PROCEDURE: CENTRIFUGE TEST FOR OIL BS&W CUT

RISK RANKING: LOW

HAZARD ASSESSMENT:

HAZARD POTENTIAL EFFECTS CONTROL

1. Flammable vapors / 1. Vapors may ignite 1 . Monitor to be used to

LEL. causing flash fire. detect LEL. Fixed fire
and LEL detection
may be in place to
initiate ESD.
SABA/SCBA may
have to be used.
2. H2S. 2. Exposure above 2. Monitor to be used to
OEL may cause detect H2S. Fixed
serious personal H2S detection may
injury, at higher be in place to initiate
concentrations; ESD.
exposure will cause
breathing to stop.
3. Worker exposure. 3. Swallowing, skin 3. Proper PPE is to be
contact and eye worn as per MSDS
contact. for chemicals used to
perform BS&W cut
thus preventing
worker exposure.

SAFETY EQUIPMENT:

Safety Glasses with side shields, hard hat, steel toe boots, FR Clothing, rubber gloves and
personal gas monitor.

NOTE: This must be done on a regular basis. Inaccuracy and non-conformance have serious
repercussions. This procedure determines the Basic Sediment and Water in a sample and
sets the percentages of hydrocarbon liquids to water and other impurities. This procedure is
based on API Standards & conforms to ASTM D 96-88.

PROCEDURE:

1. Determine the schedule for testing wells and follow the established, including well
stabilization periods required.

2. Put sampler in operation. Adjust tension on the spring to get correct timing, representative
of the oil produced throughout the period.

PROCEDURE:CENTRIFUGE TEST FOR OIL BS&W CUT

1 DateofPreparation:September1,2004
DateofRevision:September1,2004
DateofLastReview:February15,2010
PROCEDURE: CENTRIFUGE TEST FOR OIL BS&W CUT

3. For conventional production:

Take liquid sample from test separator.

4. For heavy oil production:

Take liquid sample from wellhead. Heat sample in a bath to enable it to be put in a test
tube.
A minimum of I000ml sample is required.

5. Shake sample well to make an emulsion to be sure you are getting a sample that is
representative of all the fluid collected during test.

6. Fill two 100 ml centrifuge tubes with the sample taken to the 100% level on tubes
calibrated from 0% to 200% and to the 50% level on tubes calibrated from 0% to 100%.
Add a small amount of demulsifier (knock out drops) to assist separation and shake again.
If escaping gas has left the level below the 50% or 100% level, top it off again.

7. Take warm solvent, preferably Varsol, from the centrifuge tube heater and fill the
centrifuge tubes to 100% on tubes calibrated from 0% to 100% and to 200% on tubes
calibrated from 0% to 200%.

8. Put the tubes back into the heater and let the samples heat for a period of time. Do not let
tubes boil over. If there was a line heater in service before the test separator or if the
production is warm enough more heating of the sample may not be required. Ensure
applied heat does not exceed the vapor temperature of the oil and water.

9. Place sample tubes on opposite sides of the centrifuge to maintain balance. Spin the
centrifuge for 10 minutes (tests at each field will be required to determine if 10 minutes is
sufficient to drop out all BS&W.

10.Obtain readings of combined basic sediment and water directly in percentages from the
tube to the nearest 0.05 ml (from 0.1 to the 1mI graduation) and to the nearest 0.1mI
(above the 1mI graduation).

11. Read the BS&W measurement directly from the 0% to 200% calibrated tubes. Double the
readings (to account for the solvent) to determine the BS&W content of the oil from the 0%
to 100% calibrated tubes (i.e. reading of .25ml is to be recorded as .5ml). Oil must be
below 0.5% BS&W to meet pipeline specifications. If no solvent was used, read the % of
BS&W directly from the 0% to 100% tubes.

PROCEDURE:CENTRIFUGE TEST FOR OIL BS&W CUT

2 DateofPreparation:September1,2004
DateofRevision:September1,2004
DateofLastReview:February15,2010
PROCEDURE: CENTRIFUGE TEST FOR OIL BS&W CUT

I2.Average the results from the two different tubes. Record the percentage of water and
sediment, the solvent used, the type and amount of demulsifier if used and the bath
temperature.

13.Calculate the total volume of oil produced in one day by multiplying the total fluid produced
reading (on the Floco) by the percentage of BS&W contained in the centrifuge.

14. If you have any reason to doubt the results take another test, if it comes back in the same
range and is high or low look for reasons for the change and contact your foreman.

PROCEDURE:CENTRIFUGE TEST FOR OIL BS&W CUT

3 DateofPreparation:September1,2004
DateofRevision:September1,2004
DateofLastReview:February15,2010