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This work was carried out in collaboration between all authors. Author MKA designed the study, wrote
the protocol and wrote the first draft of the manuscript. Author CCI plotted the graphs and author CEO
read proof the work and made useful corrections. All authors read and approved the final manuscript.
Article Information
DOI: 10.9734/JSRR/2016/20385
Editor(s):
(1) Mohamed Abd El-Moneim Ramadan, Pretreatment & Finishing of Cellulosic Fibres Department, Textile Research Division,
Egypt.
Reviewers:
(1) Randa M.Osman, National Research Centre, Cairo, Egypt.
(2) Danupon Tonnayopas, Prince of Songkla University, Thailand.
(3) Diene Ndiaye, University of Gaston Berger of Saint Louis, Senegal.
Complete Peer review History: http://sciencedomain.org/review-history/11904
th
ABSTRACT
This paper investigated the performance of coconut fibre particles as a filler material and highdensity polyethylene as matrix in polymer matrix composites (PMC). Three different particle sizes
of the filler material were used in formulating the composite samples and the concentration of the
filler material varied up to 40% by volume. The composite samples were prepared by injection
moulding and kept at room temperature for 48 hours prior to testing in order to promote relaxation
of stresses. The test specimens were prepared and tested in accordance with ASTM standards
D638, D790, D256, and D785 for tensile strength, elastic modulus, flexural strength, impact
strength and Rockwell hardness respectively. At optimum condition of volume fractions and particle
sizes of coconut fibre-filler, the coconut fibre reinforced HDPE (CFRP) has 28.6 MPa, 800 MPa,
_____________________________________________________________________________________________________
*Corresponding author: Email: achike4christ07@yahoo.com;
22.3 MPa, 55.0 J/m and 54.0 HR as optimum value for tensile strength, elastic modulus, flexural
strength, impact strength and hardness. It can be concluded from the results obtained that the
Coconut fibre reinforced HDPE showed improved performance for applications of HDPE.
Keywords: Reinforcement combinations; coconut fibre; volume fraction; particle size; archimedes
principle; optimum performance.
of natural fibres for their use in composite
materials such as acetylation, alkali and
isocyanates treatments. These Treatments make
the fibres more hydrophobic. It is important to
indicate that the good cohesion between fibres
and matrix is governed by many parameters
such as the surface area, the roughness and the
surface tensile of fibres.
1. INTRODUCTION
Most of the pressing scientific problems that are
currently faced today are due to the limitations of
the materials that are currently available [1].
Mulinari [2] defined composite materials as
materials made from two or more constituent
materials with significantly different physical or
chemical properties, that when combined,
produce a material with characteristics different
from the individual components. The individual
components remain separate and distinct within
the finished structure. The fact that composites in
general can be custom tailored to suit individual
requirements, have desirable properties in
corrosive environment, provide higher strength to
weight ratio and have lower life-cycle costs has
aided in their evolution [3]. Binshan, Alrik and
Bank [4] observed that these qualities in addition
to the ability to monitor the performance of the
material in the field via embedded sensors give
composites an edge over conventional materials.
The ability of composites to withstand tensile,
compressive and impact loads without failure is a
measure of their reliability [5].
2. METHODOLOGY
The methodology of this research employs
experimental and analytical methods to
investigate tensile strength, elastic modulus,
flexural strength, impact strength and hardness
value of coconut fibre particles reinforced highdensity polyethylene composite at different
volume fractions and particle sizes.
The researchers considered fibre surface
treatment, volume fraction of fibres, and particle
size of fibres as factors controlling the behavior
or characteristics of HDPE matrix filled fillers.
The ASTM specified standard particle sizes are
presented in Table 1. Archimedes principle was
employed to determine the density of coconut
fibre from where the composite samples are
designed following the method of Okafor et al.
[10] and ASTM Standards for mechanical
properties tests. Table 1 shows three grades of
fibre particle sizes and their corresponding sieve
sizes according to ASTM Standard.
2.1 Coconut
Fibre
Treatment
Extraction
and
1
2
3
ASTM
number
325
270
200
Sieve size
(7)
Specification
of size
60x6x3 mm
60x6x3 mm
80x12.5x3 mm
120x10x4 mm
80x10x4 mm
(1)
By using volume fraction of fibres 5%, 10%, 15%,
20%, 30%, and 40% and applying ASTM
standard specifications from Table 2 in equations
2 to 7 above, yields Tables 3 to 6.
(1 )
(6)
= +
Where,
(5)
(4)
(2)
(3)
Mf (g)
0.0318
0.0636
0.0954
0.1272
0.1908
0.2544
Vf (cm3)
0.054
0.108
0.162
0.216
0.324
0.432
VR (cm3)
1.026
0.972
0.918
0.864
0.756
0.648
MR (cm3)
0.9952
0.9428
0.8905
0.8381
0.7333
0.6286
Mf (g)
0.0884
0.1767
0.2651
0.3534
0.5301
0.7068
Vf (cm )
0.1500
0.3000
0.4500
0.6000
0.9000
1.2000
VR (cm )
2.8500
2.7000
2.5500
2.4000
2.1000
1.8000
MR (g)
2.7645
2.6190
2.4735
2.3280
2.0370
1.7460
Mf(g)
0.1414
0.2827
0.4241
0.5654
0.8482
1.1309
Vf (cm3)
0.240
0.480
0.720
0.960
1.440
1.920
VR (cm3)
4.560
4.320
4.080
3.840
3.360
2.880
MR (g)
4.4232
4.1904
3.9576
3.7248
3.2592
2.7936
Vf (cm3)
0.1600
0.3200
0.4800
0.6400
0.9600
1.2800
Mf (g)
0.0942
0.1885
0.2827
0.3770
0.5654
0.7540
VR (cm3)
3.0400
2.8800
2.7200
2.5600
2.2400
1.9200
MR (g)
2.9488
2.7936
2.6384
2.4832
2.1728
1.8624
4. DISCUSSION
3. RESULTS
Table 7. Tensile strength of the 3 grades of untreated and treated coconut fibre filled HDPE
composite samples at specified fibre volume fractions
Vfr (%)
0
5
10
15
20
30
40
G1U
24.6
25.4
25.8
26.1
26.6
26.2
26.0
G2U
24.6
25.0
25.2
25.6
26.0
25.8
25.6
G2T
24.6
25.5
26.2
27.4
28.2
27.8
27.4
G3T
24.6
24.0
25.0
25.4
24.8
24.4
25.0
29
28
G1U
27
G2U
26
G3U
25
G1T
24
G2T
23
0
10
20
30
40
50
G3T
Vfr (%)
Fig. 1. A plot of tensile strength of the 3 grades of untreated and treated coconut fibre filled
HDPE composite against fibre volume fractions
Table 8. Elastic modulus of the 3 grades of untreated and treated coconut fibre filled HDPE
composite samples at specified fibre volume fractions
Vfr (%)
G1U
480
500
530
580
650
780
610
0
5
10
15
20
30
40
G2U
480
600
640
630
600
730
630
G2T
480
610
670
680
720
750
710
900
800
700
600
500
400
300
200
100
0
G3T
480
570
590
610
680
730
760
GIU
G2U
G3U
G1T
G2T
G3T
0
10
20
30
40
50
Vfr (%)
Fig. 2. A plot of elastic modulus of the 3 grades of untreated and treated coconut fibre against
fibre volume fraction
at volume fraction of 30%. This observation
supports earlier study made by Pukanszkyl [14]
that strength of the interaction between the filler
material and the matrix influences tensile
modulus of the composite. This is because
modulus is a phenomenon involving very small
strain values. Small stresses are produced by
Table 9. Flexural Strength of the 3 grades of untreated and treated coconut fibre filled HDPE
composite samples at specified fibre volume fractions
Vfr (%)
G1U
17.4
18.3
18.7
20.1
20.0
21.4
21.8
0
5
10
15
20
30
40
G2U
17.4
18.0
18.1
19.6
19.3
20.1
21.3
G2T
17.4
18.0
18.5
19.6
19.5
20.0
21.6
G3T
17.4
17.3
17.5
18.2
19.0
19.8
21.0
Flexural Strenght
(MPa)
25
20
G1U
15
G2U
10
G3U
G1T
G2T
0
10
20
30
40
50
G3T
Vfr (%)
Fig. 3. A graph of flexural strength of the 3 grades of untreated and treated coconut fibre
against fibre volume fraction
Table 10. Impact strength of the 3 grades of untreated and treated coconut fibre filled HDPE
composite Samples at specified fibre volume fractions
Vfr (%)
0
5
10
15
20
30
40
G1U
48.0
49.0
50.0
51.0
53.0
50.0
48.0
G2U
48.0
49.0
49.2
49.5
50.0
48.0
46.0
G2T
48.0
48.5
49.0
50.0
52.0
49.0
47.0
G3T
48.0
48.5
49.0
49.5
48.0
45.0
43.0
Impact Strength
(J/m)
60
50
G1U
40
G2U
30
G3U
20
GIT
10
G2T
0
0
10
20
30
40
50
G3T
Vfr (%)
Fig. 4. A plot of impact strength of the 3 grades of untreated and treated coconut fibre against
fibre volume fraction
Table 11. Hardness value (HR) of the 3 grades of untreated and treated coconut fibre filled
HDPE composite Samples at specified volume fractions
Vfr (%)
0
5
10
15
20
30
40
G1U
12.5
15.3
22.4
30.5
38.3
46.8
53.4
G3T
12.5
15.0
19.2
26.4
32.4
40.2
42.8
Hardness Values
(HR)
60
50
G1U
40
G2U
30
G3U
20
G1T
10
G2T
0
0
10
20
30
40
50
G3T
Vfr (%)
Fig. 5. A plot of hardness values (HR) of the 3 grades of untreated and treated coconut fibre
filled HDPE composite samples against fibre volume fraction
Also Fig. 5 from Table 10 depicts that impact
strength increases with fibre treatment and
volume fraction but decreases with particle size
of filler at maximum optimum volume fraction of
20% with a value of 55 J/m. At higher fibre
concentrations and larger particle size, impact
strength was found to reduce. Further reductions
26.0
730
19.3
50.0
47.8
25.6
700
19.0
46.0
43.6
28.6
800
20.6
55.0
54
Average
values
21.4
909
28.2
2.79
48.7
Authors have
interests exist.
declared
that
no
competing
REFERENCES
1.
2.
3.
5. CONCLUSION
4.
24.8
730
19.0
48.0
42.8
Range of
values
11.0-43.0
450- 1500
13.8-48.3
20.0-110.0
33.0-66.0
COMPETING INTERESTS
28.2
750
19.5
52.0
48.6
HDPE-Injection
molded (MatWeb)
5.
6.
7.
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_______________________________________________________________________________
2016 Ihueze et al.; This is an Open Access article distributed under the terms of the Creative Commons Attribution
License (http://creativecommons.org/licenses/by/4.0), which permits unrestricted use, distribution, and reproduction in any
medium, provided the original work is properly cited.
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