Lampiran 1

DAFTAR KONVERSI AYAKAN DARI MESH KE MIKRON

U. S
MESH
3
4
5
6
8
10
12
14
16
18
20
25
30
35
40
45
50
60
70
80
100
120
140
170
200
230
270
325
400
625
1250
2500

INCHES

MICRONS

MILLIMETERS

0,2650
0,1870
0,1570
0,1320
0,0937
0,0787
0,0661
0,0555
0,0469
0,0394
0,0331
0,0280
0,0232
0,0197
0,0165
0,0138
0,0117
0,0098
0,0083
0,0070
0,0059
0,0049
0,0041
0,0035
0,0029
0,0024
0,0021
0,0017
0,0015
0,0008
0,0004
0,0002

6730
4760
4000
3360
2380
2000
1680
1410
1190
1000
841
707
595
500
400
354
297
250
210
177
149
125
105
8
74
63
53
44
37
20
10
5

6,730
4,760
4,000
3,360
2,380
2,000
1,680
1,410
1,190
1,000
0,841
0,707
0,595
0,500
0,400
0,354
0,297
0,250
0,210
0,177
0,149
0,125
0,105
0,088
0,074
0,063
0,053
0,044
0,037
0,020
0,010
0,005

http://www.skylighter.com/fireworks/help/Mesh_to_Microns_Coversion_Chart.a

Universitas Sumatera Utara

Lampiran 2.
Hasil Pengukuran Nanopartikel Bentonit

Universitas Sumatera Utara

Lampiran 3.
Data Hasil Pengukuran Viskositas Karet Alam

Universitas Sumatera Utara

Universitas Sumatera Utara

Lampiran 4.
Data Hasil Uji Tarik Nanokomposit Karet Alam/Bentonit

Universitas Sumatera Utara

Lampiran 5.
Data Hasil Uji Tarik Nanokomposit Karet Alam/Bentonit-CTAB

Universitas Sumatera Utara

Lampiran 6.
Data Hasil Uji Tarik Nanokomposit Karet Alam/Bentonit-PEG

Universitas Sumatera Utara

Lampiran 7.
Data Hasil Uji Tarik Nanokomposit Karet Alam/Bentonit-SDS

Universitas Sumatera Utara

Lampiran 8.
Data Hasil Analisis Uji Kestabilan Termal Nanokomposit Karet Alam/Bentonit

Universitas Sumatera Utara

Lampiran 9.
Data Hasil Analisis Uji Kestabilan Termal Nanokomposit Karet Alam/Bentonit-CTAB

Universitas Sumatera Utara

Lampiran 10.
Data Hasil Analisis Uji Kestabilan Termal Nanokomposit Karet Alam/Bentonit-PEG

Universitas Sumatera Utara

Lampiran 11.
Data Hasil Analisis Uji Kestabilan Termal Nanokomposit Karet Alam/Bentonit-SDS

Universitas Sumatera Utara

Lampiran 12.
Spektrum FT-IR Nanokomposit Karet Alam/Bentonit

Universitas Sumatera Utara

Lampiran 13.
Spektrum FT-IR Bentonit-CTAB

Universitas Sumatera Utara

Lampiran 14.
Spektrum FT-IR Bentonit-PEG

Universitas Sumatera Utara

Lampiran 15.
Spektrum FT-IR Bentonit-SDS

Universitas Sumatera Utara

Lampiran 16.
Spektrum XRD Bentonit
Sampel_Firman
800
700
600
Intensitas

500
400
300
200
100
0
0

20

40

60

80

100

2 theta

No.
1
2
3
4
5
6
7
8
9
10
11
12
13
14

Pos.
[2Th.]
10.7108
22.0416
23.8101
24.4887
26.8025
28.0081
30.4649
31.6564
35.7053
42.424
47.0161
48.4997
49.8345
51.5749

d-spacing []
8.235
3.963993
3.666463
3.56382
3.253334
3.112119
2.859381
2.751131
2.438098
2.052797
1.854272
1.798415
1.751102
1.693229

Rel. Int.
[%]
17.66
69.09
45.12
31.5
27.16
100
25.18
10.6
30.49
11.09
11.58
15.82
15.46
17

FWHM
[2Th.]
0.1181
0.2755
0.2362
0.3149
0.2362
0.3936
0.1968
0.4723
0.4723
0.9446
0.6298
0.3149
0.4723
0.2362

Area
[cts*2Th.]
7.72
70.43
39.43
36.7
23.74
145.63
18.33
18.52
53.29
38.75
26.98
18.44
27.01
14.85

Backgr.[cts]
277
335
339
340
333.37
327
308
295
265
230
201
195
198
197

Height
[cts]
66.25
259.14
169.25
118.16
101.89
375.08
94.43
39.76
114.38
41.58
43.43
59.35
57.98
63.75

Universitas Sumatera Utara

Lampiran 17.
Spektrum XRD Bentonit-CTAB

Universitas Sumatera Utara

File: THE-2.DI
29-May-2013 14:43
=============================================================
=================
Philips Analytical
PC-APD, Diffraction software
Sample identification: Sampel 2
Data measured at: 29-May-2013 12:03:00
Diffractometer type: PW1710 BASED
Tube anode: Cu
Generator tension [kV]: 40
Generator current [mA]: 30
Wavelength Alpha1 []: 1.54060
Wavelength Alpha2 []: 1.54439
Intensity ratio (alpha2/alpha1): 0.500
Divergence slit: 1
Receiving slit: 0.45
Monochromator used: NO
Start angle [2]: 5.000
End angle [2]: 44.980
Step size [2]: 0.020
Maximum intensity: 772.8400
Time per step [s]: 0.800
Type of scan: CONTINUOUS
Minimum peak tip width: 0.12
Maximum peak tip width: 1.00
Peak base width: 2.00
Minimum significance: 0.60
Number of peaks:
22
Angle d-value d-value Peak width Peak int Back. int Rel. int Signif.
[2] 1 [] 2 [] [2] [counts] [counts] [%]
10.775
13.925
15.440
20.075
22.160
23.060
23.885
24.670
25.765

8.2042
6.3546
5.7343
4.4196
4.0082
3.8538
3.7225
3.6058
3.4550

8.2244
6.3702
5.7484
4.4304
4.0181
3.8633
3.7317
3.6147
3.4635

0.240
0.240
0.960
0.480
0.240
0.280
0.240
0.160
0.160

77
38
13
42
552
135
317
185
130

296
299
299
324
324
324
324
324
324

10.0
2.36
5.0
1.01
1.7
0.97
5.5
0.98
71.5
8.39
17.4
2.05
41.0
4.57
23.9
0.96
16.8
0.67

Universitas Sumatera Utara

26.845
27.975
28.245
28.665
29.765
30.610
31.690
33.340
33.875
35.765
39.425
42.550
43.415

3.3184
3.1869
3.1570
3.1117
2.9992
2.9183
2.8212
2.6853
2.6441
2.5086
2.2837
2.1229
2.0826

3.3266
3.1947
3.1648
3.1194
3.0065
2.9255
2.8282
2.6919
2.6506
2.5148
2.2893
2.1282
2.0878

0.160
0.280
0.120
0.120
0.160
0.120
0.240
0.320
0.160
0.160
0.480
0.640
0.320

237
773
552
240
114
188
123
66
29
259
26
58
38

324
328
328
328
328
328
328
328
328
328
313
299
296

30.7
100.0
71.5
31.1
14.8
24.3
15.9
8.5
3.8
33.5
3.4
7.5
5.0

1.59
6.19
1.98
1.21
0.96
0.70
2.27
2.58
0.64
0.84
1.28
0.89
0.62

Universitas Sumatera Utara

Lampiran 18.
Spektrum

XRD

Bentonit-PEG

Universitas Sumatera Utara

File: THE-3.DI
29-May-2013 14:43
=============================================================
=================
Philips Analytical
PC-APD, Diffraction software
Sample identification: Sampel 3
Data measured at: 29-May-2013 12:49:00
Diffractometer type: PW1710 BASED
Tube anode: Cu
Generator tension [kV]: 40
Generator current [mA]: 30
Wavelength Alpha1 []: 1.54060
Wavelength Alpha2 []: 1.54439
Intensity ratio (alpha2/alpha1): 0.500
Divergence slit: 1
Receiving slit: 0.45
Monochromator used: NO
Start angle [2]: 5.000
End angle [2]: 44.980
Step size [2]: 0.020
Maximum intensity: 846.8100
Time per step [s]: 0.800
Type of scan: CONTINUOUS
Minimum peak tip width: 0.12
Maximum peak tip width: 1.00
Peak base width: 2.00
Minimum significance: 0.60
Number of peaks:
21
Angle d-value d-value Peak width Peak int Back. int Rel. int Signif.
[2] 1 [] 2 [] [2] [counts] [counts] [%]
10.715
13.920
20.865
22.065
22.960
23.800
24.565
25.705
26.765

8.2500
6.3568
4.2540
4.0253
3.8704
3.7356
3.6210
3.4629
3.3281

8.2703
6.3725
4.2645
4.0352
3.8799
3.7448
3.6299
3.4714
3.3363

0.120
0.480
0.240
0.180
0.200
0.160
0.240
0.200
0.160

59
25
86
650
161
372
199
132
266

272
279
353
350
350
346
346
342
339

7.0
0.66
3.0
0.98
10.2
0.86
76.8
7.16
19.0
1.17
44.0
2.20
23.5
2.27
15.6
0.97
31.4
1.32

Universitas Sumatera Utara

27.905
28.145
28.575
29.665
30.475
31.615
33.245
33.870
35.900
39.625
40.730
42.590

3.1947
3.1680
3.1213
3.0091
2.9309
2.8278
2.6927
2.6445
2.4995
2.2727
2.2135
2.1210

3.2026
3.1758
3.1290
3.0165
2.9381
2.8347
2.6994
2.6510
2.5056
2.2782
2.2190
2.1263

0.240
0.120
0.160
0.120
0.200
0.280
0.280
0.240
0.320
0.480
0.240
0.320

847
625
225
110
188
98
83
30
172
22
20
64

339
339
335
335
331
331
328
324
320
299
292
286

100.0
73.8
26.6
13.0
22.2
11.6
9.8
3.6
20.3
2.6
2.4
7.6

6.58
1.34
1.00
0.61
1.66
2.20
2.48
0.88
2.61
1.18
0.65
0.67

Lampiran 19.
Spektrum XRD Bentonit-SDS

Universitas Sumatera Utara

File: THE-1.DI
29-May-2013 14:43
=============================================================
=================
Philips Analytical
PC-APD, Diffraction software
Sample identification: Sampel 1

Universitas Sumatera Utara

Data measured at: 29-May-2013 11:30:00

Diffractometer type: PW1710 BASED
Tube anode: Cu
Generator tension [kV]: 40
Generator current [mA]: 30
Wavelength Alpha1 []: 1.54060
Wavelength Alpha2 []: 1.54439
Intensity ratio (alpha2/alpha1): 0.500
Divergence slit: 1
Receiving slit: 0.45
Monochromator used: NO
Start angle [2]: 5.000
End angle [2]: 44.980
Step size [2]: 0.020
Maximum intensity: 707.5600
Time per step [s]: 0.800
Type of scan: CONTINUOUS
Minimum peak tip width: 0.12
Maximum peak tip width: 1.00
Peak base width: 2.00
Minimum significance: 0.60
Number of peaks:
18
Angle d-value d-value Peak width Peak int Back. int Rel. int Signif.
[2] 1 [] 2 [] [2] [counts] [counts] [%]
7.700 11.4723
10.710 8.2538
13.875 6.3774
22.145 4.0109
22.965 3.8695
23.875 3.7241
24.660 3.6073
25.840 3.4451
26.830 3.3202
27.965 3.1880
28.255 3.1559
28.625 3.1160
29.760 2.9997
30.505 2.9281
31.635 2.8260

11.5005
8.2741
6.3931
4.0208
3.8790
3.7332
3.6161
3.4536
3.3284
3.1958
3.1637
3.1236
3.0070
2.9353
2.8330

0.120
0.200
0.480
0.220
0.200
0.160
0.280
0.120
0.200
0.240
0.120
0.120
0.240
0.160
0.200

26
88
26
462
77
276
139
94
207
708
484
177
94
169
86

310
276
272
339
339
335
335
331
331
328
328
328
324
324
320

3.7
0.86
12.5
1.55
3.7
0.97
65.3
8.49
10.9
0.90
38.9
1.87
19.7
2.54
13.3
0.80
29.3
2.34
100.0
4.46
68.4
0.78
25.0
1.14
13.3
1.76
23.9
1.23
12.2
0.91

Universitas Sumatera Utara

33.295 2.6888 2.6954

35.800 2.5062 2.5124
39.705 2.2683 2.2738

0.240
0.280
0.640

71
222
18

317
320
299

10.0
31.4
2.5

0.66
3.07
0.70

Lampiran 20.
Spektrum XRD Nanokomposit Karet Alam/Bentonit

Universitas Sumatera Utara

File: THE-9.DI
29-May-2013 14:44
=============================================================
=================

Universitas Sumatera Utara

Philips Analytical

PC-APD, Diffraction software

Sample identification: Sampel 9

Data measured at: 28-May-2013 13:38:00
Diffractometer type: PW1710 BASED
Tube anode: Cu
Generator tension [kV]: 40
Generator current [mA]: 30
Wavelength Alpha1 []: 1.54060
Wavelength Alpha2 []: 1.54439
Intensity ratio (alpha2/alpha1): 0.500
Divergence slit: 1
Receiving slit: 0.45
Monochromator used: NO
Start angle [2]: 5.000
End angle [2]: 44.980
Step size [2]: 0.020
Maximum intensity: 1324.960
Time per step [s]: 0.800
Type of scan: CONTINUOUS
Minimum peak tip width: 0.12
Maximum peak tip width: 1.00
Peak base width: 2.00
Minimum significance: 0.60
Number of peaks:
10

Angle d-value d-value Peak width Peak int Back. int Rel. int Signif.
[2] 1 [] 2 [] [2] [counts] [counts] [%]
6.645 13.2911
10.815 8.1739
19.650 4.5142
22.130 4.0136
24.010 3.7034
26.825 3.3208
28.065 3.1769
31.945 2.7993
34.565 2.5929

13.3238
8.1940
4.5253
4.0235
3.7125
3.3290
3.1847
2.8062
2.5993

0.240
0.480
0.640
0.480
0.560
0.240
0.480
0.360
0.320

38
30
166
79
21
67
112
1011
400

420
538
1253
1069
930
756
708
600
557

2.9
0.63
2.3
0.97
12.6
0.67
6.0
1.71
1.6
0.88
5.1
0.77
8.5
2.03
76.3 14.79
30.2
7.19

Universitas Sumatera Utara

36.340 2.4702 2.4763

0.440

1325

543

100.0

34.43

Lampiran 21.
Spektrum XRD Nanokomposit Karet Alam/Bentonit-CTAB

Universitas Sumatera Utara

File: THE-5.DI
29-May-2013 14:43
=============================================================
=================
Philips Analytical
PC-APD, Diffraction software
Sample identification: Sampel 5
Data measured at: 28-May-2013 15:28:00
Diffractometer type: PW1710 BASED
Tube anode: Cu
Generator tension [kV]: 40
Generator current [mA]: 30
Wavelength Alpha1 []: 1.54060
Wavelength Alpha2 []: 1.54439
Intensity ratio (alpha2/alpha1): 0.500
Divergence slit: 1
Receiving slit: 0.45
Monochromator used: NO
Start angle [2]: 5.000
End angle [2]: 44.980
Step size [2]: 0.020
Maximum intensity: 1576.090
Time per step [s]: 0.800
Type of scan: CONTINUOUS
Minimum peak tip width: 0.12
Maximum peak tip width: 1.00
Peak base width: 2.00
Minimum significance: 0.60
Number of peaks:
11

Universitas Sumatera Utara

Angle d-value d-value Peak width Peak int Back. int Rel. int Signif.
[2] 1 [] 2 [] [2] [counts] [counts] [%]
6.290 14.0404
9.470 9.3316
10.610 8.3314
17.675 5.0139
18.840 4.7064
21.945 4.0470
27.605 3.2287
28.555 3.1234
31.745 2.8165
34.435 2.6024
36.240 2.4768

14.0750 0.240
9.3546 0.160
8.3519 0.120
5.0262 0.640
4.7180 0.240
4.0570 0.240
3.2367 0.240
3.1311 0.320
2.8234 0.180
2.6088 0.120
2.4829 0.200

69
119
130
253
292
49
79
71
1260
449
1576

586
676
740
1296
1310
1109
745
718
600
552
543

4.4
7.5
8.2
16.0
18.6
3.1
5.0
4.5
80.0
28.5
100.0

1.62
1.02
0.66
0.69
0.66
0.82
1.04
0.96
13.34
2.01
19.81

Lampiran 22.
Spektrum XRD Nanokomposit Karet Alam/Bentonit PEG

Universitas Sumatera Utara

File: THE-4.DI
29-May-2013 14:43
=============================================================
=================

Universitas Sumatera Utara

Philips Analytical

PC-APD, Diffraction software

Sample identification: Sampel 4

Data measured at: 28-May-2013 15:57:00
Diffractometer type: PW1710 BASED
Tube anode: Cu
Generator tension [kV]: 40
Generator current [mA]: 30
Wavelength Alpha1 []: 1.54060
Wavelength Alpha2 []: 1.54439
Intensity ratio (alpha2/alpha1): 0.500
Divergence slit: 1
Receiving slit: 0.45
Monochromator used: NO
Start angle [2]: 5.000
End angle [2]: 44.980
Step size [2]: 0.020
Maximum intensity: 1239.040
Time per step [s]: 0.800
Type of scan: CONTINUOUS
Minimum peak tip width: 0.12
Maximum peak tip width: 1.00
Peak base width: 2.00
Minimum significance: 0.60
Number of peaks:
10

Angle d-value d-value Peak width Peak int Back. int Rel. int Signif.
[2] 1 [] 2 [] [2] [counts] [counts] [%]
10.300
19.150
21.865
22.965
26.635
27.575
31.620
34.305
36.085
42.785

8.5814
4.6309
4.0616
3.8695
3.3441
3.2322
2.8273
2.6119
2.4871
2.1118

8.6026
4.6423
4.0716
3.8790
3.3523
3.2401
2.8343
2.6184
2.4932
2.1170

0.320
0.800
0.480
0.200
0.160
0.240
0.140
0.280
0.120
0.120

18
125
44
207
86
130
1043
335
1239
66

475
918
762
702
520
488
392
361
353
313

1.4
10.1
3.5
16.7
7.0
10.5
84.2
27.0
100.0
5.3

0.73
1.36
1.23
2.08
0.69
1.65
4.24
8.03
3.24
1.16

Universitas Sumatera Utara

Lampiran 23.
Spektrum XRD Nanokomposit Karet Alam/Bentonit-SDS

Universitas Sumatera Utara

File: THE-8.DI
29-May-2013 14:44
=============================================================
=================
Philips Analytical
PC-APD, Diffraction software
Sample identification: Sampel 8
Data measured at: 28-May-2013 14:49:00
Diffractometer type: PW1710 BASED
Tube anode: Cu
Generator tension [kV]: 40
Generator current [mA]: 30
Wavelength Alpha1 []: 1.54060
Wavelength Alpha2 []: 1.54439
Intensity ratio (alpha2/alpha1): 0.500
Divergence slit: 1
Receiving slit: 0.45
Monochromator used: NO
Start angle [2]: 5.000
End angle [2]: 44.980
Step size [2]: 0.020
Maximum intensity: 1849.000
Time per step [s]: 0.800
Type of scan: CONTINUOUS
Minimum peak tip width: 0.12
Maximum peak tip width: 1.00
Peak base width: 2.00
Minimum significance: 0.60
Number of peaks:
16
Angle d-value d-value Peak width Peak int Back. int Rel. int Signif.
[2] 1 [] 2 [] [2] [counts] [counts] [%]

Universitas Sumatera Utara

10.540
11.465
16.685
17.780
21.885
23.025
25.815
26.495
27.705
27.975
28.560
31.760
34.375
36.250
37.800
42.435

8.3866
7.7119
5.3091
4.9845
4.0580
3.8596
3.4484
3.3614
3.2173
3.1869
3.1229
2.8152
2.6068
2.4761
2.3781
2.1284

8.4072
7.7309
5.3222
4.9968
4.0680
3.8691
3.4569
3.3697
3.2252
3.1947
3.1306
2.8221
2.6132
2.4822
2.3839
2.1337

0.240
0.200
0.800
0.640
0.160
0.160
0.120
0.480
0.160
0.120
0.240
0.200
0.240
0.160
0.480
0.800

45
114
119
196
243
1436
79
77
225
154
72
1537
515
1849
24
27

655
708
1176
1267
1109
992
795
767
724
713
692
590
552
538
529
493

2.4
6.2
6.4
10.6
13.2
77.7
4.3
4.2
12.2
8.3
3.9
83.1
27.9
100.0
1.3
1.5

0.73
2.09
0.64
0.91
1.77
14.33
0.92
2.30
1.19
0.68
0.68
21.62
8.46
13.05
1.16
0.93

Universitas Sumatera Utara