CRODA CHEMICALS INDIA PVT.

LTD
CARBENDAZIM 50 SC

Objective: - Formulation of Carbendazim 50 SC, using Atlox 4913 & Atlox 4894.
Recipe:-
Raw materials Function in formulation % w/w
Carbendazim Technical 98% @ 50.2% Active Ingredient 51.22
Propylene Glycol Antifreeze 8.00
Atlox 4913 Dispersing Agent 3.00
Atlox 4894 Wetting Agent 2.00
Proxel GXL Preservative 0.30
Xanthum Gum 2% dispersion Rheology modifier 6.00
Cresmer AD 09 Antifoam 0.10
Water Dispersion media 29.38
Total 100.00

Procedure for Carbendazim 50 SC formulation

SCHEMATIC DIAGRAM

Oil Phase.

Step 1a :- Water + preservative +

xanthum gum
Addition of gum under continuous
Step 1: Propylene glycol + surfactants + stirring
60 % water + Antifoam + preservative +
Technical

Homogenization & then carry out wet milling

Step 3:- milled slurry

Post milling Step 2:Add remaining (Homogenizer: Remi engineering )

water and mix until
homogeneous slurry

Conditions:
All process was carried out under 25-300 C temperature.

Non-warranty
Information in this leaflet is given in good faith. Croda Chemicals Europe Ltd and its associate companies
cannot assume any liability expressed or implied in the presentation of this data, nor should information
contained herein be construed as granting license to practice any methods or compositions of matter
covered by British or other Patents.
 CRODA CHEMICALS INDIA PVT. LTD
PROCEDURE

Xanthum gum 2% dispersion: - take required quantity of water in beaker, add part Proxel GXL
into it under continuous stirring followed by slow addition of Xanthum gum (Keltrol CGT). Continue
stirring until homogeneous dispersion is formed.

Components Wt. in g
Xanthum gum (Keltrol CGT) 2
Proxel GXL 1
Water 97
Total 100

Preparation of mill base & bead milling :-

Take Propylene glycol, Atlox 4913, Atlox 4894 mix well until homogeneous solution is formed. Add
water, Proxel GXL, defoamer and stir well until homogeneous dispersion is formed. Finally add
technical slowly under continuous stirring. Continue to obtain homogeneous dispersion.

Mill the slurry through bead mill until required particle size is achieved.

Components %w/w
PG 8.00
Atlox 4913 3.00
Atlox 4894 2.00
Water 29.03
Proxel GXL 0.15
Cresmer AD 09 0.06
Carbendazim technical 51.22
Total 93.46

Note: - Batch size of the mill base should be designed based on the capacity of the mill & expected
minimum output.

Final Formulation:-
Take the milled slurry into one beaker; based on the output from the mill calculate required amount
of other ingredients. Add Defoamer, water & finally add xanthum gum (2% dispersion) under
continuous stirring to get desired viscosity. Continue stirring for about 45 min to obtain
homogeneous formulation.

Component %W/W
Milled slurry 93.46
Cresmer AD 09 0.04
Water 0.50
Xanthum Gum 2% dispersion 6.00
Total 100.00

* Mill output is considered as 100 % in this case.

Non-warranty
Information in this leaflet is given in good faith. Croda Chemicals Europe Ltd and its associate companies
cannot assume any liability expressed or implied in the presentation of this data, nor should information
contained herein be construed as granting license to practice any methods or compositions of matter
covered by British or other Patents.