Académique Documents
Professionnel Documents
Culture Documents
and Updates
By
UNPUBLISHED
Copyright Henry Z. Kister, Jeffrey Scherffius, Khashayar Afshar, and Emil Abkar
The AIChE shall not be responsible for statements or opinions contained in its
publications
Summary
For several decades, the Sherwood-Eckert GPDC (Generalized Pressure Drop Correlation) chart
has been the standard of the industry for predicting packing flood points and pressure drops.
Strigles GPDC chart for random packings (Figure 1) and Kister and Gills GPDC(SP) chart for
structured packing are the best and latest versions of the GPDC as discussed in the latest
distillation texts. Plotting experimental flood and pressure drop data on the GPDC contours for
each packing extended the GPDC into an atlas of accurate and useful interpolation charts. This
interpolation procedure desensitized the GPDC to inaccuracies in packing factors and watches
out for data-lean regions where uncertainties prevail. This is especially important since
deviations from packing pressure drop correlations tend to be systematic rather than random. The
use of the GPDC interpolation procedure for tower rating, debottleneck evaluation, analysis of
operation, and retrofits is discussed with examples based on actual experiences.
Two major problems have been experienced with the GPDC interpolation procedure: misuse and
need for updating. This paper discusses correct and incorrect applications of the procedure.
Incorrect calculation of kinematic viscosity, using a packing factor different from that shown on
the chart, calculating pressure drops above the flood point, and extrapolation to data-lean
regions, have been the main misuses. Updating is needed with new developments in the field.
With the last update 12 years ago, and some exciting developments since, the paper presents 22
new interpolation charts. During these 12 years high-capacity structured packings were very
successfully introduced to the industry. The paper adds interpolation charts for many popular
high-capacity structured packings, for other popular new packings, and for some popular
packings for which supplier data had been updated.
Overall, this paper guides engineers on correct and incorrect uses of this GPDC interpolation
procedure, and updates the method for todays new state of the art packings.
For several decades, the Sherwood-Eckert GPDC (Generalized Pressure Drop Correlation) chart
has been the standard of the industry for predicting packing flood points and pressure drops.
This chart, initially developed by Sherwood et al.(1), and later modified by Lobo et al. (2),
contained only a single curve that predicted packing flood points. Leva (3) retained the flood-
point curve and added a new family of curves onto the chart to predict packing pressure drop.
Copigneaux (4) and Eckert (5,6) proposed further modifications. In a later version, Eckert (7)
omitted the flood curve from the chart, retained only the pressure drop curves, and preformed
other minor modifications. Finally, Strigle (8) changed the scales of Eckerts later version from
log-log to semi-log to make interpolation between adjacent pressure drop curves easier. Strigles
chart (Figure 1) is the best and latest and preferred version of the GPDC as discussed in the
latest distillation texts (8-10).
All the versions of the GPDC discussed above were based on random packing only. For
structured packings, Kister and Gill (11) produced a modified chart [GPDC (SP), where SP
stands for Structured Packings, Figure 2] that empirically gave better fit to a large database of
published structured packing data
In Eq. (1), v is the kinematic viscosity of the liquid [NOTE: the kinematic viscosity (centistokes)
is obtained by dividing the dynamic viscosity (centipoises) by the specific gravity, not by the
liquid density in English units]. FP is the packing factor, which is an empirical factor
characteristic of the packing size and shape. The packing factor for each GPDC chart is always
listed on the GPDC chart. An atlas of GPDC interpolation charts, as well as an early update, are
presented elsewhere (10, 18).
CS is the C-factor, i.e., the superficial gas velocity US corrected for vapor and liquid densities (
V and L), given by Eq. (2):
G
CS = US (2)
L G
The GPDC chart ordinate describes the balance between the vapor momentum force, which acts
to entrain swarms of liquid droplets, and the gravity force, which resists the upward entrainment.
This closely resembles the force balance used by Souders and Brown for entrainment flooding in
The GPDC chart abscissa is the flow parameter, Flv, given by:
0.5
L
Flv = G (3)
G L
The flow parameter [Eq. (3)] represents the ratio of liquid kinetic energy to vapor kinetic energy.
High flow parameters are typical of high liquid rates (the L term) and high pressures (the vapor
density term). Conversely, low flow parameters are typical of vacuum and low liquid rate
operation.
Removal of the flood curve from recent versions of the GPDC curtailed its capability to predict
flood. This capability was reinstated by a simple correlation by Kister and Gill (13).
Equation (4) expresses the pressure drop at the flood point as a function of the packing factor
alone. Once this pressure drop is known, the flood velocity can be calculated from the GPDC (or
any other good pressure drop prediction method). Equation 4 states that the pressure drop at the
flood point decreases as the packing capacity increases, as observed earlier by Zenz (15), Strigle
and Rukovena (16), and Mackowiak (17). The numerical constant originally proposed by Kister
and Gill was 0.115. Strigle (8) endorsed this equation, but with the upward rounded coefficient
of 0.12 in equation 4.
Strigle (8) and Kister and Gill (11, 13) compared predictions from the latest version of the GPDC
(Fig. 1 and 2) to thousands of packing pressure drop measurements. The GPDC correlation was
shown to give good predictions for most pressure drop data. It generally works well for the air-
water system for flow parameters as low as 0.01 and as high as 1 (8). For nonaqueous systems, it
works well for flow parameters of 0.03 to 0.3 (typical of atmospheric distillation).
The GPDC correlation was shown (11, 13) to be optimistic for flow parameters greater than 0.3
(typical of pressure distillation and/or high liquid rate applications). Strigle (8) attributes these
optimistic predictions to enhanced liquid frothiness at higher pressure. Robbins (14) identified
another limitation at low liquid rates (flow parameters <0.03) where liquid properties have a
much lesser effect on pressure drop than the GPDC predicts.
There were two other issues that have been problematic to the GPDC. First, predictions from the
GPDC correlation are sensitive to the packing factor. Strigle (8) and Kister and Gill (13) found
that most packing factors reported in the literature are satisfactory. However, for a few packings,
the packing factors gave poor fit to experimental pressure drop data. Also, for some packings,
the dependence of pressure drop on vapor and liquid loads was not adequately predicted by the
GPDC correlation.
An interlinked issue identified in our analysis (13) is that deviations from the correlation tend to
be systematic rather than random. Further, some regions where the correlation tended to provide
poor pressure drop predictions are those of great commercial interest. It was stressed that an
excellent fit to experimental data is insufficient to render a packing pressure drop correlation
suitable for design. In addition, the correlation limitations must be fully explored. This message
extends beyond the GPDC to any other packing pressure drop correlation.
Superimposing experimental data points (for a given packing) on the curves of the GPDC chart
converts the GPDC into an interpolation chart (for the packing). Every chart in the Appendix is a
GPDC interpolation chart. Pressure drops are calculated by interpolating the plotted pressure-
drop data. The correlation curves solely help guide the interpolation. An entire atlas of
interpolation charts and an application procedure are available elsewhere (10). An early
addendum updating this atlas has also been published (18).
Charts 10.2502 through 10.2514 in the Appendix are random packing interpolation charts, and
the other charts in the Appendix are structured packing interpolation charts. For random and grid
packings, the curves on the interpolation charts are those of the Strigle version of the Eckert
GPDC (Fig. 1). For structured packings, the curves on these interpolation charts are those of the
Kister and Gill GPDC (SP) (Fig. 2). For all charts (random, structured or grid packings), the
abscissa of the correlation is the flow parameter, given by Eq. (3), and the ordinate is the
capacity parameter, given by Eq. (1).
Flood and maximum operational capacity (MOC) data are also plotted on the GPDC
interpolation charts, and the charts are invaluable for interpolating these. The MOC (also
referred to as the maximum efficient capacity) is defined as (8) Maximum vapor rate that
Kister and Gill (11,13) compared flood-point predictions from Eq. (4) to their massive data bank
for modern random and structured packing. Pressure drops were calculated using the GPDC
interpolation charts. They showed that Eq. (4) predicted all the flood points in their data bank to
within + 15 percent and most to within + 10 percent. It was also shown (10) that this procedure
is insensitive to reasonable errors in packing factors.
The suitability of the GPDC interpolation charts as a basis for interpolation is not accidental.
Packing pressure drops correlate extremely well with GPDC coordinates, i.e., the flow parameter
and the capacity parameter. The dependence does not always follow the correlation contours,
but always appears to exist. Further, the correlation coordinates are essentially a performance
diagram, i.e., a plot of a vapor load against liquid load, a tool commonly used for charting
column hydraulic performance.
The conversion of the GPDC into interpolation charts overcomes the multitude of correlation
limitations. The GPDC interpolation charts readily identify any regions where data veer off the
correlation curves and give unreliable estimates (by data interpolation) in these regions. Packing
factors, often criticized for being inaccurate and inconsistent, cease to be critical variables.
Inaccuracies in packing factors merely cause data to veer off the curves, and have no effect on
the interpolation.
It may be argued that the interpolation procedure breaks down when data are absent. The
counter-argument is that the GPDC correlation curves are always there to fall back on and to get
a prediction, but now there is also a tool to warn that there are no data in this region and that
uncertainty is involved.
A shortcoming of the GPDC interpolation data chart procedure is that it replaces a single
correlation chart by an atlas. The interpolation charts consume more storage space in the design
manual or on the computer and require a greater updating effort.
Updates
As stated, the GPDC interpolation procedure does require updating. The last update was issued
in 1995 (18). Much happened in packing technology since, and this is addressed by this update.
1) A recent development followed the realization that liquid drainage in structured packings
was restricted at the element-to-element transition rather than inside elements. This
means that the liquid accumulation leading to flood initiates at the element transition
region. A fourth generation of structured packing evolved, in which the main body of
each element has layers inclined at 45 degree, but the ends of each element are rounded
or vertical to promote drainage at this end region. These high-capacity structured
packings offer more capacity compared to equivalent 45 degree inclined packings with
efficiency the same with some (19-22) and slightly lower with others (23). Charts
10.6801 through 10.7104 are for these packings.
2) Inside each element of a structured packing, corrugated sheets are most commonly
inclined at about 45 degrees to the vertical (typically indicated by the letter Y following
the packing size). This angle is large enough for good drainage of liquid, avoiding
stagnant pockets and regions of liquid accumulation, and small enough to prevent gas
from bypassing the metal surfaces. In some packings, the inclination angle to the vertical
is steepened to 30 degrees (typically indicated by the letter X following the packing
size). This improves drainage, and therefore capacity, but at the expense of reduced gas-
liquid contact, and therefore, efficiency. Many new X type packing were added after
the last update of our charts. Charts 10.6152 through 10.6156 are for these packings.
3) For one line of popular structured packing, Flexipac 1, 2, 3 and 4Y, the original GPDC
interpolation charts (10) were based on pressure drop data measured in an extensive air-
water test program by Koch Engineering in 1982 (24). Recent publications by the same
vendor appear to have shifted support to the vendors new air-water data (21, 26) which
show significantly more pressure drop under equivalent conditions. Further discussion in
Example 3 below. Charts 10.6102R1 through 10.6108R1 are revised charts for these
packings based on the vendors latest data
4) The Raschig Super-Ring high-capacity random packing has become available and
gained popularity. Charts 10.2502 through 10.2514 are new GPDC charts for various
sizes of this packing.
5) Data and GPDC charts for Hyperfil Knitted Mesh Tower Packing were recently
published (29). No further update is needed.
All the examples below are based on actual experiences. Some details could have been changed
in order to make it difficult to recognize where the experience occurred.
A 6-0 chemical vacuum tower contains a 20-ft bed of #1.5 metal Raschig Super-Ring
packing. The tower is to be retrofitted for the following flow rates:
SOLUTION
AT = Tower area = 6 2 = 28.27 ft. 2
4
0.036
C-factor (eq. 2) = 10.9 = 0.299 ft / s
48 0.036
3) Calculate the kinematic viscosity in cS. This is obtained by dividing the dynamic
viscosity in cP by the liquid density in g/cm3. Centistokes, centipoises and g/cm3 are all
units in the CGS system, and are consistent. An easy way to remember is that kinematic
viscosity cS is the dynamic viscosity in cP divided by the specific gravity (SG).
The 48 is the density in English units (lb/ ft3), which are inconsistent with the units of viscosity
(cP). In the authors experience, mixing units in kinematic viscosity calculation has been the top
cause of getting incorrect answers out of GPDC. What makes it worse is that the kinematic
viscosity is raised to the power of 0.05 in the calculation (equation 1). The conversion factor
between the English units of lb/ft3 and the CGS units of g/cm3 is 62.4. When 62.4 is raised to the
0.05, it produces an error of 23%, which makes a large difference to the final answer, yet the
wrong answer makes sense, making the error difficult to identify.
Eq. 1 gives
Chart 10.2503 does not contain flood data, so equation 4 is used to give
The flood capacity parameter is the ordinate at the flood pressure drop and at the flow
parameter of 0.022, about 1.73. Therefore,
Therefore, the existing packing (# 1.5 (M) Raschig Super-Ring) will comfortably
achieve the retrofit flow rates.
7) Structured packing retrofit. For this calculation, steps 1-3 are as above. Step 4 to 6 need
to be recalculated based on charts 10.6904 and 10.6804.
Actual pressure drop (from Flv, CP) 0.25 (Note 2) 0.22 (Note 3)
inch water / ft
Notes:
1) Here there are actual flood data, so there is no need to use equation 4. The flood point is a direct
interpolation of flood data, so it is predicted with a high degree of confidence.
2) Here limited extrapolation is needed, but it is quite straight forward and involves low risk.
3) As per Note 1, here the data permit a high degree of confidence in the pressure drop prediction.
8) Comparing the pressure drop in Steps 6 and 7, the pressure drop reduction that can be
expected is 0.10 0.13 inches of water per ft of packing. This will save about 2 to 2.5
inch of water over the 20 ft bed.
This small pressure drop reduction is unlikely to be beneficial enough to justify the cost
of a structured packing retrofit in this tower. However, if the structured packings can
also offer a significant efficiency improvement, such a retrofit may be justified.
Suppose that the packing factor in Example 1 was grossly excessive. Figure 3 shows a chart with
a grossly excessive packing factor of 27 for the same packing as in Example 1 (the correct chart
shows a packing factor of 18).
SOLUTION
Steps 1 through 3 are the same as in Example 1. Steps 4 on are different and based on Figure 3.
Figure 3 (a variation of Chart 10.2503 in which an excessive packing factor of 27 is used with
the same data for # 1.5(M) Raschig Super-Ring that are on Chart 10.2503).
Eq. 1 gives
Chart 10.2503 does not contain flood data, so equation 4 is used to give
The flood capacity parameter is the ordinate at the flood pressure drop and at the flow
parameter of 0.022, about 2.27. Therefore,
So a packing factor increase of 50% changes the calculated flood point only by 7%. This
change is entirely due to the effect of packing factor on the flood point per Eq. 4. The
flood point would not have been impacted had flood data been present on the chart.
6) Calculate the pressure drop. Locate a point on the chart whose abscissa is the flow
parameter (0.022) and whose ordinate is the capacity parameter (1.53). At that point, the
pressure drop is about 0.35 inches of water per foot of packing. For a 20-ft bed, the total
pressure drop is 0.35 x 20 = 7 inches of water. This is the same as the value calculated
with the correct packing factor of 18.
GPDC interpolation charts are simple plots of measured C-factors against flow parameters at
constant pressure drops. Due to the low power there is little impact of the kinematic viscosity.
The packing factors play the sole role of moving the data points up or down relative to the
curves, but what is being interpolated is the data, not the curves. For a given packing, the
packing factor is simply a constant on the ordinate. As long as the packing factor used in the
calculation is the same as that used in the chart (as in Examples 1 and 2 above), it plays no role
in the pressure drop calculation. If Eq. 4 is used, the packing factor plays a small role in the flood
calculation.
In preparing the charts, we took care to pick packing factors that move the data closest to the
curves. This minimizes errors in the use of equation 4. For the pressure drop interpolation, the
closer the data match the curves, the better the guide that the curves can provide for the
interpolation. For the pressure drop interpolation, we could have picked any packing factor
(within reason) and obtained the same pressure drop result as per Example 2 above.
No. 3 MISUSE
Figure 4, based on reference 27, is a classic example of this misuse. For this packing (Flexipac
2Y), there were quite a few flood data points plotted on the GPDC chart in the relevant region
(10), measured by the Separation Research Program (SRP). Interpolation of these flood data
would give a flood point vapor rate 9.5% higher than the experimental flood point, yet the
calculation displayed on Figure 4 (27) extended to more than 30% above the measured flood
point! The portion of the graph between 9.5% and 32% above the GPDC flood point is totally
The difference between the valid portion of the calculated curve and the experimental curve in
Figure 4 is addressed in Example 4 below.
There is nothing magic about GPDC interpolation. The charts are simple plots of C-factors vs.
flow parameters at constant pressure drops. As stated above, the kinematic viscosity and packing
factors play minor, if any, roles. What is being interpolated is the measured data. Therefore, if
GPDC interpolation starts giving unsatisfactory predictions, the data should be high up on the
troubleshooting list.
The 1982 curve on Figure 5 shows a sample of the pressure drop data that were used to derive
the GPDC chart for this packing (Flexipac 2Y). These data were taken from the measurements
obtained in a very extensive test program published by Koch Engineering (24) and used in their
catalogues for over a decade (25). Recent Koch-Glitsch publications (21, 26) substituted the
1982 data by new data, some from the same test unit, showing significantly higher pressure
drops for each packing from the same family. Figure 5 illustrates the differences. It is not clear
why the pressure drop of these packings has risen in the last decade or so. However, it is clear
that charts based on the 1982 data are too optimistic to predict the best and latest pressure
drops measurement supported by the vendor for the same packings. The vendors quarterly
newsletter correctly stated that the existing GPDC charts for the packing do not adequately
reflect the new data (27). They cannot, they are based on the old data. For this reason, Charts
10.6102R1 through 10.6108R1 (R1 stands for Revision 1) in the Appendix are revised charts for
the Flexipac 1, 2, 3 and 4Y based on the revised data.
It is important to note that unlike the changed pressure drop calculation, the flood prediction of
the same superseded GPDC interpolation chart for Flexipac 2Y is quite close to the measured
flood point (within 10%). This is because the flood point interpolation is based on measured
flood point data by SRP that were not affected by the pressure drop data substitution.
It is therefore most important to be alert to data changes and reliability. Fortunately, data
changes for a given packing do not happen too often.
A refinery crude tower is 14-ft ID, but has a packed stripping section contained in a 5 ft ID
cylinder (can). The packed bed is 10 ft tall. The plant is measuring a pressure drop of 13-20
inches water across the bed. Evaluation by others using proprietary software concluded that the
bed should be operating at 87% of flood with a pressure drop of 8 inches of water. The vapor
and liquid loading are highest at the top of the bed, and gradually diminish as one descends. At
the bottom of the bed the vapor loads are about half those at the top. Operating conditions at the
top of the bed are:
SOLUTION
Tower area = 5 2 = 19.64 ft 2
4
0.45
CS = 2.42 = 0.255 ft / s
41 0.45
5) A point with the abscissa of the flow parameter and the ordinate of the capacity
parameter is now plotted on Figure 6. Figure 6 shows that the operating point in this
Fortunately, flood data (these were measured by the packing vendor) are available all the
way to a flow parameter of 0.56, and from there to 0.79 the extrapolation only needs to
travel a short path. Also, the flood data appear to trend well, and should give a
reasonable prediction, despite the uncertainty. The flood data extrapolate to a capacity
parameter of about 0.8 at a flow parameter of 0.79. From this
6) Unlike the proprietary method, the GPDC interpolation procedure predicted flooding at
the operating conditions. Considering that the high loads were only at the top of the bed,
the entire pressure drop of unflooded packing in this service should have been less than
3-5 inches of water, as can be calculated from Figure 6 and integrated over the bed. The
actual measured pressure drop was about 4 times higher.
7) In this case, the GPDC interpolation calculation also invalidated a revamp proposal with
a more open packing. While the proposal estimated that the new packing will operate at
88% of flood, the GPDC interpolation chart for the proposed packing showed that
although the more open packing will satisfactorily handle current conditions, it will
experience flooding at the revamp loads. On this basis, the stripping section cylinder
(can) was replaced by a larger one, and trouble-free operation was re-instated.
SOLUTION
1) The Flv, CS and kinematic viscosity are the same as in Example 4. For Flexipac 3X, the
packing factor is much lower, at 5, so the capacity parameter is
In the absence of flood data, eq. 4 is used for the flood pressure drop
The closest data points for this pressure drop are at flow parameters of 0.3 0.4, much
lower than the 0.79 in the tower. The operating point is well outside the available data
range for Flexipac 3X. This interpolation chart is therefore unable to tell where the
flood point is at a flow parameter of 0.79. Therefore, the interpolation chart cannot tell
whether Flexipac 3X will permit operation without flooding at the current loads.
No. 4 MISUSE
Any extrapolation must be performed with good engineering judgment. In Example 5, the
extrapolation was to a close-by region, there were well-defined flood data, and the data trends
were clear. Although there was some uncertainty, extrapolation here could be expected to yield
a reasonable estimate.
The converse occurred with Example 6. Here there were no flood data, the operating point was
quite far from the pressure drop data points, and the data trends were not completely clear at the
higher flow parameter. Under these circumstances, extrapolation will be unreliable and must be
avoided.
EXAMPLE 7. This example presents a number of experiences in which vendor and simulator
predictions for a packed tower were optimistic. In each one of these, the Kister and Gill equation
(eq. 4) gave excellent prediction for the maximum capacity.
TOWER A This chemical tower, equipped with wire-mesh structured packing with a packing
factor of 21, ran completely smoothly until reaching a pressure drop of 1 inch of water per foot
of packing. It would then rapidly lose efficiency, exactly as predicted from equation 4.
Simulation prediction (both vendor and general options) predicted a much higher capacity.
TOWER B This chemical tower, equipped with random packing with a packing factor of 18,
would rapidly lose efficiency when the pressure drop increased above 0.67 inch of water per foot
of packing. This compares to a flood pressure drop of 0.9 from equation 4. The measurement
TOWER C This chemical absorber was equipped with random packing with a packing factor of
18. The highest pressure drop at which operation was stable was 0.8 inch of water per foot of
packing. Above this, the pressure drop would rapidly rise. This compares to a flood pressure
drop of 0.9 from equation 4. Simulation predictions (both vendor and general options) were of a
20 percent higher capacity.
TOWER D Random packing installed in a chemical tower fell short of achieving design
capacity. The vendor method predicted flooding at a pressure drop of 1.5 inch of water per foot
of packing. With a packing factor of 18, equation 4 predicted that the packing would flood
significantly earlier, at a pressure drop of 0.9 inches of water per foot of packing. The packing
flooded exactly at that pressure drop.
Greek Letters
L Liquid viscosity
Subscripts
Fl At flood
MOC At MOC
1. Sherwood, T. K., G. H. Shipley, and F. A. L. Holloway, Ind. Eng. Chem. 30(7), p. 765, 1938.
2. Lobo, W. E., L. Friend, F. Hashmall, and F. A. Zenz, Trans. Am. Inst. Chem. Engrs. 41, p.
693, 1945.
3. Leva, M., Chem. Eng. Prog. Symp. Ser. 50(10), p. 51, 1954.
8. Strigle, R. F., Jr., Packed Tower Design and Applications, 2nd Ed., Gulf Publishing,
Houston, TX , 1994 (1st Ed. was in 1987).
9. Perry, R. H., and D. Green, Chemical Engineers Handbook, 8th Ed., McGraw-Hill, NY, to
be published in 2007.
11. Kister, H. Z., and D. R. Gill, IChemE Symp. Ser. 128, p. A109, 1992.
12. Souders, M. Jr., and G. G. Brown, Ind. Eng. Chem. 26(1), p. 98, 1934.
13. Kister, H. Z., and D. R. Gill, Predict Flood Points and Pressure Drop for Modern Random
Packings Chem. Eng. Prog., 87(2), p. 32, 1991.
16. Strigle, R. F., Jr., and F. Rukovena, Jr., Chem. Eng. Progr. 75(3), p. 86, 1979.
17. Makowiak, J., Fluiddynamik von Kolonnen mit Modernen Fullkrpern und Packungen fr
Gas/Flssigkeitssysteme, Otto Salle Verlag, Frankfurt am Main, und Verlag Sauerlnder,
Aarau, Frankfurt am Main, 1991.
19. Lockett, M. J., R. A. Victor, and J. F. Billingham, Structured Packing Flooding: Its
Measurement and Prediction, IChemE Symp. Ser. 152, p. 400, 2006.
20. Pilling, M. and Haas, Distillation Topical Conference Proceedings, p. 132, AIChE Spring
Meeting, March 10-14, New Orleans, LA, 2002.
21. McNulty, K. and R. A. Sommerfeldt, New Twist Adds Capacity to Flexipac Structured
Packings, in Distillation: Horizons for the New Millennium, Topical Conference
Proceedings, p. 89, AIChE Spring Meeting, Houston, TX, March 1999.
22. Schultes, M., and S. Chamber How to Surpass Conventional and High Capacity Structured
Packings with Raschig Super-Pak, Chem. Eng. Res. And Des., Vol. 85, No. A1, p. 118,
January 2007.
23. Olujic, Z., A. F. Seibert, B. Kaibel, H. Jansen, T. Rietfort, and E. Zich, Chem. Eng. & Proc.,
42, 55-60, 2003.
24. McNulty, K. and C. L. Hsieh, Hydraulic Performance and Efficiency of Koch Flexipac
Structured Packings, paper presented at the 1982 Annual Meeting of the AIChE, Los
Angeles, CA., Nov 14-19, 1982.
25. Koch Engineering Company Inc., Flexipac Structured Packing, Bulletin KFP-3, Wichita,
Kansas, 1989.
26. Koch-Glitsch LP, Bulletin, Flexipac Structured Packing, Bulletin KFP-5, Wichita,
Kansas, 1997.
27. Koch-Glitsch KG-TOWER - Reliability Predicting Packed Tower Pressure Capacity and
Pressure Drop, Wichita, Kansas, 4th Quarter, 2006.
28. Kister, H. Z., Distillation Troubleshooting John Wiley and Sons, Inc, NJ, 2006.
29. Cooling, M., and M. Neuman, Hyperfil Knitted Mesh Tower Packing A High efficiency
Leader for the Future, in Distillation 2005: Learning from the Past and Advancing the
Future, Topical Conference Proceedings, p. 389, AIChE Spring Meeting, Atlanta, GA, April
10 13, 2005.
FLOW PARAMETER
FIGURE 3
GPDC CHART FOR THE SAME PACKING AS CHART 10.2503,
BUT WITH A GROSSLY EXCESSIVE PACKING FACTOR
3.0
LEGEND
2.8 P curves from top to bottom represent
1.5, 1.0, 0.50, 0.25, 0.10 inches H2O/ft
2.6
2.4 DATA POINTS
CAPACITY PARAMETER
1.4
1.2
1.0
0.8
0.6
0.4
0.2
0.0
0.005 0.01 0.05 0.10 0.50 1.00 5.00
Basis: Fp = 27
Pressure drop measured in inches H2O/ft FLOW PARAMETER
Large symbols represent non-aqueous data
FIGURE 4
INCORRECT APPLICATION OF GPDC
BEYOND THE FLOOD POINT
1.5
1.4 GPDC
Vendor New Test Data
1.3
1.2
1.1
PRESSURE DROP
1
(inches H2O/ft)
0.9
NO. 3 MISUSE
0.8
0.7
0.6
0.5
0.2
0.1
0
0.50 0.60 0.70 0.80 0.90 1.00 1.10 1.20 1.30 1.40
1.40 1.40
McNulty & Hsieh
McNutly & Sommesfeldt
1.20 1.20
P,inches H2O/ft
P,inches H2O/ft
1.00 1.00
0.80 0.80
0.60 0.60
0.40 0.40
0.20 0.20
0.00 0.00
0 0.1 0.2 0.3 0.4
Cs, ft/sec
FLEXIPAC 2Y Metal Structured Packing FIGURE 5b
Pressure Drop vs. C-Factor
2
Air-Water, 10 gpm/ft , KOCH/KOCH GLITSCH Data
1.60 1.60
1.40 1.40
McNulty & Hsieh
KFP-5
1.20 1.20
P,inches H2O/ft
P,inches H2O/ft
1.00 1.00
0.80 0.80
0.60 0.60
0.40 0.40
0.20 0.20
0.00 0.00
0.1 0.2 0.3 0.4 0.5
Cs, ft/sec
APPENDIX
TABLE 1 DATA USED IN CHARTS
Test
Column
10.2502 #1 (M) Raschig Super-Ring 25 This work A1 (Ruhr Uni, Bochum) Air Water Atm 0.05 1.2 17 6.6 29
A2 (Ruhr Uni, Bochum) Air Water Atm 0.04 0.35 11 6.4 17
10.2503 #1.5 (M) Raschig Super-Ring 18 This work A1 (Ruhr Uni,, Bochum) Air Water Atm 0.02 0.28 11 6.6 20
10.2504 #2 (M) Raschig Super-Ring 15 This work A1 (Ruhr Uni, Bochum) Air Water Atm 0.05 1.7 30 9.8 39
A3 (Raschig) Air Water Atm 0.02 0.24 11 4.6 16
A1 (FRI) C6 C7 24 psia 0.09 48 12 5
A1 (FRI) iC4 nC4 100 psia 0.18 48 12 4
A1 (FRI) iC4 nC4 165 psia 0.24 48 12 4
10.2506 #3 (M) Raschig Super-Ring 11 This work A1 (Ruhr Uni, Bochum) Air Water Atm 0.02 0.81 17 6.6 32
10.2514 #2 (P) Raschig Super-Ring 15 This work A1 (Ruhr Uni, Bochum) Air Water Atm 0.02 0.23 11 6.6 20
10.6102R1 Flexipac 1Y 30 This work A4 (Koch-Glitsch) Air Water Atm 0.041 0.95 36 20
A5 (Koch) Air Water Atm 0.10, 0.29 36 2 2
10.6103 Flexipac 1.6Y 18 This work A6 (Koch-Glitsch) Air Water Atm 0.03 0.58 36 20
10.6104R1 Flexipac 2Y 15 This work A6 (Koch-Glitsch) Air Water Atm 0.03 0.49 36 20
A5 (Koch) Air Water Atm 0.067, 0.15 36 2 2
A7 (SRP) C6 C7 5 60 psia 0.04 0.15 18 10 3
10.6106R1 Flexipac 3Y 9 This work A6 (Koch-Glitsch) Air Water Atm 0.02 1.2 36 30
A5 (Koch) Air Water Atm 0.05 0.19 36 3 3
10.6108R1 Flexipac 4Y 7 This work A6 (Koch-Glitsch) Air Water Atm 0.018 0.82 36 29
10.6152 Flexipac 1 16 This work A6 (Koch-Glitsch) Air Water Atm 0.033 0.52 36 20
10.6153 Flexipac 1.6X 10 This work A6 (Koch-Glitsch) Air Water Atm 0.024 0.44 36 20
10.6154 Flexipac 2X 7 This work A6 (Koch-Glitsch) Air Water Atm 0.020 0.32 36 20
10.6156 Flexipac 3X 5 This work A6 (Koch-Glitsch) Air Water Atm 0.018 0.72 36 30
TABLE 1 DATA USED IN CHARTS
Test
Column
10.6802 Mellapak Plux 452Y 21 This work A8 (Sulzer) Chlorobenzene Ethylbenzene 100-960 mbar 0.020 0.060 39 16
10.6804 Mellapak Plus 252Y 12 This work A8 (Sulzer) Chlorobenzene Ethylbenzene 100-960 mbar 0.020 0.060 39 18
A9 (FRI) p-o Xylene 100 mmHg 0.022 48 7
A9 (FRI) C6 C7 5, 24 psia 0.041, 0.087 48 14
10.6901 Flexipac HC 700Y 68 This work A10 (Koch-Glitsch) Air Water Atm 0.015 0.66 36 33
10.6902 Flexipac HC 1Y 25 This work A4, A10 (Koch-Glitsch) Air Water Atm 0.03 0.93 36 20
10.6903 Flexipac HC 1.6Y 17 This work A11 (Koch-Glitsch) p-o Xylene 75,200 mmHg 0.022 0.35 16 10 10
A11 (FRI) p-o Xylene 75,175 mmHg 0.022 0.032 48 11.4 10
10.7104 Montz B1-250M 13 This work A12 (Montz) Air Water Atm 0.006 0.71 18
A12 (SRP) C 6 C7 2.5 60 psia 0.032 0.15 17 10 23
Data References
A12 Julius Montz, GmbH, Montz-Pack Type B1-350M, and Montz-Pak Type
B1-250M, www.montz.de/pics/service/download.htm # Type M, Hilden,
Germany, 4/11/2007.
CHART 10.2502
#1 (M) RASCHIG SUPER-RING
PRESSURE DROP
3.0
LEGEND
2.8 P curves from top to bottom represent
1.5, 1.0, 0.50, 0.25, 0.10 inches H2O/ft
2.6
1.4
1.2
1.0
0.8
0.6
0.4
0.2
0.0
0.005 0.01 0.05 0.10 0.50 1.00 5.00
Basis: Fp = 25
Pressure drop measured in inches H2O/ft FLOW PARAMETER
Large symbols represent non-aqueous data
CHART 10.2503
#1.5 (M) RASCHIG SUPER-RING
PRESSURE DROP
3.0
LEGEND
2.8 P curves from top to bottom represent
1.5, 1.0, 0.50, 0.25, 0.10 inches H2O/ft
2.6
1.4
1.2
1.0
0.8
0.6
0.4
0.2
0.0
0.005 0.01 0.05 0.10 0.50 1.00 5.00
Basis: Fp = 18
Pressure drop measured in inches H2O/ft FLOW PARAMETER
Large symbols represent non-aqueous data
CHART 10.2504
#2 (M) RASCHIG SUPER-RING
FLOOD & PRESSURE DROP
3.0
LEGEND
2.8 P curves from top to bottom represent
1.5, 1.0, 0.50, 0.25, 0.10 inches H2O/ft
2.6
1.4
1.2
1.0
0.8
0.6
0.4
0.2
0.0
0.005 0.01 0.05 0.10 0.50 1.00 5.00
Basis: Fp = 15
Pressure drop measured in inches H2O/ft FLOW PARAMETER
Large symbols represent non-aqueous data
CHART 10.2506
#3 (M) RASCHIG SUPER-RING
PRESSURE DROP
3.0
LEGEND
2.8 P curves from top to bottom represent
1.5, 1.0, 0.50, 0.25, 0.10 inches H2O/ft
2.6
1.4
1.2
1.0
0.8
0.6
0.4
0.2
0.0
0.005 0.01 0.05 0.10 0.50 1.00 5.00
Basis: Fp = 11
Pressure drop measured in inches H2O/ft FLOW PARAMETER
Large symbols represent non-aqueous data
CHART 10.2514
#2 (P) RASCHIG SUPER-RING
PRESSURE DROP
3.0
LEGEND
2.8 P curves from top to bottom represent
1.5, 1.0, 0.50, 0.25, 0.10 inches H2O/ft
2.6
1.4
1.2
1.0
0.8
0.6
0.4
0.2
0.0
0.005 0.01 0.05 0.10 0.50 1.00 5.00
Basis: Fp = 15
Pressure drop measured in inches H2O/ft FLOW PARAMETER
Large symbols represent non-aqueous data
CHART 10.6102R1
FLEXIPAC 1Y
FLOOD & PRESSURE DROP
3.0
LEGEND
2.8 P curves from top to bottom represent
1.5, 1.0, 0.50, 0.25, 0.10 inches H2O/ft
2.6
2.4 DATA POINTS
CAPACITY PARAMETER
CHART 10.6103
FLEXIPAC 1.6Y
PRESSURE DROP
3.0
LEGEND
2.8 P curves from top to bottom represent
1.5, 1.0, 0.50, 0.25, 0.10 inches H2O/ft
2.6
2.4 DATA POINTS
CAPACITY PARAMETER
CHART 10.6106R1
FLEXIPAC 3Y
FLOOD & PRESSURE DROP
3.0
LEGEND
2.8 P curves from top to bottom represent
1.5, 1.0, 0.50, 0.25, 0.10 inches H2O/ft
2.6
2.4 DATA POINTS
CAPACITY PARAMETER
CHART 10.6152
FLEXIPAC 1X
PRESSURE DROP
3.0
LEGEND
2.8 P curves from top to bottom represent
1.5, 1.0, 0.50, 0.25, 0.10 inches H2O/ft
2.6
2.4 DATA POINTS
CAPACITY PARAMETER
CHART 10.6154
FLEXIPAC 2X
PRESSURE DROP
3.0
LEGEND
2.8 P curves from top to bottom represent
1.5, 1.0, 0.50, 0.25, 0.10 inches H2O/ft
2.6
2.4 DATA POINTS
CAPACITY PARAMETER
CHART 10.6802
MELLAPAK PLUS 452Y
FLOOD & PRESSURE DROP
3.0
LEGEND
2.8 P curves from top to bottom represent
1.5, 1.0, 0.50, 0.25, 0.10 inches H2O/ft
2.6
2.4 DATA POINTS
CAPACITY PARAMETER
CHART 10.6902
FLEXIPAC HC 1Y
PRESSURE DROP
3.0
LEGEND
2.8 P curves from top to bottom represent
1.5, 1.0, 0.50, 0.25, 0.10 inches H2O/ft
2.6
2.4 DATA POINTS
CAPACITY PARAMETER
CHART 10.6904
FLEXIPAC HC 2Y
PRESSURE DROP
3.0
LEGEND
2.8 P curves from top to bottom represent
1.5, 1.0, 0.50, 0.25, 0.10 inches H2O/ft
2.6
2.4 DATA POINTS
CAPACITY PARAMETER