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Faculty of Engineering and Materials Science, the German University in Cairo, Cairo, Egypt
Mechanical Design and Production Department, Faculty of Engineering, Zagazig University, Zagazig, Egypt
Department of Materials Science and Engineering, POSTECH (Pohang University of Science and Technology), Pohang 790-784, Republic of Korea
a r t i c l e
i n f o
Article history:
Received 12 June 2009
Received in revised form 6 October 2009
Accepted 10 October 2009
Keywords:
ECAP
AlCu alloys
FEM
Microhardness
Homogeneity of deformation
a b s t r a c t
Equal channel angular pressing (ECAP) is a material processing method that allows very high strains
to be imposed, leading to extreme work hardening and microstructural renement. To investigate the
deformation homogeneity in the transverse direction, rigid-viscoplastic 3D nite element simulations
were conducted for the different numbers of ECAP passes of Al with Cu contents 05%. The simulation
results indicated that the material on the outer side of the die channel undergoes less deformation than
that in the inner side due to the formation of a corner gap. It was also found that the homogeneity increased
with increasing the number of ECAP passes and the copper content due to the decrease in the size of the
corner gap. To verify the 3D nite element simulation results, the microhardness homogeneity across
the transverse direction of the billet was measured. The same trend was observed: the homogeneity
in hardness increased with increasing the number of ECAP passes and Cu contents from 0% to 5%. The
homogeneity of deformation indicated by microhardness and by FEM results was higher for route A
compared with route Bc and increases with the number of ECAP passes. The homogeneity in route A was
higher than that in route Bc by 10% after 2 passes up to 8 passes.
2009 Elsevier B.V. All rights reserved.
1. Introduction
Materials with nanometer or sub micrometer grain size have
received great interest in the last decades because of their unique
mechanical and physical properties and high performance [14].
Recently, several methods of severe plastic deformation (SPD) were
developed to process bulk nanostructured materials with a grain
size from 20 to 200 nm depending on a number of factors [58].
Equal channel angular pressing (ECAP) is considered the most popular among the various SPD processes. The principle of ECAP has
been discussed in many different works [7,8].
However, there are many works on Al 6000 series alloys [9] and
steels [10], but only a few works available on AlCu alloys processed
by ECAP. The microstructure and hardness of Al1.7 wt.% Cu alloy
after ECAP was studied [11], as well as the cyclic deformation and
fatigue properties of Al0.7 wt.% Cu alloy [12], the shear feature
of Al33 wt.% Cu eutectic alloy at 400 C [13], the tensile properties
Corresponding author at: Mechanical Design and Production Department, Faculty of Engineering, Zagazig University, Zagazig, Egypt. Tel.: +20 127195264;
fax: +20 55 2304987.
E-mail addresses: eng mohabdelall@yahoo.com, engmohabdela@postech.ac.kr
(M.I.A.E. Aal).
0921-5093/$ see front matter 2009 Elsevier B.V. All rights reserved.
doi:10.1016/j.msea.2009.10.032
and fracture modes of cast Al0.63 wt.% Cu and Al3.9 wt.% Cu alloys
[14] subjected to ECAP. Recently, Prados et al. studied the tensile
behavior of an ECAP processed Al4% Cu alloy [15]. However, there
is no work concerned with the homogeneity of these AlCu alloys,
as far as the authors know.
The nite element method (FEM) is one of the most important
numerical methods that can be used to explain the deformation
process during the ECAP and related processes [1622]. Most of the
previous studies done on the ECAP by FEM are in two dimensions
(2D) of the plain strain condition. They include the plastic deformation analyses of metallic materials during ECAP [16], the correct
selection of die channel in ECAP [17,18], die design for homogeneous plastic deformation during ECAP [19], FEM analysis of ECAP
in strain rate sensitive metals [20], texture evolution [21,22], modied ECAP processing [23], bending behavior [24], and the die corner
gap formation in ECAP [25]. Also, there is very little work on FEM
that has been done by the three dimensional (3D) method. Recently,
Suo et al. [26] and Basavaraj et al. [27] have done some 3D analyses to trace the homogeneity during the ECAP processes after the
rst pass. Xu et al. [28] and Jiang et al. [29] studied the distribution
of strain in the cross-section of the sample of pure Al and CP-Ti,
respectively, during the 3D FEM simulations for the multiple passes.
However, no work has been found for theoretical investigations and
tracing of the homogeneity of multiple passes during ECAP process.
N.E. Mahallawy et al. / Materials Science and Engineering A 527 (2010) 14041410
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Fig. 1. (a) ECAP die complete drawing and (b) the shape of the sample in the exit
from the die and the transverse direction (TD) of measuring the microhardness.
MaxH MinH
AvgH
(1)
(Maxp Minp)
,
Avgp
(2)
(3)
Fig. 2. True stress true strain relation pure aluminum, Al3%Cu alloy and Al5%Cu
alloy.
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The distribution of the microhardness along the traverse direction for the different alloys is used as an index of the inhomogeneity
of the plastic deformation across the samples. Fig. 4 indicates that
the microhardness values increase from the bottom to the top of
Fig. 4. The distribution of microhardness in the transverse direction (a) pure aluminum, (b) Al3%Cu alloy and (c) Al5%Cu alloy.
Fig. 5. The formation of the corner gap in (a) the second pass and (b) the eighth pass in the case of Al3%Cu homogenized alloy.
N.E. Mahallawy et al. / Materials Science and Engineering A 527 (2010) 14041410
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Table 1
3-D FEM simulation values of the corner gap angle for aluminum and Al3%Cu alloy.
Fig. 6. Effect of ECAP number of passes and copper content on inhomogeneity index
in microhardness.
the specimens. The lower values of the microhardness at the bottom of the specimens can be attributed to the formation of corner
gaps between the bottom of the specimen and the die during the
ECAP process, as shown in Fig. 5. As the gap made a corner gap in
the bottom of the specimen, the specimen was no longer in contact
with the die in this area. This reduced the deformation in the bottom part of the specimen. However, it should be noticed that the
difference between the values of microhardness from the bottom
to the top of the specimen decreased with the increasing number
of ECAP passes, due to the increase in homogeneity with further
deformation.
There have been analyses on the deformation behavior according to properties of matter in the case of the ECAP process because
Material
Processing route
Number of passes
Al
Al
Al
Al
Al
Al3%Cu alloy
Al3%Cu alloy
Route A
Route A
Route A
Route Bc
Route Bc
Route A
Route A
2
8
10
2
8
2
8
35
23
21
33
25
26
15
Fig. 7. Effective plastic strain distribution and the formation of corner gap (a) route A during the second pass of pure aluminum and (b) route A at the end of second pass of
pure aluminum.
Fig. 8. Effective plastic strain distribution and the formation of corner gap (a) route A during the tenth pass of pure aluminum and (b) route A at the end of tenth pass of pure
aluminum.
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Fig. 9. Effective plastic strain distribution and the formation of corner gap (a) route Bc during the second pass of pure aluminum and (b) route Bc at the end of second pass
of pure aluminum.
Fig. 10. Effective plastic strain distribution and the formation of corner gap (a) route Bc during the eighth pass of pure aluminum and (b) route Bc at the end of eighth pass
of pure aluminum.
Fig. 11. Effective plastic strain distribution and the formation of corner gap (a) route A during the second pass of Al3%Cu alloy and (b) route A at the end of second pass
Al3%Cu alloy.
is more representative for strain distribution, not on the outer surface of the workpiece as was investigated in previous work [28,29].
It was found that the value of strain at the top of the workpiece
was higher than that in the bottom. The distribution of the strain
along the transverse direction of the sample for Al and AlCu alloys
is shown in Fig. 13. It can be observed that the strain increased
Fig. 12. Effective plastic strain distribution and the formation of corner gap (a) route A during the eighth pass of Al3%Cu alloy and (b) rout A at the end of eighth pass
Al3%Cu alloy.
N.E. Mahallawy et al. / Materials Science and Engineering A 527 (2010) 14041410
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Fig. 13. The distribution of effective plastic strain in the transverse direction (a) pure aluminum, (b) Al3%Cu alloy and (c) Al5%Cu alloy.
from the bottom to the top of the sample. This behavior of strain
distribution was observed for Al processed by route A and route
Bc, for different AlCu alloys, and for different numbers of ECAP
passes. The same trend of strain distribution for different processing routes with Al was also observed in previous work with 3D
FEM simulations [2628,33] and 2D FEM simulations [16,18,19,25].
However, Tham et al. [34] indicated different 2D FEM results for Al
6061 alloy, for which the strain was higher at the bottom side of
specimen than at the top of the specimen. The formation of the
corner gap during the ECAP process can be the main reason for
the difference in the effective strain distribution from the top to
the bottom of the workpiece. The formation of the corner gap can
be observed during the ECAP for Al and Al3%Cu alloy, as shown
in Figs. 712 during 3D simulations, which was detected during
the actual ECAP for Al3%Cu alloy, as shown in Fig. 5. The size of
the gap was observed to be reduced with the increasing number
of ECAP passes. The corner gap angle in the case of Al process by
route A was reduced from 35 after 2 passes, down to 23 , and
then to 21 after 8 and 10 passes, respectively. The same behavior
was also observed for Al processed by route BC and for Al3%Cu
alloy of route A, as shown in Figs. 912. Table 1 indicates the values of the corner gap angle in pure Al processed by routes A and
Bc, and Al3%Cu alloy of route A. The formation of the corner gap
was detected in previous nite element works [25,27]. The reduction of the work harden ability that occurs during the ECAP can
explain the reduction of the corner gap with the increasing number of ECAP passes due to the increasing material ability to ll the
die corner.
It is observed that the size of the corner gap was reduced with
increasing Cu content. That is, after 2 passes the corner gap angle
was 35 , 33 and 26 in the cases of Al by route A, Al by route Bc,
and Al3%Cu alloy by route A, respectively. It is also observed that
after 8 passes the corner gap angle becomes 23 , 25 and 15 in the
cases of Al by route A, Al by route Bc, and Al3%Cu alloy by route A,
respectively. In the literature [30], the AlCu alloys were observed
to be more homogenized than the pure Al with the increasing number of ECAP passes. The formation and the reduction in the size of
the corner gap with the increasing number of ECAP passes is in good
agreement with the experimental results that shows that the size
of the corner gap decreases with the number of passes for Al3%Cu
alloy, as shown in Fig. 5. Also, the values of the corner gap angle
from the simulation results in the case of Al3%Cu alloy were very
close to those in the case of the experimental work, as indicated in
Table 1. The inhomogeneity indices of the effective plastic strain for
the different alloys are shown in Fig. 14. It can be observed that the
deformation homogeneity increased with the increasing number
of ECAP passes and the Cu content.
It is very interesting that the homogeneity simulated by FEM in
the case of route A was higher than that in case of route Bc, i.e., route
A homogeneity is higher than that for route Bc by about 10% after
the second pass. This trend stays the same after 6 and 8 passes. This
trend was conrmed from the experimental results, which show
that the homogeneity of route A was higher than that for route Bc
as shown in Fig. 6 except for the second pass. The present experimental and theoretical fact that route A ECAP is better than route
Bc is contradictory to the received knowledge that route Bc is better than route A in terms of grain renement. Therefore, a different
Fig. 14. Effect of ECAP number of passes and copper content on inhomogeneity
index in effective plastic strain.
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