Gambar 1.

Perhitungan Analisis Data

Standarisasi NaOH
volume H2C2O4 2H2O
N H2C2O4 2H2O

= 5.00 mL
= 0.5 N

V NaOH

N NaOH

5.1+ 4.8+4.9
3

= 4.93

=
V (H2C2O4 2H2O) x N (H2C2O4 2H2O) = V NaOH x N NaOH
5 mL x 0.5 N
N NaOH

= 4.93 N x N NaOH
= 0.507 N

Menentukan Konsentrasi CH3COOH mula-mula

Konsentrasi variasi Ke-1

V NaOH x N NaOH = V (CH3COOH) x N (CH3COOH)

1.55 mL x 4.93
= 5mL x N CH3COOH
N CH3COOH = 0.1572 N

Konsentrasi variasi ke-2

V NaOH x N NaOH = V (CH3COOH) x N (CH3COOH)
1.225 mL x 4.93
= 5mL x N CH3COOH
N CH3COOH = 0.1572 N
Konsentrasi variasi ke-3
V NaOH x N NaOH = V (CH3COOH) x N (CH3COOH)
1.05 mL x 4.93
= 5mL x N CH3COOH
N CH3COOH = 0.1245 N
Konsentrasi variasi Ke-4
V NaOH x N NaOH = V (CH3COOH) x N (CH3COOH)
0.65 mL x 4.93
= 5mL x N CH3COOH
N CH3COOH = 0.0659 N
Konsentrasi variasi Ke-5
V NaOH x N NaOH = V (CH3COOH) x N (CH3COOH)
0.35 mL x 4.93
= 5mL x N CH3COOH
N CH3COOH = 0.0355 N

Gambar 2. Perhitungan Analisis Data

 Menentukan Konsentrasi CH3COOH dalam air

Konsentrasi variasi Ke-1

V NaOH x N NaOH = V (CH3COOH) x N (CH3COOH)

1.325 mL x 4.93
= 5mL x N CH3COOH
N CH3COOH = 0.1344 N

Konsentrasi variasi ke-2

V NaOH x N NaOH = V (CH3COOH) x N (CH3COOH)
1.125 mL x 4.93
= 5mL x N CH3COOH
N CH3COOH = 0.0127 N
Konsentrasi variasi ke-3
V NaOH x N NaOH = V (CH3COOH) x N (CH3COOH)
0.875 mL x 4.93
= 5mL x N CH3COOH
N CH3COOH = 0.0887 N
Konsentrasi variasi Ke-4
V NaOH x N NaOH = V (CH3COOH) x N (CH3COOH)
0.575 mL x 4.93
= 5mL x N CH3COOH
N CH3COOH = 0.0583 N
Konsentrasi variasi Ke-5
V NaOH x N NaOH = V (CH3COOH) x N (CH3COOH)
0.225 mL x 4.93
= 5mL x N CH3COOH
N CH3COOH = 0.0228 N

Gambar 3. Perhitungan Analisis Data

Menentukan Konsentrasi CH3COOH dalam eter

Konsentrasi variasi ke-1

N eter = N mula-mula N air

= 0.1572 N 0.1344N

= 0.0288 N

N eter = N mula-mula N air

Konsentrasi variasi ke-2

= 0.0659 N - 0.0583 N

N eter = N mula-mula N air

= 0.0076 N

= 0.1243N 0.0127 N
= 0.1116 N

Konsentrasi variasi ke-4

Konsentrasi variasi ke-5

N eter = N mula-mula N air

Konsentrasi variasi ke-3

= 0.0355 N 0.0288 N

N eter = N mula-mula N air

= 0.0127 N

= 0.1065 N 0.0887 N
= 0.0175 N

Gambar 4. Perhitungan Analisis Data

Nilai Koefisien distribusi pada masing-masing konsentrasi

Konsentrasi variasi ke-1

Kd

[ CH 3 COOH ] eter
[ CH 3COOH ] air

0.1344
0.0228

= 0.1696

Kd

[ CH 3 COOH ] eter
[ CH 3COOH ] air

[ CH 3 COOH ] eter
[ CH 3COOH ] air

= 0.1304

Konsentrasi variasi ke-5

0.0127
0.1116

0.0887
0.0178

= 0.2007

0.0583
0.0076

Kd

[ CH 3 COOH ] eter
[ CH 3COOH ] air

= 8.7874

Kd

Konsentrasi variasi ke-3

Kd

[ CH 3 COOH ] eter
[ CH 3COOH ] air

Konsentrasi variasi ke-2

Konsentrasi variasi ke-4

0.0228
0.0127

= 0.5570