etl ual Asubell Glacial Ab citi i 2D- NMR Altes lected 152: Thymol dyad OS y+ ye 2D - NMR fables uli : he STH ONMR isin a eat 59) Ol See -1 ad oe Galil abel) Gla Be cues aby Salt NMR ol cit 0 Suid ote yas OM add. pall jut 5 Asal de pial AED oth Sal ya dB ys Gy pd Nea ght Gk at Cut Cit) eo la Gb ygly Uyall | H¢ NMR igule pad Mish clues (1) Spin acing ( gil) gaat gle (cel) ual glad 2 * sal 1 - NMRSe nh gals CHS 3303 game Sanh gia ss (7) Sosa la Go Sed esas A GD Ja “Cpl Ibs Gly ( PPM 1.25) Bin: Denk on 65 tse 98 oI ola ye NS fl gg ttl lidyy . CDCLI (8 =3.1 PPM) cui8 se Sel La of a Aa CHAS ob toys 2p 3 Aged Sa S18 2.3 CUNT ae Ay. Sad Syne LoS sil aD a DB Ses pied Seiad ae gt ( P =4.6PPM) ae ch 580 LI CH3)5 365 Gp pe Spl Ay La Chala Ung H-NMR Gi gel Opt ASD Se cee ea a pie Saad pa GL Oy ta he logy Yeas TSC = NMR igs 5 geal sgl) Quill ila -2. PRY ae le Le pb tlh GILL) pte ny Tens C-NMR Gite Ss Gy Hin ab EE aay pln Ja ae a, gah end ae oily oe SD by as 153 PPM cu sAl sie aii ince 359 Aa, 50d yh ped Sad Se DI ge nd tates (Tay 8D 9S) Ung aed bed a wg dhe Byes a8 3810 gay Kl li of etd ear NM ino Me e ¢ ‘ . .{DEPT ) Ayibisast Jit » gt pant SAB LSE, A) Lhlel aos eg ial Gb us st ae Gas a a 76 AB By ip SIA) BE ow SB go) ais J DEPT Sih on 5.8 (Si apy Bg sth GAL LE ge is ty (PPM, 126,121,116,27) Vest sta! ( oH 8D po5 Shy BLD, ASI oy SI yj A yal GI dey oe aay ASIEN ALM SG ane Dag ell ah ED WAL 7.6.435> on Sl SARS on S 8 GS any A std abit SHS SED syn yB got Gu ge Hd, (PPM 126,121,116,27)shas Eovpe Ua hL 14, (/23,23.21 ) Azesll Weald (9.8;10 dy ons LS) Ly DERE gs Test gin Da A Gk Ge BA Gael Gakht) La) «(PEM 156,137,131) ya tied Webs dad on S oe + (2D) su SuINMR obits Ga —4 toatl) Spa hay gad Ba gRINMR hit tS gb) glee Sail alae et gla sl) Shea! U8 Gu : HMQ@C gi HETCOR Gb 4-1 #1 2a, Spectrum of Hetéonuclear chemical shift correlatin Sy ae 5 ae Ue sa hs ty se SYS Oo RD oh a 5 ISD SED i J pail HM@C Gib geliy 1928 53 SS) Aas pall Gam gg CS Qe one| ssl) geal LSAT oe Maly I Dia ged JN BU as ae Sat AN sod Wye ES es eS athe Gy A oy OM th SU goed ye US SS Cae Ge Ud F2 sy Hd Sw SI 5s ipa 28g al py AN ge Saas Fl on All Asana QD cle pD til pd oy 9 58512) oe FQ yr ye thd Ha Lt Seale 4G J ans FY gyal iJ ye Une il pad yh 5 ALS GE Cage Ge Luddy PPM. OAS A Ae on 501 J gl 21 PPM cla gi Su Sty ths 23 ay AN gle hea Ub La) UE phe Me GS LI. CHB Saal bey Daa NS tS (7) ysall Gays 9S 9 SS a yl Son pall Sd alain $ See SI ala IS Spal eg ie gh Ge SII SNS Als aS OHI Jyully Ae ES She GE geal NY caked OUR FGA slat gy lef | jbl! HTH COSY ib 2 Correlationspectroscopy UL Jaaisl guy ASD 1D odin DOF - COSY jest Gihll Id iy SS oe CB Bae Ge tihuly Seay Double ~Quantum Filtrcol St ge WEE ty My gd J DEF ty eae ce Anat om val 1H Ge CALEY ie pat ali ISA nes jal iy SD OGD ane seall—'H Cosy orcosy snaBES CS Yd Sy HH Cosy sib J Jaa) Oa Gly a ade Bs: SHAY ge Bo oe oc \ as Ansa le ila ot Leb J Yd pal ah ship pled alll AAS CrOSS Kase fne ayn y a. A) LL jhall W Aacly Ged bte ats GEM Oe FEZ yaad ly coal on Lage Cal os els © 18 pealgs YI-CHOCHB}2 £059 JY pias 3.2 CUBM Hi sia CS ans FT gyal 9p eB ogy ALD oye BOM Cam, lady Cabal 1 3.2 chsf ~ ses Bahay 1.33 CUM SB bss tls ye asleel7 ows SS osaH Spey ADU 13 Gill gh NT Lilay 2.3 PPM CUA cud 5L2Y) Usal 136CHS 2923 cus giasaad ow ets on I gl (6.7, 6.6) Leal in fas as F286 oe SI bbs al odeadl ee (10 oe ose) Sj asee (4 csse isas pl) BN aa (6 cae St a Auta) ( PPM 6.6 ) csi li a Us) Gx 8B 48 Anil) (PPM 6.7 ,2.3) Legals) cain finn ad aps Aad Gall LL CIF (6 Gms 5S atr2) 6.6 CUR 8 OSs ow LaF ge lids 510 eared she tie cs (10 an SI ey bs) Tid n5 oss ee Sod PPM 6.7 clit Sis yt Wish WY (A ce 6 5s hiya) cla By} sig (PPM 7.1, Weald kin ine aif OO aos las (4 oe TLE oul) on ES) Ake WE oe oD ser a Mosse I 166,23) Sas beds AN) Shed AN Ge SIS Ose ee Sd cE CIE (4 BAY thy) Bd bs Bey Bad CIB cdkey Bay OB 328 oD oe AS a) ka Ge ES sa Oe oe (10 on sd Hana ones les (6-3 (Rata esl ase at yl ub) : HMBC Gb § Hetronvlear Multiple Bond Coheince Spectrum AC ee cam ally SO CIS Gee CID Rae Oe Ra ge OM Sse, GH A A a dalyg gol af AB islets J hag dag SDE gd Uae Bd HMBC ile 1 rns at E e peall Bly al AS) y Cl gyn ge — CHS ual ej Gwe sl le 8) COSY eb Gl 88.2 chil Si ed ste 61 Ge Lek Uae Naar 0d oe bane SS BO ay SICA Aas CHa MI Ge paal FI pea alee (7 Oss) 28 (C89) eS (7 oe odes) cin 643 oor ed OS Le ae Digs S88 we (1) Gor Slls day SPE ge (C-3 )s cathy I) oe (C-2)s uth Bay oad CLM ed =2.2 8 ps ae FL sonal Gye the Leas Hy (5) 605 Bas 228 pe (4) Sp 80 2s a fe a DE (10) 2e (Tse Sl ae Susy dl Ban) Mtl sige TAS Ge Lig aay clad aePENA SS 03 oy hy, 08 se 2) nA ooh) TP Mid tis es 500 on ial assy yy, ne = (ilees MBE 6), 300555 8) 395 oy ts sy Sass MO 8) SANS 6 P) 965 Met sous sy 13. PAAVVO MMOH oO Hoenti C z 2 a8 C 23 cea = 2 os cHler L = cd a 52 Manes | | 6723 66 6 ee fe 3206) | = sta) 67 7 6 hana a “ 131 (hana ot ny a 137 kon ¢ ee at on wh 153, a nee Pye 8.