Procedure

Standard Preparation

About 5mg of naphthalene is weighed and dissolved in a small amount of

dichloromethane in a beaker. It is then transferred into a 50mL volumetric flask
and diluted to the calibrated mark with dichloromethane. The mixture is injected
into a small vial by usage of syringe with 0.5 millipore filter attached to it.

Sample Preparation

There are two sample used; 2T oil (Shell oil) and lubricant oil (Petronas oil). Each
sample is prepared from each stock solution about 10mg of respective oils which
are dissolved in dichloromethane in 100mL volumetric flask (100ppm solution).
From these stock solutions, 1ppm solution is prepared by pipetting 0.5mL of each
stock into 50mL volumetric flask and filled to the calibrated mark with
dichloromethane solution. Again, they are injected into small vial by the usage of
syringe with millipore filter attached to it.