B.tech. - Chemical Engg - R13 - Syllabus

JAWAHARLAL NEHRU TECHNOLOGICAL UNIVERSITY ANANTAPUR
(Established by Govt. of A.P., Act. No. 30 of 2008)

ANANTHAPURAMU 515 002 (A.P) INDIA
Course Structure & Syllabus for B.Tech. (Regular)

R13 Regulations
CHEMICAL ENGINEERING
B.Tech. I Year
Course
S.No Subject Th Tu / Drg /Lab Credits
code
1. 13A52101 Communicative English 2 - - - 3
2. 13A56101 Engineering Physics 2 - - - 3
3. 13A51101 Engineering Chemistry 2 - - - 3
4. 13A54101 Mathematics - I 3 1 - - 5
5. 13A12101 Programming in C & Data 3 1 - - 5
Structures
6. 13A01101 Engineering Mechanics 3 1 - - 5
7. 13A03101 Engineering Drawing * 1 - 5 - 5
8. 13A12102 Programming in C & Data - - - 3 4
Structures Lab
9. 13A99102 Engineering Physics & - - - 3 4
Engineering Chemistry Lab **
10. 13A99103 Engineering & IT Workshop # - - - 3 4
11. 13A52102 English Language Comm. Skills - - - 3 4
Lab
Total Credits 45
Th = Theory; Tu = Tutorial, Drg= Drawing & Lab = Laboratory:
* Engineering Drawing will have University External Exam.
** The students shall attend the Physics lab and Chemistry lab in alternate weeks. The end
exam shall be conducted separately and average of the two exams shall be recorded by the
University exam section.
# The students shall attend Engineering workshop and IT work shop as a single lab every week
and the end exam is conducted as a single lab. Sharing the Maximum marks and time for one
task each from Engineering workshop and IT workshop. The sum of the marks awarded shall
be recorded
1
B.Tech. II - I Semester
Course Code Theory Tu / Lab

S.No. Subject Credits
1. 13A54301 Mathematics-II 3 1 - 3
13A99302 Electrical & Electronics 1 -
2. 3 3
Engineering
13A08301 Chemical Engineering Fluid 1 -
3. 3 3
Mechanics
4. 13A01403 Environmental Science 3 1 - 3
13A08302 Physical & Analytical 1 -
5. 3 3
Chemistry
6. 13A08303 Chemical Process Calculations 3 1 - 3
13A08304 Chemical Engineering Fluid
7. - - 3 2
Mechanics Lab
13A08305 Physical & Analytical
8. - - 3 2
Chemistry Lab
Total Credits 22
B.Tech. II - II Semester
Course code Theory Tu / Lab

S.No Subject Credits
1. 13A54303 Probability & Statistics 3 1 - 3
2. 13A08401 Process Heat Transfer 3 1 - 3
13A08402 Materials Science for Chemical 1 - 3
3. 3
Engineers
4. 13A08403 Organic Chemistry 3 1 - 3
13A08404 Chemical Engineering 1 - 3
5. 3
Thermodynamics
6. 13A08405 Mechanical Unit Operations 3 1 - 3
7. 13A08406 Process Heat Transfer Lab - - 3 2
13A08407 Mechanical Unit Operations
8. - - 3 2
Lab
13A52301 Human Values & Professional
9. 2 - - -
Ethics (Audit)
Total Credits 22
2
B.Tech. III - I Semester
S.No Course code Subject Theory Tu / Lab Credits

1. 13A08501 Energy Engineering 3 1 - 3
13A08502 Instrumentation & Process
2. 3 1 - 3
Control
3. 13A08503 Phase and Chemical Equilibria 3 1 - 3
13A08504 Chemical Reaction
4. 3 1 - 3
Engineering-I
5. 13A08505 Mass Transfer Operations-I 3 1 - 3
13A52501 Managerial Economics &
6. 3 1 - 3
Financial Analysis
13A08506 Energy & Environmental
7. - - 3 2
Engineering Lab
13A08507 Process Dynamics & Control
8. - - 3 2
Lab
Total Credits 22
B.Tech. III - II Semester

1. 13A52601 Management Science 3 1 -- 3
2. 13A08601 Chemical Technology 3 1 -- 3
3. 13A08602 Mass Transfer Operations II 3 1 - 3
13A08603 Chemical Reaction
4. 3 1 - 3
Engineering-II
13A08604 Process Modeling and
5. 3 1 - 3
Simulation
13A08605 Chemical Plant Design and
6. 3 1 - 3
Economics
13A08606 Chemical Reaction Engineering
7. - - 3 2
Lab
8. 13A08607 Mass Transfer Operations Lab - - 3 2
13A52502 Advanced English Language - 3
9. - --
Comm. Skills Lab (Audit)
Total Credits 22
3
B.Tech. IV - I Semester
1. 13A08701 Transport Phenomena 3 1 - 3
13A08702 Chemical Process Equipment
2. 3 1 - 3
Design
13A08703 Optimization of Chemical
3. 3 1 - 3
Processes
13A08704 Separation Techniques for
4. 3 1 - 3
Bioprocessing
5. Elective I (Open Elective) 3 1 - 3
Elective - II
Petroleum and Petro-Chemical
13A08705 Technology
6. 13A08706 3 1 - 3
Fluidization Engineering
13A08707 Fertilizer Technology
13A08708 Computational Fluid Dynamics
13A08709 Process Equipment Design and
7. - 2
Drawing Lab - 3
8. 13A08710 Process Simulation Lab - - 3 2
Total Credits 22
B.Tech IV - II Semester
1. 13A08801 Biochemical Engineering 3 1 - 3
13A08802 Industrial Pollution Control
2. 3 1 - 3
Engineering
Elective III
13A08803 Technology of Pharmaceuticals
& Fine Chemicals
3. 13A08804 Interfacial Engineering 3 1 - 3
13A08805 Polymer Technology
13A08806 Design & Analysis of
Experiments
Elective IV
13A08807 Computer Aided Process
13A08808 Design
4. 3 1 - 3
13A08809 Food Processing Technology
13A08810 Entrepreneurship Development
Corrosion Engineering
13A08811 Seminar & Comprehensive
5. - - - 3
Viva-Voce
6. 13A08812 Project - - - 10
Total Credits 25
4
B.Tech. I Year Th Tu C
2 0 3
Common to All Branches
(13A52101) COMMUNICATIVE ENGLISH

Preamble:
English is an international language as well as a living and vibrant one. People have found
that knowledge of English is a passport for better career and for communication with the entire
world. As it is a language of opportunities in this global age, English is bound to expand its domain
of use everywhere. The syllabus has been designed to enhance communication skills of the students
of Engineering and Technology. The prescribed books serve the purpose of preparing them for
everyday communication and to face global competitions in future.
The first text prescribed for detailed study focuses on LSRW skills and vocabulary
development. The teachers should encourage the students to use the target language. The classes
should be interactive and student-centered. They should be encouraged to participate in the
classroom activities keenly.
The text for non-detailed study is meant for extensive reading/reading for pleasure by the
students. They may be encouraged to read some selected topics on their own, which could lead into
a classroom discussion. In addition to the exercises from the texts done in the class, the teacher can
bring variety by using authentic materials such as newspaper articles, advertisements, promotional
material etc.
Course Objective:
To enable the students to communicate in English for academic and social purpose.
To enable the students to acquire structure and written expressions required for their profession.
To develop the listening skills of the students.
To inculcate the habit of reading for pleasure.
To enhance the study skills of the students with emphasis on LSRW skills.
Learning Outcome:
The students will get the required training in LSRW skills through the prescribed texts and
develop communicative competence.
UNIT I
Chapter entitled Humour from Using English
Chapter entitled Biography - (Homi Jehangir Bhabha) from New Horizons
Listening - Techniques - Importance of phonetics
L- Meet & Greet and Leave taking, Introducing Oneself and Others (Formal and Informal situations)
R- Reading Strategies -Skimming and Scanning
W- Writing strategies- sentence structures
G-Parts of Speech Noun-number, pronoun-personal pronoun, verb- analysis
V-Affixes-prefix and suffix, root words, derivatives
UNIT II
Chapter entitled Inspiration from Using English
Chapter entitled Biography - (Jagadish Chandra Bose) from New Horizons
L- Listening to details
S- Apologizing, Interrupting, Requesting and Making polite conversations
R- Note making strategies
W- Paragraph-types- topic sentences, unity, coherence, length , linking devices
G-Auxiliary verbs and question tags
5
V- synonyms-antonyms, homonyms, homophones, homographs, words often confused
UNIT III
Chapter entitled Sustainable Development from Using English
Chapter entitled Short Story - (The Happy Prince) from New Horizons
L- Listening to themes and note taking
S- Giving instructions and Directions, making suggestions, Accepting ideas, fixing a time and
Advising
R- Reading for details -1
W- Resume and cover letter
G- Tenses Present tense, Past tense and Future tense
V-Word formation and One-Word Substitutes
UNIT IV
Chapter entitled Relationships from Using English
Chapter entitled Poem - (IF by Rudyard Kipling) from New Horizons
L- Listening to news
S- Narrating stories, Expressing ideas and opinions and telephone skills
R- Reading for specific details and Information
W- Technical Report writing-strategies, formats-types-technical report writing
G- Voice and SubjectVerb Agreement
V- Idioms and prepositional Phrases
UNIT V
Chapter entitled Science and Humanism from Using English
Chapter entitled Autobiography - (My Struggle for an Education by Booker T.Washington)
from New Horizons
L- Listening to speeches
S- Making Presentations and Group Discussions
R- Reading for Information
W- E-mail drafting
G- Conditional clauses and conjunctions
V- Collocations and Technical Vocabulary and using words appropriately
Text Books:
1. Using English published by Orient Black Swan.
2. New Horizons published by Pearson.
Reference Books:
1. Raymond Murphys English Grammar with CD, Murphy, Cambridge University Press,
2012.
2. English Conversation Practice Grant Taylor, Tata McGraw Hill, 2009.
3. Communication Skills, Sanjay Kumar & Pushpalatha Oxford University Press, 2012.
4. A Course in Communication Skills- Kiranmai Dutt & co. Foundation Books, 2012.
5. Living English Structures- William Standard Allen-Pearson, 2011.
6. Current English Grammar and Usage, S M Guptha, PHI, 2013.
7. Modern English Grammar-Krishna SWAMI,.McMillan, 2009.
8. Powerful Vocabulary Builder- Anjana Agarwal, New Age International Publishers, 2011.
6
2 0 3
(13A56101) ENGINEERING PHYSICS
Preamble:
There has been an exponential growth of knowledge in the recent past opening up new areas
and challenges in the understanding of basic laws of nature. This helped to the discovery of new
phenomena in macro, micro and nano scale device technologies. The laws of physics play a key role
in the development of science, engineering and technology. Sound knowledge of physical principles is
of paramount importance in understanding new discoveries, recent trends and latest developments in
the field of engineering.
To keep in pace with the recent scientific advancements in the areas of emerging
technologies, the syllabi of engineering physics has been thoroughly revised keeping in view of the
basic needs of all engineering branches by including the topics like optics, crystallography,
ultrasonics, quantum mechanics, free electron theory. Also new phenomenon, properties and device
applications of semiconducting, magnetic, superconducting and nano materials along with their
modern device applications have been introduced.
Course Objective:
To evoke interest on applications of superposition effects like interference and diffraction,
the mechanisms of emission of light, achieving amplification of electromagnetic radiation
through stimulated emission, study of propagation of light through transparent dielectric
waveguides along with engineering applications.
To enlighten the periodic arrangement of atoms in crystals, direction of Bragg planes,
crystal structure determination by X-rays and also to understand different types of defects in
crystals adnoun-destructive evaluation using ultrasonic techniques.
To get an insight into the microscopic meaning of conductivity , classical and quantum free
electron model, the effect of periodic potential on electron motion, evolution of band theory
to distinguish materials and to understand electron transport mechanism in solids.
To open new avenues of knowledge and understanding on semiconductor based electronic
devices, basic concepts and applications of semiconductor and magnetic materials have been
introduced which find potential in the emerging micro device applications.
To give an impetus on the subtle mechanism of superconductors in terms of conduction of
electron pairs using BCS theory, different properties exhibited by them and their fascinating
applications. Considering the significance of microminiaturization of electronic devices and
significance of low dimensional materials, the basic concepts of nanomaterials, their
synthesis, properties and applications in modern emerging technologies are elicited.
Learning Outcome:
The different realms of physics and their applications in both scientific and technological
systems are achieved through the study of physical optics, lasers and fibre optics.
The important properties of crystals like the presence of long-range order and periodicity,
structure determination using X-ray diffraction are focused along with defects in crystals and
ultrasonic non-destructive techniques.
The discrepancies between the classical estimates and laboratory observations of physical
properties exhibited by materials would be lifted through the understanding of quantum
picture of subatomic world.
The electronic and magnetic properties of materials were successfully explained by free
electron theory and focused on the basis for the band theory.
The properties and device applications of semiconducting and magnetic materials are
illustrated.
The importance of superconducting materials and nanomaterials along with their
engineering applications are well elucidated.
7
UNIT 1
PHYSICAL OPTICS, LASERS AND FIBRE OPTICS:
Physical Optics: Introduction - Interference in thin films by reflection Newtons Rings Fraunhofer
diffraction due to single slit, double slit and diffraction grating.
Lasers: Introduction - Characteristics of laser Spontaneous and stimulated emission of radiation
Einsteins coefficients - Population inversion Excitation mechanisms and optical resonator - Ruby
laser - He-Ne laser Applications of lasers.
Fibre optics: Introduction Construction and working principle of optical fiber Numerical aperture
and acceptance angle Types of optical fibers Attenuation and losses in fibers - Optical fiber
communication system Applications of optical fibers in communications, sensors and medicine.
UNIT II
CRYSTALLOGRAPHY AND ULTRASONICS:
Crystallography: Introduction Space lattice Unit cell Lattice parameters Bravias lattice
Crystal systems Packing fractions of SC, BCC and FCC - Structures of NaCl and Diamond
Directions and planes in crystals Miller indices Interplanar spacing in cubic crystals X-ray
diffraction - Braggs law Laue and Powder methods Defects in solids: point defects, line defects
(qualitative) - screw and edge dislocation, burgers vector.
Ultrasonics: Introduction Production of ultrasonics by piezoelectric method Properties and
detection Applications in non-destructive testing.
UNIT III
QUANTUM MECHANICS AND FREE ELECTRON THEORY:
Quantum Mechanics: Introduction to matter waves deBroglie hypothesis - Heisenbergs
uncertainty principle and its applications - Schrodingers time independent and time dependent wave
equation Significance of wave function - Particle in a one dimensional infinite potential well -
Eigen values and Eigen functions.
Free electron theory: Classical free electron theory - Sources of electrical resistance - Equation for
electrical conductivity - Quantum free electron theory Fermi-Dirac distribution Kronig-Penny
model(qualitative) Origin of bands in solids Classification of solids into conductors,
semiconductors and insulators.
UNIT IV
SEMICONDUCTORS AND MAGNETIC MATERIALS:
Semiconductor Physics: Introduction Intrinsic and extrinsic semiconductors Drift & diffusion
currents and Einsteins equation Hall effect - Direct and indirect band gap semiconductors
Working principle of p-n junction diode, LED, laser diode and photodiode.
Magnetic materials: Introduction and basic definitions Origin of magnetic moments Bohr
magneton Classification of magnetic materials into dia, para, ferro, antiferro and ferri magnetic
materials Hysteresis - Soft and hard magnetic materials and applications.
UNIT V
SUPERCONDUCTIVITY AND PHYSICS OF NANOMATERIALS:
Superconductivity: Introduction Meissner effect - Properties of superconductors Type I and type
II superconductors Flux quantization London penetration depth ac and dc Josephson effects
BCS theory(qualitative) High Tc superconductors - Applications of superconductors.
Physics of Nanomaterials: Introduction - Significance of nanoscale - Surface area and quantum
confinement Physical properties: optical, thermal, mechanical and magnetic properties Synthesis
of nanomaterials: ball mill, chemical vapour deposition, sol-gel, plasma arcing and thermal
evaporation Properties of Carbon nanotubes High strength applications Properties of graphene
Graphene based Field Effect Transistor - Applications of nanomaterials.
8
Text Books:
1. Engineering physics S. ManiNaidu, Pearson Education, I Edition, 2012.
2. Engineering Physics V. Rajendran, MacGraw Hill Publishers, I Edition,2008.
Reference Books:
1. Engineering Physics V. Rajendran, K.Thyagarajan Tata MacGraw Hill Publishers, III
Edition, 2012.
2. Engineering Physics RV.S.S.N. Ravi Kumar and N.V. Siva Krishna, Maruthi
Publications , 2013
3. Engineering Physics - Sanjay D. Jain, D. Sahasrambudhe and Girish University Press, I
Edition, 2009.
4. Engineering Physics D K Pandey, S. Chaturvedi, Cengage Learning, I Edition, 2012
5. Engineering Physics Hitendra K Mallik and AK Singh, McGraw Hill Education Pvt. Ltd,
New Delhi , I Edition, 2010
6. Engineering Physics M. Arumugam, Anuradha Publications II Edition, 1997.
7. Engineering physics M.N. Avadhanulu and P.G. KshirSagar, Chand and Co, Revised
Edition, 2013.
8. Solid State Physics A.J. Dekkar, McMillan Publishers, Latest edition, 2012.
9. Engineering Physics Gaur and Gupta Dhanapati, Rai Publishers , 7th Edition, 1992.
9. Text book of Nanoscience and Nanotechnology: B S Murthy, P.Shankar, Baldev Raj B B
Rath, James Murday, University Press, I Edition, 2012.
10. Carbon Nanotubes and Graphene Device Physics H.S. Philip Wong, Deji Akinwande,
Cambridge University Press, 2011.
9
2 0 3
(13A51101) ENGINEERING CHEMISTRY
Preamble:
Knowledge in chemistry serves as basic nutrient for the understanding and thereby design of
materials of importance in life. Thus the advancement in Engineering is depend on the outcome of
basic sciences. Many advances in engineering either produce a new chemical demand as in the case
of polymers or wait upon chemical developments for their applications as in the case of implants and
alloys. Currently the electronics and computer engineers are looking forward for suitable
biopolymers and nano materials for use in miniature super computers, the electrical materials
engineers are in search of proper conducting polymers, the mechanical engineers are on lookout for
micro fluids and the civil engineers are looking for materials that are environmental friendly,
economical but long lasting.
Course Objective:
The Engineering Chemistry course for undergraduate students is framed to strengthen the
fundamentals of chemistry and then build an interface of theoretical concepts with their
industrial/engineering applications.
The course main aim is to impart in-depth knowledge of the subject and highlight the role of
chemistry in the field of engineering.
The lucid explanation of the topics will help students understand the fundamental concepts
and apply them to design engineering materials and solve problems related to them. An
attempt has been made to logically correlate the topic with its application.
The extension of fundamentals of electrochemistry to energy storage devices such as
commercial batteries and fuel cells is one such example.
After the completion of the course, the student would understand about the concepts of
chemistry in respect of Electrochemical cells, fuel cells, mechanism of corrosion and factors
to influence, polymers with their applications, analytical methods, engineering materials and
water chemistry.
Learning Outcome:
The student is expected to:
Understand the electrochemical sources of energy
Understand industrially based polymers, various engineering materials.
Differentiate between hard and soft water. Understand the disadvantages of using hard water
domestically and industrially. Select and apply suitable treatments domestically and
industrially.
UNIT 1
ELECTROCHEMISTRY:
Review of electrochemical cells, Numerical calculations, Batteries: Rechargeable batteries (Lead acid,
Ni-Cd, Lithium Ion Batteries). Fuels cells: (Hydrogen-Oxygen and Methanol-Oxygen).
Electrochemical sensors: Potentiometric Sensors and voltammetric sensors. Examples: analysis of
Glucose and urea.
Corrosion: Electrochemical Theory of corrosion, Factors affecting the corrosion. Prevention: Anodic
and cathodic protection and electro and electroless plating.
UNIT II
POLYMERS:
Introduction to polymers, Polymerisation process, mechanism: cationic, anionic, free radical and
coordination covalent, Elastomers (rubbers), Natural Rubber, Compounding of Rubber,
Synthetic Rubber: Preparation, properties and engineering applications of Buna-S, buna-N,
Polyurethene, Polysulfide (Thiokol) rubbers. Plastomers: Thermosetting and Thermoplatics,
10
Preparation, properties and Engineering applications , PVC, Bakelite, nylons.
Conducting polymers: Mechanism, synthesis and applications of polyacetyline, polyaniline. Liquid
Crystals: Introduction, classification and applications.
Inorganic Polymers: Basic Introduction, Silicones, Polyphospazins (-(R)2-P=N-) applications.
UNIT III
FUEL TECHNOLOGY:
Classifications of Fuels Characteristics of Fuels- Calorific Value Units, Numerical Problems,
Solid FuelsCoal, Coke : Manufacture of Metallurgical Coke by Otto Hoffmanns by product oven
processes.
Liquid Fuels: Petroleum: Refining of Petroleum, Gasoline: Octane Number, Synthetic Petrol:
Bergius Processes, Fischer Trophs synthesis.
Power Alcohol: Manufacture, Advantages and Disadvantages of Power Alcohol
Gaseous Fuels: Origin, Production and uses of Natural gas, Producer gas, Water gas, Coal gas and
Biogas. Flue Gas analysis by Orsats apparatus, Solving of problems on Combustion.
UNIT IV
CHEMISTRY OF ENGINEERING MATERIALS:
Semiconducting and Super Conducting materials-Principles and some examples, Magnetic materials
Principles and some examples, Cement: Composition, Setting and Hardening (Hydration and
Hydrolysis), Refractories: Classification, properties and applications, Lubricants: Theory of
lubrication , properties of lubricants and applications, Rocket Propellants: Classification,
Characteristics of good propellant
UNIT V
WATER TREATMENT:
Impurities in water, Hardness of water and its Units, Disadvantages of hard water, Estimation of
hardness by EDTA method, Numerical problems on hardness, Estimation of dissolved oxygen,
Alkalinity, acidity and chlorides in water, Water treatment for domestic purpose (Chlorination,
Bleaching powder, ozonisation)
Industrial Use of water: For steam generation, troubles of Boilers: Scale & Sludge, Priming and
Foaming, Caustic Embrittlement and Boiler Corrosion.
Treatment of Boiler Feed water: Internal Treatment: Colloidal, Phosphate, Carbonate, Calgon and
sodium aluminate treatment.External Treatment: Ion-Exchange and Permutit processes.
Demineralisation of brackish water: Reverse Osmosis and Electrodialysis
Text Books:
1. Engineering Chemistry by KNJayaveera, GVSubba Reddy and C. Ramachandraiah, McGraw
Hill Higher Education, New Delhi, Fourth Edition, 2012.
2. A Text book of Engineering Chemistry by S.S Dhara, S.S.Umare, S. Chand Publications, New
Delhi, 12th Edition, 2010.
Reference Books:
1. A Text Book of Enigneering Chemistry, Jain and Jain, Dhanapath Rai Publishing
Company, New Delhi, 15th Edition, 2010.
2. Engineering Chemistry by K.B.Chandra Sekhar, UN.Das and Sujatha Mishra,
SCITECH, Publications India Pvt Limited, Chennai, 2nd Edition, 2012.
3. Concepts of Engineering Chemistry- Ashima Srivastava and N.N. Janhavi, Acme
Learning Pvt Ltd, First Edition, 2013.
4. Text Book of Engineering Chemistry C. Parameswara Murthy, C.V.Agarwal and
Andra Naidu, BS Publications, Hyderabad, 3rd Edition, 2008.
5. Text Book of Engineering Chemistry, Shashichawla, Dhanapath Rai Publications, New Delhi,
4th Edition, 2011.
6. Engineering Chemistry, K. Sesha Maheswaramma and Mrudula Chugh, Pearson
Education, First Edition, 2013.
11
3 1 5
(13A54101) MATHEMATICS I
Course Objective:
To train the students thoroughly in Mathematical concepts of ordinary differential equations
and their applications in electrical circuits, deflection of beams, whirling of shafts.
To prepare students for lifelong learning and successful careers using mathematical concepts
of differential, Integral and vector calculus, ordinary differential equations and Laplace
transforms.
To develop the skill pertinent to the practice of the mathematical concepts including the
student abilities to formulate the problems, to think creatively and to synthesize information.
Learning Outcome:
The students become familiar with the application of differential, integral and vector
calculus, ordinary differential equations and Laplace transforms to engineering problems.
The students attain the abilities to use mathematical knowledge to analyze and solve
problems in engineering applications.
UNIT I
Exact, linear and Bernoulli equations, Applications to Newtons law of cooling, law of natural growth
and decay, orthogonal trajectories.
Non-homogeneous linear differential equations of second and higher order with constant coefficients
with RHS term of the type eax, Sin ax, cos ax, polynomials in x, eax V(x), xV(x), method of variation
of parameters. Applications to oscillatory electrical circuits, Deflection of Beams, whirling of shafts.
UNIT II
Taylors and Maclaurins Series - Functions of several variables Jacobian Maxima and Minima of
functions of two variables, Lagranges method of undetermined Multipliers with three variables only.
Radius of curvature, center of curvature, Involutes evolutes, envelopes.
UNIT III
Curve tracing Cartesian, polar and parametric curves. Length of curves.
Multiple integral Double and triple integrals Change of Variables Change of order of
integration. Applications to areas and volumes, surface area of solid of revolution in Cartesian and
polar coordinates using double integral.
UNIT IV
Laplace transform of standard functions Inverse transform First shifting Theorem, Transforms of
derivatives and integrals Unit step function Second shifting theorem Diracs delta function
Convolution theorem Laplace transform of Periodic function.
Differentiation and integration of transform Application of Laplace transforms to ordinary
differential equations of first and second order.
UNIT V
Vector Calculus: Gradient Divergence Curl and their properties; Vector integration Line
integral - Potential function Area Surface and volume integrals. Vector integral theorems:
Greens theorem Stokes and Gausss Divergence Theorem (Without proof). Application of Greens
Stokes and Gausss Theorems.
12
Text Books:
1. Higher Engineering Mathematics, B.S.Grewal, Khanna publishers-42 Edition(2012)
2. Engineering Mathematics, Volume - I, E. Rukmangadachari & E. Keshava Reddy, Pearson
Publisher 1st Edition (2010)
Reference Books:
1. Engineering Mathematics Volume-I, by T.K.V. Iyengar, S.Chand publication-12th
Edition(2013)
2. Engineering Mathematics, Volume - I, by G.S.S.Raju, CENGAGE publisher.(2013)
3. Advanced Engineering Mathematics, by Erwin Kreyszig, Wiley India-10thEdition(2012)
4. Higher Engineering Mathematics, by B.V.Ramana, Mc Graw Hill publishers(2008)
5. Advanced Engineering Mathematics, by Alan Jeffrey, Elsevier-1st Edition(2001)
13
3 1 5
(13A12101) PROGRAMMING IN C & DATA STRUCTURES
Course Objective:
To make the student understand problem solving techniques
Students will be able to understand the syntax and semantics of C programming
language and other features of the language
Get acquaintance with data structures, searching and sorting techniques
Learning Outcome:
Student can effectively apply problem solving techniques in designing the solutions
for a wide-range of problems
Student can choose appropriate data structure and control structure depending on
the problem to be solved
Student can effectively use existing data structures and design new data structures
appropriate to the problem to be solved
Student can modularize the problem and also solution
Student can use appropriate searching and sorting technique to suit the application.
UNIT I
Introductory Concepts: Introduction to computers, What is a Computer, Block diagram of
Computer, Computer Characteristics, Hardware Vs Software, How to develop a program,
Software development life cycle, Structured programming, Modes of operation, Types of
programming languages, Introduction to C, Desirable program characteristics.
Introduction to Computer problem solving: Introduction, The problem solving aspect, Top
down design, Implementation of algorithms.
Introduction to C programming: The C character set, Writing first program of C, Identifiers
and key words, A more useful C program, Entering the program into the computer, Compiling
and executing the program, Data types, Constants, Variables and arrays, Declarations,
Expressions, Statements, Symbolic Constants.
Operators and Expressions: Arithmetic operators, Unary operators, Relational and Logical
operators, Assignment operators, Conditional operator, Library functions.
Fundamental algorithms: Exchanging the values of two variables, Factorial computation,
Sine function computation, Reversing the digits of an integer, Generating prime numbers.
UNIT II
Data Input and Output: Preliminaries, Single character input-getchar function, Single
character output-putchar function, Entering input data-the scanf function, More about the
scanf function, Writing output data-The printf function, More about the printf function, The
gets and puts functions, Interactive(conversational) programming.
Preparing and running a complete C program: Planning a C program, Writing a C
program, Error diagnostics, Debugging techniques.
Control statements: Preliminaries, Branching: if-else statement, Looping: The while
statement, More looping: The do-while statement, Still more looping: The for statement,
Nested control structures, The switch statement, Break statement, Continue statement, The
comma operator, The goto statement.
Functions: A brief overview, Defining a function, Accessing a function, Function prototypes,
Passing arguments to a function, Recursion
14
UNIT III
Program Structure: Storage classes, Automatic variables, External (global) variables, Static
variables, Multi file programs, More about library functions.
Arrays: Defining an array, Processing an array, Passing arrays to functions, Multi
dimensional arrays.
Array Techniques: Array order reversal, Removal of duplicates from an ordered array,
Finding the Kth smallest element.
Merging, Sorting and Searching: The two way merge, Sorting by selection, Sorting by
exchange, Sorting by insertion, Sorting by partitioning, Recursive Quick sort, Binary Search.
Strings: Defining a string, NULL character, Initialization of strings, Reading and Writing a
string, Processing the strings, Character arithmetic, Searching and Sorting of strings, Some
more Library functions for strings
UNIT IV
Pointers: Fundamentals, Pointer Declarations, Passing pointer to a function, Pointers and one
dimensional array, Dynamic memory allocation, Operations on pointers, Pointers and multi
dimensional arrays, Arrays of pointers, Passing functions to other functions, More about
pointer declarations.
Structures and Unions: Defining a structure, Processing a structure, User defined data type
(typedef), Structures and Pointers, Passing structures to functions, Unions.
File Handling: Why files, Opening and closing a data file, Reading and Writing a data file,
Processing a data file, Unformatted data files, Concept of binary files, Accessing the file
randomly (using fseek).
Additional Features: Register variables, Bitwise operations, Bit Fields, Enumerations,
Command line parameters, More about Library functions, Macros, The C Preprocessor
UNIT V
Introduction to Data Structures: Data abstraction
Stacks and Queues: Stacks, Stacks using dynamic arrays, Queues, Circular Queues using
dynamic arrays
Evaluations of expressions: Expressions, Evaluating postfix expressions, Infix to Postfix,
Multiple Stacks and Queues.
Linked Lists: Singly Linked lists and chains, Representing chains in C, Linked Stacks and
Queues.
Text Books:
1. Programming with C, Byron Gottfried, Third Edition, Schaums Outlines, Mc
Graw Hill.
2. Fundamentals of Data Structures in C, Horowitz, Sahni, Anderson-freed, Second
Edition, Universities Press.
3. How to Solve it by Computer, R.G. Dromey, Pearson. (Pascal implementations
may be considered without loss of generality or Instructors may replace them with C
language programs)
Reference Books:
1. Programming in C, Pradip Dey, Manas Ghosh, Oxford Higher Education
2. Programming in C and Data Structures, Hanly, Koffman, Kamthane, Ananda Rao,
Pearson.
3. Programming in C, Reema Thareja, Oxford Higher Education.
4. Computer Fundamentals and C Programming, First Edition, Dr.P.Chenna Reddy,
Available at: www.pothi.com.
5. Data Structure and Program Design in C, Second Edition, Kruse, Tondo, Leung,
Mogalla, Pearson.
6. Programming with C, R.S. Bichkar, University Press.
7. Computer Science A Structured Programming Approach Using C, Third Edition,
Fourouzan & Gilberg, Cengage Learning.
15
3 1 5
(13A01101) ENGINEERING MECHANICS

Course Objective:
This course will serve as a basic course by introducing the concepts of basic mechanics which will
help as a foundation to various courses.
UNIT I
Introduction of Engineering Mechanics Basic concepts - System of Forces Moment of Forces
and its Application Couples and Resultant of Force System Equilibrium of System of Forces -
Degrees of Freedom Free body diagrams Types of Supports Support reactions for beams with
different types of loading concentrated, uniformly distributed and uniformly varying loading.
UNIT II
Friction: Types of friction laws of Friction Limiting friction- Cone of limiting friction static and
Dynamic Frictions Motion of bodies Wedge, Screw jack and differential Screw jack.
UNIT III
Centroid and Center of Gravity: Centroids of simple figures Centroids of Composite figures
Centre of Gravity of bodies Area moment of Inertia - Parallel axis and perpendicular axis theorems -
Moments of Inertia of Composite Figures.
Mass Moment of Inertia: Moment of Inertia of Simple solids Moment of Inertia of composite
masses.( Simple problems only)
UNIT IV
Kinematics: Rectilinear and Curvilinear motion Velocity and Acceleration Motion of A Rigid
Body Types and their Analysis in Planar Motion.
Kinetics: Analysis as a particle and Analysis as a Rigid Body in Translation Central Forces of
motion Equations of Plane Motion Fixed Axis Rotation Rolling Bodies Work Energy Method
Equation for Translation Work Energy application to Particle Motion, Connection System Fixed
axis Rotation and Plane Motion.
UNIT V
Analysis of Perfect Frames: Types of frames cantilever frames and simply supported frames
Analysis of frames using method of joints, method of sections and tension coefficient method for
vertical loads, horizontal loads and inclined loads.
Mechanical Vibrations: Definitions, Concepts-Simple Harmonic motion-Free vibrations-Simple
Compound and Torsional pendulum- Numerical problems
Text Books:
1. Engineering Mechanics by Shames & Rao Pearson Education.
2. Engineering Mechanics by Dr.R.k.Bansal, Lakshmi Publications.
3. Engineering Mechanics B. Bhattacharyya, Oxford University Publications.
Reference Books:
1. Engineering Mechanics by Fedrinand L.Singer Harper Collings Publishers.
2. Engineering Mechanics by Seshigiri Rao, Universities Press, Hyderabad.
3. Engineering Mechanics by Rajsekharan, Vikas Publications.
16
4. Engineering Mechanics (Statics and Dynamics) by Hibller and Gupta; Pearson Education.
5. Engineering Mechanics by S.Timoshenko, D.H.Young and J.V.Rao, Tata McGraw-Hill
Company.
6. Engineering Mechanics by Chandramouli, PHI publications.
7. Engineering Mechanics Arthur P. Boresi and Richard J. Schmidt. Brooks/Cole Cengage
Learning.
17
B.Tech. I Year Th Drg C

1 5 5
(13A03101) ENGINEERING DRAWING
Course Objective:
By studying the engineering drawing, a student becomes aware of how industry communicates
technical information. Engineering drawing teaches the principles of accuracy and clarity in
presenting the information necessary about objects.
This course develops the engineering imagination i.e., so essential to a successful design, By
learning techniques of engineering drawing changes the way one things about technical
images.
It is ideal to master the fundamentals of engineering drawing first and to later use these
fundamentals for a particular application, such as computer aided drafting. Engineering
Drawing is the language of engineers, by studying this course engineering and technology
students will eventually be able to prepare drawings of various objects being used in
technology.
UNIT I
Introduction to Engineering Drawing: Principles of Engineering Graphics and their Significance-
Conventions in Drawing-Lettering BIS Conventions. Curves used in Engineering Practice.
a) Conic Sections including the Rectangular Hyperbola- General method only,
b) Cycloid, Epicycloids and Hypocycloid
c) Involutes
d) Helices
UNIT II
Projection of Lines: Inclined to one or both planes, Problems on projections, Finding True lengths &
traces only.
Projections of Planes: Projections of regular plane surfaces/figures, Projection of lines and planes
using auxiliary planes.
UNIT III
Projections of Solids: Projections of Regular Solids inclined to one or both planes-Auxiliary Views.
Sections and Developments of Solids: Section Planes and Sectional View of Right Regular Solids-
Prism, cylinder, Pyramid and Cone. True shapes of the sections.Development of Surfaces of Right
Regular Solids-Prism, Cylinder, Pyramid, Cone and their Sectional Parts.
UNIT IV
Isometric and Orthographic Projections: Principles of isometric projection- Isometric Scale-
Isometric Views- Conventions- Isometric Views of lines, Planes Figures, Simple and Compound
Solids- Isometric Projection of objects having non-isometric lines. Isometric projections of spherical
parts. Conversion of isometric Projections/Views of Orthographic Views-Conventions.
UNIT V
Interpenetration of Right Regular Solids: Projections of Curves of intersection of Cylinder Vs
Cylinder, Cylinder Vs Prism, Cylinder Vs Cone, Square Prism Vs Square Prism.
Perspective Projections: Perspective Vice of Plane Figures and simple Solids, Vanishing point
method ( General Methods only).
Text Books:
1. Engineering Drawing, N.D. Bhat, Charotar Publishers
2. Engineering Drawing, K.L. Narayana& P. Kannaih, Scitech Publishers, Chennai
18
Reference Books:
1. Engineering Drawing, Johle, Tata McGraw-Hill Publishers
2. Engineering Drawing, Shah and Rana,2/e, Pearson Education
3. Engineering Drawing and Graphics, Venugopal/New age Publishers
4. Engineering Graphics, K.C. John, PHI,2013
5. Engineering Drawing and Graphics, Venugopal / New age Publishers
6. Engineering Drawing, B.V.R. Guptha, J.K. Publishers
Suggestions:
1. Student is expected to buy a book mentioned under Text books for better understanding.
2. Students can find the applications of various conics in engineering and application of involute
on gear teeth. The introduction for drawing can be had on line from:
Introduction to engineering drawing with tools youtube
Http-sewor. Carleton.ca /- g kardos/88403/drawing/drawings.html
Conic sections-online. red woods.edu
3. This subject also paves the way for learing Auto Cad, CAD / CAM, CATIA and Pro E which
are advanced software packages needed for every mechanical engineer (To be taught &
examined in First angle projection). The skill acquired by the student in this subject is very
useful in conveying his ideas to the layman easily.
19
B.Tech. I Year L C
3 4
(13A12102) PROGRAMMING IN C & DATA STRUCTURES LAB
Course Objective:
To make the student learn C Programming language.
To make the student solve problems, implement them using C language.
To strengthen the ability to identify and apply the suitable data structure for the given real
world problem.
Learning Outcome:
Apply problem solving techniques to find solutions to problems.
Able to use C language features effectively and implement solutions using C language.
Be capable to identity the appropriate data structure for a given problem or application.
Improve logical skills.
LIST OF EXPERIMENTS/TASKS
1. Practice DOS and LINUX Commands necessary for design of C Programs.
2. Study of the Editors, Integrated development environments, and Compilers in chosen
platform.
3. Write, Edit, Debug, Compile and Execute Sample C programs to understand the
programming environment.
4. Practice programs: Finding the sum of three numbers, exchange of two numbers, maximum
of two numbers, to read and print variable values of all data types of C language, to find the
size of all data types, to understand the priority and associativity of operators using
expressions, to use different library functions of C language.
5. Write a program to find the roots of a quadratic equation.
6. Write a program to compute the factorial of a given number.
7. Write a program to check whether the number is prime or not.
8. Write a program to find the series of prime numbers in the given range.
9. Write a program to generate Fibonacci numbers in the given range.
10. Write a program to find the maximum of a set of numbers.
11. Write a program to reverse the digits of a number.
12. Write a program to find the sum of the digits of a number.
13. Write a program to find the sum of positive and negative numbers in a given set of
numbers.
14. Write a program to check for number palindrome.
15. Write a program to evaluate the sum of the following series up to n terms e
x 2 3 4
=1+x+x /2!+x /3!+x /4!+--------
16. Write a program to generate Pascal Triangle.
17. Write a program to read two matrices and print their sum and product in the matrix form.
18. Write a program to read matrix and perform the following operations.
i. Find the sum of Diagonal Elements of a matrix.
ii. Print Transpose of a matrix.
iii. Print sum of even and odd numbers in a given matrix.
19. Write a program to accept a line of characters and print the count of the number of Vowels,
Consonants, blank spaces, digits and special characters.
20. Write a program to insert a substring in to a given string and delete few characters from the
string. Dont use library functions related to strings.
20
21. Write a program to perform the operations addition, subtraction, multiplication of complex
numbers.
22. Write a program to split a file in to two files, say file1 and file2. Read lines into the file
from standard input. File1 should consist of odd numbered lines and file2 should consist of
even numbered lines.
23. Write a program to merge two files.
24. Write a program to implement numerical methods Lagranges interpolation, Trapezoidal
rule.
25. Write a program to read a set of strings and sort them in alphabetical order.
26. Write a program to sort the elements of an array using sorting by exchange.
27. Write a program to sort the elements of an array using Selection Sort.
28. Write a program to perform Linear Search on the elements of a given array.
29. Write a program to perform Binary Search on the elements of a given array.
30. Write a program to find the number of occurrences of each number in a given array of
numbers.
31. Write a program to read two strings and perform the following operations without using
built-in string Library functions and by using your own implementations of functions.
i. String length determination ii .Compare Two Strings
iii. Concatenate them, if they are not equal iv. String reversing
32. Write programs using recursion for Factorial of a number, GCD, LCM, Towers of Hanoi.
33. Write a program to convert infix expression to postfix expression and evaluate postfix
expression.
34. Write a program to exchange two numbers using pointers.
35. Write a program to implement stack, queue, circular queue using array and linked lists.
36. Write a program to perform the operations creation, insertion, deletion, and traversing a
singly linked list
37. Write a program to read student records into a file. Record consists of rollno, name and
marks of a student in six subjects and class. Class field is empty initially. Compute the
class of a student. The calculation of the class is as per JNTUA rules. Write the first class,
second class, third class and failed students lists separately to another file.
38. A file consists of information about employee salary with fields employeeid, name, Basic,
HRA, DA, IT, other-deductions, Gross and Net salary. Initially only employeeid, name,
and basic have valid values. HRA is taken as 10% of the basic, DA is taken as 80% of
basic, IT is 20% of the basic, other deductions is user specified. Compute the Gross and
Net salary of the employee and update the file.
39. Write a program to perform Base (decimal, octal, hexadecimal, etc) conversion.
40. Write a program to find the square root of a number without using built-in library function.
41. Write a program to convert from string to number.
42. Write a program to generate pseudo random generator.
43. Write a program to remove duplicates from ordered and unordered arrays.
44. Write a program to sort numbers using insertion sort.
45. Write a program to implement quick sort using non-recursive and recursive approaches.
Use randomized element as partitioning element.
46. Write a program to search a word in a given file and display all its positions.
47. Write a program to generate multiplication tables from 11 to 20.
48. Write a program to express a four digit number in words. For example 1546 should be
written as one thousand five hundred and forty six.
49. Write a program to generate a telephone bill. The contents of it and the rate calculation etc
should be as per BSNL rules. Student is expected to gather the required information
through the BSNL website.
50. Write a program for tic-tac-toe game.
51. Write a program to find the execution time of a program.
21
52. Design a file format to store a person's name, address, and other information. Write a
program to read this file and produce a set of mailing labels
Note: The above list consists of only sample programs. Instructors may choose other programs to
illustrate certain concepts, wherever is necessary. Programs should be there on all the concepts
studied in the Theory on C programming and Data structures. Instructors are advised to change
atleast 25% of the programs every year until the next syllabus revision.
References:
1. Programming with C, Byron Gottfried, Third Edition, Schaums Outlines, Mc Graw
Hill.
2. Fundamentals of Data Structures in C, Horowitz, Sahni, Anderson-freed, Second
Edition, Universities Press.
3. How to Solve it by Computer, R.G. Dromey, Pearson.
4. The C Programming Language, Brian W. Kernighan, Dennis M. Ritchie, Pearson.
5. Classic Data Structures, Samantha, PHI
6. Let us C, Yeswant Kanetkar, BPB publications
7. Pointers in C, Yeswant Kanetkar, BPB publications
22
B.Tech. I Year L C
3 4

(13A99102) ENGINEERING PHYSICS & ENGINEERING CHEMISTRY LAB
ENGINEERING PHYSICS LAB
LIST OF EXPERIMENTS
Any 10 of the following experiments has to be performed:

1. Determination of wavelengths of various colours of mercury spectrum using diffraction
grating in normal incidence method
2. Determination of dispersive power of the prism
3. Determination of thickness of thin object by wedge method
4. Determination of radius of curvature of lens by Newtons Rings
5. Laser : Diffraction due to single slit
6. Laser : Diffraction due to double slit
7. Laser: Determination of wavelength using diffraction grating
8. Determination of Numerical aperture of an optical fiber
9. Meldes experiment: Determination of the frequency of tuning fork
10. Sonometer: Verification of the three laws of stretched strings
11. Energy gap of a material using p-n junction diode
12. Electrical conductivity by four probe method
13. Determination of thermistor coefficients ( , )
14. Hall effect : Determination of mobility of charge carriers in semiconductor
15. B-H curve
16. Magnetic field along the axis of a current carrying coil Stewart and Gees method.
17. Determination of lattice constant using X-ray spectrum.
ENGINEERING CHEMISTRY LAB
Preamble:
The experiments are designed in a manner that the students can validate their own theory
understanding in chemistry by self involvement and practical execution. Thus the execution of these
experiments by the student will reinforce his/her understanding of the subject and also provide
opportunity to refine their understanding of conceptual aspects. As a result, the student gets an
opportunity to have feel good factor at the laboratory bench about the chemical principles that he/she
learned in the classroom.
Course Objective:
Will learn practical understanding of the redox reaction
Will able to understand the function of fuel cells, batteries and extend the knowledge to the
processes of corrosion and its prevention
Will learn the preparation and properties of synthetic polymers and other material that would
provide sufficient impetus to engineer these to suit diverse applications
Will also learn the hygiene aspects of water would be in a position to design methods to
produce potable water using modern technology
Learning Outcome:
Would be confident in handling energy storage systems and would be able combat
chemical corrosion
23
Would have acquired the practical skill to handle the analytical methods with confidence.
Would feel comfortable to think of design materials with the requisite properties
Would be in a position to technically address the water related problems.
LIST OF EXPERIMENTS
Any 10 of the following experiments has to be performed:
1. Determination of total hardness of water by EDTA method.
2. Determination of Copper by EDTA method.
3. Estimation of Dissolved Oxygen by Winklers method
4. Determination of Copper by Iodometry
5. Estimation of iron (II) using diphenylamine indicator (Dichrometry Internal indicator
method).
6. Determination of Alkalinity of Water
7. Determination of acidity of Water
8. Preparation of Phenol-Formaldehyde (Bakelite)
9. Determination of Viscosity of oils using Redwood Viscometer I
10. Determination of Viscosity of oils using Redwood Viscometer II
11. Conductometric titration of strong acid Vs strong base (Neutralization titration).
12. Conductometric titration of Barium Chloride vs Sodium Sulphate (Precipitation Titration)
13. Determination of Corrosion rate and inhibition efficiency of an inhibitor for mild steel in
hydrochloric acid medium.
14. Estimation of Chloride ion using potassium Chromite indicator (Mohrs method)
References:
1. Vogels Text book of Quantitative Chemical Analysis, J. Mendham et al, Pearson
Education, Sixth Edition, 2012.
2. Chemistry Practical Lab Manual by K.B.Chandra Sekhar, G.V. Subba Reddy and
K.N.Jayaveera, SM Publications, Hyderabad, 3rd Edition, 2012.
24
B.Tech. I Year L C
3 4
(13A99103) ENGINEERING & I.T. WORKSHOP
ENGINEERING WORKSHOP
Course Objective:
The budding Engineer may turn out to be a technologist, scientist, entrepreneur, practitioner,
consultant etc. There is a need to equip the engineer with the knowledge of common and newer
engineering materials as well as shop practices to fabricate, manufacture or work with materials.
Essentially he should know the labour involved, machinery or equipment necessary, time required to
fabricate and also should be able to estimate the cost of the product or job work. Hence engineering
work shop practice is included to introduce some common shop practices and on hand experience to
appreciate the use of skill, tools, equipment and general practices to all the engineering students.
1. TRADES FOR EXERCISES:

a. Carpentry shop Two joints (exercises) involving tenon and mortising, groove and tongue:
Making middle lap T joint, cross lap joint, mortise and tenon T joint, Bridle T joint from
out of 300 x 40 x 25 mm soft wood stock
b. Fitting shop Two joints (exercises) from: square joint, V joint, half round joint or dove tail
joint out of 100 x 50 x 5 mm M.S. stock
c. Sheet metal shop Two jobs (exercises) from: Tray, cylinder, hopper or funnel from out of
22 or 20 guage G.I. sheet
d. House-wiring Two jobs (exercises) from: wiring for ceiling rose and two lamps (bulbs)
with independent switch controls with or without looping, wiring for stair case lamp,
wiring for a water pump with single phase starter.
e. Foundry Preparation of two moulds (exercises): for a single pattern and a double pattern.
f. Welding Preparation of two welds (exercises): single V butt joint, lap joint, double V butt
joint or T fillet joint.
2. TRADES FOR DEMONSTRATION:

a. Plumbing
b. Machine Shop
c. Metal Cutting
Apart from the above the shop rooms should display charts, layouts, figures, circuits, hand tools,
hand machines, models of jobs, materials with names such as different woods, wood faults,
Plastics, steels, meters, gauges, equipment, CD or DVD displays, First aid, shop safety etc. (though
they may not be used for the exercises but they give valuable information to the student). In the
class work or in the examination knowledge of all shop practices may be stressed upon rather than
skill acquired in making the job.
References:
1. Engineering Work shop practice for JNTU, V. Ramesh Babu, VRB Publishers Pvt. Ltd.,
2009
2. Work shop Manual / P.Kannaiah/ K.L.Narayana/ SciTech Publishers.
3. Engineering Practices Lab Manual, Jeyapoovan, SaravanaPandian, 4/e Vikas
4. Dictionary of Mechanical Engineering, GHF Nayler, Jaico Publishing House.
25
I.T. WORKSHOP
Course Objective:
To provide Technical training to the students on Productivity tools like Word processors,
Spreadsheets, Presentations
To make the students know about the internal parts of a computer, assembling a
computer from the parts, preparing a computer for use by installing the operating system
To learn about Networking of computers and use Internet facility for Browsing and
Searching.
Learning Outcome:
Disassemble and Assemble a Personal Computer and prepare the computer ready to
use.
Prepare the Documents using Word processors
Prepare Slide presentations using the presentation tool
Interconnect two or more computers for information sharing
Access the Internet and Browse it to obtain the required information
Install single or dual operating systems on computer
Preparing your Computer ( 5 weeks)

Task 1: Learn about Computer: Identify the internal parts of a computer, and its peripherals.
Represent the same in the form of diagrams including Block diagram of a computer. Write
specifications for each part of a computer including peripherals and specification of Desktop
computer. Submit it in the form of a report.
Task 2: Assembling a Computer: Disassemble and assemble the PC back to working condition.
Students should be able to trouble shoot the computer and identify working and non-working
parts. Student should identify the problem correctly by various methods available (eg: beeps).
Students should record the process of assembling and trouble shooting a computer.
Task 3: Install Operating system: Student should install Linux on the computer. Student may
install another operating system (including proprietary software) and make the system dual boot
or multi boot. Students should record the entire installation process.
Task 4: Operating system features: Students should record the various features that are
supported by the operating system(s) installed. They have to submit a report on it. Students
should be able to access CD/DVD drives, write CD/DVDs, access pen drives, print files, etc.
Students should install new application software and record the installation process.
Networking and Internet (4 weeks)

Task 5: Networking: Students should connect two computers directly using a cable or wireless
connectivity and share information. Students should connect two or more computers using
switch/hub and share information. Crimpling activity, logical configuration etc should be done
by the student. The entire process has to be documented.
Task 6: Browsing Internet: Student should access the Internet for Browsing. Students should
search the Internet for required information. Students should be able to create e-mail account
and send email. They should get acquaintance with applications like Facebook, skype etc.
If Intranet mailing facility is available in the organization, then students should share the
information using it. If the operating system supports sending messages to multiple users
(LINUX supports it) in the same network, then it should be done by the student. Students are
expected to submit the information about different browsers available, their features, and search
process using different natural languages, and creating e-mail account.
Task 7: Antivirus: Students should download freely available Antivirus software, install it and
use it to check for threats to the computer being used. Students should submit information about
the features of the antivirus used, installation process, about virus definitions, virus engine etc.
Productivity tools (6 weeks)
Task 8: Word Processor: Students should be able to create documents using the word processor
26
tool. Some of the tasks that are to be performed are inserting and deleting the characters, words
and lines, Alignment of the lines, Inserting header and Footer, changing the font, changing the
color, including images and tables in the word file, making page setup, copy and paste block of
text, images, tables, linking the images which are present in other directory, formatting
paragraphs, spell checking, etc. Students should be able to prepare project cover pages, content
sheet and chapter pages at the end of the task using the features studied. Students should submit
a user manual of the word processor considered.
Task 9: Spreadsheet: Students should be able to create, open, save the application documents
and format them as per the requirement. Some of the tasks that may be practiced are Managing
the worksheet environment, creating cell data, inserting and deleting cell data, format cells,
adjust the cell size, applying formulas and functions, preparing charts, sorting cells. Students
should submit a user manual of the Spreadsheet application considered.
Task 10: Presentations: creating, opening, saving and running the presentations, Selecting the
style for slides, formatting the slides with different fonts, colors, creating charts and tables,
inserting and deleting text, graphics and animations, bulleting and numbering, hyperlinking,
running the slide show, setting the timing for slide show. Students should submit a user manual
of the Presentation tool considered.
Optional Tasks:
Task 11: Laboratory Equipment: Students may submit a report on specifications of various
equipment that may be used by them for the laboratories in their curriculum starting from I
B.Tech to IV. B.Tech. It can vary from department to department. Students can refer to their
syllabus books, consult staff members of the concerned department or refer websites. The
following is a sample list. Instructors may make modifications to the list to suit the department
concerned.
Desktop computer
Server computer
Switch (computer science related)
Microprocessor kit
Micro controller kit
Lathe machine
Generators
Construction material
Air conditioner
UPS and Inverter
RO system
Electrical Rectifier
CRO
Function Generator
Microwave benches
Task 12: Software: Students may submit a report on specifications of various software that may
be used by them for the laboratories in their curriculum starting from I B.Tech to IV. B.Tech.
The software may be proprietary software or Free and Open source software. It can vary from
department to department. Students can refer to their syllabus books, consult staff members of
the concerned department or refer websites. The following is a sample list. Instructors may make
modifications to the list to suit the department concerned.
Desktop operating system
Server operating system
Antivirus software
27
MATLAB
CAD/CAM software
AUTOCAD
References:
1. Introduction to Computers, Peter Norton, Mc Graw Hill
2. MOS study guide for word, Excel, Powerpoint & Outlook Exams, Joan Lambert, Joyce
Cox, PHI.
3. Introduction to Information Technology, ITL Education Solutions limited, Pearson
Education.
4. Networking your computers and devices, Rusen, PHI
5. Trouble shooting, Maintaining & Repairing PCs, Bigelows, TMH
28
B.Tech. I Year L C
3 4
(13A52102) ENGLISH LANGUAGE COMMUNICATION SKILLS (ELCS) LAB
The Language Lab focuses on the production and practice of sounds of language and familiarizes the
students with the use of English in everyday situations and contexts.
Course Objective:
To train students to use language effectively in everyday conversations.
To expose the students to a varied blend of self-instructional learner-friendly modes of
language learning through computer-aided multi-media instruction.
To enable them to learn better pronunciation through stress on word accent, intonation, and
rhythm.
To help the second language learners to acquire fluency in spoken English and neutralize
mother tongue influence
To train students to use language appropriately for interviews, group discussion and public
speaking
Learning Outcome:
Becoming active participants in the learning process and acquiring proficiency in spoken
English of the students
Speaking with clarity and confidence thereby enhancing employability skills of the students
PHONETICS
Importance of speaking phonetically correct English
Speech mechanism-Organs of speech
Uttering letters-Production of vowels sounds
Uttering letters -Production of consonant sounds
Uttering words-Stress on words and stress rules
Uttering sentences-Intonation-tone group
LISTENING
Listening as a skill
Listening activities
PRESENTATIONAL SKILLS
Preparation
Prepared speech
Impromptu speech
topic originative techniques
JAM (Just A Minute)
Describing people/object/place
Presentation-
Stage dynamics
Body language
SPEAKING SKILLS
Telephone skills
Role plays
Public Speaking
GROUP ACTIVITIES
Debates
Situational dialogues
29
MINIMUM REQUIREMENT FOR ELCS LAB:
The English Language Lab shall have two parts:
Computer Assisted Language Learning (CALL) Lab:
The Computer aided Language Lab for 60 students with 60 systems, one master console,
LAN facility and English language software for self- study by learners.
The Communication Skills Lab with movable chairs and audio-visual aids with a P.A.
system, Projector, a digital stereo-audio & video system and camcorder etc.
System Requirement (Hardware component):

Computer network with LAN with minimum 60 multimedia systems with the following
specifications:
o P IV Processor
o Speed 2.8 GHZ
o RAM 512 MB Minimum
o Hard Disk 80 GB
o Headphones of High quality
SUGGESTED SOFTWARE:
Clarity Pronunciation Power Part I (Sky Pronunciation)
Clarity Pronunciation Power part II
K-Van Advanced Communication Skills
TOEFL & GRE (KAPLAN, AARCO & BARRONS, USA, Cracking GRE by CLIFFS)
DELTAs key to the Next Generation TOEFL Test: Advanced Skill Practice.
Lingua TOEFL CBT Insider, by Dreamtech
English Pronunciation in Use (Elementary, Intermediate, Advanced) CUP
Cambridge Advanced Learners English Dictionary with CD.
Oxford Advanced Learners Compass, 8th Edition
Communication Skills, Sanjay Kumar & Pushp Lata. 2011. OUP
References:
1. Strengthen Your Steps, Maruthi Publicaions, 2012.
2. A Course in Phonetics and Spoken English, Dhamija Sethi, Prentice-Hall of India
Pvt.Ltd.
3. A Textbook of English Phonetics for Indian Students 2nd Ed T. Balasubramanian.
(Macmillian),2012.
4. Speaking English Effectively, 2nd Edition Krishna Mohan & NP Singh, 2011.
(Mcmillan).
5. Listening in the Language Classroom, John Field (Cambridge Language Teaching
Library),2011
6. A Hand Book for English Laboratories, E.Suresh Kumar, P.Sreehari, Foundation
Books,2011
7. English Pronunciation in Use. Intermediate & Advanced, Hancock, M. 2009. CUP.
8. Basics of Communication in English, Soundararaj, Francis. 2012.. New Delhi:
Macmillan
9. Spoken English (CIEFL) in 3 volumes with 6 cassettes, OUP.
10. English Pronouncing Dictionary, Daniel Jones, Current Edition with CD.Cambridge,
17th edition, 2011.
30
B.Tech. II - I Sem. Th Tu C
3 1 3
(13A54301) MATHEMATICS II
Course Objective:
This course aims at providing the student with the concepts of Matrices, Fourier series, Fourier
transforms and partial differential equations which find the applications in engineering.
Our emphasis will be more on the logical and problem solving development in the Numerical
methods and its applications.
Learning Outcome:
The student becomes familiar with the application of Mathematical techniques like Fourier
series and Fourier transforms.
The student gains the knowledge to tackle the engineering problems using the concepts of
Partial differential equations and Numerical methods.
UNIT I
Rank Echelon form, normal form Consistency of System of Linear equations. Linear
transformations
Complex Matrices:- Hermitian, Skew-Hermitian and Unitary matrices and their properties. Eigen
Values, Eigen vectors for both real and complex matrices. Cayley Hamilton Theorem and its
applications Diagonolization of matrix. Calculation of powers of matrix. Quadratic forms Reduction
of quadratic form to canonical form and their nature.
UNIT II
Solution of Algebraic and Transcendental Equations: Introduction The Method of False Position
Newton-Raphson Method.
Interpolation:-Introduction Newtons forward and backward interpolation formulae Lagranges
Interpolation formula.
Curve fitting: Fitting a straight line Second degree curve Exponentional curve-Power curve by
method of least squares.
UNIT III
Numerical Differentiation and Integration Trapezoidal rule Simpsons 1/3 Rule Simpsons 3/8
Rule.
Numerical solution of Ordinary Differential equations: Solution by Taylors series-Picards Method of
successive Approximations-Eulers Method-Runge-Kutta Method Predictor-Corrector Method
Milnes Method.
UNIT IV
Fourier Series: Determination of Fourier coefficients Fourier series Even and odd functions
Fourier series in an arbitrary interval Even and odd period, continuation Half-range Fourier sine and
cosine expansions.
Fourier integral theorem Fourier sine and cosine integrals. Fourier transforms Fourier sine and
cosine transforms Properties Inverse transforms Finite Fourier transforms.
UNIT V
Formation of partial differential equations by elimination of arbitrary constants and arbitrary functions
Method of separation of variables Solutions of one dimensional wave equation, heat equation and
two-dimensional Laplaces equation under initial and boundary conditions.
31
Text Books:
1. Higher Engineering Mathematics, B.S.Grewal, Khanna publishers.
2. Introductory Methods of Numerical Analysis, S.S. Sastry, PHI publisher.
Reference Books:
1. Engineering Mathematics, Volume - II, E. Rukmangadachari & E. Keshava Reddy, Pearson
Publisher.
2. Engineering Mathematics, Volume - II, by G.S.S.Raju, CENGAGE publisher.
3. Mathematical Methods by T.K.V. Iyengar, S. Chand publication.
4. Higher Engineering Mathematics, by B.V.Ramana, Mc Graw Hill publishers.
5. Advanced Engineering Mathematics, by Erwin Kreyszig, Wiley India.
32
3 1 3
(13A99302) ELECTRICAL AND ELECTRONICS ENGINEERING
PART A ELECTRICAL ENGINEERING
Course Objective:
In this course the different types of DC generators and motors, Transformers, 3 Phase AC
Machines which are widely used in industry are covered and their performance aspects will be
studied.
UNIT I DC MACHINES
D.C.GENERATOR: Principles of Operation Constructional Details-Expression for Generated Emf-
Types of Generators-Losses in D.C.Generator Characteristics of D.C.Generators-Applications of
D.C.Generators.
D.C. MOTOR: Principles of Operation Constructional Details-Back EMF-Types of Motors-Armature
Torque of a D.C. Motor - Characteristics of D.C.Motors -Applications of D.C.Motors-3 Point Starter-
Speed Control of Shunt Motors
UNIT II TRANSFORMERS
Principles of Operation- Constructional Details- Types of Transformers- Emf Equation of a Transformer
Voltage Transformation Ratio-Equivalent Circuit- Equivalent Resistance- Equivalent Reactance-
Losses in the Transformer-Copper Loss, Iron Loss-Transformer Tests-Open Circuit, Short Circuit Test-
Efficiency of a Transformer Regulation of Transformer
UNIT III 3 PHASE AC MACHINES

INDUCTION MACHINES:
Introduction to 3-Phase Induction Motor- Principle of Operation- Constructional Details-Slip,
Frequency of Rotor Current-Expression for Torque -Torque-Slip Characteristics- Applications of 3
Phase Induction Motors
ALTERNATORS:
Principle of Operation-Constructional Details-EMF Equation-Voltage Regulation by Synchronous
Impedance Method
Text Books:
1. Basic Electrical Engineering by D P KOTHARI & I J NAGRATH, Tata McGraw Hill, Second
Edition, 2007.
2. Electrical Circuit Theory and Technology by JOHN BIRD, Routledge publisher, 4Th Edition,
2011.
Reference Books:
1. Electrical & Electronic Technology by Edward Hughes, 10th Edition, Pearson, 2008.
33
PART B ELECTRONICS ENGINEERING
UNIT I
SEMICONDUCTOR DEVICES: Intrinsic semiconductors-Electron-Hole Pair Generation,
Conduction in Intrinsic Semiconductors, Extrinsic Semiconductors-N-Type and P-Type
Semiconductors, Comparison of N-Type and P-Type Semiconductors. The p-n Junction - Drift and
Diffusion Currents, The p-n Junction Diode-Forward Bias, Reverse Bias, Volt-Ampere Characteristics-
Diode Specifications, Applications of Diode, Diode as a Switch. Diode as a Rectifier-Half-wave
Rectifier, Full-Wave Rectifier, Full-Wave Bridge Rectifier, Rectifiers with Filters, Zener Diode- Volt-
Ampere Characteristics, Zener Diode as Voltage Regulator. Silicon Controlled Rectifier- Two
Transistor Analogy of an SCR, Characteristics, Applications of SCR, DIAC, TRIAC.
UNIT II
BJT and FETs: Bipolar Junction Transistor (BJT) Types of Transistors, Operation of NPN and PNP
Transistors, Input-Output Characteristics of BJT-CB, CE and CC Configurations, Relation between IC,
IB and IE. Transistor Biasing- Fixed Bias, Voltage Divider Bias, Transistor Applications- Transistor as
an Amplifier, Transistor as a Switch,. Junction Field Effect Transistor (JFET)- Theory and Operation of
JFET, Output Characteristics, Transfer Characteristics, Configurations of JFET-CD, CS and CG
Configurations, JFET Applications- JFET as an Amplifier, JFET as a Switch, Comparison of BJT and
JFET,MOSFET-The Enhancement and Depletion MOSFET, Static Characteristics of MOSFET,
Applications of MOSFET.
UNIT III
DIGITAL ELECTRONICS: Number Systems-Decimal System, Binary System, Octal System,
Hexadecimal System, Code Conversions, Binary Arithmetic- Binary Addition, Binary Subtraction,
Logic Gates and Truth Tables-NOT, OR, AND, EX-OR, EX-NOR, Universal Gates- NAND, NOR
Gates. Boolean algebra and De Morgans Theorems, Combinational Circuits-Adders and Subtractors.
Text Books:
1. Basic Electrical and Electronics Engineering, M.S.Sukhija, T.K.Nagsarkar, Oxford University
Press, 1st Edition, 2012.
2. Basic Electrical and Electronics Engineering, S.K Bhattacharya, Pearson Education, 2012.
34
3 1 3
(13A08301) CHEMICAL ENGINEERING FLUID MECHANICS
Course Objective:
The behavior of fluids is important to process Engineering and constitutes foundations for the
study of unit operations. An understanding of fluids is essential to students not only for
accurately treating problems on the moment of fluids through pipes, pumps, but for dealing with
all kinds of process equipment.
Learning Outcome:
To apply the concept of hydrostatic equilibrium and to have knowledge on fluid flow
phenomena and to determine engineering design quantities for laminar and turbulent flows.
UNIT I
Unit operations and unit processes, unit systems, basic concepts, nature of fluids, hydrostatic
equilibrium, applications of fluid statics. Dimensional analysis including Buckingham Theorem and
Rayleighs method.
Fluid flow phenomena-Laminar flow, Shear rate, Shear stress, Rheological properties of fluids,
Turbulence, Boundary layers.
UNIT II
Basic equation of fluid flow Mass balance in a flowing fluid; continuity equation, differential
momentum balance; equations of motion, Macroscopic momentum balances, Bernoulli equation, pump
work in Bernoulli equation.
Incompressible Flow in pipes and channels- shear stress and skin friction in pipes, laminar flow in pipes
and channels, turbulent flow in pipes and channels, friction from changes in velocity or direction.
UNIT III
Flow of compressible fluids- Definitions and basic equations, Processes of compressible flow,
Isentropic flow through nozzles, adiabatic frictional flow, and isothermal frictional flow.
UNIT IV
Flow past immersed bodies, Drag and Drag coefficient, friction in flow through beds of solids, Kozeny-
Carman, Blake-Plummer and Ergun equations, motion of particles through fluids.
Fluidization, Conditions for fluidization, Minimum fluidization velocity, Types of fluidization,
Expansion of fluidized beds, Applications of fluidization. Continuous fluidization; slurry and pneumatic
transport.
UNIT V
Transportation and Metering of fluids- Pipes, fittings and valves, Fluid moving machinery, pumps,
Fans, blowers, and compressors.
Measurement of flowing fluids- variable head meters- Orifice meter, Venturi meter, Pitot tube; Area
meters- Rota meter.
Text Books:
1. Unit Operations of Chemical Engineering by W.L.McCabe, J.C.Smith & Peter Harriot, McGraw-
Hill, 7th ed, 2007
2. Chemical Engineering Fluid Mechanics by Rom Darby CRC Press, 2nd Ed , 2001
Reference Books:
1. Transport processes and unit operations by Christie J. Geankoplis, PHI, 4th edition, 2003.
2. Unit operations of Chemical Engineering, Vol-1 Chattopadhya, Khanna publishers, 2nd
edition, 1996.
3. Principles of Unit Operations, Foust et al, 2nd ed., John Wiley, 1999
4. Chemical Engineering, Vol-I, Coulson and Richardson, Pergamon Press, 5th edition, 1995.
Codes/tables: Friction factor versus Reynolds number should be provided
Pre-requisite: Nil
35
B.Tech. II - I Sem. T Tu C
3 1 3
(13A01403) ENVIRONMENTAL SCIENCE
Course Objective:
To make the students to get awareness on environment, to understand the importance of
protecting natural resources, ecosystems for future generations and pollution causes due to the
day to day activities of human life to save earth from the inventions by the engineers.
UNIT I
MULTIDISCIPLINARY NATURE OF ENVIRONMENTAL STUDIES: Definition, Scope and
Importance Need for Public Awareness.
NATURAL RESOURCES : Renewable and non-renewable resources Natural resources and
associated problems Forest resources Use and over exploitation, deforestation, case studies
Timber extraction Mining, dams and other effects on forest and tribal people Water resources Use
and over utilization of surface and ground water Floods, drought, conflicts over water, dams benefits
and problems Mineral resources: Use and exploitation, environmental effects of extracting and using
mineral resources, case studies Food resources: World food problems, changes caused by agriculture
and overgrazing, effects of modern agriculture, fertilizer-pesticide problems, water logging, salinity,
case studies. Energy resources:
UNIT II
ECOSYSTEMS: Concept of an ecosystem. Structure and function of an ecosystem Producers,
consumers and decomposers Energy flow in the ecosystem Ecological sucession Food chains,
food webs and ecological pyramids Introduction, types, characteristic features, structure and function
of the following ecosystem:
a. Forest ecosystem.
b. Grassland ecosystem
c. Desert ecosystem
d. Aquatic ecosystems (ponds, streams, lakes, rivers, oceans, estuaries)
BIODIVERSITY AND ITS CONSERVATION: Introduction 0 Definition: genetic, species and
ecosystem diversity Bio-geographical classification of India Value of biodiversity: consumptive use,
Productive use, social, ethical, aesthetic and option values Biodiversity at global, National and local
levels India as a mega-diversity nation Hot-soports of biodiversity Threats to biodiversity: habitat
loss, poaching of wildlife, man-wildlife conflicts Endangered and endemic species of India
Conservation of biodiversity: In-situ and Ex-situ conservation of biodiversity.
UNIT III
ENVIRONMENTAL POLLUTION: Definition, Cause, effects and control measures of :
a. Air Pollution.
b. Water pollution
c. Soil pollution
d. Marine pollution
e. Noise pollution
f. Thermal pollution
g. Nuclear hazards
SOLID WASTE MANAGEMENT: Causes, effects and control measures of urban and industrial
wates Role of an individual in prevention of pollution Pollution case studies Disaster management:
floods, earthquake, cyclone and landslides.
36
UNIT IV
SOCIAL ISSUES AND THE ENVIRONMENT: From Unsustainable to Sustainable development
Urban problems related to energy Water conservation, rain water harvesting, watershed management
Resettlement and rehabilitation of people; its problems and concerns. Case studies Environmental
ethics: Issues and possible solutions Climate change, global warming, acid rain, ozone layer
depletion, nuclear accidents and holocaust. Case Studies Wasteland reclamation. Consumerism and
waste products. Environment Protection Act. Air (Prevention and Control of Pollution) Act.
Water (Prevention and control of Pollution) Act Wildlife Protection Act Forest Conservation Act
Issues involved in enforcement of environmental legislation Public awareness.
UNIT V
HUMAN POPULATION AND THE ENVIRONMENT: Population growth, variation among
nations. Population explosion Family Welfare Proggramme. Environment and human health
Human Rights Value Education HIV/AIDS Women and Child Welfare Role of information
Technology in Environment and human health Case studies.
FIELD WORK: Visit to a local area to document environmental assets River/forest
grassland/hill/mountain Visit to a local polluted site-Urban/Rural/Industrial/Agricultural Study of
common plants, insects, birds river, hill slopes, etc..
Text Books:
1. Text book of Environmental Studies for Undergraduate Courses by Erach Bharucha for
University Grants Commission, Universities Press, 2005.
2. Environmental Studies by Palanisamy, Pearson education, 2012.
3. Environmental Studies by R.Rajagopalan, Oxford University Press, 2nd edition, 2011.
Reference Books:
1. Textbook of Environmental Studies by Deeksha Dave and E.Sai Baba Reddy, Cengage
Pubilications, 2nd edition, 2012.
2. Text book of Environmental Science and Technology by M.Anji Reddy, BS Publication, 2009.
3. Comprehensive Environmental studies by J.P.Sharma, Laxmi publications, 2nd edition, 2006.
4. Environmental sciences and engineering J. Glynn Henry and Gary W. Heinke Printice hall
of India Private limited, 2nd edition, 1996.
5. Introduction to Environmental engineering and science by Gilbert M. Masters and Wendell P.
Ela - Printice hall of India Private limited, 3rd edition, 2007.
37
3 1 3
(13A08302) PHYSICAL & ANALYTICAL CHEMISTRY

Course Objective:
To acquire basic principles of simple instrumental methods for estimation of organic/inorganic
species.
To acquire basic knowledge of industrial separations
To acquired knowledge in the characterization of materials synthesized by chemical industry
To understand the Preparations, properties and reactions of materials
Learning Outcome:
The student may acquire enough knowledge on industrial processes and Products
UNIT I
Spectrophotometric Methods:
Introduction to Analysis: Qualitative & Quantitative Analysis; Conventional & Instrumental methods of
analysis. Molecular spectrophotometry-Beers law Block diagram of UV-Visible Spectrophotometer
quantitative analysis direct method for the determination metal ions: Chromium, manganese, iron, etc in
alloys. Simultaneous spectrophotometric determination of chromium, manganese. Infrared
spectrometry-Functional group analysis of organic compounds using infrared spectra. Quantitative
analysis of organic molecules. Flame photometry-principles & applications. (determination of sodium,
potassium and calcium.)
UNIT II
Chromatographic Methods:
Colum chromatography-general principles, terminology: retention time, rotation volume, separation
factor , resolution of peaks. Principles of gas chromatography, block diagram of gas chromatograph -
detectors (FID, ECD), stationary phases for column, mobile phases, chromatogram, qualitative analysis,
special plots, quantitative analysis, HPLC: Principles of High Performance Liquid Chromatography.
Block diagram of HPLC Systems, function of each component, stationary phases, eluting solvents,
pumps, detectors, quantitative applications of HPLC. Ion chromatography-seperation of anions and
cations. Suppressed & non-suppressed ion chromatography. Numerical calculations.
UNIT III
Thermal methods of Analysis:
Introduction to Thermal methods, Thermogravimetric Analysis (TGA)-principles, and applications
(determination of drying temperatures, kinetic methods, automatic thermo gravimetric Analysis) DTA:
Differential thermal analysis-Principles and applications (exothermic and endothermic peaks, heat of
reaction, catalysis, decompositions etc.,)
DSC: Differential scanning calorimettry, principles & applications (exothermic & endothermic peaks,
compound purity determination, percentage crystallinity, glass transition temperature).
UNIT IV
Kinetics & Colloids
Introduction to chemical kinetics-theories of reaction rates-Collision theories-Modified collision theory
Absolute reaction rate theory (Transition state theory)-reaction between ions,reactions-Hydrogen and
bromine, hydrogen and oxygen (Steady state treatment)-. Definition of colloids, classification of
colloids, solids in liquids (Sols) properties, kinetics, optical and electrical, stability of colloids,
protective action, Hardy-Schultze Law, Gold Number. Liquids in liquids (Emulsions) -Types of
Emulsions, preparation, Emulsifier. Liquids in solids (Gels) Classification, preparation & properties,
Inhibition, General, applications of colloids.
38
UNIT V
Surface Chemistry
Adsorption, characteristics of adsorption, physical & chemical adsorption, Langumuir adsorption
isotherm, B.E.T. equation, BET plot, surface area determination of solids. Numerical calculations of
surface area, Heterogenous catalysis, Mechanism of catalysis-Langmuir-Hinsel Wood mechanism of
surface catalyzed reactions, Eley-Rideal mechanism surface catalysed reactions. Applications of
catalysis in industry.
Text Books:
1. Quantitative analysis, R.A.Day & A.L. Underwood , 5th edition, Printice- Hall of India
Pvt. Ltd., 2000.
2. Vogels Text Book of Qualitative chemical analysis, J. Mendham, R.C.Denney,
J. Darnes, M.J.K. Thomas, Persar education 6th edition, 2002.
3. Elements of Physical Chemistry-Peter Atkins, Oxford Uni.Press, 3rd Edition, 2010.
Reference Books:
1. Atkins Physical Chemistry P. Atkins and J. De Paula, Oxford Univ.Press, 9th Edition,
2012
2 Instrumental lMethods of Chemical Analysis, Gurdeep R.Chatwal, Sham K.Ananad,
Himalayha publishing House,5th Edition, 2012.
3. Advanced physical chemistry Gurudeepraj, Goel Publishing House, 2000
4. Essentials of Physical Chemistry- Arun Bahl, B.S.Bahl and G.D.Rulasi, S.Chand & Co Ltd.
Publishers, New Delhi, 24th edition, 2000.
39
3 1 3
(13A08303) CHEMICAL PROCESS CALCULATIONS

Course Objective:
To develop the basic knowledge in material and energy balance calculations of industrial
problems.
Learning Outcome:
This course will enable students to evaluate the effeciency of a process in terms of yield, energy
and provide guidance to improve upon them.
UNIT I
Stoichiometric & Composition relations: Stoichiometric relation, basis of calculations, methods of
expressing compositions of mixtures and solutions, density and specific gravity, Baume and API gravity
scales.
Behavior of Ideal gases: Kinetic theory of gases, application of ideal gas law, gaseous mixtures, gases
in chemical reactions.
UNIT II
Vapor pressure: Liquefaction and liquid state, vaporization, boiling point, effect of temperature on
vapor pressure, Antoine equation, vapor pressure plots, estimation of critical properties, vapor pressure
of immiscible liquids and ideal solutions, Raoults law, Non volatile solutes.
Humidity and Saturation: Partial saturation, Humidity- Absolute Humidity, Vaporization process,
Molal humidity, Relative and percentage saturation, dew point, humid heat, wet bulb
and dry bulb temperatures, use of humidity charts, adiabatic vaporization.
UNIT III
Material balances: Tie substance, Yield, conversion, limiting reactant, excess reactant, processes
involving reactions, Material balances with the help of Stoichiometric equations, Material balances
involving drying, dissolution, & crystallization. Material balance calculations for processes involving
recycle, bypass and purge.
UNIT IV
Thermo physics: Energy, energy balances, heat capacity of gases, liquid and mixture solutions. Kopps
rule, latent heats, heat of fusion and heat of vaporization, Troutons rule, Kistyakowsky equation for non
polar liquids enthalpy and its evaluation.
Thermo chemistry: Calculation and applications of heat of reaction, combustion, formation and
neutralization, Kirchoffs equation, enthalpy concentration change, calculation of theoretical and actual
flame temperatures.
UNIT V
Combustion Calculations: Introduction, fuels, calorific value of fuels, coal, liquid fuels, gaseous fuels,
air requirement and flue gases, combustion calculations, incomplete combustion, material and energy
balances, thermal efficiency calculations.
Text Books:
1. Chemical process principles, Part -I, Material and Energy Balance, Hougen O A, Watson K.M. and
Ragatz R.A. 2nd Edition, John Wiley and Sons, New York, 1963.
Reference Books:
1. Basic principles and calculations in chemical engineering by D.H. Himmelblau, 7th Ed. PHI, 2013
2. Stoichiometry by B.I. Bhatt and S.M. Vora (3rd Ed.) Tata McGraw Hill publishing company, Ltd.
New Delhi ,1996.
Pre-requisite: ---Nil---
Codes/tables: Humidity chart should be provided in the examination hall.
40
B.Tech. II - I Sem. L C
3 2
(13A08304) CHEMICAL ENGINEERING FLUID MECHANICS LAB
Course Objective:
The lab provides knowledge on various flow patterns, flow measuring devices and pumps.
Learning Outcome:
Student will be able to understand the concept of fluid flow phenomena, different flow regimes,
flow measuring devices like venturi, orifice and rotameter.
1. Identification of laminar and turbulent flows

Major equipment - Reynolds apparatus
2. Measurement of point velocities
Major equipment - Pitot tube setup
3. Verification of Bernoullis equation
Major equipment Bernoullis Apparatus
4. Calibration of Rotameter
Major equipment Rotameter Assembly
5. Variation of Orifice coefficient with Reynolds Number
Major equipment - Orifice meter Assembly
6. Determination of Venturi coefficient
Major equipment Venturi meter Assembly
7. Friction losses in Fluid flow in pipes with and without bending
Major equipment - Pipe Assembly with provision for Pressure measurement
8. Pressure drop in a packed bed for different fluid velocities
Major equipment - Packed bed with Pressure drop measurement
9. Pressure drop and void fraction in a fluidized bed
Major equipment - Fluidized bed with Pressure drop measurement
10. Studying the coefficient of contraction for a given open orifice
Major equipment - Open Orifice Assembly
11. Studying the coefficient of discharge in a V-notch
Major equipment - V-notch Assembly
12. Studying the Characteristics of a centrifugal pump
Major equipment - Centrifugal Pump
41
B.Tech. II - I Sem. L C
3 2
(13A08305) PHYSICAL & ANALYTICAL CHEMISTRY LAB
Course Objective:
To confirm the formation and nature of the product in a chemical processes, the knowledge of
some physical, chemical and instrumental methods is essential for a chemical engineer.
I. PHYSICAL CHEMISTRY LAB:
1. Determination of specific rotation of substance by polarimeter.

2. Study of inversion of sucrose by Polarimetry.
3. Conductometric titration of strong acid v/s strong base.
4. Conductometric titration of Weak acid v/s strong base.
5. Potentiometric titration between potassium dichromate and ferrous iron.
II. ORGANIC CHEMISTRY LAB:
1. Criteria of purity of solid and liquid, determination of melting point & boiling point.
Detecting nitrogen, sulphur, and halogens in organic compounds.
2. Identification of an unknown substance from the following classes of organic compounds,
Alcohols, phenols, Aldehydes, ketenes, carbobhydrates and carboxylic acids.
III. PREPARATIONS: Aspririn, Paracetamol, Acetanilide and Azodye

Course Outcome:
Student will get the knowledge of methods to confirm the formation and the nature of the
product.
References:
1. Vogels Text Book of Qualitative Organic Analysis, Willey, John & Sons, Incorporated, 4th
edition, 2006.
2. Experiments in Physical Chemistry, 7th edition by David P Shoemaker, Joseph W Nibler, Tata Mc
Graw Publications, 2003.
42
B.Tech. II - II Sem. T Tu C
3 1 3
(13A54303) PROBABILITY AND STATISTICS
Course Objective:
To help the students in getting a thorough understanding of the fundamentals of probability and
usage of statistical techniques like testing of hypothesis, ANOVA, Statistical Quality Control
and Queuing theory.
Learning Outcome:
The student will be able to analyze the problems of engineering & industry using the techniques
of testing of hypothesis, ANOVA, Statistical Quality Control and Queuing theory and draw
appropriate inferences.
UNIT I
Conditional probability Bayes theorem. Random variables Discrete and continuous Distributions
Distribution functions. Binomial and poison distributions Normal distribution Related properties.
UNIT II
Test of Hypothesis: Population and Sample - Confidence interval of mean from Normal distribution -
Statistical hypothesis - Null and Alternative hypothesis - Level of significance - Test of significance -
Test based on normal distribution - Z test for means and proportions; Small samples - t- test for one
sample and two sample problem and paired t-test, F-test and Chi-square test (testing of goodness of fit
and independence).
UNIT III
Analysis of variance one way classification and two way classification (Latic square Design and RBD)
UNIT IV
Statistical Quality Control: Concept of quality of a manufactured product -Defects and Defectives -
Causes of variations - Random and assignable - The principle of Shewhart Control Chart-Charts for
attribute and variable quality characteristics- Constructions and operation of X- bar Chart, R-Chart, P-
Chart and C-Chart.
UNIT V
Queuing Theory: Pure Birth and Death process, M/M/1 & M/M/S & their related simple problems.
Text Books:
1. Probability & Statistics for engineers by Dr. J. Ravichandran WILEY-INDIA publishers.
2. Probability & Statistics by T.K.V. Iyengar, S.Chand publications.
Reference Books:
1. Probability & Statistics by E. Rukmangadachari & E. Keshava Reddy, Pearson
Publisher.
2. Statistical methods by S.P. Gupta, S.Chand publications.
3. Probability & Statistics for Science and Engineering by G.Shanker Rao, Universities
Press.
4. Probability and Statistics for Engineering and Sciences by Jay L.Devore, CENGAGE.
5. Probability and Statistics by R.A. Jhonson and Gupta C.B.
43
B.Tech. II - II Sem. Th Tu C
3 1 3
(13A08401) PROCESS HEAT TRANSFER

Course Objective:
To impart the students about knowledge on different modes of heat transfer and design of heat
transfer equipment, evaporators, etc.
Learning Outcome:
Student will be able to use the heat transfer principles in selection and design of heat
exchanger, evaporator, etc. for a chemical industry.
UNIT I
Introduction: Nature of heat flow, conduction, convection, natural and forced convection, radiation.
Heat transfer by conduction in Solids: Fouriers law, thermal conductivity, steady state conduction in
plane wall & composite walls, compound resistances in series, heat flow through a cylinder, conduction
in spheres.
Unsteady state heat conduction: Equation for one-dimensional conduction, Semi-infinite solid.
UNIT II
Principles of heat flow in fluids: Typical heat exchange equipment, countercurrent and parallel current
flows, energy balances, rate of heat transfer, overall heat transfer coefficient, electrical analogy, critical
radius of insulation, logarithmic mean temperature difference, variable overall coefficient, multi-pass
exchangers, individual heat transfer coefficients, resistance form of overall coefficient, fouling factors,
classification of individual heat transfer coefficients, magnitudes of heat transfer coefficients, effective
coefficients for unsteady-state heat transfer.
UNIT III
Heat Transfer to Fluids without Phase change: Regimes of heat transfer in fluids, thermal boundary
layer, heat transfer by forced convection in laminar flow, heat transfer by forced convection in turbulent
flow, the transfer of heat by turbulent eddies and analogy between transfer of momentum and heat, heat
transfer to liquid metals, heating and cooling of fluids in forced convection outside tubes.
Natural convection: Natural convection to air from vertical shapes and horizontal planes, effect of
natural convection in laminar-flow heat transfer.
UNIT IV
Heat transfer to fluids with phase change: Heat transfer from condensing vapors, heat transfer to
boiling liquids.
Radiation: Introduction, properties and definitions, black body radiation, real surfaces and the gray
body, absorption of radiation by opaque solids, radiation between surfaces, radiation shielding, radiation
to semi transparent materials, combined heat transfer by conduction, convection and radiation.
UNIT V
Heat exchange equipment: General design of heat exchange equipment, heat exchangers, condensers,
boilers and calendrias, extended surface equipment, heat transfer in agitated vessels, scraped surface
heat exchangers, heat transfer in packed beds, heat exchanger effectiveness (NTU method)
Evaporators: Evaporators, performance of tubular evaporators, capacity and economy,
multiple effect evaporators, methods of feeding, vapor recompression.
Text Books:
1. Unit Operations of Chemical Engineering,, W.L. McCabe, J.C. Smith and P.
Harriot, McGraw-Hill, New York, 2001
2. Heat transfer: Principles and Appplications by B.K. Datta, PHI, 2005
44
Reference Books:
1. Process Heat Transfer, D.Q. Kern, Tata McGraw-Hill, New Delhi, 1997.
2. Heat Transfer, 4th ed., J.P. Holman, McGraw-Hill, New York, 1976.
3. Chemical Engineering, Volume-I, J. Coulson and R.F. Richardson, Pergamon Press, 6th edition,
2000.
Codes/tables: Steam tables should be provided at the time of examination.
45
3 1 3
(13A08402) MATERIALS SCIENCE FOR CHEMICAL ENGINEERS
Course Objective:
This course will help students to learn about the relationship between structure and properties
of materials, application of various classes of materials including metals, ceramics, polymers.
Learning Outcome:
This course will enable the student to learn about proper selection of materials for designing
various equipment in a chemical industry.
UNIT I
Introduction: Engineering Materials Classification levels of structure.
Crystal Geometry and Structure Determination: Space lattice and Unit cell. Bravais lattices, crystal
systems with examples. Lattice coordinates, Miller indices, Bravais indices for directions and places:
crystalline and non crystalline solids; ionic, covalent and metallic solids; packing efficiency,
coordination number; structure determination by Braggs X-ray diffraction and powder methods.
UNIT II
Crystal Imperfection: Point defects, line defects-edge and screw dislocation, Bergers circuit and
Bergers vectors, dislocation reaction, dislocation motion, multiplication of dislocations during
deformation , role of dislocation on crystal properties; surface defects, dislocation density and stress
required to move dislocations.
UNIT III
Basic thermodynamic functions: phase diagrams and phase transformation: Primary and binary
systems-general types with examples; tie line& lever rule, non equilibrium cooling: phase diagrams of
Fe-Fe3-C, Pb-Sn, Cu-Ni systems.
Phase transformations in Fe-Fe3-C steels, Time-Temperature-Transformation (TTT) curves for eutectoid
steels and plain carbon steels; effect of alloying elements on properties of steels; types of steels, alloys
and other metals used in chemical industry.
UNIT IV
Elastic, an elastic and plastic deformations in solid materials; rubber like elasticity, visco elastic
behavior (models); shear strength of real and perfect crystals, work hardening mechanisms, cold
working, hot working; dynamic recovery, recrystallization, grain growth, grain size and yield stress,
Brief description of heat treatment in steels.
Magnetic materials: Terminology and classification, magnetic moments due to electron spin, ferro-
magnetism and related phenomena, domain structure, hysteresis loop, soft and hard magnetic materials.
UNIT V
Fracture in ductile and brittle materials, creep: mechanism of creep and methods to reduce creeping
in materials, creep rates and relations. Fatigue-mechanisms and methods to improve fatigue resistance in
materials. Composite materials: types; stress-strain relations in composite materials, applications.
Oxidation and Corrosion: Mechanisms of oxidation, oxidation resistant materials, principles and types
of corrosion, protection against corrosion.
Text Books:
1. Materials Science and Engineering, 5th ed. V. Raghavan, PHI Learning Pvt. Ltd., New Delhi, 2009.
Reference Books:
1. Elements of Materials Science & Engineering, L.H. Van Vlack,Prentice Hall, 6th edition, 1989.
2. Science of Engineering Materials, vols. 1&2, Manas Chanda, McMillan Company of India Ltd., 4th
edition, 2006.
Codes/tables: Nil
46
3 1 3
(13A08403) ORGANIC CHEMISTRY

Course Objective:
The Mechanism of organic chemical reaction is essential to synthesis new organic compounds
in drug and pharmaceutical industries. In order to study their kinetics of reactions to regulate
the process for optimization of production of drugs and pharmaceutical, the principles of
organic chemistry are essential.
For chemical engineer to carry out a processes industrially for the manufacture of drgus and
pharmaceuticals, Comprehension on basic reactions, reagents and their applications is needed.
He/She should know the electronic behavior of organic molecules, their special and geometrical
arrangement of functional groups.
He/she should have insight of reaction mechanisms for different types of reactions.
He/She must have knowledge to conduct the most common reactions like addition, substitution,
oxidation, reduction etc., on large scale.
Learning Outcome:
Student will get the knowledge of methods to confirm the formation and the nature of the
product
UNIT I
Polar effects Inductive effect, electromeric effect, resonance, hyper conjugation, steric hindrens, and
aromaticity examples.
UNIT II
Electrophilic reactions: a) Friedel-Craft reaction b) Riemer- Teimenn Reaction c) Backmann
rearrangement.
Nucleophillic reactions : a) Aldol condensation b) Perkin Reaction c) Benzoin condensation.
UNIT III
Stereo isomerism; Optical isomerism; Symmetry and chirality; Optical isomerism in lactic acid and
tartaric acid; Sequence rules; Enantiomers, diastereomers; Geometrical Isomerism; E-Z system of
nomenclature, conformational analysis of ethane and Cyclohexane.
UNIT IV
Some Reagents of Synthetic importance:
Preparation and applications of Aluminum Chloride, N-Bromosuccnamide (NBS), Diazomethane,
Dicyclohexylcarbodiimide(DCC), Potassiumtertiarybutoxide and Grignard reagent
UNIT V
Some Useful Reactions in Organic Synthesis:
i. Protection of functional groups: Hydroxyl, Carbonyl and amino groups
ii).Oxidation: Oxidation of alcohols and carbonyl compounds with suitable examples
iii). Reduction: Reduction of double and triple bonds and carbonyl compounds with suitable examples
Text Books:
1. Text book of Organic Chemistry Morrsion and Boyd, Preintice Hall, 6th edition, 1992.
2. Organic Reaction Mechanisms by VK Ahulwalia and RK Parashar, Narosa Book Distributors Pvt.
Ltd., 4th edition, 2011.
47
Reference Books:
1. Guide book to Mechanism in Organic Chemistry, Peter Skyes, Prentice hall, 6th edition, 1986.
2. Text book of Organic Chemistr, P.L. Soni, Sultan chand & sons, 29th edition, 2012.
3. Organic Chemistry Vol- I-IL. Finar, Pearson, 6th edition, 2002.
4. Reactions and Reagents , O.P. Agrawal, Krishna prakasham Media Pvt Ltd., 1st edition , 1975.
5.A Text Books of Organic Chemistry- Bahl and Arun Bahl, S. Chand company, New Delhi, ist edition,
2003.
6. Polymer Science and Technology- Hema Singh, Acme Learning, New Delhi, 13th edition, 2012.
48
3 1 3
(13A08404) CHEMICAL ENGINEERING THERMODYNAMICS
Course Objective:
To provide the students with the terminology of thermodynamics like system, properties,
processes, reversibility, equilibrium, phases, components; the relationship between heat and
work by understanding the significance of the thermodynamic laws.
Learning Outcome:
This course will enable the student to understand the spontaneity and energy efficiency of a
process.
UNIT I
Introduction: The scope of thermodynamics, temperature, defined quantities; volume, pressure, work,
energy, heat, Joules Experiments.
The first law and other basic concepts: The first law of thermodynamics, thermodynamic state and
state functions, enthalpy, the steady-state steady-flow process, equilibrium, the phase rule, the reversible
process, constant-V and constant- P processes, heat capacity, isobaric, isochoric, isothermal, adiabatic
and polytrophic processes.
UNIT II
Volumetric properties of pure fluids: The PVT behavior of pure substances, virial equations, the ideal
gas, the applications of the virial equations, second virial coefficients from potential functions. Cubic
equations of state, generalized correlations for gases, generalized correlations for liquids, molecular
theory of fluids.
UNIT III
The second law of thermodynamics: Statements of the second law, heat engines, thermodynamic
temperatures scales, thermodynamic temperature and the ideal gas scale
Entropy, Entropy changes of an ideal gas, mathematical statement of the second law, the third law of
thermodynamics, entropy from the microscopic view point, calculation of ideal work and lost work.
UNIT IV
Power cycles: Carnot cycle, Rankine cycle, Otto cycle, Diesel cycle.
Refrigeration and liquefaction: The Carnot refrigerator, the vapor compression cycle, the comparison
of refrigeration cycles, the choice of refrigerant, absorption refrigeration, the heat pump, liquefaction
processes.
UNIT V
Thermodynamic properties of fluids: Property relations for homogeneous phases, residual properties,
two phase systems, thermodynamic diagrams, tables of thermodynamic properties, generalized property
correlation for gases.
Heat effects: Sensible heat effects, Internal energy of ideal gases: Microscopic view, Latent heats of
pure substances, heat effects of industrial reactions, heat effects of mixing processes.
Standard heat of reaction, Standard heat of formation, Standard heat of combustion, temperature
dependence of heat of reaction.
Text Books:
1. J.M.Smith and HC Van Ness, Introduction to Chemical Engineering Thermodynamics, 6th
ed, McGraw Hill,2003.
49
Reference Books:
1. Chemical, Biochemical and Engineering Thermodynamics by Stanley I. Sandler, 4th
Edition, Wiley , 2007.
2. Y.V. C.Rao, Chemical Engineering Thermodynamics, University publications, 1st edition, 1997.
3. K. V. Narayanan, Chemical Engineering Thermodynamics, PHI,2001
Codes/Tables: Compressibility chart should be provided during examination
50
3 1 3
(13A08405) MECHANICAL UNIT OPERATIONS

Course Objective:
This course deals with the different mechanical unit operations in chemical engineering.
Specific attention is given on particle and separation techniques.
Learning Outcome:
Student will gain knowledge on various mechanical separation operations used in chemical
industry.
UNIT I
Properties, handling and mixing of particulate solids: Characterization of solid particles, properties of
particulate masses, storage and mixing of solids, types of mixers, mixers for cohesive solids, mixers for
free flowing solids.
Transportation of solid particulate mass, belt, screw, apron conveyers, bucket elevators, pneumatic
conveying.
UNIT II
Size reduction: Principles of comminution, computer simulation of milling operations, size reduction
equipment-crushers, grinders, ultra fine grinders, cutting machines, Equipment operation. Laws of
crushing: Kicks law, Bonds law, Rittingers law
Screening, Industrial screening equipments, Effectiveness of the screen, differential & cumulative
analysis.
UNIT III
Filtration, cake filters, centrifugal filters, cyclone separators, electro-static precipitators.
Principles of cake filtration. Clarifying filters, liquid clarification, gas cleaning, principles of
clarification. Cross flow filtration, types of membranes, permeate flux for ultra-filtration, Concentration
polarization, particle rejection of solutes, micro filtration.
UNIT IV
Separations based on motion of particles through fluids, gravity settling processes and centrifugal
settling processes, float and sink method, differential settling, coagulation, Flotation-separation of ores,
flotation agents
Agitation and mixing of liquids: Agitation of liquids, circulation velocities, power consumption in
agitated vessels. Blending and mixing of liquids, suspension of solid particles, dispersion operations.
UNIT V
Transportation of solids: Belt, screw, apron conveyers, bucket elevators, pneumatic conveyors.
(Qualitative treatment).
Flotation: General description, flotation reagents, applications, flotation machines, capacities, flotation
economics.
Text Books:
1. Unit Operations in Chemical Engineering by W.L. McCabe and J.C. Smith and Peter
Harriott, Mc Graw Hill 7th ed. 2001.
Reference Books:
1. Chemical engineers hand book, J.H. Perry, 7th ed., Mc Graw Hill, 1999.
2. Introduction to Chemical Engineering by J.T.Banchero & W.L. Badger., TMH, 1997.
Codes/Tables: Power number verses Reynolds number graphs should be provided during examination
51
B.Tech. II - II Sem. L C
3 2
(13A08406) PROCESS HEAT TRANSFER LAB
Course Objective:
This lab will provide practical knowledge on various heat transfer process and equipment like
heat exchangers and evaporators.
Learning Outcome:
The student will be able to understand the thermal conductivity measurement, heat transfer
coefficient, calculation in natural and forced convection and some of the radiation aspects.
1. Determination of total thermal resistance and thermal conductivity of composite wall.
2. Determination of thermal conductivity of a metal rod.
3. Determination of natural convective heat transfer coefficient for a vertical tube.
4. Determination of critical heat flux point for pool boiling of water.
5. Determination of forced convective heat transfer coefficient for air flowing through a pipe
6. Determination of overall heat transfer coefficient in Double pipe heat exchanger.
7. Determination of overall heat transfer coefficient in Shell and Tube heat exchanger: Parallel,
Counterflow.
8. Study of the temperature distribution along the length of a pin-fin under natural and forced
convection conditions
9. Estimation of un-steady state film heat transfer coefficient between the medium in which the body
is cooled.
10. Determination of Stefan Boltzmann constant.
11. Determination of emissivity of a given plate at various temperatures.
12. Determination of radiation constant of a given surface.
52
B.Tech. II - II Sem. L C
3 2
(13A08407) MECHANICAL UNIT OPERATIONS LAB
Course Objective:
The course will equip students with the practical knowledge of different mechanical unit
operations & operational conditions of different equipments.
Learning Outcome:
Student will be able to develop knowledge on various mechanical separation operations used in
a chemical industry.
1. To determine the time of grinding in a ball mill for producing a product with 80 % passing a given
screen.
Major equipment - Ball mill Apparatus, Sieve shaker, Different sizes of sieves,
weighing balance.
2. To verify the laws of crushing using any size reduction equipment like crushing rolls or vibrating
mills and to find out the working index of the material.
Major equipment Jaw Crusher, Sieve shaker, Different sizes of sieves, Weighing Balance, Energy
meter.
3. To find the effectiveness of hand screening and vibrating screen of a given sample.
Major equipment - Vibrating Sieve shaker, Different sizes of sieves, Weighing Balance.
4. To achieve beneficiation of a ore using froth flotation technique.
Major equipment - Froth flotation cell
5. To obtain batch sedimentation data and to calculate the minimum thickner area under given
conditions.
Major equipment- Sedimentation apparatus
6. To determine the specific cake resistance and filter medium resistance of a slurry in plate and frame
filter press.
Major equipment - Plate and frame filter press.
7. To separate a mixture of particles by Jigging.
Major equipment - Jigging apparatus
8. To calculate separation efficiency of particles in a mixture using cyclone separator.
Major equipment - Cyclone separator
9. To determine reduction ratio of a given sample in a pulverizer.
Major equipment - Pulverizer
10. To Verify Stokes law.
Major equipment Stokes law apparatus
11. To determine reduction ratio of a given sample in .a grinder Major equipment - Grinder
53
B.Tech. II - II Sem.
(13A52301) HUMAN VALUES & PROFESSIONAL ETHICS (AUDIT COURSE)
Course Objective:
This course deals with professional ethics which includes moral issues and virtues, social
responsibilities of an engineer, right, qualities of Moral Leadership
UNIT I
ENGINEERING ETHICS
Senses of Engineering Ethics Variety of Moral Issues Types of Inquiry Moral Dilemmas Moral
Autonomy Kohlbergs Theory Gilligans Theory Consensus and Controversy Professions and
Professionalism Professional Ideals and Virtues Uses of Ethical Theories
UNIT II
ENGINEERING AS SOCIAL EXPERIMENTATION
Engineering as Experimentation Engineers as Responsible Experimenters Research Ethics Codes
of Ethics Industrial Standards A Balanced Outlook on Law The Challenger Case Study
UNIT III
ENGINEERS RESPONSIBILITY FOR SAFETY
Safety and Risk Assessment of Safety and Risk Risk Benefit Analysis Reducing Risk The
Government Regulators Approach to Risk Chernobyl Case Studies and Bhopal
UNIT IV
RESPONSIBILITIES AND RIGHTS
Collegiality and Loyalty Respect for Authority Collective Bargaining Confidentiality Conflicts
of Interest Occupational Crime Professional Rights Employee Rights Intellectual Property Rights
(IPR) Discrimination
UNIT V
GLOBAL ISSUES
Multinational Corporations Business Ethics Environmental Ethics Computer Ethics - Role in
Technological Development Weapons Development Engineers as Managers Consulting Engineers
Engineers as Expert Witnesses and Advisors Honesty Moral Leadership Sample Code of
Conduct
Text Books:
1. Mike Martin and Roland Schinzinger, Ethics in Engineering, McGraw Hill, New York
2005.
2. Charles E Harris, Michael S Pritchard and Michael J Rabins, Engineering Ethics
Concepts and Cases, Thompson Learning, 2000.
Reference Books:
1. Charles D Fleddermann, Engineering Ethics, Prentice Hall, New Mexico, 1999.
2. John R Boatright, Ethics and the Conduct of Business, Pearson Education, 2003.
3. Edmund G Seebauer and Robert L Barry, Fundamentals of Ethics for Scientists and
Engineers, Oxford University Press, 2001.
4. Prof. (Col) P S Bajaj and Dr. Raj Agrawal, Business Ethics An Indian Perspective,
Biztantra, New Delhi, 2004.
5. David Ermann and Michele S Shauf, Computers, Ethics and Society, Oxford University
Press, 2003.
54
B.Tech. III-I Sem. Th Tu C

3 1 3
(13A08501) ENERGY ENGINEERING
Course Objective:
To acquaint students with the conventional and non-conventional energy sources and their utilization.
To stress upon the importance of non-conventional energy sources, energy auditing and conservation in
process industries.
Learning Outcome:
The students will be exposed to knowing different energy sources and advantages and disadvantages of
each of these sources. Further the student will also be knowing about the energy auditing.
UNIT I
Sources of energy, types of fuels-energy and relative forms: Calorific value- gross and net value,
calculation of calorific value from fuel analysis, experimental determination energy resources present
and future energy demands with reference to India.
Coal: origin, occurrence, reserves, petrography, classification, ranking, analysis, testing, storage, coal
carbonization and byproduct recovery, liquefaction of coal, gasification of coal, burning of coal and
firing mechanism, burning of pulverized coal.
UNIT II
Liquid fuels: Petroleum: origin, occurrence, reserves, composition, classification, characteristics,
fractionation, reforming, cracking, petroleum products, specification of petroleum products, burning of
liquid fuels.
Gaseous Fuels: Natural gas, coke oven gas, producer gas, water gas, LPG, burning of gaseous fuels.
UNIT III
Energy scenario and renewable energy sources: Global and Indian situation, potential of non
conventional energy sources, economics . Renewable and Future Energy Sources: Principles and
applications of wave energy, tidal energy, biomass energy, OTEC and Geothermal energy. MHD
Engineering. Fuel Cells. Wind Energy potentials.
UNIT IV
Solar energy: Radiation, flat plate and concentrating collectors, fluid flow and heat transfer analysis,
estimation of solar radiation, Active systems, solar pond, passive space conditioning, power generation,
photovoltaics.
Combined Heat and Power Systems: Waste heat recovery, sources of waste heat and potential
application, various types of heat recovery systems, regenerators, recuperators, waste heat boilers.
UNIT V
Energy Auditing and Conservation: short term, medium term, long term schemes, energy conversion,
energy index, energy cost, representation of energy consumption, sanky diagram, energy auditing.
Conservation methods in process industries, theoretical analysis, practical limitations.
Text Books:
1. Fuels, furnaces and refractories by O.P.Gupta, 3rd edition, Khanna Publishers, 1996.
2. Fuels and combustion by Sami sarkar 2nd edition orient Longman (1998).
3. Solar Energy Fundamentals Design, Modelling and Applications by G.N. Tiwari, Nwrosh.
4. Renewable Energy sources and Engineering Technologies D.p. Kothari, K.C. Singal,
Rakesh Ranjan, 2013 , 2nd Edi, PHI publications
55
Reference Books:
1. Non-conventional energy resources by G.D.Rai, Khanna Publishers
2. Solar energy by S.P.Sukhetme
3. Conventional energy technology, Fuel and chemical energy by Tata McGraw-Hill book Co.Ltd.
(1987)
4. Fuel and energy by harker and Backhurst Academic press London 1981
5. Fuel science- harker and Allen Oliver and Boyd 1972
6. Energy management, 1st edition W.R.Murphy, G.Mc.Kay Butterwolfer & Co.Ltd.(2001)
7. Energy management by Turner
Codes/Tables: Nil
Pre-requisite: Nil
56
B.Tech. III - I Sem. Th Tu C

3 1 3
(13A08502) INSTRUMENTATION AND PROCESS CONTROL
Course Objective:
To provide the students about the working knowledge of Laplace transforms to express the dynamics of
linear control systems in terms of transfer functions and understand about different controllers. Also the
student is exposed to principles of various measuring instruments.
Learning Outcome:
Ability to model the dynamic processes, to analyze the dynamic processes, to design feedback control
system for chemical, mechanical & electrical engineering systems and to design advanced control
system for complex and normal processes.
UNIT I
Elements of instruments, static and dynamic characteristics, basic concepts of response of first order
type instruments, mercury in glass thermometer, bimetallic thermometer, pressure spring thermometer,
static accuracy and response of thermometers.
Thermo electricity: Industrial thermocouples, thermocouple wires, thermo couple wells and response
of thermocouples. Thermal coefficient of resistance, industrial resistance thermometer bulbs and
circuits, radiation receiving elements, radiation, photoelectric and optical pyrometers.
UNIT II
Introduction to process dynamics and control: Laplace transforms, Inverse Laplace transform,
Response of First Order Systems. Physical examples of first order systems- Liquid level, Mixing
process, R- C circuit. Linearization.
Response of first order systems in series- interacting and non- interacting systems, second order
systems, transportation lag.
UNIT III
Control system: Components of a control system, Servo Vs regulator problem, development of block
diagram.
Controllers and final control elements: Control valve and its construction, sizing and characteristics,
P, PD, PI, PID controllers.
UNIT IV
Stability: Concept of Stability, Stability criterion, Routh test for stability
Root locus: concept of root locus, plotting the root locus diagram.
Introduction to frequency response, Bode diagrams.
Control systems design by frequency response: Bode stability criterion, Gain and Phase margins.
UNIT V
Process identification: Step, frequency and pulse testing, process identification using response curve,
tangent method.
Tuning of P, PD, PI, PID controllers, trial and error method, Ultimate gain and ultimate period, Ziegler-
Nichols technique, Cohen and Coon rules.
Text Books:
1. Process Systems Analysis and Control, 2nd ed., D.R. Coughanowr, McGraw-Hill, 1991
2. Industrial instrumentation by Donald P.Eckman, Wiley eastern, 1950.
Reference Books:
1. Chemical Process Control, G. Stephanopoulos, PHI Learning Pvt. Ltd., New Delhi, 2010
2. Process Control, B.W. Bequette, PHI Learning Pvt. Ltd., New Delhi, 2010
Codes/Tables: Nil
57

3 1 3
(13A08503) PHASE AND CHEMICAL EQUILIBRIA
Course Objective:
To impart knowledge about the behavior of real fluids and to modify the idea behavior characteristics
to deal with the real systems. In this context this subject deals with the concepts of chemical potential,
partial properties, property relations for ideal gases, fugacity excess properties and to develop the
theoretical foundation for applications of thermodynamics to gas mixtures and liquid solutions and to
perform the phase equilibrium calculations using simple models for VLE, Gamma/Phi approach and
equation of state approach.
Learning Outcome:
Students will be able to understand the procedures for estimating the thermodynamic properties of real
systems and perform thermodynamic calculations oriented to the analysis and design of chemical
processes.
UNIT I
Solution Thermodynamics: Theory, Fundamental property relation, chemical potential as a criterion
for phase equilibrium, partial properties, ideal gas mixtures, fugacity and fugacity coefficient for pure
species, fugacity and fugacity coefficient for species in solutions, generalized correlations for Fugacity
coefficient, The ideal solutions, excess properties.
UNIT II
Solution Thermodynamics: Applications: The liquid phase properties from VLE data, models for the
excess Gibbs energy, property changes of mixing.
Introduction to Molecular Thermodynamics : Molecular Theory of Fluids, Second Virial
Coefficients from Potential Functions, Internal Energy of Ideal Gases: Microscopic view.
UNIT III
VLE at low to moderate pressures: The nature of equilibrium, the phase rule, Duhems theorem, VLE:
Qualitative behavior, the gamma /Phi formulation of VLE, Dew point and bubble point calculations,
flash calculations, solute (1)/solvent (2) systems.
Thermodynamic Properties and VLE from Equations of State: properties of fluids from the virial
equations of state, properties of fluids from cubic equations of state, fluid properties from correlations of
the Pitzer type, VLE from cubic equations of state
UNIT IV
Topics in Phase Equilibria: Equilibrium and stability, Liquid-Liquid Equilibrium (LLE), Vapor-
LiquidLiquid Equilibrium (VLLE), Solid-Liquid Equilibrium (SLE), Solid Vapor Equilibrium (SVE).
UNIT V
Chemical Reaction Equilibria: The reaction coordinate, application equilibrium criterion to chemical
reactions, The standard Gibbs energy change and the equilibrium constant, effect of temperature on
equilibrium constants, relation of equilibrium constants to composition, equilibrium conversion for
single reactions, Phase rule and Duhems theorem for reacting systems.
Text Books:
1. Introduction to Chemical Engineering Thermodynamics, 6th ed., J.M. Smith, H.C. Van
Ness and M.M. Abbott, Tata McGraw-Hill, New Delhi, 2003.
58
Reference Books:
1. Chemical Engineering Thermodynamics, Pradeep Ahuja, PHI Learning Pvt. Ltd., New
Delhi, 2009
2. A Text Book of Chemical Engineering Thermodynamics, K.V. Narayanan, PHI Learning
Pvt. Ltd., New Delhi, 2001.
Codes/Tables: Nil
Pre-requisite: Chemical Engineering Thermodynamics
59

3 1 3
(13A08504) CHEMICAL REACTION ENGINEERING I
Course Objective:
To provide a foundation on deriving rate expressions for series, parallel, reversible reactions and the
knowledge about product distribution in multiple reactions, recycle reactors and auto catalytic
reactions.
Learning Outcome:
This course provides necessary knowledge for selection of the chemical reactors for a particular
process, design and simulation of existing reactor.
UNIT I
Overview of chemical reaction engineering- classification of reactions, variables affecting the rate of
reaction definition of reaction rate. Kinetics of homogenous reactions- concentration dependent term of
rate equation, Temperature dependent term of rate equation, searching for a mechanism, predictability
of reaction rate from theory.
Interpretation of batch reactor data- constant volume batch reactor:- Analysis of total pressure
data obtained in a constant-volume system, the conversion, Integral method of analysis of data general
procedure, irreversible unimolecular type first order reactions, irreversible bimolecular type second
order reactions, irreversible trimolecular type third order reactions, empirical reactions of nth order,
zero-order reactions, overall order of irreversible reactions from the half-life, fractional life method,
irreversible reactions in parallel, homogenous catalyzed reactions, autocatalytic reactions, irreversible
reactions in series.
UNIT II
Constant volume batch reactor first order reversible reactions, second order reversible reactions,
reversible reactions in general, reactions of shifting order, Differential method of analysis of data.
Varying volume batch reactordifferential method of analysis, integral method of analysis, zero order,
first order, second order, nth order reactions, temperature and reaction rate, the search for a rate
equation.
UNIT III
Introduction to reactor design- general discussion, symbols and relationship between CA and XA.
Ideal reactors for a single reaction- Ideal batch reactor, Steady-state mixed flow reactor, Steady-state
plug reactors.
Design for single reactions- Size comparison of single reactors, Multiple- reactor systems, Recycle
reactor, Autocatalytic reactions.
UNIT IV
Design for parallel reactions- introduction to multiple reactions, qualitative discussion about product
distribution, quantitative treatment of product distribution and of reactor size.
Multiple reactions-Irreversible first order reactions in series, quantitative discussion about product
distribution, quantitative treatment, plug flow or batch reactor, quantitative treatment, mixed flow
reactor, first-order followed by zero-order reaction, zero order followed by first order reaction.
UNIT V
Temperature and Pressure effects- single reactions- heats of reaction from thermodynamics, heats of
reaction and temperature, equilibrium constants from thermodynamics, equilibrium conversion, general
graphical design procedure, optimum temperature progression, heat effects, adiabatic operations, non
60
adiabatic operations, comments and extensions. Exothermic reactions in mixed flow reactors-A special
problem, multiple reactions.
Text Books:
1. Chemical Reaction Engineering, 3rd ed., O. Levenspiel, John Wiely & Sons, 1999.
Reference Books:
1. Elements of Chemical Reaction Engineering, 2nd ed., H.S. Fogler, PHI Learning Pvt. Ltd.,
New Delhi, 2010.
2. Chemical Engineering Kinetics, 3rd ed., J.M. Smith, McGraw-Hill, New York, 1981.
Codes/Tables: Nil
61

3 1 3
(13A08505) MASS TRANSFER OPERATIONS-I
Course Objective:
To impart the basic concepts of molecular diffusion, mass transfer coefficients and analysis of different
mass transfer processes.
Learning Outcome:
Fundamental knowledge on mass transfer mechanisms and operations like absorption, stripping and
humidification. This course enables the studies for selection and design of the column internals like
packing, tray efficiency, calculation of transfer units, etc.
UNIT I
Diffusion and mass Transfer- Mass Transfer Operations and their applications.
Molecular Diffusion- Ficks first law- steady state molecular Diffusion in binary mixtures of gases,
liquids and solids- Determination of Diffusivity in gases by Stefans method- estimation of diffusion
coefficients in binary mixtures of liquids and gases by correlation.
UNIT II
Diffusion in solids:- Unsteady state diffusion, diffusion through polymers, crystallin solids, porous and
non porous solids. Eddy diffusion- Basic concepts of mass transfer theories- Film mass transfer
coefficients for the cases of equimolar counter diffusion and diffusion of one component (A) in stagnant
component (B) Correlations for mass transfer coefficients and Reynolds & Colburn analogies.
UNIT III
Interphase mass transfer- overall mass transfer coefficients- Two resistance theory- Gas phase &
liquid- phase controlled situations.
Equipment for gas- liquid contact- Description of continuous and stage wise contact equipment-
packing for packed columns- Liquid distribution- Mass transfer coefficients in packed columns-
Flooding in packed and plate columns- Ideal- plate- Murphree, point, plate and column efficiency-
Comparison of packed and plate columns.
UNIT IV
Absorption and Stripping- counter current and co- current isothermal absorption and stripping of single
component- Operating lines- Minimum flow rates- Determination of number of transfer Units and
height of the Continuous contact absorbers. Multistage absorption and determination of number of
plates- absorption factor- Kremser- Brown equation.
UNIT V
Vapor, gas mixtures- Humidity and relative saturation. Dew point adiabatic saturation and wet bulb
temperatures- psychometric Charts- Enthalpy of gas-vapor mixtures.
Humidification and Dehumidification- Operating lines and Design of Packed Humidifiers,
Dehumidifiers and Cooling towers, Spray Chambers.
Text Books:
1. Mass Transfer Operations, 3rd ed., R. E. Treybal, McGraw-Hill, New York, 1980.
Reference Books:
1. Transport Processes and Separation Process Principles 4th ed., C. J. Geankoplis, PHI Learning Pvt.
Ltd., New Delhi, 2009.
2. Fundamentals of Momentum, Heat and Mass Transfer, 3rd ed., J.R. Welty, C.E. Wicks and R.E.
Wilson, John Wiley & Sons, New York, 1984.
Codes/Tables: Humidity Charts, Unsteady Diffusion Plots.
62
B.Tech. III - I Sem. Th Tu C

3 1 3
(13A52501) MANAGERIAL ECONOMICS & FINANCIAL ANALYSIS (MEFA)
Course Objective:
The objectives of this course are to equip the student with the basic inputs of Managerial Economics
and Economic Environment of business and to enrich analytical skills in helping them take sound
financial decisions for achieving higher productivity.
Learning Outcome: The thorough understanding of Managerial Economics and Analysis of Financial
Statements facilitates the Technocrats cum Entrepreneurs to take-up decisions effectively and
efficiently in the challenging Business Environment.
UNIT I
INTRODUCTION TO MANAGERIAL ECONOMICS
Managerial Economics - Definition, nature and scope contemporary importance of Managerial
Economics - Demand Analysis: Determinants- Law of Demand - Elasticity of Demand. Significance
types measurement of elasticity of demand - Demand forecasting- factors governing demand
forecasting- methods of demand forecasting Relationship of Managerial Economics with Financial
Accounting and Management.
UNIT II
THEORY OF PRODUCTION AND COST ANALYSIS
Production Function Short-run and long- run production - Isoquants and Isocosts, MRTS, least cost
combination of inputs - Cobb-Douglas production function - laws of returns - Internal and External
economies of scale - Cost Analysis: Cost concepts - Break-Even Analysis (BEA) - Managerial
significance and limitations of BEA - Determination of Break Even Point (Simple Problems)
UNIT III
INTRODUCTION TO MARKETS AND NEW ECONOMIC ENVIRONMENT
Market structures: Types of Markets - Perfect and Imperfect Competition - Features, Oligopoly -
Monopolistic competition. Price-Output determination - Pricing Methods and Strategies. Forms of
Business Organization Sole Proprietorship- Partnership Joint Stock Companies Public Sector
Enterprises New Economic Environment- Economic systems Economic Liberalization
Privatization and Globalization
UNIT IV
CAPITAL AND CAPITAL BUDGETING
Concept of Capital - Over and Under capitalization Remedial measures - Sources of Short term and
Long term capital - Estimating Working Capital requirement Capital budgeting Features of Capital
budgeting proposals Methods and Evaluation of Capital budgeting Pay Back Method Accounting
Rate of Return (ARR) Net Present Value (NPV) Internal Rate Return (IRR) Method (simple
problems)
UNIT V
INTRODUCTION TO FINANCIAL ACCOUNTING AND ANALYSIS
Financial Accounting Concept - emerging need and importance - Double-Entry Book Keeping-
Journal - Ledger Trial Balance - Financial Statements - - Trading Account Profit & Loss Account
Balance Sheet (with simple adjustments). Financial Analysis Ratios Techniques Liquidity,
Leverage, Profitability, and Activity Ratios (simple problems).
63
Text Books:
1. Aryasri: Managerial Economics and Financial Analysis, 4/e, TMH, 2009.
2. Varshney & Maheswari: Managerial Economics, Sultan Chand, 2009.
Reference Books:
1. Premchand Babu, Madan Mohan:Financial Accounting and Analysis,Himalaya, 2009
2. S.A. Siddiqui and A.S. Siddiqui: Managerial Economics and Financial Analysis, New Age
International,. 2009.
3. Joseph G. Nellis and David Parker: Principles of Business Economics, Pearson, 2/e, New
Delhi.
4. Domnick Salvatore: Managerial Economics in a Global Economy, Cengage,
2009.
5. H.L.Ahuja: Managerial Economics, S.Chand, 3/e, 2009
64
B.Tech. III - I Sem. L C

3 2
(13A08506) ENERGY & ENVIRONMENTAL ENGINEERING LAB
Course Objective :
To impart practical knowledge on water, air analysis and also to provide the knowledge on various
energy aspects.
Learning Outcome:
Student will able to understand the importance of environment, energy and also to analyze the various
parameters that will effect the quality of environment. It will also provide the how to carry energy
auditing.
1. Estimation of chemical and physical parameters of Ground and Surface water:

PH, TDS & Conductivity, Hardness, Turbidity, Fluoride, Color analysis.
Pesticide Microbial analysis: e-coli/ total coliforms bacteria
2. Estimation of physical parameters of waste water:
PH, TDS, Hardness, Turbidity, Alkalinity etc.
3. Estimation of chemical parameters of waste water:
COD, BOD, TSS
4. Water and waste water treatment:
Small RO system for treatment of ground water.
Same above system with UF membrane for turbidity removal and water disinfection.
5. Analysis of Air:
Estimation of SPM, RSPM, Sox, Nox, CO and ozone in atmospheric air to study air pollution.
6. Fuel cell Test Kit [Energy]
A small watt to 1 watt fuel cell with water electrolysis kit (H2 and O2 Generation) plus small
volt meter and ammeter for measuring fuel cell performance.
7. One small transparent anaerobic/aerobic biological reactor with slurry pump and aerator for
treatment of industrial effluents to reduce COD levels.
8. Measurement of Flash point, fire point and calorific value of petroleum products.
9. Energy auditing of your Department.
List of Equipment
PH meter, Colorimeter, TDS meter, Aerobic /Anaerobic reactor 25L capacity, BOD incubator, High
accuracy analytical balance (5 digit), Dessicators, RO system with domestic 2x12 Membrane
module, H2S vial kit, Water analysis kit, UV-Vis spectrophotometer, High volume air sampler, Bomb
calorimeter, Fuel cell test kit, Microscope.
65
B.Tech. III- I Sem. L C

3 2
(13A08507) PROCESS DYNAMICS AND CONTROL LAB
Course Objective:
To provide the fundamental background in understanding the dynamic behavior of physical systems and
various controllers.
Learning Outcome:
This lab provides the basic practical knowledge of different dynamic systems and their control aspects.
1. Dynamics of a single capacitance system subjected to impulse change

2. Dynamics of system subjected to step change (thermal system)
3. Dynamics of non-interacting system subjected to step change
4. Dynamics of second order interacting system subjected to step change
5. Dynamics of single capacitance system subjected to a step change
6. Response of first order system subjected to linear change
7. Dynamics of Bimetallic thermometer
8. Level measurement by air purge method
9. Experiments on proportional, reset, rate mode of control and their combinations
10. Estimation of damping coefficient, time constant for U-tube manometer
66
B.Tech. III- II Sem. Th Tu C

3 1 3
(13A52601) MANAGEMENT SCIENCE
Course Objective:
The objectives of this course are to equip the student the fundamental knowledge of Management
Science and its application to effective management of human resources, materials and operations of an
organization. It also aims to expose the students about the latest and contemporary developments in the
field of management.
Learning outcome:
This course enables the student to know the principles and applications of management knowledge and
exposure to the latest developments in the field. This helps to take effective and efficient managerial
decisions on physical and human resources of an organization. Besides, the knowledge of Management
Science facilitates for his/her personal and professional development.
UNIT 1
INTRODUCTION TO MANAGEMENT
Definition of Management- Function of Management- Management as a Science and Art-Management
as a Profession- Universality of Management- Henri Faylos Administrative Theory Elton Mayos
Human Relations Movement- Systems theory Contingency theory- Monetary and non-monetary
incentives to motivate work teams- Leadership Definition- Qualities of successful leaders- Different
leadership styles.
UNIT II
ORGANIZATION DESIGN AND STRUCTURE
Organization design and structure- PrinciplesTypes of organization structure-Mechanic and Organic
Structures- Line organization- Line & Staff organization- Functional Organization Matrix
organization structures- merits and demerits- Departmentation and Decentralization-Power and
Authority- Delegation of authority-Principles for effective delegation of authority.
UNIT III
HUMAN RESOURCE AND MATERIALS MANAGEMENT
Concept of HRM-functions Human Resource Planning-Job Analysis-Recruitment and Selection-
Training and Development- Performance appraisal methods- Wage and Salary Administration-
Grievances handling Procedure-Material Management- Need for Inventory control- Economic order
quantity- ABC analysis- Management of purchase, stores and stores records.-Marketing Management
Concept- Channels of distribution- Marketing mix and product mix.
UNIT IV
MANAGEMENT OF OPERATIONS & PROJECT MANAGEMENT
Nature of organizational control- Marketing control- HR control- effective control systems- Operations
Management- Essentials of operations management- Trends in operational management- Designing
operation system for effective management of an organization-Project Management Network Analysis-
PERT and CPM-Project crashing (Simple problems)
UNIT V
CONTEMPORARY MANAGEMENT ISSUES
Strategic Management-Concept- Mission-Vision-Core values-Setting objectives-Corporate planning
Environmental scanning-SWOT analysis- Steps in strategy formulation & implementation-
Management Information System (MIS)- Enterprise Resource Planning (ERP)-Just-in-Time (JIT)- Total
Quality Management (TQM) Supply Chain Management-Six Sigma-Business Process Outsourcing
(BPO).
67
Text Books:
1. Stoner, Freeman, Gilbert, Management, Pearson, Six Edition 2008
2. Aryasri: Management Science, Fourth Edition TMH, 2012.
Reference Books:
1. Vijay Kumar & Apparo, Introduction to Management Science, Cengage, 2011.
2. Kotler Philip & Keller Kevin Lane: Marketing Management, 14th Edition, Pearson, 2012.
3. Aswathappa, Human Resource Management, Himalaya, 2012.
4. Kanishka Bedi, Production and Operations Management, Oxford University Press, 2011.
5. Schermerhorn, Capling, Poole & Wiesner: Management, Wiley, 2012.
6. Joseph M Putti, Management Principles, Mc Millan Publishers, 2012.
68
B.Tech. III - II Sem. Th Tu C

3 1 3
(13A08601) CHEMICAL TECHNOLOGY

Course Objective:
To teach the unit operations unit processes involved manufacture of important and widely employed
organic and inorganic chemicals. Also to provide knowledge on flow sheeting
Learning Outcome:
The student will know about the different unit operations and unit processes used for manufacture of
different chemical products. It will provide the knowledge on making flow chart in sequential order
during the manufacture of new compound.
UNIT I
Water and Air: Importance of water, sources, plant location factors related to water, water shortage
problems, methods of treating fresh water, methods of obtaining fresh water from saline waters, waste
water treatment and disposal, air as a chemical raw material. Soda ash, caustic soda and chlorine, Glass:
manufacture of special glasses
UNIT II
Industrial gases: carbon dioxide, hydrogen and oxygen products of water gas, producer gas. Nitrogen
industries: synthetic ammonia, urea, nitric acid (ammonium nitrate), ammonium chloride, ammonium
phosphate and complex fertilizers Sulphur and sulphuric acid, manufacture of sulphuric acid,
hydrochloric acid and some other chemicals Aluminum sulphate and alum.
UNIT III
Cement manufacture, special cements, miscellaneous calcium compounds, magnesium compounds.
Manufacture of phenols, formaldehyde, vinyl chloride and vinyl acetate, manufacture of phenol-
formaldehyde resin and polyvinyl chloride polymer, SBR
UNIT IV
Oils: Definition, constitution, extraction and expression of vegetable oils, refining and hydrogenation of
oils.
Synthetic fibers: Classification, manufacture of Nylon 66, polyester fiber and viscose rayon fiber.
Soaps and detergents: Definitions, continuous process for the production of fatty acids, glycerin and
soap, production of detergents.
UNIT V
Pulp and paper industry: methods of pulping, production of sulphate and sulphite pulp, production of
paper wet process
Pharmaceutical Industries: Classification, Alkylation, Carboxylation and Acetylation, Condensation and
Cyclization, Dehydration,Halogenation, Oxidation, Sulfonation, Amination, Radio isotopes in
Medicine, Fermentation and Life processing for Antibiotics, Hormones, and Vitamines, Biologicals,
Steroid hormones, isolates and Animals.
Text Books:
1. Shreves Chemical Process Industries edited by Austin, Mc.graw-Hill.5th ed.1985.
2. Drydens Outlines of Chemical Technology edited by M. Gopal Rao and M. Sittig, 2nd ed. 1973.
69
Reference Books:
1. Industrial Chemistry by B.K. Sharma,
2. Hand book of industrial chemistry Vol 1& II K.H.Davis & F.S. Berner Edited by S.C. Bhatia, CBS
publishers
3. Chemical Technology: G.N. Panday, Vol 1& Vol II.
Pre-requisite:
Chemical Engineering Fluid Mechanics, Heat Transfer, Mass Transfer, Chemical Reaction
Engineering, Thermodynamics
70

3 1 3
(13A08602) MASS TRANSFER OPERATIONS-II

Course Objective:
To understand the principles, applications and process design of distillation, liquid- liquid extraction,
drying and leaching processes.
Learning Outcome:
Student will be able to learn the methodology for process design of equipments like extractors,
distillation columns and dryers in chemical industries.
UNIT I
Distillation: VLE phase diagrams, Tie lines and mixture rule- Flash vaporization and differential
distillation for binary mixtures- Steam distillation. Batch distillation with reflux for binary mixtures.
UNIT II
Distillation: Continuous fractionation of binary mixtures, multistage tray towers Ponchon and Savarit
method, Mc Cabe and Thiele method of determination of ideal plates for binary mixtures- enriching
section, exhausting section, feed introduction, total reflux, minimum and optimum reflux ratios, use of
total and partial condensers. Use of open steam. Types of Condensers and Reboilers. Packed bed
distillation. Principles of azeotropic and extractive distillation.
UNIT III
Liquid-Liquid Extraction: Solubilities of ternary liquid systems. Triangular and solvent free
coordinate systems. Choice of solvent. Extraction with insoluble and partially soluble systems- single
stage, multistage cross current and multistage counter current extraction without reflux and with reflux.
Continuous contact extraction (packed beds). Equipments for liquid- liquid extraction operation.
UNIT IV
Leaching: Preparation of solid for leaching, Unsteady state operation, in- place leaching, heap leaching,
percolation leaching, Shanks system, agitated vessels, Percolation vs Agitation. Steady state continuous
operation- equipments- methods of calculation, stage efficiency and particle equilibrium. Single stage
leaching, multistage cross current leaching, multistage counter current leaching.
UNIT V
Drying- moisture contents of solids- equilibrium content, bound and unbound moisture. Drying
conditions- Rate of batch drying and under constant drying conditions- Mechanism of batch drying-
Drying time of batch drying- through circulation drying- Description of batch and continuous dryers.
Text Books:
1. Mass Transfer Operations, 3rd ed., R. E. Treybal, McGraw-Hill, New York, 1980.
Reference Books:
1 Transport Processes and Separation Process Principles 4th ed., C. J. Geankoplis, PHI, Learning Pvt.
Ltd., New Delhi, 2009.
2 Principles of Mass Transfer and Separation Processes, B.K. Dutta, PHI Learning Pvt. Ltd., New
Delhi, 2007.
Prerequisite: Mass Transfer Operations I, Phase & Chemical Equilibrium, Chemical Process
Calculations.
71

3 1 3
(13A08603) CHEMICAL REACTION ENGINEERING II

Course Objective:
To understand the characteristic features of non- ideal flow and mixing of fluids in reaction vessels. To
give the introductory aspects of the design for heterogeneous reacting systems.
Learning Outcome:
This course will give knowledge on selection of catalyst and design of multiple reactors and their
evaluation of performance, concepts of heterogeneous reaction system applications.
UNIT I
Basics of non-ideal flow: E-curves, the exit age distribution function of fluid, the RTD, conversion in
non-ideal flow reactors, diagnosing reactors (qualitative discussion only).
The dispersion model: axial dispersion, correlations for axial dispersion, chemical reaction and
dispersion.
UNIT II
The tanks in series model: pulse response experiments and the RTD, chemical conversion. The
convection model for laminar flow- the convective model and its RTD, chemical conversion in laminar
flow reactors
Earliness of mixing, segregation and RTD: self-mixing of a single fluid, mixing of two miscible
fluids.
UNIT III
Catalysis and Catalytic reactors: catalysts, steps in catalytic reactions, synthesizing a rate law,
mechanism and rate limiting step. (From chapter 10, Fogler)
Heterogeneous reactions: Introduction to Solid catalyzed reactions: The rate equation for Surface
Kinetics- Pore diffusion resistance combined with surface kinetics, Porous catalyst particles, heat effects
during reaction, Performance equations for reactors containing porous catalyst particles.
UNIT IV
Solid catalyzed reactions- Experimental methods for finding rates. Deactivating catalysts- mechanisms
of catalyst deactivation, the rate and performance equations.
UNIT V
Fluid-fluid reactions: kinetics- the rate equation. Fluid-particle reactions: kinetics- selection of a
model, shrinking core model for spherical particles of unchanging size, rate of reaction for shrinking
spherical particles, extensions, determination of rate controlling step.
Text Books:
1. Chemical Reaction Engineering, 3rd ed., O. Levenspiel, John Wiley & Sons, 1999.
2. Elements of Chemical Reaction Engineering, 4th ed., H.S. Fogler, PHI Learning Pvt. Ltd., New Delhi,
2010.
Reference Books:
1. Chemical Engineering Kinetics, 3rd ed., J.M. Smith, McGraw-Hill, New York, 1981.
2. The Engineering of Chemical Reactions, 2nd ed., L.D. Schmidt, Oxford University Press, New Delhi,
2010
Pre-requisite:--Chemical Reaction Engineering-I
72

3 1 3
(13A08604) PROCESS MODELING AND SIMULATION
Course Objective:
To impart knowledge on modeling of various equipments and their simulation using different numerical
techniques.
Learning Outcome:
The student will be able to learn the basic principles of modeling with some examples and simulate the
model equations using numerical methods.
UNIT I
Mathematical models for chemical engineering systems: classification of mathematical models-
steady state vs dynamic models, lumped vs distributed parameter models, deterministic vs stochastic
models. Examples of mathematical models- Two heated tanks, batch reactor, constant volume CSTRs,
non-isothermal CSTR, reactor with mass transfer, ideal binary distillation column, batch distillation
with holdup.
UNIT II
Empirical model building- method of least squares, linear, polynomial and multiple regression, non-
Linear regression. Solution of Non- Linear Algebraic equations- bisection, false position, Quasi
Newton and Newton- Raphson methods.
UNIT III
Numerical integration- Trapezoidal rule, Simpsons rule and Newton Cotes formula. Numerical
solution of differential equations- Eulers method, Runge- Kutta methods, predictor corrector
methods.
UNIT IV
Numerical solution of partial differential equations- elliptic, parabolic and hyperbolic equations.
finite difference methods, Leibmans method, Crank Nicholson method. Apllications to steady state and
Unsteady state heat conduction and temperature distribution problems.
UNIT V
Process Simulation examples: VLE dew point and bubble point calculations, binary distillation
column, gravity flow tank, batch reactor, Non- isothermal CSTR, countercurrent heat exchanger.
Process simulation using modular and equation based solving approaches: Developing a simulation
model, a simple flow sheet, Sequential modular approach, Simultaneous modular approach, Equation
solving approach.
Text Books:
1. Process modeling, Simulation and Control for Chemical Engineers, 2nd ed., W. L. Luyben, McGraw-
Hill, New York, 1990.
2. Numerical Methods for Engineers, S.K. Gupta, Wiley Eastern, New Delhi, 1995.
Reference Books:
1. Numerical Methods for Engineers and Scientists, S.S. Rao
2. Introduction to Numerical Methods in Chemical Engineering, P. Ahuja, PHI learning Pvt. Ltd., New
Delhi, 2010
3. Process Modeling and Simulation, Amiya K. Jana, 2012.
4 Programming for Chemical Engineers Using C, C++ and MatLab, Raul Raymond, A. Kapuno.Jr,
Laxmi Publications, Pvt Ltd, 2010
Codes / Tables: --Nil--
73

3 1 3
(13A08605) CHEMICAL PLANT DESIGN AND ECONOMICS

Course Objective:
To familiarize to the students about various economic aspects of chemical processes.
Learning Outcome:
The student will be able to perform the economic evaluation of chemical processes and projects in the
industry
UNIT I
Introduction, Process Design development. Flow diagrams, General design considerations, Preliminary
design. Cost and asset accounting. Cash flow for industrial operations, factors effecting investment and
production cost, capital investments, estimation of capital investments, cost indices, cost factors in
capital investment
UNIT II
Organizations for presenting capital investments, estimates by compartmentalization, estimation of total
product of cost direction, production costs, fixed charges, plant overhead costs, financing.
Interest and investment cost, type interest, nominal and effective interest rates, continuous interest,
present worth and discount annuities, cost due interest on investment, source of capital.
UNIT III
Taxes and insurances, type of taxes: federal income taxes, insurance-types of insurance, self insurance.
Depreciation : types of depreciation, services life, salvage value, present value, methods for determining
depreciation, single unit and group depreciation.
UNIT IV
Profitability: alternative investments and replacements, profitability standards, discounted cash flow,
capitalized cost, pay out period ,alternative investments, analysis with small investments, increments
and replacements.
UNIT V
Optimum design and design strategy, incremental cost, general procedure for determining optimum
condition, comparison of graphical and analytical methods, optimum production rates, semi continuous
cyclic operation, fluid dynamics, mass transfer strategy of linearization
Text Books:
1. Plant Design and Economics for Chemical Engineering, 4th ed., M.S. Peters and K.D. Timmerhaus,
McGraw-Hill,1991
Reference Books:
1. Process Engineering Economics, Schweyer
Codes / Tables: -- nil--
74
B.Tech. III - II Sem. L C

3 2
(13A08606) CHEMICAL REACTION ENGINEERING LAB
Course Objective:
To impart the skills of deriving the kinetic expressions by performing the experiments on batch and
continuous flow reactors. To understand the effects of non ideal flow
Learning Outcome:
Student will able to gain the knowledge on kinetics and also to measure the conversion in various
reactors. Further, he/she will understand about the importance of non-ideality in reactors.
1. Determination of the order of a reaction using a batch reactor and analyzing the data by (a)
differential method (b) integral method.
2. Determination of the activation energy of a reaction using a batch reactor.
3. To determine the effect of residence time on conversion and to determine the rate constant using
a CSTR.
4. To determine the specific reaction rate constant of a reaction of a known order using a batch
reactor.
5. To determine the order of the reaction and the rate constant using a tubular reactor.
6. CSTRs in series- comparison of experimental and theoretical values for space times and
volumes of reactors.
7. Mass transfer with chemical reaction (solid-liquid system) determination of mass transfer
coefficient.
8. Mass transfer with chemical reaction (liquid-liquid system) determination of mass transfer
coefficient
9. Axial mixing in a packed bed. Determination of RTD and dispersion number for a packed-bed
using tracer
10. Determination of RTD and dispersion number in a tubular reactor using a tracer.
75
B.Tech. III- II Sem. L C

3 2
(13A08607) MASS TRANSFER OPERATIONS LAB
Course Objective:
To carry out the experimental studies related to diffusion, VLE data and other mass transfer operations.
Learning Outcome
Student will get practical knowledge to generate the equilibrium data and applying this knowledge for
design of distillation, extraction, leaching columns, etc. He/she will also gain knowledge on
measurement of composition.
1. Estimation of diffusivity coefficients for solids

2. Estimation of diffusivity coefficients for liquids
3. Steam distillation
4. Differential distillation
5. Packed towers, HETP evaluation
6. Vapor Liquid Equilibria
7. Hydrodynamics of Spray column
8. Studies on Batch Drying Experiment
9. Evaluation of Mass transfer coefficients
(a) Surface Evaporation (b) Wetted wall column
10. Liquid- Liquid Equilibria
11. Ternary Liquid Equilibria (binodal curve)
12. Leaching
13. Crystallization
76
B.Tech. III - II Sem.
(13A52502) ADVANCED ENGLISH LANGUAGE COMMUNICATION SKILLS LAB

(Audit Course)
Introduction:
The introduction of the Advanced Communication Skills Lab is considered essential at 3rd year level. At
this stage, the students need to prepare themselves for their careers which may require them to listen to,
read, speak and write in English both for their professional and interpersonal communication in the
globalised context.
The proposed course should be a laboratory course to enable students to use good English and
perform the following:
Gathering ideas and information to organise ideas relevantly and coherently.
Engaging in debates.
Participating in group discussions.
Facing interviews.
Writing project/research reports/technical reports.
Making oral presentations.
Writing formal letters.
Transferring information from non-verbal to verbal texts and vice-versa.
Taking part in social and professional communication.
Course Objective:
This Lab focuses on using multi-media instruction for language development to meet the following
targets:
To improve the students fluency in English, through a well-developed vocabulary and enable
them to listen to English spoken at normal conversational speed by educated English speakers
and respond appropriately in different socio-cultural and professional contexts.
Further, they would be required to communicate their ideas relevantly and coherently in
writing.
To prepare all the students for their placements.
Learning Outcome:
Accomplishment of sound vocabulary and its proper use contextually
Flair in Writing and felicity in written expression.
Enhanced job prospects.
Effective Speaking Abilities
The following course content to conduct the activities is prescribed for the Advanced English Language
Communication Skills (AELCS) Lab:
UNIT I
COMMUNICATIVE COMPETENCY:
1. Reading Comprehension
2. Listening comprehension
3. Vocabulary for competitive purpose
4. Spotting errors
UNIT II
TECHNICAL WRITING
1. Report writing
2. Curriculum vitae
3. Covering letter
4. E-mail writing
77
UNIT III
PRESENTATIONAL SKILLS
1. Oral presentation
2. Power point presentation
3. Poster presentation
4. Stage dynamics
UNIT IV
CORPORATE SKILLS
1. Dress code
2. Telephonic skills
3. Net Etiquettes
UNIT V
GETTING READY FOR JOB
1. Group discussions
2. Interview skills
3. Psychometric tests
MINIMUM REQUIREMENT:
The Advanced English Language Communication Skills (AELCS) Laboratory shall have the following
infra-structural facilities to accommodate at least 60 students in the lab:
Spacious room with appropriate acoustics.
Round Tables with movable chairs
Audio-visual aids
LCD Projector
Public Address system
P IV Processor, Hard Disk 80 GB, RAM512 MB Minimum, Speed 2.8 GHZ
T. V, a digital stereo & Camcorder
Headphones of High quality
SUGGESTED SOFTWARE:
The software consisting of the prescribed topics elaborated above should be procured and used.
1. K-VAN SOLUTIONS-Advanced communication lab

2. DELTAs key to the Next Generation TOEFL Test: Advanced Skill Practice.
3. TOEFL & GRE( KAPLAN, AARCO & BARRONS, USA, Cracking GRE by CLIFFS)
4. Train2success.com
References:
1. Objective English For Competitive Exams, Hari Mohana Prasad, 4th edition, Tata Mc Graw
Hill.
2. Technical Communication by Meenakshi Raman & Sangeeta Sharma, O U Press 2009.
3. Books on TOEFL/GRE/GMAT/CAT/ IELTS by Barrons/DELTA/Cambridge University
Press.2012.
4. Soft Skills for Everyone, Butterfield Jeff, Cengage Publications, 2011.
5. Practice Psychometric Tests: How to familiarize yourself with genuine recruitment tests, 2012.
6. Management Shapers Series by Universities Press (India) Pvt Ltd., Himayatnagar, Hyderabad
2008.
7. Handbook for Technical Writing by David A McMurrey & Joanne Buckely CENGAGE Learning
2008.
8. English for Technical Communication for Engineering Students, Aysha Vishwamohan, Tata
Mc Graw-Hill 2009.
9. Word Power Made Handy, Shalini Verma, S Chand Publications, 2011.
10. Effective Technical Communication, Ashrif Rizvi, TataMcGrahill, 2011.
78
B.Tech. IV - I Sem. Th Tu C
3 1 3
(13A08701) TRANSPORT PHENOMENA
Course Objective:
To assimilate the transfer process in a unified manner.
Learning Outcome
Ability to analyze the processes involving simultaneous flow, heat and mass transfer
UNIT I
Viscosity and the mechanisms of momentum transfer: Newtons law of viscosity (molecular momentum
transport), generalization of Newtons law of viscosity, pressure and temperature dependence of
viscosity, molecular theory of the viscosity of gases at low density, molecular theory of the viscosity of
liquids.
Thermal conductivity and the mechanisms of energy transport: Fouriers law of heat conduction
(molecular energy transport), temperature and pressure dependence of thermal conductivity, and theory
of thermal conductivity of gases at low density.
Diffusivity and the mechanisms of mass transport: Ficks law of binary diffusion (molecular mass
transport), temperature and pressure dependence of diffusivities, theory of diffusion in gases at low
density.
UNIT II
Shell momentum balances and velocity distributions in laminar flow: shell momentum balances and
boundary conditions, flow of a falling film, flow through a circular tube, flow through annulus, flow of
two adjacent immiscible fluids, creeping flow around a sphere.
UNIT III
Shell energy balances and temperature distributions in solids and laminar flow: shell energy balances;
boundary conditions, heat conduction with an electrical heat source, heat conduction with a nuclear heat
source, heat conduction with a viscous heat source, heat conduction with a chemical heat source, heat
conduction through composite walls, heat conduction in a cooling fin, forced convection, free
convection.
UNIT IV
Concentration distributions in solids and laminar flow: shell mass balances; boundary conditions,
diffusion through a stagnant gas film, diffusion with a heterogeneous chemical reaction, diffusion with a
homogeneous chemical reaction, diffusion into a falling liquid film (gas absorption), diffusion into a
falling liquid film (solid dissolution), diffusion and chemical reaction inside a porous catalyst.
UNIT V
The equations of change: Derivation of the equation of continuity in Rectangular and Polar coordinates,
the equation of motion, the equation of energy, the equation of continuity of a component in multi
component mixture (in rectangular coordinates only) the equations of change in terms of the substantial
derivative. Use of equations of change to solve one dimensional steady state problems of momentum,
heat and component transfer, Introduction to Turbulent flow and Time smoothing
Text Books:
1. Transport phenomena by Bird R.B., Stewart W.C., Lightfoot F.N., 2nd ed. John Wiley & Sons
Inc,U.S.A,1960.
Reference Books:
1. Transport phenomena for engineers by L. Theodore, International text book company, U.S.A.1971.
2. Transport processes and unit operations by C.J. Geankoplis, PHI, 3rd ed. 1997.
3. Fundamental of heat, momentum and mass transfer, Welty, Wickson, Wilson, John Wiley.
79
Codes / Tables: 1. Leonaurd Jones potential parameters and critical properties.
2. Equations of change (from Bird)
Pre-requisite: Chemical Engineering Fluid Mechanics, Process heat transfer, Mass Transfer
operations- I & II
80
B.Tech. IV- I Sem. Th Tu C

3 1 3
(13A08702) CHEMICAL PROCESS EQUIPMENT DESIGN
Course Objective:
Chemical process engineers have to deal with process design and the unit operations involved in the
process. A most suitable equipment from technical and economical point of view has to be suggested,
designed, installed and put in operation. To do all the exercise, comprehensive information has to be
efficient from process as well as mechanical point of view. This course attempts to provide necessary
information on the process design of certain common equipment used in chemical process industries.
Learning Outcome:
The student will be able to design various equipments in chemical process plants.
UNIT I
Design of Shell and Tube heat exchangers: 1-2 heat exchanger, arrangements for increased heat
recovery, and calculations for process conditions. Design calculations of a double-pipe heat exchanger:
Double pipe exchangers in series-parallel arrangement.
UNIT II
Transportation of gases and Liquids: Pressure and vacuum service Selecting device, estimation of pipe
diameter, estimation of pressure drop-performance curves.
Transportation of solids: Mechanical devices: Vertical lift, inclined lift, horizontal movement, feeders,
special devices. Fluidic devices: Pneumatic conveying; hydraulic conveying.
Transportation of Slurries
UNIT III
Design of packed towers for absorption: Flow of liquid over packings, limiting gas velocities, Pressure-
drop calculations, design of packed towers using absorption coefficients, design of packed tower using
transfer-unit method.
UNIT IV
Design of sieve tray tower for distillation: Introduction, sieve tray, tower diameter, plate spacing,
entrainment, flooding, weepage, tray layout, hydraulic parameters.
Design of rotary dryer, tray dryer and spray dryer.
UNIT V
Cooling tower practice: Mechanism, types, rating duty and physical size of cooling towers, Cooling
tower components, construction material, practical aspects of tower selection
Cooling tower design calculations: Heat transfer calculations, selection of tower size for a given duty,
corrections for altitude, use of charts for calculation of cooling tower duties.
Text Books:
1. Process Heat Transfer by D.Q. Kern, Tata McGraw Hill, 2001
2. Process equipment design by S. D. Dawande
3. Chemical Engineering by Coulson & Richardson series, Volume 6,
4. Mass Transfer operations Robert E. Treybal, McGraw Hill,
Reference Books:
1. Process design and Engineering practice, Donald R. Woods, Prentice Hall
2. Transport process and unit operations Christe J. Geanopkins
3. Unit operations Foust et al.
4. Absorption towers- Morris and Jackson Butter worths Scientific Publications
5. Cooling tower principles and practice- Hill, Pring and Osborn Butter worth-Heinemann
6. Process plant design- Harker and Backhust
81
Codes/Books : As required to solve the problems
Pre-requisites: Chemical Engineering Fluid mechanics, Process Heat Transfer and

Mass transfer Operations 1 & 2
82
B.Tech-IV-I Sem. Th Tu C
3 1 3
(13A08703) OPTIMIZATION OF CHEMICAL PROCESSES
Course Objective:
To acquaint the student with the concepts and techniques of single and multivariable optimization.
Learning Outcome:
The student will enable to optimize the problems related to design, planning and operations involved in
a chemical industry.
UNIT I
Nature and organization of optimization problems- introduction to optimization scope and hierarchy of
optimization, examples of applications of optimization, essential features of optimization problems,
general procedure for solving optimization problems, Optimization of a manufacturing problem with a
stepwise procedure, obstacles of optimization, constraints in optimization, examples and formulation of
constrained optimization problems.
Basic concepts of optimization: Continuity of functions, unimodal versus Multimodel functions.
Convex and Concave functions, Convex region, Necessary and sufficient conditions for an extremum of
an unconstrained function.
UNIT II
Optimization of unconstrained single variable functions: Region elimination methods: Fibonacci
search, Golden section search. Polynomial approximation methods- Sequential search,. Methods
specifying optimum by a point: Newtons method, Secant method, Quadratic interpolation, Cubic
interpolation. Applications of one- dimensional search methods to chemical engineering problems.
UNIT III
Unconstrained multivariable optimization: Random search methods, grid search, uni-variate search,
multivariable Newtons method, Steepest descent method, Conjugate search directions, Conjugate
gradient method, Powells method.
Constrained multi variable optimization- direct substitution, penalty function approach, slack variables,
method of Lagrangian multipliers, Kuhn- Tucker conditions.
UNIT IV
Optimization of Unit operations: Optimal pipe diameter, minimum work of compression, Economic
operation of a fixed bed filter, optimizing recovery of waste heat, optimization of multiple effect
evaporator, optimization of flow rates in Liquid- Liquid extraction column, Determination of optimal
reflux ratio for staged distillation column.
UNIT V
Linear programming and applications: Basic concepts in linear programming, graphical solution,
artificial variable technique, exceptional cases in LPP, non-existing feasible solution, degeneracy,
duality in linear programming, dual simplex method, revised simplex method, linear programming
applications including optimization of a thermal cracker. Introduction to Genetic Algorithms
(Qualitative Treatment only)
Text Books:
1. Optimization of Chemical Processes, T.F. Edgar and D.M. Himmelblau, McGraw-Hill, New York,
2001.
2. Optimization for Engineering Design, Kalyan Moy Deb, PHI Pvt. Ltd., New Delhi, 2000
Codes/Books : Nil
Pre-requisites: Nil
83

3 1 3
(13A08704) SEPARATION TECHNIQUES FOR BIO PROCESSING
Course Objective:
The objective of this course is to facilitate the students with the novel techniques that are required in
downstream processing of biotechnology based industries.
Learning Outcome:
The student will know about handling of separations using solid- fluid and separation techniques for the
low-temperature, heat sensitive materials.
UNIT I
Crystallization: crystal geometry, principles of crystallization equilibria and yields, nucleation, crystal
growth, adsorption and mass transfer theories, precipitation, crystallization from melts. (Textbook 3)
UNIT II
Adsorption: Adsorption, types of adsorption, nature of adsorbents, adsorption equilibrium, single gases
and vapors, Adsorption Hysteresis, effect of temperature, Heat of adsorption, vapor and gas mixtures:
One component adsorbed, Effect of change of temperature or pressure. Liquids, Adsorption of solute
from dilute solution, The Freundlich equation, Adsorption from concentrated solutions, adsorption
operations, stage wise operation, application of Freundlich equation to single and Multistage adsorption
(cross current & counter current).
Fluidized and teeter beds, adsorption of vapor from a gas, fluidized bed, continuous contact, steady state
moving bed adsorbers, unsteady statefixed bed adsorbers, adsorption wave, elution, adsorption-
desorption operations- thermal desorption of gases, activated carbon solvent recovery, pressure swing
and vacuum swing adsorption (qualitative treatment), regeneration with purge and desorbent, ion-
exchange: principles of ion exchange, techniques and applications, ion-movement theory, ion exclusion.
(Textbook 2)
UNIT III
Chromatography: Types of chromatography: Gas and liquid chromatography, paper and thin layer
chromatography, polarization chromatography, and continues chromatography. Solute movement
theory, superposition in linear systems, linear dispersion model, and linear stage models for
chromatography, use of Gausian solution, large-scale chromatography. Eectrophoretic separations:
Theory of electrophoresis, basic concepts of electrophoresis, forces in electrophoresis, complicating
factors in electrophoresis, methods of electrophoresis: Moving boundary electrophoresis, gel membrane
and paper electrophoresis, zone spreading in zonal electrophoresis, affinity electrophoresis, free solution
and capillary electrophoresis, sequential two dimensional electrophoresis. (Textbook 1)
UNIT IV
Pressure driven membrane separation processes, reverse osmosis, ultrafiltration, micro filtration, nano
filtration, gas separation through porous membranes, governing equations, effect of operating
parameters on flux and rejection, applications. Concentration and electrical driven membrane processes
Gas separation in non-porous membrane, pervaporation, dialysis, electro-dialysis, liquid membranes,
governing equations, effect of operating parameters on flux and selectivity, applications (Textbook 1)
UNIT V
Theories for membrane separations, concentration polarization, approximate analysis for concentration
polarization, mass transfer correlations, gel formation and fouling, completely mixed system of RO &
UF with concentration polarization, counter current gas permeation with no concentration polarization,
membrane modules. (Textbook 1)
84
Text Books:
1. Rate controlled separation by Phillip C. Wankat, Springer international, 2005
2. Mass transfer operations by R.E. Tryebal, Mc Graw Hill, 3rd ed. 1980.
3. Unit operations of Chemical Engineering by Mc.Cabe & Smith, McGraw-Hill, 5th edition 1993
Reference Books:
1. Separation processes, C. J. King, Tata McGraw Hill.
2. Transport processes and unit operations, C.J. Geankoplis, Prentice-Hall India, 3rd edition, 2000
Codes/Books : Nil
Pre-requisite: Mass Transfer operations-I, II, Phase and Chemical Equilibria, Chemical Process
Calculations.
85
B.Tech. IV-I Sem. Th Tu C

3 1 3
(13A08705) PETROLEUM AND PETROCHEMICAL TECHNOLOGY
(Elective-II)
Course Objective:
To study the origin of petroleum and the details of various petro-chemical industries. To study the
derivatives of different petro chemicals.
Learning Outcome:
The student will gain familiarity with various processes deployed in petroleum industries.
UNIT I
Origin, formation and composition of petroleum: Origin and formation of petroleum, Reserves and
deposits of world, Indian Petroleum Industry.
Petroleum processing data: Evaluation of petroleum, thermal properties of petroleum fractions,
important products, properties and test methods.
UNIT II
Fractionation of petroleum: Dehydration and desalting of crudes, heating of crude-pipe still heaters,
distillation of petroleum, blending of gasoline.
Treatment techniques: fraction-impurities, treatment of gasoline, treatment of kerosene, treatment of
lubes.
UNIT III
Thermal and catalytic processes: Cracking, catalytic cracking catalytic reforming, Naphtha cracking,
coking, Hydrogenation processes, Alkylations processes, Isomerization process.
UNIT IV
Petrochemical Industry Feed stocks, Chemicals from methane: Introduction, production of Methanol,
Formaldehyde, Ethylene glycol, PTFE, and Methylamines
UNIT V
Chemicals from Ethane-Ethylene-Acetylene: Oxidation of ethane, production of Ethylene, Manufacture
of Vinyl Chloride monomer, vinyl Acetate manufacture, Ethanol from Ethylene, Acetylene
manufacture, Acetaldehyde from Acetylene.
Text Books:
1. Petroleum refining Engineering; WL Nelson Mc Graw Hill company IV addition.
2. Modern Petroleum Refining Processes, 4th ed.,, B.K.Bhaskara Rao, Oxford & IBH Publishing,
2002.
3. Petrochemicals by B. K Bhaskara Rao, Oxford & IBH Publishing, 2002.
Reference Books:
1. The Petroleum chemicals industry by R.F.Goldstine, e & fn London, 1967
2. Chemical technology of petroleum by W.S.Gruese and D.R. Stevens, Mcgraw ` Hill, 1980
3. Fundamentals of petroleum chemical technology by P Below.
4 Petro Chemicals Volume 1 and 2 ; A Chauvel and Lefevrev ; Gulf Publishing company 1989
5. Handbook of Petroleum Processing by David SJ Jones, Peter R. Pujado Springer, 2006
6. Petroleum Refining Technology and Economics, 4th Ed, James H. Gary and Glenn E.
Handwerk, Marcel Dekker, 2001
Codes/Books : Nil
86
3 1 3
(13A08706) FLUIDIZATION ENGINEERING
(Elective-II)
Course Objective:
To teach the student about the basic principles of fluidization and its application in chemical industry.
Learning Outcome:
The student will enable to learn the importance and applications of fluidization in chemical and allied
industries.
UNIT I
Introduction: The phenomenon of fluidization; liquid like behavior of a fluidized bed; Comparison
with other contacting methods; Advantages and disadvantages of fluidized beds.
UNIT II
Industrial applications of fluidized beds: Coal gasification; gasoline from other petroleum fractions;
Gasoline from natural and synthesis gases; Heat exchange; Coating of metal objects with plastics;
Drying of solids; Synthesis of phthalic anhydride; Acrylonitrile; Polymerization of olefins; FCCU;
Fluidized combustion of coal; incineration of solid waste; Activation of carbon; gasification of waste;
bio-fluidization.
UNIT III
Fluidization and mapping of regimes: Minimum fluidization velocity; Pressure drop vs. velocity
diagram; effect of temperature and pressure on fluidization; Geldart classification of particles; terminal
velocity of particles, Transport disengaging height; turbulent fluidization; pneumatic transport of solids;
fast fluidization; solid circulation systems; Voidage diagram; Mapping of regimes of fluidization.
UNIT IV
Bubbles in dense bed: Single rising bubbles; Davidson model for gas flow at bubbles; Evaluation of
models for gas flow at bubbles.
Bubbling Fluidized beds: Experimental findings; Estimation of bed Voidages; Physical models: simple
two phase model; K-L model.
UNIT V
High velocity Fluidization: Turbulent fluidized bed; Fast fluidization pressure drop in turbulent and
fast fluidization.
Solids Movement, Mixing, Segregation and staging: Vertical movement of solids; Horizontal
movement of solids; Staging of fluidized beds.
Gas Dispersion and Gas interchange in Bubbling Beds: Dispersion of gas in beds; Gas interchange
between bubble and emulsion; Estimation of gas interchange coefficients.
Text Books:
1. Fluidization Engineering by Kunii, Diazo and Octave Levenspiel, John Wiley & Sons
Inc, New York, 1991.
2. Fluidazation Engineering by J.R. Howard, Adam Heilgar
Codes/Books : Nil
87

3 1 3
(13A08707) FERTILIZER TECHNOLOGY
(Elective-II)
Course Objective:
To familiarize with different types of fertilizers, their manufacturing processes. To study the
applications of various fertilizers
Learning Outcome:
Student will understand the importance of fertilizer for plant growth and its manufacturing processes
UNIT I
Source of nitrogen and hydrogen, steam reformation of hydrocarbons, coal gasification process, partial
oxidation of fuel oils. Gas purification, high and low temperature shift conversion, CO removal
processes, methanation.
UNIT II
Manufacture of ammonia, ammonia synthesis by various processes, by product ammonia recovery by
direct and indirect methods
UNIT III
Manufacture of nitric acid and production of urea, urea once through, total and partial recycle processes
prilling. Manufacture of other nitrogenous fertilizer such as ammonium sulfate, calcium ammonium
nitrate, ammonium chloride etc granulation techniques.
UNIT IV
Phosphatic fertilizers, single and triple super phosphate, manufacture and production of ammonium
phosphate and nitro phosphates, manufacture of phosphoric acid. Potassium fertilizers, mixed and
compound fertilizers, liquid fertilizers and biofertilizers
UNIT V
Indian fertilizer industry, production economics and future plans, fertilizer application techniques for
different soils, controlled release fertilizers.
Text Books:
1. Chemistry and technology of fertilizers by V.Seucheli, Reinhold 1960/
2. Ammonia by Slack A.V. Marcel Dekker, 1973.
Reference Books:
1. Out lines of chemical technology by CE. Dryden
2. Manual of fertilizer processing by F.T.Nielsson, Dekker 1987
Codes/Books : Nil
88
3 1 3
(13A08708) COMPUTATIONAL FLUID DYNAMICS
(Elective-II)
Course Objective:
This subject deals with different mathematical methods like finite difference techniques to solve Navier -
Stokes equations & other fluid flow problems
Learning Outcome:
The student will apply the principles of fluid dynamics to solve different problems of the industry
UNIT I
Introduction - Finite difference methods- finite element method - finite volume method- Treatment of
boundary conditions- Governing differential equations. Finite difference methods - Taylors series -
Errors associated with FDE- FDE formulation for steady state heat transfer problems
UNIT II
Cartesian, cylindrical and spherical coordinate systems- boundary conditions- Un steady state heat
conduction Explicit Method - Stability criteria - Implicit Method - Crank Nickolson method - 2-D FDE
formulation ADI- ADE. Finite volume method - Generalized differential equation, Basic rules for
control volume approach, Source term linearization, boundary conditions. Un-steady state one, two,
three dimensional heat conduction
UNIT III
convection and diffusion, different methods i.e., upwind scheme, Exponential scheme, Hybrid scheme,
power law scheme, calculation of flow field, staggered grid method, pressure and velocity corrections,
SIMPLE Algorithms & SIMPLER (revised algorithm). Solution methods of elliptical, parabolic and
hyperbolic partial differential equations in fluid mechanics - Burgers equation.
UNIT IV
Formulations for incompressible viscous flows - vortex methods -pressure correction methods.
UNIT V
Treatment of compressible flows- potential equation, Navier - Stokes equation - flow field dependent
variation methods, boundary conditions. Linear fluid flow problems, 2-I) and 3- 1) fluid flow problems.
Text Books:
1. Numerical heat transfer and fluid flow - S.V. Patankar
2. Computational Fluid Dynamics, T.J. Chung, Cambridge University
3. Text Book of Fluid Dynamics, Frank Chorlton, CBS Publishers
Codes/Books : Nil
89
B.Tech. IV- I Sem. L C

3 2
(13A08709) PROCESS EQUIPMENT DESIGN AND DRAWING LAB
Course Objective:
To make the student familiar with design and drawing aspects of chemical processes equipments.
Learning Outcome:
Student will able to understand the design and drawing of various chemical equipments like heat
exchanger, distillation columns, reactors, open vessels, etc.
1. Drawing of flow sheet symbols.
2. Drawing of instrumentation symbols.
3. Drawing of instrumentation diagrams.
4. Mechanical aspects chemical equipment design and drawing of following equipment.
a) Double pipe heat exchanger
b) Shell and tube heat exchanger
c) Evaporator
d) Distillation column
e) Batch reactor.
Text Books:
1. Process Equipment Design by M. V. Joshi

2. Chemical Process Equipment Design and Drawing, S.C. Maidargi, PHI, 2013
Reference Books:
1. Process Equipment Design by Brownell and Young
2. Chemical Process Equipment Design by Bhattacharya
3. Process Equipment Design by Wallas
Pre-requisite: Chemical Process equipment design
90
B.Tech. IV- I Sem. L C

3 2
(13A08710) PROCESS SIMULATION LAB

Course Objective:
To make the student familiar with softwares and simulation of chemical processes equipments.
Learning Outcome:
Student will gain knowledge how to represent the physical problem in mathematical relation and will
also understand the solution to the problem.
The following experiments have to be conducted using C/C++/ Simulink and MATLAB
1. Gravity Flow tank.

2. Three CSTRs in series open loop
3. Three CSTRs in series Closed loop
4. Non isothermal CSTR
5. Binary Distillation column ( Also by using ASPEN )
6. Batch Reactor isothermal; Batch reactor non isothermal closed loop
7. Isothermal batch reactor open loop
8. Heat Exchanger- Double pipe, Shell and Tube (Counter, Parallel)
9. Interacting System- two tank liquid level
10. Non interacting system-two tank liquid level
11. Plug flow reactor ( Also by using ASPEN )
12. Bubble point calculations
13. Dew point calculations
14. Using ASPEN Software simulating a flow sheet of a simple process
Text Books:
1. C++ and MATLAB for Chemical Engineers
2. Process Simulation and Control Using ASPEN by Jana, PHI Learning Pvt Limited, New Delhi,
2011
91
B.Tech. IV- II Sem. Th Tu C

3 1 3
(13A08801) BIOCHEMICAL ENGINEERING
Course Objective:
To study the introductory aspects of microbiology, enzymes, growth kinetics and bioreactor design.
Learning Outcome:
This course will help the students to understand and apply the principles of biochemical engineering in
analysis and design of industrial biochemical processes.
UNIT I
Introduction to microbiology: Biophysics and the cell doctrine, the structure of cells, important cell
types, from nucleotides to RNA and DNA, amino acids into proteins. Kinetics of enzyme catalyzed
reaction: the enzyme substrate complex and enzyme action, simple enzyme kinetics with one and two
substrates. Media and bioreactor sterilization, thermal death of micro organism, design of sterilizing
equipment-sterilization and continuous sterilization.
UNIT II
Immobilized enzyme technology: enzyme immobilization, industrial processes, utilization and
regeneration of cofactors. Immobilized enzyme kinetics: effect of external mass transfer resistance,
analysis of intraparticle diffusion and reaction.
Kinetics of cellular growth in batch and continuous culture, models for cellular growth unstructured,
structured and cybernetic models. Thermal death kinetics of cells and spores
UNIT III
Introduction to metabolic pathways, biosynthesis, transport across cell membranes, end products of
metabolism, stoichiometry of cell growth and product formation.
Design and analysis of biological reactors: batch reactors, fed-batch reactors, enzyme catalyzed
reactions in CSTR, CSTR reactors with recycle and cell growth, ideal plug flow reactors. Fermentation
technology: medium formulation, design and operation of a typical aseptic, aerobic fermentation
process.
UNIT IV
Transport phenomena in bioprocess systems: Gas-liquid mass transfer in cellular systems, determination
of oxygen transfer rates, overall kLa estimates and power requirements for sparged and agitated vessels,
scaling of mass transfer equipment, heat transfer.
UNIT V
Downstream processing: Strategies to recover and purify products; separation of insoluble products-
filtration and centrifugation; cell disruption-mechanical and non-mechanical methods; separation of
soluble products: liquid-liquid extractions, membrane separation (dialysis, ultra filtration and reverse
osmosis), chromatographic separation-gel permeation chromatography, electrophoresis, final steps in
purification crystallization and drying.
Text Books:
1. Biochemical Engineering Fundamentals, 2nd ed., J.E. Bailey and D.F. Ollis, McGraw-Hill, New York,
1987.
2. Bioprocess Engineering, 2nd ed., M. L. Shuler and F. Kargi, PHI Learning Pvt. Ltd, New Delhi, 2009.
Reference Books:
1. Biochemical Engineering, J. M. Lee, Prentice-Hall, New Jersey 1992.
2. Fundamentals of Biochemical Engineering, A.V.N. Swamy, B.S. Publications, 2007.
92

3 1 3
(13A08802) INDUSTRIAL POLLUTION CONTROL ENGINEERING

Course Objective:
To expose the students to various industrial air, water and solid pollution problems and their abatement
techniques.
Learning Outcome:
The student will be able get the knowledge on different types of pollution caused by industries, solid and
hazard waste management.
UNIT I
Types of emissions from chemical industries and effects of environment, environment legislation, Type
of pollution and their sources, Effluent guidelines and standards.
Characterization of effluent streams, oxygen demands and their determination (BOD, COD, and TOC),
Oxygen sag curve, BOD curve mathematical, controlling of BOD curve, self purification of running
streams, sources and characteristics of pollutants in fertilizer, paper and pulp industry, petroleum and
petroleum industry, Tannery Industry.
UNIT II
Methods of primary treatments: screening, sedimentation, flotation, neutralization, and methods of
tertiary treatment. A brief study of carbon absorption, ion exchange, reverse osmosis, ultra filtration,
chlorination, ozonation, treatment and disposal
UNIT III
Introduction to waste water treatment, biological treatment of wastewater, bacterial and bacterial growth
curve, aerobic processes, Activated sludge process, activated aerated lagoons and stabilization ponds,
Attached growth processes, trickling filters, rotary drum filters, anaerobic processes.
UNIT IV
Air pollution sampling and measurement: Types of pollutant and sampling and measurement, ambient
air sampling: collection of gaseous air pollutants, collection of particulate air pollutants. Stack
sampling: sampling system, particulate sampling, and gaseous sampling.
Air pollution control methods and equipments: Gravitational settling chambers, Cyclone separators,
fabric filters, ESP. Scrubbers: wet scrubbers, Centrifugal scrubbers, Venturi scrubbers.
UNIT V
Hazardous waste management: Nuclear wastes: health and environment effects, sources and disposal
methods. Chemical wastes: health and environmental effects, treatment and disposal: treatment and
disposal by industry, off site treatment and disposal, treatment practices in various countries.
Biomedical wastes: types of wastes and their control.
Text Books:
1. Environmental pollution and control engineering by Rao C. S. Wiley Eastern Limited, India,
1993.
2. Environmental Engineering, G.N. Pandey, G.C. Carney-Tata Mc.Graw Hill Ltd., 6th reprint, 2013.
Reference Books:
1. Pollution control in process industries by S.P. Mahajan TMH.,1985.
2. Waste water treatment by M.Narayana Rao and A.K.Datta,Oxford and IHB publ. New Delhi.
3. Air pollution control by P.Prathap mouli and N.Venkata subbayya. Divya Jyothi Prakashan,
Jodhpur.
Codes / Tables: -Nil-
93

3 1 3
(13A08803) TECHNOLOGY OF PHARMACEUTICALS AND FINE CHEMICALS
(Elective-III)
Course Objective:
To acquaint the student with the preparation and testing of pharmaceuticals and fine chemicals and
their industrial manufacture.
Learning Outcome:
The student will get an overview on the design, development and manufacturing of different
pharmaceuticals and fine chemicals.
UNIT I
A brief outline of grades of chemicals, sources of impurities in chemicals, principles (without going into
details of individual chemicals) of limit test for arsenic, lead, iron, chloride and sulfate in
Pharmaceuticals.
UNIT II
Outlines of Preparation, properties, uses and testing of the following Pharmaceuticals - sulfacetamide,
paracetamol, riboflavin, nicotinamide,
Outlines of Preparation, properties, uses and testing of the following fine chemicals - Methyl orange,
fluorescence, procaine hydrochloride, paramino salicylic acid, isonicatinic acid hydrazide.
UNIT III
Manufacture with flowsheets, properties uses and testing of the following Pharmaceuticals aspirin,
penicillin, calcium gluconate.
UNIT IV
Manufacture with flowsheets, properties uses and testing of the following ferric ammonium citrate,
pthallic anhydride and phenol flourobenzene process and benzene sulfate process, other processes in
outline only.
UNIT V
Tablet making and coating, granulation equipments
Preparation of capsules, extraction of crude drugs.
Sterilization: introduction, risk factor, methods of sterilization, heat (dry and moist), heating with
bactericide, filtration, gaseous sterilization and radiation sterilization, suitable example to be discussed.
Text Books:
1. Remingtons Pharmaceutical Science,16th ed, Mac publishing company, 1980.
2. Industrial Chemicals, 3rd ed., Faith, Kayes and Clark, John Wiley & Sons,. 1965.
Reference Books:
1. Blentlys Text Book of Pharmaceutical Chemistry, 8th ed, H A Rawlins, B Tindell and Box,. Oxford
University Press, London, 1977.
.
94
B.Tech. IV - II Sem. Th Tu C
3 1 3
(13A08804) INTERFACIAL ENGINEERING
Elective-III
(Qualitative Treatment only)
Course Objective:
To provide the knowledge on various types of surface forces like Interfacial and vander Waals forces
which play important role in the nano particles
Learning Outcome:
Student will understand about the various types of surface forces and their applications
UNIT I
Thermodynamics of surfaces: Introduction, surface energy and its consequences, Thermodynamics of
surfaces, The Gibbs adsorption equation. Thermodynamic behavior of small particles, Equilibrium
shape of a crystal, behavior of liquids in capillaries, homogeneous nucleation.
UNIT II
Limits of applicability of the Kelvin and Young-Laplace equations, Contact angle and wetting
behaviour, theoretical estimation of surface properties, contact angle hysteresis, measurements of
surface tension and contact angle: maximum bubble pressure method, drop weight method, ring method,
wilhelmy side method, pendant method, sessile drop or bubble method, flow methods, capillary waves
method.
UNIT III
van der Waals Forces: Introduction, van der Waals forces and their importance in colloid and surface
chemistry, molecular interactions and power laws, molecular origins and the microscopic implications
of van der Waals forces, van der Waals forces between large particles and over large distances.
Calculation of van der Waals forces between macroscopic bodies, theories of van der Waals forces
based on bulk properties, effect of the medium on the van der Waals attraction;
UNIT IV
The electrical Double Layer and Double-layer Interactions: Introduction, surface charges and electrical
double layer: background.The capacitor model of the double layer, the diffuse double layer: The Debye-
Huckel approximation, The Debye-Huckel approximation: results, the electrical double layer: Gouy-
Chapman theory, overlapping double layers and inter particle Repulsion, Not-Quite-Indifferent
electrolytes: stern adsorption.
UNIT V
Adsorption at Gas-Liquid Interfaces: Introduction, experimental and theoretical treatments of
adsorption: an overview, Thermodynamics of adsorption: Phenomenological Perspective,
Thermodynamics of adsorption: A statistical Perspective, Multi layer adsorption: The Brunauer-
Emmett-Teller Equation, energetic of adsorption, adsorption in porous solids.Wetting, Flotation and
Detergency: Introduction, Wetting, water repellency, Flotation, Detergency.
Text Books:
1. Foundations of Colloid Science by Robert J. Hunter, Oxford science Publications, Volume-I
2. Principles of Colloid and Surface Chemistry, Third edition, Revised and Expanded, By Paul C.
Hiemenz and Raj Rajagopalan.
3. Physical Chemistry of Sciences by Arthur Adamson.
Pre-requisites: ---Nil---
95

3 1 3
(13A08805) POLYMER TECHNOLOGY
(Elective-III)
Course Objective:
To understand the basic concepts of plastics and polymers. To study different types of polymerization.
To study the manufacture of different polymer products
Learning Outcome:
The student will learn about synthesis of various polymers and their processing to get particular shape.
UNIT I
Introduction; definitions: polymer& macro molecule, monomer, functionality, average functionality, co-
polymer, polymer blend., plastic and resin.
Classification of polymers: based on source, structure, applications, thermal behavior, mode of
polymerization.
Methods of polymerization: mass or Bulk polymerization process, solution polymerization process,
suspension polymerization process and emulsion polymerization method comparison of merits and
demerits of three methods.
UNIT II
Mechanism and kinetics of Addition or chain polymerization
a) Free radical addition polymerization
b) Ionic addition polymerizations
c) Coordination polymerization.
d) Coordination or step growth or condensation polymerization.
UNIT III
Measurement of molecular weight and size:
End group analysis, Colligative property measurement, light scattering, ultra centrifugation, solution
viscosity and molecular size and gel permeation chromatography, poly-electrolytes
Polymer structure and physical properties: The crystalline melting point, the glass transition
temperature, properties involving large deformations, properties involving small deformations, Property
requirements and polymer utilization.
UNIT IV
Degradation of polymers, Role of the following additives in the polymers:
Fillers and reinforcing fillers ii) Plasticizers iii) Lubricants iv) Antioxidants and UV stabilizers v)
Blowing agents vi)Coupling agents vii)Flame retardents viii) Inhibitors
Brief description of manufacture, properties and uses of:
i) Polyethylene (HDPE&LDPE), ii) Poly propylene iii) Polyvinylchloride iv) Polystyrene v) Polytetra
floroethylene vi) Polymethyl mehacrylate vii) Polyvinylacetate & Polyvinylalcohol.
UNIT V
Polymer Processing: Molding, Extrusion, other processing methods (calandering, casting, coating,
foaming, forming, laminating), multi-polymer systems and composites, additives and compounding.
Text Books:
1. Polymer science and technology, Joel R. Fried, Prentice Hall India
2. Textbook of polymer science, Bill meyer, F.W.Jr. (3rd ed.) John Wiley & sons 1984
Reference Books:
1. Introduction to plastics, J.H. Brison and C.C. Gosselin, Newnes, London 1968.
2. Polymeric Materials, C.C.Winding and G.D.Hiatt Mc Graw Hill Book Co. 1961
3. Polymer science by Gowarikar
Codes/Tables:---Nil---
96

3 1 3
(13A08806) DESIGN AND ANALYSIS OF EXPERIMENTS

(Elective-III)
Course Objective:
The objective of this course is to enable the student to learn the importance of design of experiments
and its obtaining maximum information about a process with a minimum experimental work.
Learning Outcome:
It gives knowledge on how to minimize the number of experiments when several parameters effecting
the given process.
UNIT I
Introduction to probability, probability laws, Bayes theorem. Probability distributions, parameters and
statistics.
Normal and t-distributions, central limit theorem, random sampling and declaration of independence
significance tests
UNIT II
Randomization and blocking with paired comparisons significance tests and confidence interval for
means, variances, proportions and frequencies.
UNIT III
Analysis of variance, experiments to compare k-treatment means, Two-way factorial designs, blocking,
Yates algorithm
UNIT IV
Fractional factorial designs at two levels, concept of design resolution, Simple modeling with least
squares (regression analysis), Matrix versions of normal equations
UNIT V
Mechanistic model building, Empirical and mechanistic models, model building process, model testing
with diagnostic parameters.
Text Books:
1. Statistics for experimenters by G.E.P. Box, William G. Hunter and J.S. Hunter, John Wiley & Sons.
Reference Books:
1. Design and analysis of experiments by D.C. Montgomery, 2nd edition John Wiley and sons,
NewYork (1984).
97

3 1 3
(13A08807) COMPUTER AIDED PROCESS DESIGN
(Elective-IV)
Course Objective:
To impart the basics of process design, flash calculations and optimization in process design.
To impart the knowledge of using simulation software for process design of chemical systems like
UniSim/Aspen Plus.
Learning Outcome:
Through the course the student is expected to learn:
Optimum design of chemical process equipments like flash drum, heat exchangers, evaporators,
absorbers, distillation column, multiphase reactors.
Knowledge of heat integration in process plants to reduce the energy costs.
UNIT I
Introduction to process design; General design considerations; Hierarchy of chemical process design;
Nature of process synthesis and analysis; Developing a conceptual design and flow sheet synthesis;
Optimum process design. Material and Energy balance, Introduction to special software for steady state
and dynamic simulation of chemical engineering systems UniSim Design/Aspen Plus
UNIT II
Use of computers for physical property evaluation, Thermodynamic properties of gases, Liquids and
binary mixtures, Methods of calculating vapour liquid equilibrium data for ideal and non- ideal mixture,
Bubble point and dew point calculations, Flash calculations. Design of multi phase Flash drum.
UNIT III
Design of Pipe lines, Filter press, Centrifuge, Cyclone. Computer aided design of heat exchanger
systems - double pipe and shell and tube heat exchangers; Computer aided design of evaporators -
design of single effect evaporator and multiple effect evaporator systems.
UNIT IV
Computer aided design of Absorption tower- both plate as well as packed type and extraction columns;
Computer aided design of bubble - cap distillation column.
Design of chemical reactors: Design of multiphase reactors - Fixed, fluidized, trickle bed, and slurry
reactors.
UNIT V
Pinch analysis; Heat integration of heat exchangers, Reactors, Distillation columns, Evaporators and
driers; Process change for improved heat integration; Heat and mass exchange networks and network
design. Applications of simulation software in process design (UniSim/ Aspen).
Text Books:
1. James M. Douglas Conceptual Design of Chemical Processes, McGraw Hill, New York, 1988.
2. B.C. Bhattacharyya and C.M. Narayanan, Computer Aided Design of Chemical Process
Equipment", 1st Edtn., New Central Book Agency (P) Ltd., New Delhi, 1992.
Reference Books:
1. Douglas Erwin P E,Industrial Chemical Process Design, McGraw hill.
2. Brownel and Young, Process Equipment Design .Wiley (1968).
3. G.F. Froment, K.B. Bischoff, "Chemical Reactor Analysis and Design", 2nd ed., John Wiley, New
York, 1990.
98

3 1 3
(13A08808) FOOD PROCESSING TECHNOLOGY

(Elective-IV)
Course Objective:
To teach the student about different unit operations involved in the food processing industry.
Learning Outcome:
The student will enable to learn microwave heating and preservation methods and strategies in food
technology.
UNIT I
Food process engineering - Fundamentals: Fundamentals of food process engineering, application of
quantitative methods of material and energy balances in food engineering practices.
UNIT II
Unit Operations in food industries: Fluid flow, thermal process calculations, refrigeration,
evaporation and dehydration operations in food processing.
UNIT III
Microwave heating: Theory of microwave heating, microwave properties of foods, comparison of
microwave and conventional heating, benefits of microwave heating, applications in food processing,
microwave heating equipment, hazards of microwave heating.
UNIT IV
Mechanical Operations in food processing: Conversion operations, Size reduction and screening of
solids, mixing and emulsification, filtration and membrane separation, centrifugation, crystallization,
extraction.
UNIT V
Preservation operations: Preservation methods & Strategies, Thermal Methods, Nabla Factor
Sterilization Types Pasteurization Dehydro freezing Irradiation Dosimetry Transport of food &
Preservation strategies Cheap and applicable everywhere.
Text Books:
1. R. T. Toledo, "Fundamentals of Food Process Engineering", AVI Publishing Co., 1980.
2. R. Angold,G.Beech and J.Taggart, " Food Biotechnology", Cambridge University Press, 1989.
3. Fundamentals of Food Engineering, D G Rao, PHI, New Delhi, 2012.
Reference Books:
1. J. M. Jackson and B. M. Shinn, "Fundamentals of Food Canning Technology", AVI Publishing Co.,
1978.
2. J. G. Bernnan, J. R. Butters, N. D. Cowell and A.E.V.Lilley, "Food Engineering Operations", 2nd Edn.,
Applied Science, 1976.
99

3 1 3
(13A08809) ENTERPRENEURSHIP DEVELOPMENT
(Elective-IV)
Course Objective:
It gets exposure to business management principles
Learning Outcome :
This course will provide the knowledge to become entrepreneur.
UNIT I
Introduction to entrepreneurship: Definition of entrepreneur, Entrepreneurial Traits, Entrepreneur vs.
Manager, Entrepreneur vs Intrapreneur. The Entrepreneurial decision process. Role of Entrepreneurship
in Economic Development, Ethics and social responsibility of Entrepreneurs. Opportunities for
Entrepreneurs in India and abroad. Woman as Entrepreneur.
UNIT II
Creating and starting the Venture: Sources of new Ideas, Methods of generating Ideas, Creating
problem solving, product planning and development process.
The Business Plan: Nature and scope of business plan , Writing Business Plan ,Evaluating Business
plans, Using and implementing business plans. Marketing plan, financial plan and the organizational
plan, Launching formalities
UNIT III
Financing and Managing the new venture: Sources of capital, Record keeping, recruitment,
motivating and leading teams, financial controls, Marketing and sales controls. E-commerce and
Entrepreneurship, internet advertising.
New venture Expansion Strategies and Issues: Features and evaluation of joint ventures ,
acquisitions, merges, franchising. Public issues, right issues, bonus issues and stock splits.
UNIT IV
Choosing location and layout. Production and Marketing Management: Thrust of production
management, Selection of production techniques, plant utilization and maintenance, Designing the work
place, Inventory control, material handling and quality control, Marketing functions, market
segmentation, market research and channels of distribution, Sales promotion and product pricing.
UNIT V
Global aspects of Entrepreneurship.
Text Books :
1. Robert Hisrich, & Michael Peters: Entrepreneurship, TMH,5th Edition.
2. Dollinger: Entrepreneurship, 4/e , Pearson, 2004.
Reference Books:
1. Vasant Desai:Dynamics of Entrepreneurial Development and management,Himalaya publishing
house, 2004.
2. Harvard Business Review on Entrepreneurship. HBR paper back, 1999.
3. Robert J. calvin : Entrepreneurial management, TMH, 2004 .
4. Gurmeet Naroola: The Entrepreneurial Connection,TMH,2001.
5. BOLton &Thompson: Entrepreneurs-Talent, Temperament, Technique, Butterworth
Heinemann,2001.
6. Agarwal :Indian Economy, Wishwa Prakashan 2005.
100
7. Dutt& Sundaram:Indian Economy.s.chand,2005.
8. Srivastava: Industrial Relations &Labour laws , Vikas,2005.
9. Aruna Kaulgud:Entrepreneurship Management by, Vikas publishing house,2003.
10. Thomos W.zimmerer & Norman M. Scarborough: Essential of Entrepreneurship and small business
management,PHI,4/e,2005.
11. Mary coulter: Entrepreneurship in Action,PHI,2/e.2005.
12. Kaplan: Patterns of Entrepreneurship ,Willey,2005.
13. ND Kapoor:Industrial Law, Sultan chand &Sons,2005.
101

3 1 3
(13A0810) CORROSION ENGINEERING
(Elective-IV)
Course Objective:
To acquaint the student with the techniques of identification and testing of different forms of corrosion
encountered in process industry and the various methods of prevention of corrosion.
Learning Outcome:
The course will provide the knowledge about various types of corrosion and its prevention techniques.
UNIT I
Introduction: Corrosion principles, electro-chemical aspects, environmental effects, metallurgical and
other aspects.
UNIT II
Forms of corrosion: uniform attack, galvanic, crevice, pitting, Inter granular, selective, leaching, erosion
and stress corrosion.
UNIT III
Corrosion testing procedures, Corrosion prevention: Material, alteration of environment.
Design cathodic and anodic protection, coating.
UNIT IV
Modern Theory, Principles, thermodynamics and electrode kinetics
UNIT V
Predicting corrosion behavior, corrosion prevention and rate measurement.
Text Books:
1. Corrosion engineering by M.G. Fontana, McGraw Hill, 3rd Ed.
Reference Books:
1. Handbook of corrosion by Uhlig.
102
B.Tech. IV- II Sem.
(13A08812) PROJECT WORK
The project work may consist of any one of the following works.
a) The project work should consist of a comprehensive design project of a chemical plant in the form of
a report with the following chapters.
1. Introduction
2. Physical and Chemical Properties and uses
3. Literature survey for different processes
4. Selection of the process
5. Material and Energy balances
6. Specific equipment design, (Process as well as mechanical design with drawing), including
computer programs where possible, of Heat Transfer equipments or separation equipments or
reactors
7. General equipment Specifications
8. Plant location and layout
9. Materials of construction
10.Health and Safety factors
11.Preliminary cost estimation
12.Bibliography
b) Modelling & Simulation of any Chemical Engineering Process
c) Any experimental work with physical interpretations
103

B.tech. - Chemical Engg - R13 - Syllabus

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JAWAHARLAL NEHRU TECHNOLOGICAL UNIVERSITY ANANTAPUR

(Established by Govt. of A.P., Act. No. 30 of 2008)

Course Structure & Syllabus for B.Tech. (Regular)

Th = Theory; Tu = Tutorial, Drg= Drawing & Lab = Laboratory:

* Engineering Drawing will have University External Exam.

Course Code Theory Tu / Lab

Course code Theory Tu / Lab

S.No Course code Subject Theory Tu / Lab Credits

B.Tech. III - II Semester

S.No Course code Subject Theory Tu / Lab Credits

(13A52101) COMMUNICATIVE ENGLISH

(13A01101) ENGINEERING MECHANICS

B.Tech. I Year Th Drg C

(13A12102) PROGRAMMING IN C & DATA STRUCTURES LAB

Common to All Branches

ENGINEERING PHYSICS LAB

Any 10 of the following experiments has to be performed:

ENGINEERING CHEMISTRY LAB

1. TRADES FOR EXERCISES:

2. TRADES FOR DEMONSTRATION:

Preparing your Computer ( 5 weeks)

Networking and Internet (4 weeks)

(13A52102) ENGLISH LANGUAGE COMMUNICATION SKILLS (ELCS) LAB

System Requirement (Hardware component):

PART A ELECTRICAL ENGINEERING

UNIT III 3 PHASE AC MACHINES

(13A08302) PHYSICAL & ANALYTICAL CHEMISTRY

(13A08303) CHEMICAL PROCESS CALCULATIONS

(13A08304) CHEMICAL ENGINEERING FLUID MECHANICS LAB

1. Identification of laminar and turbulent flows

I. PHYSICAL CHEMISTRY LAB:

1. Determination of specific rotation of substance by polarimeter.

II. ORGANIC CHEMISTRY LAB:

III. PREPARATIONS: Aspririn, Paracetamol, Acetanilide and Azodye

(13A08401) PROCESS HEAT TRANSFER

Codes/tables: Steam tables should be provided at the time of examination.

(13A08403) ORGANIC CHEMISTRY

Codes/Tables: Compressibility chart should be provided during examination

(13A08405) MECHANICAL UNIT OPERATIONS

(13A08406) PROCESS HEAT TRANSFER LAB

1. Determination of total thermal resistance and thermal conductivity of composite wall.

2. Determination of thermal conductivity of a metal rod.

3. Determination of natural convective heat transfer coefficient for a vertical tube.

4. Determination of critical heat flux point for pool boiling of water.

6. Determination of overall heat transfer coefficient in Double pipe heat exchanger.

10. Determination of Stefan Boltzmann constant.

11. Determination of emissivity of a given plate at various temperatures.

12. Determination of radiation constant of a given surface.

(13A52301) HUMAN VALUES & PROFESSIONAL ETHICS (AUDIT COURSE)

B.Tech. III-I Sem. Th Tu C

(13A08501) ENERGY ENGINEERING

B.Tech. III - I Sem. Th Tu C

B.Tech. III-I Sem. Th Tu C

(13A08503) PHASE AND CHEMICAL EQUILIBRIA

Pre-requisite: Chemical Engineering Thermodynamics

B.Tech. III-I Sem. Th Tu C

B.Tech. III-I Sem. Th Tu C

Codes/Tables: Humidity Charts, Unsteady Diffusion Plots.

B.Tech. III - I Sem. Th Tu C

B.Tech. III - I Sem. L C

1. Estimation of chemical and physical parameters of Ground and Surface water:

B.Tech. III- I Sem. L C

(13A08507) PROCESS DYNAMICS AND CONTROL LAB

1. Dynamics of a single capacitance system subjected to impulse change