50
457
443
72
508
496
72
508
496
72
508
496
100
610
596
100
610
596
100
610
596

Height,
mm (A)
550
550
550
550
550
550
570
570
570
680
680
680

Neck
Height,
mm
75
75
75
75
75
75
75
75
75
75
75
75

Center
Neck, mm Side Port
(Inches) Size (mm)
100 (4)
60
150 (6)
60
200 (8)
60
100 (4)
100
150 (6)
100
200 (8)
100
100 (4)
100
150 (6)
100
200 (8)
100
100 (4)
100
150 (6)
100
200 (8)
100

Glass Cap, 60mm


Glass Cap, 100mm
CAPFE ORing, 60mm
CAPFE ORing, 100mm
CAPFE ORing, 150mm
CAPFE ORing, 200mm
Clamp, 60mm, quick release
Clamp, 100mm, quick release
Clamp, 150mm, quick release
Clamp, 200mm, quick release

Order Code
6530-42
6530-43
6530-44
6530-47
6530-48
6530-49
6530-52
6530-54
6530-56
6530-64
6530-65
6530-66

Each
2012.46
2111.69
2182.55
2047.89
2154.20
2239.22
2402.22
2501.43
2636.06
4917.80
4974.49
5073.69

15312-30
15312-33
7855-878
7855-880
7855-881
7855-884
6517-22
6517-25
6517-27
6517-31

60.05
107.78
28.10
28.63
59.65
75.27
87.08
98.23
117.67
145.09

6530-47

6530 FLASK Reaction, Spherical, 3-Neck, Flange Top


Rugged, spherical reaction flask with three 45/50 side necks, all vertical. Center is a
Schott-Duran style oring grooved flange supplied with a CAPFE (PTFE encapsulated
silicone) oring for use with 6517 quick release clamp. Supplied with capacity reference
gradations. Order clamp and extra orings (listed below) separately.
Capacity, Nominal Nominal
Liters O.D., mm I.D., mm
22
350
336
50
457
443
72
508
496
100
610
596

Height,
mm (A)
450
550
570
680

Neck Height,
mm
100
75
75
75

CAPFE ORing, 100mm


CAPFE ORing, 200mm
Clamp, 100mm, quick release
Clamp, 200mm, quick release

Center Neck,
mm (Inches)
100 (4)
200 (8)
200 (8)
200 (8)

Order Code
6530-06
6530-08
6530-15
6530-20

Each
1046.04
2807.79
2643.93
4893.78

7855-880
7855-884
6517-25
6517-31

28.63
75.27
98.23
145.09

6530-08

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Subject to Ace Discount (Page 4)

Net

Components / Flasks

103

6530 FLASK Reaction, Spherical, 4-Neck, 8-in. Flange, with Bottom Outlet
Spherical reaction flask with Schott-Duran style flat, ground flange and bottom valve
assembly. Supplied with capacity reference gradations. Nominal flange I.D. is 200mm
(8 inches). Uses 6517-31 clamp and 7855-884 CAPFE oring. Flask has three 45/50
side joints. 35/25 oring/ball joint connection off 0-20 and piston-style valve. Each flask
is supplied with one CAPFE (PTFE encapsulated silicone) oring.
Capacity, Nominal Nominal
Liters O.D., mm I.D., mm
50
457
443
50
457
443
50
457
443
50
457
443
50
457
443
72
508
496
72
508
496
72
508
496
72
508
496
72
508
496
100
610
596
100
610
596
100
610
596
100
610
596
100
610
596

Height,
mm (A)
550
550
550
550
550
570
570
570
570
570
680
680
680
680
680

Neck Height,
mm
75
75
75
75
75
75
75
75
75
75
75
75
75
75
75

Bottom Outlet
Style
0-20 mm
Piston
Sink
Beaded
Flush
0-20 mm
Piston
Sink
Beaded
Flush
0-20 mm
Piston
Sink
Beaded
Flush

Order
Code
6530-10
6530-11
6530-12
6530-13
6530-14
6530-17
6530-18
6530-19
6530-22
6530-21
6530-23
6530-24
6530-25
6530-26
6530-27

Each
2917.90
2229.72
2196.69
2196.69
2196.69
2883.44
2669.82
2623.40
2,385.00
2626.12
5066.97
5006.93
4952.73
4934.18
4831.04

6530-11

6957 FLASK Reaction, Spherical, 4-Neck, Side Port


Rugged, spherical reaction flask with Schott-Duran style 60mm (2.4 inch) I.D. oring
grooved side port, angled 45 for ease in adding material to flask. In addition to the
60mm side port, flask has a 45/50 center neck and three side necks, all vertical.
Supplied with capacity reference gradations. For 60mm side port, order cap, oring and
clamp separately.
Capacity, Nominal Nominal
Liters O.D., mm I.D., mm
22
350
336
22
350
336
22
350
336
50
457
443

Height,
mm (A)
450
450
450
550

Neck
Height,
mm
100
100
100
75

Center
Neck
45/50
45/50
45/50
45/50

Side
Necks
45/50
29/42
24/40
45/50

Glass Cap, 60mm


CAPFE ORing, 60mm
Clamp, 60mm, quick release

Order Code
6957-28
6957-26
6957-24
6957-65

Each
1026.50
907.56
896.76
Call

15312-30
7855-878
6517-22

60.05
28.10
87.08

Cap, clamp, and


ORing for side port
(not included)

6957-65

For a full listing of round-bottom reaction flasks in smaller


sizes, see our Laboratory Glassware & Equipment Catalog

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

104

Components / Flasks
6522/6472 FLASK Reaction, Cylindrical, with Bottom Outlet
Similar to 6521 but with bottom outlet for draining contents. Easy Action and Piston style
bottom outlets have 28/15 oring ball joint connection. Flasks have capacity reference
graduations, and each flask is supplied with one CAPFE (PTFE encapsulated silicone)
oring. Plain silicone orings are also available.

6522-31

Cap.,
Liters
1
2
3
6
10
15
20
30
50
100
200
10
15
20
30
50
100
200
10
15
20
30
50
100
200
10
15
20
30
50
100
200
10
15
20
30
50
100
200

O.D.,
mm
110
110
110
205
205
240
236
301
301
443
436
205
205
236
301
301
443
436
205
205
236
301
301
443
436
205
205
236
301
301
443
436
205
205
236
301
301
443
436

Nominal
I.D., Height, Flange I.D.
mm mm (A) mm (in.)
100 180
100 (4)
100 265
100 (4)
100 400
100 (4)
215 280
200 (8)
215 470
200 (8)
250 470
200 (8)
250 570
200 (8)
315 540
200 (8)
315 890
200 (8)
457 940
200 (8)
450 1575
200 (8)
215 470
200 (8)
215 470
200 (8)
250 570
200 (8)
315 540
200 (8)
315 890
200 (8)
457 940
200 (8)
450 1575
200 (8)
215 470
200 (8)
215 470
200 (8)
250 570
200 (8)
315 540
200 (8)
315 890
200 (8)
457 940
200 (8)
450 1575
200 (8)
215 470
200 (8)
215 470
200 (8)
250 570
200 (8)
315 540
200 (8)
315 890
200 (8)
457 940
200 (8)
450 1575
200 (8)
215 470
200 (8)
215 470
200 (8)
250 570
200 (8)
315 540
200 (8)
315 890
200 (8)
457 940
200 (8)
450 1575
200 (8)

Use
Clamp
6517-25
6517-25
6517-25
6517-31
6517-31
6517-31
6517-31
6517-31
6517-31
6517-31
6517-31
6517-31
6517-31
6517-31
6517-31
6517-31
6517-31
6517-31
6517-31
6517-31
6517-31
6517-31
6517-31
6517-31
6517-31
6517-31
6517-31
6517-31
6517-31
6517-31
6517-31
6517-31
6517-31
6517-31
6517-31
6517-31
6517-31
6517-31
6517-31

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Top
CAPFE
ORing
7855-880
7855-880
7855-880
7855-884
7855-884
7855-884
7855-884
7855-884
7855-884
7855-884
7855-884
7855-884
7855-884
7855-884
7855-884
7855-884
7855-884
7855-884
7855-884
7855-884
7855-884
7855-884
7855-884
7855-884
7855-884
7855-884
7855-884
7855-884
7855-884
7855-884
7855-884
7855-884
7855-884
7855-884
7855-884
7855-884
7855-884
7855-884
7855-884

Valve
Size
mm
0-8
0-8
0-8
0-8
0-14
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20

Bottom
Outlet Style
Easy Action
Easy Action
Easy Action
Easy Action
Easy Action
Easy Action
Easy Action
Easy Action
Easy Action
Easy Action
Easy Action
Piston
Piston
Piston
Piston
Piston
Piston
Piston
Sink
Sink
Sink
Sink
Sink
Sink
Sink
Beaded
Beaded
Beaded
Beaded
Beaded
Beaded
Beaded
Flush Valve
Flush Valve
Flush Valve
Flush Valve
Flush Valve
Flush Valve
Flush Valve

Order
Code
6522-11
6522-13
6522-15
6522-17
6522-21
6522-26
6472-167
6522-31
6522-36
6522-41
6522-45
6522-51
6522-52
6472-168
6522-53
6522-54
6522-55
6522-56
6522-61
6522-62
6472-169
6522-63
6522-64
6522-65
6522-66
6522-71
6522-72
6472-170
6522-73
6522-74
6522-75
6522-76
6522-81
6522-82
6472-02
6522-83
6522-84
6522-85
6522-86

Each
538.78
549.56
561.92
1359.86
1131.71
1471.89
2481.48
2013.47
2568.90
4619.10
10955.90
1512.39
1571.04
2383.33
2093.14
2901.33
5027.94
10873.32
1361.17
1435.21
2180.03
1990.82
2824.17
4933.81
12387.33
1327.19
1404.35
2166.02
1963.03
2793.30
4904.48
12084.53
1365.80
1447.56
2242.57
2006.24
2833.42
4953.87
12084.53

Subject to Ace Discount (Page 4)

Net

Components / Flasks

105

6473 FLASK Reaction, Cylindrical, with Bottom Outlet, KF Plane Flange


Cylindrical reaction flask with top KF plane flange and bottom outlet for draining contents.
Easy Action bottom outlet has 28/15 oring ball joint connection. Sink bottom outlet has
#36 AceThred connection. Flasks have capacity reference graduations. Gasket and
coupling must be purchased separately.
Cap.,
Liters
100
100
200
100
200
100
200

O.D.,
mm
457
457
450
457
450
457
450

Nominal
I.D., Height, Flange I.D.
mm mm (A) mm (in.)
443 940 300 (12)
443 940 300 (12)
436 1575 300 (12)
443 940 300 (12)
436 1575 300 (12)
443 940 300 (12)
436 1575 300 (12)

Use
Coupling
6525-30
6525-30
6525-30
6525-30
6525-30
6525-30
6525-30

Top
PTFE
Gasket
6525-51
6525-51
6525-51
6525-51
6525-51
6525-51
6525-51

Valve
Size
mm
0-20

Bottom
Outlet Style
Easy Action
Flush Valve
Flush Valve
Sink
Sink
Beaded
Beaded

Order
Code
6473-02
6473-05
6473-11
6473-22
6473-26
6473-40
6473-44

Each
5531.62
4977.90
10958.02
5371.03
12176.20
4983.43
10880.50

6473-02

6523 FLASK Reaction, Cylindrical, Jacketed

6523

Rugged cylindrical reaction flask with Schott-Duran style flat flange with oring groove,
for use with 6517 quick release clamp. Inlet and outlet connections on jacket, sealed
tangentially, are oring size 35/25 ball joints. Ten (10) liter and larger are supplied with
capacity reference graduations. Each flask is supplied with one CAPFE (PTFE encapsulated
silicone) oring for flange. Plain silicone orings are also available. For reaction heads,
see 6528 or 6530. Jacket is direct sealed to inner flask.
Capacity, O.D.,
Liters
mm
1
160
2
160
3
160
6
270
10
270
15
315
20
315
30
350
50
350

I.D.,
mm
100
100
100
205
205
240
236
301
301

Height,
mm (A)
230
395
425
315
525
575
675
540
925

Nominal
Flange I.D.
mm (In.) Use Clamp
100 (4)
6517-25
100 (4)
6517-25
100 (4)
6517-25
200 (8)
6517-31
200 (8)
6517-31
200 (8)
6517-31
200 (8)
6517-31
200 (8)
6517-31
200 (8)
6517-31

Top
APFE
C
ORing
7855-880
7855-880
7855-880
7855-884
7855-884
7855-884
7855-884
7855-884
7855-884

Order
Code
6523-12
6523-14
6523-16
6523-19
6523-22
6523-27
6523-30
6523-32
6523-37

Each
574.48
655.16
725.63
2164.47
2287.00
2967.46
3077.56
3297.79
3958.44

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

106

Components / Flasks
6524/6472 FLASK Reaction, Cylindrical, with Bottom Outlet, Jacketed
Rugged cylindrical reaction flask with Schott-Duran style flat flange with oring groove, for
use with quick release clamp. Inlet and outlet connections on jacket, sealed tangentially, are
oring ball joints. Ten (10) liter and larger are supplied with capacity reference graduations.
Each flask is supplied with one CAPFE (PTFE encapsulated silicone) oring. Plain silicone
orings are also available. For reaction heads, see 6528 or 6530. Bottom Easy Action and
Piston outlets on 15L and larger flasks have size 35/25 oring ball joint; below 15L, oring
ball joints are size 28/15.

6524-33

Cap.,
Liters
1
2
3
6
10
15
20
30*
50*
10
15
20
30*
50*
10
15
20
30*
50*
10
15
20
30*
50*
10
15
20
30*
50*

O.D.,
mm
160
160
160
270
270
315
315
350
350
270
315
315
350
350
270
315
315
350
350
270
315
315
350
350
270
315
315
350
350

I.D.,
mm
100
100
100
205
205
240
236
301
301
205
240
236
301
301
205
240
236
301
301
205
240
236
301
301
205
240
236
301
301

Hgt, Nominal
Top
Valve Inlet/ Bottom
mm Flange I.D. Use
CAPFE Size, Outlet Outlet
Bottom
Order
(A) mm (In.) Clamp ORing mm Size Size Outlet Style
Code
205 100 (4) 6517-25 7855-880 0-8 28/15 28/15 Easy Action 6524-13
240 100 (4) 6517-25 7855-880 0-8 28/15 28/15 Easy Action 6524-15
425 100 (4) 6517-25 7855-880 0-8 28/15 28/15 Easy Action 6524-17
340 200 (8) 6517-31 7855-884 0-8 28/15 28/15 Easy Action 6524-20
530 200 (8) 6517-31 7855-884 0-14 35/25 28/15 Easy Action 6524-23
545 200 (8) 6517-31 7855-884 0-20 35/25 35/25 Easy Action 6524-28
700 200 (8) 6517-31 7855-884 0-20 35/25 35/25 Easy Action 6472-175
550 200 (8) 6517-31 7855-884 0-20 35/25 35/25 Easy Action 6524-33
900 200 (8) 6517-31 7855-884 0-20 35/25 35/25 Easy Action 6524-38
530 200 (8) 6517-31 7855-884 0-20 35/25 35/25
Piston
6524-43
545 200 (8) 6517-31 7855-884 0-20 35/25 35/25
Piston
6524-44
700 200 (8) 6517-31 7855-884 0-20 35/25 35/25
Piston
6472-176
550 200 (8) 6517-31 7855-884 0-20 35/25 35/25
Piston
6524-45
900 200 (8) 6517-31 7855-884 0-20 35/25 35/25
Piston
6524-46
530 200 (8) 6517-31 7855-884

Sink
6524-53
545 200 (8) 6517-31 7855-884

Sink
6524-54
700 200 (8) 6517-31 7855-884

Sink
6472-177
550 200 (8) 6517-31 7855-884

Sink
6524-55
900 200 (8) 6517-31 7855-884

Sink
6524-56
530 200 (8) 6517-31 7855-884

Beaded
6524-63
545 200 (8) 6517-31 7855-884

Beaded
6524-64
700 200 (8) 6517-31 7855-884

Beaded
6472-178
550 200 (8) 6517-31 7855-884

Beaded
6524-65
900 200 (8) 6517-31 7855-884

Beaded
6524-66
530 200 (8) 6517-31 7855-884

Flush Seal 6524-73


545 200 (8) 6517-31 7855-884

Flush Seal 6524-74


700 200 (8) 6517-31 7855-884

Flush Seal 6472-16


550 200 (8) 6517-31 7855-884

Flush Seal 6524-75


900 200 (8) 6517-31 7855-884

Flush Seal 6524-76

Each
883.96
995.14
1106.33
2885.36
3002.10
3218.92
5722.92
3502.45
7044.57
2946.51
3057.70
6112.53
3280.08
7116.10
2946.51
3057.70
5705.98
3280.08
7116.10
2946.51
3057.70
5666.74
3280.08
7116.10
2890.91
3330.11
4361.31
3363.47
7116.10

*Jackets on 30 and 50 Liter capacities are silicone rubber sealed at bottom only.

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Subject to Ace Discount (Page 4)

Net

Components / Flasks

107

6473 FLASKReaction, Jacketed, Cylindrical, with Bottom Outlet,


KF Plane Flange,

Cylindrical, jacketed reaction flask with top KF plane flange and bottom flush style outlet
for draining contents. Inlet and outlet connections on jacket, sealed tangentially, are 35/25
oring ball joints. Flasks has capacity reference graduations. Gasket and coupling must
be purchased separately.
Nominal
Cap., O.D., I.D., Height, Flange I.D.
Use
Liters mm mm mm (A) mm (in.) Coupling
100 460 443 940
300 (12) 6525-30

Top
PTFE
Gasket
6525-51

Bottom
Outlet Style
Flush

Order
Code
6473-09

Each
14341.21

6473-09

6533 FLASK Reaction, Spherical, Plain, 4, 6, or 8 in. Flange


Rugged spherical reaction flask with Schott-Duran style flat flange with oring groove,
for use with 6517 quick release clamp. Each flask is supplied with one CAPFE (PTFE
encapsulated silicone) oring. Flasks (12L and above) are supplied with capacity reference
graduations. Plain silicone orings are also available. For reaction heads, see 6529 or
6530. For cooling/heating coils, see 12067. For mantles, see 12043.
Capacity,
Liters
3
5
5
12
22
50
72

O.D.,
mm
180
226
226
285
350
457
508

I.D.,
mm
166
212
212
270
336
443
496

Height,
mm (A)
270
320
320
380
450
550
570

Nominal
Flange I.D.,
mm (In.)
100 (4)
100 (4)
150 (6)
150 (6)
150 (6)
200 (8)
200 (8)

Use
Clamp
6517-25
6517-25
6517-27
6517-27
6517-27
6517-31
6517-31

Top
CAPFE
ORing
7855-880
7855-880
7855-881
7855-881
7855-881
7855-884
7855-884

Order
Code
6533-03
6533-05
6533-07
6533-12
6533-15
6533-25
6533-28

Each
247.75
302.81
338.67
453.98
649.78
1596.59
1789.29

6533

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Components / Flasks

108

6534 FLASK Reaction, Spherical, Flange Top, with Bottom Outlet


Rugged spherical reaction flask with Schott-Duran style flat flange with oring groove, for
use with 6517 quick release clamp. Flasks have capacity reference gradations, and can
be configured with one of several different bottom outlets (see page 92 for a description
of each outlet style). Each flask is supplied with one CAPFE (PTFE encapsulated silicone)
oring. Plain silicone orings are also available. For reaction heads, see 6529 or 6530.
For cooling/heating coils, see 12067. For mantles, see 12044. Easy Action and Piston
bottom outlets have size 35/25 oring ball joint connection.

6534-13

Cap.,
Liters
3
5
5
12
22
50
72
12
22
50
72
12
22
50
72
12
22
50
72
12
22
50
72

O.D.,
mm
180
226
226
285
350
457
508
285
350
457
508
285
350
457
508
285
350
457
508
285
350
457
508

I.D.,
mm
166
212
212
270
336
443
496
270
336
443
496
270
336
443
496
270
336
443
496
270
336
443
496

Height, Nominal
mm Flange I.D.,
(A)
mm (In.)
270
100 (4)
320
100 (4)
320
150 (6)
380
150 (6)
450
150 (6)
550
200 (8)
570
200 (8)
380
150 (6)
450
150 (6)
550
200 (8)
570
200 (8)
380
150 (6)
450
150 (6)
550
200 (8)
570
200 (8)
380
150 (6)
450
150 (6)
550
200 (8)
570
200 (8)
380
150 (6)
450
150 (6)
550
200 (8)
570
200 (8)

Use
Clamp
6517-25
6517-25
6517-27
6517-27
6517-27
6517-31
6517-31
6517-27
6517-27
6517-31
6517-31
6517-27
6517-27
6517-31
6517-31
6517-27
6517-27
6517-31
6517-31
6517-27
6517-27
6517-31
6517-31

Repl.
Outlet
Bottom
CAPFE
Size,
Outlet
Order
ORing
mm
Style
Code
7855-880 0-8 Easy Action 6534-04
7855-880 0-8 Easy Action 6534-06
7855-881 0-8 Easy Action 6534-09
7855-881 0-14 Easy Action 6534-13
7855-881 0-20 Easy Action 6534-16
7855-884 0-20 Easy Action 6534-26
7855-884 0-20 Easy Action 6534-29
7855-881 0-20
Piston
6534-30
7855-881 0-20
Piston
6534-32
7855-884 0-20
Piston
6534-34
7855-884 0-20
Piston
6534-36
7855-881

Sink
6534-40
7855-881

Sink
6534-42
7855-884

Sink
6534-44
7855-884

Sink
6534-46
7855-881

Beaded
6534-50
7855-881

Beaded
6534-52
7855-884

Beaded
6534-54
7855-884

Beaded
6534-56
7855-881

Flush Seal 6534-60


7855-881

Flush Seal 6534-62


7855-884

Flush Seal 6534-64


7855-884

Flush Seal 6534-66

Each
611.88
634.18
705.66
976.91
1257.47
2604.68
2529.79
1099.16
1379.75
2463.76
2652.04
976.91
1257.47
2341.50
2529.79
928.00
1208.58
2292.59
2480.87
964.68
1245.25
2329.27
2517.55

6535 FLASK Reaction, Spherical, Jacketed


Rugged spherical jacketed reaction flask with Schott-Duran style flat flange with oring
groove, for use with 6517 quick release clamp. Each flask is supplied with one CAPFE
(PTFE encapsulated silicone) oring. Plain silicone orings are also available. 12L size
is supplied with capacity reference graduations. Inlet and outlet are size 28/15 oring
ball joints, sealed tangentially. For reaction heads, see 6529. For cooling/heating coils,
see 12076.

6535-12

Capacity,
Liters
3
5
5
12

O.D.,
mm
225
285
285
360

I.D.,
mm
170
212
121
270

Height,
mm (A)
370
435
450
505

Nominal
Flange I.D.,
mm (In.)
100 (4)
100 (4)
150 (6)
150 (6)

Use
Clamp
6517-25
6517-25
6517-27
6517-27

Top
CAPFE
ORing
7855-880
7855-880
7855-881
7855-881

Order
Code
6535-03
6535-05
6535-07
6535-12

Each
967.87
1190.00
1238.87
2889.92

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Subject to Ace Discount (Page 4)

Net

Components / Flasks

109

6536 FLASK Reaction, Spherical, Jacketed, with Bottom Outlet


Rugged spherical reaction flask with Schott-Duran style flat flange with oring groove, for
use with 6517 quick release clamp. See listing below for different bottom outlet styles.
The 0-14 Easy-Action and Piston bottoms have a 28/15 ball joint bottom connector. Each
flask is supplied with one 7855 CAPFE (PTFE encapsulated silicone) oring. Plain silicone
orings are also available. All capacities have size 28/15 oring ball joints on inlet and outlet,
sealed tangentially. For reaction heads, see 6529. For cooling/heating coils, see 12067.
Capacity,
Liters
3
5
5
12
12
12
12
12

O.D.,
mm
225
285
285
360
360
360
360
360

Nominal
Bottom
Top
I.D., Height, Flange I.D.,
Outlet
Use
CAPFE
mm mm (A) mm (In.)
Style
Clamp
ORing
170
370
100 (4)
Easy-Action 6517-25 7855-880
212
435
100 (4)
Easy-Action 6517-25 7855-880
212
450
150 (6)
Easy-Action 6517-27 7855-881
270
505
150 (6)
0-14mm
6517-27 7855-881
270
505
150 (6)
Piston
6517-27 7855-881
270
505
150 (6)
Sink
6517-27 7855-881
270
505
150 (6)
Beaded
6517-27 7855-881
270
505
150 (6)
Flush
6517-27 7855-881

Order
Code
6536-06
6536-09
6536-11
6536-15
6536-25
6536-35
6536-45
6536-55

Each
1132.26
1520.22
1573.96
3245.52
3369.57
3245.52
3195.17
3232.54

6536-15

6537 FLASK Reaction, Spherical, Indented Style


Rugged spherical reaction flask with Schott-Duran style flat flange with oring groove,
for use with 6517 quick release clamp but with indents for greater agitation. Each flask
is supplied with one 7855-881 CAPFE (PTFE encapsulated silicone) oring. Plain silicone
orings are also available. For reaction heads, see 6529. For cooling/heating coils, see
12067. NOT suitable for vacuum or high temperature operation.
Capacity, O.D.,
Liters
mm
3
180
5
226
5
226
12
285

Nominal
I.D., Height, Flange I.D.,
mm mm (A) mm (In.)
166
270
100 (4)
212
320
100 (4)
212
320
150 (6)
270
380
150 (6)

Use
Clamp
6517-25
6517-25
6517-27
6517-27

Top
CAPFE
ORing
7855-880
7855-880
7855-881
7855-881

Order
Code
6537-07
6537-12
6537-17
6537-24

ted

Inden

Each
320.35
363.68
428.55
534.04

6537

New

6310 FLASK Reaction, Three-Wall, Double-Jacketed


Unique ACE proprietary designed triple-wall, or double-jacketed, flasks. Available with
various bottom outlets. These flasks are designed with an outside, third wall, vacuum
evacuated and sealed for better thermal control and stability of the jacketed reactor.
The first wall is the main reactor body, the second is the thermal fluid compartment with
inlet/outlet oring ball joints and the third is the evacuated compartment. The double
jacket also eliminates frosting-up on the outer jacket as seen in low temperature with
traditional jacketed flasks. The jacket I/O are 35/25 oring ball joints for easier recircula
tor hose connection. The top has an 8-inch oring groove Schott-Duran style flange. All
sizes have reference graduations. Flask comes with CAPFE (PTFE encapsulated silicone)
oring. Other sizes and bottom valves are available on special request.
Inner
Flask
Cap.,
Liters
10
10
15
15
20
20

Inner
Overall
Inner
Flask
Length, Flask ID, Length,
mm
mm
mm
Bottom Outlet Style
2-inch Bead/Flush Valve
626
201
490
626
201
490
No Outlet/Rounded
785
201
645
2-inch Bead/Flush Valve
785
201
645
No Outlet/Rounded
800
235
665
2-inch Bead/Flush Valve
800
235
665
No Outlet/Rounded

Order Code
6310-100
6310-105
6310-120
6310-125
6310-130
6310-135

Each
Priced
Upon
Request

6310

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Components / Flasks

110

6300 FLASK Reaction, with ORing Groove Flange,


Fritted Disc, Heavy Wall

Cylindrical, heavy wall reaction flasks, with integral fritted disc and bottom tube outlet.
Top of flask has Schott-Duran style flange with a groove for use with oring. For reaction
heads, see 6528, 6529 and 6530 series. Can be used with two-piece or 6517 quick
release clamps.

Capacity, O.D.,
Liters
mm
1
110
1
110
1
110
4
155
4
155
4
155
6
215
6
215
6
215

6300

I.D.,
mm
100
100
100
145
145
145
205
205
205

Bottom
Frit
Height, Flange I.D., Tube O.D.
Frit
Diameter,
mm (A) mm (In.)
(In.)
Porosity
mm
210
100 (4)
5/8
A
100
210
100 (4)
5/8
B
100
210
100 (4)
5/8
C
100
330
150 (6)
1-1/4
A
145
330
150 (6)
1-1/4
B
145
330
150 (6)
1-1/4
C
145
275
200 (8)
1-1/4
A
178
275
200 (8)
1-1/4
B
178
275
200 (8)
1-1/4
C
178

Order
Code
6300-06
6300-08
6300-10
6300-18
6300-20
6300-22
6300-30
6300-32
6300-34

Each
419.05
419.05
419.05
508.85
508.85
508.85
808.17
808.17
808.17

GLASS FRIT CHARACTERISTICS


ACE
Designation
A
B
C
D
E

Porosity
Maximum Pore Dia.
Range (micron)
145-174
70-100
25-50
10-20
4-8

Corning, Kimble, &


ChemGlass Equivalent
EC (170-220)

C (40-60
M (10-15)
F (4-5.5)

Most Frequent Uses


Coarse filtration. Gas Dispersion
Coarse filtration. Gas Dispersion
Filtration. Gas Dispersion
Filtration and extraction
Filtration and extraction

6497 FLASK Reaction, Stainless Steel, 4-inch Conical Flange

6497

Cylindrical flask fabricated from 18-8, type 316 electro polished, heliarc welded stainless
steel.* Can be used with 6478 Glas-Col mantles. Interchangeable with our glass units.
Nominal Nominal
Capacity, mL O.D., mm I.D., mm
500
4.0
4.5
1000
4.1
4.5
2000
4.1
4.5

Height,
mm (A)
3.5
6.0
9.0

Order Code
6497-07
6497-12
6497-17

Priced on
Application

*Other metals are available, phone ACE.

6498

6498 FLASK Reaction, Stainless Steel, 4-inch Conical Flange


Spherical flask fabricated from 18-8, type 316 electro-polished, heliarc-welded stainless
steel. Interchangeable with our glass units. Can be used with 12043 or 12053 Glas-Col
mantles.

Nominal Nominal Height,


Capacity, Liters O.D., mm I.D., mm mm (A)
3
178
177
254
5
216
215
317
12
292
291
380
22
343
342
416
50
444
443
546
72
508
507
600

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Order Code
6498-12
6498-17
6498-22
6498-27
6498-32
6498-37

Priced on
Application

Subject to Ace Discount (Page 4)

Net

Components / Flasks

111

D120676 FLASK Instatherm Robo Reactorfor ASTM D7528-09


Flask for use with ASTM Protocol D7528-09 Standard Test Method. For bench oxidation
of engine oils by ROBO. Use ONLY 9698-16 controller cord (supplied) for connection to
temperature controllers. Conical style four-inch flange. Uses 6495 gaskets.
Capacity,
Liters
1

Volts/Amps
40/10

Order Code
D120676

D120676

Each
Call

New

9655 REACTION FLASKInstatherm Heated, Schott-Duran Flange


Rugged cylindrical reaction flask with Schott-Duran, flat, ground 4-inch flange with
oring groove for use with 6517-25 quick release clamp and integral heating element
that eliminates the local superheating commonly associated with more conventional
heating methods and eliminates cumbersome oil baths. The heating response is rapid
and accurate. Supplied with silicone coating for insulation and protection. O-Ring
(supplied with flask) is CAPFE (PTFE encapsulated silicone). Flask is coated to within
approximately 38mm of the flange for 250C operation. Interchangeable with ACE
4-inch reactor heads with Schott-Duran flange. Three-pronged plug for insertion into
ACE temperature controllers. Integral six-foot controller cord.
Capacity, O.D.,
Liters
mm
1
110
2
110

I.D.,
mm
100
100

Height,
mm (A)
180
200

Volt/Amp
Rating
40/8
120/5

Watts
400
600

Order
Code
9655-17
9655-22

Each
766.76
869.89

9655

9656 REACTION FLASKInstatherm Heated, Conical, 4-Inch Flange


Same flask as listed under 6476, except with Instatherm coating. Has flat-ground,
4-inch conical flange. This integral heating element eliminates the local super-heating
commonly associated with more conventional heating methods. Eliminates cumbersome
and dangerous oil baths. The heating response is rapid and accurate. Supplied with
9698-20 cord for connection to variable voltage or termperature controller. Flask is
coated to within 38mm of the flange for 200C operation. Interchangeable with ACE
4-inch reactor heads with Schott-Duran flange. For controllers, see ACE or J-Kem
temperature controllers with voltage limiting output, such as 12125, 12324. Use 6496
clamp for securing head to flask.
Capacity, O.D.,
Liters
mm
1
110
2
114

I.D.,
mm
100
104

Height,
mm (A)
180
260

Volt/Amp
Rating
40/8
120/5

Watts
400
500

Order
Code
9656-08
9656-12

Each
758.58
864.03

9656

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

112

Components / Flasks

6945

HEAVY
DUTY

6945 FLASK Three Necks, Jacketed, Heavy Wall


Round bottom flask with three in-line reinforced outer joints. Fabricated with heavy
walls, approximately 30% heavier than standard-wall flasks. Inlet/outlet connections are
28/15 oring ball joints, sealed tangentially.
Cap.,
mL
500
500
1000
1000
2000
3000
3000
3000
3000
5000

Center
Neck
24/40
29/42
24/40
29/42
29/42
29/42
29/42
34/45
45/50
29/42

Side
Necks
24/40
24/40
24/40
24/40
24/40
24/40
29/42
24/40
24/40
24/40

Order
Code
6945-217
6945-219
6945-223
6945-225
6945-245
6945-255
6945-257
6945-259
6945-261
6945-264

Each
530.52
539.65
612.62
621.78
661.37
741.98
749.51
779.12
807.61
840.76

Cap.,
mL
5000
5000
5000
6000
6000
6000
6000
6000
6000

Center
Neck
29/42
34/45
45/50
24/40
29/42
29/42
45/50
45/50
45/50

Side
Necks
29/42
24/40
24/40
24/40
24/40
29/42
24/40
29/42
45/50

Order
Code
6945-266
6945-268
6945-270
6945-274
6945-276
6945-278
6945-280
6945-282
6945-284

Each
849.92
879.83
901.08
933.60
946.65
953.17
998.89
1005.41
1039.36

7127 FLASK Volumetric, Pilot Plant


Large capacity volumetric flask with outer joint, without graduation mark. Supplied
without stopper.
7127

Capacity,
mL
5000
10000

Flask only
Joint
34/28
40/35

Order Code
7127-25
7127-30

Stopper only

Each
202.74
290.74

Order Code
8255-18
8255-20

Each
30.08
45.82

Guide to Flange Styles


Schott-Duran
Flange

(with or without ORing


groove)

(with or without ORing


groove)

Conical Flange

KF Plane Flange

Beaded
Process Pipe
Flange

Uses Clamp:
6508, 6509, 6510
Flat clamp

Uses Clamp:
6517
Quick release clamp

Uses Clamp:
6496
Standard clamp

Uses Clamp:
6525
Coupling

Uses Clamp:
8856
Coupling

Flat Flange

See page 8 for flange dimensions.

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Subject to Ace Discount (Page 4)

Net

Components / Heads

113

6472 HEAD Glass, Flat, Pilot Plant


Borosilicate glass head with holes drilled to match (included) 6413 PTFE inserts. Head is
11/4inch (32mm) thick, designed for use with 300mm (12-inch) flat ground flanges on reaction
flasks. Use 6525 clamp assembly. Requires 6472-161 bolt/nut assembly (not included).
Center Joint
45/50
45/50

Side Joints
(4) 45/50; (2) 29/42
(4) 45/50; (2) 29/32; (1) 71/60

Accessories
71/60 Stopper
300mm Coupling
Nuts & Bolts, 8 inch length

Order Code
6472-20
6472-21

Each
2018.25
2225.25

Order Code
8250-28
6525-30
6472-161

Each
161.88
1056.54
11.74

6472-21

6472 HEAD Stainless Steel, Pilot Plant


Reaction flask head fabricated from 316 stainless steel. Replaces flat or domed glass
heads. This 1/4-inch thick head has the same openings as the flat glass head and accepts
PTFE joint inserts secured top and bottom of plate with threaded nuts. 10L size uses
one 45/50, three 29/42 and three 24/40 inserts; 30L and 50L sizes use five 45/50
and two 29/42 inserts (6472-17 also requires a 71/60 insert). See 6412 (below) for
inserts. Stainless head is assembled to reaction flask in the same manner as flat glass head
using 6525 coupling (not included) and one spacer. Optional: flat sheet of PTFE covers
entire underside of stainless steel head and is secured by coupling and joint inserts.

Description
Head only
Head only
Head only
Flat PTFE cover only
Flat PTFE cover only
Flat PTFE cover only

For
Uses
Diameter, Reactor Number of
Coupling
mm
Size
Openings
6525-25
200
10L
7
6525-30
300
30L & 50L
7
6525-30
300
30L & 50L
8

200
10L
7

300
30L & 50L
7

300
30L & 50L
8

Order
Code
6472-25
6472-26
6472-17
6472-29
6472-30
6472-15

6472-17

Each
822.56
835.47
Call
197.90
219.16
295.00

6472-26

6412 JOINT INSERTS PTFE, Standard Taper, for Stainless Steel Heads
Solid, virgin PTFE, standard taper joint inserts for 6472 series stainless steel, flat heads
for ACE reactors. Top of insert is machined for outside standard taper joint that matches
glass inner standard taper joints. Bottom is reverse threaded and has a PTFE collar and
FETFE o-ring for attaching to the flat heads. Tops are also machined to accept the 7597
joint clips. 71/60 size fits glass stopper for 71/60 sample port on 6472-17 head.
For

Joint Size
24/40
29/42
45/50
71/60

Order Code Each


6412-05
76.50
6412-07
90.78
6412-09
111.18
6412-11
162.18

6412

6413 JOINT INSERTS PTFE, Standard Taper, for Flat Glass Heads
Solid, virgin PTFE, standard taper joint inserts for 6472 series flat glass heads. This low
profile insert allows for increased working space above the head. The insert is secured
to the head with a reverse threaded locking nut and sealed using a FETFE o-ring. The
top of the insert is formed to allow the use of 7597 joint clips.
For

Joint Size
24/40
29/42
45/50
71/60

Order Code Each


6413-05
76.50
6413-07
90.78
6413-09
111.18
6413-11
162.18

6413

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Components / Heads

IN C O R
S
S

P
ATED

ACE G

OR

VI

USA
N
NE
LAND,

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

114

Components / Heads
6433 HEAD For Pressure or Filter Reactors, AceThreds
Reactor head, only, with Schott-Duran style flange and AceThreds for use with 6384,
6386 or 6388 reactor bodies. Pressure rating is 35 psi. Uses 6517 quick release clamp.
For Flask
Cap., mL
150-600
1000-2000
3000-6000

Flange I.D.,
mm (in.)
60 (2.4)
100 (4)
150 (6)

Center
Neck
#15
#15
#15

Side Necks
(2)#15-(1)#7
(3)#15-(1)#7
(4)#15-(1)#7

Order Code
6433-23
6433-35
6433-44

115

6433-23

Each
295.48
396.77
544.04

6433-35

6484 HEAD Reaction, Conical Flange, 4 Necks

6484

Standard 4-inch (100mm) head for use with 6475, 6476, 6477, 6479, 6480, 6481, 6491,
and 6492 ACE reaction flasks. Supplied with three outer joints in line, plus a 10/30
joint for a ground joint thermometer or 8299 thermometer adapter. Use 6496 clamp for
securing to flasks. Uses 6495 gaskets.
Center
Joint
24/40
29/42
45/50

Side
Joints
24/40
24/40
24/40

Thermometer
Joint
10/30
10/30
10/30

Order Code
6484-10
6484-20
6484-40

Each
254.31
266.40
275.48

6485 HEAD Reaction, AceThred, Conical Flange, 4 Necks

6485

Standard 4-inch (100mm), four-outlet head for use with 6475, 6476, 6477, 6479, 6480,
6481, 6491, and 6492 ACE reaction flasks. Supplied with three outer joints in line, plus a
thermometer side neck which is internally threaded (with #7 AceThred) for use with 5029
nylon bushing. Use of the threaded side neck permits easy adjustment of thermometer
depth. Use 6496 clamp for securing to flasks. Supplied complete with 5029 bushing and
FETFE oring. For extra bushings, see 5029-10. For extra FETFE orings, see 7855-704.
Uses 6495 gaskets.
Center Joint
24/40
29/42

Side Joints
(2) 24/40; (1) #7
(2) 24/40; (1) #7

Order Code
6485-16
6485-22

Each
268.18
270.37

6486 HEAD Reaction, Conical Flange, 3 Necks

6486

Standard 4-inch (100mm), three-outlet head for use with 6475, 6476, 6477, 6479, 6480,
6481, 6491, and 6492 ACE reaction flasks. Supplied with three outer joints. Use 6496
clamp for securing to flasks. Uses 6495 gaskets.
Center Joint
24/40
29/42
29/42
45/50

Side Joints
24/40
24/40
29/42
24/40

Order Code
6486-10
6486-20
6486-25
6486-40

Each
232.01
238.00
240.51
245.01

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

116

Components / Heads
6487 HEAD Reaction, Conical Flange, 3 Necks

6487

Standard 4-inch (100mm), three-outlet head for use with 6475, 6476, 6477, 6479, 6480,
6481, 6491, and 6492 ACE reaction flasks. Supplied with three socket joints. Use 6496
clamp for securing to flasks. Uses 6495 gaskets.
Center Joint
35/25

Order Code
6487-25

Side Joints
35/25

Each
268.74

6488 HEAD Reaction, Conical Flange, 4 Necks

6488

This standard 4-inch (100mm) head has three outer joints in line, plus a 14/35 side
joint which takes a 5021, 5028-26 or 8300-07 bushing adapter to be used with ACE 8314
10/30 thermometer. The 6500 thermometer well can also be used with this head, when
using a standard thermometer. For use with 6475, 6476, 6477, 6479, 6480, 6481, 6491,
and 6492 ACE reaction flasks. Use 6496 clamp for securing head to flask.
Center
Joint
24/40
29/42
29/42
45/50

Side
Joints
24/40
24/40
29/42
24/40

Thermometer
Joint
14/35
14/35
14/35
14/35

Order Code
6488-10
6488-15
6488-20
6488-40

Each
252.82
261.60
267.50
276.12

6489 HEAD Reaction, Conical Flange, 4 Necks


6489

Standard 4-inch (100mm) head with three socket joints in line, plus a 14/35 side joint
for thermometer. Use 6496 clamp for securing to flasks. For use with 6475, 6476, 6477,
6479, 6480, 6481, 6491, and 6492 ACE reaction flasks.
Center
Joint
35/25

Side
Joint
35/25

Thermometer
Joint
14/35

Order Code
6489-20

Each
281.51

6490 HEAD Reaction, Stainless Steel, Conical Flange, 3 Necks

6490-17

Fabricated from 18-8 type 316 electro-polished, heliarc-welded stainless steel.


Interchangeable with our glass flasks. Fits all ACE four-inch conical neck reaction flasks
such as 6469, 6475, 6476, 6477, 6479, 6480, 6481, 6491, 6492, 6497, 6498 and 9656.
Use 6496 clamp for securing head to flask.
Center Joint
24/40
29/42
29/42
35/25

Side Joints
24/40
24/40
29/42
35/25

Order Code
6490-12
6490-17
6490-22
6490-27

6490-27

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Each
Priced
Upon
Request

Components / Heads
6499 HEAD Reaction, Conical Flange, 4 Necks

6499

Conical flange with 4-inch (100mm) opening. One center joint and three side necks.
Similar to 6488 series except all the side necks are 24/40. For use with 6475, 6476, 6477,
6479, 6480, 6481, 6491, and 6492 ACE reaction flasks Use 6496 clamp to secure head.
Center Joint
24/40
29/42
45/50

(3) Side Joints


24/40
24/40
24/40

Order Code
6499-10
6499-14
6499-18

117

Each
280.59
285.17
297.77

6512 HEAD Reaction, Flat Flange, 3 Necks

6512

For use with 6511 ground flat flange flasks. With three in-line joints. Uses 6508 or 6510
clamps.
For Flask
Cap., mL
1000
2000-4000
2000-4000
2000-4000

Center
Joints
24/40
24/40
29/42
45/50

(2) Side
Joints
24/40
24/40
24/40
24/40

Order Code
6512-16
6512-20
6512-24
6512-28

Each
271.96
293.65
309.75
329.96

6513 HEAD Reaction, Flat Flange, 4 Necks, with #7 AceThred

6513

For use with 6511 ground flat flange flasks. With three in-line joints and a #7 AceThred,
internally threaded side opening for thermometer (#7 accepts 6-7mm O.D.). Thread forms a
compression seal with 5029 nylon bushing and permits vertical adjustment of thermometer.
Supplied complete with bushing and FETFE oring. Uses 6508 or 6510 clamps.
For Flask
Cap., mL
1000
2000-4000
2000-4000
2000-4000

Center
Joints
24/40
24/40
29/42
45/50

(2) Side
Joints
24/40
24/40
24/40
24/40

Order Code
6513-26
6513-30
6513-34
6513-38

Each
299.58
316.60
330.61
351.51

6515 HEAD Reaction, Flat Flange, 4 Necks


For use with 6511 ground flat flange flasks. With three in-line joints and a 10/30 side
joint for thermometer. Uses 6508 or 6510 clamps.
For Flask
Cap., mL
1000
2000-4000
2000-4000
2000-4000

Center
Joints
24/40
24/40
29/42
45/50

Side
Joints
(2) 24/40; (1) #7
(2) 24/40; (1) #7
(2) 24/40; (1) #7
(2) 24/40; (1) #7

6515
Order Code
6515-46
6515-50
6515-54
6515-58

Each
294.29
312.62
327.92
356.63

All ACE full-length outer joints are tooled with reinforcement


rings for added strength and stability.

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

118

Components / Heads

6527-26

6527/6528/6529 HEAD For Filter Reactors


Reactor head, only, with Schott-Duran style flange and joints for use with 6384, 6386
or 6388 reactor bodies. 6527-26 has three angled 24/40 joints; 6528-31 and 6529-32
have four vertical 24/40 joints. Use 6517 clamp.
For Flask
Cap., mL
150-600
1000-2000
3000-6000

# of
Necks
3
4
4

Flange I.D., mm (in.)


60 (2.4)
100 (4)
150 (6)

Order Code
6527-26
6528-31
6529-32

Each
278.81
281.42
387.69

6528-31/6529-32

6528 HEAD Reaction, Schott-Duran Flange, 4 Necks

6528-31

Flat ground Schott-Duran style flange for use with all reaction flasks that have a 100mm
(4-inch) Schott-Duran ground mating flange. Supplied with three in-line ground joints
and one side joint. For clamp, order 6517-25.
Center Joint
24/40
29/42
45/50

Flange I.D.,
mm (in.)
100 (4)
100 (4)
100 (4)

(3) Side Joints


24/40
24/40
24/40

Order Code
6528-31
6528-35
6528-38

Each
281.42
282.28
296.74

6528 HEAD Reaction, Schott-Duran Flange, 5 Necks


Flat ground Schott-Duran style flange for use with all reaction flasks that have a 100mm
(4-inch) Schott-Duran ground mating flange. Supplied with three in-line ground joints
and two side joints, for thermal probe connection, etc. For clamp, order 6517-25.
Center Joint
24/40
29/42
29/42
45/50

Flange I.D.,
mm (in.)
100 (4)
100 (4)
100 (4)
100 (4)

(4) Side Joints


24/40
24/40
29/42
24/40

Order Code
6528-42
6528-44
6528-46
6528-49

6528-44

All ACE full-length outer joints are tooled with reinforcement


rings for added strength and stability.

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Each
308.50
308.72
310.39
324.05

Components / Heads
6529 HEAD Reaction, Schott-Duran Flange, 4 Necks

119

6529-39

Flat ground Schott-Duran style flange for use with all reaction flasks that have a 150mm
(6-inch) Schott-Duran ground mating flange. Supplied with four ground joints. For
clamp, order 6517-27.
Center Joint
24/40
29/42
45/50

Flange I.D.,
mm (in.)
150 (6)
150 (6)
150 (6)

(3) Side Joints


24/40
24/40
24/40

Order Code
6529-32
6529-36
6529-39

Each
387.69
391.40
411.13

6529 HEAD Reaction, Schott-Duran Flange, 5 Necks


Flat ground Schott-Duran style flange for use with all reaction flasks that have a 150mm
(6-inch) Schott-Duran ground mating flange. Supplied with five ground joints. For
clamp, order 6517-27.
Center Joint
24/40
29/42
29/42
45/50

Flange I.D.,
mm (in.)
150 (6)
150 (6)
150 (6)
150 (6)

(4) Side Joints


24/40
24/40
29/42
24/40

Order Code
6529-23
6529-25
6529-27
6529-29

Each
390.96
391.19
392.04
438.72

6529-25

6529 HEAD Reaction, Schott-Duran Flange, 4 Necks


Flat ground Schott-Duran style flange for use with all reaction flasks that have a 150mm
(6-inch) Schott-Duran ground mating flange. Supplied with two in-line ground joints
and one side, 10/30 joint, for thermal probe connection, etc. For adapter with #7
AceThred for connecting thermometer or other type probe and permits easy vertical
depth adjustment, see 5028. For clamp, order 6517-27.
Center Joint
24/40
29/42
29/42
45/50

Flange I.D.,
mm (in.)
150 (6)
150 (6)
150 (6)
150 (6)

(2) Side Joints


24/40
24/40
29/42
24/40

Order Code
6529-03
6529-04
6529-05
6529-06

6529

Each
371.08
374.60
333.01
388.06

All ACE full-length outer joints are tooled with reinforcement


rings for added strength and stability.

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

120

Components / Heads
6530 HEAD Reaction, Schott-Duran Flange
Flat ground Schott-Duran style flange for use with all reaction flasks that have a 200mm
(8inch) Schott-Duran ground mating flange. Supplied with one through seven ground
joints. For clamp, order 651731.

6530-33

Center Joint
45/50
45/50
45/50
45/50
45/50
45/50
45/50
45/50
45/50
45/50

Flange I.D.,
mm (in.)
200 (8)
200 (8)
200 (8)
200 (8)
200 (8)
200 (8)
200 (8)
200 (8)
200 (8)
200 (8)

Side

Joints

(3) 24/40
(2) 29/42
(3) 29/42
(3) 45/50
(2) 45/50 (2) 29/42
(4) 24/40
(3) 45/50 (3) 29/42
(2) 29/42 (2) 24/40
(2) 45/50

Order Code
6530-32
6530-30
6530-33
6530-31
6530-34
6530-35
6530-36
6530-38
6530-39
6530-40

Each
425.01
626.07
594.98
749.14
938.98
984.56
992.36
1009.37
981.02
975.35

6530 HEAD Domed, Schott-Duran Flange, 6 Necks, 60mm Side Port


6530-37

Domed-style glass head with Schott-Duran style 200mm (8-inch) flange for use with
matching flanged reactor flasks like 6472-02, 6472-16, 6522-21, etc. Features a
Schott-Duran flange 60mm (2.4-inch) I.D. side port with oring groove, angled 45
degrees, for ease in adding materials to the reactor. In addition to the 60mm port,
head has a 45/50 center neck, (1) 45/50, (2) 29/42, and (2) 24/40 side necks.
Complete item includes head, 60mm glass cap, CAPFE (PTFE encapsulate silicone)
oring, and 60mm quick release clamp. Main head uses 6517-31 quick release clamp
(not included).
HEAD, only, 200mm (8-inch) flange
GLASS CAP, 60mm
CAPFE ORing, 60mm
CLAMP, 60mm, Quick Release
COMPLETE

6530-45

Order Code
6530-37
15312-30
7855-878
6517-22
6530-50

Each
1095.60
60.05
28.10
87.08
1270.83

6530 HEAD Domed, KF Plane Flange, 7 Necks, 100mm Side Port


Domed-style glass head with 300mm (12-inch) flat KF plane flange for use with
matching reactor flasks like 647203, 647205, 6472030, 6472050 etc. Features a
large Schott-Duran flange 100mm (4-inch) I.D. side port with oring groove, angled 30
degrees, for ease in adding materials to the reactor. In addition to the 100mm port,
head has a 45/50 center neck, (4) 45/50, and (2) 29/42 side necks. Complete
item includes head, 100mm glass cap, CAPFE (PTFE encapsulate silicone) oring,
and 100mm quick release clamp. Main head uses 6525-30 clamp (not included).
HEAD, only, 300mm (12-inch) KF flange
GLASS CAP, 100mm
CAPFE ORing, 100mm
CLAMP, 100mm, Quick Release
COMPLETE

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Order Code
6530-45
15312-33
7855-880
6517-25
6530-60

Each
2562.18
107.78
28.63
98.23
2796.82

Components / Heads
6530 HEAD Domed, Schott-Duran Flange, 5 Necks, 60mm Side Port

121

6530-85

Domed-style glass photochemical reactor head with Schott-Duran style 200mm (8-inch)
flange for use with matching flanged reactors and flasks like 6472-02, 6472-16, 6522-21,
6524-73, etc. Features a Schott-Duran flange 60mm (2.4inch) I.D. side port with oring
groove, angled 45 degrees, for ease in adding materials to the reactor. In addition to the
60mm port, head has a 45/50 center neck, (1) 45/50, (1) 29/42, (1) 24/40, and (1)
#50 AceThred side necks.
HEAD, only, 200mm (8-inch) flange
GLASS CAP, 60mm
CAPFE ORing, 60mm
CLAMP, 60mm, Quick Release

Order Code
6530-85
15312-30
7855-878
6517-22

Each
1213.52
60.05
28.10
87.08

6472 HEADDomed, KF Plane Flange, 7 Necks

6472-23

Domed-style glass head with 300mm (12-inch) flat KF plane flange for use with matching
reactor flasks like 647203, 647205, 6472030, 6472050 etc. Head has a 45/50 center
neck, (4) 45/50, and (2) 29/42 side necks. Uses 6525-30 clamp (not included).
Order Code
6472-23

HEAD, only

Each
2379.08

12858 HEADPTFE, Reaction Flask, 60mm


60mm PTFE heads allow for various combinations of jointed and/or compression fitting
openings as well as the ability to plug unused openings. For use with any Schott-Duran
style, o-ring grooved flanged reaction vessels such as ACE codes 6521, 6522, 6523,
6524 and 6526. For fittings, see ACE codes 12866, 12867, 12869 and 12871. Uses 6517
quick release clamps.

12858-15

A) vertical 1/2-inch center neck for PTFE standard taper adapter


B) 10 x 10 1/2-inch compound angle side neck
C) vertical 1/4-inch side neck
Order Code
12858-10
12858-15

Number of
openings
4
4

Each
208.12
193.24

12858-10

All ACE full-length outer joints are tooled with reinforcement


rings for added strength and stability.

See page 121 for PTFE adapters, plugs, and connectors.

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

122

Components / Heads

PTFE Inserts
Description

NPT
Size
(In.)

for PTFE Reaction Vessel Heads

Order
Code

Each

Joint Inserts
19/38 PTFE
Standard Taper Adapter,
Outer
19/38 PTFE
Standard Taper Adapter,
Outer
24/40 PTFE
Standard Taper Adapter,
Outer
24/40 PTFE
Standard Taper Adapter,
Outer
24/40 PTFE
Standard Taper Adapter,
Outer
29/42 PTFE
Standard Taper Adapter,
Outer
29/42 PTFE
Standard Taper Adapter,
Outer
29/42 PTFE
Standard Taper Adapter,
Outer
29/42 PTFE
Standard Taper Adapter,
Outer
45/50 PTFE
Standard Taper Adapter,
Outer
45/50 PTFE
Standard Taper Adapter,
Outer
45/50 PTFE
Standard Taper Adapter,
Outer

Order
Code

Each

AceThred Compression Fittings


1/2

12866-05 40.48

3/4

12866-08 40.51

1/2

12866-14 45.62

3/4

12866-16 45.59

12866-18 50.56

1/2

12866-21 63.25

3/4

12866-23 63.26

12866-25 65.72

1-1/2 12866-27 88.51


3/4

12866-33 100.08

12866-35 110.59

1-1/2 12866-37 106.30

Plugs
PTFE Plug
PTFE Plug
PTFE Plug
PTFE Plug

Description

NPT
Size
(In.)

1/4
1/2
3/4
1

12867-04
12867-12
12867-18
12867-24

11.74
14.86
19.93
24.57

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

PTFE AceThred
#7-NPT
PTFE AceThred
#7-NPT
PTFE AceThred
#11-NPT
PTFE AceThred
#15-NPT
PTFE AceThred
#18-NPT
PTFE AceThred
#25-NPT
PTFE AceThred
#25-NPT

1/4

12871-03 56.38

1/2

12871-07 58.87

1/2

12871-11 61.38

3/4

12871-14 81.42

3/4

12871-18 83.95

12871-25 86.46

1-1/2 12871-28 93.96

Supplied with 5029 PTFE Bushing for #7 thread


and 7506 PTFE Bushing for all other threads.

Components / Heads

123

12860 HEADPTFE, Reaction Flask, 100mm,

12860-25

100mm PTFE heads allow for various combinations of jointed and/or compression fitting
openings as well as the ability to plug unused openings. For use with any Schott-Duran
style, o-ring grooved flanged reaction vessels such as ACE codes 6521, 6522, 6523,
6524 and 6526. For fittings, see ACE codes 12866, 12867, 12869 and 12871. Uses 6517
quick release clamps.
A) vertical 3/4-inch center neck for PTFE standard taper adapter
B) vertical 3/4-inch side neck for PTFE standard taper adapter
C) 10 x 10 1-inch compound angle side neck
D) vertical 1/4-inch side neck
E) 10 angled 3/4-inch side neck
12860-12

Order Code
12860-12
12860-25

Number of
Openings
7
7

Each
348.95
402.49

12862 HEADPTFE, Reaction Flask, 150mm

12862

150mm PTFE heads allow for various combinations of jointed and/or compression fitting
openings as well as the ability to plug unused openings. For use with any Schott-Duran
style, o-ring grooved flanged reaction vessels such as ACE codes 6521, 6522, 6523,
6524 and 6526. For fittings, see ACE codes 12866, 12867, 12869 and 12871. Uses 6517
quick release clamps.
A) vertical 1-inch center neck for PTFE standard taper adapter
B) vertical 1-inch side neck for PTFE standard taper adapter
C) 10 x 10 1-inch compound angle side neck
D) vertical 1/2-inch side neck
Order Code
12862-16

Number of
Openings
9

Each
561.95

12864 HEADPTFE, Reaction Flask, 200mm,

12864-20

200mm PTFE heads allow for various combinations of jointed and/or compression fitting
openings as well as the ability to plug unused openings. For use with any Schott-Duran
style, o-ring grooved flanged reaction vessels such as ACE codes 6521, 6522, 6523,
6524 and 6526. For fittings, see ACE codes 12866, 12867, 12869 and 12871. Uses 6517
quick release clamps.
A) vertical 1-inch center neck for PTFE standard taper adapter
B) vertical 1-1/2-inch side neck for PTFE standard taper adapter
C) 10 x 10 1-inch compound angle side neck
D) vertical 1/2-inch side neck for PTFE standard taper adapter
E) 10 x 10 1-1/2-inch compound angle side neck
F) 10 angled 1-inch side neck

12864-27

Order Code
12864-20
12864-27

Number of
Openings
8
8

Each
723.33
866.52

Blank heads and custom configurations available. See page 121


for PTFE adapters, plugs, and connectors.

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

124

Components / Heads
6525 COUPLING, ACCESSORIESFor KF Style Flange
Coupling for clamping reaction flask to reaction flask heads like 653045. Complete
652525 or 652530 coupling consists of two plastic, phenolic resin rings, set of three
clamp inserts with clamp insert clips, and appropriate number of stainless steel bolts,
springs, nuts and washers. The 652572 or 652674 inserts are placed inside the coupling
and used with the 6525-80 clamp insert clips to firmly secure the flask to the head. Preset
optional T-handle torque wrench, 30 in-lbs maximum, and 1/4inch socket are available
for safe tightening of coupling. Gaskets (required), wrench, and socket are not included
with coupling, and must be ordered separately.

6525-25,
-30

6525-72,
-74

Description
Coupling, Complete
Coupling, Complete
Accessories
Torque Wrench, only
1/4-inch Socket, only
Replacement Parts
Clamp Insert (each insert = 3 arcs)
Clamp Insert (each insert = 3 arcs)
Clamp Insert Clips (package of three)

Size
200mm
300mm

Order Code
6525-25
6525-30

Each
840.64
1056.54

6525-60
6525-61

144.09
10.69

200mm
300mm

6525-72
6525-74
6525-80

59.46
160.80
6.21

Note: Flat heads require 6525 coupling, but with 6472-161 (longer) bolts/nuts

6525 GASKET
PTFE crescent ring L shaped gaskets for use with 6525 coupling. These gaskets are
placed between the flat ground glass surfaces of the head and flask. Consists of a flat
ring with locating skirt. Temperature limit, 200C.
6525-51

Size
200mm
300mm

Order Code
6525-46
6525-51

Each
164.23
326.26

Color Coated Glassware


Ace Glass offers many of our existing
glass vessels in various coated versions.
Flasks, Pressure Bottles, Beakers,
Bottles and many other items listed
in this catalog can be amber or color
coated on request. The coating is a
proprietary process and gives excellent
UV protection characteristics. Contact
ACE for more details and pricing.

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Components / Adapters

125

5021/9061 ADAPTERReducing
Reducing adapter, bushing type, larger outside
Top
Inside
10/18
10/30
10/30
10/30
10/30
10/30
14/20

Bottom
Outside
14/20
14/20
14/35
19/38
24/40
29/42
19/22

Order
Code
9061-05
9061-10
5021-05
5021-07
5021-09
5021-12
9061-16

Each
31.70
31.70
36.10
38.47
41.53
45.16
31.70

Top
Inside
14/20
14/20
14/35
14/35
14/35
19/38
19/38

Bottom
Outside
24/40
29/42
19/38
24/40
29/42
24/40
29/42

Order
Code
5021-14
5021-15
5021-18
5021-20
5021-22
5021-24
5021-26

joint, smaller inside


Each
36.21
40.10
35.53
39.53
43.11
37.41
43.06

Top
Inside
24/40
24/40
29/42
24/40
29/42
34/45

Bottom
Outside
29/42
34/45
34/45
45/50
45/50
45/50

joint.

Order
Code
5021-28
5021-30
5021-35
5021-36
5021-94
5021-39

Each
42.04
54.42
66.77
88.33
88.63
88.94

5021
9061

I
AT

S IN N O
AS
L
5028 ADAPTERVMini #7 AceThred, with PTFE Ferrule
ON

AC E

With inner joint atTH bottom and #7 AceThred at top. Suitable for most vacuum work.
Supplied complete with nylon bushing and PTFE ferrule in place of oring. For extra
ferrules, order 1171007.
A N N I V E R S A R Y

Bottom Joint
14/20
N 24/40
E

1936 2011

LAND

Order Code
5028-27
5028-31

Complete
27.95
28.05

5028-27

5028 ADAPTER Electrode, Mini #7 AceThred


With inner joint at bottom and #7 AceThred at top. For use with any probes up to 8mm
diameter. Suitable for most vacuum work. Supplied complete with 5029-30 nylon bushing
and FETFE oring. For extra orings, order 7855-704.
Bottom Joint
14/20
24/40

Order Code
5028-117
5028-119

Complete
32.39
34.63

5028-117

6500 THERMOWELL with Joint


For reaction flasks, can be used with either cylindrical or spherical type. With 14/35
joint. Length measurement is distance below joint to bottom of tube.
For Flask
Cap., mL
500
1000
1500
2000
3000

Length
mm,
190
230
270
310
325

Order
Code
6500-01
6500-02
6500-03
6500-20
6500-04

Each
32.32
32.32
32.32
34.10
35.64

For Flask
Cap., mL
5000
12000
22000
50000
72000

Length
mm,
360
400
475
582
600

Order
Code
6500-05
6500-06
6500-08
6500-10
6500-12

6500

Each
35.87
37.90
47.74
54.52
67.07

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

126

Components / Adapters
5029 BUSHING Nylon or PTFE, #7 AceThred
If orings are a
problem, see 11710,
PTFE ferrules
for use with
AceThreds.

Machine threaded nylon or #7 AceThred PTFE bushing with hole in center or solid. For
use with 5027, 5028, 5031, 5032, 5034, 5086, 5092, 5101, 5136, 5261, 5263 and other
apparatus with #7 internal threads. Two FETFE orings supplied with bushing. Note: Solid
bushing is for drilling different size hole, only. NOT intended for use as a stopper. For
stoppers, see 5803 or 5846. Nylon version has a maximum temperature of 100C.
PTFE version has a maximum temperature of 160C.
Nylon
With 7.5mm hole
With 8mm hole
Solid
With 7.5mm hole, for use
with PTFE Ferrule

5029

Order Code
5029-10
5029-30
5029-20

PTFE
Each
2.77
8.65
8.28

Order Code
5029-35
5029-31
5029-40

Each
14.08
14.08
13.85

5029-45
7855-704

14.08
13.68

5029-12
2.91
Extra FETFE ORings

5030/7506/8042 ADAPTER Maxi #15 Ace-Thred


5030-40

With ground joint at bottom and #15 Ace-Thred at top. Will accept tubes with diameters
of 12.5 to 14mm such as electrodes, inlet and outlet tubes, etc. Suitable for most vacuum
work. Supplied complete with nylon bushing and FETFE oring. For extra orings, order
7855-716.

5030-44
Bottom
Joint
24/40
29/42
45/50
35/25

Glass Only
Order
Code
Each
8042-15 31.22
8042-17 33.38
8042-21 50.57
8042-35 35.92

Nylon Bushing Only


Order
Code
Each
7506-06
12.35
7506-06
12.35
7506-06
12.35
7506-06
12.35

Complete
Order
Code
Each
5030-40 43.57
5030-42 45.73
5030-45 62.92
5030-44 48.27

5030/7506/8067 ADAPTER Giant #25 or #36 AceThred


With ground inner joint at bottom and either a #25 or #36 AceThred that accepts outside
diameters of 24-25mm and 34-35mm, respectively (Note: Joint size limits size O.D. of
inserted tube). Complete item supplied with nylon bushing and FETFE oring. For oring
replacements, see Reference Guide to AceThreds on page 5.
Bottom AceThred
Joint
Size
24/25
#25
24/25
#36
45/50
#36
45/50
#25
50/55
#25
71/60
#25
55/50
#36

5030-70

Glass Only
Order
Code
Each
5030-52 35.83
5030-55 60.00
5030-78 77.88
8067-18 106.40
8067-20 102.13
8067-22 112.06
8067-24 104.94

Nylon Bushing Only


Order
Code
Each
7506-10
21.17
7506-12
50.46
7506-12
50.46
7506-10
21.17
7506-10
21.17
7506-10
21.17
7506-12
50.46

Complete
Order
Code
Each
5030-70 57.00
5030-76 110.46
5030-80 128.34
5030-84 127.57
5030-86 123.30
5030-88 133.23
5030-90 155.40

5031 ADAPTER Twin AceThred


With inner joint at bottom and two offset AceThred ports at top. Two threaded openings
enable you to insert two inner tubes, such as a thermometer and bleed tubes, through
the same joint. The 24/25 medium length joint is compatible with 24/40 full length
outer joints. Supplied complete with two nylon bushings and FETFE orings. For extra
orings, order 7855-704 (for #7), 7855-708 (for #11) or 7855-716 ( for #15).
5031

Thread Size
#7
#7
#11
#15
#11 & #15

Joint
24/25
29/42
45/50
45/50
45/50

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Order Code

Each

5031-10
5031-12
5031-24
5031-33
5031-86

79.08
83.26
99.60
106.17
119.50

Subject to Ace Discount (Page 4)

Net

Components / Adapters
5032 ADAPTER Offset, #7 AceThred
Thermometer adapter with inner joint at bottom and top threaded piece offset and angled
approximately 10 for use in multiple neck flasks. Threaded nylon bushing tightens into glass
piece to form an oring compression seal with thermometers, bleed tubes, etc. up to 7mm
diameter. Thread at top not only allows for variable vertical positioning of thermometers,
etc. but also, because of the 10 angle, by rotating joint you can position the thermometer in
the bottom of the flask. Supplied complete with nylon bushing and FETFE oring. For extra
orings, order 7855-704. For extra bushings, order 5029-10.
Bottom Joint
19/22
24/40
29/42

Order Code
5032-18
5032-22
5032-25

5040
9074

With inner joints at bottom and side, reinforced outer joint at top.
Side Inner
Joint
14/20
19/22
24/40
29/42
45/50

Order
Code
9074-02
9074-04
5040-10
5040-12
5040-96

Bottom Inner
Joint
14/20
19/22
24/40
29/42
45/50

Each
48.70
49.16
56.65
58.67
169.62

5050 ADAPTER 105 Side Arm

5050-10

With reinforced outer joints at top and side, inner joint at bottom.
Joints

5032

Complete
40.00
34.31
37.09

5040/9074 ADAPTER 75 Side Arm


Top Outer
Joint
14/20
19/22
24/40
29/42
24/40

127

Order Code

Each

5050-10
5050-12

58.60
60.25

24/40
29/42

5050 ADAPTER 105 Side Arm, with AceThred


With reinforced outer joint on side, inner joint at bottom, and AceThred at top. Not
supplied with bushing and FETFE oring, which must be ordered separately.
Joints
45/50
45/50

AceThred
Size
#25
#15

Order Code
5050-86
5050-96

Each
172.91
169.40

Bushing w/FETFE ORing, only


Bushing w/FETFE ORing, only

For Size
#15
#25

Order Code
7506-06
7506-10

Each
12.35
21.17

5050-86

5090 ADAPTER 75 Angle


With

joint at bottom and side. Top thermometer joint is for 76mm immersion.
Top Outer
Joint
10/30
10/30

Immersion
Depth
76mm
76mm

Side Inner
Joint
24/40
29/42

Bottom Inner
Joint
24/40
29/42

Order
Code
5090-10
5090-15

Each
54.70
59.40

5090

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

128

Components / Adapters

5221-20

5221-05

5221 ADAPTER Connecting, Outer Socket Joint, Glass

5221-24

For connecting to comparable oring/ball joints.


Outer Joint Connects to
10mm tube
#11 AceThred
#15 AceThred
3/4-inch tube
#15 AceThred
#25 AceThred

5221-28

Size
28/15
28/15
28/15
35/25
35/25
35/25

Order Code
5221-05
5221-09
5221-11
5221-20
5221-24
5221-28

Each
27.40
33.57
39.05
28.77
36.64
39.05

5221-11

5221-09

5263 ADAPTER Multineck, Mini #7 AceThred


With inner joint at bottom, two #7 AceThreds and one side reinforced outer joint at
top. AceThreds would commonly be used for thermometers and gas inlet tubes thus
leaving joint for condenser, addition funnel, still head, etc. 24/25 medium length bottom
joint is compatible with 24/40 full length joint. Supplied complete with two 5029-10
nylon bushings and FETFE orings. For extra FETFE orings, order 7855-704.
Top Outer
24/40

Bottom Inner
24/25

Order Code
5263-17

Each
126.79

5263

5268/9089 ADAPTEROffset
WITHOUT BOTTOM DRIP TIP

5268-54
9089-40

5268-10
9089-08

5268-35

Joints
14/20
24/40
29/42
45/50
35/25

Order Code
9089-08
5268-10
5268-15
5268-21
5268-35

Each
25.36
36.56
40.74
109.58
48.17

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

WITH BOTTOM DRIP TIP


Joints
14/20
24/40
29/42
45/50

Order Code
9089-40
5268-54
5268-56
5268-58

Each
34.88
37.33
41.60
110.94

Subject to Ace Discount (Page 4)

Net

Components / Adapters
5278 ADAPTER pH Probe, Pilot Plant
Adapter tube, 25mm O.D., with a #15 AceThred at one end, other end open.
Insert 1/2-inch probe in open end down to and through the AceThred, leaving
enough exposed to secure with 7506 bushing and size 110 FETFE oring to make
a compression seal. Adapter tube is held in flask joint with 5030 maxi adapter
with nylon bushing and size 212 FETFE oring, again with a compression seal,
thus making the tube vertically adjustable. Complete item consists of glass adapter
tube, 7506 PTFE bushing with size 110 FETFE or Chemraz oring and 5030 maxi
adapter. Takes any standard size pH probe.
With FETFE ORing
Length,
cm (Inches)
61 (24)
91 (36)
122 (48)

Order Code
5278-40
5278-44
5278-48

With Chemraz ORing

Each
146.63
147.40
148.16

Order Code
5278-141
5278-145
5278-149

Each
194.96
195.73
196.49

129

5278

5278-14
Adapter Tube
7506 Bushing

Adapter, Maxi
8067-18

Replacement Items:
ADAPTER TUBE, Glass only
Length,
Order
cm (Inches)
Code
Each
61 (24)
5278-14
22.14
91 (36)
5278-18
22.91
122 (48)
5278-23
23.67

Bottom BUSHING, PTFE only, with ORing


For Thread ORing
Order
Size
Type
Code
Each
15
FETFE
7506-27
40.65
15
Chemraz
7506-127
88.98

ADAPTER, Maxi, #25 AceThred to 45/50 Joint, only

Complete item includes glass member, nylon bushing and size 212 FETFE o-ring.
Joint
45/50

Glass Member
Order Code
Each
8067-18
106.40

Nylon Bushing
Order Code
Each
7506-10
21.17

Complete
Order Code
Each
5030-84
127.57

Bushing, PTFE

*pH probe not included.

12990 PROBE pH, Process Pilot Plants


pH probe for process applications consists of three parts; a rugged standard combination
pH probe, 3-ft lead and a 3-ft extension cord, total lead length 6-ft. BNC connector end for
connecting to ACE Impresario controller. Probe is 127mm long and has Ag/AgCl internals
and rugged epoxy body. 80C max temperature. Fits easily into Ace 5278 probe adapter.
Order
Code
12990-01

Each
300.85

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

130

Components / Adapters
5853 ACE-SAFE CONNECTIONS Tubing, Polypropylene
Replacement tubing connector, used with nylon bushing to make easy and safe connect/
disconnect of coolant or steam tubing to jacketed reaction flasks, condensers, or any
vessel utilizing the AceThred as the connection port. Connector is fitted with a silicone
oring. Bushing compresses connector and oring for leak-tight seal. Once tubing is
attached to serrated end of connector, bushing will not come off. Hose connections are
supplied with silicone oring. For replacement orings, order 7855-207 for Code -03;
7855-206 for codes -09 and -10; 7855-210 for code -18 and -21; 7855-772 for code -31
and -33. Maximum temperature is 110C.

5853

For #7 AceThred
to 1/4-inch I.D. Tubing
Hose Connection, only, w/ORing
Nylon Bushing, only
Complete

Order Code
5853-03
5029-05
5853-06

Each
11.06
2.50
13.53

For #15 AceThred


to 3/8-inch ID Tubing

Hose Connection, only, w/ORing


Nylon Bushing, only
Complete

Order Code
5853-19
7506-05
5853-23

Each
11.43
12.20
24.36

For #11 AceThred


to 1/4-inch I.D. Tubing
Order Code
5853-09
7506-01
5853-12

Order Code
5853-18
7506-05
5853-20

Each
10.54
10.83
22.02

For #15 AceThred


to 1/2-inch ID Tubing

Order Code
5853-21
7506-05
5853-26

For #15 AceThred


to 1/4-inch I.D. Tubing

For #11 AceThred


to 3/8-inch I.D. Tubing
Order Code
5853-10
7506-01
5853-15

Each
11.43
12.20
24.36

For #25 AceThred


to 3/4-inch ID Tubing

Order Code
5853-31
7506-09
5853-35

Each
12.32
12.20
25.25

Each
10.54
10.83
22.02

For #25 AceThred


to 1-inch ID Tubing

Order Code
5853-33
7506-09
5853-37

Each
26.93
19.30
47.44

Each
28.27
19.30
48.76

5858 ACE-SAFE CONNECTIONS Tubing, PTFE


Same as 5853 above, but manufactured from PTFE instead of polypropylene.
Connectors are supplied with FETFE oring. For replacement orings, order 7855-707
for Code -03; 7855-706 for codes -05 and -10; 7855-710 for code -07, -12, and -14.
Maximum temperature is 200C.

5858

For #7 AceThred
to 1/4-inch I.D. Tubing
Hose Connection, only, w/ORing
PTFE Bushing, only, w/O-Ring

Order Code
5858-03
5029-35

Each
20.14
14.08

For #15 AceThred


to 3/8-inch ID Tubing

Hose Connection, only, w/ORing


PTFE Bushing, only, w/O-Ring

Order Code
5858-12
7506-27

Each
31.11
40.65

For #11 AceThred


to 1/4-inch I.D. Tubing
Order Code
5858-05
7506-23

For #15 AceThred


to 1/4-inch I.D. Tubing

Each
27.82
39.80

Order Code
5858-07
7506-27

For #11 AceThred


to 3/8-inch I.D. Tubing

Each
31.11
40.65

Order Code
5858-10
7506-23

Each
27.82
39.80

For #15 AceThred


to 1/2-inch ID Tubing

Order Code
5858-14
7506-27

Each
33.49
40.65

5853/5858 Tubing Connector Reference Chart


Tubing Connector
Catalog No.
5853-03/5858-03
5853-09/5858-05
5853-10/5858-10
5853-18/5858-07
5853-19/5858-12
5853-21/5858-14
5853-31
5853-33

Fits
AceThred
Size
7
11
11
15
15
15
25
25

(Flow Rate @10 lbs. H20)

Connector Nominal
I.D.,
Flow Rate
in. (mm)
Gal./Min.
.125 (3.18)
1.5
.125 (3.18)
1.5
.187 (4.74)
3.3
.125 (3.18)
1.5
.187 (4.74)
3.3
.375 (9.5)
13.3
.500 (12.7)
23.6
.750 (19)
53.3

Use Bushing
Number
5029-05/5029-35
7506-01/7506-23
7506-01/7506-23
7506-05/7506-27
7506-05/7506-27
7506-05/7506-27
7506-09
7506-09

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Use O-Ring
Number
7855-207/7855-707
7855-206/7855-706
7855-206/7855-706
7855-210/7855-710
7855-210/7855-710
7855-210/7855-710
7855-772
7855-772

For Tubing I.D.,


In. (mm)
1/4 (6.35)
1/4 (6.35)
3/8 (9.5)
1/4 (6.35)
3/8 (9.5)
1/2 (12.7)
3/4 (19)
1 (25.4)

Subject to Ace Discount (Page 4)

Net

Components / Adapters

131

6472 ADAPTER Beaded Pipe, for Flush Valve, Glass


Attach to 1-inch beaded pipe outlet on 6472-245 Martin style flush valve to adapt to
tubing NPT fitting.
Style
1-inch BP x 1/2-inch O.D. Tube
1-inch BP x 1/2-inch I.D. Hose Conn. (Size G)
1-inch BP x #15 AceThred
1-inch BP x #25 AceThred

Order Code
6472-275
6472-276
6472-277
6472-278

Each
50.38
53.03
59.67
64.97

6472-277, -278

12067 ADAPTER Connecting, Heat Exchange Coil


Stainless steel adapter for connecting 12067 heat exchange coil tubing to pipe thread
(NPT). Adapter fits over tubing and makes a compression seal via oring for working
pressure of 25 psig. Complete item includes compression adapter, elbow, and pipe nipple.
Elbow
(FPT)
1/4-inch
1/4-inch
1/2-inch

Adapter Size (Inches)


1/4 O.D. tube x 1/4
3/8 O.D. tube x 1/4
1/2 O.D. tube x 1/2

Nipple
(MPT)
1/4-inch
1/4-inch
1/2-inch

ORing
(Size)
-010
-012
-014

Order Code
12067-02
12067-04
12067-06

Each
39.63
48.29
60.73

12067-02

See coils on page 150

12187 ADAPTERS Stainless Steel, Circulator Hose


304 Stainless steel adapters designed for use with ACE jacketed glass pilot plant
reactors and circulator hoses for popular circulating chillers. One style connects oring
ball joints on jacket inlet/outlet to hoses to/from circulator. The other style connects
M style to NPT thread.
Connection Description
Flask to Hose, 28/15 Socket to M16x1 Male
Flask to Hose, 35/25 Socket to M16x1 Male
Flask to Hose, 35/25 Socket to M24x1 Male
Flask to Hose, 35/25 Socket to M30x1 Male
Flask to Hose, 35/25 Socket to M38x1.5 Male
Hose to Circulator, M16x1 Male to 3/4 inch NPT Male
Hose to Circulator, M30x1.5 Male to 3/4 inch NPT Male
Hose to Circulator, M24x1.5 Male to 3/4 inch NPT Male

Order
Code
12187-05
12187-07
12187-10
12187-12
12187-14
12187-100
12187-101
12187-102

12187-100
12187-05

Each
88.40
93.60
93.60
93.60
93.60
93.60
93.60
93.60

5299 ADAPTER Distillation


Distillation adapter for use with bench or pilot plant reactors. Moisture is collected in
center vessel and drained off through the bottom stopcock which is ground to accept
a compression style fitting. Stopcock is PTFE plug. Available with either one or two top
standard taper outer joints.
With one top/outer T
S
joint
Joint
24/40
29/42
45/50

Stopcock Size,
mm
6
6
10

Compression Fitting
Joint Size, In.
1/2
1/2
3/4

Order
Code
5299-01
5299-03
5299-07

Complete
198.26
247.40
326.01

1/2
1/2
3/4

5299-10
5299-12
5299-16

231.20
260.69
398.83

5299-16

With two top/outer T


S
joints
24/40
29/42
45/50

6
6
10

5299-07

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

132

Components / Funnels
12560 FUNNEL Buchner, Table Top
POROUS FILTER PLATE type or PERFORATED PLATE type, fixed or removable,
polyethylene Buchner funnel. Features one-piece, welded construction with welded-in
plate and multiple-ring support grid below plate. A non-porous ring around plate seals
filter paper. Vacuum connection accepts 1/2-inch I.D. tubing. For use below 125F (52C).
FILTER PLATE is available in medium (M) or coarse (C) porosity, 1/4-inch (6.4mm) thick.
PERFORATED PLATE is 3/16 inches (4.8mm) thick with 3/16-inch perforations on 7/16-inch
(11mm) centers. Good for coarse filtration or use with cloth or paper filter.

12560

I.D.,
Inches (cm)
10-1/4 (26)
10-1/4 (26)
10-1/4 (26)
10-1/4 (26)
18 (45.7)
18 (45.7)
18 (45.7)
18 (45.7)
24 (61)
24 (61)
24 (61)
24 (61)
36 (91.4)
36 (91.4)
36 (91.4)
36 (91.4)

Overall
Height
(Inches)
7
7
7
7
11-1/2
11-1/2
11-1/2
11-1/2
13
13
13
13
14-3/4
14-3/4
14-3/4
14-3/4

Rim to
Plate
(Inches)
5
5
5
5
9
9
9
9
10-1/2
10-1/2
10-1/2
10-1/2
12
12
12
12

Perforated Plate
Order
Code
12560-14
12560-14
12560-50
12560-50
12560-16
12560-16
12560-57
12560-57
12560-18
12560-18
12560-59
12560-59
12560-20
12560-20
12560-63
12560-63

Each
352.50
352.50
352.50
352.50
745.50
745.50
745.50
745.50
1182.60
1182.60
1182.60
1182.60
2108.10
2108.10
2108.10
2108.10

Porus Plate
Plate Type/
Porosity ( )
Fixed/(M)
Fixed/(C)
Removable/(M)
Removable/(C)
Fixed/(M)
Fixed/(C)
Removable/(M)
Removable/(C)
Fixed/(M)
Fixed/(C)
Removable/(M)
Removable/(C)
Fixed/(M)
Fixed/(C)
Removable/(M)
Removable/(C)

Order
Code
12560-02
12560-04
12560-30
12560-32
12560-05
12560-06
12560-35
12560-37
12560-07
12560-08
12560-38
12560-39
12560-09
12560-10
12560-41
12560-53

Each
352.50
347.70
352.50
352.50
862.90
862.90
862.90
862.90
1793.40
1793.40
1793.40
1793.40
2818.95
2818.95
2818.95
2818.95

FILTER PAPER is to fit 12560 funnels. Rough crepe surface, 0.25mm thick, flow rate
235mL/min., retention of 24 microns and wet strength of 25cm of water. Packed 100
per box.
For Funnel Size
(Inches)
10-1/4
18
24
36

Order Code
12560-70
12560-72
12560-74
12560-76

Per Box
91.05
169.95
216.30
862.15

12563 FUNNEL Buchner, All Stainless Steel


316 stainless steel Buchner funnel for organic or inorganic chemical synthesis. This funnel
incorporates a removable perforated plate that allows thorough manual cleaning and
autoclaving. Since the plate is removable, yield is increased because internal supports
that would trap product are eliminated. Will not chip, crack or break. Offered in 24cm and
50cm sizes that accept commercially available filter sizes. Completely electropolished
for critical applications, i.e., pharmaceuticals. Outlet port is 1/2-inch O.D.

12563

Height
Inside Dia., Above Disc
cm (In.)
(Inches)
5
24 (9.5)
50 (20)
10

Overall
Height
(Inches)
7
12

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Grit
Finish
240
240

Order
Code
12563-09
12563-27

Each
6454.08
8153.06

Subject to Ace Discount (Page 4)

Net

Components / Funnels

133

7233 FUNNEL Powder Dispensing, Vertical


A vertical, compact, screw feed funnel for the addition of powders and solids (up to 25
mesh) into reactions without seizing or binding. Features a flexible PTFE screw thread
wrapped on a precision PTFE-ceramic shaft and contained within a precision bore
housing. This offers a unique flexibility in that the thread can move aside temporarily;
as one spacing increases, the adjacent spacing decreases, thereby maintaining an
average feed rate. Completely inert materials allow flushing with solvents without fear of
contamination. #15 AceThred at top offers easy disassembly for cleaning. Large 1-1/4inch knob makes turning smooth and easy. Top side port is S
T 14/20 outer joint, bottom
inner joint is S
T 24/40. Overall height, 9-1/2 inches.
Capacity, mL
50
100

Order Code
7233-20
7233-30

7233

Each
250.88
282.08

7234 FUNNEL Powder Dispensing


Side operated screw feed funnel for the addition of powders and solids (up to 25 mesh)
to reactions without problems of seizing or binding.
Features a flexible PTFE screw thread wrapped on a precision PTFE-ceramic shaft and
contained within a precision bore housing. This offers a unique flexibility in that the thread
can move aside temporarily; as one spacing increases, the adjacent spacing decreases,
thereby maintaining an average feed rate.
Completely inert materials allow flushing with solvents without fear of contamination. #15
AceThred offers easy disassembly for cleaning. Large 1-1/4-inch knob makes turning
smooth and easy. Top outer and bottom inner joints are S
T 24/40. S
T 14/20 outer joint atop
inner joint is for easier flushing.
Capacity, mL
100
250

Order Code
7234-25
7234-35

7234

Each
331.84
358.50

9485 FUNNEL Powder Dispensing


A vertical, compact, screw feed funnel for the addition of powders and solids (up to 25
mesh) into reactions without seizing or binding. Features a flexible PTFE screw thread
wrapped on a precision PTFE-ceramic shaft and contained within a precision bore
housing. This offers a unique flexibility in that the thread can move aside temporarily;
as one spacing increases, the adjacent spacing decreases, thereby maintaining an
average feed rate. Completely inert materials allow flushing with solvents without fear
of contamination. #7 AceThred offers easy disassembly for cleaning. Top outer and bottom
inner joints are S
T14/20. Approximate capacity, 15mL.
Capacity, mL
100

Order Code
9485-15

Each
238.41

9485

7239 FUNNEL Powder Dispensing


T14/20 outer joint atop bottom
Side operated screw feed funnel similar to 7234 except S
Tjoint and top S
Touter joints are 24/40. Same
inner joint has been eliminated. Bottom S
features as 7233.
Capacity, mL
100
250

Order Code
7239-30
7239-40

Each
267.61
331.07

7239

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

134

Components / Funnels
7236/9488 FUNNEL Powder
Useful in pouring powders or liquids into ground joint containers. Available with JSor
joint.

S
T inner

7236/9488

S
Approx.
T
Top Dia., Bottom Order
mm
Joint
Code
65
14/20 9488-10
65
19/38 7236-06
75
24/40 7236-08
100
24/40 7236-10
125
24/40 7236-11
100
29/42 7236-12
125
34/45 7236-14

Each
32.15
42.84
45.15
47.70
48.44
51.13
60.00

Approx.
Top Dia.,
mm
100

S
J

Bottom
Joint
35/25

Order
Code
7236-20

Each
51.37

7238 FUNNEL Powder, 58 Offset, Heavy Wall


Offset funnel with heavy walls for greater durability when pouring powders or liquids into
multi-neck flasks.
Approx. Top
Dia., mm
75
100

7238

S
T

Bottom Joint
24/40
24/40

Order Code
7238-06
7238-08

Each
71.38
74.72

7245 FUNNEL Powder, Angled, H eavy Wall


Borosilicate funnel angled to permit use in multi-neck flasks. On angled neck flasks such
as 6948, this funnel will bring the mouth of the funnel back to vertical.
Top Diameter,
mm
75
100
100
200

A
7245

S
T

Bottom
Joint
24/40
24/40
29/42
45/50

Order Code
7245-07
7245-15
7245-21
7245-25

Each
59.51
69.98
81.25
98.28

7250/6469 FUNNEL Powder, Flat Side

Powder funnel with S


T joint and flattened side for easy use with multi-neck flasks.
S
T

A
7250/
6469

Height A,
mm
120
150
195
200

Bottom
Joint
14/20
24/40
24/40
29/42
29/32
45/50
71/60

Top Opening (B),


mm
50
75
100
145
145
150
255

Height (A),
mm
70
90
145
145
145
250
255

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Order Code
7250-01
7250-05
7250-09
7250-10
7250-12
6469-52
7250-15

Each
40.10
52.51
60.85
65.68
65.68
228.81
280.66

Subject to Ace Discount (Page 4)

Net

Components / Funnels

135

7252 FUNNEL Powder, Schott-Duran Flange Bottom


Borosilicate glass powder or liquid addition funnels with a Schott-Duran Flange bottom.
Glass funnel fits onto 100mm or 60mm side ports on ACE 6530 glass reactor heads. Funnels
are slightly angled to allow for easy pouring of ingredients into reactors. Use the 6517 quick
release clamp to add to head.
Approx.
Volume, mL
1,800
2,800

A, mm
200
200

B, mm
160
200

Order Code
7252-06
7252-10

Each
247.56
296.00

7252

For Port Size


C, mm
60
100

7295 FUNNEL Addition, with Offset


Graduated, borosilicate glass, liquid addition funnels with an offset bottom outlet and
S
T joint. Bottom outlet has a PTFE stopcock. Top outlet has the same size S
T joint as the
bottom. This design is ideal for crowded reactor heads, and allows for a larger addition
funnel to be used.
Capacity, mL
125
250
500
1000
1000

Approximate
Length, mm
125
250
500
1000
1000

S
T

Joint Size
24/40
24/40
24/40
24/40
29/42

Order Code
7295-03
7295-05
7295-07
7295-09
7295-11

Each
180.52
201.64
216.42
248.09
254.42

7295

New

7297 FUNNEL Graduated, Pressure Equalizing, PTFE Stopcock


Borosilicate glass addition funnel. Cylindrical shape with S
T joints top and bottom.
Funnel has a side pressure equalizing tube and has a PTFE plug stopcock. Inner drip
tube at bottom doesnt extend below the main joint, to reduce breakage. 5L size has
100mL graduations.
Capacity, Stopcock Plug
mL
Bore, mm
125
2
250
2
500
4
1000
4
2000
4
5000
8

S
T

Joint
Size
24/40
24/40
24/40
24/40
29/42
45/50

Overall
O.D., Length,
Graduations mm
mm
1mL
38
345
5mL
51
390
5mL
64
430
100mL
75
500
85
650
100mL
100mL
155
565

Order
Code
7297-31
7297-33
7297-35
7297-37
7297-39
7297-45

7297-45

Each
220.00
251.93
275.87
332.65
373.35
840.01

All full-length outer standard taper joints are reinforced.

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

136

Components / Funnels
7298 FUNNEL Pressure Equalizing, Graduated,
with PTFE Needle Valve Stopcock

Graduated addition funnel with threaded stopcock with PTFE plug permits smooth needle
valve adjustment down to 0.1mL/min. flow rate. Double PTFE ring seals prevent exposure
of backup oring to corrosive liquids. Angled position makes manipulation of stopcock
easier than conventional style. ST 24/40 joints top and bottom, double scale graduations.
Capacity,
mL
125
250
500
500
1000
2000

Overall
Length, mm
380
385
500
500
565
760

Stopcock
Bore, mm
0-3
0-3
0-3
0-5
0-5
0-5

Order
Code
7298-05
7298-10
7298-15
7298-20
7298-24
7298-28

Each
231.90
249.35
278.92
346.69
326.09
529.40

Replacement Stopcock Plugs:

7298
9493-40

For Size

Order Code

Each

0-3 mm
0-5 mm

8192-261
8192-263

37.87
52.16

7278 FUNNEL Addition, Separatory, Jacketed


Graduated addition funnels like 7268 series, except with outside jacket for cooling or
heating. Jacket extends from just below shoulder of vessel down to the bottom tube just
above the bottom stopcock. Stopcock is 4mm bore PTFE. Bottom drip tube extends to
the bottom edge of the lower, inner standard taper, joint, Top outer stopcock size matches
the bottom joint size. Side hose connections are size D for 3/8-inch (9.5mm) ID tubing.

7278

Capacity,
mL
1000
1000
1000
2000
2000

Joints
24/40
29/42
29/32
29/42
29/32

Order
Code
7278-15
7278-17
7278-19
7278-23
7278-25

Each
462.40
462.40
462.40
502.51
502.51

7281 FUNNELAddition, Pressure Equalizing, Jacketed


Jacketed version of 7297 series addition funnels. Jacket runs from shoulder at top of
vessel to just above the PTFE stopcock with size D hose connections for 3/8-in ID tubing.
Equalizing side arm runs from top of vessel to just below the stopcock. Graduations are
both ascending and descending volume. Top and bottom standard taper joints are the
same size. Bottom drip tip extends to the edge of the bottom inner joint. Top outer joint
is reinforced. PTFE stopcock plug is 4MM bore.

7281

Capacity, mL
1000
1000
1000
2000
2000

Joints
24/40
29/42
29/32
29/42
29/32

Order Code
7281-14
7281-16
7281-18
7281-22
7281-24

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Each
484.57
484.57
484.57
626.03
626.03

Subject to Ace Discount (Page 4)

Net

TH

A N N I V E R S A R Y

TED
RA

ACE G

S
A

C
N
OR
I
S

137

1936 2011

VI

USA

NE

N
,
LAND

Components / Condensers

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Components / Condensers

138

5945 CONDENSER Allihn, Pilot Plant


Bulb type, approximately one bulb per every 50mm, with or joint at bottom and top.
Use with 3/8inch I.D. tubing, size D hose connections. See page 5 for more detailed
hose connection information.

5945

Jacket
Length, mm
500
600
500
600

Joints
24/40
24/40
29/42
29/42

Order Code
5945-16
5945-17
5945-26
5945-27

Each
142.23
145.06
150.81
173.65

5945/5946 CONDENSER Allihn, with AceThred Connectors


e
lu
Va

E-SA

Jacket
Length, mm
250
300
300
500

Joints
24/40
24/40
29/42
45/50

Order Code
5946-116
5946-118
5946-122
5945-76

Each
143.67
152.29
152.29
382.96

OR

ON

FE

AC

5946

Bulb type, approximately one bulb per 50mm, with inner and outer joint at bottom and
top, #7 AceThred and Ace-Safe hose connections on inlet and outlet with barb for
1/4-inch I.D. tubing. For replacement connectors, see 5853.

N ECT

5958 CONDENSER Cold Finger, Pilot Plant Reactors


Jacket length is measured from the lower shoulder of the bulb to the bottom of the
finger. Diameter of tube is 14mm. Used in 6472 pilot plant reactors. Use with 5030-45
#15 AceThred adapter to fit top 45/50 joint in 5945-76 condenser. Can also be used
with 6015, 6016, and 6020 condensers. Use with 5/16-inch or 3/8-inch I.D. tubing, size
C hose connections. See page 5 for more detailed hose connection information.
Jacket
Length, mm
625

Order
Code
5958-99

Each
92.87

5958

All full-length outer standard taper joints are reinforced.

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Subject to Ace Discount (Page 4)

Net

Components / Condensers

139

5960 CONDENSER Cold Finger


With joint. The 5960-12 condenser is used with our 6606, 6609, and 6613 distilling
heads and 5943, 5945 and 5946 condensers. See page 5 for more detailed hose
connection information.
Length Below
Joint, mm
110
215

Order
Code
5960-08
5960-12

Tubing
Size (Inches)
3/8 (D)
3/8 (D)

Joint
24/40
24/40

Each
94.16
88.67

5960

6012 CONDENSER Pilot Plant, Long Path


Turbulent flow created makes this condenser very desirable for use under reduced
pressure. Internal and external cooling surfaces result in high efficiency per unit length.
24/40inner and outer joints. Use with 7/16-inch or 1/2-inch I.D. tubing, size F hose
connections. See page 5 for more detailed hose connection information.
Jacket
Length, mm
500
600

Order Code
6012-16
6012-17

Each
829.93
849.88

6012

Custom condensers with various joint or length sizes are


available upon special request.

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Components / Condensers
E-SA

FE

AC

140

OR

ON

N ECT

6015 CONDENSER Double Coil, High Capacity, Pilot Plant


High throughput double coil condensers are made for larger systems and large-scale
reactors, to handle larger scale reactions. These are also similar to rotary evaporator
type condensers where a lot of material is being condensed at a higher temperature and
where large amounts of cooling water are needed to generate higher efficiency. The unit
can be ordered with standard taper joints or beaded pipe end connections. The overall
length is approximately 390mm and O.D.is approximately 85-90 mm. Both units have
#15 AceThred side connections for Ace-Safe hose connections. Supplied with full Ace
Safe connections.
Jacket Length,
mm
315
290

6015-17

Condensing
Area, cm2
1480
1400

End Finish
1-inch bead pipe
45/50

Order Code
6015-12
6015-17

Each
644.26
708.70

6015-12

6016 CONDENSER Pilot Plant


Highly efficient. May be used either for thorough condensation or refluxing. Internal
baffling acts as impinging surface for entrained particles and discourages diffusion loss.
Use with 7/16-inch or 1/2-inch I.D. tubing, size F hose connection. Available with either
spherical or standard taper joint.

6016

Joint Size 45/50


Jacket
Length, Order
mm
Code
Each
500
6016-36 923.04
750
6016-39 1059.31
1000
6016-41 1255.92

Joint Size 71/60

Joint Size 35/25

Joint Size 65/40

Order
Code
Each

6016-52 1176.47

Order
Code
Each
6016-66 919.15

6016-69 1237.21

Order
Code
Each
6016-75 972.51
6016-77 1048.01
6016-79 1328.76

6016 CONDENSER Pilot Plant, with Side AceThred Connectors

E-SA

OR

ON

FE

AC

Highly efficient. May be used either for thorough condensation or refluxing. Internal
baffling acts as impinging surface for entrained particles and discourages diffusion loss.
With #11 side AceThred and Ace-Safe hose connections on inlet and outlet with
barb for 1/4-inch I.D. tubing. Available with either spherical or standard taper joints.

N ECT

Jacket
Length, mm
500
750
1000

Joint Size 45/50


Order
Code
Each
6016-137 947.33
6016-139 1083.60
6016-141 1280.21

Joint Size 35/25


Order
Code
Each
6016-167 930.09

6016-170 1243.55

Joint Size 65/40


Order
Code
Each
6016-176 982.69
6016-178 1057.13
6016-180 1333.79

6016

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Subject to Ace Discount (Page 4)

Net

Coil
Length, mm
220

Condensing
Area, cm2
1600

Glass only
Order Code
6017-210

E-SA

6017

OR

ON

With three internal cooling coils, this new design gives even higher throughput than the
double coil or any rotary evaporator condenser. Designed for pilot plants and larger
reactors where a lot of cooling area is needed for condensing or for higher temperature
reactions where more throughput is needed. Comes with #15 AceThred ports with or
without Ace-Safe connections. Top and bottom connections are 2-inch beaded pipe.
Overall length is approximately 460mm and O.D. is approximately 110mm.

141

FE

6017 CONDENSER Triple Coil, High Capacity

AC

Components / Condensers

N ECT

Complete

Each
822.02

Order Code
6017-212

Each
870.74

6020 CONDENSER Spiral, Reflux


With spiral condensing tube having both inlet and outlet connections at top, on same
side.With inner and outer joints at bottom and top. Length between joints is approximately
80-90mm longer than coil length.
Coil Length,
mm
200
250
300
400
300
400

Joints
24/40
24/40
24/40
24/40
29/42
45/50

Tubing Size
(Inches)
3/8 (D)
3/8 (D)
3/8 (D)
3/8 (D)
3/8 (D)
3/8 (D)

Order Code
6020-02
6020-04
6020-06
6020-08
6020-10
6020-12

Each
213.34
229.00
236.11
260.30
240.15
315.13

6020

6021 CONDENSER Modified Keenan, Dual Coil, Horizontal


Highly efficient, double coil condenser with 30 degree horizontal angle vs. typical
vertical style. Great for under hoods or on pilot plant reactors where height may be an
issue and a high level of distillation is required. Condenser has a 45/50 bottom joint
to fit on reactor heads, all other connections are either #7 or #15 Ace-Safe, (supplied).
Comes with either a PTFE or glass stopcock. Overall length is approximately 470mm.
Height from top of bottom joint to highest point at top is 90mm.
Joints
45/50
45/50

Stopcock Type
PTFE
Glass

Order Code
6021-20
6021-30

6021
Priced Upon
Request

6022 CONDENSER Keenan, Single Tube, Horizontal


Highly efficient, newly designed condenser. Features a horizontal angle for low clearence
but extremely good capacity and throughput. Especially useful when assembling large
reactor in limited height clearance situations. Surface area is 710 cm2. Cooling fluid
volume: 600 mL. Condenser has a 45/50 bottom joint. All other connections are #7 or
#15 AceThred that accepts a 7mm O.D. tube or 5853 Ace-Safe connectors (supplied)
to attach tubing. Overall length: 475mm.
Joints
45/50
45/50

Stopcock Type
Glass
PTFE

Order Code
6022-22
6022-30

6022
Priced Upon
Request

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

142

Components / Condensers
6810 CONDENSER Pilot Plant, Bulb Type
Pilot plant bulb-type Soxhlet condenser. Use with 7/16-inch or 1/2-inch I.D. tubing, size
F hose connections. See page <OV> for more detailed hose connection information.

6810

Overall
Length
(mm)
450
525
930

Condenser
Length
Bottom
(mm)
Joint
71/60
340
375
103/60
730
55/50

Length, mm Order Code


340
6810-04
460
6810-14
730
6810-24

Each
296.18
551.81
702.05

7744 RECEIVER, MOISTURE TEST Barrett Type, Pilot Plant


One liter Barrett type moisture test receiver. 2mm PTFE stopcock on bottom for
draining contents. 45/50 joints at top and on side arm. 60mm distance between
side arm and body for clearance on spherical or cylindrical reactor bodies. Graduated
in 10mL subdivisions.
Order
Code
7744-50

Each
1810.83

7744

Custom configurations are available. Call 800-223-4524


or email sales@aceglass.com.

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Subject to Ace Discount (Page 4)

Net

OR

ON

N ECT

143

6024/6029 CONDENSERWest

E-SA

FE

AC

Components / Condensers

6029

West style condenser for use with 6433 threaded or 6527, 6528 or 6529 jointed heads.
6024-20 supplied with #15 AceThred at top for 5846 plug (not supplied) and drip stem
with groove, and long enough to be secured in #15 AceThred with 7506-06 bushing
and oring (not supplied) to restrict blowout. With #7 AceThred on inlet/outlet for use
with Ace-Safe 5853 tubing connectors. Supplied with bushing and connectors for
1/4inch I.D. tubing.
6029-13 supplied with 24/40 joint at top and bottom and D size barbed hose connection
on inlet/outlet for 1/4inch I.D. tubing.
Use with Head No.
6433
6527,6528,6529

Jacket Length, mm
200
250

Order Code
6024-20
6029-13

Each
129.75
105.87

6024

New

6042 CONDENSER Reflux, Bulb 


New style, compact, high-output reflux condenser, has an inner double wall, thimbleshape internal bulb. Overall height is approximately 250mm, but has the output equal
to condensers with twice the length. Unit has outer top joint and drip-tip inner
joint bottom. Top and bottom hose connections size D (see page 5 for sizing),
for 3/8inch tubing.
Angled Top
Joint
24/40
29/42
29/32
45/50

Inner Drip-Tip
Bottom Joint
24/40
29/42
29/32
45/50

Order Code
6042-04
6042-06
6042-08
6042-10

Each
205.40
216.06
200.78
343.50

6042

6046 CONDENSER Angled 


New

6046

Condenser similar to the 5945 series except with a 45 degree angle on the bottom joint.
When using with ACE reactor heads, this allows for height space savings vs. the standard
vertical condensers in reactor systems. Has joints at top and bottom. Hose barbs are
glass size D (see page 5 for sizing) for 3/8-inch ID tubing.
Jacket Length, mm
300
300
400
400
400
500
500
600
600
600

Joint Size
24/40
29/42
24/40
29/42
35/45
24/40
29/42
24/40
29/42
35/45

Order Code
6046-03
6046-05
6046-09
6046-11
6046-13
6046-17
6046-19
6046-23
6046-25
6046-27

Each
114.75
128.11
130.56
131.58
137.70
131.58
139.74
139.74
145.86
151.98

All full-length outer standard taper joints are reinforced.

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

144

Components / Condensers

3965-10,
-15
3965-05,
-07

3965-26,
-28

3965-19,
-22

3965 CONDENSERS Triple Coil


The condensers are available in either poly-coated or plain, non-coated versions. All condensers fit easily into the glass sets listed
below. DN40 inner ball joints include CAPFE (PTFE-encapsulated silicone rubber) o-rings. Black caps (included) are SVL-22 threads;
red cap (included) is GL-14 thread.

Description
Triple-Coil Condenser
Triple-Coil Condenser
Triple-Coil Condenser
Triple-Coil Condenser
Glass Condenser (Bullfrog)
Glass Condenser (Bullfrog)
Glass Condenser (Bullfrog)
Glass Condenser (Bullfrog)

Fits
Glassware
Set
R, D2
R, D2
D, D2
D, D2
DB, DB2
DB, DB2
RB, DB2
RB, DB2

Coated?
Yes
No
Yes
No
Yes
No
Yes
No

Similar
to Buchi
Part No.
41159
41399
27308
41333
27825
46516
27824
41458

Fits
Buchi Models
R220,
R200EX, SE
R220
R200EX, SE
R220
R220EX, SE
R220
R220

Ball/Socket
DN Joint
Sizes
40
40
40
40
40
40
40
40

Uses O-Ring
Size/Code
225/7855-844
225/7855-844
225/7855-844
225/7855-844
225/7855-844
225/7855-844
225/7855-844
225/7855-844

Order
Code
3965-05
3965-07
3965-10
3965-15
3965-19
3965-22
3965-26
3965-28

Each
3114.32
3008.75
3747.74
3642.17
5273.22
5162.37
5273.75
5067.36

Also available with standard taper or process pipe joints

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Subject to Ace Discount (Page 4)

Net

Components / Distillation Columns

145

6565 DISTILLATION COLUMN Perforated Plate


Perforated plate column, without jacket. Holes are 0.032-inch diameter
Plate
No. of Dia.,
Plates mm
5
28
10
28
15
28
20
28
30
28
5
33
10
33
15
33
20
33
30
33
5
40
10
40
15
40
20
40
30
40

Joint
29/42
29/42
29/42
29/42
29/42
34/45
34/45
34/45
34/45
34/45
45/50
45/50
45/50
45/50
45/50

Order
Code
6565-02
6565-04
6565-06
6565-08
6565-10
6565-12
6565-14
6565-16
6565-18
6565-20
6565-22
6565-24
6565-26
6565-28
6565-30

Each
801.86
1324.56
1840.10
2368.22
3789.74
972.95
1903.54
2703.86
3746.43
5832.12
1273.57
2431.16
3335.31
4453.18
5893.46

Plate
No. of Dia.,
Plates mm
5
50
10
50
15
50
20
50
30
50
5
75
10
75
15
75
20
75
5
10
15
20

100
100
100
100

Joint
55/50
55/50
55/50
55/50
55/50
71/60
71/60
71/60
71/60

Order
Code
6565-32
6565-34
6565-36
6565-38
6565-40
6565-42
6565-44
6565-46
6565-48

Each
1453.40
2421.26
3263.06
4167.04
6349.38
3068.00
6014.81
7540.85
9462.64

103/60
103/60
103/60
103/60

6565-52
6565-54
6565-56
6565-58

5466.54
8586.13
11998.06
14435.73

6565

Large-scale Chromatography columns, see page 261

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

146

Components / Distillation Columns


6566 DISTILLATION COLUMN Perforated Plate, Internal Bellows, Silvered
Similar to 6565 except with vacuum-jacketed internal bellows and silvered internally.
Plate
No. of Dia.,
Order
Plates mm Joint
Code
5
28 29/42 6566-03
10
28 29/42 6566-05
15
28 29/42 6566-07
20
28 29/42 6566-09
30
28 29/42 6566-11
5
33 34/45 6566-13
10
33 34/45 6566-15
15
33 34/45 6566-17
20
33 34/45 6566-19
30
33 34/45 6566-21
5
40 45/50 6566-23
10
40 45/50 6566-25
15
40 45/50 6566-27
20
40 45/50 6566-29
30
40 45/50 6566-31

Each
1110.48
1786.20
2473.18
3367.70
4420.88
1731.53
2285.59
3575.66
4395.96
5917.11
2125.66
3276.51
4219.64
5436.73
6097.17

Plate
No. of Dia.,
Order
Plates mm Joint
Code
Each
5
50 55/50 6566-33 2052.65
10
50 55/50 6566-35 3902.58
15
50 55/50 6566-37 4625.35
20
50 55/50 6566-39 5491.75
30
50 55/50 6566-41 7603.81
5
75 71/60 6566-43 3805.55
10
75 71/60 6566-45 6392.42
15
75 71/60 6566-47 8738.56
20
75 71/60 6566-49 10933.52
5
10
15
20

100
100
100
100

103/60
103/60
103/60
103/60

6566-53
6566-55
6566-57
6566-59

6308.82
9149.10
13377.08
15244.10

Ace Glass offers various types of column packing


material. Please contact Technical Services at
800-223-4524 or visit our website.

6566

6088 SPLITTER Distillation, Reflux


6088

Reflux distillation splitter adapters for all size reactors. Standard taper, inner joint bottom,
standard taper, outer joint top. A slight angle to bottom inner standard taper joint allows
for addition to reactor heads with angled side necks and keeps splitter straight for flow
upward to the condenser. Three standard joint sizes are available. Side valve is 0-10 with
a 1/2-inch precision ground bottom take-off that matches 1/2-inch compression fittings.
Valve replacement FETFE o-rings are size -011 and -111.
Joints
24/40
29/42
29/32
45/50

Qty.
1
1
1
1

Order Code
6088-08
6088-10
6088-12
6088-14

Each
326.40
351.90
351.90
402.90

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Subject to Ace Discount (Page 4)

Net

Components / Distillation Columns

147

6569 DISTILLATION COLUMN Vacuum Jacketed


With internal expansion bellows. Baked out and evacuated to 10-6 Torr. All top
joints are jacketed. Spherical joints are not jacketed in order to allow for clamping.
All vacuum jacketed distilling columns are furnished with internal type expansion
bellows to compensate for the unequal expansion between the inside tube and the
outer jacket and will withstand a temperature differential of 180C. All columns,
regardless of length, are supplied with the proper number of bellows to withstand the
above temperature differential at all times. Standard silvered columns are supplied
with an observation stripe running down the entire length of the jacket.
The packing support is a conical tripod in which the free area is at least 90% of the
diametrical area. In addition to the columns listed, we also have facilities for fabricating
a complete line of special vacuum jacketed units to your specifications. This includes
additional bellows to enable you to maintain temperature differentials greater than 180C.
When ordering a special column, please specify the highest temperatures which may
be reached in the column, so that we can supply the unit with sufficient bellows to take
care of the expansion which may take place during distillation.
Length, cm
61
61
61
91
91
91
122
122
122

I.D., mm
12.7
25.4
25.4
12.7
25.4
25.4
12.7
25.4
25.4

Joints
24/40
29/42
35/25
24/40
29/42
35/25
24/40
29/42
35/25

Order Code
6569-40
6569-50
6569-60
6569-42
6569-52
6569-62
6569-44
6569-54
6569-64

Each
1169.98
1187.37
1193.17
1309.28
1326.68
1332.48
1547.10
1564.50
1570.30

6569

6087 SPLITTER Distillation, Reflux


Used to take off liquid distillate, splitter is installed between boil-up pot or fractionating
column and condenser. Main body is approximately 4 inches in diameter with #7 AceThred
and bushing for 1/4-inch diameter thermoprobe to monitor vapor temperature. Upper
alembic chamber has 2-inch diameter domed tube with two 1-1/4-inch diameter holes
for vapor flow upwards to condenser while preventing condensate from returning to pot.
Side 0-20mm PTFE stopcock allows take off when closed and reflux return when open.
Take-off tube terminus is 35/25 oring ball joint. 350mm overall height. All orings are
Kalrez for maximum chemical resistance. Joints are 45/50 inner on bottom, 45/50
outer on top.
Joint Size
45/50

Side Port
35/25 oring Ball Joint

Order Code
6087-10

Each
2122.41

6087

Columns can be custom designed and quoted to meet your


specifications. Non-silvered columns are available via special order.

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

148

Components / Spargers
6452 SPARGER Easy Action Stopcock and Hose Connection
Sparger tube with ACE frit at bottom, 0-3mm or 0-5mm Easy Action stopcock at top,
and 90 hose barb connecztion side port. See page 5 for more detailed hose connection
information. To connect this sparger to a head, use a 5030 adapter that matches the
AceThred sizes listed below.

6452-14

Overall
Length,
mm
400
400
400
575
575
575
775
915

Tubing
Stopcock Connection
Porosity
Size Size (Inches)
A (145-174 micron)
0-3
C (5/16)
B (70-100 micron)
0-3
C (5/16)
C (25-50 micron)
0-3
C (5/16)
A (145-174 micron)
0-5
D (3/8)
B (70-100 micron)
0-5
D (3/8)
C (25-50 micron)
0-5
D (3/8)
B (70-100 micron)
0-5
D (3/8)
B (70-100 micron)
0-5
D (3/8)

Glass
Fits
Tube AceThred
O.D., Adapter
Order
mm
Size
Code
10
11
6452-03
10
11
6452-05
10
11
6452-07
14
15
6452-14
14
15
6452-16
14
15
6452-18
14
15
6452-33
14
15
6452-44

Each
188.78
188.78
188.78
217.94
217.94
217.94
228.06
234.39

E-SA

OR

ON

Sparger tube with ACE frit at bottom, 0-3mm or 0-5mm Easy Action stopcock at top,
and 90 #7 Ace-Safe Connector side port for use with 7mm O.D. tubing. Supplied with
5853-06 AceSafe Connector (complete item includes nylon bushing and FETFE o-ring).
For replacement nylon bushing only, order 5029-05. For replacement FETFE oring only,
order 7855-706. For replacement Ace-Safe Connector only, order 5853-03. To connect
this sparger to a head, use a 5030 adapter that matches the AceThred sizes listed below.

FE

AC

6452 SPARGER Easy Action Stopcock and #7 Ace-Safe Connection

N ECT

Overall
Length, mm
400
400
400
575
575
575
775
915

Porosity
A (145-174 micron)
B (70-100 micron)
C (25-50 micron)
A (145-174 micron)
B (70-100 micron)
C (25-50 micron)
B (70-100 micron)
B (70-100 micron)

Glass
Fits
Tube AceThred
Stopcock O.D., Adapter
Size
mm
Size
Order Code
0-3
10
11
6452-104
0-3
10
11
6452-106
0-3
10
11
6452-108
0-5
14
15
6452-121
0-5
14
15
6452-123
0-5
14
15
6452-125
0-5
14
15
6452-132
0-5
14
15
6452-145

Each
234.39
234.39
234.39
239.47
239.47
239.47
252.14
259.72

6452-121

See page 149 for 5030 adapters.

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Subject to Ace Discount (Page 4)

Net

Components / Spargers

149

6453 SPARGER Straight and #7 AceThred

Orde Code
6453-105
6453-107
6453-109
6453-122
6453-124
6453-126
6453-133
6453-146

Each
144.58
144.58
144.58
147.13
147.13
147.13
147.13
154.82

E-SA

OR

ON

FE

Porosity
A (145-174 micron)
B (70-100 micron)
C (25-50 micron)
A (145-174 micron)
B (70-100 micron)
C (25-50 micron)
B (70-100 micron)
B (70-100 micron)

Tube O.D.,
mm
10
10
10
14
14
14
14
14

Overall
Length, mm
400
400
400
575
575
575
775
915

Fits
AceThred
Adapter
Size
11
11
11
15
15
15
15
15

Use 5853-06
Ace-Safe Connector
here!

AC

Straight sparger tube with ACE frit at bottom and #7 AceThred connection at top for
7mm O.D. tubing connection. Supplied with 5853-06 AceSafe Connector (complete item
includes nylon bushing and FETFE o-ring). For replacement nylon bushing only, order
5029-05. For replacement FETFE oring only, order 7855-706. For replacement Ace-Safe
Connector only, order 5853-03. To connect this sparger to a head, use a 5030 adapter
that matches the AceThred sizes listed below.

N ECT

6453-122

6453 SPARGER Straight with Hose Connection


Straight sparger tube with ACE frit at bottom and size F hose connection at top for 1/2inch
I.D. hose. See page 5 for more detailed hose connection information. To connect this
sparger to a head, use a 5030 adapter that matches the AceThred sizes listed below.

Overall
Length, mm
400
400
400
575
575
575
775
915

Porosity
A (145-174 micron)
B (70-100 micron)
C (25-50 micron)
A (145-174 micron)
B (70-100 micron)
C (25-50 micron)
B (70-100 micron)
B (70-100 micron)

Tube O.D.,
mm
10
10
10
14
14
14
14
14

Fits
AceThred
Adapter
Size
11
11
11
15
15
15
15
15

Order Code
6453-04
6453-06
6453-08
6453-21
6453-23
6453-25
6453-32
6453-45

Each
83.17
83.17
83.17
88.27
88.27
88.27
92.12
94.66

6453-21

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

150

Components / Baffles
12177 BAFFLEPTFE
Fabricated from virgin PTFE (meets USP Class 6 requirements), this fully encapsulated,
seamless baffle with a stainless steel reinforcing core fits through standard taper joint of
reaction flasks to increase agitation and promote mixing. Takes the place of indented or
Morton vessels that can be a problem when using pressure or vacuum. Shaft of baffle
is sized to be secured using 5030 AceThred adapter with nylon bushing and FETFE
oring. This connection allows vertical and rotational adjustment of the baffle inside the
flask for optimum effect. In place of oring, a PTFE ferrule can be used for maximum
chemical resistance.
Fits
Shaft
Shaft AceThred
Baffle
Overall
Diameter, Length, Adapter
W x L x D,
Length, Use Adapter
mm
mm
Size
mm
mm
(sold separately)
6.4
175
#7
18 x 152 x 10
327
5028-30
10
180
#11
18 x 150 x 10
330
5030-22
13
220
#15
30 x 150 x 12
380
5030-42/-45
13
300
#15
30 x 250 x 12
550
5030-42/-45
25
250
#25
32 x 360 x 14
610
5030-80

12177

Order
Code
12177-145
12177-148
12177-152
12177-154
12177-157

Each
379.26
424.39
649.26
717.88
746.38

12177 BAFFLEGlass
Borosilicate glass baffle fits through standard taper joint of reaction flasks to increase
agitation and promote mixing. Takes the place of indented or Morton vessels that can be
a problem when using pressure or vacuum. Shaft of baffle is sized to be secured using
5030 AceThred adapter with nylon bushing and FETFE oring. This connection allows
vertical and rotational adjustment of the baffle inside the flask for optimum effect. In place
of oring, a PTFE ferrule can be used for maximum chemical resistance. Order baffle,
adapter and optional ferrule separately. Custom sizes can be made to order.
Fits
Shaft
Shaft AceThred
Baffle
Overall
Diameter, Length, Adapter
W x L x D,
Length, Use Adapter
mm
mm
Size
mm
mm
(sold separately)
10
250
#11
18 x 60 x 6.4
310
5030-22
10
350
#11
18 x 90 x 6.4
440
5030-22
12.7
400
#15
36 x 65 x 9.5
465
5030-42
12.7
500
#15
36 x 100 x 9.5
600
5030-42

12177

Order
Code
Each
12177-10 54.90
12177-13 61.23
12177-19 99.24
12177-23 102.40

12193 BAFFLEPTFE, for Temperature Probe


Similar to 12177 PTFE baffle but with stainless steel inner reinforcing tube and #7 AceThred
machined into PTFE at bottom that accepts 1/4-inch diameter thermocouple or tubing.
The AceThred makes a compression seal with bushing and Kalrez oring. Probe or tubing
can be extended below baffle tip to any desired length. Can be used for subsurface liquid
addition or withdrawl when used with tubing. Thermocouple not included.

New

Each
459.23
770.66
809.72

E-SA

OR

ON

FE

AC

12193

Fits
Shaft
Shaft AceThred
Baffle
Overall
Diameter, Length, Adapter
W x L x D,
Length, Use Adapter
Order
mm
mm
Size
mm
mm
(sold separately)
Code
10
180
#11
18 x 150 x 10
330
5030-22
12193-03
13
220
#15
30 x 250 x 12
380
5030-42/-45 12193-07
25
250
#25
32 x 360 x 14
610
5030-80
12193-09

N ECT

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Subject to Ace Discount (Page 4)

Net

Components / Adapters

151

5030/7506 ADAPTER Midi #11 AceThred


With ground joint at bottom and #11 AceThred at top. Will accept inner tubes with
diameters of 9mm to 10.5mm such as thermowells, gas dispersion tubes, vacuum
take-offs, etc. Suitable for most vacuum work. Supplied complete with nylon bushing 5030-28
and FETFE oring. For extra orings, order 7855-708. See 6470 for thermowell.

40.00

7506-02

Complete

Each
11.39
11.39
11.39
11.39

Order
Code
5030-20
5030-22
5030-24
5030-19

Each
39.31
40.04
44.98
62.97

11.39

5030-28

51.39

E-SA

ON

AC

With ground joint at bottom and #15 AceThred at top. Will accept tubes with diameters
of 12.5 to 14mm such as electrodes, inlet and outlet tubes, etc. Suitable for most vacuum
work. Supplied complete with nylon bushing and FETFE oring. For extra orings, order
7855-716.
Nylon Bushing Only

E-SA

ON

Glass Only

N ECT

FE

5030/7506/8042 ADAPTER Maxi #15 AceThred

OR

5030-16

Each
27.92
28.65
33.59
51.58

Order
Code
7506-02
7506-02
7506-02
7506-02

OR

35/25

Nylon Bushing Only

FE

Order
Code
5030-04
5030-06
5030-08
5030-60

AC

Glass Only
Bottom
Joint
19/22
24/40
29/42
45/50

5030-20

N ECT

5030-40

Complete

Bottom
Joint
24/40
29/42
45/50

Order
Code
8042-15
8042-17
8042-21

Each
31.22
33.38
50.57

Order
Code
7506-06
7506-06
7506-06

Each
12.35
12.35
12.35

Order
Code
5030-40
5030-42
5030-45

Each
43.57
45.73
62.92

35/25

8042-35

35.92

7506-06

12.35

5030-44

48.27

5030-44

Bottom AceThred
Joint
Size
24/25
#25
24/25
#36
45/50
#36
45/50
#25
50/55
#25
71/60
#25
55/50
#36

Order
Code
5030-52
5030-55
5030-78
8067-18
8067-20
8067-22
8067-24

Each
35.83
60.00
77.88
106.40
102.13
112.06
104.94

Nylon Bushing Only


Order
Code
7506-10
7506-12
7506-12
7506-10
7506-10
7506-10
7506-12

Each
21.17
50.46
50.46
21.17
21.17
21.17
50.46

OR

FE

Glass Only

E-SA

ON

With ground inner joint at bottom and either a #25 or #36 AceThred that accepts
outside diameters of 24-25mm and 34-35mm, respectively (Note: Joint size limits size
O.D. of inserted tube). This item can be used with ultrasonics equipment. 503070 will
accept 985241 slide adapter; 503076 will accept 985245 slide adapter and/or 9814
ultrasonic horn with extenders. (Note: When using horn with extenders, depth distances
must be determined for proper operation.) Complete item supplied with nylon bushing
and FETFE oring.

AC

5030/7506/8067 ADAPTER Giant #25 or #36 AceThred

N ECT

Complete
Order
Code
5030-70
5030-76
5030-80
5030-84
5030-86
5030-88
5030-90

5030-70
Each
57.00
110.46
128.34
127.57
123.30
133.23
155.40

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

152

Components / Temperature Control

6472 TEMPERATURE CONTROL SYSTEM Pilot Plant


A complete package to enable the user to control the temperature of pilot plant reactors.
Consists of:
1) 12111-15, Type J auto-tune PID temperature controller with
fuzzy logic featuring digital display of reactor temperature.
hi and lo alarm set points, 120 volt/3 amp alarm outlet, a
16-segment ramp and soak program, and an auto rate circuit to
control temperature rise time.
2) 7832, auxiliary relay control unit allowing simultaneous
control of heating mantles. Relay unit is activated by
temperature controller and requires a 230 volt, 30A with
neutral and ground 4-wire, 50/60 Hz power source.
3) 12141, PFA-covered Type J temperature sensor,
with detachable lead, for use with 12111 temperature
controller to measure temperature inside reactor. 24-inch
for 10L & 20L cylindrical, 50L, 72L and 100L spherical;
36-inch for 36L cylindrical; 48-inch for 50L and 100L
cylindrical/200L spherical; 60-inch for 150L; 72-inch
for 200L cylindrical.
4) 7482-33 or 5028-30, glass and PTFE adapter, #25#7
5) 8067-18, adapters to secure temperature sensor in
head of reactor.
6) 5029-10, nylon bushing.

6472-77

Item
Temperature Controller
Power Strip, Four Outlets
Adapter, #7 29/42
Auxiliary Relay Control
Adapter, Glass, 45/50-#25
Adapter, PTFE, #25-#7
Bushing, Nylon, #7
J Thermocouple Sensor,
PFA Covered, Detachable
Sensor Lead, only
Complete

Item
Temperature Controller
Auxiliary Relay Control
Adapter, Glass, 45/50-#25
Adapter, PTFE, #25-#7
Bushing, Nylon, #7
J Thermocouple Sensor,
PFA Covered, Detachable
Sensor Lead, only
Complete

FOR 10L & 20L


CYLINDRICAL
Order
Each
Code
1424.21
12111-15
12195-20
47.00
5028-32
32.61

FOR 30L
CYLINDRICAL
Order
Each
Code
12111-15
1424.21

7832-14
1080.76
8067-18
106.40
7482-33
53.10
5029-10
2.77

FOR 50L
SPHERICAL
Order
Each
Code
12111-15
1424.21

7832-14
1080.76
8067-18
106.40
7482-33
53.10
5029-10
2.77

FOR 72L & 100L


SPHERICAL
Order
Each
Code
12111-15
1424.21

7832-19
1080.76
8067-18
106.40
7482-33
53.10
5029-10
2.77

12141-26

171.58

12141-28

200.08

12141-26

171.58

12141-26

171.58

12141-80
6472-67

69.68
1745.08

12141-80
6472-77

69.68
2937.00

12141-80
6472-73

69.68
2908.50

12141-80
6472-75

69.68
2908.50

FOR 50L & 100L


CYLINDRICAL
Order
Each
Code
1424.21
12111-15
7832-14
1080.76
8067-18
106.40
7482-33
53.10
5029-10
2.77

FOR 200L
SPHERICAL
Order
Each
Code
12111-15
1424.21
7832-17*
1606.29
8067-18
106.40
7482-33
53.10
5029-10
2.77

FOR 200L
CYLINDRICAL
Order
Each
Code
12111-15
1424.21
7832-19
1080.76
8067-18
106.40
7482-33
53.10
5029-10
2.77

12141-29

251.90

12141-29

251.90

12141-30

280.65

12141-80
6472-79

69.68
2988.82

12141-80
6472-83

69.68
3514.35

12141-80
6472-87

69.68
3017.57

*7832-17 is 230v, 50A with ground wire.

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Subject to Ace Discount (Page 4)

Net

Components / Temperature Control

153

8318 THERMOMETER Digital Display, Electronic, with Recorder Output


A complete package to enable the user to monitor the temperature of cylindrical jacketed
pilot plant reactors.

Consists of:

8318-35, Type J input digital


thermometer with 5/8 inch LED
display for reading across the
room. 120v 50/60 Hz operation, 1C
resolution, 20C to 390C range,
2% accuracy reading, 1C with
recorder output, fused with clamp
for mounting to 1/2 inch bars.
12141 PFA covered type J
t h e r m o c o u p l e s e n s o r, w i t h
detachable cord, to measure

temperature inside reactor. 24


inch for 10L cylindrical, 36 inch
for 30L cylindrical, 48 inch for 50L
cylindrical.
7482-33 or 5028-30, PTFE adapter,
#25#7
8067-18, adapters to secure
temperature sensor in head of
reactor
5029-10, #7 nylon bushing
For Use with
10L & 20L Cylindrical

Item
Thermometer, Digital
Adapter, Glass 45/50 #25
Adapter, PTFE, #25 #7
Bushing, Nylon, #7
Adapter, #7 24/40
J Thermocouple Sensor, PFA Covered, Detachable
Sensor Cord, only
Complete

Order Code
8318-35

5028-30
12141-26
12141-80
8318-204

Each
596.25

27.61
171.58
69.68
865.12

8318
For Use with
30L Cylindrical

For Use with


50L & 100L Cylindrical

Order Code Each


8318-35
596.25
8067-18
106.40
7482-33
53.10
5029-10
2.77

12141-28
200.08
12141-80
69.68
8318-207 1028.28

Order Code
Each
8318-35
596.25
8067-18
106.40
7482-33
53.10
5029-10
2.77

12141-29
251.90
12141-80
69.68
8318-209
1080.10

12327 DIGITAL TEMPERATURE MONITORJ-Kem


Monitors and displays the temperature of an attached piece of equipment on a bright
LED display. Built-in USB port and free data logging software allows remote temperature
monitoring, and provides a GMP, GLP compliant temperature history. Audible digital alarm
available as an option. 230vac versions are CE marked.
2.5 x 4.75 x 5.5 (Inches, HxWxD) / 50 watts, 120VAC, USB 2.0
J-Kem Model
DM120-T
DM120-J
DM120-K

Temperature
Range (C)
200 to 250
0 to 800
50 to 1200

Thermocouple
Type
T
J
K

Order Code
12327-03
12327-05
12327-07

Each
391.00
391.00
391.00

12327 DIGITAL TEMPERATURE MONITORJ-Kem


230VAC, CE-marked version of digital temperature monitor, above.
J-Kem Model
DM230-T
DM230-J
DM230-K

Temperature
Range (C)
200 to 250
0 to 800
50 to 1200

Thermocouple
Type
T
J
K

Order Code
12327-33
12327-35
12327-37

12327

Each
391.00
391.00
391.00

6470 THERMOWELL without Joint


For use with 5030 Midi AceThred adapter. The completely adjustable depth feature
of this combination means the well is less expensive and more versatile than the jointed
style. Outside diameter, 10mm.
For Flask Cap., mL
250-3000
3000-5000
12000
22000
50000-72000

Length, mm
300
350
400
465
570

Order Code
6470-38
6470-40
6470-42
6470-44
6470-46

6470

Each
16.99
16.49
16.99
16.99
18.53

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

154

Components / Temperature Control


12067 COIL Cooling/Heating, Cylindrical Flasks
For use with pilot plant reactors with cylindrical flasks, with 200mm (8-inch) or 300mm
(12inch) size flanges. Coils are ideal for steam heating or water cooling of reactor contents.
See chart below for tubing size and materials selection; PTFE coated copper, Hastelloy
or stainless steel. Available in 1/4-inch or 1/2-inch O.D. sizes.

12067

Copper/PTFE
Flask Neck Tubing
Size, Size, Size
Order
L
In.
(In.)
Code
Each
10
8
1/4 12067-39
547.05
10
8
1/2 12067-71 1110.49
15
8
1/2 12067-71 1110.49
20
8
1/4 12067-48
600.74
20
8
1/2 12067-71 1110.49
30
8
1/2 12067-40 1134.78
50
8
1/2 12067-44 1692.90
100
12
1/2 12067-79 1773.43
200
12
1/2 12067-80 2123.00

316 Stainless Steel


Hastalloy C-276
Order
Order
Code
Each
Code
Each
12067-239 636.09 12067-439

12067-248 686.14 12067-448


12067-240 1001.74
12067-244 1310.98
12067-279 1584.81
12067-280 1826.24

12067-440
12067-444
12067-479
12067-480

Call
for
Pricing

12067 COIL Cooling/Heating, Spherical Flasks


For use with pilot plant reactors with spherical flasks, with 200mm (8-inch) or 300mm
(12inch) size flanges. Coils are ideal for steam heating or water cooling of reactor contents.
See chart below for tubing size and materials selection; PTFE coated copper, Hastelloy
or stainless steel. Available in 1/4-inch, 1/2-inch and 3/8-inch O.D. sizes.

12067

Copper/PTFE
Flask Neck Tubing
Size, Size, Size
Order
L
In. (Inches) Code
Each
12
6
3/8
12067-58 803.64
22
6
3/8
12067-58 803.64
50
8
3/8
12067-61 892.76
50
8
1/4
12067-52 598.00
72
8
3/8
12067-63 995.02
72
8
1/4
12067-54
Call
100
8
3/8
12067-65 1045.32
100
8
1/2
12067-84 1446.60
100
8
1/4
12067-56
Call
200
12
1/2
12067-68 2011.00

316 Stainless Steel


Order
Code
Each

Hastalloy C-276
Order
Code
Each

12067-261

827.92 12067-461

12067-263

876.97 12067-463

12067-265

1482.00 12067-465

12067-268

1620.67 12067-468

Call
for
Pricing

12069 COILCooling/Heating, Halar Coated


Halar coated 1/4-inch O.D. stainless steel coil for heating and cooling. Designed for small
reactors like the ACE 1000mL PTFE reactor (page <?>) or 1L filter reactors. Fits PTFE
threaded adapters for PTFE heads.

New

Order
Code
12069-06

Each
835.14

12069

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Subject to Ace Discount (Page 4)

Net

Components / Temperature Control

155

12067 HEAT EXCHANGER TUBING Fluorocarbon Covered


Copper tubing encapsulated with Fluorocarbon for use as a make-your-own heat exchanger coil.* Can be used in corrosive solutions or strong solvents like ammonia, fuming
sulfuric acid, potassium hydroxide concentrate, sodium sulfate, etc. Eliminates need for
costly metals like Tantalum. Highly temperature resistant, electrically insulated and will
not stain, corrode or contaminate. Does not support bacteria, and anti-stick property of
Fluorocarbon rinses easily of sticky or clinging materials.
Easy to custom make your own exchanger for heat or cooling by wrapping around
simple mandrel or form to desired size.* Tubing ends can be connected to most any
compression type fitting.
*Shipped in 2-3 foot diameter coils for forming to desired shape, 50 foot max. continuous run. ACE can supply coiled exchanger to suit your needs. For a quotation, please
send us specifications.
Nominal
Copper
O.D., in.
1/4
3/8
1/2

Fluorocarbon
Wall
(Inches)
.015
.015
.020

Copper
Wall
(Inches)
.030
.030
.030

Approx.
Approx.
Sq. Ft. of
Min. Bend Surface Per
Order
Dia., in.
Linear Ft.
Code
2
.0733
12067-15
4
.106
12067-20
8
.141
12067-25

12067

Each
20.62
25.21
31.22

12111 TEMPERATURE CONTROLLER Time Proportional, Digital


Microprocessor based, compact, temperature controller, with bright LED display. Temperature range is -70 to 870 C with 0.1 C resolution. Temperature readout in farenheit or
centigrade is field selectable. Designed to use Type J thermocouple sensors. The code
-15 and -33 units have two, 120V front outlets. The -47 and -58 units have 2-120 volt rear
outlets and one selectable, 20V or 40V front outlet. Both models have 16 segment ramp
and soak selectable profile. This model has an over-temp cutoff and alarm output for added
safety. Output circuitry utilizes zero-crossing fired solid state relay for proportional control
that provides interference free power (RFI) to electric heater type resistive loads. 120volt,
15Amp, 60Hz input. Unit is 6-inch x 6.5-inch x 5.5-inch (HxDxW); weight = 4 lbs. Three-year
conditional warranty. Complete unit comes with type J thermocouple.

12111-15

Order
Code
Each
12111-15 1424.21
12110-15 103.65
12111-33 1527.86

With Two Front 120v Outlets


Controller, only
Sensor, Type J Thermocouple, 318mm, 1/4-inch O.D.
Complete (above two components)
OPTIONAL COMPONENTS:
Sensor, Type J Thermocouple, 102mm, 3/16-inch
Sensor, Type J Thermocouple, 305cm, fiberglass insulated, w/ot sheath
Sensor, Type J Thermocouple, 305cm, double PTFE insulated, w/o sheath
Sensor Extension, 2.4M (8-inch) w/mating connectors, double PTFE insulated

12110-17
12110-24
12110-25
12110-26

89.63
50.88
50.88
59.97

Contact ACE to get a copy of our Laboratory Glassware


and Equipment catalog!

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

156

Components / Temperature Control

ACE Economy Model Temperature Controller


for general laboratory use
Economy model
Ultra compact (2 inches high)
New digital technology
16 segment ramp and soak function
Fuzzy logic auto tune PID
Temp. Range Field Selectable
Features & Specifications

12125-32

Bar mountable or benchtop operation.


Single loop type, downsized and lightweight.
Temperature range: 50 to 800C, adjustable.
0.1C* or 0.1F temperature resolution, selectable.
Absolute accuracy: 0.25% of range, max. 2C.
Control accuracy: 0.1C typical.
Microprocessor-based 1/32 DIN model for digital accuracy and
reliability.
Dual four-digit LED display for instant recognition of process
temperature and setpoint 1 value.
Auto tune PID control can maintain 0.1 under normal
conditions.
Ramp and soak, field selectable, 16 segment with hold or
shut-off.
Field selectable output % power limit when heating smaller
vessels or when using very low setpoints. See OEM manual
(SIOH) secure menu, affects all heaters.
Output circuitry utilizes zero crossing fired solid state relay
proportional control that provides interference free power (RFI)
to electrical heater type resistive loads.
Rear heater outlet provides time proportional control, meaning
overshoot is minimized. Percent output decreases as set
temperature is approached.
Input power: 120 volts, 50/60 Hz, 15 amps maximum
Unit measures: 2 inches high x 5-1/4 inches wide x 5-1/4 inches
deep; weight: 2 lbs, 2 oz.
Operating instruction label on top for quick reference.
Three-year warranty

Valu
e

12125 TEMPERATURE CONTROLLER


Economy Model

Controller, only (J type)


Controller, only (T type)
Controller, only (K type)
Sensor, Type J Thermocouple,
318 mm, 1/4 inch
Complete (J Type only)

Order Code

Each

12125-14
12125-16
12125-18

797.11
797.11
797.11

12110-15

103.65

12125-32

900.76

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

For use in
all
controlling es
antl
Glas-Col M olts
v
rated at 115

Subject to Ace Discount (Page 4)

Net

Components / Temperature Control

157

Improved ACE Temperature Controller


for General Laboratory Use...
Including mantles up to 22 Liters
Features & Specifications:

Two

front-mounted 120v outlets

Two front-mounted outlets.

Compact

(3.5 inches high)

Bar mountable or benchtop operation.


Single loop type, downsized and lightweight.

New

digital technology

Temperature range: 70 to 870C, adjustable.

16
segment ramp and soak function

0.1C/0.1F temperature resolution, field selectable.


Absolute accuracy: 0.25% of range, max. 2C.

Fuzzy

logic auto tune PID

Control accuracy: 0.1C typical.


Microprocessor-based 1/32 DIN model for digital
accuracy and reliability.
Dual four-digit LED display for instant recognition of
process temperature and setpoint 1 value.
Auto tune PID control can maintain 0.1 under
normal conditions.
Ramp and soak, field selectable, 16 segment with
hold or shut-off.
Field selectable output % power limit when heating
smaller vessels or when using very low setpoints.
(factory set at 60% for safety). See OEM Manual
(S1OH) secure menu.
Output circuity utilizes zero crossing fired solid state
relay proportional control that provides interference
free power (RFI) to electrical heater type resistive
loads.
Heater outlets provide time proportional control,
meaning overshoot is minimized. Percent output
decreases as set temperature is approached.
Universal TC input jack for mini or standard
plugs.
Input power: 120 volts, 50/60 Hz, 15 amps maximum,
fused.
Unit measures: 3.5 inches high x 6-3/16 inches wide x
6-5/16 inches deep; weight: 2.5 lbs.
Operating instruction label on top for quick reference

For use in
all
controlling tles
an
Glas-Col M volts
5
rated at 11

12126 TEMPERATURE CONTROLLER Improved Model


Controller, only
Sensor, Type J Thermocouple, 318mm, 1/4 in.
Complete

Order Code
12126-24
12110-15
12126-45

Each
874.72
103.65
978.37

Digital interface available. Call for details.

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

158

Components / Temperature Control


12127 TEMPERATURE CONTROLLERInstatherm Model
Bar mountable or benchtop operation. Single loop type, downsized and lightweight.
Temperature range: 70 to 870C, field settable to F. FIeld selectable 0.1C/0.1F temperature
resolution. Absolute accuracy: 0.25% of range, maximum 2C. Control accuracy: 0.1C
typical. Supplied with two 120v controlled rear outlets for up to 22L mantles or 120v
ACE oil baths. Supplied with single 20v or 40v controlled limit front outlet for low voltage
Instatherm or small mantles. Ramp and soak, field selectable, 16 segment with hold or
shut-off. Field adjustable rear sensitivity control to tweek the speed of response to setpoint,
if necessary, this eliminates overshoot. Universal TC input jack for mini or standard
plugs. Input power: 120 volts, 50/60 Hz, 15 amps maximum, fused. Unit measures: 3.5
high x 6-3/8 wide x 8 deep inches; weight: 3.4 lbs. Operating instruction label on top for
quick reference. Three-year warranty.

12127

Order Code

Each

Controller, only
Sensor, Type J Thermocouple, 318 mm, 1/4-inch OD
Complete (above components)

12127-30
12110-15
12127-40

1350.16
103.65
1453.81

Controller, only
Sensor, Type J Thermocouple, 102 mm, 3/16-inch OD
Complete (above components)

12127-30
12110-17
12127-52

1350.16
89.63
1439.79

12312 TEMPERATURE CONTROLLER J-Kem Apollo Series, Dual Channel


Has all the features of the Gemini series, above, but also has an independent 100-hour
digital timer on each controller channel.
4 x 8 x 9 (Inches, HxWxD) / 120vac, 15 amps, 1800 watts total / 1200 watts maximum
per channel
J-Kem Model
Apollo-T
Apollo-J
Apollo-K
Apollo-Pt

12312

With Sensor, Cord


and Adapter
No
No
No
No

Temperature
Range (C)
200 to 250
0 to 800
50 to 1200
200 to 400

Thermocouple
Type
T
J
K
RTD

Order
Code
12312-03
12312-05
12312-07
12312-09

Each
1393.80
1393.80
1393.80
1393.80

The Apollo Series units noted above require two


thermocouple sensors, two cords and two adapters.

12314 TEMPERATURE CONTROLLER J-Kem Quad Series, Four Channel


The Quad is your solution when bench space is at a premium the Quad packs four
independent temperature controllers into a single unit! Each of the four controller channels
has 1200 watts of power, an independent display, and an over-temperature protection circuit.
5.25 x 7 x 7.5 (Inches, HxWxD) / 120vac, 15 amps, 1800 watts total / 1200 watts max.
per channel

12314

J-Kem Model
Quad-T
Quad-J
Quad-K
Quad-Pt

With Sensor, Cord


and Adapter
No
No
No
No

Temperature
Range (C)
200 to 250
0 to 800
50 to 1200
200 to 400

Thermocouple
Type
T
J
K
RTD

Order
Code
12314-05
12314-07
12314-09
12314-11

Each
2295.40
2295.40
2295.40
2295.40

The Quad Series units noted above require four


thermocouple sensors, four cords and four adapters.

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Subject to Ace Discount (Page 4)

Net

Components / Temperature Control

159

12167 LAB SAFETY CONTROLLER J-Kem Model LS-120


Lab safety controller by J-Kem combines all the features of the digital temperature monitor
and the water-flow monitor into a single versatile instrument. Plug any piece of equipment
into the monitor, then if the water flow rate falls below the set level, or if the reaction temperature goes above or below the user set limits, the outlet power turns off automatically.
The unit will also cut off power if the main power is interrupted. The controller then has to
be reset. See ACE 12168 product family for flow sensors.
J-Kem Model
LS-120-T
LS-120-J
LS-120-K
J-Kem Model
WFM-01
WFM-02
WFM-03

Thermocouple
Order
Type
Code
T
12167-01
J
12167-03
K
12167-05

With Sensor Cord


and Adapter
No
No
No

Temperature
Range (C)
200 to 250
0 to 800
50 to 1200

Description
Flow Sensor
Flow Sensor
Flow Sensor
Shut-Off Valve

Flow Rate, LPM


0.1 to 2.5
1 to 10
2 to 30

Order Code
12168-01
12168-02
12168-03
12168-10

Each
772.80
772.80
772.80

Each
240.00
240.00
240.00
172.50

12167

12160 WATER FILTER


Installs ahead of sensing head. 50 micron screen prevents failure of sensing head due
to dirt or rust coming from the water supply. Supplied with replaceable filter cartridge.
Has 3/8-inch O.D. hose connections. Labeled inlet and outlet.
Order Code
12160-35

Each
32.40

12160-35

12162 WATER-FLO POWER CUT-OFF 15 amps, with Timer


Supplied with front panel mounted timer. In the event of water flow failure and subsequent
power shut-off at the outlets, timer indicates accumulated elapsed time. Timer runs for
up to 10,000 hours before starting at zero again, smallest reading is 0.1 hour. Cannot
be reset. Note: a reset-able timer is available, at slightly higher cost. Call for quotation.
Sensing Head, w/Water Filter
Power Pack, only
Complete

Order Code
12160-06
12162-07
12162-14

Each
235.19
823.95
1059.14

12162-14

12164 WATER-FLO POWER CUT-OFF 20 amps (230 volts)


Will control one or two apparatus at 4.6 kilowatts AC power, 208-250 volts, 50/60
Hz. (up to 20 amps), fused. Two rear outlets allow use with our 7830-71 power
supply and 12165 shut-off water valve (230v).
Sensing Head, w/Water Filter
Power Pack, only
Complete

Order Code
12160-06
12164-20
12164-30

12164

Each
235.19
962.41
1197.60

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

160

Components / Temperature Control


12165 ELECTRO-FLO SHUT-OFF VALVE
A water or air* shut-off solenoid valve for use with 12160, 12162 or 12164 water-flo power
cut-off or as a general laboratory shut-off valve. Operates from 0.35Kg/cm2 to 10.5Kg/
cm2 (5 to 150 psi) for water or 0.35Kg/cm2 for air and up to 91C. Internal design of pilotoperated, piston-type, valve assures exceptional flow performance. Constructed of cast
bronze with waterproof cast-coil that has a lifetime warranty. Valve must be installed in
horizontal piping with solenoid in vertical position. Supplied with 1.8 meter grounded
cord and female pipe thread. Codes -14, -20 and -26 for use with 12160 and 12162.
Codes -48, -54 and -57 for use with 12164. Note: a pre-filter is recommended when this
product is used with water or air (15 micron or less).
(For 120v)

12165

Pipe Sizes, mm Order Code


9.5 (3/8 in.)
12165-14
12.7 (1/2 in.)
12165-20
19.1 (3/4 in.)
12165-26

(For 230v)

Each
243.47
259.87
307.21

Order Code
12165-48
12165-54
12165-57

Each
246.19
260.33
307.11

*When used as air shut-off valve, a strainer is recommended.

12168 WATER FLOW MONITOR J-Kem Model WFM-120


12168

J-Kem monitor precisely measures the flow of water through a condenser, bath or a
photochemical reactor. Upon interruption or if the flow drops below an operator set
rate, power to the monitored equipment is cutoff. Manual power reset. Inclusion of
a 1216810 shut-off valve and either a 1216901 audible alarm or a 1216905 digital
alarm is recommended.
J-Kem Model
WFM-01
WFM-02
WFM-03

WFM-120

Description
Flow Sensor
Flow Sensor
Flow Sensor
Shut-Off Valve
Water Flow Monitor

Flow Rate, LPM


0.1 to 2.5
1 to 10
2 to 30

Order Code
12168-01
12168-02
12168-03
12168-10
12168-120

Each
240.00
240.00
240.00
172.50
354.20

12169 ALARMJ-Kem
Digital alarm outlet and audible alarm accessories for J-Kem safety controller and waterflow monitors. Allows 12167 and 12168 units to be set up for alarm warnings when in
unsafe conditions. The audible alarm sounds during low or no water conditions for the
12168 monitor and the digital alarm activates on either the water flow monitor or the safety
controller when conditions are out of set ranges.
J-Kem Model Alarm Type
WFM-AA
Digital
WFM-OC
Audible

For Controllers
12167 & 12168
12168

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Order Code
12169-01
12169-05

Each
65.00
35.00

Subject to Ace Discount (Page 4)

Net

Components / Sensors

161

TYPE: Thermocouple Sensor Probes (continued)


Length of
Max. Lead
Inconel Sheath, Sheath
Sheath Sheath Lgth.,
Lead
Order
Type
mm (In.)
O.D. mm/In. Coating Temp.
Ft. Attachment
Code
K
305 (12)
6.35/0.25
Plain
550C 3-15 Detachable* 12141-43
K
600 (24)
6.35/0.25
Plain
550C 3-15 Detachable* 12141-44
K
900 (36)
6.35/0.25
Plain
550C 3-15 Detachable* 12141-47
K
1200 (48)
6.35/0.25
Plain
550C 3-15 Detachable* 12141-48
K
1800 (72)
6.35/0.25
Plain
550C 3-15 Detachable* 12141-50
K
305 (12)
6.35/0.25
PFA
260C 3-15 Detachable* 12141-52
K
600 (24)
6.35/0.25
PFA
260C 3-15 Detachable* 12141-53
K
900 (36)
6.35/0.25
PFA
260C 3-15 Detachable* 12141-58
K
1200 (48)
6.35/0.25
PFA
260C 3-15 Detachable* 12141-59
K
1800 (72)
6.35/0.25
PFA
260C 3-15 Detachable* 12141-60
*Lead only, for TYPE J Sensor (Black)
12141-80
*Lead only, for TYPE K Sensor (Yellow)
12141-83
PFA: (Tetrafluoroethylene-perfluoro(propylvinyl ether) copolymer), colored
black, less permeable than either FEP or TFE. Maximum temperature
260C.

Each
76.26
90.73
104.96
171.88
154.65
125.41
171.23
196.65
248.64
287.50
69.68
77.70

12141-80, -83
12141

3' coiled PVC


patch cord
stretchable to 15';
detachable
from sheath via
color-coded
universal
connectors with
mini-male plug

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

162

Components / Sensors
TYPE: Thermocouple Sensor Probes
Thermocouple
Subminiature
flat blade male
connectors

12140
PTFE covered
with stainless
steel overbraid

Permanently
attached lead
with spring
transition for
strain relief

Plain Inconel or
PFA covered

12110
12140

Type
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
K
K
K
K
K
K
K
K
K
K
K
K
K
K
K
K

Length of
Max. Lead
Inconel Sheath,
Sheath
Sheath Sheath Lgth.,
Lead
Order
mm (In.)
O.D. mm/In. Coating Temp.
Ft.
Attachment
Code
Each
102 (4)
4.76/0.19
Plain
550C
6
Permanent 12110-17 89.63
305 (12)
1.59/0.06
Plain
550C
12
Permanent 12140-04 180.56
305 (12)
3.17/0.12
Plain
550C
12
Permanent 12140-05 178.30
305 (12)
6.35/0.25
Plain
550C
6
Permanent 12110-15 103.65
305 (12)
6.35/0.25
Plain
550C
12
Permanent 12140-06 179.64
600 (24)
6.35/0.25
Plain
550C
12
Permanent 12140-10 188.31
900 (36)
6.35/0.25
Plain
550C
12
Permanent 12140-14 213.71
1200 (48)
6.35/0.25
Plain
550C
12
Permanent 12140-16 266.78
1800 (72)
6.35/0.25
Plain
550C
12
Permanent 12140-18 284.70
305 (12)
1.59/0.06
PFA
260C
12
Permanent 12140-17 228.66
305 (12)
3.17/0.12
PFA
260C
12
Permanent 12140-19 230.76
305 (12)
6.35/0.25
PFA
260C
12
Permanent 12140-20 232.59
600 (24)
6.35/0.25
PFA
260C
12
Permanent 12140-21 237.17
900 (36)
6.35/0.25
PFA
260C
12
Permanent 12140-25 267.68
1200 (48)
6.35/0.25
PFA
260C
12
Permanent 12140-26 302.55
1800 (72)
6.35/0.25
PFA
260C
12
Permanent 12140-28 335.48
305 (12)
6.35/0.25
Plain
550C 3-15 Detachable* 12141-11 77.05
600 (24)
6.35/0.25
Plain
550C 3-15 Detachable* 12141-12 94.56
900 (36)
6.35/0.25
Plain
550C 3-15 Detachable* 12141-17 98.68
1200 (48)
6.35/0.25
Plain
550C 3-15 Detachable* 12141-18 126.23
1800 (72)
6.35/0.25
Plain
550C 3-15 Detachable* 12141-20 160.06
305 (12)
6.35/0.25
PFA
260C 3-15 Detachable* 12141-25 118.70
600 (24)
6.35/0.25
PFA
260C 3-15 Detachable* 12141-26 171.58
900 (36)
6.35/0.25
PFA
260C 3-15 Detachable* 12141-28 200.08
1200 (48)
6.35/0.25
PFA
260C 3-15 Detachable* 12141-29 251.90
1800 (72)
6.35/0.25
PFA
260C 3-15 Detachable* 12141-30 280.65
102 (4)
4.76/0.19
Plain
550C
6
Permanent 12113-22 88.14
305 (12)
1.59/0.06
Plain
550C
12
Permanent 12140-36 177.96
305 (12)
3.17/0.12
Plain
550C
12
Permanent 12140-61 178.30
305 (12)
6.35/0.25
Plain
550C
6
Permanent 12113-20 99.72
305 (12)
6.35/0.25
Plain
550C
12
Permanent 12140-39 177.00
600 (24)
6.35/0.25
Plain
550C
12
Permanent 12140-41 191.48
900 (36)
6.35/0.25
Plain
550C
12
Permanent 12140-45 216.89
1200 (48)
6.35/0.25
Plain
550C
12
Permanent 12140-46 246.44
1800 (72)
6.35/0.25
Plain
550C
12
Permanent 12140-48 284.70
305 (12)
1.59/0.06
PFA
260C
12
Permanent 12140-37 228.87
305 (12)
3.17/0.12
PFA
260C
12
Permanent 12140-62 228.87
305 (12)
6.35/0.25
PFA
260C
12
Permanent 12140-51 226.79
600 (24)
6.35/0.25
PFA
260C
12
Permanent 12140-53 236.39
900 (36)
6.35/0.25
PFA
260C
12
Permanent 12140-57 270.30
1200 (48)
6.35/0.25
PFA
260C
12
Permanent 12140-58 302.55
1800 (72)
6.35/0.25
PFA
260C
12
Permanent 12140-59 335.48

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Subject to Ace Discount (Page 4)

Net

Components / Sensors

163

Thermocouple Sensors for


J-Kem Temperature Controllers
12180 T-TYPE SENSORS

12182 K-TYPE SENSORS

Type T thermocouple temperature sensors for use with


all J-Kem T type model temperature controllers. Either
1/4- or 1/8-inch O.D. Available in 304 stainless steel or
PTFE coated stainless steel sheaths of various lengths.
See ACE 12190 series extension cords.
O.D. Lgth.
PTFE
Order
(in.)
(in.) Coated?
Code
Each
6
No
12180-03
34.00
1/8
1/8
12
No
12180-05
34.00
1/8
18
No
12180-07
45.00
1/8
24
No
12180-09
49.00
1/8
36
No
12180-11
62.00
6
Yes
12180-20
64.00
1/8
1/8
12
Yes
12180-22
64.00
1/8
18
Yes
12180-24
75.00
1/8
24
Yes
12180-26
79.00
1/8
36
Yes
12180-28
92.00
6
No
12180-31
38.00
1/4
1/4
12
No
12180-33
38.00
1/4
18
No
12180-35
49.00
1/4
24
No
12180-37
53.00
1/4
36
No
12180-39
66.00
6
Yes
12180-40
68.00
1/4
1/4
12
Yes
12180-42
68.00
1/4
18
Yes
12180-44
79.00
1/4
24
Yes
12180-46
83.00
1/4
36
Yes
12180-48
96.00

Type K thermocouple temperature sensors for use with


all J-Kem K type model temperature controllers. Either
1/4- or 1/8-inch O.D. Available in 304 stainless steel or
PTFE coated stainless steel sheaths of various lengths.
See ACE 12190 series extension cords.
O.D. Lgth.
PTFE
Order
(in.)
(in.) Coated?
Code
Each
6
No
12182-01
34.00
1/8
1/8
12
No
12182-03
34.00
1/8
18
No
12182-05
45.00
1/8
24
No
12182-07
49.00
1/8
36
No
12182-09
62.00
6
Yes
12182-20
64.00
1/8
1/8
12
Yes
12182-22
64.00
1/8
18
Yes
12182-24
75.00
1/8
24
Yes
12182-26
79.00
1/8
36
Yes
12182-28
92.00
6
No
12182-32
38.00
1/4
1/4
12
No
12182-34
38.00
1/4
18
No
12182-36
49.00
1/4
24
No
12182-38
53.00
1/4
36
No
12182-40
66.00
6
Yes
12182-41
68.00
1/4
1/4
12
Yes
12182-43
68.00
1/4
18
Yes
12182-45
79.00
1/4
24
Yes
12182-47
83.00
1/4
36
Yes
12182-49
96.00

12181 J-TYPE SENSORS

12183 RTD TYPE SENSORS

Type J thermocouple temperature sensors for use with


all J-Kem J type model temperature controllers. Either
1/4- or 1/8-inch O.D. Available in 304 stainless steel or
PTFE coated stainless steel sheaths of various lengths.
See ACE 12190 series extension cords.
O.D. Lgth.
PTFE
Order
(in.)
(in.) Coated?
Code
Each
6
No
12181-02
34.00
1/8
1/8
12
No
12181-04
34.00
1/8
18
No
12181-06
45.00
1/8
24
No
12181-08
49.00
6
Yes
12181-21
64.00
1/8
1/8
12
Yes
12181-23
64.00
1/8
18
Yes
12181-25
75.00
1/8
24
Yes
12181-27
79.00
1/8
36
Yes
12181-29
92.00
6
No
12181-32
38.00
1/4
1/4
12
No
12181-34
38.00
1/4
18
No
12181-36
49.00
1/4
24
No
12181-38
53.00
1/4
36
No
12181-39
72.00
6
Yes
12181-41
68.00
1/4
1/4
12
Yes
12181-43
68.00
1/4
18
Yes
12181-45
79.00
1/4
24
Yes
12181-47
83.00
1/4
36
Yes
12181-49
96.00

RTD (Pt/100) type thermocouple temperature sensors


for use with J-Kem model RTD temperature controllers.
Either 1/4- or 1/8-inch O.D. All PTFE coated stainless steel
sheaths of various lengths. Uncoated available via special
order. See ACE 12190 series extension cords.
O.D. Lgth.
PTFE
Order
(in.)
(in.) Coated?
Code
Each
6
Yes
12183-02
129.00
1/8
1/8
12
Yes
12183-04
129.00
1/8
18
Yes
12183-06
140.00
1/8
24
Yes
12183-08
144.00
1/8
36
Yes
12183-10
157.00
6
Yes
12183-40
132.00
1/4
1/4
12
Yes
12183-42
132.00
1/4
18
Yes
12183-44
144.00
1/4
24
Yes
12183-46
148.00
1/4
36
Yes
12183-48
161.00

For extension cords, see ACE


12190 straight and coiled cords,
on the following page.

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Components / Sensors

164

Sensor extension cords for use with all J-Kem thermocouple probes. Cords match color of probe type: blue, black, yellow
or white. Available in either 10- or 20-foot coiled or straight styles. Select length, type, and connector, SMP (flat plug) or
OST (round plug).

12190
(Straight)

12190
(Coiled)

12190 SENSOR CORDSCoiled


Probe Lgth. Connector Order
Style
(ft.)
Type
Code
J
10
SMP
12190-01
K
10
SMP
12190-02
T
10
SMP
12190-03
RTD
10
SMP
12190-04
J
10
OST
12190-08
K
10
OST
12190-10
T
10
OST
12190-11
J
20
SMP
12190-20
K
20
SMP
12190-21
T
20
SMP
12190-22
J
20
OST
12190-26
K
20
OST
12190-27
T
20
OST
12190-28

Each
33.80
33.80
33.80
56.20
38.80
38.80
38.80
67.00
67.00
67.00
67.00
67.00
67.00

Probe Lgth. Connector Order


Style
(ft.)
Type
Code
J
10
SMP
12190-40
K
10
SMP
12190-41
T
10
SMP
12190-42
J
10
OST
12190-44
K
10
OST
12190-45
T
10
OST
12190-46
J
20
SMP
12190-50
K
20
SMP
12190-51
T
20
SMP
12190-52
J
20
OST
12190-56
K
20
OST
12190-57
T
20
OST
12190-58

Each
26.25
26.25
26.25
26.25
26.25
26.25
36.30
36.30
36.30
36.30
36.30
36.30

SMP

OST

12190 SENSOR CORDSStraight


12184 DUAL SENSORS PTFE Coated
Dual coupling temperature thermocouple sensors for use
with Model HCC and 270 J-Kem temperature controllers.
Available in J, T or K types. Probes are PTFE coated
stainless steel in various lengths and O.D. Probes require
12191 extension cords.
O.D. Lgth. Sensor
Order
(in.)
(in.)
Type
Code
Each
1/8
12
T
12184-02
103.00
1/4
12
T
12184-04
115.00
1/4
24
T
12184-06
137.00
1/4
36
T
12184-08
151.00
1/8
12
J
12184-12
103.00
1/4
12
J
12184-14
115.00
1/4
24
J
12184-16
137.00
1/4
36
J
12184-18
151.00
1/8
12
K
12184-20
103.00
1/4
12
K
12184-22
115.00
1/4
24
K
12184-24
137.00
1/4
36
K
12184-26
151.00

12191 DUAL SENSOR CORDS


Dual element extension cords for use with dual element
12184 sensors for J-Kem models HCC and 270
temperature controllers. Available in T, K, and J
types in 10 or 25-ft. lengths.
Probe Lgth.
Order
Style
(ft.)
Code
Each
T
10
12191-02
59.50
J
10
12191-06
59.50
K
10
12191-08
59.50
T
25
12191-20
94.25
J
25
12191-22
94.25
K
25
12191-24
94.25

12184

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Subject to Ace Discount (Page 4)

Net

TH

A N N I V E R S A R Y

TED
RA

ACE G

S
A

C
N
OR
I
S

165

1936 2011

VI

USA

NE

N
,
LAND

Components / Temperature Control

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

166

Components / Heating Mantles


6478 MANTLEFabric/Cloth
6478-05

For use with 6476 and 6477 reaction flasks. Upper temperature limit, 450C. Must be
operated through a temperature controller. CSA approved. Detachable 4-foot cord and
locking connector.
For Flask
Size, mL
500
1000
1500
2000
3000

6478

I.D. x Depth, inches/mm


4.63/117.4 x 2.5/63.5
4.63/117.4 x 5.63/142.8
4.63/117.4 x 6.63/168.2
4.63/117.4 x 8. 89/225.4
4.63/117.4 x 10/254

Watts/Volts
250w-115v
300w-115v
380w-115v
450w-115v
600w-115v

Order
Code
6478-05
6478-10
6478-15
6478-20
6478-25

Each
346.55
322.54
350.06
374.61
381.58

6478 MANTLE Aluminum Housing, For Cylindrical Flasks


Cylindrical type for use with 6476 and 6477 reaction flasks. With hard aluminum housing.
CSA approved, 115 volt c
omplete with 4-foot detachable cord with locking connector.
Temperature range is Ambient +10C to 450C. Must be operated through a temperature
controller. 230V versions available.
For Flask Maximum Flask
Size, mL Dia., in./mm
500
4.63/117.4
1000
4.63/117.4
1500
4.63/117.4
2000
4.63/117.4
3000
4.63/117.4

I.D. x Depth, inches/mm


4.63/117.4 x 2.5/63.5
4.63/117.4 x 5.63/142.8
4.63/117.4 x 6.63/168.2
4.63/117.4 x 8. 89/225.4
4.63/117.4 x 10/254

Watts/Volts
250w-115v
300w-115v
380w-115v
450w-115v
600w-115v

Order
Code
6478-45
6478-47
6478-49
6478-51
6478-53

Each
320.00
334.00
347.00
356.00
382.41

12031 MANTLE Spherical, Fabric/Cloth


Covers both top and bottom of 1-, 2-, or 3-neck flasks. Temperature range is Ambient
+10C to 450C. The circumferential zipper holds the halves snugly together to prevent
heat loss, and the side split in the top section allows for easy flask removal. CSA certified.
Each half has a four-foot cord and locking connector. 230v CE-approved versions are
available.

12031

Silicone
Impregnated
Glass
Fabric

For Flask
Size, mL
1000
2000
3000
5000

Distribution
Lower Half Upper Half
380w-115v 140w-115v
500w-115v 200w-115v
500w-115v 200w-115v
600w-115v 300w-115v

Order Code
12031-19
12031-21
12031-23
12031-25

Each
588.00
616.00
647.00
768.00

12035 MANTLE Hemispherical, Fabric/Cloth


12035

Adaptable to unusual shapes and sizes. Temperature to 450C. Detachable 4-foot cord,
2-wire cord and locking connector. CSA certified. Requires 12095 or 12096 supports.
Must be operated through a temperature controller.

Silicone
Impregnated
Glass
Fabric

For Flask Size mL


1000
2000
3000
5000
12000

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Watts/Volts
380w-115v
500w-115v
500w-115v
600w-115v
(2) 650w-115v

Order Code
12035-19
12035-21
12035-23
12035-25
12035-27

Each
219.00
239.00
266.00
324.00
657.00

Subject to Ace Discount (Page 4)

Net

Components / Heating Mantles

167

12036 MANTLESFabric/Cloth
For use with 6504 or 6511 reaction flasks. Upper temperature limit, 450C. Four-foot cord
and locking connector. Must be operated through a temperature controller. CSA approved.
For Flask
Size, mL
500
1000
2000
3000
4000

I.D. x Depth, inches/mm


3.75/95.2 x 4.5/114.3
4.25/107.9 x 5.2/132
5.5/139.7 x 6.0/152.3
5.5/139.7 x 9.0/228.6
5.5/139.7 x 11.0/279.4

Watts/Volts
270w-115v
335w-115v
470w-115v
550w-115v
750w-115v

Order
Code
12036-17
12036-19
12036-21
12036-23
12036-24

Each
334.00
350.00
361.00
387.00
393.00

12036

12041 MANTLE Cylindrical Reaction Flasks, Fabric/Cloth


Girdle style mantles for ACE large size cylindrical and spherical flasks and pilot plant
assemblies. Codes -10 through -37 fit 6521, 6522 and 6472 flasks. -40, -42, -44 fit 6530
and 6533 spherical flasks. Fit easily into our four-post stands for large reactor assemblies.
Flask Size, Liter
6/10
15
30
50
30
50
50
50
72
100
100
200

Flask Type
Cylindrical
Cylindrical
Cylindrical
Cylindrical
Cylindrical
Cylindrical
Cylindrical
Spherical
Spherical
Spherical
Cylindrical
Cylindrical

Watts/Volts
495w115v
700w115v
(2) 880w115v
(2) 880w115v
(2) 825w115v
(2) 725w115v
(3) 1100w115v
1200w115v
(2) 1800w230v
(3) 1400w230v
(4) 1200w115v
(4) 1100w115v

Order Code
12041-10
12041-12
12041-16
12041-18
12041-32
12041-35
12041-37
12041-40
12041-42
12041-44
12041-48
12041-52

Each
860.65
777.15
1201.84
1090.99
979.40
1236.96
1617.65
1394.13
1771.47
2335.70
2222.22
2228.41

12041

12043 MANTLE Aluminum Housing


Offers the benefit of grounding through aluminum housing. The heating element is embedded in layers of glass fabric to protect the flask wall from thermal strain, and is thoroughly covered with glass insulation to prevent heat from being radiated outward. Glass
fabric affords operating temperatures to 450C. With detachable 4-foot, 3-wire cord and
locking connector. Requires 12094 support. CSA certified. Must be operated through a
temperature controller. 230v version is also available for 250mL and larger mantles.
For Flask Size, mL
1000
2000
3000
5000
12000
22000
50000
50000 (For Schott)
72000

Max. Flask
Dia., in./mm
5.1/130
6.6/170
7.2/183
8.6/220
11.5/293
13.6/347
17.9/456
19.9/506
20.5/522

I.D. x Depth, inches/mm


5.1/130 x 2.5/65
6.6/170 x 3.3/85
7.2/184 x 3.6/91.5
8.7/222 x 4.3/110
11.5/294 x 5.8/147.6
13.7/350 x 6.8/173.5
18.0/458 x 8.9/228
19.9/506 x 8.9/228
20.6/525 x 10.1/258.9

Watts/Volts
Order Code
380w-115v 12043-19
500w-115v 12043-21
500w-115v 12043-23
600w-115v 12043-25
(2)650w-115v 12043-27
(2)770w-115v 12043-29
(3)1000w-115v 12043-31
(3)1000w-115v 12043-32
(2)2000w-230v 12043-33

12043

Each
295.00
312.00
375.00
470.00
871.00
984.00
1624.37
1942.40
1784.00

12044 MANTLE Aluminum Housing, with Bottom Opening


Same as 12043, above, but with bottom opening to accommodate flasks such as 6450,
6469, 6534, and 6536.
For Flask Max. Flask
Bottom Opening
Size, mL Dia., in./mm I.D. x Depth, inches/mm
Watts/Volts
Dia., In./mm
3000
7.2/183
7.2/184 x 3.6/91.5
500w-115v
2.5/63.5
5000
8.6/220
8.7/222 x 4.3/110
600w-115v
2.5/63.5
12000
11.5/293
11.5/294 x 5.8/147.6
(2)650w-115v
2.5/63.5
12000
11.5/293
11.5/294 x 5.8/147.6
(2)650w-115v
5.0/127
22000
13.6/347
13.7/350 x 6.8/173.5
(2)770w-115v
2.5/63.5
22000
13.6/347
13.7/350 x 6.8/173.5
(2)770w-115v
5.0/127
50000
17.9/456
18.0/458 x 8.9/228 (3)1000w-115v
5.0/127
72000
20.5/522
20.6/525 x 10.1/258.9 (2)2000w-230v
5.0/127

Order
Code
12044-24
12044-26
12044-28
12044-29
12044-30
12044-31
12044-34
12044-37

12044

Each
579.43
655.20
1091.72
1085.97
1207.35
1144.15
1730.49
1935.06

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168

Components / Heating Mantles


12045 STIRMANTLE Aluminum Housing
Mantle with magnetic stirrer built-in, able to handle up to 72L spherical flask. Ideal
for continuous distillations. The variable speed control (included) offers total mixing
management. DC filtering allows the 1/50 hp motor to run cooler, thus extending motor
life. With four bottom, 4-inch high feet to allow bench clearance and air flow. Stir
motor control is detachable and allows speeds of 1001850 rpm. Heaters are supplied
with a detachable four-foot cord on codes -12, -22; codes -50,-55 and -72 must be
hard wired. Temperature range is Ambient +10C to 450C. Supplied with .75-inch
diameter x 3-inch long magnetic stirring bar. CSA certified. Must be operated through
a temperature controller.
For Flask Size, mL
12000
22000
50000
50000 (For Schott)
72000

12045

Maximum Flask
Dia., in./mm I.D. x Depth, inches/mm
Watts/Volts
(2) 650w115v
11.5/293
11.6/295 x 5.7/147
13.6/347
13.7/348 x 6.8/173.5
(2) 770w115v
17.9/456
18.1/460 x 8.9/228
(3) 1000w230v*
19.9/506
20/508 x 10.1/258.8
(3) 1000w230v*
20.5/522
20.6/525 x 10.1/258.8 (2) 2000w230v*

Order Code
12045-12
12045-22
12045-50
12045-55
12045-72

Each
1452.00
1551.00
2086.00
2163.00
2160.00

*Codes -50, -55 and -72 must be hard wired. 115v units are also available in 230v versions.

12047 HEATING TOPSFabric/Cloth


For use with 1-, 2- and 3-neck flasks. Top can be put on flask without disturbing
permanently attached equipment. mperature range is Ambient +10C to 450C.For
use with 12043, 12045, 12053 and 12058 mantles. With detachable 4-foot, 2-wire
cord and locking connector. 115v units are CSA certified. Must be operated through
a temperature controller.

12047

For Flask Size, mL


1000
2000
3000
5000
12000
22000
50000
72000

Watts/Volts
140w115v
200w115v
200w115v
300w115v
590w115v
650w115v
1000w115v
1000w230v

Order Code
12047-19
12047-21
12047-23
12047-25
12047-27
12047-29
12047-31
12047-33

Each
268.00
277.00
306.00
387.00
646.00
697.00
1082.00
1248.00

All 115v units are also available in 230v versions.

12050

12050 MANTLE Aluminum Housing, Low Profile


For use with ACE 6530 and 6474 reaction assemblies. CSA certified. Easily fits into ACE
4-post reactor stands. Temperature range is Ambient +10C to 450C. Must be operated
through a temperature controller. With detachable 4-foot cord and locking connector.
For 6530 Assembly
(Without Bottom Opening)
For Flask
Order
Size, Liter Watts/Volts
Code
Each
50
1000w115v 12050-34
909.03
72
1300w230v 12050-36 1530.57
100
1600w230v 12050-38 2044.00

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

For 6474 Assemby


(With Bottom Opening)
For Flask
Order
Size, Liter Watts/Volts
Code
Each
50
1000w115v 12050-41
813.52
72
1300w230v 12050-43 1121.28
100
1600w230v 12050-45 1586.14

Subject to Ace Discount (Page 4)

Net

Components / Heating Mantles

169

12053 MANTLE Aluminum Housing, Standard Height, Solid Bottom,


for Spherical Flasks

Solid, aluminum housed, heating mantles can be used on benches for smaller sizes
and can be used on floor or reactor stands for large flasks. Temperature range ambient
+10C to 450C. Must be operated through a temperature controller. Smaller sizes have
4-foot detachable cord with interlocking connector. Larger sizes, codes -31 through -37,
are supplied with a terminal box for hard wiring. CSA approved.
For Flask Maximum Flask
I.D. x Depth,
Size, mL
Dia., in./mm
inches/mm
1000
5.1/130
5.1/130 x 2.5/65
2000
6.6/170
6.6/170 x 3.3/86
3000
7.2/183
7.2/183 x 3.6/91.5
5000
8.6/220
8.6/220 x 4.3/109.5
6000
9.25/235
9.25/235 x 4.7/120.6
12000
11.5/293
11.5/293 x 5.7/146.6
10000
Schott
3.9/100 x 5.7/146.6
22000
13.6/347
13.6/347 x 6.8/173
20000
Schott
13.7/350 x 6.8/173
50000
17.9/456
17.9/457x 8.9/228
50000
Schott
18.3/465 x 8.9/228
72000
20.5/522
20.5/522 x 10.1/258.9
100000
Schott
200000
Schott

Watts/Volts
380w115v
500w115v
500w115v
600w115v
700w115v
(2) 650w115v
(2) 650w115v
(2) 770w115v
(2) 770w115v
(3) 1000w115v
(3) 1000w230v
(2) 2000w230v
(2) 2000w230v
(2) 2000w230v

Order
Code
12053-19
12053-21
12053-23
12053-25
12053-26
12053-27
12053-28
12053-29
12053-30
12053-31
12053-32
12053-33
12053-35
12053-37

12053

Each
271.00
282.00
336.00
417.00
906.51
779.00
786.76
898.00
904.49
1424.00
1635.80
1623.00
3226.29
3903.47

12053 MANTLE Aluminum Housing, Low Form, Solid Bottom,


for Cylindrical Flasks

12053

Solid, aluminum housed, heating mantles can be used on benches for smaller sizes and
can be used on floor or reactor stands for large flasks. Temperature range ambient +10C
to 450C. Must be operated through a temperature controller. Smaller sizes have 4-foot
detachable cord with interlocking connector. Larger size, code -45, is supplied with a
terminal box for hard wiring. CSA approved.
For Flask Maximum Flask
Size, mL
Dia., in./mm
6000
8.7/222.2
10000
8.7/222.2
15000
9.9/251
30000
12.5/317.5
50000
12.5/317.5

I.D. x Depth,
inches/mm
7.73/194 x 2.22/56.4
7.73/194 x 2.22/56.4
9.9/251.5 x 5/127
10.9/276.9 x 3.12/79.3
10.9/276.9 x 3.12/79.3

Watts/Volts
180w115v
180w115v
250w115v
370w115v
370w115v

Order
Code
12053-40
12053-40
12053-43
12053-45
12053-45

Each
585.95
585.95
1047.62
744.73
744.73

12053 MANTLE Aluminum Housing, Standard Height, Bottom Opening


Aluminum housed, heating mantles with a bottom opening to accommodate flasks with
bottom valves. Can be used on benches for smaller sizes and can be used on floor or
reactor stands for large flasks. Fits cylindrical and spherical flasks with bottom valves.
Temperature range ambient +10C to 450C. Must be operated through a temperature
controller. Smaller sizes have 4-foot detachable cord with interlocking connector. Larger
sizes are supplied with a terminal box for hard wiring. CSA approved.
For Flask
Size, mL
600
6000
10000
15000
30000
100000
200000
200000

Maximum Flask
I.D. x Depth,
Dia., in./mm
inches/mm
7.63/193.8
7.63/193.8 x 2.22/56.4
9.25/235
9.25/235 x 5/127
7.63/193.8
7.63/193.8 x 2.2256.4
9.06/230
9.06/230 x 2.75/69.9
10.9/276.9
10.9/276.9 x 3.12/79.2
14.38/365.3 14.38/365.3 x 4.12/104.7
18.5/470
18.5/470 x 9.25/235
29.53/750
29.53/750 x 15/381.1

For Flask
Type
Watts/Volts
Cylindrical
180w115v
Spherical
700w115v
Cylindrical
180w115v
Cylindrical
250w115v
Cylindrical
370w115v
Cylindrical
625w115v
Cylindrical
775w115v
Cyl./Schott (4) 2000w230v

12053

Order
Code
Each
12053-61
717.37
12053-162 944.83
12053-50
676.91
12053-64
874.66
12053-54
697.89
12053-70
936.71
12053-74 1462.92
12053-78 4360.53

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170

Components / Heating Mantles

12058

12058 MANTLE Aluminum Housing, Cylindrical Flasks


Resin and reaction flask mantle mainly used for ACE pressure reactors, but fit many other
cylindrical reaction flasks such as 6476, 6511-06 series, 6521, Aluminum housed with
solid bottom. The code -03 is for a flask with a flat bottom with rounded corners such
as the 6511-24 series. CSA approved. 4-foot detachable cord with locking connector.
Temperature range is ambient +10C to 450C. Must be operated through a temperature
controller.
For Flask
Size, mL
500 (tall)
500 (short)
3000
5000

12058

Max. Flask
Dia., in./mm
2.75/69.9
4.38/111.3
6.38/162
6.38/162

Watts/Volts
280w115v
250w115v
600w115v
1000w115v

Order
Code
12058-03
12058-07
12058-30
12058-33

Each
622.85
825.72
652.46
864.71

12058 MANTLES Aluminum Housing


Resin and reaction flask mantle. Bench top size with small footprint, aluminum housing.
For use with ONLY the following ACE flasks: 652112, 652114, 647215, 647220
and 647225. CSA approved, 115 volt. Complete with 4-foot detachable cord with locking
connector. Must be operated through a temperature controller.
For Flask Maximum Flask
Size, mL
Dia., in./mm
500
3.75/95.2
1000
4.25/107.9
2000
5.5/139.7
3000
5.5/139.7
4000
5.5/139.7

12058

I.D. x Depth,
inches/mm
2.76/70 x 6.25/158.8
4.5/114.3 x 3.0/76.2
6.4/162.6 x 6.0/152.4
6.4/162.6 x 10.9/276.9

I.D. x Depth,
inches/mm
3.75/95.2 x 4.5/114.3
4.25/107.9 x 5.25/133.3
5.5/139.7 x 6.0/152.3
5.5/139.7 x 9.0/228.6
5.5/139.7 x 11.0/279.4

Watts/Volts
270w-115v
335w-115v
470w-115v
550w-115v
750w-115v

Order
Code
12058-08
12058-12
12058-16
12058-22
12058-28

Each
312.00
325.00
335.00
376.00
410.00

12058 MANTLES Aluminum Housing, Cylindrical Flasks, Bottom Opening


Resin and reaction flask mantle mainly used for ACE pressure reactors with a bottom
valve or outlet, but fit many other cylindrical reaction flasks such as 6518, 6522, 6521,
6300. The code -44 is for a flask with a flat bottom with rounded corners such as 6437
series. Aluminum housed with bottom opening. CSA approved. 4-foot detachable cord
with locking connector. Temperature range is ambient +10C to 450C. Must be operated
through a temperature controller.
For Flask
Size, mL
500 (tall)
500 (short)
1000
2000
3000
5000

Max. Flask
Dia., in./mm
2.75/69.9
4.38/111.3
4.25/107.9
5.5/139.7
6.38/162.1
6.38/162.1

I.D. x Depth,
inches/mm
2.8/70 x 6.25/158.8
4.4/111.8 x 3.0/76.2
4.28/109 x 5.25/133.4
5.7/144.8 x 6.0/152.4
6.4/162.6 x 6.0/152.4
6.4/162.6 x 10.8/276.4

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Watts/Volts
280w115v
250w115v
335w115v
470w115v
600w115v
1000w115v

Order
Code
12058-44
12058-47
12058-49
12058-51
12058-53
12058-55

Each
676.56
594.66
603.06
561.86
750.88
884.42

Subject to Ace Discount (Page 4)

Net

Components / Heating Mantles


12075 MANTLE Aluminum Housing, For Cylindrical Flasks
Resin and reaction flask mantle. Bench top size with small footprint. Aluminum housing
for 6423, 6436, 6526, 6476, 6477, 9526, 6516-01, 6521-10,-12,-14, 6511-06,-42,-24,-53
ACE flasks. CSA approved, 115 volt complete with 4-foot detachable cord with locking
connector. Temperature range is Ambient +10C to 450C. Must be operated through a
temperature controller. 230V versions available.
For Flask
Size, mL
1000
2000
3000

Maximum Flask
I.D. x Depth,
Order
Dia., in./mm
inches/mm
Watts/Volts
Code
4.5/114.3
4.5/114.3 x 4.5/114.3 270w-115v 12075-08
4.5/114.3
4.5/114.3 x 7.5/190.5 400w-115v 12075-10
4.5/114.3
4.5/114.3 x 11/279.4 600w-115v 12075-12

171

12075

Each
334.00
348.00
386.00

6494 FLASK HEATER Fabric/Cloth


Specially designed glass/fiber cloth mantle with bottom opening and zipper for use
with 6491, 6492, 6518, and 6522 flasks to allow valve to protrude below heater. Upper
temperature limit, 450C. Must be operated through a temperature controller. CSA approved. Complete with 4-foot cord and locking connector.
For Flask
Size, mL
1000
1500
2000
3000

I.D. x Depth,
inches/mm
4.625/117.4 x 5.625/142.8
4.625/117.4 x 6.625/168.2
4.625/117.4 x 8.875/225.4
4.625/117.4 x 10/254

Watts/Volts
300w-115v
380w-115v
450w-115v
600w-115v

Order
Code
6494-10
6494-15
6494-20
6494-25

6494
Each
412.26
435.16
461.47
491.58

12032 BLANKETS Flask Insulating


Insulating blankets for jacketed reactor flasks. Over 1-inch thick blanket has a grey PTFE
material outside for chemical resistance and 1-inch (25.4mm) fiberglass insulator internal
for excellent insulating of jacketed reactor flasks. Blanket fits in between the Inlet/Outlet
ports on the flask. Each has an overlapping front flap with grommets and lace closure for
easy off/on. Non-electric nor heat. There are six different sizes to fit from 1L up to 100L
jacketed flasks.
Height,
mm
292
457
310
310
560
510

Width,
mm
270
315
350
562
350
510

Folded
I.D., mm
270
315
350
460
350
510

For Flask Size, L


10
20
30
50 (Low Profile)
50
100

Order Code
12032-03
12032-05
12032-07
12032-09
12032-11
12032-13

Each
457.19
822.42
587.29
625.96
1078.44
1703.35

12032

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172

Components / Heating Mantles


12085 VOLTAGE CONTROLLER Mantle Minder II

12085

For controlling all Glas-Col mantles. Time proportioning, 1/16 DIN, automatic control for
use with mantles, tapes, cords, small ovens, and other resistive heating loads up to 1800
watts at 120 volts. Features a detachable iron-constantan J thermocouple with 6-inch
stainless steel probe, lighted ON/OFF power switch with auxiliary indication, load and
thermocouple receptacles located on front panel for easy accessibility, and set point dial
calibrated in C in 20 degree increments. Fused to protect small loads. Operates on 120
VAC, 50/60 Hz input. Range 0750C. Ambient temperature range 30130F. Accuracy
1.5% of full scale. Supplied with three-wire load receptacle, three-wire line cord with
molded plug. Power consumption four watts plus load. Thermocouple included. Measures
8 wide x 6 deep x 3-3/8 (inches) high.
Order Code
12085-20

Each
569.00

12087 VOLTAGE CONTROLLER 0120v at 10 Amps, Solid State


Variable control from zero output to 95% line voltage. A voltage-limit, rear-mounted centeroff switch is used to select a 40v or 120v maximum output with the control knob full on.

12087

With 010 ammeter. 5% accuracy. (Since this is a solid state transformerless line voltage
controller, it is NOT recommended for heaters rated less than 120 volts.) Warning glow
light, mounted next to correcting switch, will illuminate when dangerous reversed wiring
condition exists. Simply flip the switch to extinguish the light and correct the condition.
Easy-access 10 amp fuse type 3 AG (rear mounted). Line voltage pilot light. Standard
1.8 meter heavy duty neoprene three-wire power cord (grounded to case) with NEMA
plug. Dimensions: 17.8cm (7 inches) x 10.2cm (4 inches) x 8.9cm (3-1/2 inches). Weight:
794 grams. Input 120 volts, 60 cycles.
Order Code
12087-10

Each
621.30

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Subject to Ace Discount (Page 4)

Net

IN C O R

TH

A N N I V E R S A R Y

TED
RA

ACE G

S
AS

Components / Heating Mantles

173

Contact Ace Glass at

800-223-4524
and ask for a copy of our

IN U S A
E L A N D,

1936 2011

Laboratory Glassware
& Equipment Catalog

75th Anniversary Laboratory


Glassware and Equipment
Catalog
You can also view or download a
digital copy at our website

www.aceglass.com

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174

Components / Heating Mantles

Mantle Guide
Heating Mantles for 6521 and 6522 Cylindrical Reaction Flasks
The corresponding 12053 aluminum mantles have a 2-inch bottom opening to match the bottom outlets on the 6522 series flasks.
The 12053 mantles for the 6521 flask have a solid bottom.

Aluminum Hard Mantles


For Flask
Size, Liters
1
1

For
Flask No.
6521-10
6522-11

Watts/Volts

Order Code

2
2

6521-12
6522-13

3
3

6521-14
6522-15

6
6

6521-16
6522-17

180w-115v
180w-115v

12053-40
12053-61

10
10

6521-20
6522-21

180w-115v
180w-115v

15
15

6521-25
6522-26

30
30

Fiber/Soft Girdle Mantles


Order Code
6478-10
6494-10

Each
322.54
412.26

450w-115v
450w-115v

6478-20
6494-20

374.61
461.47

600w-115v
600w-115v

6478-25
6494-25

381.58
491.58

585.95
717.37

495w-115v
495w-115v

12041-10
12041-10

860.65
860.65

12053-40
12053-50

585.95
676.91

495w-115v
495w-115v

12041-10 (2)
12041-10 (2)

860.65
860.65

250w-115v
250w-115v

12053-43
12053-64

1047.62
874.66

2-880w-115v
2-880w-115v

12041-12
12041-12

777.15
777.15

6521-30
6522-31

370w-115v
370w-115v

12053-45
12053-54

744.73
697.89

2-825w-115v
2-825w-115v

12041-32
12041-32

979.40
979.40

50
50

6521-35
6522-36

370w-115v
370w-115v

12053-45
12053-54

744.73
697.89

3-1100w-115v
3-1100w-115v

12041-37
12041-37

1617.65
1617.65

100
100

6521-40
6522-41

625w-115v
625w-115v

12053-56
12053-70

Call
936.71

4-1200w-115v
4-1200w-115v

12041-48
12041-48

2222.22
2222.22

200
200

6521-44
6522-45

775w-115v
775w-115v

12053-58
12053-74

Call
1462.92

4-1100w-115v
4-1100w-115v

12041-52
12041-52

2228.41
2228.41

Each

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Watts/Volts
300w-115v
300w-115v

Subject to Ace Discount (Page 4)

Net

TH

A N N I V E R S A R Y

TED
RA

ACE G

S
A

C
N
O
I
R
S

175

1936 2011

VI

USA

NE

N
,
LAND

Stirrers, Trubore

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Stirrers, Trubore

Glass pressure bearings (8044) are for use with 8074 plain stainless
steel or 8075 polished glass shafts.
8050 Mechanical Seal Bearing may be used with polished or
precision-ground glass and plain stainless steel shafts (10, 19
& 28mm). Not recommended for use with PTFE-covered shafts.
13443 PTFE Collet Bearing may be used with any type shaft
(6, 8 & 10mm).
13445 Debris-free PTFE Bearing should be used with polished
glass shafts or plain, stainless steel shafts. They are not
recommended for precision-ground glass shafts or PTFE-covered,
stainless steel shafts (6, 10 & 19mm).

A N N I V E R S A R Y

IN

1936 2011

Trubore bearings with a PTFE Inner component are for use with
polished glass shafts and plain, stainless steel shafts. They are
not recommended for precision-ground glass shafts or PTFEcovered, stainless steel shafts.

TH

ACE

Trubore, glass bearings are for use with precision-ground glass


shafts or PTFE-covered, stainless steel (8071) shafts. They are
not recommended for use with polished glass or plain, stainless
steel shafts.

Glass, Polished: use only in


8044 glass, pressure bearings or
Trubore bearings with a PTFE
inner component (8066) or our
13443 PTFE collet type, 8050
PTFE mechanical seal and 13445
PTFE debris-free bearings.

SS INN OV

ON

Bearings:

LA

I
AT

General Stirring Information

176

LAND
Glass, Precision-Ground: use

only Trubore glass bearings


such as our 8059, 8060, 8061,
8065, etc. series, or our 13443 PTFE collet seal type and 8050
PTFE mechanical seal bearings.
Stainless Steel, Plain: use only in 8044 glass, pressure bearings
or Trubore bearings with a PTFE inner component (8066) or our
13443 PTFE collet type, 8050 PTFE mechanical seal and 13445
debris-free bearings.
Stainless Steel, PTFE-Covered: use with Trubore glass bearings
such as our 8059, 8060, 8061, 8065, etc. series, or our 13443
PTFE collet type bearings. Not recommended for use with our
PTFE debris-free 13445 bearing.

Stirring Shafts:

Trubore Stirring Equipment Precision Fit and Performance

Bearings and shafts guaranteed 1mm absolute with unlubricated introduced into a solvent system
surfaces at speeds less than 100 reaction, they will not react with
interchangeable
Trubore stirrers, pioneered and
developed by Ace, are the most
widely used precision glass
stirrers in research today.
If both shaft and bearing of a
given size are manufactured by
Ace, we guarantee them to be
interchangeable.

Precision fit and performance


Every shaft and bearing is
individually inspected to insure
clearance fit of less than .025 mm
(0.001-inch).
ACE bearings are smooth
and transparent. This feature
automatically reduces leak
path for a given fit clearance
and surface roughness; it also
prolongs bearing life.
Special plateau grinding
is employed on shafts. This
provides maximum smoothness
consistent with optimum
retention of lubricant. In terms
of performance, this texture
means a low leak rate, which
permits attainment of at least

rpm. It also means that plastic


shafts, including Fluorocarbon
coated glass shafts, may be used
with bearings a practice not
feasible with ground bearings.

Operation
If the components have been
p ro p e r l y c l e a n e d p r i o r t o
operatition, a Trubore stirring
unit can be run unlubricated for a
limited time at a maximum speed
of 500 rpm.
For continuous operation, or
operation at speeds greater than
500 rpm, proper lubrication is
required. We recommend ACE
8117 StirLube be used as a
proper all-purpose lubricant up
to 2000 rpm (water cooled) or
1500 rpm (non-cooled).
For high-speed stirring over
2000 rpm, we recommend
a thin base of 8229 grease
with application of 8119 HiLube heavy-duty liquid stirrer
lubricant. Both materials are also
chemically inert. If accidentally

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your product, but will be removed


with the solvent. Under no
circum
stances should glycerin
be used; it acts as a grinding
medium rather than a lubricant.
Note that only a small lubricant
well is provided at the top of
some ACE bearings; this is
because only a slight amount of
Stir-Lube is needed for many
hours of stirring.

Care and cleaning


Because of the very close fit
between shaft and bearing, a
slight amount of dust or grit
will quickly scratch the smooth
surface of the bearing. To prevent
this, both shaft and bearing
should be washed with a good
detergent and dried with acetone
instead of with a wiping cloth
prior to use.
ACE lubricants may be
completely removed with
acetone or most other ketones.

Subject to Ace Discount (Page 4)

Net

Stirrers, Trubore

177

Matching ACE Stir Bearings to the Appropriate Shafts


Bearing Type

Size

ACE Stir Bearing Codes

Use with ACE Code Stirring Shafts


Listed Below

Trubore, Glass

5mm

952404, 952708

953404, 953506, 954104, 954115

Trubore, Glass

6mm

952406, 952408, 952712, 952714, 9529

953406

Vacuum

9mm

8098, 8099, 8133, 9528

8134, 9530

Trubore, Glass

10mm

8036, 8038, 8039, 8040, 8042, 8043, 8047,


8051, 8053, 8055

8068, 8070, 8071, 8073, 9532, 9533

Trubore, Glass

10mm

8041

Complete Assemblies

Trubore, Glass

19mm

8059, 8060, 8061, 8065

8076*, 8077, 8078, 8079

Glass, Pressure

10mm

8044

8074, 8075

Trubore , PTFE/Glass

10mm

8066 (Plain), 8066 (Debris Trap)

8074, 8075

Trubore, PTFE/Glass

19mm

8067 (Trubore), 8067 (Debris Trap)

8076

Trubore , PTFE/Glass

28mm

8067 (Trubore ), 8067 (Debris Trap)

8080

Mechanical Seal/PTFE

10mm

8050

8068, 8073, 8074, 8075, 9532, 9533

Mechanical Seal/PTFE

19mm

8050

8076, 8077, 8078

Mechanical Seal/PTFE

28mm

8050

8080

Collet Type/PTFE

6mm

13443-06, 13443-08

9534-06, 9534-40

Collet Type/PTFE

8mm

13443-10

9534-06, 9534-40

Collet Type/PTFE

10mm

13443-12

8068, 8070, 8071, 8073, 8074, 8075,


9532, 9533

PTFE

6mm

13445-06, 13445-09

9534-40

PTFE

10mm

13445-30, 13445-32, 13445-34, 13445-36

8074, 8075

PTFE

19mm

13445-46, -44

8076

*Polished shaft not recommened for 8076.

Custom Pilot Plant Reactor Designs


Selecting components and designing a Pilot Plant System requires you to
consider specific site and application aspects, such as:
Space limitations: what depth, width and height
are available for the support stand, stirrer motor,
condenser, etc.?

How much distance is needed below the bottom of


the reactor outlet?

Do you want a domed or flat head reactor?

What type of stirring motor (air, electronic, for hazardous or non-hazardous location)?

What will be the operating temperature?

What type of stirrer shaft (glass or PTFE)?

Vacuum or pressure?

Heat exchange coil needed? PTFE-covered copper or


other type metal?

What type bottom outlet (standard, threraded, stopcock, sink type valve, etc.?
Do you want temperature monitoring/control?

What accessories are needed (condensers, take-offs,


adapters, spargers, gas inlet/outlet, etc.?

Custom Assemblies
In addition to our standard 10 through 200 L Cylindrical and Spherical Assemblies, ACE can
assist you in designing a specific component reactor. Many of the dimensions and items listed
can be modified to accommodate your needs.
Consult ACE by calling our Technical Design and Support Staff toll-free at 18002234524 or

visiting us on the web at www.aceglass.com.

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178

Stirrers, Trubore

ACE Stir Shaft Quick Reference Chart


Size

Recommended Use

Ace Code O.D., mm L, mm


5
318
9534-04
318
9534-06
6
9534-40
318
9535-06
318
9541-04
5
318
9541-15
318
8134-15
380
8134-25
9
610
9530
416
8068-02
440
8068-03
580
8068-04
690
8068-06
740
8068-08
440
8068-17
580
8068-18
440
8068-25
440
8068-27
580
8068-30
440
8068-31
690
8068-32
580
8070-05
440
8070-10
690
8071-05
460
8071-07
640
8071-10
690

Type

8073

10

410

8074-02
8074-04
8074-07
8075-12
8075-14
8075-15
8075-21
8075-23
8075-24
8075-32
8075-34
8075-36

420
450
580
440
580
690
440
580
690
440
580
690

9523

445

9533

475

8076-05
8076-07
8076-10
8076-40
8076-42
8076-43
8076-44
8076-45
8076-46
8076-48
8077-23
8077-25
8077-27
8078-05
8078-10
8079-03
8079-05
8079-10
8080-12
8080-14
8080-18
8080-22
8080-24
8080-25
8080-30

700
900
1200
900
800
800
1200
1140
1400
1400
700
900
1200
900
1200
700
900
1200
1010
1140
1320
1470
1400
2030
1600

Button Bottom
Knob Bottom
With Paddles

Material
Solid Ground Borosilicate Glass
Solid Polished Borosilicate Glass
Hollow Borosilicate Glass
Solid Ground Borosilicate Glass
PTFE Coated Stainless Steel
Solid Polished Borosilicate Glass

28

Chuck

9524-04, 9527-08

8124, 8126

Multi-Blade

8133, 9528, 8098, 8099

9541-06
9541-07
Attached
8083, 8084, 8085, 8086
9530
8083, 8082, 8085,
8086,8087,8096

Solid Ground Borosilicate Glass

Double Multi-Blade

Agitators
9542

Button Bottom

8036, 8038, 8039, 8040, 8041,


8042, 8043, 8047, 8051, 8053,
8055, 13443,8050

Attached
8083, 8082, 8085,
8086,8087,8096

Button Bottom

Hollow Ground Borosilicate Glass

Bead Bottom

Solid Ground Borosilicate Glass

Button Bottom

PTFE Coated Glass

Bottom Drilled Hole

PTFE Coated Stainless Steel

Crescent Shaft

Solid Ground Borosilicate Glass

8036, 8038, 8039, 8040, 8041,


8042, 8043, 8047, 8051, 8053,
8055, 8066, 8133, 13443, 8050

Attached

Remove Button Bottom

Stainless Steel

8044, 8055, 8066, 13443, 13445

8082,8083,8085,8086,
8096, 8094, 8095

8089, 8090,8088
8083, 8082,
8085,8086,8087,8096

8036, 8038, 8039, 8040, 8041,


8042, 8043, 8047, 8051, 8053,
8055, 8066, 8133,13443

8089, 8090, 8088

8083, 8082,
8085,8086,8087,8096

Button Bottom
8044, 8066
Plain Shaft

Solid Polished Borosilicate Glass

Bead Bottom
Hollow Polished Borosilicate Glass
Complete W/Vanes

19

Bearing
9524-04, 9527-08, 9524-06,-08,
9529, 9527-12, 9527-14
8066-120

Solid Ground Borosilicate Glass

8124, 8125,
8126

8094, 8095

8044, 8066,8050,13443, 13445

8088, 8089, 8090

8036, 8038, 8039, 8040, 8041,


8042, 8043, 8047, 8051, 8053,
8055, 8066, 8133,13443,8050
8043, 8047, 8050, 8051, 8036,
8038, 8039, 8040, 8041, 8042,
8053, 8055, 13443, 13000

Attached

Button Bottom

Hollow Polished Borosilicate Glass

8085

Bottom Drilled Hole


Bottom Knob
Bottom Drilled Hole
Bottom Knob
Bottom Drilled Hole
Bottom Knob
Bottom Drilled Hole

Solid Polished Borosilicate Glass


Hollow Polished Borosilicate Glass
Solid Polished Borosilicate Glass
Hollow Polished Borosilicate Glass
Solid Polished Borosilicate Glass
Hollow Polished Borosilicate Glass
Solid Polished Borosilicate Glass

Button Bottom

Solid Ground Borosilicate Glass

8059, 8060, 8061,8065,


8059, 13445

8085

Bottom Knob

Hollow Ground Borosilicate Glass

8059, 8060, 8061, 8050,


8065,13445

8091, 8100, 8092, 8093

Bottom Drilled Hole

PTFE Coated Stainless Steel

8059, 8060, 8061, 8065

8091, 8092, 8093,8100

Bottom Drilled Holes

Solid Polished Borosilicate Glass

8067, 13445, 8050


8091, 8100,8092,8093

8067, 8050

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6472-15,
6472-155,
6472-156

8091, 8093, 8101

Subject to Ace Discount (Page 4)

Net

Stirrers, Trubore

179

5 & 6mm Shafts, Bearings & Agitators


9524 BEARINGTrubore, 5 & 6mm
Trubore bearing with standard taper joint for use with our 9534, 9535 and 9541 precision
ground stir shafts. Lubricant well at top will accept enough 8117 Stir-Lube to provide
hours of operation at up to 1000 rpm. Match bearing I.D. with stir shaft O.D.
Joint
14/20
14/20
19/22

I.D., mm
5
6
6

Order Code
9524-04
9524-06
9524-08

9524

Each
46.94
48.34
50.33

9527 BEARINGTrubore, Water Cooled, 5 & 6mm


Jacketed, Trubore bearing with standard taper joint for use with our 9534, 9535 and
9541 precision ground stir shafts. Hose connections fit 5/16-inch or 3/8-inch ID tubing.
Match bearing ID of 5mm or 6mm to stir shaft O.D.
Joint
14/20
14/20
19/22

I.D., mm
5
6
6

Order Code
9527-08
9527-12
9527-14

9527

Each
87.55
90.02
92.84

9529 BEARINGTrubore, Economy, 6mm


Trubore bearing, heavy duty, standard taper joint, self-aligning. Unique design is forgiving
of slight misalignment of stir motor and shaft. Recommended for use with our 9534 6mm
precision ground stir shaft. Glass member has 19/22 inner joint.

7855-716

15.66

AceThred Adapter
Complete

Order
Code
5030-04
9529-10

Each
27.92
89.94

ON

FE

E-SA

OR

Each
33.13
28.89

AC

Inner Bearing, only


Bushing, w/ORing
Size 110 FETFE
ORing, Pk. 12

Order
Code
9529-04
9529-07

9529

N ECT

9534 STIRRING SHAFT 5 & 6mm, Glass


Button type solid glass stirring shafts, 5mm & 6mm O.D. Precision ground shafts, codes
-04 & -06, should be used in matching glass Trubore 9524 and 9527 bearings. Polished
shaft, code -40, should be used only in our 8066-120, 6mm PTFE inner bearing. All accept
our 9542 blades. Join to stirrer motor using 8124 series chucks. 318mm overall length
ideal for use in 250ml and smaller flasks.
Rod Size O.D., mm
5
6
6

Glass Type
Ground
Ground
Polished

Order Code
9534-04
9534-06
9534-40

9534

Each
35.53
37.18
42.71

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180

Stirrers

5 & 6mm Shafts, Bearings & Agitators


13443 STIRRER BEARING PTFE, 6mm

13443

Inert PTFE stirrer bearing. Features a totally enclosed bearing body for non-shedding,
anti-whip, chemically resistant design. The bearing can also be used in slight vacuum or
slight pressure applications. The design has a composite PTFE/PEEK main internal seal
and a specially fabricated glass ball-bearing for rigidity and smoothness during lengthy
operation. Maximum recommended speeds up to 500 rpm continuous operation. Ideal for
glass, metal or PTFE stir shafts. Bottom is a molded, inner standard taper joint. Average
length is 96mm and 45mm OD at bearing center.
Joint
19/22
24/40

Order Code
13443-06
13443-08

Each
349.97
349.97

13445 BEARING Debris Free, PTFE, 6 mm


Vacuum tight (~5 Torr), flake free, chemically resistant stirrer bearing makes a mechanical
seal against a polished glass shaft. Debris trap section consists of a PTFE sleeve for a
wide range of joint and shaft diameter sizes. For use with 6 mm polished glass or stainless
steel shafts, NOT recommended for PTFE shafts. Bearing consists of a PTFE standard
taper body with added PEEK for better stability, glass filled polypropylene screw cap,
PEEK compression spring, PTFE/PEEK sleeve and a glass filled polypropylene loosening
nut. For use up to 500 rpm.
Joint
13445

19/22
24/40

Order Code

Each

13445-06
13445-09

171.73
173.37

Replacement Seals & Springs:


PTFE/PEEK sleeve seal
PEEK compression spring

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Order Code

Each

13445-302
13445-304

32.16
35.26

Subject to Ace Discount (Page 4)

Net

Stirrers

181

5 & 6mm Shafts, Bearings & Agitators


9535 STIRRING SHAFT Hollow Glass, 5mm
Precision ground, hollow, 5mm glass stirring shaft. Button type shaft accepts 9542 blades
and can be used in matching 9524 and 9527 bearings. Holes are provided in the side of
the shaft for material introduction and at the bottom for emission into the flask contents.
Join to stirrer motor using 8124 series chucks.
Shaft Size O.D., mm
5

Order Code
9535-06

9535

Each
49.32

9541 STIRRING SHAFT with PTFE Agitator, 5mm


Stirring shaft agitator combination available in either a solid, precision ground glass
shaft or all PTFE knob type shaft with a PTFE snap-fit agitator designed to fit through
14/20 and 18/11 joints. Designed for use with our 5mm I.D. 9524 or 9527 bearings
and flasks of 50ml and smaller.

Type Rod
Glass
PTFE

Rod
Order
Code
Each
9541-04
32.03
9541-15
37.90

Agitator
Order
Code
Each
9541-06
71.08
9541-07
71.08

Complete
Order
Code
Each
9541-10
103.11
9541-40
108.98

9541

9542 STIRRING BLADE 5 & 6mm


PTFE stirring blades for use with our button type 9524 and 9527 stirring shafts. Blades
are 41mm wide x 12mm high and are designed for use in flasks 250ml and less. Match
blade to shaft O.D.
Rod Size O.D., mm
5
6

Order Code
9542-10
9542-20

Each
9.45
9.45

9542

8124 CHUCK Flex-Grip, 5 & 6mm


Nylon chuck for use with ACE stirring shafts or other shafts of the same dimensions. Chuck
has flexible insert which allows for misalignment of shaft without danger of breakage.
For Stirring
Shaft Size, mm
6
5
6

For Motor
Shaft, mm (In.)
6.4 (1/4)
8 (5/16)
8 (5/16)

Insert Only Size Qty.


6 mm
6
5 mm
6

Order Code
8124-04
8124-05
8124-07

Order Code
8124-24
8124-26

Each
39.72
37.74
37.51

8124

Per Package
17.04
17.04

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182

Stirrers

9mm Shafts, Bearings & Agitators


8133 BEARING High Speed Vacuum,9mm
Used with 8111 aluminum packing box. For shaft speeds of 1000 r.p.m. and higher,
and vacuum operation down to 0.5mm Hg. The seal is made entirely by the packing
box. Only infrequent lubrication is required using 8122 packing and 8117 Stir-Lube. We
recommend that you use 8113 vacuum adapter to avoid contaminating the flask contents
with lubricant. For use with 9mm O.D. shafts.

8133-10,
-15

8133-40

Bottom Joint
24/40
29/42
35/25

Order Code
8133-10
8133-15
8133-40

Each
54.03
61.76
52.01

8098 STIRRER BEARING Vacuum, 9mm


A rugged, compact, inexpensive stirrer. The upper member turns with stirring shaft,
bottom member remains stationary. Upper member supplied with vinyl connector. Use
with ACE 8134 size 9mm stirring shafts. Assembly may also be used to make your own
rotary evaporator.

8098-12

Lower Member
Order
Joint
Code
Each
24/40
8098-04
60.19

Upper Member
Order
Joint
Code
Each
18/10
8098-01
25.02

Vinyl Connector only, for all sizes

Order Code
8098-45

Per Dozen
37.77

8134 STIRRING SHAFTS 9mm


Unground, 9mm OD shaft for use in liquid seal bearings and our debris free 8098 and
8099 stirrer assemblies. Code -25 is a button type shaft which accepts our 8083, 8084,
8085 and 8086 blades. Shaft length accommodates flasks from 500ml to 5000ml.
Style
C
E

Qty.
12

Complete
Order
Code
Each
8098-12
85.21

Length, mm
380
610

Order Code
8134-15
8134-25

Each
33.18
18.85

8134

9528 VACUUM STIRRER BEARING ASSEMBLY 9mm


9528

Rotating ball joint seal gives vacuum-tight connection good into the micron range.
Ultimate vacuum is determined primarily by the tightness of the vinyl tubing connector
which fastens the unground shaft to the ball member. Operate below 500 rpm. Use with
unground stirring shafts (8134,9530). Lubricate the 18/11 rotating ball joint with our
8117 Stir-Lube. Bottom joint is 19/22. Upper member is supplied with a vinyl connector.

Upper Member
Lower Member
Complete

Order
Code
9528-02
9528-04
9528-10

Each
32.30
66.80
99.10

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Vinyl Conn., only

Qty.

Order
Code

Per
Dozen

12

8098-45

37.77

Subject to Ace Discount (Page 4)

Net

Stirrers

183

9mm Shafts, Bearings & Agitators


8099 STIRRER BEARING Vacuum, Threaded, 9mm

8099

Complete
Order
Code
Each
8099-40 119.90

E-SA

ON

OR

Nylon Bushing
Order
Code
Each
8099-38 19.97

FE

Upper Member
Order
Joint Code
Each
18/10 8099-03 40.77

Lower Member
Order
Joint Code
Each
24/40 8098-04 60.19

AC

Modified version of 8098 in that upper member is internally threaded on the top. #7
AceThred nylon bushing and FETFE oring form a compression seal on stirring shaft in
place of the conventional tubing arrangement. Easier to adjust shaft, suitable for vacuum
work. For use with 8134 stirring shafts.

N ECT

9530 STIRRING SHAFTS 9mm


Unground, 9mm O.D. stirring shaft design for use with our 9528 vacuum and debris free
stirrer assembly. 380mm straight section, 416mm overall length. Use our 9530-08 blade.
Rod
Blade

Order Code
9530-04
9530-08

9530

Each
21.22
10.73

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184

Stirrers, Trubore

10mm Shafts, Bearings & Agitators


8036 BEARINGTrubore, 10mm
Interchangeable bearing designed to be used with our precision ground stirring shafts
(8068, 8070, 8071, 8073, 9532, 9533). Recommended top stirring speed with our 8117
Stir-Lube is 1500 rpm.

8036

Order Code
8036-10

Each
39.94

8038 BEARINGTrubore, 10mm


Interchangeable ground joint bearing for use with our precision ground stirring shafts
(8068, 8070, 8071, 8073, 9532, 9533). Recommended top stirring speed with our 8117
Stir-Lube is 1500 rpm.

8038-10

8038-40

Joint
19/22
19/38
24/40
29/42
34/45
45/50

Order Code
8038-04
8038-05
8038-10
8038-20
8038-30
8038-32

Each
73.43
71.27
74.38
74.96
75.09
80.41

Joint
35/20 & 35/25
65/40

Order Code
8038-40
8038-55

Each
77.20
92.20

8039 BEARINGTrubore, 10mm


8039-10

8039-35

Interchangeable ground joint bearing with top lubricant well for use with our precision
ground stirring shafts (8068, 8070, 8071, 8073, 9532, 9533). Recommended top stirring
speed with our 8117 Stir-Lube is 1500 rpm.
Order Code
8039-03
8039-05
8039-10
8039-20
8039-25

Joint
19/22
19/38
24/40
29/42
34/45

Each
79.08
79.08
79.55
84.01
85.80

Order Code
8039-35

Joint
35/25

Each
86.26

8040 BEARINGTrubore, Water-Cooled, 10mm


Interchangeable, ground joint bearing with jacket for water cooling. May be operated
as high as 2000 rpm using our 8119 high-speed lubricant. Can be operated at 1500
rpm unevacuated using our 8117 Stir-Lube. Hose connections for use with 5/16-inch
or 3/8-inch ID tubing. Available with PTFE-clad joint to eliminate the need for grease.
Use with our precision ground stirring shafts (8068, 8070, 8071, 8073, 9532, 9533).
Joint
24/40
29/42
34/45
45/50

Order Code Each


8040-10
104.16
8040-20
107.01
8040-30
111.06
8040-35
120.39

Joint
35/20 & 35/25
65/40

Order Code
8040-40
8040-55

Each
114.01
217.99

8040 BEARINGTrubore, Water-Cooled, PTFE-Clad, 10mm


8040-40

Similar to 8040, above, except bottom joint is PTFE-clad to eliminate the need for grease.
8040-10
8040-60

Joint
24/40
29/42
34/45
45/50

Order Code
8040-60
8040-64
8040-68
8040-70

Each
149.22
149.33
152.43
156.31

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Subject to Ace Discount (Page 4)

Net

Stirrers, Trubore

10mm Shafts, Bearings & Agitators


8041 STIRRER ASSEMBLY Glass Blade, 10mm
Precision Trubore Stirrer Assembly consisting of 10mm I.D. glass bearing, ground
glass shaft with button, and glass blade. Bearing consists of inner glass bearing, #15
bushing, FETFE oring and threaded glass adapter (see bearing only listing under 8042).
For Flask
Cap., mL
250-500
500-1000
2000-3000
5000-12000

Joint
24/40
29/42
29/42
45/50

Bearing No.
8042-115
8042-117
8042-117
8042-121

Shaft No.
8068-03
8068-03
8068-03
8068-02

Blade No.
8083-08
8083-12
8083-16
8083-20

Replacement size 110 FETFE oring, Pk. 12

Order
Code
8041-11
8041-15
8041-19
8041-20

Each
135.83
158.66
158.80
180.38

7855-716

15.66

185

Complete
Trubore
Assemblies

8041 STIRRER ASSEMBLY PTFE Blade, 10mm


Precision Trubore Stirrer Assembly consisting of 10mm I.D. glass bearing, ground
glass shaft with button, and PTFE blade. Bearing consists of inner glass bearing, #15
bushing, FETFE oring and threaded glass adapter (see bearing only listing under 8042).
Blade No.
8085-07
8085-11
8085-15
8085-19

Replacement size 110 FETFE oring, Pk. 12

Order
Code
8041-30
8041-34
8041-38
8041-40

Each
137.11
141.10
144.99
169.77

7855-716

15.66

8041-11
E-SA

ON

8041-30

OR

Shaft No.
8068-03
8068-03
8068-03
8068-02

AC

Bearing No.
8042-115
8042-117
8042-117
8042-121

FE

Joint
24/40
29/42
29/42
45/50

For Flask
Cap., mL
250-500
500-1000
2000-3000
5000-12000

N ECT

Order Code
8042-05
8042-09

Threaded Glass Adapter, only

OR

FE

Inner Bearing, only


#15 Bushing with size 110 FETFE ORing

E-SA

ON

Self-aligning three-piece bearing. Complete consists of inner Trubore glass bearing, #15
nylon bushing with FETFE oring, and threaded adapter. Unique design eliminates costly
replacement since inner bearing will spin if shaft binds or will self-align at oring seal in
the event the motor is slightly cocked. Inner bearing and bushing can be used with any
joint size. For use with 10mm O.D. shafts 8068, 8070, 8071, 8073, 9532, and 9533. For
replacement size 110 FETFE oring, order 7855-716.

AC

8042 BEARINGTrubore, Glass*, AceThred, 10mm

N ECT

Each
27.48
27.69
Complete Assembly

Joint

Order Code

Each

Joint

Order Code

Each

24/40
29/42
34/45
45/50
35/25

8042-15
8042-17
8042-19
8042-21
8042-35

31.22
33.38
39.78
50.57
35.92

24/40
29/42
34/45
45/50
35/25

8042-115
8042-117
8042-119
8042-121
8042-135

86.39
88.55
94.95
105.74
91.09

8042-135

8042-115

*For assembly with inner PTFE bearing, see 8066.

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

186

Stirrers, Trubore

10mm Shafts, Bearings & Agitators


8043 BEARINGTrubore, AceThred, 10mm
Designed for use with #25 AceThred bushing. Consists of a Trubore bearing, pressure
bushing, gland with two FETFE o-rings and retainer bushing with FETFE o-ring. For use
with our precision ground stirring shafts (8068, 8070, 8071, 8073, 9532, 9533).

E-SA

OR

ON

Each
85.78
26.94
15.14
41.79
169.65

Glass bearing with #15 AceThred at each end and glass tubing between for use with
10mm O.D. 8074 and 8075 stirring shafts. PTFE coupling, with internal FETFE oring
seal, connects bottom of bearing to either #15 or #25 AceThred on vessels such as 6433
pressure reactor head or one-piece pressure reactors. Top bushing also has an internal
FETFE oring seal for additional seal on shaft to allow pressure reactions. Maximum
operating speed 600 rpm. Coupling and bushing supplied with FETFE orings. For
replacement orings: for #15#15 coupling, 7855-730 external, 7855-716 internal; for
#15#25 coupling, 7855-730 and 7855-742 external, 7855-716 internal; for #15 bushing,
7855730 external, 7855-716 internal.

N ECT

8044-55

8044-24

Order Code
8043-08
8043-16
8043-20
8043-30
8043-45

8044 BEARING Pressure, with AceThreds, 1 0mm

E-SA

FE

AC

N ECT

OR

ON

Bearing, only
Pressure Bushing
Gland with Two ORings
Retainer Bushing with ORing
Complete

FE

AC

8043

For Coupling to #15 AceThred


Order
Code
Each
Glass Bearing, only, #15-#15 8044-07 39.14
Coupling, PTFE, #15-#15
5840-60 113.73
Bushing, PTFE, #15
8044-13 80.21
Complete
8044-24 233.08

For Coupling to #25 AceThred


Order
Code
Each
Glass Bearing, only, #15-#15 8044-07 39.14
Coupling, PTFE, #15-#25
5843-62 128.31
Bushing, PTFE, #15
8044-13 80.21
Complete
8044-55 247.66

8047 BEARINGTrubore,10mm
8047

This glass bearing is supplied with tubulation for feeding inert gases around the
bearing to balance any pressure possibly being developed in the flask. Can also
be used for gas-liquid reactions and gas dispersions using hollow shafts as listed
under 8068 and 9532. I.D. is 10mm. Also for use with 8070, 8071, 8073, and 9533
10mm shafts. Use with 3/8-inch or 5/16-inch I.D. tubing, size C hose connection.
Joint
24/40
29/42

Order Code
8047-10
8047-15

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Each
127.94
129.99

Subject to Ace Discount (Page 4)

Net

187

Stirrers, Trubore

10mm Shafts, Bearings & Agitators


8051 BEARINGTrubore, 10mm
Used with 8111 aluminum packing box. It may be used for low positive pressure and
vacuum applications. Using the graphite-impregnated PTFE packing 8122 and 8117
ACE Stir-Lube, a very high film strength lubricant, pressures down to 7 microns have
been obtained at 170 rpm using only a mechanical pump. Speeds over 1000 rpm are not
advisable due to the heat generated. Lubrication (4 or 5 drops) is required at intervals
depending on the speed of operation (about every two hours at 200 rpm). Packing life
is indefinite. Frequent tightening of the packing box is unnecessary once the packing
has run in. The high-vacuum lubricant trap adapter, No. 8113, prevents lubricant from
running into material being stirred. I.D. is 10mm. For use with 8068, 8070, 8071, 8073,
9532, and 9533 shafts (10mm).
Joint
24/40
29/42
34/45
45/50

Order Code
8051-10
8051-15
8051-20
8051-25

Each
136.81
137.49
141.17
100.15

Joint
35/20 & 35/25

Order Code
8051-35

Each
137.49

8051-10

8051-35

8053 BEARINGTrubore,10mm
Especially useful for controlled atmospheric work. Used with 8068 solid shaft to balance
small pressure differentials across the bearing. Used with No. 8068 hollow shafts for
introduction and dispersion of gaseous catalysts, etc. Holes in bearing and shaft coincide.
I.D. is 10mm. Use with 3/8-inch I.D. tubing, size D hose connection.
Each
204.41

8055 BEARING High Vacuum, Trubore, 10mm


This bearing is the standard liquid seal type except that the use of Trubore tubing enables
this unit to perform very satisfactorily under high vacuum conditions. I.D. is 10mm. For
use with 8068, 8070, 8071, 8073, 9532, and 9533 10mm shafts.
Joint
24/40

Order Code
8055-10

8055

Each
142.03

8050 STIRRER BEARING Mechanical Seal, PTFE, 10mm


Newly designed mechanical stirrer bearing from ACE. All PTFE, Rulon or PEEK wetted
area construction provides for low extractables. Completely contained bearing and
internal parts also provides non-shedding of materials into the reaction. The bearing is
excellent for vacuum applications and can be operated at sub-torr levels. Rated for up
to 400 rpm speeds. It can be used on either glass polished or stainless steel 8068, 8073,
8074, 8075, 9532, and 9533 stir shafts. See below for joint sizes.
Joint Size

Replacement size 116 Outside FETFE oring, Pk. 12

Order Code
8050-02
8050-04
8050-10
8050-12

Each
547.19
577.60
596.17
614.21

7855-726

26.57

8050

E-SA

ON

FE

24/40
29/42
#15 AceThred
#25 AceThred

New

OR

Order Code
8053-10

AC

Joint
24/40

8053

N ECT

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

188

Stirrers, Trubore

Complete 10mm Shafts, Bearings & Agitators


Trubore
Assemblies
8064 STIRRER ASSEMBLY Glass Shaft, PTFE Blade, 10mm
Precision Trubore stirrer sssembly consisting of 10mm I.D. glass and PTFE bearing,
polished glass shaft with button, and PTFE blade. Bearing consists of PTFE inner
bearing, glass-filled PTFE bushing and lock nut, compression saddle with FETFE oring
and threaded glass adapter (see complete component listing under 8066).
For Flask
Cap., mL
250-500
500-1000
2000-3000
5000-12000
5000-12000

ON

FE

E-SA

OR

8064-13

AC

8064-34

N ECT

Joint
24/40
29/42
29/42
34/45
45/50

Bearing No. Shaft No.


8066-43
8075-12
8066-46
8075-12
8066-46
8075-12
8066-50
8075-14
8066-55
8075-14

Blade No.
8085-07
8085-11
8085-15
8085-19
8085-19

Order
Code
8064-13
8064-18
8064-21
8064-22
8064-24

Each
177.93
183.27
187.16
199.21
213.21

8064 STIRRER ASSEMBLY Stainless Steel Shaft, PTFE Blade, 10mm


Precision Trubore stirrer assembly consisting of 10mm I.D. glass and PTFE bearing,
polished stainless steel shaft with button, and PTFE blade. Bearing consists of PTFE
inner bearing, glass-filled PTFE bushing and lock nut, compression saddle with FETFE
oring and threaded glass adapter (see complete component listing under 8066).
For Flask
Cap., mL
250-500
500-1000
2000-3000
5000-12000

Joint
24/40
29/42
29/42
45/50

Bearing No. Shaft No.


8066-43
8074-02
8066-46
8074-02
8066-46
8074-04
8066-55
8074-07

Blade No.
8085-07
8085-11
8085-15
8085-19

Order
Code
8064-34
8064-39
8064-42
8064-45

Each
262.26
267.60
277.76
305.68

8066 BEARINGTrubore, PTFE, AceThred,10mm


Bushing 8066-12
Lock Nut 8066-13
Compression Saddle
8066-15 With FETFE
ORing

Self-aligning, lubricant-free PTFE Trubore glass and PTFE bearing for use with 8074
stainless steel or 8075 glass 10mm stirring shafts. Complete consists of PTFE inner
Trubore bearing, AceThred glass adapter, non-flaking PTFE compression saddle with
oring and glass-reinforced PTFE bushing and lock nut with FETFE oring. The lock nut
permits stirring in either direction without fear of unthreading. The compression saddle
with oring maintains constant force with little attention. Vacuum down to 1mm. Not
recommended for precision ground glass shafts. For replacement compression saddle
oring, see 7855-718; for bearing oring, see 7855-712.

FETFE ORing 7855-712


PTFE Inner Bearing
8066-06

Threaded Glass Adapter, only

E-SA

OR

ON

FE

8066-43

AC

Thred Adapter
24/408066-20
29/428066-24
34/458066-28
45/508066-32

PTFE Inner Bearing w/ FETFE ORing, only


Glass Filled/PTFE Bushing, only
Glass Filled/PTFE Lock Nut, only
Compression Saddle w/ FETFE ORing, only

N ECT

Joint
24/40
29/42
34/45
45/50
35/25

Order Code
8066-20
8066-24
8066-28
8066-32
8066-33

Each
29.21
32.72
37.91
51.91
34.43

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Order Code
8066-06
8066-12
8066-13
8066-15

Each
31.08
30.46
9.94
11.06

Complete Assembly
Joint
24/40
29/42
34/45
45/50
35/25

Order Code
8066-43
8066-46
8066-50
8066-55
8066-60

Each
111.75
115.26
120.45
134.45
116.97

Subject to Ace Discount (Page 4)

Net

Stirrers, Trubore

189

10mm Shafts, Bearings & Agitators


8066 BEARING/DEBRIS TRAP PTFE, AceThred,10mm
Combination all-in-one stirring shaft bearing and debris trap, designed to prevent particles
from entering reaction vessel. Lubricant free PTFE bearing with compression saddle oring
makes a mechanical seal against a polished glass shaft. Debris trap section consists
of a PTFE washer and particle well. #7 AceThred on glass body side allows access
for clean out, or may be used for evacuation/gas purge port. Complete item supplied
with glass body, inner PTFE bearing, PTFE bushing and lock nut, Rulon saddle FETFE
oring, Ace-Safe connector for 1/4inch tubing, and PTFE plug. Use with 8074 and
8075 10mm shafts.

Complete Assembly

Replacement FETFE orings


FETFE, Size 014, Pk. 12
7855-712

Order Code
8066-320
8066-324
8066-328
8066-332
8066-333

Joint
24/40
29/42
34/45
45/50
35/25

Each
267.21
269.91
275.33
286.14
271.28

E-SA

ON

FE

Order Code Each


8066-220 106.83
8066-224 109.53
8066-228
114.95
8066-232
125.76
8066-233 110.90

Joint
24/40
29/42
34/45
45/50
35/25

8066-320

Each
44.46
30.46
9.94
11.06
28.78
22.15
13.53

AC

Threaded Glass Adapter, only

Order Code
8066-08
8066-12
8066-13
8066-15
8066-03
5846-44
5853-06

OR

PTFE Inner Bearing w/ FETFE ORing, only


Glass Filled/PTFE Bushing, only
Glass Filled/PTFE Lock Nut, only
Compression Saddle w/ FETFE ORing, only
PTFE Washer
PTFE Plug, #7
Ace-Safe Connector, #7 x 1/4-inch

N ECT

12.93

NOTE: Glass Trap Body is also available without side port. Call or email for details.

8066 BEARINGTrubore, PTFE, AceThred,10mm


Self-aligning, lubricant-free PTFE Trubore bearing for use with 8074 stainless steel or 8075
glass 10mm stirring shafts. Added side port hose connection allows purging flask contents with
a gas, or in airless work, allows for an inert gas blanket. Complete consists of PTFE inner
Trubore bearing, AceThred glass adapter, non-flaking PTFE compression saddle with oring,
and glass-reinforced PTFE bushing and lock nut with FETFE o-ring. The lock nut permits
stirring in either direction without fear of unthreading. The compression saddle with oring
maintains constant force with little attention. Vacuum down to 1mm. Not recommended
for precision ground glass shafts. Use with 8074 and 8075 10mm shafts. For replacement
compression saddle o-ring, order 7855-718; for bearing FETFE o-ring, order 7855-712.

Each
39.50
42.98
48.19
62.18
44.71

Complete Assembly
Joint
24/40
29/42
34/45
45/50
35/25

Order Code
8066-130
8066-132
8066-134
8066-136
8066-140

Each
122.04
125.52
130.73
144.72
127.25

E-SA

ON

FE

Order Code
8066-70
8066-71
8066-72
8066-73
8066-79

Side port hose


connection

Joint
24/40
29/42
34/45
45/50
35/25

Each
31.08
30.46
9.94
11.06

OR

Threaded Glass Adapter, only

Order Code
8066-06
8066-12
8066-13
8066-15

AC

PTFE Inner Bearing w/ FETFE ORing, only


Glass Filled/PTFE Bushing, only
Glass Filled/PTFE Lock Nut, only
Compression Saddle w/ FETFE ORing, only

8066-130

N ECT

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190

Stirrers

10mm Shafts, Bearings & Agitators


13445 BEARING Debris Free, PTFE, 1 0mm
Vacuum tight (~5 Torr), flake free, chemically resistant stirrer bearing makes a mechanical
seal against a polished glass shaft. Debris trap section consists of a PTFE sleeve for a
wide range of joint and shaft diameter sizes. For use with 10mm polished glass or stainless
steel shafts, NOT recommended for PTFE shafts. Bearing consists of a PTFE standard
taper body with added PEEK for better stability, glass filled polypropylene screw cap,
PEEK compression spring, PTFE/PEEK sleeve and a glass filled polypropylene loosening
nut. For use up to 500 rpm.
For Shaft Size, mm
13445

10
10
10
10

Joint

Order Code
13445-30
13445-32
13445-34
13445-36

24/40
29/42
34/45
45/50

Each
173.35
182.64
202.49
204.60

Replacement Seals & Springs:


Order Code
13445-420
13445-426

PTFE/PEEK sleeve seal


PEEK compression spring

Each
27.53
29.91

8068 STIRRING SHAFT Borosilicate, Precision Ground, 10mm


Precision ground glass stirring shafts, 10mm OD, paddled, button type and bead type.
Button type shafts accept 8083, 8085, 8086, 8087 and 8096 stir blades. Beaded shafts
accept 8088, 8089 and 8090 agitators. Use with Trubore bearings 8036, 8038, 8039, 8040,
8042, 8043, 8047, 8051, 8053, 8050 and 13443. Join to motor using 8124 series chucks.

F
G

Lengths, mm
For Flask
Size, mL
Ground Overall
250-3000
420
440
3000-5000
560
580
A 12000-22000
660
690
50000
710
740

Order
Code
8068-03
8068-02
8068-04
8068-06

Each
40.19
42.86
44.97
48.00

B 250-3000

420

440

8068-08

61.45

250-3000
D 3000-5000

360
500

440
580

8068-18
8068-17

87.17
89.77

250-3000
F 3000-5000

420
560

440
580

8068-25
8068-27

67.23
91.49

250-3000
G 3000-5000
12000-22000

420
560
660

440
580
690

8068-30
8068-32
8068-31

53.04
54.62
59.13

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Description
BUTTON TYPE, used with
any blade listed under 8083,
8084, 8085, and 8086. For
bearings, see 8036, 8038,
8039, 8040, 8042, 8043, 8051
or 8055.
PADDLE TYPE, will fit through
45/50 joint on boiling flask.
PADDLE TYPE, for large neck
boiling flask such as 71/60
or larger.
HOLLOW TYPE, for material
introduction. Use with 8053
bearing.
BEAD TYPE, for use with
8088, 8089 and 8090 PTFE
Agitators.

Subject to Ace Discount (Page 4)

Net

Stirrers

191

10mm Shafts, Bearings & Agitators


8070 STIRRING SHAFT PTFE-Coated Glass, 1 0mm
Precision ground glass stirring shafts, 10mm O.D., button type, PTFE coating permits
higher stirring speeds with Trubore bearings. If used unlubricated, 500 rpm max with
water-cooled 8040 bearing. Compatible with 8036, 8038, 8039, 8043, 8047, 8051, 8055
and 13443 bearings. Button type shafts accept 8083, 8085, 8086, 8087 and 8096 stir
blades. Join to stirrer motor using 8124 series chucks.
For Flask Cap., mL
250-5000
12000-22000

Length, mm
440
690

Order Code
8070-05
8070-10

8070

Each
75.72
83.86

8071 STIRRING SHAFT PTFE-Coated Steel, 10mm


PTFE covered stainless steel stirring shafts, 10mm O.D., drilled type. If used unlubricated,
500 rpm max with water cooled 8040 bearing, 100 rpm maximum recommended with
8036, 8038, 8039, 8043, 8047, 8051 and 8055 bearings. With condensate film as added
heat transfer agent, 2000 rpm can be attained. Drilled type shaft accepts 8088, 8089
and 8090 agitators. Compatible with our 13443 collet-type bearing. Join to stirrer motor
using 8124 series chucks.
For Flask Cap., mL
250-5000
12000-22000
12000-22000

Length, mm
460
640
690

Order Code
8071-05
8071-07
8071-10

Each
207.66
264.62
267.94

8071

13443 STIRRER BEARING PTFE, 8, & 10mm


Inert PTFE Stirrer bearing. Features a totally enclosed bearing body for non-shedding,
anti-whip, chemically resistant design. The bearing can also be used in slight vacuum or
slight pressure applications. The design has a composite PTFE/PEEK main internal seal
and a specially fabricated glass ball-bearing for rigidity and smoothness during lengthy
operation. Max recommended speeds up to 500 rpm continuous operation. Ideal for
glass, metal or PTFE stir shafts. Bottom is a molded, inner standard taper joint. Average
length is 96mm and 45mm O.D. at bearing center.
For Shaft Size, mm
8
10

Joint
24/40
24/40

Order Code
13443-10
13443-12

13443

Each
428.93
428.93

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

192

Stirrers

10mm Shafts, Bearings & Agitators


13850 AGITATOR, STIRRING SHAFT PTFE, 1 0mm

13850

Chemically resistant, PTFE, three bladed, retreat curve stir shaft. Fully molded bottom blade
is designed with a 30 retreat angle. 10mm shaft is PTFE encapsulated stainless steel.

New

New

Blade
Shaft O.D., mm Length, mm Height, mm
10
400
10
10
400
10

O.D., mm
50
70

Order Code Each


13850-01
309.15
13850-04
335.81

13852 AGITATOR, STIRRING SHAFT PTFE, 1 0mm


Chemically inert, four bladed, screw propeller design, PTFE stir shaft. The 10mm O.D.,
steel reinforced shaft has approximately 50mm exposed for easier/better connection to
the stir motor chuck.
Shaft O.D., mm Length, mm
10
400
10
400

Blade O.D.,
mm
50
70

Order Code
13852-10
13852-15

Each
335.81
335.81

13852

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Subject to Ace Discount (Page 4)

Net

Stirrers

193

10mm Shafts, Bearings & Agitators


8073 STIRRING SHAFT C Type, Borosilicate, 1 0mm
Precision ground glass stirring shafts,10mm O.D., crescent type. Useful for stirring viscous
materials at low rpm. Available for round bottom flasks of 1, 3 and 5 liters. Code -19,
three liter size will fit a two liter flask, but closely. Flask opening must be 29/42 or larger.
Use with Trubore bearings 8036, 8038, 8039, 8040, 8043, 8047, 8051, 8053 and 8055.
Compatible with our 8050 PTFE mechanical seal and 13443 PTFE collet type bearings.
Join to stirrer motor using 8124 series chucks.
For Flask Cap., mL
1000
3000
5000

Order Code
8073-16
8073-19
8073-23

Each
63.11
63.11
63.11

8073

8074 STIRRING SHAFT Stainless Steel, 1 0mm


Polished stainless steel stirring shafts, 10mm O.D., drilled type with removable button.
When used with 8066 PTFE bearing, a lubricant-free vacuum seal can be realized at
speeds up to 200 rpm. Recommended for use with 8044, 8050, 8066, 13443 and 13445
bearings. With button, shaft accepts 8083, 8085, 8086, 8087 and 8096 stir blades. With
button removed, shaft will accept 8094 and 8095 agitators secured with a set-screw
anywhere along its ground flat section. Join to stirrer motor using 8124 series chucks.
For Flask
Cap., mL
250-1000
2000-5000
5000-12000

Lengths, mm
Flat Section
Overall
100
420
200
450
280
580

Order Code
8074-02
8074-04
8074-07

8074

Each
139.98
146.25
150.06

Replacement Buttons:
Order Code
8074-40

Each
248.02

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

194

Stirrers

10mm Shafts, Bearings & Agitators


8075 STIRRING SHAFT Borosilicate, Polished, 10mm
Polished glass stirring shafts, 10mm O.D. Only recommended for use with our 8050,
8066, 13443 and 13445 bearings. Join 8083, 8085, 8086, 8087 & 8096 blades to button
type shafts. Join 8088, 8089 and 8090 agitators to beaded shafts. Plain shafts will accept 8094 and 8095 agitators secured with a set-screw anywhere along its ground flat
section. Join to stirrer motor using 8124 series chucks.

8075

Knob

Button

For Flask Cap., mL


250-3000
3000-5000
12000-22000
250-3000
3000-5000
12000-22000
250-3000
3000-5000
12000-22000

Type
With Button
With Button
With Button
Plain, w/o Button
Plain, w/o Button
Plain, w/o Button
With Bead/Knob
With Bead/Knob
With Bead/Knob

Length, mm
440
580
690
440
580
690
440
580
690

Order Code
8075-12
8075-14
8075-15
8075-21
8075-23
8075-24
8075-32
8075-34
8075-36

Each
55.65
57.59
60.15
47.14
49.17
51.16
57.11
60.33
65.83

Plain

9532 STIRRING SHAFT Hollow, Borosilicate, 10mm


9532

Precision ground glass stirring shaft with attached vanes, 10mm. For use when agitation
and gas introduction are desired at the same time. Agitator will fit through a 45/50 joint.
Designed for use with our 9523 Trubore bearing and 9443 or 9446 mini-lab flask heads.
Introduced gas exits the hollow shaft within the agitator and produces a fine dispersion.
Join to stirrer motor with 8124 series chucks.
Order Code
9532-10

Each
140.16

9533 STIRRING SHAFT Borosilicate, Ground, 10mm


9533

Precision ground glass stirring shaft, 10mm OD, attached vanes. Vanes will fit through a
45/50 joint and are contoured for use with our 9448 and 9456 series Mini-Lab flasks.
Use with Trubore bearings 8036, 8038, 8039, 8040, 8042, 8043, 8047, 8051, 8053 and
8055. Compatible with our 8050 mechanical seal and 13443 PTFE collet type bearings.
Join to stirrer motor using 8124 series chucks.
Order Code
9533-02

Each
85.70

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Subject to Ace Discount (Page 4)

Net

Stirrers

195

10mm Shafts, Bearings & Agitators


8082 STIRRER BLADES PTFE, Oval, 10mm
PTFE oval stir blades for 10mm O.D. button type stir shafts. 10mm O.D. shafts can be
found in our 8068, 8070, 8074 and 8075 series.
Width, mm
19
19
24
24

Length, mm
40
60
80
115

Flask Cap., mL
100-500
250-500
1000-2000
2000-3000

Order Code
8082-02
8082-04
8082-06
8082-08

Each
8.39
10.03
12.60
14.04

8082

8083 STIRRER BLADES Borosilicate Glass, 10mm


Glass stir blades for 10mm O.D. button type stir shafts. 10mm O.D. stir shafts can be
found in our 8068, 8070, 8074 and 8075 series.
Width, mm
19
19
19
23
24
24

Length, mm
48
60
76
113
134
160

Flask Cap., mL
100-500
250-500
500-1000
2000-3000
5000-12000
22000-72000

Order Code
8083-04
8083-08
8083-12
8083-16
8083-20
8083-24

Each
9.16
9.25
29.92
30.06
31.78
31.95

8083

8085 STIRRER BLADES PTFE, 10mm


PTFE stir blades for button type stir shafts. 10mm O.D. shafts can be found in our
product series 8068, 8070, 8074 and 8075. 19mm O.D. shafts can be found in our 8076
and 8077 series.
Width, mm
19
19
19
23
24
24

Length, mm
48
60
76
113
130
160

Flask Cap., mL
100-500
250-500
500-1000
2000-3000
5000-12000
22000-72000

Order Code
8085-03
8085-07
8085-11
8085-15
8085-19
8085-23

Each
9.69
10.53
12.36
16.25
21.17
26.51

8085

8086 STIRRER BLADES Stainless Steel, 10mm


304 stainless steel stir blades for 10mm O.D. button type stir shafts. 10mm O.D. stir
shafts can be found in our 8068, 8070, 8074 and 8075 series.
Width, mm
19
23
24
24

Length, mm
76
113
134
160

Flask Cap., mL
500-1000
2000-3000
5000-12000
22000-72000

Order Code
8086-04
8086-08
8086-12
8086-16

Each
31.06
30.82
36.19
39.46

8086

8126 STIRRING SHAFT Pass-through Assembly, 10mm


Item includes the 8126-10 stir shaft coupling with pin that is attached to 7mm O.D.
stainless steel drive shaft. Shaft that is 305mm long and fits up through the chuck and
opening in the Heidolph RZR model and Caframo BDC model overhead stir motors and
allows for adjusting the height of the entire stir shaft assembly. For 10mm stir shafts.
Order Code
8126-24

8126-24

Each
75.13

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

196

Stirrers

10mm Shafts, Bearings & Agitators


8096 STIRRER BLADES Stainless Steel, 10mm
316 stainless steel, football shaped, stir blades for 10mm O.D. button type stir shafts.
Holed versions, codes -70 thru -74, provide even greater agitation. 10mm O.D. stir shafts
can be found in our 8068, 8070, 8074 and 8075 series.
Without holes

8096-06

8096-72

Width, mm
19
24
24

Length, mm
40
80
115

Order Code
8096-04
8096-06
8096-10

Each
31.43
32.42
37.65

Length, mm
60
80
115

Order Code
8096-70
8096-72
8096-74

Each
36.01
36.66
41.91

With holes
Width, mm
19
24
24

8087 STIRRER BLADES Banana Type, PTFE, 10mm


PTFE banana shaped stir blades for 10mm O.D. button type stir shafts. 3mm thick blades
have a number of perforations and are designed to closely fit various sizes of round bottom
flasks. 10mm O.D. stir shafts can be found in our 8068, 8070, 8074 and 8075 series.

8087

For Flask Width, Lgth., Order


Cap., mL mm
mm
Code
500
21
87 8087-05
1000
23
109 8087-07
2000
31
146 8087-09
3000
31
157 8087-11

For Flask Width,


Cap., mL mm
5000
35
12000
37
22000
40

Each
26.39
31.94
34.59
41.36

Lgth.,
mm
175
222
263

Order
Code
8087-13
8087-15
8087-19

Each
49.01
51.67
72.10

8088 AGITATOR PTFE, Single Blade Type, 10mm


8088

PTFE agitator with removable blade secured with a PTFE pin. Supplied 76mm long blade
will fit through a 29/42 joint. Fits 10mm O.D. drilled type or beaded type 8068, 8071
and 8075 shafts.
Complete
Order Code
8088-10

Replacement Blade
Each
222.39

Order Code
8088-03

Each
33.93

8089 AGITATOR PTFE, Multi-Paddle, 10mm


8089

PTFE multi-paddle agitator for 10mm O.D. drilled or knob type shafts. Paddles are
replaceable. Fits 10mm O.D. drilled or knob type 8068, 8071 and 8079 shafts.
Complete
Size, mm
38
64
76

Order Code Each


8089-04
104.10
8089-06
111.43
8089-08
112.73

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Blades, Only
Order Code
8089-14
8089-16
8089-18

Each
18.50
24.15
26.33

Subject to Ace Discount (Page 4)

Net

Stirrers

197

10mm Shafts, Bearings & Agitators


8090 AGITATOR PTFE, Turbine, 10mm
All-PTFE, turbine type agitator. Unique locking arrangement assures positive grip. Agitator
fits 10mm shafts. Shaft opening is drilled straight through to allow positioning of agitator
at any height on shaft as well as at the bottom. For use with glass stirring shaft, 8068,
8075 or PTFE shaft, 8071.
Blade Size, mm
38
64

Order Code
8090-04
8090-08

8090

Each
138.47
151.38

8094 AGITATOR 316 Stainless Steel, Multi-Paddle, 10mm


For use with 8074 stainless steel shaft or 8075 borosilicate straight shaft. Center hole
is 10mm I.D. and one or more can be positioned on shaft at various locations using
set screws to secure. With stainless shaft use stainless set screw; with glass shaft use
Kel-F-tipped set screw. Both screws supplied with agitator.
Size,
mm
75
89

Order Code
8094-23
8094-27

Replacement set screws:

Each
193.83
205.47

Stainless
Stainless/Kel-F

Order Code

Each

8094-50
8094-52

4.45
6.84

8094

8095 AGITATOR 316 Stainless Steel, Turbine, 10mm


10mm steel agitator with multiple fins which may be bent, with care, to different angles.
See 8094 listing, above, for replacement set screws.
Size, mm
75
89

Order Code
8095-31
8095-35

Each
204.88
218.88

8095

8113 ADAPTER Lubricant Trap, High Vacuum, 10mm


Primarily designed for use with ACE 8051 bearings. The inner tube through which the
stirring shaft passes, plus the PTFE oring supplied with each unit, prevents the lubricant
or foreign particles from contaminating the flask contents. For replacement PTFE ring,
order 8113-89.
Top Joint
24/40
29/42
29/42

Bottom Joint
24/40
29/42
34/45

Order Code
8113-10
8113-20
8113-25

8113

Each
73.58
76.73
85.03

8124 CHUCK Flex-Grip, 10mm


Nylon chuck for use with ACE stirring shafts or other shafts of the same dimensions. Chuck
has flexible insert which allows for misalignment of shaft without danger of breakage.
Top has set screw for coupling to stir motor shaft.
For Stirring
Shaft Size, mm
10
10
10

For Motor
Shaft, mm (In.)
8 (5/16)
9.5 (3/8)
13

Insert Only Size, mm


10

Qty.
6

Order Code
8124-10
8124-12
8124-13

8124

Each
43.92
43.92
43.92

Order Code Per Package


8124-25
17.04

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

198

Stirrers, Trubore

19mm Shafts, Bearings & Agitators


8059 BEARINGTrubore, Water-Cooled, 19mm

8059

Trubore 19mm I.D., stirrer bearing with standard taper joint bottom. Jacketed for water
cooling. Designed for use with 19mm O.D. 8077 and 8078 precision ground glass shafts
and 8079 PTFE shafts with stainless steel core. Hose connections are size D for use
with 3/8inch I.D. tubing.
Joint
45/50
55/50

Order Code
8059-05
8059-09

Each
229.99
234.51

8060 BEARINGTrubore, Water-Cooled, 19mm


Trubore 19mm I.D., glass stirrer bearing with bottom spherical ground joint. Joint can
be clamped to prevent rotation. Length is 15.2cm (6 inches). Designed to accommodate
ACE 8112-10 packing box which sits directly into the top of the bearing. Designed for
use with 19mm O.D. 8077 and 8078 precision ground glass shafts and 8079 PTFE shafts
with stainless steel core. Hose connections are size D for use with 3/8inch I.D. tubing.

8060

Joint
65/40

Order Code
8060-10

Each
299.67

8061 BEARINGTrubore, Heavy Duty, 19mm


Heavy duty, 19mm I.D., Trubore stir bearing with bottom standard taper joint. Designed
to accommodate ACE 8112-10 packing box which sits directly into the top of the bearing.
Designed for use with 19mm O.D. 8077 and 8078 precision ground glass shafts and 8079
PTFE shafts with stainless steel core. Length is 20.3 cm (8 inches). Heavy duty style for
use with larger capacity flasks.

8061

Joint
45/50

Order Code
8061-04

Each
178.71

8065 BEARINGTrubore, Glass, Heavy Duty, 19mm

8065

T
S 34/45 Bottom Joints

E-SA

OR

ON

FE

AC

Trubore, self aligning, heavy duty three piece bearing. Complete consists of inner 19mm
I.D. Trubore bearing, compression seal nylon busing, with FETFE o-ring and #25 AceThred
adapter with standard taper, ground joint bottom. Design allows for slight misalignment
of stir motor and the bearing without breaking or shaft seizing, as the inner bearing will
spin. Designed for use with 19mm O.D. 8077 and 8078 precision ground glass shafts and
8079 PTFE shafts with stainless steel core. Heavy duty style for use with larger capacity
flasks. For replacement size 212 FETFE oring, see 7855-734.

N ECT

Inner Bearing, only


Bushing with ORing
#25 AceThred Adapter, only
Complete

Order Code
8065-06
8065-10
8065-14
8065-60

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Each
66.43
40.49
59.23
166.15

T
S 45/50 Bottom Joints
Order Code
8065-06
8065-10
8065-16
8065-64

Each
66.43
40.49
62.67
169.59

Subject to Ace Discount (Page 4)

Net

199

Stirrers, Trubore

19mm Shafts, Bearings & Agitators

#25 AceThred Glass Adapter, only


Joint
45/50
55/50
71/60

Order Code
8067-18
8067-20
8067-22

Each
106.40
102.13
112.06

Bushing 8067-08
Lock Nut 8067-11
Compression
Saddle 8067-13
With FETFE ORing

Each
83.40
45.97
16.79
16.49
Complete Assembly
Bottom
Joint Order Code
Each
45/50
8067-30
269.05
55/50
8067-34
264.78
71/60
8067-38
274.71

N ECT

FETFE ORing
7855-734
PTFE Inner Bearing
8067-05
Thread Adapter
45/50 8067-18
55/50 8067-20
71/60 8067-22

8067-30

8067 BEARING/DEBRIS TRAP PTFE, AceThred,19mm

#25 AceThred Glass Adapter, only


Bottom
Joint
Order Code
Each
45/50
8067-45
148.02
55/50
8067-47
162.68
71/60
8067-49
179.22

Order Code
8067-07
8067-08
8067-11
8067-13
8067-09
5846-46
5853-15

AC

ON

PTFE Inner Bearing w/ORing, only


Glass Filled/PTFE Bushing, only
Glass Filled/PTFE Lock Nut, only
Compression Saddle w/ORing, only
PTFE Washer
PTFE Plug, #11
Ace-Safe Connector, #11 x 3/8-inch

E-SA

FE

Combination all-in-one stirring shaft bearing and debris trap. Designed to prevent
particles from entering the reaction vessel. Lubricant-free PTFE bearing with compression
saddle oring makes a mechanical seal against 8076 polished glass shaft. Debris trap
section consists of a PTFE washer and particle well. #11 AceThred on glass body side
allows access for clean-out, or may be used for evacuation/gas purge port. Complete
item supplied with glass body, inner PTFE bearing, PTFE bushing and lock nut, Rulon
saddle with FETFE oring, Ace-Safe connector for 3/8inch tubing, and PTFE plug.

OR

Order Code
8067-05
8067-08
8067-11
8067-13

ON

PTFE Inner Bearing w/ORing, only


Glass Filled/PTFE Bushing, only
Glass Filled/PTFE Lock Nut, only
Saddle ORing, only

E-SA

OR

Self-aligning, lubricant-free PTFE Trubore bearing for use with 8076, 19mm polished glass
stirring shaft. Complete consists of PTFE inner Trubore bearing, #25 AceThred glass adapter,
non-flaking PTFE compression saddle with oring and glass-reinforced PTFE bushing and
lock nut with FETFE oring. The lock nut permits stirring in either direction without fear of
unthreading. The compression saddle with FETFE oring maintains constant force with little
attention. Vacuum down to 1mm of Hg. Not recommended for precision ground glass shafts.
For replacement saddle oring, order 7855-730; for bearing FETFE oring, order 7855-734.

FE

AC

8067 BEARINGTrubore, PTFE, AceThred, 19mm

N ECT

Each
78.33
45.97
16.79
16.49
33.16
32.14
22.02
Complete Assembly
Bottom
Joint
Order Code
Each
45/50
8067-54
392.92
55/50
8067-57
407.58
71/60
8067-59
424.12

8067-54
NOTE: Glass trap body
is available without side
port. Call or e-mail for
details.

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

200

Stirrers

19mm Shafts, Bearings & Agitators


8076 STIRRING SHAFT Borosilicate, Polished, 19mm
Polished glass stirring shafts, 19mm O.D. Available in solid and hollow styles and in
various lengths. Join 8085 blades to button type shafts, Join 8091, 8092, 8093 and 8100
agitators to either knob or drilled style shafts. Join all shafts to stirrer motor using 8124
series chucks. Recommended for use with our 8050 mechanical seal, 8067 PTFE and
13445 PTFE debris-free bearings.

8076-05
Button

For Flask
Cap., Liters
22
22
50-72

Length, mm
(Inches)
700 (28)
900 (36)
1,200 (48)

Bottom Style
Button
Button
Button

Order Code
8076-05
8076-07
8076-10

Each
190.01
191.42
192.26

8076 STIRRING SHAFT Borosilicate, Polished,19mm


19mm O.D. polished stirring shaft. Can be used with 8050, 8059, 8060, 8061, 8065, 8067,
or 13445 bearings and 8091, 8092 or 8093 agitators. Fits 8124 chuck.

8076-40,
-43, -45, -48
Drilled

8076-42,
-44, -46
Knobed

For Flask
Cap., Liters
10
10
20
30
50
50
50

Type Shaft
Hollow
Solid
Solid
Hollow
Solid
Hollow
Solid

Length, mm
(Inches)
800 (32)
800 (32)
900 (36)
1,200 (48)
1,140 (45)
1,400 (54.5)
1,400 (54.5)

Bottom Style
Knobed Bottom
Drilled Holes
Drilled Holes
Knobed Bottom
Drilled Holes
Knobed Bottom
Drilled Holes

Order
Code
8076-42
8076-43
8076-40
8076-44
8076-45
8076-46
8076-48

Each
211.14
240.03
248.02
211.14
290.38
294.62
306.64

8077 STIRRING SHAFT Precision-Ground, Borosilicate, 19mm


19mm O.D. button type, hollow shaft for use with all 19mm I.D. ACE Trubore bearings,
8059, 8060, 8061 or 8065. Also compatible with 8050 mechanical seal and 13445 PTFE
bearings. Fits 8124 or 8126 chucks. Ground surface approximately 380mm long. For
stir blades, see 8085.
8077

For Flask
Cap., Liters
22
22
50-72

Length, mm (Inches)
700 (28)
900 (36)
1,200 (48)

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Order Code
8077-23
8077-25
8077-27

Each
113.52
127.93
122.22

Subject to Ace Discount (Page 4)

Net

Stirrers

201

19mm Shafts, Bearings & Agitators


13852 STIRRING SHAFT PTFE, 19mm

New

Chemically inert, four bladed, screw propeller design, PTFE stir shaft. The 19mm O.D.,
steel reinforced shaft has approximately 50mm exposed for easier/better connection to
the stir motor chuck.
Shaft O.D., mm Length, mm
19
900

Blade O.D.,
mm
95

Order Code
13852-19

522.36

13852

8126 STIRRING SHAFT Pass-through Assembly, 19mm


Item includes the 8126-19 stir shaft coupling with pin that is attached to 7mm O.D.
stainless steel drive shaft. Shaft that is 305mm long and fits up through the chuck and
opening in the Heidolph RZR model and Caframo BDC model overhead stir motors and
allows for adjusting the height of the entire stir shaft assembly. For 19mm stir shafts.
Order Code
8126-22

Each
276.11

8126-22

8078 STIRRING SHAFT Precision-Ground, Heavy Duty, 1 9mm


Precision ground glass stirring shafts, 19mm O.D., hollow, heavy duty. Knob type shafts
accept 8091,8092,8093,8100 agitators and can be used in all 19mm I.D. Trubore 8059,
8060, 8061 and 8065 bearings. Compatible with our 8050 mechanical seal and 13445
PTFE debris-free bearings. Join to stirrer motor using 8124 series chucks. Heavy duty
design intended for use with large flasks up to 72 liters.
For Flask
Cap., Liters
22
50-72

Length, mm
(Inches)
900 (36)
1,200 (48)

Order Code
8078-05
8078-10

8078

Each
178.44
194.12

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

202

Stirrers

19mm Shafts, Bearings & Agitators


8079 STIRRING SHAFT Precision, PTFE, Heavy Duty, 19mm
Precision PTFE covered stainless steel stirring shafts, 19mm O.D. Drilled type shafts
accept 8091, 8092, 8093, 8100 agitators and can be used in 19mm Trubore bearings
(8059, 8060, 8061 & 8065). Not recommended for PTFE bearings 8050, 8067 and 13445.
Join to stirrer motor using 8124 series chucks.
For Flask
Cap., Liters
22
22
50-72

8079

Length, mm (Inches)
700 (29)
900 (36)
1,200 (48)

Order Code
8079-03
8079-05
8079-10

Each
477.57
484.69
528.19

8085 STIRRER BLADE PTFE, 19mm


PTFE stir blades for button type stir shafts. 10mm O.D. shafts can be found in our
product series 8068, 8070, 8074 and 8075. 19mm O.D. shafts can be found in our 8076
and 8077 series.
Width, mm
35
39
44
54

8085-52

Length, mm
150
160
175
190

Order Code
8085-52
8085-54
8085-56
8085-58

Each
62.91
81.66
91.30
94.72

8091 AGITATOR PTFE, Multi-Paddle, 19mm


8091-10

PTFE agitators for use with large-scale reactors with 6-inch, 8-inch or 12-inch flanges.
These heavy-duty agitators impart maximum energy and are offset at bottom to
accomodate slurries. 19mm agitators fit drilled type or knob type 8076, 8078 & 8079
shafts. 28mm agitators fit 8080 shafts.
Replacement Blades
Size, mm
102
152

Order Code
8091-10
8091-20

Each
226.34
245.80

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Order Code
8091-14
8091-15

Each
45.75
50.33

Subject to Ace Discount (Page 4)

Net

203

Stirrers

19mm Shafts, Bearings & Agitators


8091 AGITATOR PTFE, Large Scale, Multi-Paddle, 19mm
PTFE agitators for use with large-scale reactors with 6-inch, 8-inch or 12-inch flanges.
These heavy-duty agitators impart maximum energy and are offset at bottom to
accomodate slurries. 19mm agitators fit drilled type or knob type 8076, 8078 & 8079
shafts. 28mm agitators fit 8080 shafts.
Size, mm
(Inches)
140 (5.5)
203 (8)

8091-40

Replacement Blades
Order Code
8091-26
8091-40

Order Code
8091-28
8091-44

Each
318.61
352.23

Each
68.53
101.81

8100 AGITATOR PTFE, Multi-Paddle with Receptacle, 19mm


PTFE, large-scale, multi-paddle agitator design to accept pinned bottom valves, like
our 6482 flush-seal valve. The pin helps reduce wobble or flexing at higher rpm. 19mm
agitators will fit drilled type or knob type 8076, 8078 and 8079 shafts.
Size, mm
140
200

Order Code
8100-09
8100-19

8100

New

Each
369.95
854.95

8092 AGITATOR PTFE, Single Blade, 19mm


PTFE bottom agitator, with single 152mm length, removable blade. Agitator body is
secured to 19mm shaft by removable PTFE pin. Top forked tines are then secured
with threaded PTFE nut. Blade will fit through a 45/50 joint opening. Fits 8076, 8078
and 8079 drilled or knob-type 19mm shafts.
Complete
Order Code
8092-10

8092

Replacement Blade

Each
256.36

Order Code
8092-14

Each
32.82

8093 AGITATOR PTFE, Turbine, 19mm


A 102mm or 152mm total diameter agitator for 19mm O.D. 8076, 8078 or 8079 drilled
or knob-type shafts. Turbine blade unit is removable. Shaft opening is open straight
through to allow positioning of agitator at any height on shaft. NOT supplied with shaft.
Complete
Size, mm
102
152

Order Code
8093-12
8093-22

Replacement Blades
Each
186.56
430.35

Order Code
8093-15
8093-16

Each
53.93
94.66

8093

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

204

Stirrers

19mm Shafts, Bearings & Agitators


8124 CHUCK Flex-Grip, 19mm
Nylon chuck for use with ACE stirring shafts or other shafts of the same dimensions. Chuck
has flexible insert which allows for misalignment of shaft without danger of breakage.
8124

For Stirring
Shaft Size, mm
19
19
19
19
19
Insert Only Size
19 mm

For Motor
Shaft, mm (In.)
8 (5/16)
9.5 (3/8)
12.7 (1/2)
13
15.9 (5/8)
Qty.
Pkg/3

Order Code
8124-15
8124-17
8124-20
8124-22
8124-23

Order Code
8124-30

Each
152.25
152.25
152.25
152.25
152.25

Per Package
21.21

8050 STIRRER BEARING Mechanical Seal, PTFE, 19mm


Newly designed mechanical stirrer bearing from ACE. All PTFE, Rulon or PEEK wetted
area construction provides for low extractables. Completely contained bearing and
internal parts also provides non-shedding of materials into the reaction. The bearing is
excellent for vacuum applications and can be operated at sub-Torr levels. Rated for up
to 400 rpm speeds. It can be used on either glass polished or stainless steel stir shafts.

8050

Shaft Size, mm
19

Joint Size
45/50

Replacement Outside size 128 oring

Order Code
8050-06

Each
601.93

7855-773

19.41

New

13445 BEARING Debris Free, PTFE, 1 9mm


Vacuum tight (~5 Torr), flake free, chemically resistant stirrer bearing makes a mechanical
seal against a polished glass shaft. Debris trap section consists of a PTFE sleeve for a
wide range of joint and shaft diameter sizes. For use with 19mm polished glass or stainless
steel shafts, NOT recommended for PTFE shafts. Bearing consists of a PTFE standard
taper body with added PEEK for better stability, glass filled polypropylene screw cap,
PEEK compression spring, PTFE/PEEK sleeve and a glass filled polypropylene loosening
nut. For use up to 500 rpm.
For Shaft Size, mm
19

13445

Joint
45/50

Order Code
13445-46

Each
329.01

Replacement Seals & Springs:


PTFE/PEEK sleeve seal, for 19 mm
PEEK compression spring, for 19mm

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Order Code
13445-504
13445-506

Each
45.92
54.78

Subject to Ace Discount (Page 4)

Net

205

LA

SS I N N OV

AC E

TH

ON

28mm Shafts, Bearings & Agitators

I
AT

Stirrers, Trubore

A N N I V E R S A R Y

VI

8050 STIRRER BEARING Mechanical Seal, PTFE

Joint Size
45/50
45/50
45/50

Replacement Outside size 128 oring, Pkg. 6

Order Code
8050-08
8050-16
8050-18

Each
667.58
661.28
661.28

7855-773

19.41

8067 BEARINGTrubore, PTFE, AceThred, 28mm


Self-aligning, lubricant-free PTFE Trubore bearing for use with 8080, 28mm polished
glass stirring shaft. Complete consists of PTFE inner Trubore bearing, AceThred glass
adapter (#36 to 45/50), PTFE compression saddle with oring and glass-reinforced PTFE
bushing, and lock nut with FETFE oring. The lock nut permits stirring in either direction
without fear of unthreading. The compression saddle with oring maintains constant force
with little attention. Vacuum down to 1mm Hg. Not recommended for precision ground
glass shafts. For replacement saddle oring, see 7855-739; for bearing size 217 FETFE
oring, see 7855-740.
Order Code
8067-55
8067-58
8067-60
8067-65
5030-78
8067-105

Each
114.72
75.44
21.59
30.45
77.88
320.08

New

8067-105
Bushing 8067-58
Lock Nut 8067-60
Compression
Saddle 8067-65
With FETFE ORing
FETFE ORing
7855-740
PTFE Inner Bearing
8067-55
Thread Adapter
45/50 5030-78

E-SA

ON

FE

PTFE Inner Bearing w/ORing, only


Glass Filled/PTFE Bushing, only
Glass Filled/PTFE Lock Nut, only
Compression Saddle w/ORing, only
Threaded Glass Adapter, 45/50, only
Complete

A ND

OR

Shaft Size, mm
28
25.4
30

EL

8050

AC

Newly designed mechanical stirrer bearing from Ace. All PTFE, Rulon or PEEK wetted
area construction provides for low extractables. Completely contained bearing and
internal parts also provides non-shedding of materials into the reaction. The bearing is
excellent for vacuum applications and can be operated at sub-torr levels. Rated for up
to 400 rpm speeds. It can be used on either glass polished or stainless steel stir shafts.
The 25.4mm size fits Chemglass size shafts.

NJ

1936 2011

N ECT

8067 BEARING/DEBRIS TRAP PTFE, AceThred, 28mm

Order Code
8067-70
8067-58
8067-60
8067-65
8067-72
5846-48
5853-23
8067-75
8067-80

Each
102.42
75.44
21.59
30.45
43.69
38.41
24.36
193.24
529.60

ON

OR

AC

E-SA

FE

PTFE Inner Bearing w/ORing, only


Glass Filled/PTFE Bushing, only
Glass Filled/PTFE Lock Nut, only
Compression Saddle w/ORing, only
PTFE Washer
PTFE Plug, #15
Ace-Safe Connector, #15 x 3/8-inch
Glass Trap Body, only, 45/50
Complete

8067-80

Combination all-in-one stirring shaft bearing and debris trap. Designed to prevent
particles from entering the reaction vessel. Lubricant free PTFE bearing with compression
saddle oring makes a mechanical seal against an 8080 polished glass shaft. Debris
trap section consists of a PTFE washer and particle well. #15 AceThred on glass
body side allows access for clean-out, or may be used for evacuation/gas purge port.
Complete item supplied with glass body, inner PTFE bearing, PTFE bushing and lock
nut, Rulon saddle oring, Ace-Safe connector for 3/8-inch tubing, and PTFE plug.
45/50 bottom joint. For replacement saddle oring, see 7855-739; for bearing size
217 FETFE oring, see 7855-740.

N ECT

NOTE:
Glass Trap Body
is available without side port. Call
or e-mail for
details.

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

206

Stirrers

28mm Rods, Bearings & Agitators


8080 STIRRING SHAFT Polished, Heavy Duty, 28mm
8080

Upper hole
for turbine
agitator located
8 inches from
bottom.

Position can
be changed
to meet your
specifications.

8 inches

Heavy duty, 28mm O.D. glass stirring shaft for use with ACE 6472, 6473 and 6474 reactors.
Shaft has pre-drilled holes at top and bottom for positive attachment to motor coupling
and agitator, respectively. Recommended for use with 8067 PTFE Trubore and 8050
mechanical seal bearings. Use with 8091, 8093, 8101 agitators for 28mm rods. Fits ACE
6472-155 swivel connector and 6472-157 chuck.
For Flask Capacity Length, mm (Inches) Order Code
30L Cylindrical
1,140 (45)
8080-14
50L Low Profile
1,010 (40)
8080-12
50L Cylindrical
1,320 (52)
8080-18
72L & 100L Spherical
1,140 (45)
8080-14
100L Cylindrical
1,470 (58)
8080-22
100L Cylindrical
1,600 (63)
8080-30
200L Spherical
1,400 (55)
8080-24
200L Cylindrical
2,030 (80)
8080-25

Each
402.64
378.55
446.02
402.64
472.33
586.44
458.41
634.97

6472 CONNECTOR Flexible Beam with Pin


Coated steel flex-beam connector, for attaching directly to stir motor drive shaft. Fits
three different standard motor shaft, sizes, (top). Comes with -in stainless steel pin,
(bottom) that attaches to top of 6472-157, 28mm nylon chuck.

6472-159

6472-157

Motor Shaft
Size, in. (mm)
1/2 (12.7)
5/8 (15.9)
3/8 (9.5)

Order Code
6472-155
6472-156
6472-159

Each
55.71
54.09
55.71

6472 CHUCK for 28mm Stir Shaft


Nylon chuck with nylon side pin for connecting to a 28mm glass stir shaft, (8080) to the
6472-155, -156 or -159 flex beam connectors or a 6462 telescoping chuck coupling. Top
hole fits onto 1/2-inch steel pin on 6472 flex beam or 6462 telescoping couplings.
Nylon Chuck
Order Code
6472-157

Replacement Nylon Side Pin


Each
89.89

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Order Code
6472-158

Each
13.58

Subject to Ace Discount (Page 4)

Net

Stirrers

207

28mm Shafts, Bearings & Agitators


8091 AGITATOR PTFE, Large Scale, Multi-Paddle, 28mm
A four-blade, multipaddle agitator, used at lower end of 8080, 28mm stirring shaft.
Supplied with PTFE bolt and nut for securing to 8080 shaft to prevent detachment during
operation. Blades on code -34 are 140mm (5.5 inches) long; on code -36 they are 178mm
(7 inches) long x 6.35mm (.25inch) thick. The increased length and depth of the blades
imparts more energy to the load. NOT supplied with shaft.
Complete
For Flask Capacity
72L & 100L Spherical
200L Spherical; 30L,
50L, 100L & 200L
Cylindrical

8091-34, -36

Replacement Nut & Bolt

Order Code
8091-34

Each
616.11

8091-36

613.84

Order Code

Each

8091-134

61.29

8093 AGITATOR PTFE, Large Scale, Turbine, 28mm


A four-blade, 45-degree-pitch, turbine-type agitator, used at upper section of 8080,
28mm stirring shaft. Supplied with PTFE bolt and nut for securing to 8080 shaft to
prevent detachment during operation. Blades on code -25 are 140mm (5.5 inches) long,
overall; on code -35 they are 152mm (6 inches) long, overall x 6.35mm (.25-inch) thick.
The increased length and depth of the blades imparts more energy to the load. NOT
supplied with shaft.
Complete
For Flask Capacity
100L Spherical
100L & 200L Spherical;
30L, 50L, 100L & 200L
Cylindrical

Replacement Nut & Bolt

Order Code
8093-25

Each
583.27

8093-35

628.06

Order Code

Each

8093-125

59.17

8093-25, -35

8101 AGITATOR PTFE, Multi-Paddle with Receptacle, 28mm


PTFE bottom agitator for large reactors. Multi-paddle solid assembly fits 8080, 28mm
glass shafts. Agitator is attached to the shaft by a PTFE bolt. The bottom of the center
piece is bored out to receive the pin from the 6482 flush seal valve. This agitator when
coupled to the 6482 valve greatly reduces flexing or wobble from the shaft. Each blade on
-28 is 180mm full length. Blades on 38 are 203mm overall length. Order shaft separately.
Complete

New

8101

Replacement Nut & Bolt

Size, mm
180

Order Code
8101-28

Each
583.27

203

8101-38

628.06

Order Code

Each

8093-125

59.17

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

208

Stirrers, Trubore

Trubore Stirrer Accessories

Use the ACE flexible shaft for added convenience and safety
Safer

when stirring corrosive liquids


Safer when stirring liquids with explosive vapor
Available in two lengths

Safety and
convenience
at your
fingertips!

Flexible Shaft
8081

8081 FLEXIBLE SHAFT

ADAPTER (G)

Fully flexible drive shaft connects the motor to any


size or type of reactor stir shaft. Designed with a ball
bearing motor coupling at one end, for connection to
any motor with an 8mm (5/16-inch) diameter shaft.
HANDPIECE (B)
The other end has a detachable handpiece with
an 8mm round aluminum pin adapter (808124) for
connection to our 8124 chucks (supplied separately).
The handpiece can be supported by a standard
lab clamp or hand held. The shafts operate up to
FLEXIBLE SHAFT (A)
14,000 rpm. Shafts should run in a counter-clockwise
direction. Typical torque ratings: sharp bend in shaft,
(4inch loop) 4.7 Kgcm, (4in-lbs). Straight shaft
28Kgcm, (24in-lbs). Shafts measure approximately
91.4cm, (36inches) or 152.4cm, (60 inches) with
handpiece and motor coupling attached. Optional
adapter 8081-27 allows for connection to motors
with 9.5mm (3/8-inch) O. D. shaft. Operating and lubrication instructions included.
Complete units consist of: either shaft A -8081-05 or shaft A-1, 8081-06, motor
coupling for 8mm motor shaft, 8081-12, handpiece with 1/4-inch collett and adapter,
chuck wrench, and key chain.
MOTOR
COUPLING (C)

8124 CHUCK Flex-Grip, Light Weight


Nylon chuck for use with 8081 flexible shaft and with
stirring shafts or other shafts of approximately the same
dimensions. Chuck has flexible insert that allows for
misalignment of stirring shaft without danger of breakage.
Fits standard 5/16-inch motor shaft or flexible shaft.
Order
Code

Size
For Stirring Shafts
approximately 6mm 8124-07
For Stirring Shafts
approximately 10mm 8124-10
For Stirring Shafts
approximately 19mm 8124-15

Each

(A) Flexible shaft only, 91.4cm


(A-1) Flexible shaft only, 152.4cm
(B) Handpiece with 8mm adapter (G), with 1/8-inch
and 1/4-inch collet, only
(B-1) Handpiece with chuck wrench with key and
chain (E), only
(C) Motor coupling for 8mm shaft, only
Complete, 91.4cm (consists of A, B, C & E)
Complete, 152.4cm (consists of A-1, B, C & E)

37.51

Additional Parts:

43.92

(E)
(F)
(G)

152.25

Chuck

(H)

Chuck wrench with key and chain


Shaft lubrication, 30mL
Adapter, handpiece
Adapter, connecting (3/8-inch O.D. motor shaft
to motor coupling)

Order
Code
8081-05
8081-06
8081-08

Each
46.58
87.61
115.42

8081-07 101.21
8081-12
8081-30
8081-32

21.96
187.03
228.99

8081-15
8081-19
8081-24
8081-27

4.46
6.67
14.21
14.11

8117 STIR-LUBE ACE Trubore, Stirrer Lubricant


8117

A superior, low melting, silicone-base lubricant which liquifies at body temperature.


Because of its composition, you need apply only a very thin film of Stir-Lube to a stirring
shaft to increase bearing and shaft life at least three times over that of bearing lubricated
with glycerine. Non-cooled ACE bearing can be operated at 1500 rpm and water-cooled
bearings up to 2000 rpm for many hours with negligible wear.
Size, grams
28 (1 oz.)
113 (4 oz.)

Order Code
8117-10
8117-20

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Each
20.34
64.93

Subject to Ace Discount (Page 4)

Net

Stirrers

8118 LUBRICANT Stopcock

209

8118

A smooth, stable, odorless petroleum based (no silicone) lubricant for lubricating joints
and stopcocks. Melts at 52C (125F). Can be removed with Xylene.
Size, grams
75 (2.65 oz.)
75 (2.65 oz.)

Qty.
1
6

Order Code
8118-10
8118-10

Each
44.58
240.72

8119 HI-LUBE Heavy-Duty Liquid Stirrer Lubricant


ACE chlorofluorocarbon grease for use at speeds up to 6000 rpm with ACE standard
glass assemblies. Use 8040 water-cooled type bearing for long-time stirring (over one
hour). Below one hour, 8038 type may be used at 1500 rpm; eight hours at 1000 rpm.

8119

High chemical inertness unaffected by strong acids and alkalis. Soluble in most
organic solvents. Suitable for use with oxidizing gases.
High heat resistance thermally stable up to 260C (500F). Non-flammable; does not
carbonize on decomposition. 30mL size.
Order Code
8119-07

Each
28.19

8111/8112 ALUMINUM PACKING BOX for 10mm or 19 mm


10mm size designed to be used with 8051 and 8133 bearings; 19 mm with 8060 or 8061
bearings s upplied with PTFE packing. For replacement packing, see 8122.
For Shaft Size
10 mm
19 mm

Order Code
8111-10
8112-10

Each
147.99
184.14

8111
8112

Photochemical Equipment
ACE Photochemical Reactors
are ideal for:
Environmental Applications
Product Aging Tests

P.O. Box 688


Vineland, NJ 08362-0688

Polymerization
Catalysis
Photo-oxidation
Nanotechnology
Toll-free:

800-223-4524

Toll-free fax:

800-543-6752

856-692-3333 Fax: 856-692-8919

www.aceglass.com

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210

Stirrers

8115 KRYTOX GPL Fluorinated Grease


Superior performance, non-contaminating, nonflammable, general purpose grease.
Excellent as a glass bearing lubricant, as a super-inert grease for stopcocks and joints,
as a high temperature grease in baked-out vacuum systems, or on distillation column
joints because it is insoluble in almost all solvents except Freon 113. Easy removal with
fluorinated solvents.
CHEMICAL STABILITY
Krytox GPL grease has demonstrated an exceptional degree of inertness when contacted
with a wide range of reactive chemicals. There is no reaction with the following chemicals:
oxygen caustic fluorine hydrazine diethylene triamine hydrocarbons
chlorine hydrogen ethanol hydrogen peroxide phosphoric acid
red fuming nitric acid sulfuric acid methanol aniline ammonia
hydrochloric acid unsymmetrical dimethyl hydrazine
THERMAL STABILITY
Krytox GPL can be used at operating temperatures up to 204C (400F) for extended
periods of time and at 290C (550F) intermittently. Approximate minimum use
temperature is -35F.
*Reg. U.S. Pat. & Tm. Office, DuPont Company. Fluorinated Greases are made only by DuPont.
Size
2 oz.

Order Code
8115-08

Each
59.40

8116 KRYTOX LVP High Vacuum Grease


Very low vapor pressure, highly inert, nonflammable grease. The grease for high-vacuum
systems. Superior performance in laboratory and pilot plant equipment, as a lubricant
and sealant for stopcocks, valves, fittings and orings operating at high vacuum or in
hostile environments.
8115/8116

DESCRIPTION
Krytox LVP high vacuum grease is a combination of an extremely low vapor pressure
perfluoroalkylpolyether oil and a fluorocarbon resin thickener. This white, buttery grease
is designed to lubricate the fittings and accessories of high vacuum systems at operating
temperatures down to 10-12 torr at 20C (1.33 x 10-13 kPa).
The optimum useful temperature range of Krytox LVP is -20 to 260C (-5 to 500F).
PROPERTIES
Krytox LVP high vacuum grease has the following important properties:
Very low vapor pressure
High degree of chemical inertness
Excellent lubricating properties
Complete nonflammability
Compatibility with metals, plastics and elastomers
Excellent oxidation and thermal stability
Vapor Pressure: torr at 20C 1 x 10-13; torr at 200C 1x 10-5
*Reg. U.S. Pat. & Tm. Office, DuPont Company. Krytox LVP is made only by DuPont.
Size
2 oz.

Order Code
8116-10

Each
105.04

8122 STIRRER PACKING


PTFE packing for use in 8112 stuffing boxes. This material conforms readily to the contour
of the stuffing box and shaft.
8122

For Shaft Size, mm


10
19

Qty. Per Jar


6
1

Order Code
8122-10
8122-40

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Per Jar
81.13
16.13

Subject to Ace Discount (Page 4)

Net

211

Stirrers

8125 SHAFT COUPLINGStirring


Couples stir motor shaft to reactor stir shaft. Flexible neoprene rubber body with
PTFE sleeve inside corrosion-resistant metal end that provides angular and parallel
misalignment of glass or metal stirring shaft without danger of breakage. Rubber body
absorbs shock and provides quiet vibration free running with great torsional stiffness.
Measures four inches overall.
Easy to Use: (1) Slip coupling end with PTFE sleeve over stirring shaft as far as it will go,
approximately three inches.

(2) Bring motor shaft down and align visually approximately 1/2-inch above coupling and shaft. Secure motor position and recheck alignment.

(3) After motor and reactor are securely in place, slide coupling over motor shaft
and tighten set screw.

(4) Slide stirring shaft up into coupling just enough to clear bottom of reactor.
Tighten PTFE sleeve over shaft, using brass set screw, just enough to prevent
slippage.
For 10mm Stirring Shaft
For Motor Shaft
Order
Size, in.
Code
Each
1/4
8125-06 43.53
5/16
8125-08 43.53
3/8
8125-11 43.53
1/2
8125-13 43.53

Motor

PTFE Sleeve

Shaft Size

4"

8125

For 19mm Stirring Shaft


For Motor Shaft
Order
Size, in.
Code
Each
3/8
8125-21 72.94
1/2
8125-25 72.94
5/8
8125-27 72.94
3/4
8125-29 80.00

8124 CHUCK Flex-Grip, Light Weight


Nylon chuck for use with 8081 flexible shaft and with stirring shafts or other shafts
of approximately the same dimensions. Chuck has flexible insert that allows for
misalignment of stirring shaft without danger of breakage. Fits standard 5/16-inch
motor shaft or flexible shaft.
Size
For Stirring Shafts approximately 6mm
For Stirring Shafts approximately 10mm
For Stirring Shafts approximately 19mm

Order Code
8124-07
8124-10
8124-15

8124

Each
37.51
43.92
152.25

8126 STIRRING SHAFT COUPLING


Universal swivel coupling for connection to stir motor metal chuck. Compression
connection secured via Allen screw for attaching various O.D. glass shafts.
For Glass
Rod O.D., mm
6
8, 9
10
19

Motor Coupling
O.D. (Inches)
1/4
1/4
1/4
3/8

Order Code
8126-05
8126-08
8126-10
8126-19

8126

Each
95.17
106.94
106.94
113.26

8127 COLLARwith PTFE Gasket


Designed to be used with 8068, 8070, 8071, 8074 or 8078 stirring shafts. Handy for
positioning shaft in bearing, and preventing shaft from dropping into flask. Supplied with
PTFE gasket to prevent scratching top of bearing and to act as dust cover.
For Rod Size, mm
Type
10
Glass-Filled/PTFE
19
Glass-Filled/PTFE
28
Glass-Filled/PTFE
10
Stainless Steel
19
Stainless Steel
28
Stainless Steel

Order Code
8127-10
8127-20
8127-28
8127-42
8127-43
8127-44

Each
24.66
36.68
73.09
26.57
42.38
80.60

8127-10

8127-42

New

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

212

Stirrers

8128 GASKET PTFE, Flat


Designed to fit 8068, 8070, 8071, 8074 or 8078 stirring shafts. Useful as dust cover and
as replacement for gasket supplied with 8127 collar. Twelve to a package.
For Rod Size, mm
10
19
28

Qty.
12
12
12

Order Code
8128-10
8128-20
8128-42

Each
19.81
27.75
42.21

8128

Safety Shields
Ace Glass fabricates safety shields for all four-post style
reactor stands. The shields cover the full height of the stand
for extra safety. Made of high impact, 1/4-inch, clear Lexan,
the three side shields are attached to the stand with stainless
steel fittings and hardware. The door has a positive catch and
handle.
The shields can be placed on both standard wall and
jacketed style reactors. The jacketed style will have holes to
accommodate the chiller inlet/outlet hoses. Make sure you
specify which side, (left or right), will have the chiller hoses.
Since these are custom made and built on each stand, the
shields do not have standard ACE number codes. Just specify
on your requirements and request for quote regarding the
shields as an accessory. The image at left normal set-up for a
10L or 20L stand for a jacketed flask.

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Subject to Ace Discount (Page 4)

Net

Stirring, Mixing

213

13365 AIR STIRRER Light Duty 


Arrow Model A

This small, compact and quiet air motor is ideal for stirring all types of solvents, lacquers,
paints, oils, synthetics, and fine and heavy chemicals where danger of explosion may exist,
as there are no sparks. It is a complete unit, ready for mounting on a laboratory stand. Air
supply of only 30 to 100 PSI is necessary. Variable speeds range from 200 rpm to 10,000
rpm merely by turning the air supply line valve. For bath sizes to 20 liters, this smooth
running unit has little or no service cost. Unit adjusts itself to compensate for wear. The
shaft and propeller are made of stainless steel to resist most acids and chemicals and
for easier cleaning. Will start in most stalled positions with low air pressure and cannot
burn out from overload. Air Motor 0-1/3 hp. at 80 lbs. Coupler and stainless steel shaft
30.5cm overall. Propeller: stainless steel 6.4cm diameter. Shaft is 9.5mm (3/8inch) O.D.
For filter/regulator/lubricator, see 13372. Air consumption = 13 cfm.
Order Code
13365-05

13365-05

Each
357.03

13365 AIR STIRRER Heavy Duty 


Arrow Model G

Specially designed air motor for use on the more viscous materials, provides speed
with power. More constant speed is attained through gear reduction, lowering speed
fluctuations due to changes in air pressure. Speeds range from 50 to 1200 rpm by
merely turning valve on air supply line. This smooth running unit is complete and ready
to mount on laboratory stand. Air supply of only 30 to 80 PSI is necessary. Another
outstanding feature of the unit is the muffler, which provides quiet operation. The shaft
and propeller are stainless steel to resist most acids and chemicals and for easier
cleaning. Service costs are almost nil as the unit adjusts itself to compensate for wear.
Air Motor 0-1/3 hp. at 80 lbs. Gear Ratio 71. coupler and stainless steel shaft
30.5cm overall. Propeller: stainless steel 6.4cm diameter. Shaft is 9.5mm (3/8inch)
O.D. For filter/regulator/lubricator, see 13372. Air consumption = 13 cfm.
Order Code
13365-10

13365-10

Each
489.08

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

214

Stirring, Mixing

13370 AIR STIRRER Heavy Duty, High Torque 


A compact, heavy duty air motor with highly damped muffler. Complete unit consists of
an air hose with a snap coupling on motor end and shut-off valve on the other end. Motor
will develop 1.5 hp. at 90 lbs. air pressure. Speeds are variable from 300 to 3000 rpm. It
consumes approximately 42 cfm at 3000 rpm. Shaft is 12.7mm (1/2-inch) diameter for
use with 8124 chuck, not included. For filter/regulator/lubricator, see 13372.
Order Code
13370-10

13370

Each
411.74

13372 FILTER/REGULATOR/LUBRICATOR
Arrow

13372

Space-saving multiple unit, recommended for use with 13665 and 13370 air motors.
Pressurized air flows through louvered deflector in swirling pattern, with liquids and dirt
falling into lower baffle where they are prevented from re-entering the air stream. Element
removes impurities down to 40 microns. Clean air then passes through precision needle
valve feed mist lubricator that can be filled under pressure. 150 PSI maximum pressure
range is adjustable through spring action of T-handle. Maximum operating temperature
is 125F. Manual drain. Shatter-proof polycarbonate bowls not recommended for use
in atmospheres containing acetone, benzene, carbon tetrachloride, ethylene dichloride,
gasoline or toluene. Inlet and outlet connections are 1/4inch NPT. Supplied complete
with gauge and mounting bracket.
Order Code
13372-45

Each
237.98

13385 GAUGE Pressure


Pressure gauges for monitoring pressure in laboratories; especially suited for use with
the Michel-Miller HP/LPLC system (see our Laboratory Glassware & Equipment Cataog),
pressure reactors (page 23) or other applications when pressure monitoring is necessary.
Available with brass or 316 SS internals. Note: Code -52 is a compound gauge, pressure
and vacuum.
13385-12

13385-44

13385-52

Pressure
Dial Size
Range, psi
(Inches)
0400
2-1/2
0400
2-1/2
060
1-1/2
0160
1-1/2
Full vacuum60
1-1/2

Male npt
Connector (In.)
1/4
1/4
1/8
1/8
1/8

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Internals
Brass
Stainless Steel
Stainless Steel
Stainless Steel
Stainless Steel

Order
Code
13385-12
13385-14
13385-44
13385-48
13385-52

Each
58.50
266.93
171.92
181.80
206.92

Subject to Ace Discount (Page 4)

Net

Stirring, Mixing

Digital or analog/dial speed display

215

RZR
Standard
Series

Two gear stages for high torque at low speeds

Over-load protection reset by power switch

Over-load protection LED display

Designed for power and reliability. Easy to operate, safe, and suitable for continuous operation.
Stirrers are equipped with a maintenance-free brushless D.C. capacitor motor with overheating
protection feature, reset by power switch. Large speed range of 40 to 2000 rpm has a mechanical
speed adjustment and is monitored via a digital speed display on 13501-21 and 13504-41 making
them ideal for reproducible applications; on 13500-10 the speed is adjusted and monitored with
the help of a scaled control knob.
Supplied with 13 mm O.D. x 160 mm long (approximately 1/2-inch x 6.3-inch) motor support rod and
key adjustable metal chuck, .5 to 10.5mm, for metal shafts like ACE 8074, 10mm O.D. (Units feature a
shaft that can be extended through the top to allow variable depth adjustment. To accomplish this,
you need to order 7mm O.D. shafts, see 8126-22 or 8126-24.)
To use 10mm O.D. glass or PTFE shafts, metal chuck should be replaced with ACE 8124-10 or
8124-15 flexgrip chuck.

13500/13501/13504 STIRRERS Heidolph RZR Standard Series


Number of Gears
Speed Range

[rpm]

Speed Display

402000

402000

402000

Analog/Dial

Digital

Digital

Max. Torque

[in-lb]

42.79

42.79

55.63

Torque at 100/1000
rpm

[in-lb]

17.12/1.71

17.12/1.71

24.07/2.35

60,000

60,000

100,000

10

10

20

82 x 206 x 176
3.23 x 8.1 x 6.9

82 x 206 x 176
3.23 x 8.1 x 6.9

82 x 211 x 176
3.23 x 8.3 x 6.9

Max. Viscosity

[cp]

Max. Mixing Vol. (H2O)

[liters]

Dimensions (W x H x D)

mm
in.

Weight

[Kg/lbs]

Input Power*
Motor Input/Output
Heidolph Model
Order Code
Each

[Watts]

3.0/6.62

3.0/6.62

3.3/7.28

115v/60Hz

115v/60Hz

115v/60Hz

50/27

50/27

70/37

2020

2021

2041

13500-10

13501-21

13504-41

1316.02

1659.48

1948.46

13501-21

*230V/50Hz version also available. 13500-10 not pictured.

13504-41

See 8126, 8126-22, and 8126-24 for


pass-through chuck assemblies for
10 & 19mm stir shafts.
Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

216

Stirring, Mixing

RZR Control
Electronic
Series

Digital speed display

Two gear stages for constant speed

Overheating protection self reset

Over-load protection LED display

Similar to Standard Series, except with added features such as constant power. The
electronic automatic control allows almost constant torque over respective speed range.
The two-stage gear provides excellent mixing results even in highly viscous media, using
only as much energy as actually needed. The speed desired is kept constant under changing
loads, even in overload mode. (Power can be increased for a limited time to 175% or 200%,
so there is no premature cutoff when overloaded.)
Changes in viscosity during the process can be followed via a digital display of the torque
on both 13507 and 13511. Also, both models are equipped with an analog interface enabling
output of speed and torque reading to an external device (such as a chart recorder), or
specification of the desired speed via PC. Analog speed and torque output, along with
computer controllability (speed), is 0-10 V/4-20 mA. See 8126-22 or 8126-24 adjustable
pass-through chuck assemblies.

13507/13511 STIRRERS  Heidolph RZR Control Series


Number of Gears

502000

12400, 602000

Speed Display

Digital

Digital

Torque Display

Digital

Digital

Speed Range

13511-02

[rpm]

Controller Response

Constant rpm under changes in viscosity

Overload Response

Constant rpm under overload

Max. Torque (continuous/limited)

[in-lb]

13.91/31.02

27.81/48.14

Torque at 100/1000 rpm

[in-lb]

13.37/2.67

26.74/5.35

up to 200%

up to 200%

10,000

100,000

Power Reserve under Overload


Max. Viscosity

[cp]

Max. Mixing Volume (H 0)


2

Dimensions (W x H x D)
Weight

[Liters]

20

40

mm
in.

72 x 206 x 176
3.23 x 8.1 x 6.9

82 x 211 x 176
3.23 x 8.3 x 6.9

[Kg/lbs]

2.8/6.17

3.7/8.16

115v/60Hz

115v/60Hz

80/50

140/100

Input Power*
Motor Input/Output

[Watts]

Heidolph Model
Order Code
Each

2051

2102

13507-51

13511-02

2363.71

3995.45

*230V/50Hz version also available. 13507-51 not pictured.

13507-51 is ideal for use with our Auto-Reactors


and ROBO Reactors.

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Subject to Ace Discount (Page 4)

Net

217

Stirring, Mixing

Three State-of-the-Art Laboratory Stirrers


Totally enclosed, non-ventilated,
permanent magnet D.C. motor
for long service life
Eye level, heavy cast aluminum
control box integrated with
motor for safe and easy
operation of stirrers
Control knob electronically
regulates speed of application
required
O v e r l o a d p r o t e c t i o n a
m a n u a l l y re s e t a b l e c i rc u i t
breaker for total safety

On/Off switch for quick stopping


if necessary
Stirrers come complete as
shown, including 9/16-inch dia.
x 10 inches long aluminum
support rod
10 0 % b a c k e d b y t h e b e s t
guarantee in the business:
30-day satisfaction guarantee
Six-month unconditional
guarantee

Not supplied with shaft, propeller or coupling.


For stainless steel shaft, propeller and coupling, order 13542-60.
For glass shafts, agitators and coupling, see 80688124.

13544

13542

13543

13542 STIRRER Laboratory, Heavy Duty, Variable Speed


Handles high viscosity fluids up to 4400 cps in 5-gallon batch or up to 100L water
Variable speed up to 1000 rpm, gear head
Constant torque throughout speed range is 7.35 in-lbs.
1/10 hp motor operates at 120 VAC, 60 hz
Motor shaft is 3/8-inch (9.5 mm)
Order Code
13542-25

Each
737.95

11082 CLAMP

Power Hold

Fits stirring stand with 3/8-inch


to 5/8-inch diameter shaft and
stirrers with mounting rod from
3/8-inch to 5/8-inch diameter.
Stop collar included.

13543 STIRRER Laboratory, Light Duty


Handles watery to light syrupy mixtures, or up to 20L water
Variable speed up to 6000 rpm, direct drive
Constant torque throughout speed range is 1.05 in-lbs.
1/10 hp motor operates at 120 VAC, 60 hz
Motor shaft is 3/8-inch (9.5mm)
Order Code
13543-12

Optional Accessory

Order
Code
11082-07

Each
54.12

Each
555.88

13544 STIRRER Laboratory, Medium Torque, Variable Speed


Handles light to syrupy mixtures, or up to 100L water
Variable speed up to 2000 rpm, direct drive
Constant torque throughout speed range is 2.43 in-lbs.
1/15 hp motor operates at 120 VAC, 60 hz
Motor shaft is 3/8-inch (9.5mm)
Order Code
13544-20

Each
582.32

SPECIFICATIONS
Model #

Type

Speed Range

Constant Torque

Motor

Power

Shipping Wgt.

13542-25

Gear Head

to 1000 rpm

7.35 in-lbs

1/10 HP

120 VAC

8 lbs.

13543-12

Direct Drive

to 6000 rpm

1.05 in-lbs

1/10 HP

120 VAC

8 lbs.

13544-20

Direct Drive

to 2000 rpm

2.43 in-lbs

1/15 HP

120 VAC

8 lbs.

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

218

Stirring, Mixing

13514/13516 STIRRERDigitalLa

oratory stirrer designed for simple tasks for quantities from

25L to

Laboratory stirrer designed for simple tasks for quantities from 25L to 40L of water. It
automatically adjusts the speed through microprocessor controlled technology within
the speed range of 0/30 to 2000 rpm. Safety circuits installed ensure automatic cut-off
in anti-stall or overload conditions. Continuous comparison of shaft speed to desired
speed is maintained and variations adjusted automatically. This guarantees a constant
speed even with changes in viscosities of the sample. Two-year manufacturers warranty.

Order Code
Price (each)
Stirring Quantity Max (H2O)
Speed Range
Viscosity Max
Setting Accuracy Speed
Weight
Chuck Range (Dia.)
Electrical Input
Output Max. (at Stir Shaft)
Torque Max. (at Stir Shaft)

13514-10 Eurostar 40

13516-20 Eurostar 60

1171.00
25L
0/30-2000 rpm
30000 mPas
1 rpm
4.4 kg
0.5-10 mm
115V, 50/60Hz
84 W
40 Ncm

1301.00
40L
0/30-2000 rpm
50000 mPas
1 rpm
4.4 kg
0.5-10 mm
115V, 50/60Hz
126 W
60 Ncm

IKA motors are available in 230v versions.

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Subject to Ace Discount (Page 4)

Net

Stirring, Mixing

13517/13518 STIRRER Removable Wireless Control

219

oratory stirrer designed for

simple tasks for quantities from 25L to

Universal laboratory stirrer designed with a removable wireless controller and a digital TFT
display. It automatically adjusts the speed through microprocessor controlled technology
with the speed range of 0/30 to 2000 rpm. The stirrer comes equipped with a RS232 and
USB interface to control and document all parameters. An integrated torque trend display
is provided for the measurement of viscosity changes. Safety circuits installed to ensure
automatic cut-off in anti-stall or overload conditions. Two-year manufacturers warranty.

Order Code
Price (each)
Stirring Quantity Max (H2O)
Speed Range
Viscosity Max
Setting Accuracy Speed
Weight
Chuck Range (Dia.)
Electrical Input
Output Max. (at Stir Shaft)
Torque Max. (at Stir Shaft)

13523 STIRRER Mechanical

13517-30 Eurostar 60

13518-02 Eurostar 100

1483.00
40L
0/30-2000 rpm
50000 mPas
1 rpm
4.7 kg
0.5-10 mm
115V, 50/60Hz
126 W
60 Ncm

2538.00
100L
0/30-2000 rpm
70000 mPas
1 rpm
4.7 kg
0.5-10 mm
115V, 50/60Hz
136 W
100 Ncm

oratory stirrer designed for simple tasks for quantities from 25L to

Powerful, mechanically controlled stirrer with LED digital display. Suitable for quantities
up to 20 l (H2O) for use in laboratories and pilot plant stations. Two speed ranges within
60-2000rpm, for highly viscous media and intensive mixing. Push-through mixing tools.
Special motor overheating protection by means of self-locking temperature limiter.
Two-year manufacturers warranty.

Order Code
Price (each)
Stirring Quantity Max (H2O)
Speed Range
Viscosity Max
Setting Accuracy Speed
Weight
Chuck Range (Dia.)
Electrical Input
Output Max. (at Stir Shaft)
Torque Max. (at Stir Shaft)

13523-10
730.00
20L
60-2000 rpm
10000 mPas
1 rpm
3.1 kg
0.5-10 mm
100V, 50/60Hz
26 W
150 Ncm

*Contact ACE regarding IKA Labworld software.

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

220

Stirring, Mixing

13565-05 STIRRER O
 verhead, Digital

BDC6015

Rugged Ultra-Speed Model with range from 40-6000 rpm. Microprocessor controlled brushless
DC motor with automatic overload protection. Digital display of RPM and torque. Keypad
adjustable. Maintains set speed as viscosity changes. 2-speed transmission selects hi-torque
or hi-speed range. Adjustable steel chuck with hinged chuck guard. 120V version UL and CSA
approved. A 230V (CE approved) version is available via special order. Threeyear warranty.

Specifications:
MODEL
Low Speed Range
High Speed Range
Maximum torque (low speed range)
Maximum torque (high speed range)
Speed Accuracy
Torque Accuracy
Electrical Input
Output Power
Weight
Chuck
Maximum Volume
Maximum Viscosity

New

Order Code
13565-05

13565-05 / BDC6015
401200 rpm
1200-6000 rpm
170 N-cm (15 in-lbs)
34 N-cm (3 in-lbs)
+/- 1% of reading or +/- 1 rpm
+/- 5% of reading or +/- 1 in-lb
120V, 50/60 Hz, 5 Amps
1/5 Hp, 150W
11 lbs (5 kg)
accepts up to 3/8-in (10.1mm) shafts
6.6 US Gallons (25 Liters)
20,000 cps

Each
1740.31

approved.

13565-10 STIRRER O
 verhead, Digital

BDC3030

Universal Model with all the specifications and features of the BDC 6015, except with lower
speed range (20-3000 rpm). Three-year warranty.
13565
Specifications:

ful

er
Pow

MODEL
Low Speed Range
High Speed Range
Maximum torque (low speed range)
Maximum torque (high speed range)
Speed Accuracy
Torque Accuracy
Electrical Input
Output Power
Weight
Chuck
Maximum Volume
Maximum Viscosity
Order Code
13565-10

13565-10 / BDC3030
20600 rpm
600-3000 rpm
339 N-cm (30 in-lbs)
68 N-cm (6 in-lbs)
+/- 1% of reading or +/- 1 rpm
+/- 5% of reading or +/- 1 in-lb
120V, 50/60 Hz, 5 Amps
1/5 Hp, 150W
11 lbs (5 kg)
accepts up to 3/8-in (10.1mm) shafts
15.8 US Gallons (60 Liters)
50,000 cps

Each
1740.31

approved.

Caframo motors are available in 230v versions.

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Subject to Ace Discount (Page 4)

Net

Stirring, Mixing

13566 STIRRER Overhead, Reversing, Digital

221

BDC2010

The 2010 has a rugged DC brushless motor that delivers from 40-2010 RPM. This model
has a small footprint and is loaded with features such as Stirlight which lights a downward
beam of light into the mixture, timer, reverse feature and xRx agitation for a controllable
vortex effect, automatic overload protection and maintains speed at all viscosities. The
2010 is the only stirrer of its kind and can be set up for automatic time and auto-reverse
for better mixing. Three-year warranty.

New
13566

Specifications:
MODEL
Speed
Timer
Maximum torque
Electrical Input
Output Power
Weight
Chuck
Maximum Volume
Maximum Viscosity
Order Code
13566-05

13566-05 / BDC2010
402010 rpm (clockwise and/or counterclockwise
Set from 1-2000 minutes (33.3 hours)
100 N-cm (8.8 in/lbs)
100-240V, 50/60 Hz
1/10 Hp, 70W
8.2 lbs (5.6 kg)
accepts up to 3/8-in (10.1mm) shafts
6.6 US Gallons (25 Liters)
20,000 cps
Each
1218.00

approved.

rse!

Reve
Auto

13565 STIRRER Overhead 

BDC1850

Compact size and powerful overhead stir motor. Rugged stir motor that delivers 12-1800
rpm with 1/5 horsepower DC brushless motor. Digital display of RPM and Torque. Keypad
adjusts speed and rotation. Set speed is automatically maintained and adjusts to torque
changes. 120V CSA and UL approved. Three year warranty. Also available in a 230V version.
Comes with adjustable chuck, chuck protective cover.

New

Specifications:
MODEL
Low Speed Range
High Speed Range
Maximum torque (low speed range)
Maximum torque (high speed range)
Speed Accuracy
Torque Accuracy
Electrical Input
Output Power
Weight
Chuck
Maximum Volume
Maximum Viscosity
Order Code
13565-20

13565-20 / BDC1850
12360 rpm
360-1800 rpm
565 N-cm (50 in-lbs)
113 N-cm (10 in-lbs)
+/- 1% of reading or +/- 1 rpm
+/- 5% of reading or +/- 1 in-lb
120V, 50/60 Hz, 5 Amps
1/5 Hp, 150W
11 lbs (5 kg)
accepts up to 3/8-in (10.1mm) shafts
21 US Gallons (80 Liters)
90,000 cps

13565

Each
1740.31

approved.

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222

Stirring, Mixing

13554 STIRRING MOTOR* AND CONTROLLER Pilot Plant,


for Hazardous Area (Motor Only)

* UL Classified:
Hazardous motors only
Class I, Div. I, Group D
Atmospheres
(Flammable Gases or Vapors)
Class II, Div. I, Group F & G
(Combustible Dust)

MOTOR: For hazardous area*, heavy duty, 1/4 or 1/2 hp, permanent magnet, DC
reversible, 90 volt DC armature type. This 56C base frame, continuous duty, ball bearing,
totally enclosed fan cooled (XPFC) motor has a variable speed range up to 1750 rpm.
Operates at a maximum temperature of 40C. With 5/8-inch O.D. motor shaft. Supplied
with 30-foot cord with mating twistlock cap. Overall length: code -40 is 10-1/2 inches;
code -50 is 12-3/4 inches. Maximum torque rating: code -40 is 9.1 in-lbs.; code -50
is 18.3 in-lbs., NEMA C-face. Shipping weight: code -40 is 34 lbs.; code -50 is 50 lbs.
CONTROLLER: Converts 120 volts AC to 90 volts DC. Supplied with 6-foot cord to a
twistlock connector for connection to motor. (NOTE: controller should be mounted remote
of hazardous area). NEMA classification 4/12 (water and dust proof for industrial use).
Maximum speed preset at factory at 900 rpm for safety, can be increased or decreased
internally, see instructions. Also has torque and current limit adjustments, all factory set.
Use 6472-872 mounting plate when using with some reactors. Use offset
adapters when using this motor with 6472 reactors to move condenser, etc.,
away from motor mount.
Motor, 1/4 hp, only
Controller, only
Complete, 1/4 hp

Order Code
13554-40
13554-24
13554-45

Each
1577.48
1092.92
2670.40

Motor, 1/2 hp, only


Controller, only
Complete, 1/2 hp

13554-50
13554-26
13554-55

2276.62
1092.92
3369.54

13554-45, -55

13554 STIRRING MOTOR AND CONTROLLER Pilot Plant

MOTOR: Non-hazardous area, heavy duty, 1/4 or 1/2 hp, permanent


magnet, DC reversible, 90 volt DC armature type. This 56C base frame,
continuous duty, ball bearing, totally enclosed fan cooled (TEFC) motor
has a variable speed range up to 1750 rpm. Operates at a maximum
temperature of 40C. With 5/8-inch O.D. motor shaft. No UL classification.
Supplied with 30-foot cord with mating twistlock cap. Overall length: code
-05 is 10-1/2 inches; code -09 is 12-1/2 inches. Maximum torque rating:
code -05 is 9.1 in-lbs.; code -09 is 18.3 in-lbs., NEMA C-face. Shipping
weight: code -05 is 17 lbs.; code -09 is 25 lbs.

13554-07, -10

CONTROLLER: Converts 120 volts AC to 90 volts DC. Supplied with


6foot cord to a twistlock connector for connection to motor. (NOTE:
controller should be mounted remote of hazardous area). NEMA
classification 4/12 (water- and dust-proof for industrial use). Maximum
speed preset at factory at 900 rpm for safety, can be increased or
decreased internally, see instructions. Also has torque and current
limit adjustments, all factory set. See listing below of offset adapters
necessary for use when using this motor with 6472 reactors. Use 6472872 mounting plate when using with some reactors.

IMPORTANT:
The controller and connectors
between controller and motor
should be in line of sight of the
motor. DO NOT disconnect
controller from motor while
operating or when controller is
powered; damage to motor or
controller could result.

Motor, 1/4 hp, only


Controller, only
Complete, 1/4 hp

Order Code
13554-05
13554-24
13554-07

Each
718.72
1092.92
1811.64

Motor, 1/2 hp, only


Controller, only
Complete, 1/2 hp

13554-09
13554-26
13554-10

765.49
1092.92
1858.41

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

OFFSET ADAPTER, only


Joints
24/40
29/42
45/50

Order Code
5268-10
5268-15
5268-21

Each
36.56
40.74
109.58

Subject to Ace Discount (Page 4)

Net

Stirring, Mixing

13557 STIRRING MOTOR AND CONTROLLER Offset,

223

13557
Hazardous Duty

Hazardous Duty Series

Stirring motor, controller and right-angle, off-set drive. Same motor and analog
controller as 13554 hazardous area unit except complete with right-angle
drive gear box.
Analog, 1/4 horse power, complete
Analog, 1/2 horse power, complete

Order Code
13557-110
13557-120

Each
3322.37
4021.51

Stirring motor, controller and right-angle, off-set drive. Same motor and controller
as 13554 hazardous area unit except complete with right-angle drive gear
box and digital control.
Digital, 1/4 horse power, complete
Digital, 1/2 horse power, complete

Order Code
13557-220
13557-240

DIgital Controller

Each
4021.01
4779.56

13557 STIRRING MOTOR AND CONTROLLEROffset,


Standard Duty Series

Analog Controller

13557
Standard Duty

Stirring motor, controller and right-angle, off-set drive. Same motor and analog
controller as 13554 standard unit except complete with right-angle drive
gear box.
Analog, 1/4 horse power, complete
Analog, 1/2 horse power, complete

Order Code
13557-310
13557-320

Each
2463.61
2510.38

Stirring motor, controller and right-angle, off-set drive. Same motor and controller
as 13554 standard unit except complete with right-angle drive gear box and
digital control.
Digital, horse power, complete
Digital, horse power, complete

Order Code
13557-420
13557-440

Each
3206.93
3299.45

DIgital Controller
Analog Controller

13557 GEAR BOX Fits Both Standard & Hazardous Duty Series
Right-angle drive 5:1 gear box only. Bolts directly to motors with a 5/8-inch diameter shaft.
For 1/4 or 1/2 horse power motors

Order Code
13557-10

Each
651.97

13557-10

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

224

Stirring, Mixing

8135 GEAR BOX Right Angle Side Drive


Right-angle, side drive gear box. Has 9-inch long aluminum support rod for attaching
to a clamp holder or flex-frame. Polished aluminum case. 10mm stainless connecting
rods on in/out drive. Can easily be used with ACE 8081 Flex-Shaft and either 812610
or 8124 chucks. Using a flex shaft allows for use with any stir motor.

8135

Order Code
8135-10

Each
831.74

New

13555 STIRRING MOTOR/CONTROLLER Digital, Haz Mat Series

New

Heavy-duty, 1/2 HP stirrer motors complete with the digital Microdrive


control box. The low-power, AC variable speed drive has a compact design
and is available in switched or non-switched enclosures. Its IP-55/NEMA 12
rating makes it ideal for use harsh environments. Control box is dust tight
construction. Easy to read LED display and flat panel controls. Controller is
wall or stand mountable. Control box has 12-ft cord to motor and control
box to plug cord is 24-ft long.
Motor is 230V 3-phase, 60Hz, which is wired to the Microdrive which steps
down to and is 115V, 50Hz. Sold complete only.
1/2 HP motor with Microdrive controller

13555

Each
3261.08

13557 GEAR REDUCER 56C Flange, 4:1 Reduction

New

In-line, offset 4:1 gear reducer. Top 56C flange accepts 13554 motor with 5/8-inch diameter
shaft. Bottom has 56C flange with 5/8-inch diameter shaft. Shaft is offset approximately
1-5/8 inches. Flange face-to-face distance is approximately 4-3/4 inches. Can be used
on new or existing reactor motor mounts to increase torque of reactor agitation system.
Order Code
13557-20

13557-20

Order Code
13555-50

Each
662.52

New

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Subject to Ace Discount (Page 4)

Net

Stirring, Mixing

225

13532 DUAL MOTOR SPEED & POWER CONTROLLER Solid State


Similar to 13530, but with buffered load control and DC filtration to provide more torque
at higher speeds and a higher top speed than motor rating.
Ratings: AC three-prong output socket, standard NEMA type, 1200 watts. 0-120 volts,
variable, 60 Hz. maximum 10 amps. DC four-prong output socket, cinch type. 360
watts, 0-150 volts, variable, filtered approximately 1/2 hp. maximum three (3) amps.
A compact 8.9 x 8.9 x 17.8cm (3-1/2 x 3-1/2 x 7 inches), lightweight 1 Kg. (2-1/4 lbs.)
solid state control with rugged control regulation and rectification circuitry. Two output
sockets AC and DC which work in conjunction. Fwd-Off-Rev. DC control switch only.
Fused for AC and DC outputs, 10 amps and three (3) amps respectively. Rear ring stand
clamp for easy mounting and access. Light blue modern type case with protective finish.
Red pilot light. Large dial plate with 0-100 divisions. Red control knob with Click-Off.
Heavy duty 1.8 meter neoprene, three-wire power cord with NEMA plug.
Uses AC output socket, rear mounted: Heating mantles Universal motors Hot plates
and heating baths Incandescent lighting, resistive loads Most loads accept 120v AC
up to 10 amps functions comparable to the autotransformer.

13532
Use of 13649 motor (page 221) is
recommended with this controller.

DC output socket, front mounted: Four-conductor output socket for DC reversible series
wound motors Plug supplied with instructions to obtain a DC output of 0150 volts
variable, maximum current three (3) amps at 360 watts.
Order Code
13532-10

Each
623.28

13586 SUPPORT STAND


All-stainless-steel support stand. Heavy base, six pounds, can accommodate vessels
up to 18 inches in diameter within its U shape. Support rod is 5/8-inch diameter,
approximately 29 or 36 inches high, fastened to base with stainless steel lock nuts. Two
additional threaded holes in base legs to accommodate extra support rods. Complete
item consists of one base and one rod.
13586

Stand complete with support rod


Rod Height (Inches)
28
36

Order Code
13586-10
13586-13

5/8-Inch Stainless Steel Support Rod, only


Rod Height (Inches)
Order Code
60
28
36

13586-15
13586-25
13586-27

Each
274.82
313.93
Each
181.78
104.64
133.18

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

226

Stirring, Mixing

13649 STIRRER Laboratory, Solid State


Totally enclosed, 1/40 hp., permanent magnet motor with dual 8mm (5/16-inch) armature
and gear shafts with milled flats. Armature shaft with maximum speed of 4000 rpm; 18:1
ratio gear shaft rated 4.2 Kg.cm (58.3 oz-in) torque, up to 333 rpm. Baked black enamel
finish, precision die-cast housing, lifetime lubricated ball bearings with steel inserts in
die-casting.

Va
lu
e

Motor: Supplied with 1.5 meter three-wire cable with plug and ground lead for connection
to controller. Measures: 5-1/2 x 4 x 4 inches. Weight: 4 lbs 7 oz.
13530-10

Controller: ACE 13530* solid state 120v, 10 amp AC maximum or 0120v, 6 amp DC
maximum. Features rear ring stand clamp, Forward/Off/Reverse switch. Supplied with
heavy duty 1.8 meter three-wire power cord with NEMA plug. Supplied with one-amp
fuse to protect motor. Controller measures 102 (4 inches) x 54 (2-1/8 inches) x 41mm
(1-5/8 inches). Weight: 4.1 lbs. Complete consists of motor, controller and mounting rod.
Motor, only, w/ Mounting Rod
Controller, only
Complete

Order Code
13649-09
13530-10
13649-19

Each
742.01
523.17
1265.18

13649-09

MOTOR ATTACHMENTS (Optional):


Three-jaw, keyless chuck, 9.5mm (3/8-inch) rod
Nylon chuck, flex-grip, for shaft size approximately 10mm
Set screw wrench
Paddle, 36.4cm blades, S-S, on 22.2cm shaft
Propeller, 33.8cm blades, S-S, on 22.2cm shaft
Attachments Complete (Does not include 8124-10)

(Stand Not Included)

Order Code

Each

13649-24
8124-10
13649-26
13649-32
13649-34
13649-40

130.00
43.92
6.10
104.00
97.00
369.04

*ACE 13530 motor controller offers better performance at slower speeds;


for more torque at higher speeds, use 13532.

13650 STIRRER Laboratory, High Torque, Economy

Motor: Totally enclosed, non-reversible, 1/17 hp. DC input with a 5/16-inch


diameter shaft 1-inch long. Recommended for use with 8081 flexible shaft (shaft
turns counter-clockwise when facing shaft) or general stirring. Motor is adjustable
from 280 to 2800 rpm and generates 60 oz-in. of nominal torque. (Note: torque
diminishes below 280 rpm with safety click off.) Cast aluminum motor case is
painted chemically resistant grey. Supplied with 6-foot cord with NEMA plug end
and 5/8-inch diameter mounting rod. Measures 4.65 x 3.25 x 3.65 inches. Weight:
4.75 lbs. Can only be plugged into controller.
Controller: Durable plastic case for table top use. Rated at 120 volts, 50/60 Hz, 1.5 amp
maximum to protect motor beyond its rated torque. Measures: 6W x 5D x 2.5H inches.
Weight: 1.8 lbs. including 6-foot power cord.
Motor and Controller

Order Code
13650-40

Each
803.57

13650

(Stand Not Included)

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Subject to Ace Discount (Page 4)

Net

Accessories
4048 BOTTLE Solution, Threaded Neck

227

ORing Seal

PYREX brand borosilicate glass bottle designed for storage of solutions. Bottles have
GL120 external thread finish neck with large 106mm (4.2-inch) I.D. opening. The 9.5 liter
and 13.25 liter sizes have a conventional bottle shape. The 19 liter and 45.5 liter sizes are
similer in d
esign to a carboy. A glass-filled PTFE cap with CAPFE (PTFE encapsulated
silicone) ORing is available. Cap sold separately.
Capacity,
Liters
9.5
13.25
19.0
45.5

Capacity,
Gallons
2.5
3.5
5
12

Approx.
Dia., mm
187
238
292
406

Approx.
Height, mm
460
380
480
520

CAP, PTFE, Solid, GL 120, with CAPFE ORing

Order
Code
4048-09
4048-13
4048-19
4048-45

Each
277.47
343.50
377.73
708.30

7622-155

184.15

4048-19

5393 BOTTLE Solution, Plastic Coated


Bottle is coated to the neck with PVC safety coating to reduce potential breakage and
exposure to laboratory personnel when handling hazardous material. The 19L bottle is
Carboy style, with sloping shoulders. The 9.5L and 13.25L sizes are bottle shaped.
Necks are tooled for uniform fit with stoppers.
Approx.
Dia.,
mm
187
238
292

Approx.
Height,
mm
470
445
508

Rubber
Stopper
No.
12
12
12

Plastic Coated

Order Code
5393-06
5393-07
5393-09

Each
332.57
382.33
451.44

5395 BOTTLE Solution, with Ace-Safe, Plastic Coated

5395

Approx.
Cap.,
Gal.
2.5
3.5
5

Approx.
Dia.,
mm
187
238
292

Approx.
Height,
mm
470
445
508

Rubber
Stopper
No.
12
12
12

FE

Cap.,
Liters
9.5
13.25
19.0

E-SA

ON

Same as 5393 bottle, except this bottle has a vacuum takeoff and is coated to the
neck with PVC safety coating to reduce potential breakage and exposure to laboratory
personnel when handling hazardous material. Takeoff has a #15 AceThred in place of a
serrated fitting for use with an Ace-Safe tubing connection barb for 3/8-inch I.D. tubing.
Supplied complete with hose connection, nylon bushing and ORing.

OR

Approx.
Cap.,
Gal.
2.5
3.5
5

AC

Cap.,
Liters
9.5
13.25
19.0

5393

N ECT

Plastic Coated

Order Code
5395-103
5395-105
5395-107

Each
433.21
482.76
518.98

5393 and 5395 bottles are also available safety coated via special request.

Surlyn is a registered trademark of E.I. Dupont & Co.

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

228

Accessories
5539 BOTTLELaboratory, GL Thread 
Duran

Chemically resistant and stable laboratory bottles, fabricated from borosilicate glass.
Supplied graduated with or wtihout red plastic cap and removable pouring ring that allows
drip-free operation. Cap has PTFE liner. For use up to 180C. Not suitable for vacuum
or pressure use. Can be hot air sterilized or autoclaved. For extra caps or pour rings,
see 7622 in our Laboratory Glassware & Equipment catalog, or visit www.aceglass.com.
Cap., Approx. GL Thread O.D.,
mL
Cap., Oz.
Size
mm
5000 169
45
186
10000 338
45
234
15000 507
45
277
20000 676
45
300

5539-35

Height, mm
w/Cap
340
415
450
510

With Cap
Order
Code
Each
5539-30 148.44
5539-35 279.42
5539-41 374.19
5539-44 515.50

Without Cap
Order
Code
Each
5539-64 176.04
5539-66 328.70
5539-68 455.12
5539-70 687.42

5539-66

5539 BOTTLELaboratory, Safety Coated, GL Thread 


Duran

Chemically resistant and stable laboratory bottles, fabricated from borosilicate glass
and plastic coated for protection against mechanical damage and to prevent leakage
of contents should the glass break. Supplied graduated with or without red plastic cap
and removable pouring ring that allows drip-free operation. Cap has PTFE liner. For use
up to 140C. Not suitable for vacuum or pressure use. Height measurement is with cap.
Autoclavable or good for hot air sterilization. For extra caps or pour rings, see 7622 in
our Laboratory Glassware & Equipment catalog, or visit www.aceglass.com.
With Cap
Capacity, GL Thread
mL
Size
5000
45

5539-130

O.D., Height,. mm
mm
w/Cap
186
340

Order
Code
5539-130

Each
195.71

Without Cap
Order
Code
5539-160

Each
229.74

5539-160

5539 BOTTLELaboratory, Ambered, GL Thread 


Duran

Chemically resistant and stable laboratory bottles, fabricated from borosilicate glass and
ambered for protection of liquids sensitive to light. Supplied graduated with or without
red plastic cap and removable pouring ring that allows drip-free operation. Cap has PTFE
liner. For use up to 180C. Not suitable for vacuum or pressure use. Height measurement
is with cap. Autoclavable or good for hot air sterilization. For extra caps or pour rings,
see 7622 in our Laboratory Glassware & Equipment catalog, or visit www.aceglass.com.

5539-235

5539-264

Capacity,
mL
5000
10000
15000
20000

GL Thread
Size
45
45
45
45

O.D., Height,. mm
mm
w/Cap
186
340
234
415
277
450
300
510

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

With Cap
Order
Code
Each
5539-230
249.98
5539-235
460.15
5539-241
547.29
5539-244 1022.69

Without Cap
Order
Code
Each
5539-262
279.44
5539-264
530.96
5539-266
635.27
5539-268 1204.27

Subject to Ace Discount (Page 4)

Net

Accessories

229

7621 CAP With Hole, GL Thread 


Open top red polybutylene teraphthalate (PBT) cap for use with 7620 GL threads. When
used with 7623 hose connection and 7624 sealing ring, will accommodate tubing of
approximate diameter.
For Thread Temperature. Aperature Size,
Size
Range, C
mm
25
45 to +180
15
32
45 to +180
20
45
45 to +180
34

O.D.,
mm
33
40
54

Height,
mm
19
24
26

Order
Code
7621-15
7621-22
7621-25

Qty.
1
1
1

7621

Each
2.91
3.46
6.10

7622 CAPS/POURING RINGSfor GL Threaded Bottles 


Screw caps and pouring rings for use with GL threads. Red caps have PTFE liner, all
others are with lip seal. For 5539, 5557, 5559, and 5560 bottles.
For
Thread
Size Material
25 Polypropylene
25 Polybutylene Teraphthalate
25 Polybutylene Teraphthalate
32 Polypropylene
32 Polybutylene Teraphthalate
32 Polybutylene Teraphthalate
45 Polypropylene
45 Polypropylene
45 Polypropylene
45 Polypropylene
45 Polybutylene Teraphthalate
45 Polybutylene Teraphthalate
80 Polypropylene
For
Thread
Size Material
32 Polypropylene
45 Polypropylene
32 Polybutylene Teraphthalate
45 Polybutylene Teraphthalate
45 Polypropylene
45 Polypropylene
45 Polypropylene
80 Polypropylene

CAPS
Color
Blue
Red
Red
Blue
Red
Red
Blue
Yellow
Green
Grey
Red
Red
Blue

Temperature
Range, C
-40 to +140
-45 to +180
-45 to +180
-40 to +140
-45 to +180
-45 to +180
-40 to +140
-40 to +140
-40 to +140
-40 to +140
-45 to +180
-45 to +180
-40 to +140

O.D.,
mm
33
33
33
40
40
40
54
54
54
54
54
54
86

Height,
mm
19
19
19
24
24
24
26
26
26
26
26
26
40

Case
Qty.
10
10
1
10
10
1
10
10
10
10
10
1
10

Order
Code
7622-02
7622-14
7622-114
7622-04
7622-21
7622-121
7622-06
7622-32
7622-35
7622-37
7622-24
7622-124
7622-38

Case
Price
26.89
53.27
5.36
26.85
83.01
8.36
32.24
32.23
32.23
32.28
123.85
12.23
49.62

POURING RINGS
Color
Blue
Blue
Red
Red
Green
Yellow
Grey
Blue

Temperature
Range, C
-40 to +140
-40 to +140
-45 to +180
-45 to +180
-40 to +140
-40 to +140
-40 to +140
-40 to +140

Height,
mm
4
4
4
4
4
4
4
7

Case
Qty.
10
10
10
10
10
10
10
10

Order
Code
7622-52
7622-54
7622-56
7622-58
7622-60
7622-62
7622-64
7622-65

Case
Price
11.39
12.38
30.10
32.54
10.51
10.51
10.51
33.91

Color-Coded Caps
and Pour Rings

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

230

Accessories
New
7627

7627 CAP & POUR RING Premium, for GL Threaded Bottles 


This premium cap is designed for GL45 thread Duran bottles. It is made of colorless,
TPCh260 resin so that there are no leachables. High Chemical resistance and leak tight
due to a PTFE coated silicone seal. Meets USP standards. Autoclavable. Retrace code.
Description
Cap
Pour Ring

Temperature. O.D., Height, Case


Range, C
mm
mm
Qty.
196 to +260 51
26
5
196 to +260 51
4
5

Order
Code
7627-02
7627-03

Case
Price
106.30
25.89

7628 CAP & POUR RING for GL80 Threaded Bottles, Quick Release, PSU 

New

Quick-release closure for new GL80 thread, wide-mouth bottles. Made of white
polyarylsulphone 1 resin, which gives high thermal, mechanical and chemical compatibility.
Inner-seal is coated both sides with PTFE. Pour ring also available in PSU.

7628

Description
Cap
Pour Ring

Maximum
Temp., C
+180
+180

O.D., Height, Case


mm
mm
Qty.
86
40
5
86
6.85
5

Order
Code
7628-03
7628-04

Case
Price
255.71
156.09

7629 CAPPTFE Membrane, for GL Threaded Bottles 

New

Polypropylene, blue cap with center-hole and welded-in, PTFE, inner gas permeable
membrane. Ideal for media sterilization and storage. For use on 5539, 5557, 5559 and
5560 bottles.

7629

For Thread Temperature. O.D., Height, Case


Size
Range, C
mm
mm
Qty.
25
40 to +140
33
19
5
32
40 to +140
41
24
5
45
40 to +140
54
25
5
80
40 to +140
86
40
2

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Order
Code
7629-25
7629-32
7629-45
7629-80

Case
Price
77.65
78.19
45.25
26.90

Subject to Ace Discount (Page 4)

Net

Accessories
7631 CAP GL80 Connection System 

231

New

The heart of the GL80 connection system is a GL80 polypropylene cap with 4, GL18
threaded ports. Modular accessories include polypropylene tube connection caps,
GL18 solid polybutylene terepthalate (PBT) caps, GL18 PBT pressure equalization
caps and PTFE cap inserts to accomodate various sizes of tubing. A typical
application is the safe transfer of liquid media within a closed and sterile system
for which youd need one two-pack code -01 GL80 cap,two -04 equalization caps,
and some combination of solid caps and tubing connections with inserts.
Description
4-Port (GL18) Polypropylene Cap
GL18 Polypropylene Tube Connection
Solid GL18 PBT Cap
GL18 PBT Cap wtih Pressure Equalizing Valve
3.2mm I.D. PTFE Cap Insert
6.0mm I.D. PTFE Cap Insert
8.0mm I.D. PTFE Cap Insert
10.0mm I.D. PTFE Cap Insert
12.0mm I.D. PTFE Cap Insert

Package
Qty.
2
2
2
1
1
1
1
1
1

Order
Code
7631-01
7631-02
7631-03
7631-04
7631-10
7631-11
7631-12
7631-13
7631-14

Package
Price
247.94
23.98
10.75
47.37
29.14
29.14
29.14
29.14
29.14

7632 CAP GL45 Connection System 

7631

New

The heart of the GL45 connection system is a GL45 polypropylene cap with GL18 threaded
ports. Modular accessories include polypropylene tube connection caps, GL18 solid
polybutylene terepthalate (PBT) caps, GL18 PBT pressure equalization caps and PTFE
cap inserts to accomodate various sizes of tubing. A typical application is the safe transfer
of liquid media within a closed and sterile system for which youd need one two-pack
GL45 cap, two -07 equalization caps, and some combination of solid caps and tubing
connections with inserts.
Description
2-Port (GL14) Polypropylene Cap
3-Port (GL14) Polypropylene Cap
GL14 Polypropylene Tube Connection
Solid GL18 PBT Cap
GL14 PBT Cap wtih Pressure Equalizing Valve
Extra Pressure Membranes for 7632-07
1.6mm I.D. PTFE Cap Insert
3.0mm I.D. PTFE Cap Insert
3.2mm I.D. PTFE Cap Insert
6.6mm I.D. PTFE Cap Insert

Package
Qty.
2
2
2
2
1
2
1
1
1
1

Order
Code
7632-01
7632-02
7632-05
7632-06
7632-07
7632-08
7632-10
7632-11
7632-12
7632-13

Package
Price
103.49
111.00
15.00
8.21
45.78
30.00
24.89
25.76
24.89
24.89

7632

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

232

Accessories

5559

New

5559 BOTTLE Wide Mouth, Clear, Amber or Plastic Coated 


Duran

Borosilicate glass wide-neck bottle with GLS 80 quick-release blue closure for use up to
140C (plastic coated up to 135C). Graduated. For extra caps or pour rings, see 7622
in our Laboratory Glassware & Equipment catalog, or visit www.aceglass.com.
Capacity,
mL
5,000
10,000
20,000
5,000
10,000
20,000
5,000
10,000
20,000

Type
Clear
Clear
Clear
Amber
Amber
Amber
Clear/Plastic Coated
Clear/Plastic Coated
Clear/Plastic Coated

O.D.,
mm
182
227
288
182
227
288
182
227
288

Height,.
mm
311
395
483
311
395
483
311
395
483

Order
Code
5559-09
5559-20
5559-24
5559-209
5559-220
5559-224
5559-304
5559-306
5559-308

Each
205.05
374.74
810.21
431.13
628.98
1289.29
388.59
451.46
976.14

6989 BOTTLE Filtering, with Removable PP Hose Connection 


6989

Duran

Heavy wall, bottle shaped, filtering flask with removable polypropylene hose connection.
Offered clear or plastic coated. Plastic coated bottles are steam autoclavable at 135C.
For replacement hose connection assembly, order 6989-40.
Capacity,
mL
3,000
5,000
10,000
15,000
20,000

Body
O.D., mm
170
185
240
255
290

Capacity,
mL
3,000
5,000
10,000
15,000
20,000

Body
O.D., mm
170
185
240
255
290

CLEAR GLASS
Height,
Neck
Order
mm
I.D., mm
Code
295
60
6989-15
360
70
6989-18
420
70
6989-21
500
70
6989-24
535
70
6989-27
PLASTIC COATED
Height,
Neck
Order
mm
I.D., mm
Code
295
60
6989-115
360
70
6989-118
420
70
6989-121
500
70
6989-124
535
70
6989-127

Each
135.99
220.06
324.62
387.51
486.59

Each
178.60
270.69
407.69
474.24
560.73

12477 BOTTLEAspirator with Spigot


12477

Constructed of polyethylene with polyethylene spigot and screw closure. Quick-action


spigot, for easy, positive control, leakproof operation and long life. Suitable for collecting
and dispensing distilled water, handling acids. Leakproof closures.
Cap., liters
4
8
20
25

Quantity
Each or case of 6
Each or case of 6
Each or case of 4
Each or case of 4

Order Code
12477-02
12477-04
12477-06
12477-08

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Each
104.85
148.35
178.80
201.55

Case Price
629.10
890.10
715.20
806.20

Subject to Ace Discount (Page 4)

Net

Accessories

233

5332 BEAKERHeavy-Wall, Pilot Plant Size 


Duran

Heavy wall beakers with spout.


Capacity,
mL
5,000*
10,000
15,000
20,000

O.D.,
mm
182
225
260
285

Order
Code
5332-28
5332-33
5332-36
5332-39

Height,
mm
256
340
390
430

Each
169.97
342.76
461.29
532.25

5332

*5,000mL size (only) is graduated.

6228/6231 BEAKER Pilot Plant 


Large sizes for batch operations and mixing large volumes of measured liquids. Graduated.
Capacity,
mL
5,000
10,000
15,000
20,000

Subdiv.,
mL
100
100
500
500

Approx.
Height, mm
457
457
390
430

O.D., mm
152
223
260
285

Order
Code
6228-05
6228-10
6231-21
6231-27

6228/6231

Each
336.30
532.31
502.02
552.35

6233 BIG JAR 

6233

Cylindrical jars with side indents for easier handling. Made of heavy wall glass, the jars are
graduated and come with pour spout. Caution: Do not apply open flame or heat. Also
available with poly safety coating.
Capacity, L
7.25
9.25
17
26.5
32

Subdiv.,
mL
500
500
1,000
2,000
2,000

Approx.
Height, mm
254
254
305
457
305

O.D., mm
222
257
305
305
406

Order Code
6233-07
6233-09
6233-17
6233-26
6233-32

Each
487.35
557.00
635.49
778.53
1263.38

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

234

Accessories
6472 SPRAYERClean-In-Place
Designed for cleaning ACE reactors without dismantling, or Clean-In-Place (CIP). One
moving part, a rotating disc at end of extension, produces heavy droplets in a 39-inch
diameter, 360 pattern to simultaneously cover entire surface of reactor. Rotating disc is
constructed of carbon-filled PTFE and stainless steel.
Wash fluid enters through a series of holes onto a precisionPressure Flow Rate
shaped disc. The disc rotates freely at high speed and the
(PSI) L/Min GPM
wash fluid is distributed in a dense spray. Can be operated
15
16 4.22
in any position. Working pressure is 15-60 psi; maximum
20
19 5.01
temperature is 120C. For pressure and flow rates, see chart
30
23 6.07
at right. Fits through openings as small as 1-1/8-inch diameter,
40
26 6.86
including a 45/50 outer joint. Assembly consists of spray
50
29 7.65
disc, stainless steel coupling, extension tube, elbow, nipple,
60
33 8.71
and a 45/50 inner to #15 AceThred glass adapter with a
nylon bushing and FETFE oring.

6472-210

Spray Disc, 1/4-inch MPT


Coupling, 1/4-inch FPT
Ext. Tube, 24-inch, 1/4-inch MPT
Elbow, 1/4-inch FPT

Order Code
6472-200
6472-201
6472-204
6472-206

Each
623.81
8.45
32.51
9.29

Nipple, 1/4-inch MPT


Adapter, Glass, 45/50#15
Nylon Bushing & ORing, #15
COMPLETE

Order Code
6472-208
8042-21
7506-06
6472-210

Each
3.60
50.57
12.35
740.58

6472 SIDE SHELF Pilot Plant Support Stand


Removable side shelf add-on for ACE pilot plant reactor support stands. Suitable for
placement of motor controllers, temperature controllers, relay units, etc. The black
powder-coated aluminum plate has a 3/8-inch wide x 3/8-inch high ledge to prevent
items from falling or sliding off. Attaches to stand with galvanized iron clamp-on tee with
set screws and backing bolt.
For Support
Stand
6473-34,-35, -36
6472-37
6474-370
6474-371
6474-372
6474-373

6472-342

Reactor Capacity/Type
100 & 150 Liter Cylindrical
200 Liter Cylindrical
50 Liter Spherical
72 Liter Spherical
100 Liter Spherical
200 Liter Spherical

Shelf Size
(W x L, in.)
12 x 28
12 x 32
12 x 26
12 x 32
12 x 40
12 x 42

Order
Code
6472-343
6472-344
6472-342
6472-344
6472-345
6472-346

Each
288.23
307.61
273.82
307.61
329.08
336.24

6517 CLAMP Quick Release


Stainless steel quick release clamp for use with reaction flasks and heads with
Schott-Duran flanges. Available with or without extension rod, 5/8-inch O.D. x
12-inch long for clamping to a support frame. Welded extension is used to stabilize
reaction assemblies. Note: Reactors should be supported from below in usual
manner namely mantles, rings, jacks, etc.
WITHOUT EXTENSION

6517-54, 56, 60
6517-22, 25, 27, 31

For Flange Size Order Code


60 mm
6517-22
100 mm (4-inches)
6517-25
120 mm (4.8-inches)
6517-24
150 mm (6-inches)
6517-27
200 mm (8-inches)
6517-31

Each
87.08
98.23
114.57
117.67
145.09

6496 STANDARD CLAMP


Anodized aluminum clamp with three stainless steel swing bolts and removable back
arm for attaching to racks. Clamp slides open to accommodate flasks. Used with 15305
conical flanges.
Complete
Extra Liners, only

Qty.
1
Set of 4

Order Code
6496-10
6496-30

WITH EXTENSION
Order Code

6517-54

6517-56
6517-60

Each
158.10
172.33
199.11

6496

Each
216.45
20.00

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Subject to Ace Discount (Page 4)

Net

Accessories
6508/6510 CLAMP

6508

For use with all flat style flanges.


For I.D., mm
100
130

Order Code
6508-06
6508-11

235

Each
225.58
244.27

For I.D., mm
100
130

Order Code
6510-05
6510-10

Each
169.50
192.87

6510

6509 CLAMP
Positive, two-piece clamp with PTFE liner for securing the 76mm or 102mm size 7519 filter
support assembly. Bolt head is flanged to secure top half as bolt is threaded into bottom half.
Size
76mm
102mm

Order Code
6509-03
6509-05

6509

Each
142.49
135.03

7669 CLAMPS Pinch Type, Stainless Steel


All stainless steel pinch clamps for use with ORing spherical joints and ball and socket
joints. Sizes 12 and 18 are available either spring loaded or with a screw-locking device.
All other sizes have the screw-locking feature. Only screw-locking clamps should be
used with ORing spherical joints.

7669

Spring Loaded
Size No.
12
18

Joint Size
12/5
18/9

Order Code
7669-03
7669-05

Each
7.79
8.64

With Screw-Locking Device


12
18
28
35
40
50
65
75
102

12/5
18/9
28/15
35/25

50/30
65/40
75/50
102/75

7669-08
7669-10
7669-12
7669-14
7669-16
7669-18
7669-20
7669-22
7669-26

14.30
14.33
16.57
18.51
41.45
32.03
35.90
72.92
246.61

6495 GASKETPTFE
PTFE gaskets, white in color, for mating ground flange surfaces on reactor flasks and
matching heads. Can be used with all conical style and flat flange style flask and heads.
PTFE makes a leak-free seal with slight clamp pressure. They also provide the added
chemical resistance and purity of PTFE.
Thickness,
inches/mm

O.D., Inches
(mm)

Fits Flask
Size, mL

Grooved

Order
Code

Each

0.03/0.8
0.03/0.8
0.03/0.8

5.250 (133.4)
5.375 (136.7)
6.625 (168.4)

500-3000mL
500-1000mL
2000-4000mL

No
Yes
Yes

6495-10
6495-21
6495-23

11.28
60.28
64.15

6495-10

6495-21

6495 GASKETFETFE

6495-43

ACE FETFE gaskets, black in color, for mating ground flange surfaces on reactor flasks
and matching heads. Can be used with all conical style and flat flange style flask and
heads. FETFE makes a leak-free seal with clamp pressure. FETFE is an exclusive
ACE product made from TFE impregnated fluoroelastomers with good chemical and
temperature resistance.
Thickness,
inches/mm
0.02/0.5
0.02/0.5

O.D., Inches
(mm)
5.375 (136.7)
6.625 (168.4)

Fits Flask
Size, mL
500-1000mL
2000-1000mL

Grooved
Yes
Yes

Order
Code
6495-43
6495-47

Each
19.53
20.12

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

236

Accessories
7855 ORINGReplacement
Replacement orings for use with 6310, 6521, 6522, 6523, 6533, 6535, 6536, 6537, 6540,
6469, and 6472 only reaction flasks with groove in ground flange.
CAPFE
For Flange
I.D., mm (In.). Order Code
Each
60 (2)
7855-878
28.10
100 (4)
7855-880
28.63
150 (6)
7855-881
59.65
200 (8)
7855-884
75.27

7855

Silicone
Order Code
7855-251
7855-254
7855-260
7855-288

Each
13.76
21.39
40.00
49.76

11081 CLAMP HOLDER Pilot Plant


Used with 11065 versatile jaw clamp to secure condenser, etc., on 6472 pilot plant
reactor. Holder clamps to 1-inch bar frame of reactor stand; 11065 clamp is held in
clamp holder with thumb screw. Vertical hole to accommodate straight bar or clamp.
Fabricated of aluminum, epoxy powder coated black.
Order Code
11081-21

Each
84.80

11081

11079 CLAMP Chain


Fast, sure way to secure large equipment to rods and lattices. Holds 76 to 165mm bottles,
flasks, and large objects. Loop steel chain around object. Attach to hook on movable
slide. Tighten slide with large nonslip knob. Holds equipment firmly in place at any angle.
You can vary distance from support rod.
Length (In.)
7.4
8.11
15.12

11079

11080

For Vessel OD
170mm
280mm
280mm

Order Code
11079-24
11079-38
11079-40

Each
51.23
75.28
79.46

11080 CLAMP HOLDERRegular


Normally used to hold the Nos. 11065 through 11072 clamps to rods and lab frame
supports. Made of heavily nickel-plated zinc. Will grip rods up to and including 19mm
diameter. Attaches clamp at right angle.
Order Code
11080-19

Each
18.82

12100 TILTING SUPPORT


Tilting support provides a finger-tip method of emptying flasks by pouring. Mantle support
ring may be adjusted to and locked at any convenient height. Upper cross member
strengthens assembly; serves as stop for tilted mantle. Base is compact, 91 x 98cm, but
extremely stable. Complete item sold with one set of rings.
For Flask
Size, mL
12000
22000
50000
72000

Order Code
12100-04
12100-07
12100-11
12100-15

Each
567.00
567.00
567.00
567.00

Order Code
12100-34
12100-38
12100-42
12100-46

Each
1465.00
1479.00
1479.00
1667.00

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

12100

Subject to Ace Discount (Page 4)

Net

Accessories
12094 EXTENSION SUPPORT
Provide convenient supports for flasks up to five-liter capacity. Generally used with flasks
having aluminum housing.
Flask Cap., mL Order Code
50-200
12094-02
250-500
12094-04
1000
12094-06

Flask Cap., mL Order Code


2000/3000
12094-08
5000
12094-12

Each
79.00
83.00
86.00

237

12094

Each
90.00
90.00

13010 CLAMP Recirculator Hose Support, Stainless Steel


All stainless steel, fully adjustable clamp for securing and supporting circulator hoses
used with jacketed pilot plants. The universal clamp adjust to any pipe style pilot plant
stand, and the clip will accommodate any standard circulator hose size.
Order Code

Each

13010-01

112.28

13010

12096 TRIPOD SUPPORT


For 5L, 12L and 22L heating mantles with soft glass outer covering instead of spun aluminum.
Flask Capacity, mL
5,000
12,000
22,000

Order Code
12096-05
12096-10
12096-14

Each
208.00
214.00
227.00

12096

12097 TRIPOD SUPPORT


For 3,000mL- 72,000mL Glas-Col Mantles.
Flask Capacity, mL
3,000
5,000
12,000
22,000
50,000
72,000

Order Code
12097-04
12097-06
12097-08
12097-10
12097-12
12097-14

Each
107.00
111.00
139.00
186.00
201.00
233.00

12097-04

12097 TRIPOD SUPPORT


Support for 12 through 72-liter Glas-Col heating mantles. Adjustable height 24 to 36
inches in 3-inch increments. Twenty four (24) inches wide at base.
Flask Capacity, mL
12,000
22,000
50,000
72,000

Order Code
12097-45
12097-47
12097-49
12097-51

Each
467.00
492.00
521.00
532.00

12097-47

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

238

Accessories
13219 CONTAINMENT TRAY Stainless Steel
Trays are heavy 14-gauge, 304 stainless steel. For safe containment of spills from larger
reactors, see recommended sizes below.

13219

Size (LxWxH,
inches)
24 x 24 x 2
24 x 24 x 3
28 x 28 x 3
28 x 28 x 4
36 x 36 x 5

For Vessel or
Reactor Size
10, 20L
3 post/30L
30, 50L
100, 150L
72, 100, 150, 200L

Order Code
13219-03
13219-05
13219-07
13219-09
13219-11

Each
Call
Call
Call
Call
Call

13220 CONTAINMENT TRAY Low Density Polyethylene

13220-16

Trays are made of rugged, molded Low Density Polyethylene (LDPE).


Size (LxWxH,
inches)
23 x 21 x 2
24 x 24 x 3
24 x 24 x 4
26 x 20 x 4
30 x 28 x 4
51 x 31 x 4

For Vessel or
Reactor Size
10L
20L
36L
30L
50L
100L

Order Code
13220-16
13220-18
13220-20
13220-22
13220-24
13220-26

Each
85.51
121.75
153.56
125.22
162.39
190.03

13220 CONTAINMENT TRAY Low Density Polyethylene, w/Spigot

13220-37

Trays are made of rugged, molded Low Density Polyethylene (LDPE). Models listed below
feature a wide lip at the top and a 1/2-inch spigot for easy draining of fluids.
Size (LxWxH,
inches)
12 x 16 x 3
16 x 20 x 3
21.5 x 25.5 x 4
17.5 x 23.5 x 6

For Vessel or
Reactor Size
up to 2L
up to 6L
up to 10L
up to 20L

Order Code
13220-33
13220-35
13220-37
13220-39

Each
115.50
120.70
154.60
178.95

12187 ADAPTERS Stainless Steel, Circulator Hose


304 stainless steel adapters designed for use with ACE jacketed glass pilot plant reactors
and circulator hoses for popular circulating chillers. Connects oring ball joints on jacket
inlet/outlet to hoses to/from circulator.
Description
Adapter, flask to hose, Stainless Steel, 28/15 Socket to M16x1 Male
Adapter, flask to hose, Stainless Steel, 35/25 Socket to M16x1 Male
Adapter, flask to hose, Stainless Steel, 35/25 Socket to M24x1 Male
Adapter, flask to hose, Stainless Steel, 35/25 Socket to M30x1 Male
Adapter, flask to hose, Stainless Steel, 35/25 Socket to M38x1.5 Male
Adapter, Hose to Circulator, Stainless Steel, M16x1 Male to 3/4 inch NPT Male
Adapter, Hose to Circulator, Stainless Steel, M30x1.5 Male to 3/4 inch NPT Male
Adpater, Hose to Circulator, Stainless Steel, M24x1.5 Male to 3/4 inch NPT Male

Order
Code
12187-05
12187-07
12187-10
12187-12
12187-14
12187-100
12187-101
12187-102

Each
88.40
93.60
93.60
93.60
93.60
93.60
93.60
93.60

12187-100

12187-05

12187 CLAMP Stainless Steel, Circulator Hose


304 stainless steel clamp designed for use with ACE jacketed glass pilot plant reactors
and circulator hoses for popular circulating chillers. Connects glass oring ball joints on
jacket inlet/outlet to hoses to/from circulator. Powder coated aluminum with glass-filled
PTFE backing.
For Joint Size
28/15
35/25

Order Code
12187-28
12187-35

Each
124.80
135.20

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

12187-28

Subject to Ace Discount (Page 4)

Net

Accessories

239

10015 PRESSURE RELIEF MANIFOLD for ACE Pilot Plants


This pressure relief manifold is designed to fit into process systems between the circulator
and the glass reaction vessel for added protection and safety. The manifold gives further
protection to the glass vessel itself and the vessel inlet fittings and alleviates excess
pressure build-up that could damage the reactor. Most circulators have an excess pressure
relief built-in, but may not be able to react fast enough to protect the glass. The system
is supplied complete with the anodized aluminum body-clamp, outlet connections and
hoses, inlet pressure gauge, relief valve assembly, which is factory preset and sealed at
10 PSI. The manifold will fit 10L and larger pilot plant systems.
See separate hose listings by manufacturer for inlet/outlet hoses and connector fittings.
See also stainless steel fittings to match to 3/4-in. female manifold inlet.
Order Code
10015-10

Each
2741.31

10015

8250 STOPPERS Full Length


Sizes 7/25 and 10/30 are solid, all others are hollow.
Size
7/25
10/30
12/30
14/35
19/38
24/40

Order Code
8250-02
8250-04
8250-06
8250-08
8250-10
8250-12

Each
14.40
15.28
15.40
18.53
19.45
19.79

Size
29/42
34/45
45/50
55/50
71/60

Order Code
8250-14
8250-16
8250-20
8250-24
8250-28

Each
25.05
31.81
44.68
56.66
161.88

8250

12631 STOPPERS PTFE,


Standard taper stoppers made of solid PTFE.

12631

Size
7/10
7/25
10/10
14/10
14/20
19/22
24/25
29/26

Order Code
12631-02
12631-03
12631-04
12631-06
12631-07
12631-09
12631-15
12631-17

Each
11.51
11.55
11.52
11.55
15.15
16.97
21.00
29.24

12633 STOPPERS PTFE,


Standard taper, PTFE stoppers with easy-to-grip handle. Codes -05 and -09 are solid,
all others are hollow.

12633

Size
14/20
19/22
24/25
24/40
29/42
45/50

Order Code
12633-05
12633-09
12633-12
12633-15
12633-17
12633-23

Each
13.80
14.55
21.57
21.70
22.40
71.00

12634 STOPPERS PTFE


Virgin TFE/PTFE stoppers with built-in black Delrin stopper extractor ring. Eliminates the
hazard of removing a frozen stopper from glass vessel. You need only turn red nut clockwise to exert a gentle force against the vessels lip and the non-stick stopper is extracted.

12634

Stopper
Size
19/22
24/40
29/42

Qty.
3
2
2

Order Code
12634-16
12634-20
12634-24

Per Pkg.
104.95
108.65
122.55

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

240

Accessories

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Subject to Ace Discount (Page 4)

Net

O-Rings

241

VITON A A linear copolymer of Vinylidine Fluoride and Hexafluoropropylene.


SILICONE A group of elastomeric materials made from Silicone, Hydrogen and Carbon.
BUNA-N A copolymer of Butadiene and Acrylonitrile.
FETFE A fluoroelastomer with special TFE Additives.
EPDM (ETHYLENE-PROPYLENE) An elastomer prepared from Ethylene and Propylene Monomers.

7855 ORINGS
Size

Dimensions
I.D.,mm W.

Qty.

VITON
Order Code

Per
Pkg.

SILICONE
Per
Order Code Pkg.

BUNA-N
Per
Order Code Pkg.

FETFE
Order Code

e
lu
Va
Per
Pkg

EPDM
Per
Order Code Pkg.

-006
-007
-008
-009
-010
-011
-012
-013
-014
-015
-016
-018
-021
-022

2.9
3.7
4.5
5.3
6.1
7.7
9.2
10.8
12.4
14.0
15.6
18.8
23.5
25.1

1.78
1.78
1.78
1.78
1.78
1.78
1.78
1.78
1.78
1.78
1.78
1.78
1.78
1.78

12
12
12
12
12
12
12
12
12
12
12
12
12
12

7855-01
7855-02
7855-04
7855-07
7855-05
7855-06
7855-08
7855-10
7855-12
7855-13
7855-14
7855-15
7855-19
7855-17

10.69
11.06
11.21
11.66
11.75
11.81
11.77
12.26
12.93
14.50
14.27
15.45
20.20
20.05

7855-201
7855-202
7855-204
7855-207
7855-205
7855-206
7855-208
7855-210
7855-212
7855-213
7855-214
7855-215
7855-219
7855-217

13.71
13.85
14.78
15.45
15.21
15.45
15.97
16.30
15.97
17.25
17.17
18.26
22.40
22.07

7855-401
7855-402
7855-404
7855-407
7855-405
7855-406
7855-408
7855-410
7855-412
7855-413
7855-414
7855-415
7855-419
7855-417

4.48
4.48
4.69
4.69
4.69
4.69
4.69
4.73
4.69
7.23
7.23
7.49
7.52
7.52

7855-701
7855-702
7855-704
7855-707
7855-705
7855-706
7855-708
7855-710
7855-712
7855-713
7855-714
7855-715
7855-719
7855-717

13.19
13.11
13.68
14.77
14.78
14.77
15.45
15.45
15.94
17.16
17.07
19.10
19.18
18.32

7855-904

7855-906
7855-908
7855-910
7855-912

7855-914

14.58

14.58
14.42
15.46
15.45

16.03

-105
-107
-108
-110
-111
-112
-113
-114
-115
-116
-118
-121
-122
-123
-125
-127
-128
-136

3.6
5.2
6.0
9.2
10.8
12.4
13.9
15.5
17.1
18.7
21.9
26.6
28.2
29.8
33.0
36.2
37.8
50.5

2.6
2.6
2.6
2.6
2.6
2.6
2.6
2.6
2.6
2.6
2.6
2.6
2.6
2.6
2.6
2.6
2.6
2.6

12
12
12
12
12
12
12
12
12
12
12
12
6
6
6
6
6
6

7855-03
7855-09
7855-11
7855-16
7855-18
7855-20
7855-21
7855-22
7855-24
7855-26
7855-70
7855-27
7855-71
7855-28
7855-72
7855-76
7855-73
7855-29

15.67
15.66
15.77
15.66
15.54
16.62
18.46
18.36
19.55
20.60
22.44
27.52
14.33
14.55
14.66
15.09
15.05
15.20

7855-203
7855-209
7855-211
7855-216
7855-218
7855-220
7855-221
7855-222
7855-224
7855-226
7855-270
7855-227
7855-271
7855-228
7855-272
7855-276
7855-273
7855-229

16.38
15.91
16.38
16.10
16.42
16.85
17.17
17.28
17.32
17.89
19.35
26.30
11.12
13.60
13.39
16.28
16.48
15.22

7855-403
7855-409
7855-411
7855-416
7855-418
7855-420
7855-421
7855-422
7855-424
7855-426
7855-470
7855-427
7855-471
7855-428
7855-472
7855-476
7855-473
7855-429

4.46
4.54
4.91
5.06
5.06
5.06
5.06
5.14
5.65
5.65
6.11
5.63
4.45
4.48
4.46
4.52
4.57
5.06

7855-703
7855-709
7855-711
7855-716
7855-718
7855-720
7855-721
7855-722
7855-724
7855-726
7855-770
7855-727
7855-771
7855-728
7855-772
7855-776
7855-773
7855-729

20.06
20.59
19.85
19.78
20.46
21.62
23.76
24.88
26.89
26.57
31.64
34.55
18.39
20.19
20.31
19.37
19.41
19.70

7855-916

7855-922

7855-926

7855-927

7855-928

7855-929

18.94

21.74

25.49

31.55

15.79

17.51

-210
-211
-212
-213
-214
-215
-216
-217
-218
-219
-220
-221
-222
-223
-225
-226
-227
-228
-229
-230

18.6
20.2
21.8
23.3
25.0
26.6
28.2
29.7
31.3
33.0
34.5
36.1
37.7
40.9
47.2
50.4
53.6
56.7
59.9
63.1

3.5
3.5
3.5
3.5
3.5
3.5
3.5
3.5
3.5
3.5
3.5
3.5
3.5
3.5
3.5
3.5
3.5
3.5
3.5
3.5

6
6
6
6
6
6
6
6
6
6
6
6
6
3
3
3
3
3
3
3

7855-30
7855-32
7855-34
7855-36
7855-38
7855-37
7855-39
7855-40
7855-41
7855-43
7855-42
7855-51
7855-52
7855-74
7855-44
7855-46
7855-45
7855-47
7855-48
7855-75

13.48
14.66
16.03
16.01
18.48
25.61
25.41
25.45
25.66
25.69
25.57
25.62
25.70
14.69
16.69
17.46
18.20
19.55
20.07
21.10

7855-230
7855-232
7855-234
7855-236
7855-238

7855-239
7855-240

7855-242

7855-274
7855-244
7855-246
7855-245
7855-247
7855-248
7855-275

15.71
15.93
15.69
15.75
15.99

16.10
16.01

16.20

6.10
8.85
8.78
8.72
9.04
9.50
21.23

7855-430
7855-432
7855-434
7855-436
7855-438
7855-437
7855-439
7855-440
7855-441
7855-443
7855-442
7855-451
7855-452
7855-474
7855-444
7855-446
7855-445
7855-447
7855-448
7855-475

4.69
4.69
4.69
4.76
4.85
4.90
4.90
4.90
4.91
4.91
4.95
4.91
4.91
2.80
3.23
4.48
4.48
4.48
4.48
4.57

7855-730
7855-732
7855-734
7855-736
7855-738

7855-739
7855-740

7855-742

7855-774
7855-744
7855-746
7855-745
7855-747
7855-748
7855-775

17.57
18.65
20.14
20.17
24.80

27.47
28.21

33.91

18.72
21.20
24.45
23.38
25.28
26.05
29.44

7855-930
7855-932
7855-934

7855-938

7855-939

7855-942

7855-944
7855-946

7855-948
7855-975

15.50
15.50
15.33

38.11

39.29

16.56

12.24
12.81

13.13
15.78

Continued on following page

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

242

O-Rings

7855 ORINGS (listing


Size

Dimensions
I.D.,mm W.

VITON A A linear copolymer of Vinylidine Fluoride and Hexafluoropropylene.


SILICONE A group of elastomeric materials made from Silicone, Hydrogen and Carbon.
BUNA-N A copolymer of Butadiene and Acrylonitrile.
FETFE A fluoroelastomer with special TFE Additives.
EPDM (ETHYLENE-PROPYLENE) An elastomer prepared from Ethylene and Propylene Monomers.
e
lu
continued from previous page)
Va

Qty.

VITON
Order Code

Per
Pkg.

SILICONE
Per
Order Code Pkg.

BUNA-N
Order Code

Per
Pkg.

FETFE
Order Code

Per
Pkg

EPDM
Order Code

Per
Pkg.

-233
-235
-239
-240

72.6
78.9
91.7
94.9

3.5
3.5
3.5
3.5

3
3
3
3

7855-64
7855-69
7855-78

22.39
Call
Call

7855-264

10.06

7855-464

Call

7855-778
7855-764

29.40
31.67

-325
-326
-327
-329
-335
-336
-338
-341
-343
-348
-349
-359

37.5
40.6
43.8
50.2
69.2
72.4
78.7
88.3
94.6
110.5
113.7
145.4

5.3
5.3
5.3
5.3
5.3
5.3
5.3
5.3
5.3
5.3
5.3
5.3

6
6
6
3
3
3
3
3
3
3
3
3

7855-65
7855-67
7855-68

7855-82
7855-77
7855-50
7855-66
7855-79

28.79
28.75
28.62

35.47
38.38
47.73
52.71
87.63

7855-278
7855-283

7855-282
7855-277
7855-250
7855-266

7855-287
7855-289

16.82
17.20

18.60
19.32
19.97
21.73

22.38
25.32

7855-453
7855-454
7855-455

7855-499

7855-450

5.50
5.50
5.50

146.28

4.66

7855-783

7855-782
7855-777
7855-750
7855-766
7855-779
7855-787

40.56

48.61
55.09
63.72
63.72
63.72
65.78

5-101
2-105
5-193
5-017

2.5

0.97 12
12
1.0 12
2.6 12
4.0
1
5.0
1
5.0
1
5.0
1

7855-80
7855-303
7855-81

18.09
Call
Call

7855-281

7855-251
7855-254
7855-260
7855-288

Call

13.76
21.39
40.00
49.76

7855-482

Call

7855-99

244.86

7855-499

146.28

8194-310
8194-313
8194-315
8194-317

69.34
78.17
76.12
51.43

4.5
6.1
75.5
110.0
150.0
215.0

ORing Kits 30 Sizes

500

ORing Sets: one box of 18 sets


ORing Sets: one box of 18 sets
ORing Sets: one box of 12 sets
ORing Sets: one box of 6 sets

*Sizes not listed are available via special order. Call or email for quotation.

CHEMICAL COMPATIBILITY CHART

Key: 1=Recommended; 2=Satistfactory; 3=Poor; 4=Marginal; 5=Not Recommended; A=Acceptable; NA=Not Acceptable
Temperature Range C
Compression set
Durometer
Steam < 120 C
Acetone
Toluene
Tetrachloroethane
THF
Methyl Ethyl Ketone
Acetonitrile
Hydrochloric Acid (conc)
Ammonia Gas (cold)
Tetrachloroethylene
Sulfuric Acid (dilute)
Nitric Acid (conc)
Calcium Carbonate
Xylene
Mineral Oils
Sodium Carbonate
Vacuum
FDA

Viton
26 to 204
2

Silicone
62 to 204
2

Buna-N
37 to 121
2

EPDM
54 to 149
2

75
3
4
2
1
4
5
5
2
4
3
2
2
2
2
1
1
1
A

70
4
3
3
3
4
5
5
5
1
5
5
5
5
4
2
1
4
A

70
4
3
3
3
4
5
5
4
2
3
1
4
1
4
1
1
2
A

70
4
2
3
3
4
2
5
5
2
3
5
5
1
3
4
1
4
A

Chemraz 514 Kalrez 4079


30 to 220
15 to 316
2
2
70
1
1
1
1
1
1
1
1
1
1
2
1
1
1
1
1
4
NA

75
1
1
1
1
1
1
1
1
1
1
2
1
1
1
1
1
4
NA

FETFE
18 to 204
2

CAPFE
60 to 204
3

70
1
5
2
1
5
5
5
2
4
3
2
2
2
2
1
1
1
NA

70
5
1
2
2
3
2
2
4
2
2
2
4
2
2
1
2
2
A

Chemical compatibility information courtesy of the respective manufacturers of each o-ring type. Ace is not responsible for errors.

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Subject to Ace Discount (Page 4)

Net

O-Rings

243

ACE Exclusive!

CAPFE A Rubbery PTFE ORing

Low friction
High chemical resistance
Low compression set compared to
solid PTFE ORings
Low gas and water vapor
permeability compared to flash
coated ORings

7855 ORINGSCAPFE
A totally different ORing having a resilient rubber core encased in a continuous, thick, non-porous FEP/PTFE encapsulation. This unique ORing solves
the sealing problems where the chemical inertness of PTFE is a MUST and
where maintenance-free dependability and long service life are required.

CAPFE Advantages
Continuous encapsulation of thick, pure
PTFE offers no seams or weak spots to
break and leak.

Resistant to all chemicals except molten


alkali metals, hot fluorine and certain
complex halogenated compounds.

CAPFE offers both resilience and chemical


resistance.

Extreme slipperiness of PTFE reduces


friction in dynamic applications.

Thick PTFE encapsulation permits wide


application without leakage or deterioration.

CAPFE ranges from 60C to +204C,


deterioration vacuum to 10,000 psi.

TYPE OF SEAL

Each
15.87
16.79
17.85
19.51
17.39
19.94
19.94
19.94
15.53
16.79
16.48
17.57
17.57
17.57
17.57
19.29
19.29
19.29
19.29
20.57
20.57
20.57
23.39
20.67
20.67
20.67

Size
-213
-214
-217
-220
-223
-225
-226
-227
-228
-229
-230
-232
-235

-317
-329
-341
-348
-349
-359
-361

BEFORE
COMPRESSION

Dimensions
I.D.,mm
W.,mm
23.4
3.5
25.0
3.5
29.7
3.5
34.5
3.5
40.9
3.5
47.2
3.5
50.4
3.5
53.6
3.5
56.7
3.5
59.9
3.5
63.1
3.5
69.4
3.5
78.9
3.5
134.37
3.5
23.2
5.3
50.2
5.3
88.3
5.3
110.5
5.3
113.7
5.3
145.4
5.3
151.8
5.3
75.0
4.0
110.0
5.0
150.0
5.0
215.0
5.0

DURING
COMPRESSION

CAPFE ORING

Order Code
7855-805
7855-806
7855-808
7855-810
7855-813
7855-815
7855-819
7855-817
7855-816
7855-818
7855-820
7855-821
7855-822
7855-824
7855-826
7855-870
7855-827
7855-871
7855-828
7855-872
7855-876
7855-873
7855-829
7855-830
7855-832
7855-834

Dimensions
Size I.D.,mm W., mm
-010
5.3
1.78
-011
6.1
1.78
-012
7.7
1.78
-013
9.2
1.78
-015
12.4
1.78
-018
17.7
1.78
-021*
22.0
1.78
-022
23.5
1.78
-110
9.2
2.6
-111
10.8
2.6
-112
12.4
2.6
-113
13.9
2.6
-114
15.5
2.6
-115
17.1
2.6
-116
18.7
2.6
-118
21.9
2.6
-121
26.6
2.6
-122
28.2
2.6
-123
29.8
2.6
-125
33.0
2.6
-127
36.2
2.6
-128
37.8
2.6
-136
50.5
2.6
-210 18.6
3.5
-211 20.2
3.5
-212 21.8
3.5

Chemically
Resistant
PTFE
Encapsulation

Order Code
7855-836
7855-838
7855-840
7855-842
7855-874
7855-844
7855-846
7855-845
7855-847
7855-848
7855-875
7855-877
7855-864
7855-885
7855-860
7855-883
7855-850
7855-879
7855-887
7855-889
7855-861
7855-878
7855-880
7855-881
7855-884

Resilient
Rubber Core

Each
Call
22.79
22.88
22.88
26.72
26.72
26.72
27.54
27.54
27.54
27.54
27.54
28.62
35.07
30.70
29.07
33.84
51.96
52.49
56.31
63.29
28.10
28.63
59.65
75.27

AFTER
COMPRESSION

e
Valu

EFFECT
CAPFE bounces back

retains sealing capability


like elastomeric ring.

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

244

O-Rings

KALREZ 4079
7855 KALREZ 4079 ORINGS

Offer the resilience and sealing force of an elastomer with


chemical inertness and thermal stability similar to PTFE
fluorocarbon resin.

Sealing Performance
Compared with other elastomers, KALREZ is normally more resistant
to swelling and embrittlement and will retain these properties for a
longer period of time.
Compared with metal seals, KALREZ is easily installed and conforms
to the sealing surface despite irregularities due to improper assembly
or wear.
Compared with PTFE seals, KALREZ is not likely to creep or cold flow.

Chemical Resistance
KALREZ has excellent chemical resistance, far above that of other
commercial elastomers. KALREZ should be considered for service in
hot, corrosive environments, including:
Polar solvents (ketones, esters, ethers)
Strong organic solvents (benzene, dimethyl formamide,
perchloroethylene, tetrahydrofuran (THF)
Inorganic and organic acids (hydrochloric, nitric, sulfuric,
trichloroacetic) and bases (hot caustic soda)
Strong oxidizing agents (dinitrogen tetroxide, fuming nitric acid)
Metal halogen compounds (titanium tetrachloride, diethylaluminum
chloride)
Hot mercury/caustic soda
Chlorine, wet or dry
Inorganic salt solutions
Fuels, (ASTM Reference Fuel C, JP-5 Jet Fuel, aviation gas, kerosene)
Hydraulic fluids (SKYDROL1, 500A, PYDRAUL1 312, ANDEROL2
L-774, and transmission fluids)
Heat transfer fluids (DOWTHERM3A)
Oil well sour gas (methane, hydrogen sulfide/carbon dioxide/steam)
Steam

Thermal Stability
KALREZ ORings retain their elastic properties in long-term service at
temperatures as high as 316C and in intermittent service up to 327C.
Registered DUPONT Trademark
U.S. Trademark of Solutia Co., 2U.S Trademark of Tenneco Chemicals,
U.S. Trademark of Dow Chemical Co.

Dim., mm
Size
-006
-007
-008
-009
-010
-011
-012
-013
-014
-015
-016
-018
-110
-021
-111
-022
-112
-113
-114
-115
-116
-121
-136
-210
-211
-212
-217
-220
-225
-229
-105
-108
-118
-122
-123
-125
-127
-128
-213
-214
-216
-223
-226
-227
-228
-230
-327
-341
-348

I.D.
2.6
2.9
3.7
4.5
5.3
6.1
7.7
9.2
10.8
12.4
15.6
18.8
9.2
23.5
10.8
25.1
12.4
13.9
15.5
17.1
18.7
26.6
50.5
18.6
20.2
21.8
29.7
34.5
47.2
59.9
3.6
6.0
21.9
28.2
29.8
33.0
36.2
37.8
23.3
25.0
28.2
40.9
50.4
53.6
56.7
63.1
43.8
88.3
110.0

W
1.78
1.78
1.78
1.78
1.78
1.78
1.78
1.78
1.78
1.78
1.78
1.78
2.6
1.78
2.6
1.78
2.6
2.6
2.6
2.6
2.6
2.6
2.6
3.5
3.5
3.5
3.5
3.5
3.5
3.5
2.6
2.6
2.6
2.6
2.6
2.6
2.6
2.6
3.5
3.5
3.5
3.5
3.5
3.5
3.5
3.5
5.3
5.3
5.3

Order
Per
Code
Pkg.
(Use)
7855-601 38.44
7855-602 38.41
(S)
7855-604 42.11 (T,C,S)
7855-607 43.34
7855-605 44.52
7855-606 44.17 (T,J,S)
7855-608 44.97 (C,T,J)
7855-610 46.66 (C,T)
7855-612 47.85
(O)
7855-613 33.55 (O,G)
7855-614 51.77
(T,J)
7855-615 49.01 (J,S)
7855-616 79.58 (J,S)
7855-617 62.93 (C,T,G)
7855-618 71.84 (C,T,S)
7855-619 64.25 (C,T,G)
7855-620 90.10
7855-621 75.60
7855-622 112.39 (J,S)
7855-623 91.63
7855-626 104.23 (C,T,G)
7855-627 139.74 (C,T,G)
7855-629 333.16 (C,T,G)
7855-630 197.70
7855-632 200.92 (T,G)
7855-634 169.41
(T)
7855-640 194.56 (C,T,G)
7855-642 251.95 (T,G,J)
7855-644 395.72 (C,T,G,J)
7855-648 482.38 (C,T,G,J)
7855-650 46.21 (C,T,G)
7855-653 55.66 (T,G)
7855-655 109.44
(O)
7855-657 97.46 (C,T,J)
7855-658 86.16 (C,T)
7855-659
97.09
(O)
7855-670 108.51
(T,J)
7855-671 109.66 (J,S)
7855-675
97.37 (C,T,G)
7855-676
85.93 (T,G)
7855-677 107.77 (C,T,G)
7855-680 158.72 (C,T,G,J)
7855-684 163.52 (C,T,G,J)
7855-685 169.46
7855-686 192.32
7855-689 189.54
7855-690 297.53
7855-691 703.41
7855-692 738.57

USE REFERENCE CODES


T=AceThreds
G=Gaskets

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

S=Stopcocks
J=ORing Joints

C=Chromatographic Fittings
O=Special

Subject to Ace Discount (Page 4)

Net

O-Rings

CHEMRAZ 514
THE

Dimensions, mm
Size
-006
-007
-008
-009
-010
-011
-012
-013
-014
-015
-016
-018
-021
-022
-105
-108
-110
-111
-112
-113
-114
-115
-116
-118
-121
-122
-123
-125
-127
-128
-136
-210
-211
-212
-213
-214
-216
-217
-220
-223
-225
-226
-227
-228
-229
-230
-327
-341
-348

WHITE ORING

7859 CHEMRAZ ORINGSWhite


Molded of a perfluoroelastomer polymer, CHEMRAZ has the broadest
chemical resistance of any elastomeric material. Combines the
resilience and sealing force of an elastomer with chemical resistance
approaching that of PTFE.

Sealing Performance
Compared with other elastomers, CHEMRAZ is normally more resistant
to swelling and embrittlement and will retain these properties for a
longer period of time.
Compared with metal seals, CHEMRAZ is easily installed and
conforms to the sealing surface despite irregularities due to improper
assembly or wear.
Compared with PTFE seals, CHEMRAZ is not likely to creep or cold
flow.

Chemical Resistance
CHEMRAZ has excellent chemical resistance, far above that of other
commercial elastomers. CHEMRAZ should be considered for service
in hot, corrosive environments including:
Polar solvents (ketones, esters, ethers)
Strong organic solvents (benzene, dimethyl formamide,
perchloroethylene, tetrahydrofuran (THF)
Inorganic and organic acids (hydrochloric, nitric, sulfuric,
trichloroacetic) and bases (hot caustic soda)
Strong oxidizing agents (dinitrogen tetroxide, fuming nitric acid)
Metal halogen compounds (titanium tetra-chloride, diethylaluminum
chloride)
Hot mercury/caustic soda
Chlorine, wet or dry
Inorganic salt solutions
Fuels, (ASTM Reference Fuel C, JP-5 Jet Fuel, aviation gas, kerosene)
Hydraulic fluids (SKYDROL1, 500A, PYDRAUL1 312, ANDEROL2
L-774, and transmission fluids)
Heat transfer fluids (DOWTHERM3A)
Oil well sour gas (methane, hydrogen sulfide/carbon dioxide/steam)
Steam

Thermal Stability

I.D.
2.6
2.9
3.7
4.5
5.3
6.1
7.7
9.2
10.8
12.4
14.0
17.7
22.0
23.5
3.6
6.0
9.2
10.8
12.4
13.9
15.5
17.1
18.7
21.9
26.6
28.2
29.8
33.0
36.2
37.8
50.5
18.6
20.2
21.8
23.3
25.0
28.2
29.7
34.5
40.9
47.2
50.4
53.6
56.7
59.9
63.1
43.8
88.3
110.5

W
1.78
1.78
1.78
1.78
1.78
1.78
1.78
1.78
1.78
1.78
1.78
1.78
1.78
1.78
2.6
2.6
2.6
2.6
2.6
2.6
2.6
2.6
2.6
2.6
2.6
2.6
2.6
2.6
2.6
2.6
2.6
3.5
3.5
3.5
3.5
3.5
3.5
3.5
3.5
3.5
3.5
3.5
3.5
3.5
3.5
3.5
5.3
5.3
5.3

Order
Code
7859-501
7859-502
7859-504
7859-507
7859-505
7859-506
7859-508
7859-510
7859-512
7859-513
7859-514
7859-515
7859-519
7859-517
7859-503
7859-511
7859-516
7859-518
7859-520
7859-521
7859-522
7859-524
7859-526
7859-570
7859-527
7859-571
7859-528
7859-572
7859-576
7859-573
7859-529
7859-530
7859-532
7859-534
7859-536
7859-538
7859-539
7859-540
7859-542
7859-574
7859-544
7859-546
7859-545
7859-547
7859-548
7859-575
7859-578
7859-550
7859-579

Per
Pkg.
31.37
31.37
41.80
33.24
34.35
34.97
36.07
36.43
43.72
40.88
39.05
45.33
54.39
54.80
41.76
45.80
47.17
48.87
51.87
56.31
56.52
65.28
65.17
72.73
75.46
77.16
81.65
101.18
108.65
122.43
164.55
95.43
95.46
96.98
108.05
112.41
145.43
121.58
142.13
174.81
196.17
215.23
229.30
233.76
230.10
247.82
326.55
607.06
779.45

245

(Use)
(O)
(S)
(T,C,S)
(O)
(T,J,S)
(T,J,S)
(C,T,J)
(C,T)
(O)
(J,S)
(T,J)
(J,S)
(C,T,G)
(C,T,G)
(C,T,G)
(T,G)
(J,S)
(C,T,S)
(T,G,J)
(C,T,G,J)
(J,S)
(S)
(O)
(C,T,G)
(C,T,J)
(C,T)
(O)
(T,J)
(J,S)
(C,T,G)
(J,S)
(T,G)
(T)
(C,T,G)
(T,G)
(C,T.G)
(T,G,J)
(T,G,J)
(C,T,G,J)
(C,T,G,J)

(C,T,G,J)

USE REFERENCE CODES


T= AceThreds
G= Gaskets

S= Stopcocks
J= ORing Joints

C= Chromatographic Fittings
O= Special

CHEMRAZ ORings retain their elastic properties longer in


harsh chemical environments at temperatures from -30F to
higher than 220C.
Chemraz is a Registered Trademark of Greene Tweed & Co.
U.S. Trademark of Solutia Co., 2U.S Trademark of Tenneco
Chemicals,
3
U.S. Trademark of Dow Chemical Co.

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

246
Recirculators & Chillers

Recirculators & Chillers


Presto Series

Air Cooled Closed System


Circulators

Contact ACE
for complete
information
on Julabo
recirculators
and
accessories.

Presto A30

Presto A40

Presto A80

Call

12262-52

12262-38

Operating Temp Range

30 to 250

40 to 250

80 to 250

Temperature Stability

Ace Order Code

+/ .01 to .05

+/ .01 to .05

+/ .01 to .05

Heating Capacity

2.3kW

2.3kW

1.5kW

Cooling Capacity @ 100C

.50kW

1.2kW

1.2kW

Cooling Capacity @ 20C

.50kW

1.2kW

1.2kW

Cooling Capacity @ 0C

.40kW

.90kW

1.2kW

Cooling Capacity @ 20C

.20kW

.60kW

1.1kW

Cooling Capacity @ 40C

.10kW

1.1kW

Cooling Capacity @ 60C

.65kW

Cooling Capacity @ 80C

.10kW

25 LPM (7.25 PSI)

20 LPM

27 LPM

Pump Connection

M24 x 1.5 Male

M24 x 1.5 Male

M24 x 1.5 Male

Condeser Cooling

Air Cooled

Air Cooled

Air Cooled

9.53" x 22.95" x 24.09"

12.72" x 22.95" x 26.06"

16.93" x 25.59" x 49.53"

Flow Rate @ 10 PSI

Dimension (LxWxH)
Weight
Power Requirement
Each

137 lbs

174 lbs

362 lbs

208V, 1PH, 60Hz, 13.5A

208V, 1PH, 60Hz, 15A

208V, 1PH, 60Hz, 20A

Call

21350.00

33125.00

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Subject to Ace Discount (Page 4)

Net

Recirculators & Chillers

Recirculators & Chillers

247

Presto Series

Water Cooled Closed System


Circulators

Contact ACE
for complete
information
on Julabo
recirculators
and
accessories.

Ace Order Code

Presto W40

Presto LH50 PLUS

Presto W80

12262-50

12262-40

Call

Operating Temp Range

40 to 250

50 to 250

80 to 250

Temperature Stability

+/ .01 to .05

+/ .01 to .05

+/ .01 to .05

Heating Capacity

2.30kW

6.00kW

1.5kW

Cooling Capacity @ 100C

1.20kW

5.50kW

1.20kW

Cooling Capacity @ 20C

1.20kW

7.00kW

1.20kW

Cooling Capacity @ 0C

1.0kW

4.6kW

1.2kW

Cooling Capacity @ 20C

.60kW

2.60kW

1.10kW

Cooling Capacity @ 40C

.10kW

.50kW

1.10kW

Cooling Capacity @ 60C

.65kW

Cooling Capacity @ 80C

.10kW

20 LPM

20 LPM

27 LPM

Pump Connection

Flow Rate @ 10 PSI

M24 x 1.5 Male

M16 x 1 Male

M24 x 1.5 Male

Condeser Cooling

Water Cooled

Water Cooled

Water Cooled

Cooling Water Connection


Dimension (LxWxH)
Weight
Power Requirement
Each

G 3/4

G 3/4

G 3/4

12.72" x 22.95" x 26.06"

15.7" x 21.7" x 50"

16.93" x 25.59" x 49.53"

172 lbs

401 lbs

351 lbs

208V, 1PH, 60Hz, 15A

230V,3PH,60Hz, 27A

208V, 1PH, 60Hz, 20A

22175.00

33750.00

Call

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

248
Recirculators & Chillers

Recirculators & Chillers


Magnum 91 Temperature Control System

12274 JULABO MAGNUM 91 TEMPERATURE CONTROL


SYSTEM
Standard Features:
Two splash proof keypads, one remote
VFD and LCD displays
RS232 & 485 interfaces
Water cooled
3 point calibration
Rapid cool and heat-up
External Pt temperature sensor
Doesnt absorb any air humidity into the bath and prevents the
formation of ice
Compensates quickly for exothermic and endothermic reactions
Integrated high and low temperature safety cut-off and low liquid
level
Integrated warning, safety and supervision functions via 9
different sensors
Built-in castors for easy mobility
Electronically adjustable pump stages and pressures

Julabo Model

Magnum 91

Operating Temperature Range-C

91 to +250

Temperature Control

ICC

Temperature Stability, External-C

0.05

Display Resolution-C

0.01

Heater Capacity-W

6000

Cooling Capacity @ 20C-kW

4.5

Refrigerant

R404a+R23

Fill Volume-L

21.5

Overall Size, Inches

28 x 34.7 x 65

Weight-Lbs.

926

Pump Flow Maximum-L/min.

Contact ACE for full


information on Julabo
recirculators and accessories.

24-35 @ 11.631.9 psi

Ambient Temperature-C
Electrical

540
230v, 3p, 60Hz

ACE Order Code

12274-100
Priced upon request

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Subject to Ace Discount (Page 4)

Net

Recirculators & Chillers

Recirculators & Chillers

249

HighTech Series
12254 JULABO RECIRCULATORS/CHILLERS
Standard Features:
For external applications.
Simultaneous display of three temperature values
Bright backlit LCD display
Powerful pressure and suction pump with electronically
adjustable pump capacity
RS 232 interface
Temperature switchable between C and F
The workhorse series for pilot plants and jacketed
reaction vessels
Upgrade feature
Energy saving performance
Front panel access and drain valve
External Pt temperature senor available
12254-51

Julabo Model

FP50HL

FP51SL

50 to +200

51 to +200

Temperature Stability-C

0.01

0.05

Cooling Capacity @ 0C-kW

0.8

1.5

Pump Flow Maximum-L/min.

22-26

22-26

11

16.6 x 19.3 x 28.3

18.1 x 21.6 x 35.0

Operating Temperature Range-C

Fill Volume-L
Overall Size, Inches
Weight-Lbs.
Electrical*
ACE Order Code
Each

12254-33

125.4

198.4

230v, 60Hz

230v 3 ph, 60Hz

12254-33

12254-51

9975.00

12812.00

*Ultra-low temperature series HighTechs also available down to 90C

14108

14108 BATH FLUIDS


New thermal series bath fluids for Julabo circulators. Available in five liter jugs. Ten liter
size available upon request. Please note fluid color, temperature ranges, and flash points
to match your circulator. Other ranges are available just call Ace Glass!
Quantity,
Liters
5
5
5
5
5

Temperature
Range, C
30 to +80
60 to +250
90 to +170
90 to +60
60 to +110

Flash
Point
120
135
75
75
135

Color
Light Yellow
Clear
Clear
Clear
Clear

Order
Code
14108-21
14108-26
14108-27
14108-28
14108-30

Each
179.00
604.00
735.00
473.00
473.00

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

250

Recirculators & Chillers

12675 TUBING & INSULATION


Type
Viton Tubing, 8mm I.D.
Viton Tubing, 10mm I.D.
Viton Tubing, 12mm I.D.
Insulation for 8 & 10mm Viton Tubing
Insulation for 12mm Viton Tubing

Temperature
Range, C
50 to +200
50 to +200
50 to +200
50 to +100
50 to +100

Qty.,
Meters
1
1
1
1
1

Order
Code
12675-08
12675-10
12675-12
12675-40
12675-42

12675-08
Each
116.00
134.00
156.00
16.00
18.00

Contact ACE for other Julabo chillers


and accessories.
12675-40, -42

12677 TUBING & INSULATIONFor Julabo Presto Series Recirculators


Metal tubing, flexible and triple insulated, with two M24 x 1.5 female fittings. Temperature
range of 100 to +350C.
Qty.,
Order
Meters
Code
1.0
12677-10
1.5
12677-15
3.0
12677-20

12677

Each
379.00
497.00
928.00

12299/12300 MISCELLANEOUS ACCESSORIES


Common fittings and adapters for Julabo circulators. Additional fittings are available.
Please call ACE with your requirements.
Description
Nut M16x1 female, pair
Adapter M16x1 male to M16x1 male
Elbow 90 M16x1 female to M16x1 male
Adapter 1/4-inch NPT male
Adapter M16x1 female to 3/8-inch NPR male
Adapter M16x1 female to 1/2-inch NPR male
Adapter 1/4-inch tube
Adapter 3/8-inch tube
Adapter 1/2-inch tube

Qty.
2
1
2
2
2
2
2
2
2

Order
Code
12299-16
12299-20
12299-25
12299-28
12300-08
12300-12
12300-24
12300-28
12300-30

12299-16

12299-28

Each
22.00
39.00
221.00
49.00
89.00
107.00
89.00
89.00
89.00

12299-20

12299-25

12307 TEMPERATURE PROBES*


For all heating and refrigerated circulators equipped with a Pt100 temperature sensor
connection to measure and control the temperature of your external system.
Item
PLAIN Stainless Steel Sheath
Pt 100 Sensor, 12" long, " O.D., with 5' Cord

Order Code

Each

12307-12

353.00

12307-42

573.43

12307-44

609.00

12307-48

877.00

12307-02

279.00

PTFE COATED Stainless Steel Sheath


Pt 100 Sensor, 12" long, " O.D., with 10' Cord
Pt 100 Sensor, 24" long, " O.D., with 10' Cord
For 5, 10 & 20L REACTORS
Pt 100 Sensor, 48" long, " O.D., with 10' Cord
For 50L REACTOR

12307

Extension Cable
3.5 meters long (11.5') for Pt 100 Sensors
*Supplied with plug for connecting to Circulators.

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Subject to Ace Discount (Page 4)

Net

Rotary Evaporators

251

HEIDOLPH LABOROTA 20 Control


Large-Scale Rotary Evaporators
Up to 20 Liter Capacity
For safe, unattended, large-scale distillation of any solvent or mixture
in any research lab, pilot plant or scale-up facility, the LABOROTA 20
series provides the perfect tool for basic solvent purification, recovery
and scale-up applications!
The LABOROTA 20 series has been designed to incorporate all
leading safety features, giving you trust not only in the product and
the results of the distillation, but also in the safety and well-being
of the laboratory and your sample. In addition, the LABOROTA 20
series is available with a wide range of options, including 10 different
condenser configurations from which to choose, water and oil baths
for various heat load requirements, integrated vacuum controllers and
a host of other exclusive features that offer the benefit of the most
efficient distillations and the highest recovery rates.

Glassware

Evaporation Flask

Product Features:
Totally programmable through digital

operating panel
Designed for 24-hour continuous use
Condensate is automatically drained off to
any receptacle
Auto system automatically delivers sample
to evaporating flask via an intricate,
accurate sensor system
Auto controlled self filling bath system
Affordable alternative to 50 and 100L
evaporators
Integrated vacuum sensor and valve
Auto distillation capability through the use
of either the constant set-point pressure
feature (P const program) or via the vapor
temperature control feature
Built-in timer can automatically stop and
start reaction
Wide choice of glassware sets
Three-year manufacturers warranty from
Heidolph

Digital
Operating
Panel
Features individually
programmable ramps
for all parameters

Receiving
Flasks

Need high-capacity cooling?


Use your Heidolph LABOROTA 20 Series Rotary Evaporator with the
Julabo Model W40 Recirculating Chiller.

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

252

Rotary Evaporators

Non-Fogging Safety Glass

LABOROTA 20 Control Safety


13302-55
Metal Framed Safety Shield

13302 LARGE SCALE ROTARY EVAPORATORSafety


Designed for maximum safety and user protection, the LABOROTA 20 Control, Safety,
includes all the features listed on page 246, and includes a safety shield and glass
panels. It is ideal for large-scale distillations where maximum protection is needed.
Its safety shield is contructed of a metal frame, and the safety glass completely
covers the bath and evaporating flask providing excellent protection against
implosion and splashing. A safety sensor stops the rotation if the safety shield is
opened during the distillation process, and the non-fogging safety glass provides
clear, visible monitoring of the process in your evaporation flask. 230V, 60Hz.
Bath Type
Water
Water
Water
Water
Water
Water
Water
Water

Glassware Style
R
R Shorty
RC
RC Shorty
A
AC
A2
A2C

Order Code
13302-55
13302-59
13302-63
13302-67
13302-71
13302-75
13302-79
13302-83

13302 BASE/SUPPORT STAND Fits all LABOROTA 20 Units


This fully maneuverable, optional base unit features removable panels for storage of
glassware, solvents or accessories.
Base/Support Stand

Order Code
13302-310

Each
35603.05
38080.75
38401.08
39767.42
40440.77
42081.67
43036.14
44716.27

13302

Per Package
1923.76

Ask ACE how you can get this item for FREE!

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Subject to Ace Discount (Page 4)

Net

Rotary Evaporators

253

HEIDOLPH LABOROTA 20 Automatic


Large-Scale Rotary Evaporators
Up to 20 Liter Capacity

LABOROTA 20 Control
Automatic

Automatic Version
Designed for unattended distillations, especially for the most demanding
production and scale-up requirements!
With the unique LABOROTA 20 Control, Automatic, solvents or samples intended for
distillation are automatically delivered into the evaporating flask via an intricate and
highly accurate sensor system that detects the need for replenishing the evaporating
flask. Throughout the distillation, the condensate is automatically drained off to any
receptacle, carboy drum or vessel of choice. Upon completion of the distillation,
and once the distillate has been collected, the LABOROTA 20 Control, Automatic
completely shuts down and prepares itself for your next application.
In addition, the self-filling, digitally controlled heating bath allows for use over an
unlimited time, including evenings and weekends, so there's no need to worry
about manually replenishing the bath liquid, either the LABOROTA 20 Control,
Automatic does that, too!

13302 LARGE SCALE ROTARY EVAPORATOR Automatic, Economy


Unit includes all the product features listed on page 246, plus choice of water bath
with temperatures up to 100C for low-boiling solvents, or oil bath (available upon
request) with temperatures up to 180C for high boiling point solvents and more
demanding distillations. 230V, 60Hz.
Bath Type
Water
Water

Glassware Style
A
A2

Order Code
13302-108
13302-112

Each
62537.41
65015.11

13302 LARGE SCALE ROTARY EVAPORATOR

Automatic, Safety
Designed for maximum safety and user protection, the LABOROTA 20 Control, Safety,
includes all the features listed on page 246, and also includes a safety shield and glass
panels. It is ideal for large-scale distillations where maximum protection is needed. Its
safety shield is contructed of a metal frame, and the safety glass completely covers
the bath and evaporating flask providing excellent protection against implosion and
splashing. A safety sensor stops the rotation if the safety shield is opened during the
distillation process, and the non-fogging safety glass provides clear, visible monitoring
of the process in your evaporation flask. 230V, 60Hz.

Control Panel

Bath Type
Water
Water

Glassware Style
A
A2

Order Code
13302-208
13302-212

Each
66224.81
68473.43

Contact ACE for Bench-Scale Rotary Evaporators and


Rotary Evaporatore Glassware.

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

254

Replacement Glassware
Glassware Assemblies for Heidolph 13302 Rotary Evaporators

Glassware Assembly R

Glassware Assembly A

This glassware assembly


includes one ascending
condenser, one 20L
evaporating flask and one
10L receiving flask and is
recommended for all
standard distillations.

This glassware assembly


includes one descending
condenser, one expansion
vessel, one 20 L evaporating
flask, and one 10L receiving
flask, and is recommended
for solvents that tend to
splash and foam.

Also comes in a shorty version


that features a condenser
320mm shorter than standard
version. Distillation capacity
remains the same. Ideal for use
with hoods where height is
restricted.

Glassware Assembly A2

Glassware Assembly RC

This glassware assembly


includes one ascending and
one descending condenser,
one expansion vessel, one
20L evaporating flask and
one 10L receiving flask, for
low-boiling solvents and
highest recovery rates.

This glassware assembly is


identical to Assembly R and
features two receiving
flasks.

Also comes in a shorty version


that features a condenser
320mm shorter than standard
version. Distillation capacity
remains the same. Ideal for use
with hoods where height is
restricted.

Glassware Assembly AC

Glassware Assembly A2C

This glassware assembly is


identical to Assembly A and
features two receiving
flasks.

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

This glassware assembly is


identical to Assembly A2 and
features two receiving
flasks.

Subject to Ace Discount (Page 4)

Net

Replacement Glassware

255

Replacement Items for Use with

Heidolph Rotary Evaporators


(Turn to page 246 for Rotary Evaporators)

6701-12

Valu
e

6701-44

6701 LARGE EVAPORATOR FLASKS


Used with Heidolph 20L rotary evaporators. These large flasks are from blanks selected
for balance and quality. Necks are carefully welded to prevent rotational whip. Flasks
can be plastic coated upon request.
Cap.,
Liters
10
20

Overall
Height,
mm
345
383

Flange
A
O.D., mm
143
143

B
I.D., mm
118
118

C
mm
18
18

Heidolph
Part #
036303000
036302990

Order
Code
6701-12
6701-22

Each
394.14
506.07

6701 LARGE RECEIVER FLASKS


Used with Heidolph 20L rotary evaporators. This receiver flask is fabricated from blanks
selected for balance and quality. Center neck is a polished 40/25 joint; side neck is a
GL-18 thread, supplied with solid cap. At bottom is a 0-10mm Easy-Action stopcock
with a GL-18 side arm, supplied with a 3/8-inch hose connection tube. Flasks can be
plastic coated upon request.
Cap.,
Liters
10

Overall
Hght.,
mm
355

Center
Neck
40/25

Side
Neck
GL18

Bottom
Outlet
0-10mm/GL-18

Heidolph
Part #
03630340

Replacement GL-18 Cap

Order
Code
6701-44

Each
858.37

7622-107

3.59

lue
Va

13286 VAPOR TUBE for Heidolph 4000 Series


13286-30

Used as replacements with Heidolph Bench-Top Series rotary evaporators. Tube is


secured in rotary drive with low-stress plastic clip that seats into groove behind joint.
Available plain or with Firestone splash guard to protect against splash-up. The
13286-30 vapor tube comes standard with all Heidolph bench-scale rotary evaporators.
Type
Plain
Plain
Plain
Plain
w/Splash Guard
w/Splash Guard

Joint
24/25
24/40
29/42
45/50
24/40
29/42

Heidolph Part #

036301110

Order Code
13286-28
13286-30
13286-32
13286-34
13286-37
13286-39

Each
76.83
76.83
79.18
91.66
99.75
102.12

Color Coated Glassware


Ace Glass offers many of our existing glass vessels in various
coated versions. Flasks, Pressure Bottles, B
eakers, Bottles
and many other items listed in this catalog can be amber or
color coated on request. The coating is a proprietary process
and gives excellent UV protection characteristics. Contact
ACE for more details and pricing.
Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

256

Replacement Glassware

New

3965-10,
-15

3965-05,
-07

3965-36,
-34

3965-30,
-32

3965-26,
-28

3965-19,
-22

3965 CONDENSERS, COOLERS


Replacement borosilicate glass components for Buchi R220, R220EX, R220SE rotary evaporators. The condensers are available
in either poly-coated or plain, non-coated versions. All condensers fit easily into the glass sets listed below. ACE also offers a
non-jacketed version of the 3965-32 lower condensate cooler. Inner ball joints include CAPFE (PTFE-encapsulated silicone rubber)
o-rings. Black caps (included) are SVL-22 threads; red cap (included) is GL-14 thread.

Description
Triple-Coil Condenser
Triple-Coil Condenser
Triple-Coil Condenser
Triple-Coil Condenser
Glass Condenser (Bullfrog)
Glass Condenser (Bullfrog)
Glass Condenser (Bullfrog)
Glass Condenser (Bullfrog)
Condensate Cooler, Jacketed
Condensate Cooler, Jacketed
Condenser Cooler, Plain
Condenser Cooler, Plain

Fits
Glassware
Set
R, D2
R, D2
D, D2
D, D2
DB, DB2
DB, DB2
RB, DB2
RB, DB2
C, RB, R
C, RB, R
C, RB, R
C, RB, R

Coated?
Yes
No
Yes
No
Yes
No
Yes
No
Yes
No
Yes
No

Similar
to Buchi
Part No.
41159
41399
27308
41333
27825
46516
27824
41458
41162
46510

Fits
Buchi Models
R220,
R200EX, SE
R220
R200EX, SE
R220
R220EX, SE
R220
R220
R220
R220EX
R220
R220EX

Ball/Socket
DN Joint
Sizes
40
40
40
40
40
40
40
40
25
25
25
25

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Uses O-Ring
Size/Code
225/7855-844
225/7855-844
225/7855-844
225/7855-844
225/7855-844
225/7855-844
225/7855-844
225/7855-844
217/7855-840
217/7855-840
217/7855-840
217/7855-840

Order
Code
3965-05
3965-07
3965-10
3965-15
3965-19
3965-22
3965-26
3965-28
3965-30
3965-32
3965-34
3965-36

Each
3114.32
3008.75
3747.74
3642.17
5273.22
5162.37
5273.75
5067.36
843.50
738.99
791.78
765.38

Subject to Ace Discount (Page 4)

Net

Replacement Glassware

257

3967 EXPANSION TANK


New

Replacement borosilicate glass components for Buchi R220, R220EX, R220SE rotary
evaporators. Upper expansion tanks for Buchi glass sets available in either poly-coated
or plain non-coated versions. DN40 ball joints on top and bottom. Inner bottom ball joint
includes 7855844 CAPFE (PTFE-encapsulated silicone rubber) o-ring, size 225.

Description
Expansion Tank
Expansion Tank

Fits
Glassware Set
D, D2, DB, DB2
D, D2, DB, DB2

Coated?
Yes
No

Similar to
Buchi
Part No.
01165
41442

Fits Buchi
Models
R220
R220EX, SE

Order
Code
3967-10
3967-15

Each
1472.70
1367.13

3967-10,
-15

3970-15,
-18

3970 HEAD Distribution


Replacement borosilicate glass components for Buchi R220, R220EX, R220SE
rotary evaporators. Lower distribution heads with improved design with easy to use
AceThreds, PTFE stem valves. 3970-30 PTFE 0-20mm valve stem includes three
Kalrez o-rings. Stems are replaceable. Available poly-coated or plain non-coated.
Upper joint is DN40 outer ball joint. Red caps (included) are GL-14 thread; black cap
(included) is SVL-15 thread. DN25 inner ball joint on 397005 and 397010 includes
7855840 CAPFE (PTFE-encapsulated silicone rubber) o-ring, size 217. End thread
is #15 AceThred, for connection to 3978 valve assembly.

New
Description
Distribution Head-R
Distribution Head-R
Distribution Head-D
Distribution Head-D

Fits
Glassware Set
C, RB, R
C, RB, R
D, D2, DB, DB2
D, D2, DB, DB2

Replacement 0-20mm PTFE valve stem


(only) for 3970-05/-10 distribution
heads. Includes two 7855-626 size 116
and one 7855-622 size 114 Kalrez
o-rings.

Coated?
No
No
Yes
No

Similar to
Buchi
Part No.
41373
46511
41335
41307

Fits Buchi
Models
R220
R220EX, SE
R220
R220EX, SE

Order Code
3970-05
3970-10
3970-15
3970-18

Each
1372.41
1266.84
1008.19
902.62

No

R220EX, SE

3970-30

237.53

3970-05,
-10

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

258

Replacement Glassware

3971 TRAPS C Set


Replacement borosilicate glass components for Buchi R220, R220EX, R220SE
rotary evaporators. Inner and outer cold trap components for Buchi C glassware Set.
Available poly-coated or plain non-coated. DN40 inner ball joints include 7855-844
CAPFE (PTFE-encapsulated silicone rubber) o-rings, size 225. Black cap (included)
is SVL-22 thread. Top 7855-881 CAPFE o-ring (included) for 397103 and 397105 is
for 150mm grooved top flat flange. 150mm clamp and PFA cap, listed below, must be
ordered separately.

Description
Inner Cold Trap
Outer Cold Trap
Outer Cold Trap
PFA Cap (Lid)
Duran Quick Clamp

Fits
Glassware
Similar to Buchi
Fits
Set
Coated?
Part No.
Buchi Models
C
No
25124
220, 220EX, 220SE
C
Yes
25978
220
C
No
46518
220EX, 220SE
C
No
25979
All
C
No

All

Order
Code
3971-01
3971-03
3971-05
3971-21
6517-27

3971-03,
-05

New

Each
1689.12
3483.81
3378.24
526.79
117.67

3971-01

3976 TUBES Vapor Duct Steam Tube, Glass


Replacement borosilicate glass vapor tubes for Buchi R220, R220EX, R220SE rotary
evaporators. 3976-05 contains a Porosity C (25-50 micron) glass frit.

Description
Vapor Duct Tube
Vapor Duct Tube w/C Frit

Fits
Glassware
Set
Coated?
All
No
All
No

Similar to
Buchi
Part No.
41084
41100

Fits Buchi
Models
R220
R220

Order Code
3976-03
3976-05

Each
918.46
1055.70

3976-03

New

3976-05

3976 TUBE Vapor Duct Steam Tube, Stainless Steel


Replacement 316 stainless steel vapor tube for Buchi R220, R220EX, R220SE rotary
evaporators.

Description
Vapor Duct Tube

Fits
Glassware
Set
All

Coated?
No

Similar to
Buchi
Part No.
41084

Fits Buchi
Models
R220

Order
Code
3976-10

New

Each
2164.19

3976-10

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Subject to Ace Discount (Page 4)

Net

Replacement Glassware

259

New
3973-01, -03

3973-08, -10

3973-04, -06

3973-30

3973 TUBES Connecting Tubes, Receiving


Replacement borosilicate glass tubes for Buchi R220, R220EX, R220SE rotary evaporators. Connecting glass tubes for Buchi
receiver assembly. Available either poly-coated or plain, non-coated. 3973-30 PTFE 0-20mm valve stem includes three Kalrez
orings. See page 257 for 6726 receiver flasks. DN25 inner ball joints have 7855-840 CAPFE (PTFE-encapsulated silicone rubber)
o-rings, size 217.
Coated?

Similar to
Buchi Part No.

Fits Buchi
Models

Order
Code

Yes
No
Yes
No

41048-1
41447-1
41049 / 41047-2
46520-2

R220
R220EX, SE
R220
R220EX, SE

3973-01
3973-03
3973-04
3973-06

791.78
686.21
1055.70
950.13

Upper Branching Piece ACE Valve


Upper Branching Piece ACE Valve

Yes
No

41053
46521

R220
R220EX, SE

3973-08
3973-10

791.78
686.21

Replacement 0-20mm PTFE valve stem (only) for 3973


branching tubes only. Includes two 7855-626 size 116 and
one 7855-622 size 114 Kalrez o-rings.

No

All

3973-30

237.53

Description
For Double Receiver Assembly
Upper Branching Piece #1 Right, ACE Valve
Upper Branching Piece #1 Right, ACE Valve
Upper Branching Piece #2 Left, ACE Valve
Upper Branching Piece #2 Left, ACE Valve

Each

For Single Receiver Assembly

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

260

Replacement Glassware

3974-25,
-27

3974-30,
3974-30,
-33 -33

3974-12,
-13

New

3974-20,
-22

3974-15,
-18

3974 TUBES Connecting, Glass Sets


Replacement borosilicate glass tubes for Buchi R220, R220EX, R220SE rotary evaporators. Upper and lower connecting tubes for
glass distillation sets available poly-coated or plain non-coated. The 3973-20 codes through -27 have two GL14 thread ports (with
red caps) on top for thermosensor, or for easy clean out. DN40 inner ball joints on -12, -13, -20, -22, -25, and -27 include 7855-844
CAPFE (PTFE-encapsulated silicone rubber) o-rings, size 225. Bottom DN25 ball joint on -15 and -18 includes 7855-840 CAPFE
o-ring, size 217. 3974-12 and -13 both include an SVL-22 thread black cap and a GL14 thread red cap.
Description
Vacuum Connector Tube
Vacuum Connector Tube
Y Bottom Tube
Y Bottom Tube
U Top Connect Tube
U Top Connect Tube
U Top Connect Tube
U Top Connect Tube
Y Bottom Tube
Y Bottom Tube

Fits Glassware Set


DB, D
DB, D
DB, D2, D
DB, D2, D
DB, DB2
DB, DB2
D, D2
D, D2
DB2
DB2

Coated?
Yes
No
Yes
No
Yes
No
Yes
No
Yes
No

Buchi Part No.


01129
41443
01169
46513
27837
46515
27150
46512
41166
46514

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Fits Buchi
Models
R220
R220EX, SE
R220
R220EX, SE
R220
R220EX, SE
R220
R220EX, SE
R220
R220EX, SE

Order
Code
3974-12
3974-13
3974-15
3974-18
3974-20
3974-22
3974-25
3974-27
3974-30
3974-33

Each
633.42
527.85
1425.20
1319.63
2109.29
1979.44
3035.14
2929.57
1476.92
1371.35

Subject to Ace Discount (Page 4)

Net

Replacement Glassware

261

New
3978-05
3978-07

3978 VALVES
Replacement borosilicate glass for Buchi R220, R220EX, R220SE rotary evaporators. PTFE valve stem parts and valve assemblies,
with Kalrez o-rings, for receiving flasks and 3970 lower distribution heads. Socket joint on 3978-07 is DN25. Joints on 3978-05 are
PTFE, AceThred #11 and #15, and they include CAPFE (PTFE-encapsulated silicone rubber) o-rings. Hose coupling on -07 is size
G, for 5/18-inch I.D. tubing. Replacement o-rings for the bushings on 3978-05 are CAPFE size 110 (7855-816) for side port and
CAPFE size 112 (7855-820) on end.
Fits
Description
Glassware Set
Glass Body (only) for 3978-05 Inlet Valve
All
Complete Inlet Valve Assembly for
All
Distribution Head
Bottom Drain Valve (Receiver)

Replacement PTFE valve stem (only) for valves. Includes two


7855-606 size 011 and one 7855-618 size 111 Kalrez o-rings.

Coated?
No

Similar to Buchi Fits Buchi


Part No.
Models
41346
All

Order Code
3978-01

Each
626.03

No

41348

All

3978-05

791.78

No

41061

All

3978-07

332.55

No

All

3978-33

142.52

ACE Glass introduces...

A full line of Replacement Glassware


for Bench-Scale Rotary Evaporators!
Ace Glass, founded in 1936, continues our long tradition of manufacturing high
quality specialty glassware. We would like to introduce a new, comprehensive
line of glassware to fit todays popular rotary evaporators. Ace also offers
both custom glass and glass repair services for rotary evaporators. Ace Glass
rotary evaporator replacement glass, all manufactured in the USA to exacting
specifications and standards.
Toll-free:

us
Contact
r a copy
today fo ew
of our n
e!
brochur

Toll-free fax:

800-223-4524 800-543-6752
856-692-3333 Fax: 856-692-8919

www.aceglass.com
sales@aceglass.com

P.O. Box 688


Vineland, NJ 08362-0688

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

262

Replacement Glassware

6726 FLASKSReceiving
Replacement borosilicate glass for Buchi R220, R220EX, R220SE rotary evaporators.
Receiving flasks are designed to fit all large-scale rotary evaporators. Now available in
coated, plain, non-coated, amberized and 6727 jacketed versions. Side necks include
7647-40 SVL-22 threaded black caps. Top and bottom socket joints are DN25, and bottom
joint includes 7855-840 CAPFE (PTFE-encapsulated silicone rubber) o-ring, size 217.

Description
Receiving Flask 10L
Receiving Flask 10L
Receiving Flask 20L
Receiving Flask 20L
Receiving Flask 10L Amber
Receiving Flask 20L Amber

Coated?
Yes
No
Yes
No
No
No

Similar to
Buchi
Part No.
37569
46519
41446
28671

Fits
Buchi
Models
All
All
All
All
All
All

SVL-22 vent cap wtih PTFE insert

Order
Code
6726-10
6726-15
6726-20
6726-25
6726-30
6726-32

Each
1102.95
992.10
1441.03
1330.18
1102.95
1441.03

7647-40

36.23

6726-20

New

6726-30

6727 FLASKSReceiving, Jacketed


Standard receiving flask for all rotary evaporators. Same as 6726 except, with outer jacket
for cooling/heating of contents. Inlet/outlet connections are 28/15 o-ring ball joints and
include 7855-726 FETFE o-rings, size 116. Top and bottom joints are DN25. Bottom
inner ball joint includes 7855-840 CAPFE (PTFE-encapsulated silicone rubber) o-ring,
size 217. Side joint is SVL-22 thread, with 7647-40 black cap included.
Description
Receiving Flask 8L

Coated?
No

Fits Rotavap
Models
Order Code
All
6727-10

SVL-22 Vent cap with insert

7647-40

6727

New

Each
1291.39
36.23

ACE Custom Glass


Design Service
www.aceglass.com

1-800-223-4524
Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Subject to Ace Discount (Page 4)

Net

Replacement Glassware

263

Large Evaporator Flasks


for All Rotary Evaporators
6702 FLASKS Evaporation, Large Scale
These large sized evaporation flasks are fabricated from heavy wall flask blanks
selected for balance and quality. Necks are carefully fabricated to prevent rotational
whip. Flask are now available in clear plain glass or poly-coated or amberized.
Amber coated flask can protect light sensitive contents. The XL sizes flange,
(see table), is compatible with the 150mm and standard for Buchi Model R220
rotary evaporators.

1. Select Flange Size.

A
C

A
O.D., mm
(Inches)
90 (3.5)
100 (3.9)
110 (4.3)
149.5 (5.9)

Flange Size
Designation

S (Small)
M (Medium)
L (Large)
XL (Extra Large)

OVERALL
HEIGHT

B
I.D., mm
(Inches)
67 (2.7)
72 (2.8)
83 (3.3)
118.8 (4.7)

C
Thickness
(mm)
18
19
23
21

2. Select Flask Capacity and match


with Flange Size.
Capacity,
Liters
6
6
6
6
6
6
10
10
10
10
10
20
20
20
20

Easy Order Instructions


1. Determine flange size (A) O.D., (B) I.D.,
(C) thickness (see diagram).
2. Match flask capacity with overall height
and flange size.

Similar to
Buchi Part
No.
27470
27470
27470
27470
27470
27470
27469
27469
27469
27469
27469
27468
27468
27468
27468

Overall
Height, mm
300
325
380
295
380
351
350
335
413
410
380
375
435
435
413

Flange
Size
S
M
M
L
L
XL
S
M
M
L
XL
M
M
L
XL

Order
Code
6702-05
6702-07
6702-10
6702-15
6702-17
6702-19
6702-20
6702-25
6702-27
6702-30
6702-33
6702-35
6702-37
6702-40
6702-44

Each
201.28
212.20
212.20
260.37
269.08
279.48
316.12
334.46
340.41
378.48
419.03
506.66
495.78
516.96
564.94

6702 COVER For Evaporating Flask, Polyethylene


Polyethylene dust cover for evaporating flasks with 149.5mm I.D. Has integral o-ring to
keep a tight seal. Comes complete with Viton o-ring.

New

Similar to Buchi
Part No.

Order
Code

Each

42895

6702-300

50.13

6702

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

264

Replacement Glassware

6702 FLASKS Evaporation, Large Scale, Poly-Coated


Same as 6702 on previous page, but poly-coated for added safety. Plastic coated flasks
are clear and will withstand temperatures up to 100C.
Capacity,
Liters
6
6
6
6
6
6
10
10
10
10
10
20
20
20
20

Similar to Buchi
Part No.

27470

27469

27468

Overall
Height, mm
300
325
380
295
380
351
350
335
413
410
380
375
435
435
413

Flange
Size
S
M
M
L
L
XL
S
M
M
L
XL
M
M
L
XL

Order
Code
6702-105
6702-107
6702-110
6702-115
6702-117
6702-119
6702-120
6702-125
6702-127
6702-130
6702-133
6702-135
6702-137
6702-140
6702-144

Each
276.56
288.27
288.27
339.91
376.40
678.90
399.68
419.34
427.81
466.54
900.68
603.97
594.73
617.70
973.30

New

6702

6702 FLASKS Evaporation, Amberized


Same as 6702 above, except with an amber coating to protect light sensitive contents.
The XL size matches Buchi large-scale rotary evaporators. Plain, not coated.
Capacity,
Liters
6
10
20

Similar to Buchi
Part No.

Overall
Height, mm
351
380
413

Flange
Size
XL/149.5
XL/149.5
XL/149.5

Order
Code
6702-219
6702-233
6702-244

6702

New

Each
495.71
634.95
818.75

6720 FLASKS Evaporation, Indented


These flasks are also referred to as drying flasks. They are particularly suited for drying
of powdered samples. The baffles, indented into the glass, provide better circulation and
mixing of the powders while rotating. Plain, not coated. NOT suitable for vacuum operation.
Capacity,
Liters
10
20

Similar to Buchi
Part No.
28592
28593

Overall
Height, mm
380
413

Flange
Size
XL/149.5
XL/149.5

Order
Code
6720-10
6720-20

6720

New

Each
692.81
859.08

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Subject to Ace Discount (Page 4)

Net

Replacement Glassware

265

Spare Parts, Glassware Assemblies


R

RB

3965-26, -28

3965-05, -07

3978-05
3973-30
3978-05
3973-30

3970-05
3965-30, -32

3970-05
3965-30, -32

3971-21

Interchangeable
Receiver (W)

3973-01,
-03

6517-27
3971-01

3973-04, -06

6726 Series
3971-05, -03
3978-05
3973-30

3978-07

Single Receiver
(E)
3973-08, -10
3970-05
3965-30, -32

6726 Series

3978-07

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Replacement Glassware

266

Spare Parts, Glassware Assemblies


D

D2

3974-25, -27

3974-25, -27

3965-10, -15

3965-10, -15

3967-10, -15

3967-10, -15
3965-05,
-07

3974-12, -13
3970-15, -18

3974-15, -18

3978-05

3970-15, -18

3974-15, -18

DB

3978-05

DB2

3974-19, -22

3974-19, -22

3967-10,
-15

39651-26,
-28

3965-20, -22
3967-10,
-15

3974-12, -13

3970-15,
-18

3978-05
3974-30, -33

3965-20,
-22

3978-05
3974-30 -33

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

3970-15,
-18

Subject to Ace Discount (Page 4)

Net

Big Columns

267

BIGCOLUMNS
All types of
special combinations
made to order
Heads can be supplied with
additional threads or joints or
combination of both
Columns available in various
lengths and diameters

5844 ADAPTER for Swagelok


PTFE adapter for use at top of 5860 column head or at bottom of 5862 column to connect
tubing via Swagelok type connector to #50 AceThred, other end has 1/4-inch NPT female
thread. Supplied with one FETFE oring. For extra orings, see 7855-729.
Order Code
5844-78

Each
172.15

5860 COLUMN HEAD


For use with 5862 chromatography column. With #50 AceThred center neck and/or
two #15 AceThred side necks and 4- or 6-inch flange at bottom, ground flat. Use with
6517 clamp.

5844

Flange Size
4-inches
6-inches
6-inches

5860

Center Neck
50
50
50

Side Necks
None
None
15

Order Code
5860-24
5860-28
5860-32

Each
234.29
285.18
398.71

5862 COLUMN (#50)

6517

Large size chromatography columns with oring grooved flat flange at top for easy access
to column. Flange is supplied with silicone oring to make seal when using 5860 head
with 6517 clamp. 4- and 6-inch I.D. columns are tapered to #50 AceThred at bottom that
accepts 5844 adapter, or 5848 and 5835 adapters. For replacement orings, see below.
Flange Size/
Col. I.D., in.
4
4
4
4
6
6
6
6

5862
(#50)
5862
(#80)

5857
5843

5848
5857

Length mm (in.)
300 (12)
450 (18)
600 (24)
1200 (48)
450 (18)
600 (24)
1200 (48)
1800 (72)

Order Code
5862-43
5862-45
5862-47
5862-49
5862-58
5862-62
5862-65
5862-68

Each
475.82
497.89
542.43
636.16
804.61
884.11
999.53
1062.72

Replacement Silicone ORings


For 4-inch Flange
For 6-inch Flange

Order Code
7855-254
7855-260

Each
21.39
40.00

Order Code
7855-880
7855-881

Each
28.63
59.65

Replacement CAPFE ORings


7506-03
B

5835-17

For 4-inch Flange


For 6-inch Flange

A
5835

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

268

Big Columns

BIGCOLUMNS
5862 COLUMN (#80)
Large size columns with oring grooved flat flange at top for easy access to column.
Flange is supplied with silicone oring to make seal when using 5860 head with 6517
clamp. Columns are tapered to #80 AceThred at bottom that accepts 5857 adapter.

5862

Length
18 inches
18 inches
18 inches
24 inches
24 inches
24 inches
48 inches
48 inches
48 inches

Flange Size
6 inches
6 inches
6 inches
6 inches
6 inches
6 inches
6 inches
6 inches
6 inches

Order Code
5862-10
5862-18
5862-26
5862-12
5862-20
5862-28
5862-14
5862-22
5862-30

Inner Diameter
6 inches
8 inches
12 inches
6 inches
8 inches
12 inches
6 inches
8 inches
12 inches

Each
910.45
1239.82
1638.36
966.02
1312.49
1827.55
1092.17
1520.41
2036.11

6517 CLAMP
6517

Stainless steel quick release clamp with three retaining clips for connecting 5860 head
and 5862 column.
For Flange Size
4 inches
6 inches

Order Code
6517-25
6517-27

Each
98.23
117.67

5848 SUPPORT PLATEPerforated


73mm diameter glass plate with 1x3mm rectangular slits for supporting column packing.
Used with 5857.
5848

Order Code
5848-60

Each
86.83

5843 COUPLING Reducing, with Support


For connecting 5835 bottom drip stopcock adapter to bottom of 5862 chromatography
column with leak-tight oring seals. One end is #50 AceThred for connecting to
column, the other #25 AceThred is for connecting to 5835B adapter. #50 end of
coupling is supplied with Porosity A glass packing support, press fitted, with taper
below disc to 25 I.D. For replacement supports, see below. Supplied with two FETFE
orings. For replacement orings, see 7855-729 (for #50); or 7855-727 (for #25).
Order Code
5843-74

5843

Each
248.13

Replacement Glass Packing Supports


Porosity A (145-175 micron)
Porosity B (70-100 micron)

Order Code
5848-49
5848-58

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Each
130.80
130.80

Subject to Ace Discount (Page 4)

Net

Big Columns

269

BIGCOLUMNS
5835 ADAPTER Bottom Drip, with 1:5 PTFE Stopcock
Drip tip for bottom of 5862 column using 5843 coupling. One end has #25 AceThred,
other with drip tip and 4mm bore PTFE stopcock for controlling flow.
Order Code
5835-17

5835-17

Each
129.37

5835 BOTTOM OUTLET VALVE with or without Stopcock


Type A With 0-8mm threaded stopcock for controlling flow.

Type B Straight stem without stopcock. Both stems to take 3/8-inch Swagelok fittings.
Secured to 5857 bottom adapter with 7506-03 bushing.
Type
A
B

Order Code
5835-32
5835-34

Each
126.39
35.94

B
A

5835

5857 BOTTOM ADAPTER UHMWPE* or PTFE


Fits #80 AceThred. Recessed for 5848 perforated support plate and 5857 retaining ring. Your
choice of bottom threaded for #11 AceThred bushing 7506-03 to secure 5835 outlet valve,
or threaded to accept 3/8-inch NPT fitting. For replacement FETFE orings, order 7855-764.
UHMWPE*
Adapter, #80 Thred
Support Plate
Retaining Ring
Bushing
Connector, 3/8-inch
COMPLETE

#11 AceThred Hole


Order Code
Each
5857-30
124.06
5848-60
86.83
5857-50
13.98
7506-03
11.86

5857-44
236.73

3/8-inch NPT Hole


Order Code
Each
5857-35
104.22
5848-60
86.83
5857-50
13.98

12770-27
31.59
5857-46
236.62

#11 AceThred Hole


3/8-inch NPT Hole
Order Code
Each
Order Code
Each
PTFE
Adapter, #80 Thred
5857-60
267.57
5857-64
267.57
Support Plate
5848-60
86.83
5848-60
86.83
Retaining Ring
5857-52
15.30
5857-52
15.30
Bushing
7506-03
11.86

Connector, 3/8-inch

12770-27
31.59
COMPLETE
5857-67
381.56
5857-69
401.29
*UHMWPE Ultra High Molecular Weight Polypropylene

5857

5861 ADAPTER
Bottom filter adapter for use with our 6384,6386 & 6388 glass reactor bodies and our 6390
all PTFE reactor bodies. Adapter differs from our codes 5838-83 & 5857-86 in that the
3/8-inch female NPT is located as a side discharge rather than thru the bottom. Adapters
are PTFE and include a CAPFE o-ring, PTFE retaining ring, 100 micron polyethylene filter
disc and 350 micron polypropylene filter screen. Code -07 includes a glass filter support
from our 5848 product family. See also our 5814 family for filter support screen options.
For Thread Size
50
80
CAPFE oring, replacement for #50, Pkg/1
CAPFE oring, replacement for #80, Pkg/1

Order Code
5861-03
5861-07
7855-829
7855-864

5861

Each
234.71
323.51
23.39
28.62

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

270

Big Columns
5820 COLUMNS Large Size, with Ace-Threds
Borosilicate glass columns for liquid chromatography, ion-exchange or activated carbon
work featuring Ace-Thred connections. Threaded ends are compatible with fittings shown
with other chromatography systems listed. Fittings can be used with these columns and
offer easy-to-change support screens with a variety of openings never before offered.
50 psi maximum pressure.
Column
I.D., mm
75
75
75
100
100
150
150
150
150

5820

Minimum
Effective Length,
mm (Inches)
300 (12)
600 (24)
1200 (48)
1200 (48)
1800 (72)
600 (24)
1200 (48)
1800 (72)
2400 (96)

Approx.
Capacity, Ace-Thred
mL
Size
Qty.
1,320
50
1
2,650
50
1
5,300
50
1
9,430
50
1
14,940
50
1
10,600
50
1
21,200
50
1
31,800
50
1
42,200
50
1

Order
Code
5820-105
5820-107
5820-109
5820-116
5820-119
5820-121
5820-125
5820-129
5820-133

Each
512.43
554.17
642.86
733.03
808.54
1094.99
1175.85
1256.70
1338.87

Note: Columns of larger I.D. and longer than listed above can be fabricated.
Also, most sizes can be jacketed. Call or email for details.
Support stand for 100 and 150mm columns listed under 12099.

5862 COLUMN EXTENDER


Glass extenders that can be added to 5862 columns to increase column height. Extenders
have an oring grooved flat flange on one end to attach 5860 column head and ground
flat flange at other end to attach the 5862 column. Supplied with one silicone oring. Use
6517 quick release clamp to secure sections.

5862

Flange Size/
Column I.D., in
4
4
4
6
6
6

Length mm (in)
300 (12)
450 (18)
600 (24)
300 (12)
450 (18)
600 (24)

Order Code
5862-72
5862-73
5862-74
5862-77
5862-78
5862-79

Each
266.26
266.26
307.74
554.83
597.85
639.61

5867 SUPPORT STAND for Large Columns

5867

Newly designed four-post stands for large scale chromatography columns feature all
stainless steel construction. Each stand is designed to accept either 24-, 48-, or 72-inch
length 5862 columns. With 150mm (6-inch) flange and 6-, 8-, or 12-inch diameter body.
Supplied with two (2) column support rings with 140mm and 175mm openings. Each
stand is designed to accommodate the height of the column and has a PTFE collar at
the bottom that accepts and supports the tapered bottom of the column. Each stand
has an adjustable stainless upper collar assembly that supports the top of the column.
All stands have locking casters for mobility.
Fits Column
(Height)
24 inches
48 inches
72 inches

Order Code
5867-24
5867-48
5867-72

Dimensions, Inches
(W x D x H)
15 x 15 x 40
15 x 15 x 60
15 x 15 x 85

Each
2391.36
2858.84
3099.77

Custom sizes are available!

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Subject to Ace Discount (Page 4)

Net

Big Columns

271

5868 SUPPORT STAND for Bench-Scale Columns


Newly designed single-post stand for 12- and 18-inch height chromatography columns.
H shaped base and a single 122cm high x 1-inch diameter stainless steel bar give great
stability for the large-scale columns. Stand comes complete with base, rod, base plate,
clamp holder and chain clamp.
Order Code
5868-122

Overall Height
125cm

Each
583.61

5848 FILTER DISC


Filter disc for use with 5837 and 5838 adapters. Available in polyethylene (100 micron
pore size), and borosilicate glass Porosity A (145-174 microns), B (70-100 microns),
C (25-50 microns) and D (10-20 microns). Sold in packages. (Caution: These discs are
intended to be removable. However, because of the tight fit, the glass disc may break
when being removed.)
Polyethylene
100 microns
For
Adapter Pkg.
Size,mm Qty.
11
6
15
6
25
6
50
6
80
1

Order
Code
5848-07
5848-10
5848-14
5848-17
5848-19

5868

Porosity A
145-174 microns

5848

Borosilicate Glass
Porosity B
Porosity C
70-100 microns
25-50 microns

Porosity D
10-20 microns

Per.
Pkg.
14.44
14.44
16.58
34.99

Order
Code
5848-43
5848-44
5848-47
5848-49

Per
Pkg.
58.53
58.53
66.12
130.80

Order
Code
5848-52
5848-54
5848-56
5848-58

Per
Pkg.
58.53
58.53
66.12
130.80

Order
Code
5848-21
5848-23
5848-25
5848-28

Per
Pkg.
58.53
58.53
66.12
130.80

Order
Code
5848-31
5848-33
5848-35
5848-38

Per
Pkg.
58.53
58.53
66.12
130.80

9.03

5848-100

126.50

5848-120

129.55

5848-122

147.23

5848-124

161.95

5814 SCREEN SUPPORT FILTER DISCS Polypropylene


Screen support filter pre-cut discs used with 5857 and 5861 end fitting adapters.
For
350
295
210
105
AceThred
Micron
Micron
Micron
Micron
Each
Size
Qty. Order Code Order Code Order Code Order Code Pkg/12
9.67
11
12
5814-42
5814-52
5814-62
5814-82
15
12
5814-44
5814-54
5814-64
5814-84
11.56
25
12
5814-46
5814-56
5814-66
5814-86
19.33
50
12
5814-48
5814-58
5814-68
5814-88
36.45
Note: Discs can also be supplied in polyethylene and fluorocarbon; however, since they
are not stock items, a minimum quantity will be supplied. Phone for quotation.

5814

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Big Columns

TH

A N N I V E R S A R Y

TED
RA

ACE G

S
A

C
N
OR
I
S

272

1936 2011

USA

NE

N
,
LAND

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

VI

Subject to Ace Discount (Page 4)

Net

Process Pipe

273

Beaded Process Pipe


Ace Glass has been manufacturing and fabricating
glassware and equipment for the scientific and research
communities for over 75 years. ACE fabricates glass
process pipe here in the USA, from medium- and heavywall borosilicate tubing such as Scimax and Schott
Duran, to provide you with a high quality product to fit
into your process stream. From glass process pipe to
glass reactors and pilot plants, to temperature equipment
and sensors, ACE offers a broad line of products to the
process engineer. ACE will also fabricate custom sizes
and shapes for your needs if you dont see what you
need in this catalog, contacts us at www.aceglass.com
to discuss your needs with our engineering staff.
Glass meets an ASTM spec for borosilicate glass, ASTM
E-438 and Federal spec DDG541B. The system can be
constructed by a contractor to meet ASTM spec C105390, ASTM spec C1053-00, Federal spec DDG541B,
Military spec MILP 2256B(YD) when it is all put together
using the same pipe and couplings.
Glass also meets specs for USP Type 1 glass.

Process Piping Systems

Low Maintenance Cost


Over the life of a piping system this can be the smallest
cost component for glass piping systems and the largest
cost consideration for many other competitive piping
systems. Chances are that low maintenance cost is the
prime reason for considering, specifying, and operating
a glass piping system.

Properties of Borosilicate Glass


Chemical Composition
The borosilicate glass used in the manufacture of our
pipeline components conforms to the standard ASTM
E 438 and has the following approximate composition.
Component

% By Weight

SiO2

81%

B2O3

13%

Na2O

4%

Al2O3

2%

Industry has long regarded borosilicate glass piping


components to be one of the best corrosion resistant
materials of construction. For a wide range of
manufacturing and process piping applications Ace Glass
brand glass pipe installations have provided excellent
service in the most difficult piping applications, positive
evidence of its outstanding performance. The use of glass
offers many advantages over other conventional piping
materials such as:

Chemical Resistance

Long Service Life

Under service conditions, the effects of turbulence and


some trace chemicals in solution may increase or decrease
the rate of attack. Therefore, it is not possible to give
precise figures for corrosion by hydrofluoric acid and
caustic solutions, but Figures 1 and 2 show typical rates.

Low-expansion borosilicate glass is resistant to


almost all substances except hydrofluoric acid, hot
concentrated phosphoric acid and strong alkalis at
elevated temperatures.

Borosilicate glass is resistant to almost all substances


except hydrofluoric acid, phosphoric acid and hot strong
caustic solutions. Of these, hydrofluoric acid has the
most serious effect and, even when a solution contains
a few parts per million, corrosion will occur. Phosphoric
acid and caustic solutions at elevated temperatures will
also attack glass.

Product Purity
All glass piping systems are comprised of chemically
inert borosilicate glass and TFE gaskets to ensure no
chemical contamination of process fluids. Materials that
do not corrode do not contaminate.

Smooth Interior Surface


The hard, liquid smooth surface inhibits or prevents scale
formation and product buildup. For example, sticky latex
dispersions easily move through smooth glass pipe. Glass
resists fouling and is easy to clean.

Transparency
You can see what is happening inside glass systems.
Process and product can be inspected at a glance.
Trouble cannot hide behind glass, so processes stay in
better control.

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

274

Process Pipe

Beaded Process Pipe


Physical Properties Borosilicate
Glass
Coefficient of mean linear expansion
Between 20C and 300C

(3.3 0.1) x 10-6 K-1

Mean thermal conductivity


Between 20C and 200C

1.3 W/mK

Mean specific heat capacity


Between 20C and 200C

0.98 kJ/kgK

Density at 20C

2.23 g/cm3

Operating Temperature (Maximum)


Short term: Do not


operate below 0C
Normal Use: 230C

Versatility
For comparison purposes, weights of various 2-inch
pipes are given in the table below.
Material

Approx. Weight of 2-inch Pipe, Lbs/Ft.

Glass Process Pipe

1.13

Steel (Schedule 40)

3.65

High Silicon Iron

7.70

Stainless Steel (Schedule 40)

3.65

TFE Lined Steel

4.10

Glass Lined Steel

3.95

FRP

1.25

Relative Thermal Expansion


The thermal expansion of ACE brand pipe is 0.022 inches
per 100 feet of pipe and 100F temperature change. Values
of other materials relative to this (assuming glass Pipe = 1)
are given below. These relative thermal expansions should
be considered when connecting glass pipe into other
materials. When other materials expand more than glass
pipe, allowance must be made for the expansion difference.
A common way to accommodate this differential expansion
is with flexible bellows or hose at critical locations.
Material

Relative Thermal Expansion

Glass Process Pipe

1.00

Steel (Schedule 40)

3.60

High Silicon Iron

4.90

Stainless Steel (Schedule 40)

6.20

TFE Lined Steel

3.65

Glass Lined Steel

3.65

FRP

7.00

Beaded Pressure System


A large bead design feature assures a tight leak-free joint
under pressure conditions.
The one-bolt compression coupling shell is made from
300-series stainless steel. The flexible, elastomeric sleeve
is lined with a tough layer of TFE fluorocarbon plastic. The
flexibility feature allows deflections up to 3 per joint from the
axis under bending loads due to misalignment or pitching.

Pressure
The permissible operating pressure for ACE beaded pipe
and fittings depends on the pipe diameter.
Pipe Diameter

Maximum Working Pressure

1-inch

100 psig

1-1/2-inch

75 psig

2-inch

75 psig

3-inch

50 psig

4-inch

50 psig

6-inch

30 psig

When a system is assembled from several glass


components with different pressure ratings, the maximum
operating pressure of the system is limited to the pressure
rating of the component with lowest permissible working
gauge pressure.
All sizes of glass piping are suitable for full vacuum
service. Full vacuum is defined as 29.92-inch (760mm)
of Hg below standard sea-level pressure. Of course the
vacuum actually achieved is a function of system design,
tightness of the gasket joints, types of gasket used and
other operating factors.
Permissible operating pressures require the use of ACE
bead to bead process couplings. ACE process pipe is
tested at 1.5x the stated maximum working pressure.

Anchor Points
An anchor point is a rigid support for the glass line t ying it
into the building structure, or to fixed equipment such as
tanks, pumps or independently supported valves. There
should be one and only one anchor point in each
straight run of pipe. The diagrams that follow show the
correct and incorrect installation methods between a
nchor
points. Note the use of right-angle bends to obtain flexibility.

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Subject to Ace Discount (Page 4)

Net

Process Pipe

275

Beaded Process Pipe


Vibration
Connection to vibrating machinery such as a pump can
be made with the use of a flexible connection consisting
of either hoses, or PTFE bellows as determined by the
characteristics of the service.

Pressure Surges
Pressure surges must be controlled to prevent end
motion in a line. If lines have hydraulic pressure surges,
(positive displacement pumps or shutoff valves), it may
be necessary to provide a pressure relief valve. It is
usually necessary to provide a protected air dome to
reduce the pressure surge. The domes can be installed
on the discharge side of the pump, next to a valve, or at
the highest point in the vertical rise of the discharge line.
Use a tee at the top of the riser, plus a straight section
and a cap.

All valves, strainers, meters or other heavy equipment


must be supported rigidly and independently of the glass
pipeline. This prevents transmitting the dead weight to
the glass pipeline. It also prevents transmitting stresses
to the line when valves are operated; equipment shifts
positions, or expands more than the glass pipe. Rigidly
supported equipment such as the above are considered
anchor points. No more than one anchor point should be
used in any straight run of glass pipe. Flexible bellows
or hose can be used at the tie-in place.

Pipe Hanging and Support


Glass piping must be installed without mechanical restraint
and the pipe should be free to move to prevent stresses.
A mechanical restraint may set up a tensile stress that
over a period of time will cause the pipe to fail. Hangers
should not clamp the pipe tightly. Some lengthwise and
sidewise movements are desirable. Padded hangers
should always be used and spaced 8-10 feet apart. Use
an extra hanger where there are two or more couplings
in an 8-10 foot span. Do not pull or spring the pipe into
place. Always move the hanger to the pipe do not force
the pipe to the hanger.

Vertical Line Support


Vertical lines should be supported by plates beneath
the couplings or by padded saddles beneath 90-degree
elbows at the bottom of vertical rises. Do not support by
rigid clamp anchorages around the vertical pipe. Usually
only one rigid support is used. Lateral guides should be
used approximately every 20 feet of unsupported riser.
The horizontal run at the top of the riser should not be
supported within 7 feet of the riser. This reduces bending
strains in the horizontal run.

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276

Process Pipe

Beaded Process Pipe


Protection

Cleaning

It is usually desirable to run glass pipe close to structures


such as walls, columns, ceilings, etc., where conditions
are favorable for obtaining a firm support. This also would
keep the pipelines away from the heaviest traffic. When
the pipelines are run through congested areas, provision
should be made for protection. Angle or channel iron,
or expanded metal guards, should be provided around
exposed sections of glass pipe.

Flush line clean with water, other cleaning fluids, or


atmospheric pressure steam (open drain). Do not use
hydrofluoric acid, hot caustic solutions, abrasives or metallic
tube cleaners.

Testing

a) Wrenches

7/16-inch Open End, 1/2-inch Open End


9/16-inch Open End, 3/4-inch Open End

Tighten bolts on all couplings and flanges at the time of


installation. The pipeline, when empty, should be examined
for stresses by gently shaking the line. There should be
some limited movement the lines. To make sure all joints
are tight when line is ready for service, test at 11/2 times
the working pressure. However, do not test at more than
the maximum working pressure. All air must be removed
from the pipeline so there is no trapped air. DO NOT TEST
WITH AIR PRESSURE. If a joint leaks, carefully check the
joint assembly, retighten to recommended torque value,
and retest. If leaking persists, remove coupling, check
the gasket surface to be sure they are free from dirt, sand
or other particles, and replace if necessary.

b) Ratchet

3/8-inch Drive

c) Sockets

7/16-inch Deep Socket, 1/2-inch Deep Socket


9/16-inch Deep Socket, 3/4-inch Deep Socket

d) Torque Wrench

Calibrated in inch-lbs. Preferred


ratchet type 3/8-inch Drive.

e) Water-pump pliers

3/8-inch Drive

Spare Parts

b) Hammer

Generally, one spare for every twelve should be provided.


The proper storage of spare parts will ensure they are
available when required. Keep lengths of pipe on racks
and store them in a protected area. Keep fittings in their
original packaging.

c) Hack saw

Tools Required
Tools need to install glass piping (installation tools):

f)

Various screw-drivers

g) Hammer

Plastic or rubber head

Structural Tools:
a) Allen wrenches

5/16-inch and 3/8-inch

Making Joints with Process Pipe Couplings


1. Dip coupling in water or wipe beaded ends with damp cloth.
2. Snap coupling over one end of pipe making certain TFE liner is behind bead...

then insert other section of pipe into opposite side of coupling.


3. Tighten coupling bolt with 6-inch ratchet wrench until the gap between segments
is approximately 3/16-inch.

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Subject to Ace Discount (Page 4)

Net

Process Pipe

277

8828 BEADED PIPE


All pipe is available from stock in lengths shown; special lengths available at slightly higher cost.
1/2-inch
A
I.D.
57/64-inch
Length
Order
(Inches)
Code
3
4
6
12
18
24
30
36
48
60
72
84
96

8828-02
8828-03
8828-05
8828-09
8828-11
8828-13
8828-15
8828-20
8828-25
8828-30
8828-38
8828-45
8828-56

B
3/4-inch
Each
26.86
27.67
26.87
29.74
32.84
34.95
36.55
39.01
43.34
46.29
51.24
55.23
59.89

A
B
2-inch I.D. 2-9/16-inch 2-5/16-inch
Length
Order
(Inches)
Code
Each
4
6
12
18
24
30
36
48
60
72
84
96
108
120

8828-403 87.31
8828-405 84.76
8828-409 95.34
8828-411 102.90
8828-413 110.16
8828-415 118.00
8828-420 121.17
8828-425 132.74
8828-430 138.93
8828-438 167.75
8828-445 195.96
8828-456 224.62
8828-460 251.53
8828-462 278.66

3/4-inch
A
I.D.
1-5/32-inch
Length
Order
(Inches)
Code

B
1-inch

8828-102
8828-103
8828-105
8828-109
8828-111
8828-113
8828-115
8828-120
8828-125
8828-130
8828-138
8828-145
8828-156

35.47
36.55
36.55
37.69
41.35
42.95
46.61
49.06
54.49
58.88
63.95
69.14
74.07

3
4
6
12
18
24
30
36
48
60
72
84
96

Each

A
B
3-inch I.D. 3-11/16-inch 3-7/16-inch
Length
Order
(Inches)
Code
Each
4
6
12
18
24
30
36
48
60
72
84
96
108
120

8828-503
8828-505
8828-509
8828-511
8828-513
8828-515
8828-520
8828-525
8828-530
8828-538
8828-545
8828-556
8828-560
8828-562

138.15
138.15
145.24
151.84
158.27
160.38
171.75
174.74
186.43
223.62
261.27
297.81
334.50
372.26

1-inch
A
B
I.D.
1-17/32-inch 1-5/16-inch
Length
Order
(Inches)
Code
Each
3
4
6
12
18
24
30
36
48
60
72
84
96
108
120

8828-202
8828-203
8828-205
8828-209
8828-211
8828-213
8828-215
8828-220
8828-225
8828-230
8828-238
8828-245
8828-256
8828-260
8828-262

4-inch
A
I.D.
4-7/8-inch
Length
Order
(Inches)
Code

6
12
18
24
30
36
48
60
72
84
96
108
120

8828-605
8828-609
8828-611
8828-613
8828-615
8828-620
8828-625
8828-630
8828-638
8828-645
8828-656
8828-660
8828-662

48.48
48.48
48.48
51.36
55.06
59.89
64.43
69.03
76.69
86.43
95.68
104.69
111.79
118.69
131.83
B
4-9/16-inch

1-1/2-inch
I.D.
Length
(Inches)

A
B
2-1/16-inch 1-27/32-inch
Order
Code
Each

4
6
12
18
24
30
36
48
60
72
84
96
108
120

8828-303 66.47
8828-305 66.47
8828-309 70.84
8828-311 75.53
8828-313 80.62
8828-315 86.06
8828-320 90.75
8828-325 95.57
8828-330 102.44
8828-338 123.13
8828-345 138.55
8828-356 163.08
8828-360 184.44
8828-362 204.59
A
7-1/8-inch
Order
Code

B
6-5/8-inch

Each

6-inch I.D.
Length
(Inches)

250.50
260.65
271.74
283.38
293.38
295.28
314.23
314.66
389.30
454.01
518.90
583.79
627.20

6
12
18
24
30
36
48
60
72
84
96
108
120

8828-705
8828-709
8828-711
8828-713
8828-715
8828-720
8828-725
8828-730
8828-738
8828-745
8828-756
8828-760
8828-762

408.88
431.45
453.86
526.80
551.99
691.94
721.81
839.77
965.57
1052.05
1206.16
1358.71
1445.22

Each

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

278

Process Pipe

8830 SWEEP ELBOW


90
Size
(inches)
1/2 90
3/4 90
1 90
1-1/2 90
2 90
3 90
4 90
6 90

A
(In.)
2
2
2
5
6
7
10
12

Order
Code
8830-03
8830-05
8830-07
8830-09
8830-11
8830-13
8830-15
8830-17

45
Size
Each
(inches)
41.33 1/2 45
50.15 3/4 45
66.37 1 45
69.87 1-1/2 45
93.82 2 45
164.88 3 45
278.32 4 45
725.54 6 45

A
(In.)
2
2
2
3
4
5
7
9

60

Order
Code
8830-103
8830-105
8830-107
8830-109
8830-111
8830-113
8830-115
8830-117

Size
Each
(inches)
42.57 1/2 60
50.15 3/4 60
66.37 1 60
69.87 1-1/2 60
93.82 2 60
164.88 3 60
278.12 4 60
726.86 6 60

A
(In.)
2
2
2
3
4
5
7
9

Order
Code
8830-203
8830-205
8830-207
8830-209
8830-211
8830-213
8830-215
8830-217

22
Size
Each
(inches)
42.57 1/2 22
50.15 3/4 22
65.97 1 22
69.87 1-1/2 22
93.82 2 22
164.88 3 22
279.25 4 22
725.50 6 22

A
(In.)
2
2
2
3
4
5
7
9

Order
Code
8830-303
8830-305
8830-307
8830-309
8830-311
8830-313
8830-315
8830-317

Each
42.57
50.15
67.96
69.87
93.82
164.94
278.58
725.50

Use catalog dimensions for piping layout as gasket thickness allowance is included.

8831 REDUCER ELBOW


Size
A
(inches) (inches)
3/4 x 1/2
2-1/2
1
x 1/2
2-3/4
1
x 3/4
2-3/4
1-1/2x 1/2
3-1/2
1-1/2x 3/4
3-1/2
1-1/2x 1
3-1/2
2
x 1/2
4
2
x 3/4
4
2
x1
4
2
x 1-1/2
4
3
x1
5
3
x 1-1/2
5
3
x2
5
4
x1
7
4
x 1-1/2
7
4
x2
7
4
x3
7
6
x 1-1/2
9
6
x2
9
6
x3
9
6
x4
9

B
(inches)
2-1/2
2-3/4
2-3/4
3
3
3
3
3
3
3-1/2
3-1/2
4
4-1/2
4
4-1/2
5
5-1/2
5-1/2
6
6-1/2
8

Order Code
8831-02
8831-04
8831-06
8831-08
8831-10
8831-12
8831-14
8831-16
8831-18
8831-20
8831-22
8831-24
8831-26
8831-28
8831-30
8831-32
8831-34
8831-36
8831-38
8831-40
8831-42

Each
78.26
93.63
100.46
100.46
100.46
100.46
127.54
153.32
153.32
153.32
233.39
233.39
233.39
422.94
422.94
422.94
422.94
834.77
834.77
834.77
834.77

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

8831

Subject to Ace Discount (Page 4)

Net

Process Pipe

279

8832 MITERED ELBOW90


Size (inches)
1-1/2
2
3
4
6

Order Code
8832-03
8832-05
8832-07
8832-09
8832-11

A (inches)
3-1/2
4
5
7
9

Each
97.35
134.04
202.77
386.37
729.38

8832

8833 SHORT RADIUS ELBOW90


Size (inches)
1-1/2
2
3
4

A (inches)
3-1/2
4
5
7

Order Code
8833-32
8833-34
8833-36
8833-38

Each
77.16
106.01
182.72
326.89

8833

8836 TEE
Straight
Size (inches)
1/2
3/4
1
1-1/2
2
3
4
6

A (inches)
4-1/2
5
5-1/2
7
8
10
14
18

B (inches)
2-1/4
2-1/2
2-3/4
3-1/2
4
5
7
9

Order Code
8836-02
8836-04
8836-06
8836-08
8836-10
8836-12
8836-14
8836-16

Each
70.67
72.80
81.03
119.15
141.36
309.49
395.01
689.80

8836

Custom lengths, O.D. and shapes are available Just ask!

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

280

Process Pipe

8837 TEE
Reducing
Size Run x Branch
(Inches)
3/4 x 1/2
1 x 1/2
1 x 3/4
1-1/2 x 1/2
1-1/2 x 3/4
1-1/2 x 1
2 x 1/2
2 x 3/4
2x1
2 x 1-1/2
3x1
3 x 1-1/2
3x2
4x1
4 x 1-1/2
4x2
4x3
6 x 1-1/2
6x2
6x3
6x4

A (inches) B (inches) C (inches)


5
2-1/2
2-1/2
5-1/2
2-3/4
2-3/4
5-1/2
2-3/4
2-3/4
7
3
3-1/2
7
3
3-1/2
7
3
3-1/2
8
3
4
8
3
4
8
3
4
8
3-1/2
4
10
3-1/2
5
10
4
5
10
4-1/2
5
14
4
7
14
4-1/2
7
14
5
7
14
5-1/2
7
18
5-1/2
9
18
6
9
18
6-1/2
9
18
8
9

Order Code
8837-03
8837-05
8837-07
8837-09
8837-11
8837-13
8837-15
8837-17
8837-19
8837-21
8837-23
8837-25
8837-27
8837-29
8837-31
8837-33
8837-35
8837-37
8837-39
8837-41
8837-43

Each
72.80
89.47
89.47
119.15
119.15
119.15
144.07
144.07
144.07
144.07
178.79
178.79
178.79
370.23
370.23
370.23
370.23
716.14
716.14
716.14
716.14

8837

8842 REDUCERStraight
Size
(Inches)
3/4 x 1/2
1 x 1/2
1 x 3/4
1-1/2 x 1/2
1-1/2 x 3/4
1-1/2 x 1
2 x 1/2
2 x 3/4
2x1
2 x 1-1/2
3 x 1

A
(Inches)
4
4
4
4
4
4
4
4
4
4
5

Order
Code
8842-03
8842-05
8842-07
8842-09
8842-11
8842-13
8842-15
8842-17
8842-19
8842-21
8842-23

Each
41.61
43.57
44.90
54.08
54.08
54.08
64.93
64.93
66.87
66.87
96.49

Size
(Inches)
3 x 1-1/2
3x2
4x1
4 x 1-1/2
4x2
4x3
6x1
6 x 1-1/2
6x2
6x3
6x4

A
(Inches)
5
5
7
7
7
7
9
9
9
9
9

Order
Code
8842-25
8842-27
8842-29
8842-31
8842-33
8842-35
8842-37
8842-39
8842-41
8842-43
8842-45

Each
96.49
96.49
138.70
147.58
174.53
210.11
383.78
383.78
407.76
435.95
449.34

8842

8845 END CAPExtended


Size (inches)
1/2
3/4
1
1-1/2
2
3
4
6

A (inches)
2
2
2
3
4
4-3/4
6
7

Order Code
8845-03
8845-05
8845-07
8845-09
8845-11
8845-15
8845-17
8845-19

Each
23.89
24.62
42.46
52.71
62.45
96.73
179.81
210.04

Order Code
8847-02
8847-04
8847-06
8847-08
8847-10

Each
29.35
33.27
44.82
91.50
125.03

8845

8847 END CAPShort


Size (inches)
1-1/2
2
3
4
6

A (inches)
7/8
1
1-1/8
1-1/4
1-1/2

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

8847

Subject to Ace Discount (Page 4)

Net

Process Pipe

281

8849 U BEND
Size
1/2
3/4
1
1-1/2
2
3
4

8849

A (inches)
2-1/4
2-1/2
5-1/2
7
7
9
12

Order Code
8849-03
8849-05
8849-07
8849-09
8849-11
8849-13
8849-15

Each
65.95
78.07
121.13
172.94
257.44
417.86
777.09

8856 PROCESS PIPE COUPLINGS Bead to Bead


Coupling assemblies consist of a 0.300 series stainless steel outer band with T-Bolt and
hex nut; Buna-N liner and a TFE seal ring.
No. 8856 coupling is designed for temperature service up to 450F.

High Temperature Buna-N Liner (450, Black)


Size
1/2
3/4
1
1-1/2
2
3
4
6

A
B
C
D
(inches) (inches) (inches) (inches)
1-5/8
1-3/8
7/8
3/16
1-3/4
1-1/2
7/8
3/16
2-5/8
1-7/8
1
3/16
3
2-5/8
1-5/16
3/16
3-1/2
3-1/8
1-5/16
3/16
4-3/4
4-1/4
1-7/16
3/16
6
5-1/2
1-1/2
3/16
8-3/4
8
1-3/4
1/4

Max.
Torque,
in-lbs
20
25
35
50
60
75
80
90

Order
Code
8856-03
8856-05
8856-07
8856-09
8856-11
8856-13
8856-15
8856-17

Each
75.13
89.96
112.13
126.08
150.55
266.40
320.70
607.58

Use catalog dimensions for piping layout as gasket thickness allowance is included.

8856

8862 PADDED PIPE HANGER with Mounting Foot


8862

Size
1-inch (25mm)
2-inch (50mm)
3-inch (76mm)

Order Code
8862-03
8862-07
8862-11

Each
14.82
16.16
32.43

8863 PADDED PIPE HANGER without Mounting Foot


8863

All hangers are zinc coated and have factory applied plastic sleeve to prevent glass-to-metal
contact. Use one hanger every 8 or 10 feet. Support all valves and gauges individually.
Size (inches)
1/2
3/4
1
1-1/2
2
3
4

Order Code
8863-02
8863-04
8863-06
8863-08
8863-10
8863-12
8863-14

Each
8.19
8.19
8.67
11.91
13.19
19.52
21.79

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

282

Process Pipe

8866 COUPLING ASSEMBLY Beaded to Conical End Pipe


To join beaded end pipe to conical end pipe. Kit includes two flanges, inserts,
bolts and TFE sheath gasket.
Order Code
8866-03
8866-05
8866-07
8866-09

Size
1"
1"
2"
3"

Each
300.43
316.33
334.87
360.90

Assembly Consists of...


Size (In.)
1

Flange
8867-68

1-1/2

8867-69

8867-70
8867-81
8867-71

Insert
8867-76
8867-77
8867-78
8867-79
8867-80
8867-82
8867-83

Gasket
8868-16

7190 Nuts & Bolts Qty.


3/8 16 x 2-1/4
4

8868-17

3/8 16 x 2-1/4

8868-18

3/8 16 x 2-1/2

8868-19

3/8 16 x 3

Pressure rating limited to that of conical pipe


stem. Not to be used with beaded armored pipe.

8871 ADAPTER Beaded Process Pipe to Female NPT, 304 Stainless Steel
A 304 stainless steel adapter for matching glass beaded process pipe to male NPT
fittings, gauges and flanges.
Order Code
8871-20
8871-22
8871-24
8871-28

Size
3/4-inch beaded pipe to 3/4-inch female NPT
1-inch beaded pipe to 1-inch female NPT
1.5-inch beaded pipe to 1.5-inch female NPT
2-inch beaded pipe to 2-inch female NPT

Each
219.66
285.01
338.95
361.26

8871

8872 ADAPTER Beaded Process Pipe to Sanitary Flange, 304 Stainless


Steel

A 304 stainless steel adapter with sanitary type flange on one end. Mates glass beaded
pipe to sanitary type flanges.
Size
3/4-inch beaded pipe to 3/4-inch sanitary flange
3/4-inch beaded pipe to 1-inch sanitary flange
1-inch beaded pipe to 1-inch sanitary flange
1-inch beaded pipe to 3/4-inch sanitary flange
1-inch beaded pipe to 1.5-inch sanitary flange
1.5-inch beaded pipe to 1.5-inch sanitary flange
1.5-inch beaded pipe to 1-inch sanitary flange
1.5-inch beaded pipe to 2-inch sanitary flange
2-inch beaded pipe to 2-inch sanitary flange
2-inch beaded pipe to 1.5-inch sanitary flange
2-inch beaded pipe to 1-inch sanitary flange

Order Code
8872-04
8872-06
8872-08
8872-10
8872-12
8872-14
8872-16
8872-18
8872-20
8872-22
8872-24

Each
145.10
192.47
192.47
192.47
192.47
207.29
192.47
209.64
222.09
207.29
207.29

8870 MALE THREADED ADAPTER 304 Stainless Steel


Used to join threaded female fittings, valves and flanges to beaded pipe. Size, below, refers
to the bead and the NPT thread. Length, below, refers to the overall length of the adapter.
Size (Inches)
1/2
3/4
1
1-1/2
2
3

Length (Inches)
2-9/16
2-9/16
2-9/16
2-9/16
2-5/8
3-1/8

Order Code
8870-02
8870-04
8870-06
8870-08
8870-10
8870-12

8872

8870

Each
210.31
219.66
285.01
338.95
361.26
420.48

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

Subject to Ace Discount (Page 4)

Net

283

Vacuum Controllers

14063 PRECISION VACUUM REGULATOR J-Kem Infinity II


Perfect for vacuum distillation, unit automatically compensates for leaks in the equipment
under test and maintains precise pressure, even in systems with a continuous gas purge.
This computer (built-in) controlled vacuum regulator maintains pressure in the range of 0.1
to 760 Torr (atm pressure) in test instruments with volumes as small as 1 mL. Standard
features include 16-step programmable pressure ramp and serial communications for
PC control and data logging. Specifications: Transducer diaphragm is stainless
steel, accuracy to 0.1%, proof pressure 200%. Controller regulation 0.015% of range;
Resolution 0.1 Torr of 0.01 psi; Vapor path materials are stainless steel and PTFE; Ramp
Rates are 100 Torr/sec to 0.1 Torr/hr.; Serial communications, RS232 (RS485 or USB
upon request).
14063

Description
Includes Netbook and pre-loaded control software
Includes Windows 7 & XP compatible software
Includes Windows 7 & XP compatible software

Power
Order Code
120v, 60Hz 14063-10
120v, 60Hz 14063-15
230v, 50Hz 14063-212

Each
2741.60
2373.60
2373.60

14066 PROPORTIONING VALVES J-Kem, Stainless Steel


14066

Select one for use with digital vacuum regulator 14063-10, above.
J-Kem Model For Reactor Volumes
Cv
Orifice Size Order Code
PSV-2
1 mL to 2 L
0.033
0.040 in.
14066-01
PSV-3
25 mL to 4 L
0.055
0.055 in.
14066-02
PSV-4
100 mL to 22 L
0.068
0.063 in.
14066-03
PSV-5
1 L to 50 L
0.12
0.093 in.
14066-04
PSV-6
Large Capacity
0.37
0.147 in.
14066-05
PSV-7
Large Capacity
0.7
0.234 in.
14066-06
PSV-8
Large Capacity
1.3
0.316 in.
14066-07
PSV-9
Large Capacity
2.0
0.375 in.
14066-08
DVR-PNV
Stainless Steel Needle Valve, improves regulation
14066-20

Each
485.00
485.00
485.00
485.00
1097.00
1097.00
1097.00
1097.00
138.20

14061 VACUUM REGULATOR J-Kem, No Mercury


Connect to any vacuum pump or vacuum source, and then to any piece of equipment, to
regulate pressure, in most cases to 1 Torr. A standard pressure ramp feature evacuates
equipment at a user-defined rate to eliminate bumping due to solvent degassing or
over-evacuation. Ideally suited for large volume distillations, rotary evporators and
vacuum chambers. Not recommended for small volume distillations or applications
which involve a continuous purge with gas. Designed for vacuum systems that run
continuously, such as oil-filled vacuum pumps, aspirators, or with systems that are
always on, like in-house vacuum systems. The unit regulates pressure by opening and
closing a valve that separates the vacuum source from the system being evacuated.
J-Kem Model
DVR-200
DVR-300

14061

Recovers >99% of solvent


from rotary evaporators
Solvent DVR Pressure
(mm Hg)
Ether
475 Torr
300 Torr
CH2CI2
CH2CI2
100 Torr
EtOAc
90 Torr
Toluene
50 Torr

Solvent
Volume
340 mL
360 mL
255 mL
316 mL
273 mL

Time To
ryness
D
14.6 min.
21.9 min.
5.9 min.
17.0 min.
15.7 Min.

Percent
Recovery
99.6%
99.8%
99.5%
99.9%
99.4%

VAC
120
230

Order Code
14061-08
14061-20

Each
1127.00
1136.20

14062 VACUUM REGULATOR J-Kem, No Mercury


Designed for use with diaphragm vacuum pumps. In some systems,
pressure is regulated by turning the vacuum pump itself on and off. This
unit extends the life of diaphragm pumps by never forcing the pump to
start against an established vacuum, which can increase pump life by
100%. Not pictured.
J-Kem Model
DVR-280
DVR-380

VAC
120
230

Order Code
14062-10
14062-20

Each
1191.40
1191.40

Ordering & Product Information: 1-800-223-4524 n www.aceglass.com

284

INDEX

Accessories

Big Jar with Handles.........................................................229


Clamp Holder....................................................................232
Clamp, Hose Support, Stainless Steel................................233
Clamp, Quick Release.......................................................230
Clean-In-Place Sprayer.....................................................230
Containment Tray, Polyethylene.........................................234
Containment Tray, Polyethylene, with Spigot......................234
Containment Tray, Stainless Steel......................................234
O-Rings.............................................................................232
Side Shelf Support Stand...................................................230
Solution Bottle, Plastic Coated...........................................223
Solution Bottle, Plastic Coated, Ace-Safe........................223
Solution Bottle, Threaded Neck..........................................223
Tilting Support Stand.........................................................233
Ace-Thred Adapter..........................................................124, 149

Adapters

10mm...............................................................................193
75 Side Arm....................................................................125
105 degree Side Arm........................................................125
105 degree Side Arm with Ace-Thred................................125
Ace-Thred..................................... 48, 49, 123, 124, 125, 149
Beaded Pipe for Flush Valve..............................................129
Bottom Drip, 1:5 PTFE Stopcock........................................265
Bottom, UHMWPE or PTFE.................................................265
Bushing...............................................................48, 123, 124
Circulator Hose.................................................129, 145, 235
Connecting, Heat Exchange Coil........................................129
Connecting, Outer Socket Joint.........................................126
Distillation.................................................................127, 129
Electrode...........................................................................123
Giant.........................................................................124, 149
High Vacuum.....................................................................193
Lubricant Trap...................................................................193
Maxi..........................................................................124, 149
Midi..................................................................................149
Mini..................................................................................123
Multineck, #7 Ace-Thred...................................................126
Offset..................................................................49, 125, 126
pH Probe...........................................................................127
Process Pipe.....................................................................277
PTFE.......................................................................18, 19, 44
PTFE, Bottom......................................................................19
PTFE Ferrule......................................................................123
Reducing...........................................................................123
Stainless Steel..................................................129, 145, 235
Swagelok....................................................................44, 263
Thermometer......................................................................48
Twin Ace-Thred.................................................................124
with Side Port......................................................................19
Adjustable Pressure Relief Valve...............................................45

Agitators

10mm.......................................................................192, 193
19mm.......................................................................198, 199
28mm...............................................................................203
Large Scale...............................................................199, 203
Multi-Paddle..................................... 192, 193, 198, 199, 203
PTFE................................................. 192, 193, 198, 199, 203
Single Blade..............................................................192, 199
Stainless Steel..................................................................193

Turbine..............................................................193, 199, 203


Air Stirrers......................................................................209, 210
Allihn Condenser.....................................................................136
Amber Bottle...................................................................224, 228
Angled Condenser..................................................................141
Angled Funnel.........................................................................132
Arrow Stirrers.........................................................................209
Aspirator Bottle.......................................................................228
Auto-Reactor............................................................................88

B
Baffles

Glass.................................................................................148
PTFE.................................................................................148
Temperature Probe............................................................148
Barret Type Receiver...............................................................140
Bath Fluid...............................................................................244
Beaded Process Pipe..................................................... 268276

Beakers

Big Jar with Handles.........................................................229


Heavy Wall........................................................................229
Pilot Plant..........................................................................229
Pilot Plant Size..................................................................229

Bearings

5mm.................................................................................175
6mm.........................................................................175, 176
8mm.................................................................................187
9mm.........................................................................178, 179
10mm........................180, 181, 182, 183, 184, 185, 186, 187
19mm...............................................................194, 195, 200
28mm...............................................................................201
Aluminum Packing Box......................................................205
Debris Free.......................................................176, 186, 200
Debris Trap........................................................185, 195, 201
Economy...........................................................................175
Heavy Duty........................................................................194
High Speed Vacuum..........................................................178
High Vacuum.....................................................................183
Mechanical Seal................................................183, 200, 201
Pressure.....................................................................48, 182
PTFE..................176, 183, 184, 185, 186, 187, 195, 200, 201
PTFE-Clad.........................................................................180
Stainless Steel..................................................................184
Stirrer Assembly........................................................181, 184
Vacuum.....................................................................178, 179
Vacuum Stirrer Bearing Assembly......................................178
Water Cooled....................................................175, 180, 194
Bench Reactor Stand................................................................52
Big Jar with Handles...............................................................229
Blanket, Flask Insulating.........................................................169

Bottles

Ace-Safe Takeoff...............................................................223
Amber.......................................................................224, 228
Aspirator...........................................................................228
Cap, PTFE Lined........................................................226, 227
Caps/Pouring Rings...........................................................225
Carboy..............................................................................228
Filtering.............................................................................228
GL Thread.........................................................................224
Laboratory........................................................................224
Plastic Coated...................................................................223

285

Bushings

Nylon..........................................................................44, 124
PTFE...........................................................................44, 124

C
Caframo Overhead Stir Motors................................................217
CAPFE O-Rings.......................................................................239

Caps

GL Thread.........................................................................226
Gl Thread, Solid.................................................................260
GL Thread with Hole..........................................................260
Pouring Rings....................................................................225
PTFE Lined................................................................226, 227
PTFE Membrane........................................................226, 227
Solid, SVL..........................................................................260
Tamper Evident.................................................................226
With Hole, SVL...................................................................260
Carboys..................................................................................228
Cart, Safety Lift.......................................................................236
Chain Clamp...........................................................................232
CHEMRAZ O-Rings..................................................................241
Chiller.....................................................................................244
Chillers...........................................................................242, 243

Chromatography

Ace-Thred Column............................................................266
Large Size Column............................................................266
Polypropylene Screen Support Filter Discs.........................267
Screen Support Filter Discs...............................................267

Chucks

5mm.................................................................................177
6mm.........................................................................177, 204
10mm.......................................................................193, 204
19mm.......................................................................200, 204
28mm...............................................................................202
Flex-Grip................................................... 177, 193, 200, 204
Pass-through Assembly.............................................191, 197
Circulator................................................................................244
Circulator Hose Adapter..........................................................129
Circulator Hose Clamp............................................................235

Clamps

76mm...............................................................................231
102mm.............................................................................231
Chain................................................................................232
Chain Clamp.......................................................................51
Circulator Hose.................................................................233
Circulator Hose Clamp.......................................................235
Clamp Holder..............................................................51, 232
Clamp Holder for LawJaws Extension Clamps.....................52
Clamp Holder for Pilot Plants...............................................53
Clamp-To-Rod.............................................................51, 232
Conical Flanges.................................................................231

Extended Arm......................................................................53
For 7519 Filter Support.....................................................231
For 15305 Conical Flange..................................................231
For Flat-Style Flanges.......................................................231
For Lab Frames...........................................................51, 232
Jumbo................................................................................52
Pinch Type..........................................................................51
Pinch Type, Stainless Steel................................................231
PTFE Lined........................................................................231
Quick Release.............................................................51, 230
Stainless Steel.............................................. 52, 53, 235, 264
Three-Prong........................................................................53
Vinylized Jaws....................................................................53
Clean-in-Place Sprayer...........................................................230
Cold Finger Condenser............................................................137
Collar, Glass-Filled PTFE..........................................................207
Collar, Stainless Steel..............................................................207
Column Extenders for 5862 Column................................265, 266
Column Heads For 5862 Column.............................................263

Columns

INDEX

Polyethylene......................................................................228
Safety Coated....................................................................224
Schott-Duran............................................................224, 228
Solution.............................................................................223
Threaded Neck..................................................................223
Wide Mouth.......................................................................228
with Removable Hose Connection......................................228
Bulb Condenser......................................................................141
Buna-N O-Rings.............................................................237, 238

#50 Ace-Thred..................................................................263
#80 Ace-Thred..................................................................264
Ace-Thred.........................................................................266
Distillation................................................................ 263264
Large Size.........................................................................266

Condensers

Allihn, with Ace-Thred.......................................................136


Allihn, with Ace-Thred Connectors.....................................136
Angled..............................................................................141
Buchi........................................................................142, 251
Bulb Type..........................................................................140
Coiled...............................................................................137
Cold Finger................................................................136, 137
High Capacity, Double Coil.................................................138
Horizontal, Single Tube......................................................139
Internal Baffling.................................................................138
Large-Scale Rotary Evaporators................................142, 251
Long Path..........................................................................137
Reflux, Bulb.......................................................................141
Spiral................................................................................139
Splitter..............................................................................145
Triple Coil, High Capacity...................................................139
West...................................................................................49
With Ace-Thred Connectors...............................................138
Connecting Tubes, Large-Scale
Rotary Evaporator Glassware......................................254, 255

Connectors

28mm...............................................................................202
Motor Shaft to Chuck........................................................202
Tubing, Ace-Safe...............................................................128
Tubing, Polypropylene.......................................................128
Containers, Polyethylene.........................................................228
Containment Tray....................................................................234
Cooler, Circulating...................................................................244

Couplings

Beaded to Conical End Pipe...............................................277


Bead to Bead....................................................................276
Process Pipe.....................................................................276
Reducing, with Support.....................................................264
Stirring Shaft.....................................................................207
Cover, Evaporating Flask.........................................................258

286

INDEX

Digital Temperature Monitor....................................................151


Digital Vacuum Monitor...........................................................278
Disc, Rupture............................................................................45

Distillation

Apparatus, High Boiling.....................................................144


Splitter..............................................................................144
Distillation Adapter..................................................................129

Distillation Columns

Perforated Plate................................................................143
Perforated Plate, Internal Bellows, Silvered........................144
Vacuum Jacketed..............................................................145
Distribution Head, Large-Scale Rotary Evaporator Glassware.....252
Dual Motor Speed And Power Controller..................................220

Electrode Adapter...................................................................123
Electro-Flo Shut-Off Valve, Photochem....................................158
End Cap, Extended..................................................................275
End Cap, Short........................................................................275
Ethylene-Propylene O-Rings...........................................237, 238
Expansion Tank, Large-Scale Rotary Evaporator Glassware.....252

FETFE O-Rings................................................................237, 238


Filter Disc.........................................................................48, 267
Filtering Bottle........................................................................228

Filter Reactors

Instatherm..........................................................................17
Jacketed.......................................................................14, 18
Jacketed, Pressure Version..................................................15
PTFE...................................................................................55
Unjacketed..............................................................12, 16, 18
Unjacketed, Pressure Version..............................................13
Flange Styles, Guide...........................................................8, 112
Flask Heater...........................................................................171
Flask Insulating Blanket..........................................................169

Flasks

4-Inch Flange......................................................................95
Amberized, Large-Scale Rotary Evaporator Glassware.......259
Beaded Drain......................................................................93
Bottom Outlet................................................................40, 43
Cylindrical, Piston Type Drain...............................................93
Cylindrical, Sink Type Drain.................................................93
Extension Support.............................................................233
Flush Seal Drain..................................................................94
Heavy Wall..................................................................94, 112
Indented............................................ 47, 95, 97, 99, 100, 259
Indented, Large-Scale Rotary Evaporator Glassware..........259
Instatherm..................................................................47, 111
Jacketed............................................... 40, 43, 100, 112, 257
Jacketed, Large-Scale Rotary Evaporator Glassware.........257
Large Evaporator...............................................................250
Large Receiver..................................................................250
Large-Scale Rotary Evaporator Glassware.................257, 259
Large-Scale Rotavap Glassware................ 250, 257, 258, 259
Poly Coated, Large-Scale Rotary Evaporator Glassware.....259
Pressure.................................................................40, 41, 43
Reaction, Spherical.............................................................96

Receiving..........................................................................257
Robo Reactor Flask...........................................................111
Spherical, with Bottom Outlet..................................... 95111
Spherical with ZDS Valve.....................................................96
Stainless Steel..................................................................110
Three-Neck.................................................................94, 112
Unjacketed....................................................................40, 41
Valve Types for Reaction Flasks...........................................92
Volumetric, Pilot Plant.......................................................112
with 4mm Bore Stopcock..............................................97, 98
ZDS Valve.......................................................... 41, 94, 96, 99
Flat Side Funnel......................................................................132
Flexible Stirring Shaft..............................................................204
Fluorinated Grease..................................................................206
Fluorine Reactor, PTFE..............................................................55

Funnels

Addition..............................................................50, 133, 134


Buchner, Polyethylene.......................................................130
Buchner, Stainless Steel....................................................130
Filter Paper for Buchner Funnel.........................................130
Flange Bottom...................................................................133
Heavy Wall........................................................................132
Jacketed...........................................................................134
Offset................................................................................133
Powder.....................................................................132, 133
Powder, Angled.................................................................132
Powder Dispensing...............................................49, 50, 131
Powder, Flat Side......................................................132, 133
Powder, Heavy Wall...........................................................132
Powder, Offset...................................................................132
Pressure Equalizing.....................................................50, 134
Pressure Equalizing, Graduated.................................133, 134
Pressure Equalizing, Pilot Plant..........................................134
Pressure Equalizing, PTFE Needle Valve Stopcock.............134
Vertical................................................................................50

G
Gasket, PTFE..................................................................207, 208
Gasket, Stainless Steel...........................................................207
Gauge, Pressure.....................................................................210
General Stirring Information....................................................172
Girdle Mantle..........................................................................171
Glas-Col Heating Products......................................................166
Glass Frit Characteristics........................................................110
Glass Glossary........................................................................290
Glassware Assemblies for 13302 Rotary Evaporators..............249
Glassware Assemblies for
Large-Scale Rotary Evaporators................................. 261262
GL Thread Bottle.....................................................................224
GL Threaded Caps..................................................................225
Graphite Rupture Disc...............................................................45
Grease, Fluorinated.................................................................206
Grease, High Vacuum..............................................................206
Guide to Flange Styles............................................................112
Guide to Ordering Custom Pilot Plants.......................................57

H
Hazardous Duty Overhead Stir Motor......................................219
Head, Distribution, Large-Scale Rotary
Evaporator Glassware.........................................................252

287

3 Necks.................................................... 114, 115, 116, 118


4 Necks.................................... 113, 114, 115, 116, 117, 118
5 Necks............................................................113, 117, 119
6 Necks............................................................................118
7 Necks....................................................................118, 119
60mm...............................................................................119
60mm Side Port........................................................118, 119
100mm.............................................................115, 117, 120
100mm Side Port......................................................118, 119
150mm.............................................................117, 118, 120
200mm.............................................................118, 119, 120
300mm.....................................................................118, 119
Ace-Thred................................................... 41, 113, 114, 116
Conical Flange..........................................................114, 115
Coupling for KF Style Flange..............................................122
Domed......................................................................118, 119
Filter Reactor.................................................................41, 42
Filter Reactors...................................................................113
Flat Flange................................................................115, 116
Flat Glass..........................................................................113
Flat Ground Flange....................................................117, 118
Flat Stainless Steel............................................................113
Gasket for KF Style Flange................................................122
Inserts for PTFE Heads......................................................121
Joint Insert........................................................................113
KF-Style Flange.........................................................118, 119
Pressure Reactor.................................................................41
Pressure Reactors.............................................................113
PTFE.........................................................................119, 120
Schott-Duran Style Flange......................... 116, 118, 119, 120
Stainless Steel..................................................................115
Thermometer Joint............................................................116
Heater, Circulating..................................................................244
Heating/Cooling Coil...............................................................152
Heating/Cooling Coil, Halar Coated..........................................152

Heating/Mantles

Aluminum Housing............................................................168
Aluminum Housing Mantle........................................165, 167
Fabric Heating Tops...........................................................166
For Cylindrical Flasks........................................................171
Girdle Type Mantle............................................................165
Hemispherical Mantle........................................................164
Spherical Mantle...............................................................164
Voltage Controller......................................................169, 170
Heavy Wall Flask.....................................................................112
Heavy Wall Funnel..................................................................132
Heidolph Overhead Stir Motors................................................212

Heidolph Rotary Evaporators

Glassware Assemblies.......................................................249
Labarota 20 Control Features....................................246, 248
Labarota Control Economy................................................247
Laborota Automatic, Economy...........................................248
Laborota Automatic, Safety................................................248
Laborota Safety.................................................................247
High Boiling Distillation Apparatus...........................................144
High Vacuum Grease...............................................................206

Filter Reactor.......................................................................17
Robo Reactor Flask...........................................................111

INDEX

Heads

Jacketed Flask................40, 43, 95, 97, 100, 105109, 112, 257


Julabo Bath Fluid....................................................................244
Julabo Magnum 91 Recirculator.............................................243
Julabo Presto Series Recriculators..........................................242
Julabo Recirculator.................................................................244
Julabo Recirculator Accessories..............................................245
Julabo Tubing & Insulation......................................................245

KALREZ O-Rings.....................................................................240

Lab Safety Controller..............................................................157

Large-Scale Rotavap Glassware

Amberized Flasks..............................................................259
Cap...................................................................................260
Condensers/Coolers..................................................142, 251
Connecting Tubes......................................................254, 255
Evaporating Flask Cover....................................................258
Evaporation Flasks....................................................258, 259
Evaporator Flasks..............................................................250
Expansion Tank.................................................................252
For Heidolph Rotavaps......................................................250
Glassware Assemblies.......................................................261
Head.................................................................................252
Indented Flasks.................................................................259
Jacketed Receiving Flasks................................................257
Poly-Coated Flasks............................................................259
Received Flasks................................................................250
Receiving Flasks...............................................................257
Receiving Tubes................................................................254
Steam Tubes.....................................................................253
Traps.................................................................................253
Tubes................................................................253, 254, 255
Valves...............................................................................256
Vapor Duct Tubes..............................................................253
Vapor Tube........................................................................250

Manifold.............................................................................20, 46

Mantles

Fabric Heating Tops...........................................................166


For Cylindrical Flasks........................................................171
Girdle Type........................................................................165
Hemispherical...................................................................164
Spherical...........................................................................164
Metal Reaction Flask..............................................................110
Metal Reaction Head...............................................................115
Mitered Elbow........................................................................274
Moisture Test Receiver, Barrett Type........................................140
Moisture Test Receiver, Pilot Plant...........................................140
Moisture Test Receiver, Pressure...............................................44

IKA Overhead Stir Motors........................................................215

Instatherm

Nylon Bushing..................................................................44, 124

288

INDEX

Offset Adapter.........................................................................125
Offset Funnel..........................................................................132
Offset Overhead Stir Motors....................................................219
O-Rings
Buna-N.....................................................................237, 238
CAPFE.......................................................................239, 263
Chemraz...........................................................................241
EPDM........................................................................237, 238
Ethylene-Propylene...................................................237, 238
FETFE.......................................................................237, 238
For Ground Flanges...........................................................232
Kalrez...............................................................................240
Silicone.............................................................237, 238, 263
Viton.........................................................................237, 238
Overhead Stir Motor Gear Box.................................................219
Overhead Stir Motor Gear Reducer..........................................220
Overhead Stir Motors...................... 212, 215, 217, 218, 221, 222

Packing Support...............................................................48, 267


Padded Pipe Hanger...............................................................276
Perforated Glass Plate...............................................................19

Photochemical Equipment

Electro-Flo Shut-Off Valve..............................................158


Pilot Plant Reactor, 10L.................................................74, 75
Pilot Plant Reactor, 20L.................................................74, 75
Water Filter.......................................................................158
Water-Flo Power Cut-Off...................................................158
ph Probe.................................................................................127
Pilot Plant Support Stand........................................................230
Pinch Clamp...........................................................................231
Pipe, Process................................................................. 268276
Plastic Safety Shield.................................................................47
Plate Support Shelf...................................................................53
Plug, Nylon...............................................................................44
Plug, PTFE................................................................................44
Polypropylene Filter Discs.......................................................267
Polypropylene Tubing................................................................45
Powder Funnel........................................................131, 132, 133
Pressure Equalizing Funnel.....................................................134
Pressure Gauge......................................................................210
Pressure Manifold...............................................................20, 46

Pressure Reactors

1 Liter...........................................................................21, 22
2 Liter...........................................................................21, 22
All-in-One.....................................................................21, 22
Bottom Outlet............................2627, 3031, 3435, 3839
One-Piece Jacketed..........................................3637, 3839
One-Piece Unjacketed.......................................3233, 3435
Two-Piece Jacketed..........................................2829, 3031
Two-Piece Unjacketed.......................................2425, 2627
Pressure Relief Manifold.........................................................235
Pressure Relief Valve................................................................45
Pressure Rupture Disc..............................................................45
Probe, pH................................................................................127

Process Pipe

90 Short Radius Elbow....................................................274


Adapter, Female NPT.........................................................277

Adapter, Male Threaded.....................................................277


Adapter, Sanitary Flange....................................................277
Adapter, Stainless Steel.....................................................277
Beaded Pipe......................................................................272
Coupling Assembly, Beaded to Conical..............................277
Couplings, Bead to Bead...................................................276
End Cap............................................................................275
End Plug...........................................................................275
Padded Pipe Hanger..........................................................276
Reducer Elbow..................................................................273
Reducer, Straight...............................................................275
Sweep Elbow....................................................................273
U Bend...........................................................................276
Process Scale Filtration Reactors..............................................91
Proportioning Valves...............................................................278

PTFE

Adapter.......................................................................44, 123
Agitator............................................. 192, 193, 198, 199, 203
Baffles..............................................................................148
Bearing.............................................................................195
Bushing.......................................................................44, 124
Filter Reactor.......................................................................55
Gasket......................................................................207, 208
Reaction Head Inserts.......................................................121
Reactor...............................................................................55
Sparger Tube.......................................................................45
Stirrer Bearing............176, 183, 184, 185, 186, 187, 200, 201
Stirrer Blade......................................................191, 192, 198
Stirring Shaft.............................................................177, 198
Stopper.............................................................................236
PTFE Lined Caps.....................................................................226

Q
Quick Disconnect Tubing...........................................................46
Quick Release Clamp..............................................................230

R
Reactors

10 Liter..................................... 60, 61, 7273, 74, 7475, 75


10 Liter Pilot Plant Package.................................................89
12 Liter.........................................................................58, 59
20 Liter..................................... 60, 61, 7273, 74, 7475, 75
20 Liter Pilot Plant Package.................................................89
22 Liter.........................................................................58, 59
30 Liter.............................................................6267, 7679
30 Liter Pilot Plant Package.................................................90
50 Liter...........................................59, 6265, 7679, 8285
50 Liter Pilot Plant Package.................................................90
72 Liter...................................................................59, 8485
100 Liter...............................................6869, 8081, 8485
200 Liter.....................................................70, 7071, 8687
All-in-One...............................................................21, 2122
Auto-Reactor................................................................ 8890
Complete......................................................................58, 59
Cylindrical.........................................................6073, 7681
Domed Head.................6063, 6873, 7677, 8081, 8487
Filter.............................................................................12, 55
Flask...................................................................................96
Flat Head..............................................6465, 7879, 8283
Guide to Ordering Custom Pilot Plants.................................57
Jacketed...........................................................62, 66, 7283

289

ROBO Reactor

Complete............................................................................54
Instatherm Reaction Flask.................................................111

Rotary Evaporator Glassware

Heidolph Replacement Flasks............................................250


Vapor Tube for Heidolph 4000 Series.................................250
Rotary Evaporators.................................................246, 247, 248
Rupture Disc, Pressure.............................................................45

S
Safety Coated Bottle...............................................................224
Safety Lift Cart........................................................................236
Safety Shield............................................................................47
Screen Support Filter Discs.....................................................267
Screen Support, Polypropylene.................................................19
Short Radius Elbow.................................................................274
Side Shelf...............................................................................230
Silicone O-Rings.............................................................237, 238

Spargers

Easy Action Stopcock, #7 Ace-Thred Connection...............146


Easy Action Stopcock, Hose Connection............................146
Sparger Tube.......................................................................45
Straight, #7 Ace-Thred Connection....................................147
Straight, Hose Connection.................................................147
Splitter....................................................................................144
Splitter Condenser..................................................................145

Stainless Steel

INDEX

Low-Profile.................................................................. 8283
Offset Overhead Stir Motor................................................219
Overhead Stir Motor..................................................218, 219
Photochem....................................................................74, 75
Photochemical............................................................. 7475
Pilot Plant Beaker..............................................................229
Pilot Plant Clamp Holder......................................................53
Pilot Plant Condenser........................................136, 137, 140
Pilot Plant Standard Design Specs.......................................56
Pressure Equalizing Funnel...............................................134
Process Scale Filtration.......................................................91
PTFE...................................................................................55
Receiver, Moisture Test......................................................140
ROBO..................................................................................54
Spherical...........................................................8485, 8687
Three-Post Stand......................................................... 6667
Unjacketed............................................60, 61, 6471, 8487
Volumetric Flask................................................................112
Receiver, Moisture Test...........................................................140
Receiving Tubes, Large-Scale Rotary Evaporator Glassware....254
Recirculator............................................................................244
Recirculators..................................................................242, 243
Recirculator Tubing & Insulation..............................................245
Reducer Elbow.......................................................................273
Reducer, Straight....................................................................275
Reflux Condenser............................................................141, 142
Retainer Ring, PTFE..................................................................19
RMI-1001-DH...........................................................................54
RMI-1002-DH...........................................................................54
RMI1003-DH.............................................................................54
RMI-1004-DH...........................................................................54
RMI-1005-DH...........................................................................54
RMI-1006-DH...........................................................................54
RMI-1007-DH...........................................................................54

Adapter.............................................................................129
Agitator.............................................................................193
Bearing.............................................................................184
Clamp.................................................................53, 231, 235
Clamp Holder......................................................................52
Head.................................................................................115
Process Pipe Adapter........................................................277
Proportioning Valves..........................................................278
Stirrer Blade..............................................................191, 192
Stirring Shaft.....................................................187, 188, 189
Tubes, Large-Scale Rotary Evaporator Glassware..............253
Stand..................................................................................51, 52

Stands

Bench Reactor....................................................................52
For Kilo Class Reactors................................................. 6087
H Support Stand...............................................................51
Three-Post..........................................................................66
T Support Stand...............................................................52
Steam Tubes, Large-Scale Rotary Evaporator Glassware.........253

Stirrer Blades

5mm.................................................................................177
6mm.................................................................................177
10mm.......................................................................191, 192
19mm...............................................................................198
Banana Type.....................................................................192
Oval..................................................................................191
PTFE.................................................................191, 192, 198
Stainless Steel..........................................................191, 192
Stirrer Lubricant..............................................................204, 205

Stirrers

5-6mm Bearing.................................................................175
5-6mm Bearing, Water Cooled..........................................175
5-6mm Blade....................................................................177
5-6mm Economy..............................................................175
5-6mm Flex-Grip Chuck....................................................177
5-6mm Glass....................................................................175
5mm Shaft, Hollow Glass..................................................177
5mm Shaft w/PTFE Agitator..............................................177
6mm Bearing, Debris Free.................................................176
6mm Bearing, PTFE...........................................................176
6mm PTFE........................................................................176
9mm Bearing, High Speed Vacuum....................................178
9mm Bearing, Threaded....................................................179
9mm Bearing, Vacuum..............................................178, 179
9mm Shaft................................................................178, 179
9mm Vacuum Bearing Assembly.......................................178
10mm Adapter, High Vacuum............................................193
10mm Adapter, Lubricant Trap...........................................193
10mm Agitator, PTFE, Multi-Paddle....................................192
10mm Agitator, Single-Blade.............................................192
10mm Agitator, Stainless Steel, Multi-Paddle.....................193
10mm Agitator, Stainless Steel, Turbine.............................193
10mm Bearing..................................................180, 182, 183
10mm Bearing, Ace-Thred........................ 181, 182, 184, 185
10mm Bearing, Debis Trap................................................185
10mm Bearing, Debris Free...............................................186
10mm Bearing, Glass........................................................181
10mm Bearing, High Vacuum............................................183
10mm Bearing, Pressure...................................................182
10mm Bearing, PTFE................................. 184, 185, 186, 187

290

INDEX

10mm Bearing, PTFE-Clad................................................180


10mm Bearing, Water Cooled............................................180
10mm Blade, Banana Type................................................192
10mm Blade, Borosilicate Glass........................................191
10mm Blade, PTFE............................................................192
10mm Blade, PTFE, Oval...................................................191
10mm Blade, Stainless Steel.....................................191, 192
10mm Complete Assembly w/Glass Blade.........................181
10mm Complete Assembly w/Glass Shaft.........................184
10mm Complete Assembly w/PTFE Blade.................181, 184
10mm Complete Assembly, w/PTFE Blade.........................184
10mm Complete Assembly, w/SS Shaft.............................184
10mm Flex-Grip Chuck.....................................................193
10mm Mechanical Seal.....................................................183
10mm PTFE, Turbine.........................................................193
10mm Shaft......................................................................186
10mm Shaft, Borosilicate Glass.........................186, 189, 190
10mm Shaft,C Type........................................................189
10mm Shaft, Ground Glass................................................190
10mm Shaft, Hollow Glass................................................190
10mm Shaft, Polished Glass..............................................190
10mm Shaft, Precision Ground..........................................186
10mm Shaft, PTFE............................................................183
10mm Shaft, PTFE-Coated Glass.......................................187
10mm Shaft, PTFE-Coated Steel.......................................187
10mm Shaft, Stainless Steel.....................................188, 189
19mm Agitator, Large-Scale..............................................199
19mm Agitator, Multi-Paddle.....................................198, 199
19mm Agitator, PTFE.................................................198, 199
19mm Agitator, Single Blade.............................................199
19mm Agitator, Turbine.....................................................199
19mm Bearing, Ace-Thred................................................195
19mm Bearing, Debris Free...............................................200
19mm Bearing, Debris Trap...............................................195
19mm Bearing, Glass........................................................194
19mm Bearing, Heavy Duty...............................................194
19mm Bearing, Mechanical Seal.......................................200
19mm Bearing, PTFE.................................................195, 200
19mm Bearing, Water Cooled............................................194
19mm Blade, PTFE....................................................198, 199
19mm Blade, Single Blade................................................199
19mm Borosilicate Glass...................................................197
19mm Flex-Grip Chuck.....................................................200
19mm, Multi-Paddle w/Receptacle....................................199
19mm Precision-Ground Glass..........................................197
19mm, PTFE.....................................................................199
19mm Shaft, Borosilicate Glass.........................191, 196, 197
19mm Shaft, Heavy Duty...........................................197, 198
19mm Shaft, Polished Glass..............................................196
19mm Shaft, Precision-Ground Glass................191, 196, 197
19mm Shaft, Precision PTFE.............................................198
28mm Agitator, Large-Scale..............................................203
28mm Agitator, Multi-Paddle.............................................203
28mm Agitator, Multi-Paddle w/Receptacle.......................203
28mm Agitator, PTFE.........................................................203
28mm Agitator, Turbine.....................................................203
28mm Bearing, Ace-Thred................................................201
28mm Bearing, Debris Trap...............................................201
28mm Bearing, Mechanical Seal.......................................201
28mm Bearing, PTFE.........................................................201
28mm Connector, Flexible Beam.......................................202
28mm Connector, Motor Shaft to Chuck............................202

28mm Shaft, Heavy Duty...................................................202


28mm Shaft, Polished.......................................................202
Aluminum Packing Box......................................................205
Collar, Glass-Filled.............................................................207
Collar, w/PTFE Gasket.......................................................207
Flex-Grip Chuck................................................................204
Flexible Shaft....................................................................204
Gasket, PTFE.....................................................................208
Heavy Duty Stirrer Lubricant..............................................205
Hi-Lube Stirrer Lubricant...................................................205
Krytox Fluorinated Grease.................................................206
Krytox High-Vacuum Grease..............................................206
Matching Bearings to Shafts.............................................173
Shaft Coupling..................................................................207
Stir-Lube...........................................................................204
Stirrer Packing..................................................................206
Stir Shaft Quick Reference................................................174
Stopcock Lubricant...........................................................205

Stirring/Mixing

Air Stirrer, Arrow, Heavy Duty.....................................209, 210


Air Stirrer, Arrow, High Torque............................................210
Air Stirrer, Arrow, Light Duty..............................................209
Air Stirrer Filter/Regulator/Lubricator.................................210
Air Stirrer Pressure Gauge.................................................210
Caframo Overhead Stirrers........................................216, 217
Dual Motor Speed And Power Controller............................220
Gear Reducer, 4:1 Reduction.............................................220
Gear Reducer, 56C Flange.................................................220
Heidolph RZR....................................................................212
IKA Eurostar..............................................................214, 215
IKA RW16 Basic................................................................214
IKA RW20 Digital...............................................................215
Overhead Stirrers...................... 212, 216, 218, 219, 221, 222
Overhead Stirrers, Caframo...............................................217
Overhead Stirrers, Gear Box..............................................219
Overhead Stirrers, Hazardous Duty............................218, 219
Overhead Stirrers, IKA.......................................................215
Overhead Stirrers, Offset...................................................219
Overhead Stirrers, Pilot Plant.....................................218, 219
Overhead Stirrers, Reversing.............................................217
Overhead Stirrer Support Stand.........................................221
Pressure Relief Manifold....................................................235

Stirring Shafts

5mm.........................................................................175, 177
6mm.................................................................................175
9mm.........................................................................178, 179
10mm....................................... 186, 187, 188, 189, 190, 191
19mm....................................................... 191, 196, 197, 198
28mm...............................................................................202
C Type...............................................................................189
Flexible.............................................................................204
Ground Glass.....................................................................190
Heavy Duty........................................................197, 198, 202
Hollow Glass.............................................................177, 190
Pass-Thru.........................................................................191
Polished Glass...................................................190, 196, 202
Precision-Ground Glass............................. 186, 191, 196, 197
PTFE......................................................... 177, 188, 197, 198
PTFE-Coated Glass............................................................187
PTFE-Coated Steel............................................................187
Stainless Steel..........................................................188, 189
Stopcock Lubricant.................................................................205

291

PTFE.................................................................................236
Standard Taper, Full Length...............................................235
Standard Taper, PTFE........................................................236
Support Plate, Perforated, 73mm............................................264

Supports

Extension..........................................................................233
Tripod........................................................................233, 234
Support Shelf............................................................................53
Support Stand for 12 and 18 Columns.................................267
Support Stand for 24, 48 or 72 Columns............................266
Support Stand for Heidolph Rotary Evaporators.......................247
Support Stand, Overhead Stir Motor........................................221
Swagelok Adapter.....................................................................44
Sweep Elbow..........................................................................273

T
Technical Information

ACE Glass Fiber Filter Discs...................................................7


Chemical Resistance for Plastic Resins @ 20C...................10
Conversion Factors................................................................6
Flask Stoppers......................................................................7
Fraction Conversion...............................................................5
Glass Properties....................................................................7
Guide to Flange Styles...........................................................8
Hose Connection Size Guide..................................................5
O-Ring Compatibility Chart....................................................6
Plastic Properties..................................................................6
Pressure Conversions............................................................7
Reference Guide to ACE Boiling Flasks..................................8
Reference Guide to Ace-Thred Sizes......................................5
Specifications for Joints........................................................5
Specifications for Stopcocks.................................................5
Specifications for Threads.....................................................5
Standard Pipe Thread Fittings................................................9
Sterilization Reference Guide.................................................9
Viscosity Conversion Factors.................................................9
Tee, Reducing.........................................................................275
Tee, Straight...........................................................................274

Temperature Control

Complete Package............................................................150
Digital, Time Proportional Controller...................................153
Heat Exchanger Tubing......................................................153
Heating/Cooling Coil..........................................................152
Thermometer, Digital.........................................................151
Thermowell, Without Joint.................................................151

Temperature Controllers

230VAC.............................................................................156
Ace...........................................................................154, 155
Alarm for Water Flow Monitor............................................159
Digital Temperature Monitor..............................................151
Dual Channel....................................................................157
Dual Sensor Cords............................................................163
Dual Sensors, PTFE Coated...............................................163
Economy...................................................................154, 156
Four Channel.....................................................................157
General Laboratory............................................................155
Instatherm........................................................................156
J-Kem....................................................... 151, 156, 157, 159
Lab Safety.........................................................................157
Sensor Cords....................................................................163

Sensor Probes...................................................160, 161, 162


Single Channel..................................................................156
Thermocouples, J-Type.....................................................162
Thermocouples, K-Type.....................................................162
Thermocouples, PFA..................................................160, 161
Thermocouples, Plain................................................160, 161
Thermocouples, PTFE........................................................160
Thermocouples, RTD-Type........................................161, 162
Thermocouples, T-Type.....................................................162
Water Flow Monitor...........................................................159
Temperature Probe.................................................................245

Thermocouples

INDEX

Stoppers

Dual Sensor Cords............................................................163


J Type....................................................................160, 162
K Type............................................................160, 161, 162
Needle Tip.........................................................................163
PFA...........................................................................160, 161
Plain.........................................................................160, 161
PTFE.........................................................................160, 161
PTFE Coated.....................................................................162
RTD Type...................................................................161, 162
Sensor Cords....................................................................163
T Type............................................................................162
Thermowell......................................................................42, 123
Three-Neck Flask.............................................................94, 112
Tilting Flask Support...............................................................233
Traps, Large-Scale Rotary Evaporator Glassware....................253
Tray, Containment...................................................................234
Tray, Containment, with Spigot................................................234
Tripod Support................................................................233, 234
Tubes, Large-Scale Rotary Evaporator Glassware............253, 255

Tubes/Tubing

Connector...................................................................46, 128
Insulation..........................................................................245
Metal................................................................................245
Polypropylene......................................................................45
Sparger Tube.......................................................................45

U Bend................................................................................276

V
Vacuum Apparatus

Digital Vacuum Monitor.....................................................278


Proportioning Valves..........................................................278
Regulator, No Mercury.......................................................278
Regulator, Precision...........................................................278

Valves

0-20mm..........41, 96, 99, 103, 104, 105, 106, 108, 252, 254
Adjustable...........................................................................45
Bottom Outlet....................................................................265
Large-Scale Rotary Evaporator Glassware.........................256
Pressure Relief....................................................................45
PTFE Bottom Shut-Off.........................................................18
Vapor Tube, Heidolph Rotary Evaporator..................................250
Vapor Tubes, Large-Scale Rotary Evaporator Glassware..........253
Viton O-Rings..................................................................237, 238
Voltage Controller...................................................................170
Volumetric Flask.....................................................................112

292

INDEX

Water Filter, Photochem..........................................................158


Water-Flo Power Cut-Off, Photochem......................................158
Water Flow Monitor................................................................159
Well, Thermometer..................................................................123
Wide Mouth Bottle..........................................................225, 228

ZDS Valve.......................................................................94, 96

293
Cat.
No.

Page
No.

Page
No.

6020........................... 139
6021........................... 139
6022........................... 139
6024......................49, 141
6029......................49, 141
6042............................141
6046............................141
6087............................145
6088............................144
6228........................... 229
6231........................... 229
6233........................... 229
6300........................... 110
6310........................... 109
6381..............................16
6384..................12, 13, 18
6386..................14, 15, 18
6388..............................17
6390..............................55
6391..............................55
6412............................113
6423..................24, 25, 40
6425..................26, 27, 40
6427..................28, 29, 40
6429..................30, 31, 40
6433......................41, 113
6436.................. 32, 33, 41
6437..................34, 35, 43
6438..................36, 37, 43
6439..................38, 39, 43
6444..............................45
6445..............................45
6448........................20, 46
6452............................146
6453............................147
6460..............................88
6465........................72, 73
6469................58, 96, 132
6470......................59, 151
6471..............................42
6472
6065, 72, 73,
7679, 93, 94, 106, 129,
150, 202, 230
6473.... 6671, 80, 81, 107
6474..................8487, 96
6478....................164, 171
6482..............................94
6483..............................94
6484............................114
6485............................114
6486............................114
6487............................114
6488............................114
6489............................115
6490............................115
6491..............................97
6492..............................98
6494....................169, 171
6495...... 54, 101, 231, 232

Cat.
No.

Page
No.

6496............................231
6497........................... 110
6498........................... 110
6499............................115
6500............................123
6508............................231
6509............................231
6510............................231
6512............................115
6513............................116
6515............................116
6516............................. 99
6517..............51, 230, 264
6518........................41, 99
6519........................... 100
6525............................122
6526......................47, 100
6527......................42, 116
6528.............. 42, 116, 117
6529..............42, 116118
6530....................118, 119
6533............................107
6534............................108
6535............................108
6536........................... 109
6537........................... 109
6539..............................22
6540..............................96
6542..............................21
6559........................82, 83
6563............................144
6565............................143
6566............................144
6569............................145
6650..............................54
6701........................... 250
6702....................258, 259
6720........................... 259
6726............................257
6727............................257
6810........................... 140
6945............................112
6989............................228
7127............................112
7233......................50, 131
7234......................49, 131
7236............................132
7238............................132
7239............................131
7245............................132
7250....................132, 133
7252............................133
7278............................134
7281.........................., 134
7295............................133
7297....................133, 134
7298......................50, 134
7299............................. 50
7506..............44, 124, 149

Cat.
No.

Page
No.

7621....................225, 260
7622....................225, 260
7626............................226
7627............................226
7628............................226
7629............................226
7631............................227
7632............................227
7633............................227
7647........................... 260
7669......................51, 231
7701..............................44
7744........................... 140
7855............232, 237240
7859............................241
7885........................74, 75
8036........................... 180
8038........................... 180
8039........................... 180
8040........................... 180
8041............................181
8042............ 124, 149, 181
8043............................182
8044......................48, 182
8047............................182
8050............ 183, 200, 201
8051............................183
8053............................183
8055............................183
8059............................194
8060............................194
8061............................194
8064............................184
8065............................194
8066....................184, 185
8067.... 124, 149, 195, 201
8068............................186
8070............................187
8071............................187
8073........................... 189
8074........................... 189
8075........................... 190
8076............................196
8077............................196
8078............................197
8079............................198
8080............................202
8081............................204
8082............................191
8083............................191
8085....................191, 198
8086............................191
8087............................192
8088............................192
8089............................192
8090............................193
8091............198, 199, 203
8092........................... 199
8093....................199, 203

Cat.
No.

Page
No.

8094............................193
8095............................193
8096............................192
8098............................178
8099........................... 179
8100........................... 199
8101............................203
8111............................205
8112............................205
8113............................193
8115............................206
8116............................206
8117............................204
8118............................205
8119............................205
8122............................206
8124............177, 193, 200,
204, 207
8125............................207
8126............ 191, 197, 207
8127............................207
8128............................208
8133............................178
8134............................178
8250............................235
8318............................151
8767..............................45
8828............................272
8830............................273
8831............................273
8832............................274
8833............................274
8836............................274
8837............................275
8842............................275
8845............................275
8847............................275
8849............................276
8856............................276
8862............................276
8863............................276
8866............................277
8870............................277
8871............................277
8872............................277
9061............................123
9074............................125
9089............................126
9485......................50, 131
9488............................132
9524............................175
9527............................175
9528............................178
9529............................175
9530........................... 179
9532........................... 190
9533........................... 190
9534............................175
9535............................177

Cat.
No.

Page
No.

9541............................177
9542............................177
9655......................47, 111
9656......................47, 111
10000......................89, 90
10015..........................235
10165............................54
11057............................53
11065............................53
11067............................53
11069............................53
11079..........................232
11080....................51, 232
11081....................53, 232
11082..........................213
11083............................52
11160............................54
11173............................53
12031..........................164
12032......................... 169
12035..........................164
12036..........................165
12041..................165, 171
12043..........................165
12044..........................165
12045..........................166
12047..........................166
12050..........................166
12053..................167, 171
12058..........................168
12067..........129, 152, 153
12069..........................152
12075......................... 169
12085..................169, 170
12087......................... 170
12094..........................233
12096..........................233
12097..................233, 234
12100..........................233
12110......................... 160
12111..........................153
12113......................... 160
12125..........................154
12126..........................155
12127..........................156
12135......................... 160
12136..........................161
12140......................... 160
12141..................160, 161
12160..........................158
12162..........................158
12164..........................158
12165..........................158
12167..........................157
12168......................... 159
12169......................... 159
12177..........................148
12180..........................162
12181..........................162

GLASS GLOSSARY

D120676................54, 111
D120677........................54
D124780........................54
D127507........................54
D127590........................54
3965....................142, 251
3967............................252
3970............................252
3971............................253
3973............................254
3974............................255
3976............................253
3978............................256
4048............................223
5021......................48, 123
5028......................48, 123
5029............................124
5030....................124, 149
5031............................124
5032............................125
5040............................125
5050............................125
5090............................125
5221............................126
5263............................126
5268....................126, 218
5269............................. 49
5278............................127
5299....................127, 129
5332........................... 229
5393............................223
5395............................223
5539............................224
5559............................228
5814......................19, 267
5820............................266
5835............................265
5838............................. 19
5839..............................18
5843............................264
5844................18, 44, 263
5846..............................44
5848........ 19, 48, 264, 267
5853............................128
5857......................19, 265
5858............................128
5860............................263
5861......................19, 265
5862................... 263266
5867............................266
5868............................267
5945............................136
5946............................136
5958............................136
5960............................137
6012............................137
6015............................138
6016............................138
6017........................... 139

Cat.
No.

294
Cat.
No.

Page
No.

GLASS GLOSSARY

12182..........................162
12183..........................162
12184..........................163
12187..................129, 235
12190..........................163
12191..........................163
12193..........................148
12254..........................244
12256..........................244
12262..........................242
12274..........................243
12299..........................245
12300..........................245
12307..........................245
12312..........................157

Cat.
No.

Page
No.

12314..........................157
12318..........................156
12322..........................156
12327..........................151
12477..........................228
12517............................46
12560......................... 130
12563......................... 130
12631..........................236
12633..........................236
12634..........................236
12675..........................245
12677..........................245
12681............................45
12770............................18

Cat.
No.

Page
No.

12840............................52
12858....................55, 119
12860......................... 120
12862......................... 120
12864......................... 120
12866..........................121
12867..........................121
12869..........................121
12871..........................121
12990..........................127
13010..........................233
13219..........................234
13220..........................234
13270............................47
13286......................... 250

Cat.
No.

Page
No.

13302..................247, 248
13365......................... 209
13370......................... 210
13372......................... 210
13385......................... 210
13443..................176, 187
13445..........176, 186, 200
13500..........................211
13501..........................211
13504..........................211
13507....................54, 212
13511..........................212
13514..........................214
13517..........................215
13520..........................214

Cat.
No.

13523..........................215
13530..........................221
13532......................... 220
13542..........................213
13543..........................213
13544..........................213
13550............................51
13554..........................218
13555......................... 220
13557..................219, 220
13565..................216, 217
13566..........................217
13586....................52, 221
13590............................54
13649..........................221

Manufactured Products in this catalog:


Manufacturer
Arrow....................................................................
Baldor...................................................................
Briskheat..............................................................
Caframo................................................................
Cowie...................................................................
Dupont..................................................................
Glas-Col...............................................................
Greene, Tweed & Co.............................................
IKA........................................................................
Heidolph...............................................................
J-Kem...................................................................
Julabo...................................................................

Page
No.

Pages
211212, 215
222
169
218, 219
119121, 178, 188190, 199, 202
239, 240, 242
164169
243
216217
213214, 248251
156,158, 161162, 280
244247

Contact Ace for our full reusable glassware catalog and general laboratory catalog.

Cat.
No.

Page
No.

13650..........................222
13850..................188, 197
13852..................188, 197
14061..........................278
14062..........................278
14063..........................278
14065..........................278
14066..........................278
14108..........................244
15616..........................236

295
Check A fissure in the glass not extending through the
thickness of the glass. A surface crack.

Anneal, Lehr The same meaning or end result: removing the strain from the glass. Different processes, however.
Annealing is usually accomplished with a flame or annealing
oven where the part is stationary and is brought up to the
strain point temperature and then cooled, thus removing any
strain in the glass. Lehring or annealing can also be accomplished via a long belt lehr that gradually takes the glass up
to the annealing point and then gradually takes it back down
to room temperature as it moves on the belt through the hot
zone.

Chill Mark A wrinkled surface condition caused by working


glass below the working point or working glass too cold.

Annealing Point The temperature corresponding to a rate


of elongation of 0.0136cm/min when measured by ASTM
method C336 test for annealing point and strain point of glass
by fiber elongation. The test describes a cooling rate of approximately 4cm/min with a fiber of approximately 0.065cm
O.D. and a suspended load of 1000g. The annealing point
numerically approximates log = 13 poises, where internal
stress is substantially relieved in a few minutes. To state this
more simply: the temperature at which the glass is relieved of
strain and stress.
Bead Enlarged edge on a tube or piece of glass. Beakers
have a bead on the top edge or lip.
Belt Center-less Grind Removes glass from the outside of
a tube or rod in a horizontal motion with an abrasive belt.
Bevel To grind away an edge at an angle, or to take off a
sharp edge on the glass. Customer may call out break edge or
chamfer edge. Can be on the I.D. or O.D.
Blank The parison or preliminary shape from which a
finished piece is formed. Any glass piece that further work will
be performed to finish it.
Blister A gaseous inclusion trapped in the glass. Also
called a bubble.
Bloom A cloudy surface that reappears on the glass due to
aging and other factors. Sometimes it shows as cloudy area
after reworking glass from excess carbon vapor. A condensing
vapor or compounds in the glass that reform after molding.
Blown-ware Term for glass pieces that are predominately
blown free or partially in a mold while still hand blowing the
glass. Volumetric lab ware is still blown by free hand. Some
large bottles or flasks are still called blown-ware.

GLASS GLOSSARY

Airline A long, straight line within the glass piece. This is


usually caused by a long, gaseous inclusion.

Chip A small piece of glass broken away from the main


piece of glass, or the residual mark left after a piece is broken
off.

Cold Seal When glass is incompletely joined at a temperature below the working or softening point. Usually has bubbles
or waves at the joint. Incomplete glass flow.
Concentricity A measure of, or the lack of uniformity of,
the wall thickness throughout a tube.

Cord A narrow band of glass having a stringy appearance


different from the main glass. Streak of differing glass within a
tube or rod. Sometimes caused by an un-melted compound in
the mixture.
Crack A fissure that goes all the way through the surface.

Crystallization A crystalline structure. A mass of glass


particles or silica particles clumped together. Sometimes used
to describe a clump of un-dissolved material.
Devitrification A crystal-like growth on the surface of the
glass. Appears frosted.

Dielectric Constant The ratio of the parallel capacitance


of a capacitor with the material as the dielectric to the capacitance of the same capacitor with a vacuum as the dielectric.
The dielectric constant determines the amount of electrostatic
energy, which can be stored in a material per unit volume, per
unit potential g
radient.
Dielectric Loss Factor The product of the dielectric
constant and the dissipation factor. At low values (below one),
the dissipation factor is less than 5% different than the power
factor, so the power factor can be used for most calculations.
The power loss in a dielectric is directly proportional to the
loss factor if voltage gradient and frequency remain constant.
Dimple An imperfection, usually a bump or depression,
caused by forming the glass.

Discolored Glass A lead deposit or surface discoloration


caused by carbon or etching. Not removed by cleaning.

Etch or Etched Usually means chemically altered glass,


such as acid etched glass. Etch can also mean weathering.
We actually etch the markings on pieces with acid.

Bow or Camber Straightness of tubing measured as the


maximum deviation from a straight line connecting any two
points on the tube. More accurately, its the LACK of straightness.

Expansion Coefficient The average increase in length per


unit length per degree C change in temperature over the range
0 -300 degrees C.

Bubble See inclusion or blister.

Forming The shaping of hot glass.

Center-less Grinding To remove glass from the outside


diameter of a tube or rod without regard to the inside diameter
or wall tolerance.

End Work or End Finish The end of a tube or rod is held


against a moving belt or a disk perpendicular to the belt.

Concentric Grinding To remove glass from the outside


of a tube using the inside diameter as a reference. Usually
ground on end centers on a lathe or mandrel.

Finish Has several similar meanings: the threads on a


threaded piece or neck; the joint on a neck; a bead; the polish
or grind; the stage that a piece of glass is free of seeds.
Fire Cracks Cracks in the glass caused by temperature
shock form overheating a specific point.

296

GLASS GLOSSARY

Fire Polish Using fire, torch, hand-held torch or bottomer


line to fire polish the end of a tube or rod. To actually melt and
seal the end and to glaze it.
Flame Cut Heating by direct flame a piece of glass and
pulling until it separates.

Flat Glass Window panes, microscope slides and microscope cover glasses, usually floated molten onto a water or
oil bath. Collected when its cooled down. Floated or poured
into a flat mold and cooled. Sometimes pressed or cast
flat. The Pilkington process glass is poured and rolled flat
between rollers and annealed in continuous sheet.
Fold A surface line caused by incomplete joining of two
pieces of glass.

Mandrel Generally a round device or reverse mold that


hot glass is pulled over or shrunk onto. Used for precision
bore shrinking and redraw tube pulling. Also used for capillary
tube pulling. Can be made of steel or other metals and materials.
Melting Temperature The temperature in the furnace
where the molten state of the particular glass formula is
reached.
Molded Glass Molten glass that is poured or blown into
mold. The glass with air pressure then takes on the shape of
the mold. Also, see paste mold. Beakers, flasks and most art
glass and all types of consumer ware products are molded.
The I.S. process the process for molding bottles which
blows a parison first and then the full bottle in a second mold.

Glass Lathe Used to horizontally hold a piece of glass and


rotate while working it. Can also be used vertically. Can have
fire ring or burner ports or be used with blowtorch or hand
torch.

Mold Mark The mark left on a piece of glass after molding,


A seam.

Glass Tank or Furnace Where the batch is injected or


dumped into a tank made of refractory brick and heated to
molten temperatures. This is where raw molten glass is pulled
from to be pulled, blown, or shot into molds. A borosilicate
tank can be at temperatures as high as 1800-2000 degrees C.

Open Blister An open gaseous inclusion at the surface of a


piece of glass.

Glass Tubing or Rod Pulled downward through a bell or


mandrel out of a furnace and then pulled horizontally on a
draw, or line, that is heated in stages to keep the glass at its
working point while air is blown back up the center to keep
the I.D. Solid rod or cane is formed the same way, except
without the air stream. The bell, air pressure and speed of the
draw determine the basic O.D. and I.D. (See Danner Process,
Down-draw).

Plunge Grind Set up a stop in the grinder so as to grind


only a portion of the length of the tube.

Glaze The same as fire polish

Grinding Remove layers of glass or imperfections using an


abrasive belt or wheel.

Hackle Marks Fine ridges on the fracture surface of glass


parallel to the direction of the crack propagation on the surface.
Hand Tooling To shape glass while hot by using a hand
tool that is shaped to the desired form. Can be turned on rollers or a lathe and worked.
Hard Glass Generally denotes borosilicate glass. Refers to
glass possessing extremely high viscosity at elevated temperatures. A glass with a high softening point. Difficult to scratch.

Interface Where two pieces of glass, particularly different


types of glass, meet.

Opaque Dense, or not clear.

Out of Round A different way of expressing concentricity,


or stating that the piece is more oval than round.

Pressed Glass Hot glass that is poured molten into a


two-piece mold and then formed in the mold by mechanical
pressure.
Reboil This phenomenon, which results in the formation of
tiny visible bubbles, shows as white lines in the surface and
interior of the glass. Usually caused by water vapor or other
contaminants. Sometimes caused by pulling tubing to fast.
Redraw The process whereby you reheat glass tubing or
rod and re-pull it through heat zones to lengthen it and make
it smaller in O.D. NOT shrinking. The difference between
re-draw and precision bore is that the tolerances of precision
bore are tighter and more consistent throughout the tube section.
Refractive Index The ratio of the speed of light in vacuum
to the speed of light through the particular glass. The value of
the refractive index is given for the sodium D line (589.3mu)
and the values listed are for annealed glass.
Scale A small piece of extraneous oxide or carbon embedded in the glass. Can be caused by dirty mandrels.
Score Significantly scratch the surface in a straight line.

Knot A transparent stone in the glass. Non-homogeneous


glass.

Scratch A major surface abrasion. A long surface indentation caused by reworking or an outside force.

Lathe Shrink Mandrel is held horizontally and tube is


shrunk onto mandrel that is attached to a lathe and rotated.
The burner is moved horizontally along the length.

Seals, Graded Glass seals made from gradients or rings


of different glasses, usually shaped into a tube that can be
used to join glass pieces or components with wide variation in
coefficient of expansion.

Lead Glass Glass with high lead content as in crystal ware,


stem ware. Also, flint glass.
Liquid Hone Same as above, only more of a slurry.

Seam Either a mold mark or the area where two pieces of


glass are joined together.
Seed Small blister (gaseous inclusion), less than .030 in
diameter.

297

Snap Cut Score and apply hand pressure on the score until
it snaps.
Stability Resistance to weathering; chemically durability.
Standard Taper Is the diameter of the large end on the
joint and the length of the taper, i.e. ST 19/22 is 2mm length
and 19mm diameter at the top.
Stones An imperfection or crystalline contamination in the
glass.
Strain/Stress A condition of tension or compression from
molding, working, cutting, grinding or drawing of raw molten
glass. Usually cant be seen but may be seen with a Polariscope. Shows as a rainbow or interference patterns.
Strain Point The temperature corresponding to a rate of
elongation of 0.00043 cm/min. when measured by ASTM
method C336. This test prescribed a linear extrapolation of
the data obtained in the annealing point determination to the
above designated rate. Internal stress is substantially relieved
at the strain point in a few hours.
Stringer An imperfection usually running along the length
of a tube, usually caused by the slow solution of a large grain
of sand or foreign material.
Stones An imperfection of crystalline contaminations in
glass.
Taper The maximum gradual dimensional change in the
O.D. of a tube or rod from one end to the other or from one
point to another on a rod or tube. S over T is standard taper
used on joints.
Temper The degree of residual stress in annealed glass
measured polarimetrically against a standard.
Tempering To improve strength, a heat treatment or
chemical treatment that can induce controlled compression
on the surface of the glass. Vycor is chemically strengthened
or tempered glass. Glass can be rapidly cooled (iced) after
being heated to the softening point and create a tempering vs
annealing.
Thermal Shock A sudden, very rapid change in temperature that causes the glass to crack or break.

TIR (Total Indicator Reading) This is the maximum dial


variation from the data or reference point when measurements
of the I.D., O.D., wall thickness, camber, etc. of a precision
bore tube are taken.

GLASS GLOSSARY

Silk Screen Process The process of decorating glass by


applying paint or ink through a steel mesh screen.

Tubing, Redraw Process in which glass tubing or rod is


reheated and redrawn (pulled), to make a smaller I.D. or O.D.
tube or rod. Capillary tubing is usually redrawn. Micropipettes
are usually from redrawn tubing.

Tubing, Shrinking (Precision bore) Glass tubing is reheated and shrunk, by pulling a vacuum on to a precision mandrel.
Type I Glass Often misunderstood, it is US Pharmacopeia
(USP) standard for glass for containers for pharmaceutical
packaging. Not ASTM. It does denote or describe a clear
borosilicate glass formula. The slightest deviation in % of an
ingredient for borosilicate would knock it out of Type I class.
Even amber borosilicate is not Type I. Type I doesnt denote
glass lab ware classes.

Type I, Class A Conforms to Federal Specification DD-G541b and ASTM E-438 is for borosilicate glass lab ware formulation and specifications. Some glass meets all three specs
such as Corning 7740 (Pyrex).
Wall Thickness of the piece between the I.D. and O.D.
There is standard, medium, and heavy wall tubing.

Wave An uneven optical effect due to uneven glass distribution.


Wet Cut Cutting a piece of glass by using a water-cooled
wheel or saw. Actually, the new definition is where water is
introduced at extreme pressure and cuts through a surface
(water jet).
Working Range The temperature range that a piece or
type of glass is heated to be able to be worked or formed.
The temperature at which the glass becomes slightly elastic
but holds its main shape and can be reshaped.
Youngs Modulus The measure or modulus of elasticity.
The stress required to produce a unit change of length.

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EL A N D,

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