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H O S T E D BY
Gulf Organisation for Research and Development
Review Article
Abstract
High demand of natural resources due to rapid urbanization and the disposal problem of agricultural wastes in developed countries
have created opportunities for use of agro-waste in the construction industry. Many agricultural waste materials are already used in con-
crete as replacement alternatives for cement, ne aggregate, coarse aggregate and reinforcing materials. This paper reviews some of the
agro-waste materials, which are used as a partial replacement of ne aggregate in concrete. Dierent properties of fresh and hardened
concrete, their durability and thermal conductivity when admixed with agro-wastes are reviewed. Agro-waste used in self-compacting
concrete and mortar are also reviewed and their properties are compared. It has been seen that the agro-waste concrete containing
groundnut shell, oyster shell, cork, rice husk ash and tobacco waste showed better workability than their counterparts did. Agro-
waste concrete containing bagasse ash, sawdust ash and oyster shell achieved their required strength by 20% of replacement as ne aggre-
gate, which were maximum among all agro-waste type concrete. Close relations were predicted among compressive strength, exural
strength, tensile strength, ultrasonic pulse velocity and elastic modulus of agro-waste concrete. Addition of bagasse ash as ne aggregate
in mortar increased the resistance of chloride penetration whereas inclusion of cork in mortar showed better thermal resistance and
improved cyclic performance. After the review, it is of considerable nding that more research is deserved on all ne aggregates replacing
agro-waste materials, which can give more certainty on their utilization in concrete.
2016 Published by Elsevier B.V. on behalf of The Gulf Organisation for Research and Development.
Contents
1. Introduction . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 00
1.1. Agricultural wastes used as a fine aggregate replacement in concrete . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 00
1.1.1. Sugarcane bagasse ash (SCBA) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 00
Corresponding author.
E-mail addresses: jkumar.prusty@gmail.com (J.K. Prusty), litusanjay@yahoo.com (S.K. Patro), sunil.basarkar@itdcem.co.in (S.S. Basarkar).
Peer review under responsibility of The Gulf Organisation for Research and Development.
http://dx.doi.org/10.1016/j.ijsbe.2016.06.003
2212-6090/ 2016 Published by Elsevier B.V. on behalf of The Gulf Organisation for Research and Development.
Please cite this article in press as: Prusty, J.K. et al. Concrete using agro-waste as ne aggregate for sustainable built environment A review. Inter-
national Journal of Sustainable Built Environment (2016), http://dx.doi.org/10.1016/j.ijsbe.2016.06.003
2 J.K. Prusty et al. / International Journal of Sustainable Built Environment xxx (2016) xxxxxx
Please cite this article in press as: Prusty, J.K. et al. Concrete using agro-waste as ne aggregate for sustainable built environment A review. Inter-
national Journal of Sustainable Built Environment (2016), http://dx.doi.org/10.1016/j.ijsbe.2016.06.003
J.K. Prusty et al. / International Journal of Sustainable Built Environment xxx (2016) xxxxxx 3
The current Green Building Rating (GBR) systems eval- as coarse aggregate in coastal regions. Sawdust is generated
uate the sustainability of buildings according to various from mechanical processing of raw wood from saw mill
categories of which the construction material is one such industry. These are dried by leaving in sun and sieved prop-
category in most of the systems. Issues like emission of car- erly before using in concrete (Oyedepo et al., 2014). Cork
bon dioxide, use of energy, water, aggregates, llers and and tobacco wastes are collected and processed from cork
demolition waste in concrete look less compatible with oak trees and cigarette making industries which were used
environmental requirement of a modern sustainable con- as ne aggregate replacement in concrete. The shape, size
struction industry. At the same time, concrete made using and availability of mentioned agro-wastes are discussed
agricultural wastes has shown better thermal property in below. The purpose of this review is to study the properties
research which can result in sustainability points in the such as workability, mechanical properties, durability,
energy and atmosphere category of the LEED rating sys- thermal conductivity of agricultural wastes used as a par-
tem (Shagh et al., 2014). tial replacement of ne aggregate in concrete.
1.1. Agricultural wastes used as a fine aggregate replacement 1.1.1. Sugarcane bagasse ash (SCBA)
in concrete The brous residue (about 4045%) of sugarcane after
crushing and extraction of its juice is known as bagasse
The Agricultural wastes used as ne aggregate in con- (Loh et al., 2013). The bagasses are reused as fuel for heat
crete are sugarcane bagasse ash, groundnut shell, oyster generation which leaves behind 810% of ash, known as sug-
shell, sawdust, giant reed ash, rice husk ash, cork and arcane bagasse ash (SCBA) Modani and Vyawahare, 2013.
tobacco waste. The major dierences of these agro-wastes Sugarcane bagasse consists of approximately 50% of cellu-
are the place from where they collected and the processes lose, 25% of hemicellulose and 25% of lignin (Modani and
to convert into a ne aggregate. It can be observed that Vyawahare, 2013). Rukzon and Chindaprasirt (2012)
sugarcane, giant reed, and rice husk are produced world- reviewed that a lot of sugarcane bagasse from the sugar fac-
wide and they have a similar type of processing, those are tory is accessible in Thailand. Sugarcane bagasse is partly
burnt to convert into sugarcane bagasse ash, giant reed utilized as fuel in sugar plant but the rest is treated as waste
ash and rice husk ash. These are used as partial replace- and unutilized. As production of sugar cane is more than
ment of ne aggregate which provide additional pozzolanic 1500 million tons in the world and in India, about 10 million
property in concrete. Groundnut shells are crushed in mill tons of sugarcane bagasse ash are treated as a waste material,
to convert into ne aggregate prior to use in concrete. Oys- it can therefore be advantageous to use it as a ne aggregate
ter shells are the sea shells generally available in coastal replacement in concrete to mitigate the disposal problem as
areas. These are used as partial replacement of ne as well well as to minimize the use of natural aggregates (Modani
Please cite this article in press as: Prusty, J.K. et al. Concrete using agro-waste as ne aggregate for sustainable built environment A review. Inter-
national Journal of Sustainable Built Environment (2016), http://dx.doi.org/10.1016/j.ijsbe.2016.06.003
4 J.K. Prusty et al. / International Journal of Sustainable Built Environment xxx (2016) xxxxxx
and Vyawahare, 2013). Fig. 2 shows the raw sugarcane sheet materials (Akindapo et al., 2015), sandcrete blocks
bagasse and the sugarcane bagasse ash which is used as ne (Mahmoud et al., 2012), as cement replacement (Olutoge
aggregate replacement in concrete. Sales and Lima (2010) et al., 2013; Buari et al., 2013; Kanagalakshmi et al.,
analysed the SCBA samples to determine the crystallinity 2015) and as ne aggregate replacement (Sada et al.,
by X-ray diractometry, leachability and particle morphol- 2013; Tata et al., 2015) in concrete. Fig. 3 shows the
ogy by scanning electron microscopy (SEM). The X-ray groundnut and its crushed shell which can be used as ne
diractometry test result revealed the absence of an amor- aggregate in concrete.
phous halo in the diractograms (Sales and Lima, 2010).
Quartz appeared as the principal element of SCBA. The
SEM analysis revealed that the SCBA samples were com-
posed of grains with varied shapes and sizes up to 150 lm. 1.1.3. Oyster shell
Authors (Sales and Lima, 2010) suggested that these ndings Aquaculture is one of the key businesses in island
reinforce the hypothesis of using SCBA as a substitute for nations. The southwestern seaside territory of Taiwan pri-
ne aggregate which has binding properties. marily develops oysters. As per the information of shery
commercial enterprises, the oyster shell yield was
300,000 tons over the last ve years, which would initiate
1.1.2. Groundnut shell environmental pollution concerns (Kuo et al., 2013).
Groundnut shell can be found in large quantities as agri- Yang et al. (2010, 2005) stated the same problem created
cultural farm waste in Nigeria, producing up to 2.699 mil- by oyster shell in South Korea, can be solved by their uti-
lion metric tons per year (Sada et al., 2013). Groundnut lization in the construction industry. One of the most pop-
shell was rst planted in South Africa mainly Brazil and ular uses of oyster shell in construction industry
later spread to other part of America, Asia, and northwest- throughout history has been in its burnt form as lime
ern Argentina (Tata et al., 2015). The outer part of ground- known as quicklime. Recently researchers (Kuo et al.,
nut is called groundnut shell. Over a period of years, it is 2013; Yang et al., 2010, 2005) studied the properties of oys-
treated as a solid waste. Utilization of groundnut shell in ter shell based concrete using oyster shell as ne aggregate,
the construction industry is expected to solve the pollution which are discussed briey in following sections. Fig. 4
problem and increase the economic base of farmers, which shows the shape of the oyster shell used in concrete. Oyster
encourage them to increase the production (Sada et al., shell grows over the years and it is found in several sizes.
2013). Groundnut shell is already used for developing roof The shells are spiral in structure and having rough surface
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J.K. Prusty et al. / International Journal of Sustainable Built Environment xxx (2016) xxxxxx 5
texture. It should be crushed properly as per the code the preservation of natural ne aggregate. Fig. 5 shows the
requirement prior to use in concrete. shape of the sawdust which is treated as a waste material.
Many researchers tested the behaviour of sawdust ash in
1.1.4. Sawdust concrete and reported that sawdust possessed unique char-
Sawdust is the main component of particleboard. It has acteristics, which make it competitive among other con-
a variety of other practical uses including serving as mulch, struction materials (Mageswari and Vidivelli, 2009).
an alternative to clay cat litter, or as a fuel. It can present as
a hazardous material in manufacturing industry, in terms 1.1.5. Wild giant reed
of its ammability (Ganiron, 2014). The use of sawdust Giant reed is an aggressive wild agricultural species
for making lightweight concrete has received some atten- which can be found all over the world. It has hollow, rigid,
tion over the past years (Udoeyo and Dashibil, 2002). woody stalks which are nearly one inch in diameter and can
Mageswari and Vidivelli (2009) reported, that as a substitu- grow over 13 feet in height as shown in Fig. 6. Continuous
tion material for natural sand, sawdust ash might be the reduction of natural resources and at the same time the
right choice as ne aggregate in concrete. It can consider- environmental hazards posed by the disposal of several
ably reduce the dumping problem and simultaneously helps waste materials create an opportunity to use this waste
Fig. 5. Sawdust.
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6 J.K. Prusty et al. / International Journal of Sustainable Built Environment xxx (2016) xxxxxx
material in concrete (Ismail and Jaeel, 2014). Research reinforce ceramic cutting tools and aggregate replacement
work on the utilization of giant reed bres and giant reed in concrete in low-cost housing.
ash is reviewed in this paper.
1.1.7. Cork
1.1.6. Rice husk Cork is a renewable resource. It is a natural lightweight
Rice husk is one of the fundamental agrarian wastes cellular material separated from the bark of Cork Oak
obtained from the external covering of rice grains amid trees. Fig. 8 shows the processing of cork and its particle
the processing procedure. Fig. 7 shows the shape of the rice size. The worlds cork creation is evaluated at 340,000 tons
husk and its ash. The rice husk has no useful application per year from approximately 22,000 km2 of cork forests
and is treated as a waste material that creates the pollution and it is assessed that yearly, 68,00085,000 tons of cork
problem (Givi et al., 2010). Because of low nutrition prop- remains an under-utilized waste (Panesar and Shindman,
erty of rice husk, it is unsuitable and does not have edibility 2012). Variety of analysts utilized cork as a part of con-
yet in a few nations, it has been utilized generally as fuel for struction industry mainly in cement mortar because of its
rice plants and electric power plants as a compelling tech- unique composition and cell structure, which gives low
nique to reduce the volume of rice husk waste density, low thermal conductivity, good sound absorption
(Madandoust et al., 2011). Many researchers in the past and water resistance (Panesar and Shindman, 2012).
had used rice husk ash as a cement replacement material Novoa et al. (2004) considered the low density and low
in concrete (Givi et al., 2010; Madandoust et al., 2011; stiness of cork and introduced it in a mortar formulation
Zaid and Ganiyat, 2009). After colossal researches Iam to diminish the material weight and brittleness respectively.
and Makul (2013) tested the properties of self- Cork also exhibited low strength and extensive compressive
compacting concrete using rice husk and limestone as a ne strain, prompting more energy absorbing material (Novoa
aggregate replacement. It was reported that use of rice husk et al., 2004).
ash in self-compacting concrete reduced the unit weight,
owability, porosity, water absorption, compressive 1.1.8. Tobacco waste
strength, ultrasonic pulse velocity and the cost. Shagh Large quantities of tobacco waste are produced annu-
et al. (2014) reported the use of rice husk as cement replac- ally by processing and cigarette making (Shagh et al.,
ing material, re making, litter material, marking the con- 2014). Fig. 9 shows the shape of tobacco waste used in con-
crete, board production, as silicon carbide whiskers to crete. Ozturk and Bayrakl (2005) carried out a study to
Please cite this article in press as: Prusty, J.K. et al. Concrete using agro-waste as ne aggregate for sustainable built environment A review. Inter-
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J.K. Prusty et al. / International Journal of Sustainable Built Environment xxx (2016) xxxxxx 7
120
sand [8]
GNS [8]
Percentage of Passing
90
WOS [15]
CORK [34]
60
Upper limit (ASTM
C33)
Lower limit (ASTM
30 C33)
Upper limit (BS 882)
Fig. 10. Sieve Analysis of sand (Sada et al., 2013), groundnut Shell (GNS) Sada et al., 2013, waste oyster shell (WOS) Kuo et al., 2013 and cork (Bras
et al., 2014).
determine the possible use of tobacco waste in concrete. The physical properties of sand, crushed granite and dif-
They tested dierent properties with varying percentage ferent agricultural waste which are used in agro-waste con-
replacement of tobacco waste and pumice. Based on den- crete are presented in Table 1. It can be observed that
sity, lightweight concretes are divided into three groups. properties such as specic gravity and neness modulus
Low density and low compressive strength which is used of agro-wastes were nearly similar or less than the range
in isolation, middle density and middle compressive of natural sand presented in that same table. Sales and
strength concretes used for briquette producing and the Lima (2010) reported that specic gravity (2.45), bulk den-
carrier lightweight concretes are used in constructing foun- sity (2040 kg/m3) and water absorption (0.88%) of SCBA
dations and supporting parts (Short et al., 1978; Bhatty met the requisites of Brazilian standards NM 52 (2004),
and Reid, 1989). Ozturk and Bayrakl (2005) found the NM 45 (2004) and NM 30 (2001) respectively. According
low density and compressive strength of tobacco waste to Shafana and Venkatasubramani (2014)s report, specic
which can be used as an isolation material in concrete. gravity and neness modulus of SCBA satised the guide-
All the material properties of tobacco waste are discussed lines of IS 2386 part-3 (Indian Standard, 1963) and part-1
in the following sections. (Indian Standard, 1963b) respectively. Bulk density of
GNS (254.55 kg/m3), SDA (1250 kg/m3) and WGR
2. Physical and chemical properties of agricultural wastes (535 kg/m3) is very much smaller than the range of sand
(14281744) which indicates that the agro-waste contains
The particle size distribution of sand and dierent agro- more voids in comparison to the conventional ne aggre-
waste used in concrete and mortar is illustrated in Fig. 10. gate and it can adversely aect the workability, strength
It can be seen that sand and groundnut shell follow the lim- and durability of the agro-based concrete or mortar. Water
its of particle size as per ASTM C33 standard (American absorption of GNS (1.61%) falls within the range of natu-
Society for Testing and Materials, 1978). Similarly, waste ral river sand (0.742.9%) however, water absorption of OS
oyster shell followed the limits of BS 882 (British ranging 2.97.66% which is higher than the range of natu-
Standard Institute, 1992). It can be observed that the over- ral aggregates as well as the other agro-wastes. Cork shows
all passing percentage of cork (Bras et al., 2014) was similar 0.1% of water absorption that indicates good water resis-
as that of sand and other materials. tance property.
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8
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Table 1
Physical properties of sand, granite and agricultural waste used as replacement of ne aggregate.
Properties Sand Crushed Granite SCBA1 GNS2 OS3 SDA5 WGR6 RHA4 Cork
Modani and Vyawahare Modani and Vyawahare Modani and Sada Kuo et al. Mageswari Ismail Iam and Panesar and
(2013), Rukzon and (2013), Rukzon and Vyawahare (2013), et al. (2013), and Vidivelli and Makul Shindman (2012),
Chindaprasirt (2012), Sada Chindaprasirt (2012), Shafana and (2013) Yang (2009) Jaeel (2013) Novoa et al. (2004),
et al. (2013), Kuo et al. Sada et al. (2013), Kuo Venkatasubramani et al. (2014) Bras et al. (2014),
(2013), Yang et al. (2010), et al. (2013), Yang et al. (2014), Shah et al. (2010), (2013), Moreira et al.
(2005), Mageswari and (2010), (2005), Mageswari (2014) (2005) (2014), Carvalho et al.
Vidivelli (2009), Ismail and and Vidivelli (2009), Iam (2013)
Jaeel (2014), Iam and and Makul (2013),
Makul (2013), Novoa et al. Shafana and
(2004), Bras et al. (2014), Venkatasubramani (2014),
(2013), Shafana and Shah et al. (2014)
Venkatasubramani (2014),
Shah et al. (2014)
Specic gravity 2.382.64 2.62.83 1.252.54 2.12.48 2.5 2.03
Fineness Modulus 2.213.44 5.967.52 1.422.12 22.8 1.78
Bulk Density (kg/m3) 14281744 13651744 8372040 254.55 1250 535 112.4
Water Absorption (%) 0.742.9 0.571.8 0.88 1.61 2.97.66 0.1
Moisture Content (%) 0.940.97 0.81
Silt Content (%) 5.713
Flakiness index (%) 1
Elongation index (%) 9.61
1
SCBA-Sugarcane Bagasse Ash.
2
GNS-Groundnut Shell.
3
OS-Oyster Shell.
4
RHA-Rice Husk Ash.
5
SDA-Saw Dust.
6
WRG-Wild Giant Reed.
J.K. Prusty et al. / International Journal of Sustainable Built Environment xxx (2016) xxxxxx 9
Table 2
Chemical properties of agro-waste.
Chemical Sugarcane Bagasse ash Oyster Shell Saw Dust Rice Husk Tobacco Waste
Compounds Modani and Vyawahare (2013), Shafana and Kuo et al. (2013), Mageswari and Ash Ozturk and
(%) Venkatasubramani (2014), Shah et al. (2014) Yang et al. (2005) Vidivelli (2009) Iam and Bayrakl (2005)
Makul (2013)
SiO2 62.4390 213.28 65.3 89.87
Al2O3 2.854.28 0.5 4 0.14
Fe2O3 4.766.98 0.2 2.23 0.94
CaO 111.8 51.0677.81 9.6 0.49
MgO 0.073.61 0.51 5.8
SO3 1.48 0.061.09
K2O 3.193.53 0.060.51 0.11 2.16
P2O5 0.232 0.43
Fe 24 0.46
N 0.20.3
Na2O 0.58 0.07 0.25
TiO2 0.02
Mn2O3 0.02
P2O5 0.18
SrO 0.09
K2+Na2 510
Cl 2.92
MnO 0.01
SO2 0.45
Zn 0.0098
Mn 0.026
Cu 0.0021
Ca 5.72
Mg 0.8
K 1.03
Na 0.09
P 0.2
Organic matter 66.21
LOI 1.864.73 44.16 4.81
The chemical properties of agricultural wastes are pre- of ne aggregate and water-cement ratio. Dierent codes
sented in Table 2. It can be observed that the chemical such as IS 10262: 2009 (Indian Standard, 2009), ACI 211.1
composition of SCBA, RHA and SD is dominated by sili- (American Concrete Institute, 1991), KCI (Korea
con dioxide (SiO2). The sum of SiO2, Al2O3 and Fe2O3 of Concrete Institute, 1999), AIK (Korea Concrete Institute
SCBA, RHA and SD is higher than 70%, the required and Architectural Institute of Korea, 1999), and CSA
chemical composition of natural pozzolana as per ASTM A23.3-09 (Canadian Standards Association, 2009) have
C618 (American Society for Testing and Materials, 2005). been followed by dierent researchers (Modani and
Thus, the utilization of these mentioned agro-wastes as ne Vyawahare, 2013; Sales and Lima, 2010; Yang et al., 2010;
aggregate replacement could help in the hydration process Panesar and Shindman, 2012; Shafana and
of the agro-based concrete or mortar. Oyster shell (OS) dif- Venkatasubramani, 2014; Shah et al., 2014) for mix propor-
fers from the other agro-wastes by its CaO content (51.06 tioning the agro-waste concrete. Researchers (Modani and
77.81%) and LOI (44.16%). The ASTM C618 standard Vyawahare, 2013; Shafana and Venkatasubramani, 2014;
(American Society for Testing and Materials, 2005) and Shah et al., 2014) targeted dierent strengths of M20, M25
Brazilian standard (NBR 12653) Brazilian Standard, 1992 and M30 by replacing SCBA of maximum 50% of ne aggre-
limits the LOI content of 6%. It can be observed that gate in concrete. Sales and Lima (Sales and Lima, 2010) have
SCBA and RHA satisfy the limitation of mentioned stan- used three dierent types of cement, sulphate resisting Port-
dards, however oyster shell does not. Tobacco waste con- land cement, blast furnace slag cement and slag modied
tains the highest percentage of organic matter (66.21). Portland cement to achieve three dierent target strengths.
They have designed the concrete with SCBA based on the
3. Mix proportion of agro-waste based concrete ABCP (Brazilian Portland cement association) method
which was adopted from ACI method (American Concrete
Selected mix proportions of agro-waste based concrete Institute, 1991). Yang et al. (2010) reported that substitution
are presented in Table 3. Researchers have attempted dier- ratio of oyster shell was determined considering chloride ion
ent target strengths ranging from 20 MPa to 51.6 MPa using amounts contained in OS to satisfy the requirement of the
dierent cement types, agro-waste types, replacement levels Korea Concrete Institute (KCI) Korea Concrete Institute,
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national Journal of Sustainable Built Environment (2016), http://dx.doi.org/10.1016/j.ijsbe.2016.06.003
10 J.K. Prusty et al. / International Journal of Sustainable Built Environment xxx (2016) xxxxxx
0.530.55
0.520.54
0.430.45
0.520.54
w/c ratio
Concrete Institute and Architectural Institute of Korea,
0.45
0.45
0.55
0.4
0.5
0.4
0.4
1999 codes. Panesar and Shindman (2012) followed the
Canadian standard (CSA 23.2-09 Canadian Standards
SP* (%)
0.82
0.8
They replaced the cork from 0 to 20% of ne aggregate with
a w/c ratio of 0.4. They have used superplasticizer of 0.82%
0, 10, 20
0, 10, 20
0, 10, 20
0, 30, 50
Groundnut shell
OPC
OPC
30 MPa
M20
M30
M30
M30
M25
IS 10262: 2009
IS 10262: 2009
Selected mix proportion of agro-waste based concrete.
Author
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J.K. Prusty et al. / International Journal of Sustainable Built Environment xxx (2016) xxxxxx 11
Table 4
Slump value of agro-waste concrete in dierent percentage of replacement.
Percentage of Bagasse ash Groundnut Oyster shell Giant reed ash Giant reed bre Tobacco waste
replacement Modani and Vyawahare shell Yang et al. Ismail and Jaeel Ismail and Jaeel Ozturk and Bayrakl
(2013) Sada et al. (2010) (2014) (2014) (2005)
(2013)
0 110 52 265 58 65
2.5 55 61
5 38 250 54 59
7.5 52 56
10 78 250 49 55
12.5 48 54
15 20 250
20 65 215 110
25 15 -
30 32 140
40 7 -
50 5 150
75 5 -
All slump values are in mm.
4.4. Flow table test 4.6. Water requirement and unit weight
Workability of fresh mortar was determined using a Iam and Makul (2013) reported that the water require-
ow table test. The measurement was done as per ment increased with increasing rice husk ash content, which
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12 J.K. Prusty et al. / International Journal of Sustainable Built Environment xxx (2016) xxxxxx
500
Reached penetration pressure 2.74 MPa of the time
8 concrete mixtures (Iam and Makul, 2013). Flow times were
Ball drop acceptable up to 20% replacement of rice husk ash, which
400 are within the acceptable limit provided by EFNARC
6
300
4
200 4.9. J-Ring test
2
100
Iam and Makul (2013) adopted the J-ring test to check
0 0
the passing ability of concrete under its own weight to com-
0 5 10 15 20 pletely ll all voids and to obtain the blocking assessment.
WOS content (%) According to American Society for Testing Materials
Fig. 11. Eect of waste oyster shell content on penetration and ball-drop (2014), 025 mm denes no visible blocking, 2550 mm
test (Kuo et al., 2013). denes minimal to noticeable blocking and greater than
50 mm denes noticeable to extreme blocking. Authors
(Iam and Makul, 2013) reported that up to 40% replace-
is due to increasing surface area, and high-unburned car- ment of rice husk ash indicated small degree of blocking,
bon content of rice husk ash. However, the use of rice husk while more than 60% of replacement indicated extreme
ash combined with limestone reduced the water require- blocking behaviour and a combination of rice husk ash
ment. The unit weight of self-compacting concrete and limestone indicated a good passing ability and good
decreased with increasing percentage of rice husk ash. resistance to segregation around congested reinforced
Unit weight of tobacco waste concrete varied between areas.
0.50 and 0.56 kg/m3, indicating that the concrete samples
were in the heat isolation lightweight concrete categories
(Sahin et al., 2000). 5. Hardened properties of concrete
concrete mixtures to ow through a funnel and provide an Fig. 12. Compressive strength of bagasse ash concrete at (a) 7 days and
evaluation of viscosity and segregation resistance of (b) 28 days of curing.
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per IS 516: 1959 (Indian Standard, 1959). Concrete using sive strength using oyster shell as ne aggregate with and
sugarcane bagasse ash as ne aggregate shows an increas- without admixture. They reported the compressive strength
ing compressive strength at 10% replacement than the con- of concrete increased at oyster shell substitution of 5%, but
trol concrete, but further increase of bagasse ash decreased the substitution ratio can be increased up to 10% using
the strength as reported by Modani and Vyawahare (2013). admixture in the concrete mix. Kuo et al. Kuo et al.
Shafana and Venkatasubramani (2014) reported the same (2013) also examined the same result regarding the oyster
result with sugarcane bagasse ash concrete in which com- shell concrete and the compressive strength decreased due
pressive strength improved by increasing the curing period. to the porous structure and the absorption rate of oyster
Fig. 12(a) and (b) represents the compressive strength of shell sand.
bagasse ash concrete in dierent mix proportions and cur- From Fig. 13 it can be observed that in the mix
ing periods. In case of M25 (Shah et al., 2014) and M30 1:1.85:2.62 (Yang et al., 2010) the strength increased mar-
(Shafana and Venkatasubramani, 2014) grade of concrete, ginally at 20% replacement of oyster shell than the control
it can be observed that concrete achieved its minimum concrete, but in the case of controlled low strength concrete
compressive strength at 20% replacement of bagasse ash. (mix 1:6.4:2 Kuo et al., 2013) the strength decreased at all
Almeida et al. (2015) reported that the use of sugarcane replacement levels than the control concrete.
bagasse ash as ne aggregate did not aect the compressive
strength of mortar. 5.1.4. Sawdust ash
Mageswari and Vidivelli (2009) have cast the concrete
using sawdust ash as ne aggregate in both cube and cylin-
5.1.2. Groundnut shell
der. They followed the procedure of compressive strength
Sada et al. (2013) performed an experiment using
test as per IS 516: 1959 (Indian Standard, 1959). It has been
groundnut shells as a ne aggregate replacement having a
seen that the strength of concrete containing 5%, 10% and
mix ratio of 1:2:3, in which they observed that the compres-
15% mix ratio of sawdust ash was higher than that of con-
sive strength increased at 5% replacement than the control
trol concrete. However, concrete containing 20%30% of
concrete. However, it decreased by further increment of
sawdust ash displayed a reduction in compressive strength
replacement, which behaved like a lightweight concrete.
than that of plain concrete.
They also reported that groundnut shell concrete could
not be used in important structural members, which are
5.1.5. Wild giant reed
exposed to water, since moisture aects the weight and
Ismail and Jaeel (2014) added giant reed ash and giant
strength (Sada et al., 2013).
reed bre in concrete as ne aggregate to check the com-
pressive strength of concrete. Casting, compaction and cur-
5.1.3. Oyster shell ing were accomplished according to BS 1881 (British
Yang et al. (2010) tested the compressive strength of Standard Institute, 1983). They reported that in earlier
oyster shell concrete over a long period of 1 year based stages of the replacement, compressive strength increased
on American Society for Testing and Materials (1979). and at higher percentages, it decreased in comparison to
They reported that oyster shell substitution as a ne aggre- the strength of control concrete. However, for all cases
gate showed a drastic increase of compressive strength the compressive strength was higher than the minimum
from 7 days to 28 days curing period and after 28 days, requirement. Fig. 14 represents comparison of the strength
eect was apparent. The compressive strength variance of giant reed ash and giant reed bres, which conrms that
was not proportional to the substitution ratio, which is at 7.5% of replacement, giant reed ash concrete provides
clear from Fig. 13. Yang et al. (2005) tested the compres- optimal strength. The cause of such behaviour of giant reed
ash concrete is due to the content of silica; giant reed ash
may have pozzolanic activity. However, silica with an alu-
35 mina content of their structure may form additional cal-
cium silicate hydrate (C-S-H) by reacting with calcium
Compressive strength (MPa)
0%
30
hydroxide occurring because of cement hydration, which
10%
25 increases the strength of concrete (Ismail and Jaeel, 2014).
20%
20
5.1.6. Rice husk ash
15
Iam and Makul (2013) have cast the self-compacting
10 concrete samples using rice husk ash (RHA), limestone
5 (LS) and a mixture of RHA and LS in cylinder of 150
mm diameter and 300 mm length. Samples were tested after
0 aging for 1, 7, 28 and 91 days in accordance with American
7days 28days 7 days 28days
Society for Testing and Materials (1979). Compressive
MIX 1:1.85:2.62 [16] MIX 1:6.4:2 [15]
strength value was very low at 100% replacement of rice
Fig. 13. Compressive strength of oyster shell concrete. husk ash and it was maximum at 10% replacement of only
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14 J.K. Prusty et al. / International Journal of Sustainable Built Environment xxx (2016) xxxxxx
45
40 7days 7days 14days 14days 28days 28days
limestone. The compressive strength value decreased, when From the above compressive strength analysis, it can be
the replacement level increased. They attributed lower observed that, in case of agro-waste concrete containing
compressive strength due to greater porosity as indicated bagasse ash, saw dust ash and oyster shell, minimum
by the higher water requirement of rice husk ash and lime- strength of concrete is achieved by a maximum 20%
stone. However, they found that rice husk ash was able to replacement, but with further increase of replacement,
ll the micro-voids in improved way within the cement par- strength decreased. However, the maximum compressive
ticles (Iam and Makul, 2013). strength of concrete containing groundnut shell and giant
reed (both GRA and GRF) was achieved at 5% and
5.1.7. Cork 7.5% respectively. Cork and rice husk ash also showed
Bras et al. Bras et al. (2013) tested the compressive good strength in mortar and self-compacting concrete as
strength of mortar containing cork as ne aggregate and ne aggregate replacement.
indicated that addition of cork generated a mortar having
lower compressive strength. These values may be expected 5.2. Tensile strength
due to higher water binder ratio than the control mortar
and an increase of cork as sand replacement. They also Researchers (Modani and Vyawahare, 2013; Mageswari
explained that when cork replacement is higher than and Vidivelli, 2009; Shafana and Venkatasubramani, 2014)
50%, there was no major dierence in compressive strength have conducted the tensile strength of agro-waste based
of mortar that is just 20% of the compressive strength of concrete in accordance with IS 5816: 1999 (Indian
control mortar (Bras et al., 2013). Standard, 1999). Modani and Vyawahare (2013) reported
Compressive strength of lightweight polymer mortar that the tensile strength of concrete decreased by addition
containing waste cork was higher than that of normal mor- of sugarcane bagasse ash whereas in case of other agro-
tar as reported by Novoa et al. (2004). Moreira et al. (2014) waste materials, tensile strength was initially increased
tested the compressive strength of lightweight screed con- and then decreased as increasing the percentage of replace-
taining expanded cork according to NP EN 12390-3:2011 ment. Shafana and Venkatasubramani (2014) also
(Portuguese Standards, 2011) at the age of 7, 28, 56, and observed that bagasse ash increased the tensile strength
84 days. They reported that the compressive strength with optimum strength gain achieved at 10% replacement
increased, with increase of cement content and it reduced value. Fig. 15 represents the relation between compressive
with increase of percentage cork granulates. strength and tensile strength of M20 and M30 grade of
concrete with the substitution of bagasse ash. Relation in
5.1.8. Tobacco waste M20 grade of concrete shows that, tensile strength of
The 28 day cube compressive strength of tobacco waste bagasse ash concrete can be predicted very closely like con-
lightweight concrete sample was within 0.20.6 N/mm2 ventional concrete in the following form:
which varied on the mix ratio. It has been observed that
minor amount of organic matter, which is tobacco waste, f t 0:7f 0:56
ck R2 0:784 1
resulted in a high compressive strength of concrete. The where f t and f ck are tensile and compressive strength of
compressive strength of tobacco waste was under 1 N/ concrete in MPa. However, in case of M30 grade of
mm2 due to which, this lightweight concrete can be sug- bagasse ash concrete the regression coecient, R2 is more
gested to be used as an insulating material for coating appropriate than the M20 grade of concrete.
and separation material into construction (Ozturk and
Bayrakl, 2005). f t 0:644f 0:521
ck R2 0:985 2
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J.K. Prusty et al. / International Journal of Sustainable Built Environment xxx (2016) xxxxxx 15
4.5 4.5
(a) ft = 0.700 (fck)0.556
Tensile strength (MPa)
4 4
R = 0.784
Bagasse ash concrete was cast in beam specimen size where f r and f ck are exural strength and compressive
100 mm 100 mm 500 mm and cured in water for strength of concrete in MPa.
28 days. After 28 days, beams were tested as per IS 516:
1959 (Indian Standard, 1959). The results indicated that 5.4. Elastic modulus (E-value)
the exural strength increased by 10% replacement and it
reduced with further increase of percentage (Shafana and Yang et al. (2010) tested the elastic modulus of concrete
Venkatasubramani, 2014). Fig. 16 shows the exural with the substitution of oyster shell over a period of 1 year
strength variation of bagasse ash concrete at dierent sub- as per ASTM C469 (American Society for Testing and
stitution ratios and curing period. Materials, 2014). The elastic modulus test results are pre-
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16 J.K. Prusty et al. / International Journal of Sustainable Built Environment xxx (2016) xxxxxx
7
7 Days 7 Days 14 Days 14 Days 28 Days 28 Days
Fig. 17. Comparison of exural strength between Giant Reed Ash (GRA) and Giant Reed Fibre (GRF) (Ismail and Jaeel, 2014).
6
Flexural strength (MPa)
5 fr = 0.68 (fck)0.56
R = 0.93
4.5
4
fr = 0.88 (fck)0.47
3.5 R = 0.75
3
2.5
2
15 20 25 30 35 40 45
Compressive strength (MPa)
Fig. 18. Correlation between exural strength and compressive strength Fig. 20. Relation between compressive strength and ultrasonic pulse
of GRA and GRF concrete at mix 1:1.78:2.23 (Ismail and Jaeel, 2014). velocity in oyster shell concrete (Kuo et al., 2013).
3.5
ticity properties of polymers, which are reported by Novoa
3 et al. (2004). They Novoa et al. (2004) also included the
predicted elastic modulus based on Kelvin-Voigt model
2.5 for the rule of mixture,
2 Ecomp Ec V c Em V m 6
14 days 28 days 6 months 1 year
where E refers to elastic modulus and V refers to volume
Curing period
fraction. The indices comp, c and m are relative to nal
Fig. 19. Elastic modulus of oyster shell concrete (Yang et al., 2010). composite, cork and matrix.
sented in Fig. 19. They observed that at 20% replacement 5.5. Ultrasonic pulse velocity (UPV)
the elastic modulus value decreased approximately 10
15% compared to other replacement level. They reasoned, Ultrasonic pulse velocity (UPV) is a form of non-
it might be more due to the lower elastic modulus of oyster destructive testing in which ultrasonic pulsing are used to
shell than the natural ne aggregate. Yang et al. (2005) test the quality of concrete and detect the depths and
measured elastic modulus at 28 days to evaluate the eect widths of crack so as to determine the density variation
of substitution of oyster shell on the elastic modulus of of the concrete (Kuo et al., 2013). Kuo et al. (2013) tested
concrete. They reported that the elastic modulus depended the ultrasonic pulse velocity of concrete with the substitu-
on the type of oyster shell, substitution ratio and use of tion of oyster shell as per ASTM C597 (American Society
admixture. Elastic modulus decreased approximately 10% for Testing and Materials, 2009). They reported that at
by increasing the substitution ratio of 20% of oyster shell. 5% replacement, UPV value was higher than the control
They also compared the experimental value with the value concrete and in all other level of replacement, it was lower
obtained from the relation proposed by ACI code than the control concrete. It can be expected that the lower
(American Concrete Institute, 1997) and CEB-FIP model UPV value may be due to the weakness of CSH gel. The
equation (CEB-FIP, 1993) and the resulting experimental relation between compressive strength and ultrasonic pulse
value was higher even without using the admixture than velocity of oyster shell concrete is presented in Fig. 20.
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J.K. Prusty et al. / International Journal of Sustainable Built Environment xxx (2016) xxxxxx 17
From the regression analysis, it can be observed that the Yang et al. (2010) conducted a series creep test to know
compressive strength of oyster shell concrete can be pre- the eect of creep on oyster shell concrete and reported that
dicted using following relationship from its UPV value at 0% replacement, the creep was larger than that at 10%
with a regression coecient of R2 = 0.87. replacement even at an early age.
f ck 0:06UPV 4:93 7
6. Durability
Iam and Makul (2013) measured the UPV value of self-
compacting concrete after aging for 1, 7, 28 and 91 days in Durability is the important characteristics of hardened
accordance with ASTM C597 (American Society for concrete to check when it contains any replacement mate-
Testing and Materials, 2009) and reported its variation rials of cement or aggregate. Many researchers conducted
was from 0.7 km/s to 4.4 km/s. Highest UPV value was the durability test such as freezing and thawing, carbona-
achieved in control concrete and lowest value was at tion, chemical attack, permeability and water absorption,
100% replacement of rice husk ash. They also noticed that etc. of concrete having agricultural waste as a ne aggre-
the UPV value increased by an addition of rice husk ash, gate replacement.
which was likely due to micro lling and pozzolanic eect
on property of concrete pore structures. They found good 6.1. Freezing and thawing
relation between compressive strength and ultrasonic pulse
velocity of self-compacting concrete with rice husk ash Yang et al. (2010) studied the freezing and thawing test
mixture having R2 = 0.9403 which is shown in Fig. 21. of oyster shell-mortar. Freezing and thawing tests were per-
formed according to ASTM C666 (American Society for
5.6. Shrinkage and creep Testing and Materials, 2015). According to their study,
the variance rates of the dynamic modulus of elasticity
Yang et al. (2010) conducted a series of tests to evaluate and weight of the concrete substituted by oyster shell
the behaviour of drying shrinkage of concrete using oyster showed smaller and more satisfactory values respectively
shell as ne aggregate. Experimental values were compared than those of control concrete. They reported that oyster
with the value obtained from several codes (ACI American shell shows improved performance of freezing and thawing
Concrete Institute, 1997; CEB-FIP, 1993), and BP model resistance of concrete, which is because the ne grain of
equations (Bazant and Wittmann, 1982) and showed a oyster shell lls the entrapped air voids scattered in con-
good agreement between these two values. The increase crete specimen (Yang et al., 2010).
in drying shrinkage based on regression analysis was 7%
and 28% in the substitution ratio of 10% and 20%, respec- 6.2. Chemical attack
tively, compared with the control concrete. They analysed
that the shrinkage increased due to the lower rigidity of Yang et al. (2010) did the chemical attack experiment on
oyster shell and eect of size of ne powder (Yang et al., concrete with the substitution of oyster shell by depositing
2010). Kuo et al. (2013) reported that the shrinkage of the concrete specimens in sulphuric acid and hydrochloric
specimen increased if the natural aggregate of higher acid. After a certain age, they tested the specimen and
Youngs modulus was replaced by waste oyster shell as ne reported that the attack of concrete increases gradually
aggregate having a lower Youngs modulus, which meant with age. The attack of sulphuric acid was continued as
that larger replacement percentage resulted in greater age increased. They also found that there is no eect of
shrinkage. the substitution ratio of oyster shell on weight loss of con-
crete specimen (Yang et al., 2010). Kuo et al. (2013)
observed the same result of sulphate attack on oyster shell
concrete. Weight loss of concrete specimen increased from
1.17% to 4.822%, according to the increasing of age period.
There is some eect of the substitution ratio of oyster shell.
Ismail and Jaeel (2014) observed the eect of alkali on
concrete containing giant reed ash and giant reed bres.
They observed that modied concrete with giant reed bres
could be aected by alkali faster than the control concrete
since they aected the lignin complex molecules causing
bre fracture.
Almeida et al. (2015) applied colorimetric treatment to
the mortar specimens for analysis of chloride penetrations.
Fig. 22 shows the average chloride penetration values in
Fig. 21. Relation between compressive strength and ultrasonic pulse millimetres obtained at dierent immersion times in a
velocity of self-compacting concrete made with replacement of RHA (Iam 3.5% NaCl solution. The M30 (30% substitution of bagasse
and Makul, 2013). ash) and M50 (50% substitution of bagasse ash) samples
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18 J.K. Prusty et al. / International Journal of Sustainable Built Environment xxx (2016) xxxxxx
12
mortar containing 50% replacement of bagasse ash than
10
the controlled mortar and mortar containing 30% of
8 bagasse ash. Fig. 23 shows the colorimetric treatment of
6 mortar for carbonation depth analysis.
4
Almeida et al. (2015) also mentioned that the carbona-
tion depth could be decreased by reducing the water
2
cement ratio and by the packing eect of cementitious
0 matrix provided by bagasse ash neness. The reduction
30 60 90 of water cement ratio and incorporation of ner materials
Imersion period (days)
lead to a denser and stronger mortar matrix.
Fig. 22. Average chloride penetration values at dierent ages for the
mortar samples (Almeida et al., 2015). 6.4. Permeability
showed signicantly dierent chloride penetration values in Yang et al. (2010) determined the permeability ratio of
the rst month of conditioning but showed same magni- mortar in accordance with ASTM C109 (American
tude at later stage. The RM (Referenced Mortar) specimen Society for Testing and Materials, 2016) and compared
showed less resistance to chloride penetrations because it with the substitution ratio of oyster shell. The permeability
showed the highest average chloride penetration values at ratio of mortar having 10% and 20% of oyster shell was
all of the studied ages. Thus, the addition of bagasse ash approximately 80% less than that of standard mortar. They
increased the chloride penetration resistance of mortar. also explained that the improvement of permeability was
due to the eect of small particle size, more akiness and
elongation of oyster shell (Yang et al., 2010). Panesar
6.3. Carbonation and Shindman (2012) tested the rapid chloride permeability
test on cement-cork mortar by an increasing percentage of
Yang et al. (2010) conducted carbonation test to evalu- cork, taking dierent size of the cork, cork gradation and
ate the eect of substitution ratio of oyster shell on carbon- weathered cork. The procedure employed was ASTM
ation characteristics of concrete. These tests were C1202 (American Society for Testing and Materials,
performed in a chamber under the temperature of 30 2012). They observed that cork content had more eect
3 C, relative humidity of 60 5%, and 10% carbon on the permeability of mortar than the size and weathered
dioxide. After splitting, a 1% of phenolphthalein alcohol cork (Panesar and Shindman, 2012). The water vapour per-
liquid was sprayed on the fractured specimen surface and meability test of cement-cork mortar and lime-cork mortar
the thickness of the discoloured portion was measured. was performed according to European norm EN1015-19
As a result, it has been observed that the carbonation depth (1988), EN 1015-19 (1999) and Bras et al. (2014). It has
increased with increasing carbonation age. Almeida et al. been observed that there was no eect of cork on changes
(2015) measured the carbonation depth of sugarcane of permeability. Cement based mortars were less permeable
bagasse ash mortar (at 0%, 30%, and 50% substitution to water vapour than lime based mortar (Bras et al., 2014).
ratio) using colorimetric treatment. They reported that, ini- But according to Moreira et al. (2014), addition of
tially the carbonation depth magnitude was similar for expanded cork granulates in the mix induced greater water
vapour permeability.
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J.K. Prusty et al. / International Journal of Sustainable Built Environment xxx (2016) xxxxxx 19
Fig. 24. Cyclic test (a) Uniaxial compression (b) Diagonal compression (c) Rupture in uniaxial compression (d) Rupture in diagonal compression
(Carvalho et al., 2013).
containing giant reed bres attained higher percentage of that the decrease was higher than the mortar containing
water absorption as compared to giant reed ash concrete expanded polystyrene (EPS). Moreira et al. (2014) added
and control concrete. It is also observed that water dierent substitution ratio of expanded cork granulates
absorption percentage increased as increasing the per- with cement mortar. They noticed the declining thermal
centage of replacement of giant reed ash in concrete conductivity coecient like other researchers and reported
mixes. Kuo et al. Kuo et al. (2013) reported that the that thermal conductivity decreased due to lower cement
absorption rate of replacing waste oyster shell sand is content in mortar mixes. The thermal conductivity of pro-
increased by 1.11.6% than the control concrete since ducing tobacco waste materials was in the range of 0.194
waste oyster shell sand has a higher porosity and 0.220, which indicated that it could be used as a coating
absorption rate. and dividing materials in concrete (Ozturk and Bayrakl,
2005).
7. Thermal conductivity
8. Cyclic behaviour
Panesar and Shindman (2012) tested the thermal resis-
tance and thermal conductivity of concrete containing cork Carvalho et al. (2013) tested the cyclic behaviour of a
and expanded polystyrene (EPS) based on the procedure composite material made from a mortar incorporated with
described in American Society for Testing and Materials granulated cork. Specimens with 0%, 15% and 30% of cork
(2010). They reported that the mixture containing 10% addition, in volume mix, were prepared and tested. Cyclic
and 20% of cork reduced the thermal conductivity by uniaxial and diagonal compression tests were carried out
approximately 16% and 30% respectively. They also to characterize the cyclic behaviour of the composite mate-
explained a relation that thermal conductivity increased rials. It has been observed that, for whole set of mortar
as the density increased. Thermal conductivity not only study, there is a tendency for improvement of performance
controlled by the density, but also inuenced by the size, when the cork granulates are added, either uniaxial or diag-
gradation and percentage of replacement of cork onal compression test. Fig. 24 shows the cyclic test of mor-
(Panesar and Shindman, 2012). Bras et al. (2014) observed tar incorporated with granulated cork.
that, for mortars with a high substitution ratio of cork They also concluded the improvement behaviour of
granulates lead to a linear decrease of thermal conductivity energy dissipation capacity and conformed that inclusion
as well as density. In another study, Bras et al. (2013) of cork granulates in controlled volume fractions in con-
reported the same result that mortar containing cork gran- struction mortar was benecial for the seismic protection
ulates shows linear decreasing thermal conductivity and of building (Carvalho et al., 2013).
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20 J.K. Prusty et al. / International Journal of Sustainable Built Environment xxx (2016) xxxxxx
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J.K. Prusty et al. / International Journal of Sustainable Built Environment xxx (2016) xxxxxx 21
10. The cyclic behaviour of cork-based mortar was British Standard Institute, 1983. BS 1881122: Method for Determination
observed. It has been seen that for the whole mortar of Water Absorption.
British Standard Institute, 1992. Specication for aggregates from natural
study, there is an improvement of performances of sources for concrete. BS 882, London.
specimen due to the inclusion of cork, which is bene- Buari, T.A., Ademola, S.A., Ayegbokiki, S.T., 2013. Characteristic
cial for seismic protection of building. strength of groundnut shell ash and ordinary Portland cement blended
concrete in Nigeria. IOSR J. Eng. 3 (7), 17.
Canadian Standards Association, 2009. CSA A23.2-09 Test Methods and
Standard Practices for Concrete.
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