7/26/2016 11:20:01 AM

Project 1
Project: Project 1
Owner: INCA
Site: Site of Interest 1

Sample: Sample 1
Type: Default
ID:

Spectrum Label: Spectrum 1

Livetime 60.0 s
Acquisition geometry ( degrees ):
Tilt = 0.0
Azimuth = 0.0
Elevation = 40.0
Accelerating voltage = 20.00 kV
Total spectrum counts = 241979
Sample data :
Strobe :

Energy (eV)
7.5

Resn. (eV)
57.89

Area
216147

Energy (eV)
-.1
6925.8

Resn. (eV)
59.50
145.48

Area
216288
93139

Optimization data : Cobalt K series

Strobe :
Optimization element :

Sample is unpolished X-ray corrections may be approximate.

Sample is uncoated
Detector efficiency : Calculation

Spectrum processing :
No peaks omitted
Processing option : All elements analyzed (Normalised)
Number of iterations = 3
Standard :
O SiO2 1-Jun-1999 12:00 AM
Fe Fe 1-Jun-1999 12:00 AM
La LaB6 1-Jun-1999 12:00 AM
Bi Bi 1-Jun-1999 12:00 AM
Element
OK
Fe K
La L
Bi M
Totals

App
Conc.
6.98
12.24
1.16
37.13

Intensity
Corrn.
0.7718
1.0304
0.9040
0.9072

Weight%
14.34
18.82
2.03
64.82
100.00

Weight%
Sigma
0.38
0.31
0.29
0.48

Atomic%
57.53
21.63
0.94
19.91

7/26/2016 11:20:25 AM

Project 1
Project: Project 1
Owner: INCA
Site: Site of Interest 1

Sample: Sample 1
Type: Default
ID:

Spectrum Label: Spectrum 2

Livetime 60.0 s
Acquisition geometry ( degrees ):
Tilt = 0.0
Azimuth = 0.0
Elevation = 40.0
Accelerating voltage = 20.00 kV
Total spectrum counts = 217308
Sample data :
Strobe :

Energy (eV)
7.5

Resn. (eV)
58.02

Area
217956

Energy (eV)
-.1
6925.8

Resn. (eV)
59.50
145.48

Area
216288
93139

Optimization data : Cobalt K series

Strobe :
Optimization element :

Sample is unpolished X-ray corrections may be approximate.

Sample is uncoated
Detector efficiency : Calculation

Spectrum processing :
No peaks omitted
Processing option : All elements analyzed (Normalised)
Number of iterations = 3
Standard :
O SiO2 1-Jun-1999 12:00 AM
Fe Fe 1-Jun-1999 12:00 AM
La LaB6 1-Jun-1999 12:00 AM
Bi Bi 1-Jun-1999 12:00 AM
Element
OK
Fe K
La L
Bi M
Totals

App
Conc.
7.67
10.21
0.97
33.39

Intensity
Corrn.
0.7824
1.0216
0.8982
0.9044

Weight%
16.97
17.29
1.87
63.88
100.00

Weight%
Sigma
0.42
0.32
0.31
0.51

Atomic%
62.78
18.33
0.80
18.10

7/26/2016 11:24:12 AM

Project 1
Project: Project 1
Owner: INCA
Site: Site of Interest 1

Sample: Sample 1
Type: Default
ID:

Spectrum Label: Spectrum 3

Livetime 60.0 s
Acquisition geometry ( degrees ):
Tilt = 0.0
Azimuth = 0.0
Elevation = 40.0
Accelerating voltage = 20.00 kV
Total spectrum counts = 203610
Sample data :
Strobe :

Energy (eV)
7.5

Resn. (eV)
57.97

Area
219014

Energy (eV)
-.1
6925.8

Resn. (eV)
59.50
145.48

Area
216288
93139

Optimization data : Cobalt K series

Strobe :
Optimization element :

Sample is unpolished X-ray corrections may be approximate.

Sample is uncoated
Detector efficiency : Calculation

Spectrum processing :
No peaks omitted
Processing option : All elements analyzed (Normalised)
Number of iterations = 3
Standard :
O SiO2 1-Jun-1999 12:00 AM
Fe Fe 1-Jun-1999 12:00 AM
La LaB6 1-Jun-1999 12:00 AM
Bi Bi 1-Jun-1999 12:00 AM
Element
OK
Fe K
La L
Bi M
Totals

App
Conc.
7.35
8.95
0.81
31.77

Intensity
Corrn.
0.7781
1.0215
0.8962
0.9064

Weight%
17.45
16.18
1.67
64.70
100.00

Weight%
Sigma
0.44
0.32
0.32
0.53

Atomic%
64.07
17.03
0.71
18.19

7/26/2016 11:34:14 AM

Project 1
Project: Project 1
Owner: INCA
Site: Site of Interest 1

Sample: Sample 1
Type: Default
ID:

Spectrum Label: Spectrum 4

Livetime 60.0 s
Acquisition geometry ( degrees ):
Tilt = 0.0
Azimuth = 0.0
Elevation = 40.0
Accelerating voltage = 20.00 kV
Total spectrum counts = 228974
Sample data :
Strobe :

Energy (eV)
7.5

Resn. (eV)
58.00

Area
217447

Energy (eV)
-.1
6925.8

Resn. (eV)
59.50
145.48

Area
216288
93139

Optimization data : Cobalt K series

Strobe :
Optimization element :

Sample is unpolished X-ray corrections may be approximate.

Sample is uncoated
Detector efficiency : Calculation

Spectrum processing :
No peaks omitted
Processing option : All elements analyzed (Normalised)
Number of iterations = 3
Standard :
O SiO2 1-Jun-1999 12:00 AM
Fe Fe 1-Jun-1999 12:00 AM
La LaB6 1-Jun-1999 12:00 AM
Bi Bi 1-Jun-1999 12:00 AM
Element
OK
Fe K
La L
Bi M
Totals

App
Conc.
7.52
12.11
2.23
33.18

Intensity
Corrn.
0.7987
1.0214
0.9062
0.8966

Weight%
15.50
19.52
4.05
60.92
100.00

Weight%
Sigma
0.40
0.32
0.31
0.50

Atomic%
59.11
21.33
1.78
17.78

7/26/2016 11:38:22 AM

Project 1
Project: Project 1
Owner: INCA
Site: Site of Interest 1

Sample: Sample 1
Type: Default
ID:

Spectrum Label: Spectrum 5

Livetime 60.0 s
Acquisition geometry ( degrees ):
Tilt = 0.0
Azimuth = 0.0
Elevation = 40.0
Accelerating voltage = 20.00 kV
Total spectrum counts = 217609
Sample data :
Strobe :

Energy (eV)
7.5

Resn. (eV)
58.27

Area
218109

Energy (eV)
-.1
6925.8

Resn. (eV)
59.50
145.48

Area
216288
93139

Optimization data : Cobalt K series

Strobe :
Optimization element :

Sample is unpolished X-ray corrections may be approximate.

Sample is uncoated
Detector efficiency : Calculation

Spectrum processing :
No peaks omitted
Processing option : All elements analyzed (Normalised)
Number of iterations = 3
Standard :
O SiO2 1-Jun-1999 12:00 AM
Fe Fe 1-Jun-1999 12:00 AM
La LaB6 1-Jun-1999 12:00 AM
Bi Bi 1-Jun-1999 12:00 AM
Element
OK
Fe K
La L
Bi M
Totals

App
Conc.
7.20
11.00
2.25
32.74

Intensity
Corrn.
0.7917
1.0229
0.9055
0.8991

Weight%
15.48
18.31
4.24
61.98
100.00

Weight%
Sigma
0.41
0.32
0.32
0.51

Atomic%
59.64
20.20
1.88
18.28

7/26/2016 11:42:04 AM

Project 1
Project: Project 1
Owner: INCA
Site: Site of Interest 1

Sample: Sample 1
Type: Default
ID:

Spectrum Label: Spectrum 6

Livetime 60.0 s
Acquisition geometry ( degrees ):
Tilt = 0.0
Azimuth = 0.0
Elevation = 40.0
Accelerating voltage = 20.00 kV
Total spectrum counts = 210007
Sample data :
Strobe :

Energy (eV)
7.5

Resn. (eV)
57.94

Area
218712

Energy (eV)
-.1
6925.8

Resn. (eV)
59.50
145.48

Area
216288
93139

Optimization data : Cobalt K series

Strobe :
Optimization element :

Sample is unpolished X-ray corrections may be approximate.

Sample is uncoated
Detector efficiency : Calculation

Spectrum processing :
No peaks omitted
Processing option : All elements analyzed (Normalised)
Number of iterations = 3
Standard :
O SiO2 1-Jun-1999 12:00 AM
Fe Fe 1-Jun-1999 12:00 AM
La LaB6 1-Jun-1999 12:00 AM
Bi Bi 1-Jun-1999 12:00 AM
Element
OK
Fe K
La L
Bi M
Totals

App
Conc.
6.96
10.93
2.12
32.16

Intensity
Corrn.
0.7906
1.0236
0.9057
0.8995

Weight%
15.29
18.54
4.06
62.10
100.00

Weight%
Sigma
0.41
0.32
0.32
0.51

Atomic%
59.21
20.57
1.81
18.41

7/26/2016 11:50:21 AM

Project 1
Project: Project 1
Owner: INCA
Site: Site of Interest 1

Sample: Sample 1
Type: Default
ID:

Spectrum Label: Spectrum 7

Livetime 60.0 s
Acquisition geometry ( degrees ):
Tilt = 0.0
Azimuth = 0.0
Elevation = 40.0
Accelerating voltage = 20.00 kV
Total spectrum counts = 265946
Sample data :
Strobe :

Energy (eV)
7.5

Resn. (eV)
58.21

Area
215041

Energy (eV)
-.1
6925.8

Resn. (eV)
59.50
145.48

Area
216288
93139

Optimization data : Cobalt K series

Strobe :
Optimization element :

Sample is unpolished X-ray corrections may be approximate.

Sample is uncoated
Detector efficiency : Calculation

Spectrum processing :
No peaks omitted
Processing option : All elements analyzed (Normalised)
Number of iterations = 3
Standard :
O SiO2 1-Jun-1999 12:00 AM
Fe Fe 1-Jun-1999 12:00 AM
La LaB6 1-Jun-1999 12:00 AM
Bi Bi 1-Jun-1999 12:00 AM
Element
OK
Fe K
La L
Bi M
Totals

App
Conc.
7.63
15.31
3.80
37.24

Intensity
Corrn.
0.8052
1.0247
0.9141
0.8924

Weight%
13.49
21.25
5.91
59.35
100.00

Weight%
Sigma
0.34
0.31
0.30
0.46

Atomic%
54.38
24.55
2.75
18.32

7/26/2016 11:54:53 AM

Project 1
Project: Project 1
Owner: INCA
Site: Site of Interest 1

Sample: Sample 1
Type: Default
ID:

Spectrum Label: Spectrum 8

Livetime 60.0 s
Acquisition geometry ( degrees ):
Tilt = 0.0
Azimuth = 0.0
Elevation = 40.0
Accelerating voltage = 20.00 kV
Total spectrum counts = 255120
Sample data :
Strobe :

Energy (eV)
7.5

Resn. (eV)
58.08

Area
215660

Energy (eV)
-.1
6925.8

Resn. (eV)
59.50
145.48

Area
216288
93139

Optimization data : Cobalt K series

Strobe :
Optimization element :

Sample is unpolished X-ray corrections may be approximate.

Sample is uncoated
Detector efficiency : Calculation

Spectrum processing :
No peaks omitted
Processing option : All elements analyzed (Normalised)
Number of iterations = 3
Standard :
O SiO2 1-Jun-1999 12:00 AM
Fe Fe 1-Jun-1999 12:00 AM
La LaB6 1-Jun-1999 12:00 AM
Bi Bi 1-Jun-1999 12:00 AM
Element
OK
Fe K
La L
Bi M
Totals

App
Conc.
7.09
14.58
3.72
36.15

Intensity
Corrn.
0.8009
1.0265
0.9147
0.8937

Weight%
13.10
21.02
6.01
59.86
100.00

Weight%
Sigma
0.36
0.31
0.31
0.47

Atomic%
53.69
24.69
2.84
18.79

7/26/2016 11:59:40 AM

Project 1
Project: Project 1
Owner: INCA
Site: Site of Interest 1

Sample: Sample 1
Type: Default
ID:

Spectrum Label: Spectrum 10

Livetime 60.0 s
Acquisition geometry ( degrees ):
Tilt = 0.0
Azimuth = 0.0
Elevation = 40.0
Accelerating voltage = 20.00 kV
Total spectrum counts = 243517
Sample data :
Strobe :

Energy (eV)
7.5

Resn. (eV)
58.12

Area
215998

Energy (eV)
-.1
6925.8

Resn. (eV)
59.50
145.48

Area
216288
93139

Optimization data : Cobalt K series

Strobe :
Optimization element :

Sample is unpolished X-ray corrections may be approximate.

Sample is uncoated
Detector efficiency : Calculation

Spectrum processing :
No peaks omitted
Processing option : All elements analyzed (Normalised)
Number of iterations = 3
Standard :
O SiO2 1-Jun-1999 12:00 AM
Fe Fe 1-Jun-1999 12:00 AM
La LaB6 1-Jun-1999 12:00 AM
Bi Bi 1-Jun-1999 12:00 AM
Element
OK
Fe K
La L
Bi M
Totals

App
Conc.
6.44
13.71
3.71
33.45

Intensity
Corrn.
0.8023
1.0269
0.9162
0.8928

Weight%
12.78
21.23
6.43
59.56
100.00

Weight%
Sigma
0.36
0.33
0.32
0.49

Atomic%
52.89
25.17
3.07
18.88

7/26/2016 12:13:01 P M

Project 1
Project: Project 1
Owner: INCA
Site: Site of Interest 1

Sample: Sample 1
Type: Default
ID:

Spectrum Label: Spectrum 12

Livetime 60.0 s
Acquisition geometry ( degrees ):
Tilt = 0.0
Azimuth = 0.0
Elevation = 40.0
Accelerating voltage = 20.00 kV
Total spectrum counts = 215370
Sample data :
Strobe :

Energy (eV)
7.5

Resn. (eV)
57.99

Area
218084

Energy (eV)
-.1
6925.8

Resn. (eV)
59.50
145.48

Area
216288
93139

Optimization data : Cobalt K series

Strobe :
Optimization element :

Sample is unpolished X-ray corrections may be approximate.

Sample is uncoated
Detector efficiency : Calculation

Spectrum processing :
No peaks omitted
Processing option : All elements analyzed (Normalised)
Number of iterations = 4
Standard :
O SiO2 1-Jun-1999 12:00 AM
Fe Fe 1-Jun-1999 12:00 AM
La LaB6 1-Jun-1999 12:00 AM
Bi Bi 1-Jun-1999 12:00 AM
Element
OK
Fe K
La L
Bi M
Totals

App
Conc.
21.04
7.59
3.22
19.61

Intensity
Corrn.
1.0087
0.9426
0.8768
0.8496

Weight%
37.47
14.46
6.59
41.47
100.00

Weight%
Sigma
0.50
0.31
0.35
0.55

Atomic%
82.27
9.10
1.67
6.97

7/26/2016 12:15:01 P M

Project 1
Project: Project 1
Owner: INCA
Site: Site of Interest 1

Sample: Sample 1
Type: Default
ID:

Spectrum Label: Spectrum 13

Livetime 60.0 s
Acquisition geometry ( degrees ):
Tilt = 0.0
Azimuth = 0.0
Elevation = 40.0
Accelerating voltage = 20.00 kV
Total spectrum counts = 234347
Sample data :
Strobe :

Energy (eV)
7.5

Resn. (eV)
58.25

Area
217248

Energy (eV)
-.1
6925.8

Resn. (eV)
59.50
145.48

Area
216288
93139

Optimization data : Cobalt K series

Strobe :
Optimization element :

Sample is unpolished X-ray corrections may be approximate.

Sample is uncoated
Detector efficiency : Calculation

Spectrum processing :
No peaks omitted
Processing option : All elements analyzed (Normalised)
Number of iterations = 3
Standard :
O SiO2 1-Jun-1999 12:00 AM
Fe Fe 1-Jun-1999 12:00 AM
La LaB6 1-Jun-1999 12:00 AM
Bi Bi 1-Jun-1999 12:00 AM
Element
OK
Fe K
La L
Bi M
Totals

App
Conc.
15.14
10.95
4.37
30.73

Intensity
Corrn.
0.8865
0.9832
0.8944
0.8718

Weight%
25.00
16.30
7.15
51.56
100.00

Weight%
Sigma
0.42
0.29
0.31
0.49

Atomic%
72.59
13.56
2.39
11.46

7/26/2016 12:19:04 P M

Project 1
Project: Project 1
Owner: INCA
Site: Site of Interest 1

Sample: Sample 1
Type: Default
ID:

Spectrum Label: Spectrum 14

Livetime 60.0 s
Acquisition geometry ( degrees ):
Tilt = 0.0
Azimuth = 0.0
Elevation = 40.0
Accelerating voltage = 20.00 kV
Total spectrum counts = 198440
Sample data :
Strobe :

Energy (eV)
7.5

Resn. (eV)
58.06

Area
219290

Energy (eV)
-.1
6925.8

Resn. (eV)
59.50
145.48

Area
216288
93139

Optimization data : Cobalt K series

Strobe :
Optimization element :

Sample is unpolished X-ray corrections may be approximate.

Sample is uncoated
Detector efficiency : Calculation

Spectrum processing :
No peaks omitted
Processing option : All elements analyzed (Normalised)
Number of iterations = 4
Standard :
O SiO2 1-Jun-1999 12:00 AM
Fe Fe 1-Jun-1999 12:00 AM
La LaB6 1-Jun-1999 12:00 AM
Bi Bi 1-Jun-1999 12:00 AM
Element
OK
Fe K
La L
Bi M
Totals

App
Conc.
20.25
6.41
2.83
19.35

Intensity
Corrn.
0.9973
0.9422
0.8730
0.8526

Weight%
38.28
12.83
6.11
42.78
100.00

Weight%
Sigma
0.52
0.31
0.36
0.56

Atomic%
83.33
8.00
1.53
7.13

7/26/2016 12:21:29 P M

Project 1
Project: Project 1
Owner: INCA
Site: Site of Interest 1

Sample: Sample 1
Type: Default
ID:

Spectrum Label: Spectrum 15

Livetime 60.0 s
Acquisition geometry ( degrees ):
Tilt = 0.0
Azimuth = 0.0
Elevation = 40.0
Accelerating voltage = 20.00 kV
Total spectrum counts = 217080
Sample data :
Strobe :

Energy (eV)
7.5

Resn. (eV)
57.92

Area
218260

Energy (eV)
-.1
6925.8

Resn. (eV)
59.50
145.48

Area
216288
93139

Optimization data : Cobalt K series

Strobe :
Optimization element :

Sample is unpolished X-ray corrections may be approximate.

Sample is uncoated
Detector efficiency : Calculation

Spectrum processing :
No peaks omitted
Processing option : All elements analyzed (Normalised)
Number of iterations = 4
Standard :
O SiO2 1-Jun-1999 12:00 AM
Fe Fe 1-Jun-1999 12:00 AM
La LaB6 1-Jun-1999 12:00 AM
Bi Bi 1-Jun-1999 12:00 AM
Element
OK
Fe K
La L
Bi M
Totals

App
Conc.
27.31
4.83
2.23
12.53

Intensity
Corrn.
1.1609
0.9069
0.8599
0.8329

Weight%
50.61
11.45
5.58
32.36
100.00

Weight%
Sigma
0.58
0.32
0.39
0.59

Atomic%
88.77
5.76
1.13
4.34

7/26/2016 12:23:47 P M

Project 1
Project: Project 1
Owner: INCA
Site: Site of Interest 1

Sample: Sample 1
Type: Default
ID:

Spectrum Label: Spectrum 16

Livetime 60.0 s
Acquisition geometry ( degrees ):
Tilt = 0.0
Azimuth = 0.0
Elevation = 40.0
Accelerating voltage = 20.00 kV
Total spectrum counts = 221027
Sample data :
Strobe :

Energy (eV)
7.5

Resn. (eV)
58.01

Area
218027

Energy (eV)
-.1
6925.8

Resn. (eV)
59.50
145.48

Area
216288
93139

Optimization data : Cobalt K series

Strobe :
Optimization element :

Sample is unpolished X-ray corrections may be approximate.

Sample is uncoated
Detector efficiency : Calculation

Spectrum processing :
Peak possibly omitted : 3.682 keV
Processing option : All elements analyzed (Normalised)
Number of iterations = 3
Standard :
O SiO2 1-Jun-1999 12:00 AM
Fe Fe 1-Jun-1999 12:00 AM
La LaB6 1-Jun-1999 12:00 AM
Bi Bi 1-Jun-1999 12:00 AM
Element
OK
Fe K
La L
Bi M
Totals

App
Conc.
12.19
10.92
4.37
26.70

Intensity
Corrn.
0.8872
0.9879
0.9012
0.8700

Weight%
22.79
18.32
8.04
50.85
100.00

Weight%
Sigma
0.42
0.32
0.34
0.51

Atomic%
69.36
15.97
2.82
11.85