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Summary
The gas penneability of some sandstones from Uinta
County, UT was measured in the laboratory. The effect
of confining pressure and partial water saturation on gas
penneability was investigated. Measurements were conducted at pressures of up to 34.5 MPa and partial liquid
saturations of up to 60 %. We noted that the slope of the
straight line relating apparent gas penneability to
reciprocal mean pore pressure decreased with increasing
net confining pressure and with increasing partial water
saturation. Gas penneabilities extrapolated to infinite
pore pressure were often higher than liquid
penneabilities under the same confining pressure conditions; scanning electron microscopic (SEM) observations indicated rocklfluid interactions.
Geologic studies of end pieces cut off from core plugs
revealed that porosity is reduced by quartz overgrowths,
authigenic clays (kaolinite, illite, and minor quantities of
chlorite), carbonate cements (calcite and dolomite), and
physical compaction of labile rock fragments. In some
samples, organic-rich laminae were found to lie parallel
to bedding surfaces. Apparently, microporosity had been
fonned by partial leaching of feldspars and rock
fragments. Most of the pores were lined with authigenic
clays that fonn highly irregular pore walls. Thin film intergranular pores, which were observed in samples impregnated with blue epoxy at ambient pressure, were not
found in samples in which the epoxy was cured under a
confining pressure of 34.5 MPa.
Introduction
The concept of slip during gas flow through capillaries
with diameters small enough to be comparable to the
mean free path of the gas was used by Klinkenberg 1 to
explain the discrepancies between gas and liquid
Now with Mobil R&D Corp.
0149-2136/82/0011-9872$00.25
NOVEMBER 1982
penneabilities of porous media. He presented the following equation, which relates the apparent gas penneability, kg, of a gas flowing at a mean pore pressure, p, to the
true penneability of the porous medium, k oog .
kg =koog(l +blp).
. ........................ (1)
. .............................
(2)
13
2512.6 to 2549.9
Mean b
Standard
Deviation c
49.1
5.9
8.1
3.9
2.8
2.3
12.7
8.2
4.2
2.4
1.5
1.8
4.4
5.7
2.7
1.9
1.8
1.0
3.4
2.8
2.2
2.6
Quartz
Feldspar
Plagioclase
Potassium
Rock Fragments
Chert
Other d
Carbonates
Calcite
Other e
Matrix
Claysf
Void
Other g
Experimental Methods
Permeability measurements were conducted with
Hassler-type core holders in which samples (approximately 0.025 m in diameter and 0.05 m long) were subjected to net confining pressures of up to 34.5 MPa. At
each confining pressure, gas permeabil~ty was measured
at at least three different mean pore pressures to obtain a
straight line plot that would relate apparent gas
permeability and reciprocal mean pore pressure.
Samples were dried at temperatures of from 80 to 90C
before these measurements were taken. Dry nitrogen was
used in gas flow measurements. After gas flow
measurements, the cores were saturated with brine (2 %
KCl+2 % NaCl). Porosity values were determined from
the change in weight on saturation. Liquid flow
measurements then were conducted. Liquid flow was
maintained by applying gas pressure on liquid that was
contained in a cylinder but separated from the gas by a
movable piston. A differential pressure of 0.689 MPa
was used to maintain flow. After the liquid flow
measurements, different saturations were established in
the core samples by allowing the liquid to evaporate
from the core. At different levels of saturation, gas flow
measurements were made at three different mean pore
pressures to obtain a "Klinkenberg plot." The samples
were weighed before and after each set of measurements
to ascertain that there had been no change in saturation.
However, there was no check on the saturation distribution in the sample.
2716
QV~R TZ
FElDSP~R
ROCK FRAGMENTS
Mineral composition was determined by X-ray diffraction; modal analyses of 300 points per thin-section were
made to define mineral distribution. Thin-sections were
prepared after epoxy injection. In some cases the epoxy
was allowed to set under a confining pressure of 34.5
MPa so that any changes in pore structure that would
result could be observed.
Petrographic Properties
The samples studied were rich in detrital quartz and rock
fragments; feldspars accounted for less than 8% of the
rock volume. Clay minerals, both authigenic and
detrital, that were found included kaolinite, illite, and
minor quantities of mixed-layer clays and chlorite. A
summary of the modal characteristics is given in Table 1;
sample classification is shown in Fig. 1. Two samples,
from depths of 2509.8 and 2510 m, contained 20% and
42 % calcite cement and were not included in the data
given in Table 1.
The basic porosity characteristics of the sandstones are
determined by the physical characteristics of the
sediments. The initial porosity of unconsolidated, finegrained, moderately well sorted sand is variable but
probably averages about 40%.12 The initial porosity
characteristics are modified, often extensively, by subsequent diagenetic processes, both physical and chemical.
Most of the porosity in these sandstones is secondary and
results from leaching-partial to extensive-of carbonate
cement, rock fragments (especially chert), and, to a
minor extent, feldspar grains. Rarely do pores reach 150
/tm; they are typically 10 /tm or less in cross section.
Fig. 2 illustrates the general distribution of the porous
and nonporous mineral components of the sandstones;
the lack of large pores is obvious. Dissolution of mineral
JOURNAL OF PETROLEUM TECHNOLOGY
(k~g), *
Sample
Core
Depth
(m)
8243.3
8243.9
8290.4
8290.9
8298.4
8298.8
8358.3
8358.7
8365.4
8365.9
2512.6
2512 .7
2526.9
2527.1
2529.4
2529.5
2547.6
2547.7
2549.8
2549.9
0.0081
0.0138
0.0421
0.0536
0.022
0.116
0.056
0.134
0.0252
0.0143
(md)
(kd, *
(md)
b,
(MPa)
(k~gh *
0.0025
0.0103
0.0063
0.583
0.274
0.236
0.246
0.147
0.076
0.158
0 .068
0.084
0.298
0.0112
0.0334
0.0606t
0.0319
0.0067
0.0121t
(kd2 *.
(md)
b 2 .*
(MPa)
0 .0005
0 .0014
0.0048
0.0028
0.0005
0 .0005
0.0005
1.674
0.970
0.256
0.83
0.0124
0.0087
0.0238
0.0004
0.0017
0.0034
0.0041t
0.0045
0.0004
0.001t
0.176
0 .285
0.160
2.66
0.558
(md)
0 .098
0.111
0 .067
0.066
0 .063
0.077
0 .079
0 .058
0.059
Fig. 2-SEM illustrating abundance of fine-grained, commonly altered rock fragments (R) containing
numerous micropores. Depth of sample is 2512.6 m.
NOVEMBER 1982
2717
0.20.
'"E
>-"
0.16
l-
:;
t!. 689
m
<!
w
::;;
0.12
cr
w
0(j)
<!
COO
<!)
IZ
cr
Ci0-
0.0.4
<!
0.
0.
~
>"
t:i
IE
0-
0..0.8
1!l
<!
W
a.
0..0 6
0..020
l!.
(j)
<>
0
142
329
42 .7
0.015
<!
L'l
W
>
o 0.04
w
Eiw
i:i
...J
0.
::E
cr
w
;3
<!
WATER SATURATION %
:;
(j)
cr
~ 0 . 0 . 2 5 , - - - - -- -- - - - - - -- - -- - - - ,
>"
I-
0.010
u.
u.
W
0..02
IZ
W
l-
W
c~_~
0.
_ _...J__ _ _ _
L __
10.
15
_ L_ _ _ _...J__ _ _L __ _
20.
25
30.
35
0..0 05
cr
It
0<!
c~
____- L_ _ _ _ _
2
~L_
_____
_ _ __...J
10r-----------------------------------~
>-
r
:J
o
o
as
w
"-
0 00
01
(f)
<!l
>
fi...J
W
cr
001
10
20
30
40
50
60
WETTING PHASE SATURATION, %
70
80
0.001
0.01
0.1
10
from Eqs. 2 and 3 and noted that the line with the best
slope had a slope of unity. They thought this was
because porosity had been taken into account in the latter
case. In essence, this means that a correlation, if it exists, should be between band k</>g/ rather than between
band k oog .
A plot of b vs. koogl for all the samples under different conditions of confining stress and partial water
saturation is shown in Fig. 9. In the case of relative
permeability data, gas-filled porosity was used in place
of . The line of best fit, determined by linear regression, was
_(1 -Sw)
-
k rg -
1.5
2
(l-Sw),
............... (3)
0.7
where S w is the fractional water saturation, and k rg is the
relative gas permeability values of the samples extrapolated to infinite gas pressure. The data for all the
core samples and the line calculated by using Eq. 3 are
shown in Fig. 8.
Note that although a value of 1.5 for n appears to fit all
the data best, the value of n for individual core relative
permeabilities ranged from 1.1 to 1.6. The data point out
the necessity of obtaining reliable values of partial water
saturation to aid in the measurement of in-situ
permeability.
Discussion
If we assume that flow through tight sands can be modeled by a bundle of parallel capillaries, a comparison of
Poiseuille's law for viscous flow and Darcy's law indicates that
r=8.886xlO- 6 (kl)0.5,
................... (4)
b=0.0955(koogl) -0.53.
. . . . . . . . . . . . . . . . . . . . (6)
The observed change in permeability resulting from confining pressure or partial water saturation can be rationalized on a physical basis. As a result of increasing
confining pressure, a number of small capillaries are
closed off, and the effective flow paths are reduced both
in size and number. This is clear both from flow
measurements and from petrographic observations. In
the case of partial water saturation, water, being the wetting phase, tends to collect in smaller pores because of
capillary effects. Consequently, some of the flow paths
are no longer available for gas flow, and permeability is
lower. Nevertheless, the slip effect persists because the
effective size of flow paths available for gas flow is
lowered as a result of the presence of the wetting phase.
Conclusions
1. The extrapolated gas permeability of tight sandstones is affected significantly by confining pressure.
The constant in the relationship describing the slip
phenomenon during gas flow, b, was found to correlate
with the permeability/porosity ratio in a manner much
like that predicted from simple models.
2. Because of confining pressure, a number of small
intergranular pores that were pre~ent under surface conditions were sealed off. This also was verified by
petrographic studies.
3. The relative permeability behavior of the samples
investigated can be described approximately by a simple
empirical correlation.
2719
Nomenclature
a
b
c
kg
kL
k rg
k oog
m
fJ
r,rb
Sw
constant In Eq. 5
constant in Eq. I, MPa (psi)
constant in Eq. 2
apparent gas permeabil ity, md
liquid permeability, md
relative gas permeability, ratio
extrapolated gas permeability, md
constant in Eq. 5
mean pore pressure, MPa (psi)
capillary radius, cm (in.)
partial water saturation, %
porosity fraction
mean free path of gas, cm (in.)
Acknowledgments
We acknowledge the financial support from Bartlesville
Energy Technology Center and the DOE-Nevada Operations Office that made this work possible. We also
acknowledge the contributions of K.C. Wei and R. Hernandez, who helped in the data acquisition, and ofW.D.
Rose, whose discussions were very helpful.
References
I. Klinkenberg, L.J.: "The Permeability of Porous Media to Liquids
and Gases," Drill. and Prod. Prac., API (1941) 200-13.
2. Loeb, B.L.: The Kinetic 771'ory of Gases. third edition, Dover
Publications Inc., New York City (1961) 281-85.
3. Keighin, C. W.: "Influence of Diagenetic Reactions on Reservoir
Properties of the Ncslen, Farrer, and Tuscher Formations, Uinta
Basin, Utah," paper SPE 7919 presented at the 1979 SPE LowPenneability Gas Reservoirs Symposium, Denver, May 20-22.
4. Keighin, C.W. and Sampath, K.: "Evaluation of Pore Geometry
of Some Low-Permeability Sandstones-Uinta Basin." J. Pet.
Tech. (Jan. 1982) 65-70.
2720
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(OF-32)/1.8
x 1.0*
x 6.894 757
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