CH200L Organic Chemistry Lab

Quiz 1: Lab. Safety & Techniques and Stoichiometry Seat # ________ Section: _______ /35
Test I. GENERAL INSTRUCTION: Choose the letter of your answer that best fits each question. Write the
letter on the answer sheet provided. Answers may be used multiple times. Do not put tentative answers on the
answer sheet. (20 pts.)
For nos. 1-5 For nos. 6-10 For nos. 11-15 For nos. 16-20
A Evaporating Dish Evaporation 1st Step Wash with alcohol
B Beaker Decantation 2nd Step Damp Cloth
C Graduated Cylinder Filtration 3rd Step Acid to Water
D Erlenmeyer Flask Sublimation 4th Step Labeling of Glassware
E Measuring Pipette Selective Dissolution 5th Step Read hazard labels

Identify the common glassware:

1. What glassware is used to measure and contain 5.50 mL of liquid reagent from the reagent bottle
2. What glassware is used to contain non-volatile liquids?
3. What glassware is used to contain volatile liquids?
4. What glassware is used to deliver liquids?
5. What glassware is used to make a liquid (usually volatile) disappear through heating?

What separation techniques to use based from the given mixtures? (Just give the 1st technique if 2 techniques
are needed)
6. Saline Solution 9. Naphthalene and sand 11. Dense amorphous milk curds
7. KCl and iron dusts 10. Orange pulps in orange juice in lactic acid solution
8.
12. How to operate a digital analytical balance?
13. Weigh material 15. Plug device to power source 17. Close balance doors
14. Check bubble 16. Press TARE 18.
19.
20. Safety practices in the laboratory or what to do when accidents happen:
21. to prevent spattering of hot liquid 23. organic solvent on skin 25. to prevent accidental mixing of
22. to know the risks of reagents 24. small fire reagents
 26.
27. Test II. A scientist wants to make a pineapple-scented pen-shaped candy. The pineapple scent, or
chemically known as allyl hexanoate (MW = 156.23 g/mol, density = 0.887 g/mL), is prepared by mixing
10.8 mL of hexanoic acid (MW = 116.16 g/mol; density = 0.929 g/mL) with 7.5 mL of allyl alcohol (MW =
58.08 g/mol; density = 0.854 g/mL) and subjected the mixture to boiling. A balanced chemical equation
for the reaction is provided. Remember that carbon is tetravalent and all vertices represent carbon
atoms. Write all your answers on the space provided. (15 pts., 5 pts. Each)

28.
29. Hexanoic Acid Allyl Alcohol Allyl Hexanoate
Water
30.
1. Which of the two reactants is the excess reagent? Show calculations.
2. How much (in mL) of allyl hexanoate can be produced?
3. If the reaction did not proceed to completion and only 12 mL of ally hexanoate is obtained, calculate the
percent yield.
31. Show all solutions here. Solution and answers outside the box will not be
32. Name: considered. Write all answers and encircle final answers in ink. Use back side
33. as scratch.
34.
35.
36.
37. Date: 40. Period:
38.
39.
1.) 41. 11.)
2.) 42. 12.)
3.) 43. 13.)
4.) 44. 14.)
5.) 45. 15.)
6.) 46. 16.)
7.) 47. 17.)
8.) 48. 18.)
9.) 49. 19.)
10.) 50. 20.)
51.